N/A Matrix : Derivative Certificate Harvest/Lot ID: J27V01 ...
N/A Matrix: Derivative Certificate · Daily 500mg N/A Matrix : Derivative Certificate of Analysis...
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This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report is an Kaycha Labs certification. The results relate only to the material or product analyzed. Test results are confidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batch material may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter, ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) and Limit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured by an analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholds for human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty of measurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for the pass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310. Jorge Segredo Lab Director State License # n/a ISO Accreditation # 97164 ___________________ Signature 06/04/2020 ___________________ Signed On 4131 SW 47th AVENUE SUITE 1408 Kaycha Labs Daily 500mg N/A Matrix: Derivative Certificate of Analysis Sample:DA00528007-004 Harvest/Lot ID: 1 Seed to Sale #n/a Batch Date :N/A Batch#: 1 Sample Size Received: 120 ml Retail Product Size: 120 ml Ordered : 05/27/20 Sampled : 05/27/20 Completed: 06/04/20 Expires: 06/04/21 Sampling Method: SOP Client Method Jun 04, 2020 | Organic scientific llc 7300 n waterway dr. Miami Fl, Usa 33143 PASSED Page 1 of 4 PRODUCT IMAGE SAFETY RESULTS MISC. Pesticides PASSED Heavy Metals PASSED Microbials PASSED Mycotoxins PASSED Residuals Solvents PASSED Filth PASSED Water Activity NOT TESTED Moisture NOT TESTED Terpenes NOT TESTED CANNABINOID RESULTS Total THC 0.021% THC/Container :24.192 mg Total CBD 0.349% CBD/Container :402.048 mg Total Cannabinoids 0.414% Total Cannabinoids/Container :476.928 mg CBC CBGA CBG THCV D8-THC CBDV CBN CBDA CBD D9-THC THCA 0.011% ND 0.022% ND ND ND 0.011% ND 0.349% 0.021% ND 0.110 mg/g ND 0.220 mg/g ND ND ND 0.110 mg/g ND 3.490 mg/g 0.210 mg/g ND LOD 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.0001 0.0001 0.001 % % % % % % % % % % % Cannabinoid Profile Test Analyzed by Weight Extraction date : Extracted By : 450 3.0863g 05/28/20 12:05:28 965 Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 05/29/20 13:17:05 Analytical Batch -DA012723POT Instrument Used : DA-LC-001 Batch Date : 05/28/20 08:28:55 Reagent Dilution Consums. ID 032320.27 40 280678841 052120.R19 918C4-918J 052120.R18 914C4-914AK 929C6-929H Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 for sample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L). Filth PASSED Analyzed By Weight Extraction date LOD(ppm) Extracted By 457 1g NA NA Analysis Method -SOP.T.40.013 Batch Date : 05/28/20 07:33:21 Analytical Batch -DA012716FIL Reviewed On - 05/28/20 15:30:22 Instrument Used : Filth/Foreign Material Microscope This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing waste and by-products. An SH-2B/T Stereo Microscope is use for inspection.
Transcript of N/A Matrix: Derivative Certificate · Daily 500mg N/A Matrix : Derivative Certificate of Analysis...
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
06/04/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha LabsDaily 500mg
N/AMatrix: Derivative
Certificateof Analysis
Sample:DA00528007-004Harvest/Lot ID: 1Seed to Sale #n/a
Batch Date :N/ABatch#: 1
Sample Size Received: 120 mlRetail Product Size: 120 ml
Ordered : 05/27/20Sampled : 05/27/20
Completed: 06/04/20 Expires: 06/04/21Sampling Method: SOP Client Method
Jun 04, 2020 | Organic scientific llc7300 n waterway dr. MiamiFl, Usa 33143
PASSEDPage 1 of 4
PRODUCT IMAGE SAFETY RESULTS MISC.
PesticidesPASSED
Heavy MetalsPASSED
MicrobialsPASSED
MycotoxinsPASSED
ResidualsSolventsPASSED
FilthPASSED
Water ActivityNOT TESTED
MoistureNOT TESTED
TerpenesNOT TESTED
CANNABINOID RESULTS
Total THC
0.021%THC/Container :24.192 mg
Total CBD
0.349%CBD/Container :402.048 mg
Total Cannabinoids
0.414%Total Cannabinoids/Container:476.928 mg
CBC CBGA CBG THCV D8-THC CBDV CBN CBDA CBD D9-THC THCA
0.011% ND 0.022% ND ND ND 0.011% ND 0.349% 0.021% ND
0.110mg/g ND
0.220mg/g ND ND ND
0.110mg/g ND
3.490mg/g
0.210mg/g ND
LOD 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.0001 0.0001 0.001
% % % % % % % % % % %
Cannabinoid Profile TestAnalyzed by Weight Extraction date : Extracted By :450 3.0863g 05/28/20 12:05:28 965
Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 05/29/20 13:17:05Analytical Batch -DA012723POT Instrument Used : DA-LC-001 Batch Date : 05/28/20 08:28:55
Reagent Dilution Consums. ID
032320.27 40 280678841052120.R19 918C4-918J052120.R18 914C4-914AK
929C6-929HFull spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 forsample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).
Filth PASSED
Analyzed By Weight Extraction date LOD(ppm) Extracted By457 1g NA NA
Analysis Method -SOP.T.40.013 Batch Date : 05/28/20 07:33:21Analytical Batch -DA012716FIL Reviewed On - 05/28/20 15:30:22Instrument Used : Filth/Foreign Material Microscope
This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing wasteand by-products. An SH-2B/T Stereo Microscope is use for inspection.
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
06/04/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha LabsDaily 500mg
N/AMatrix : Derivative
Certificate of Analysis PASSEDOrganic scientific llc
7300 n waterway dr. MiamiFl, Usa 33143Telephone: (786) 226-5002Email: [email protected]
Sample : DA00528007-004Harvest/LOT ID: 1Batch# : 1Sampled : 05/27/20Ordered : 05/27/20
Sample Size Received : 120 mlCompleted : 06/04/20Expires: 06/04/21Sample Method : SOP Client Method
Page 2 of 4
Pesticides PASSEDPesticides LOD Units Action Level ResultABAMECTIN B1A 0.01 ppm 0.3 NDACEPHATE 0.01 ppm 3 NDACEQUINOCYL 0.01 ppm 2 NDACETAMIPRID 0.01 ppm 3 NDALDICARB 0.01 ppm 0.1 NDAZOXYSTROBIN 0.01 ppm 3 NDBIFENAZATE 0.01 ppm 3 NDBIFENTHRIN 0.01 ppm 0.5 NDBOSCALID 0.01 PPM 3 NDCARBARYL 0.05 ppm 0.5 NDCARBOFURAN 0.01 ppm 0.1 NDCHLORANTRANILIPROLE 0.1 ppm 3 NDCHLORMEQUAT CHLORIDE 0.05 ppm 3 NDCHLORPYRIFOS 0.01 ppm 0.1 NDCLOFENTEZINE 0.02 ppm 0.5 NDCOUMAPHOS 0.01 ppm 0.1 NDDAMINOZIDE 0.01 ppm 0.1 NDDIAZANON 0.01 ppm 0.2 NDDICHLORVOS 0.01 ppm 0.1 NDDIMETHOATE 0.01 ppm 0.1 NDDIMETHOMORPH 0.02 ppm 3 NDETHOPROPHOS 0.01 ppm 0.1 NDETOFENPROX 0.01 ppm 0.1 NDETOXAZOLE 0.01 ppm 1.5 NDFENHEXAMID 0.01 ppm 3 NDFENOXYCARB 0.01 ppm 0.1 NDFENPYROXIMATE 0.01 ppm 2 NDFIPRONIL 0.01 ppm 0.1 NDFLONICAMID 0.01 ppm 2 NDFLUDIOXONIL 0.01 ppm 3 NDHEXYTHIAZOX 0.01 ppm 2 NDIMAZALIL 0.01 ppm 0.1 NDIMIDACLOPRID 0.04 ppm 3 NDKRESOXIM-METHYL 0.01 ppm 1 NDMALATHION 0.02 ppm 2 NDMETALAXYL 0.01 ppm 3 NDMETHIOCARB 0.01 ppm 0.1 NDMETHOMYL 0.01 ppm 0.1 NDMETHYL PARATHION 0.005 ppm 0.1 NDMEVINPHOS 0.01 ppm 0.1 NDMYCLOBUTANIL 0.01 ppm 3 ND
Pesticides LOD Units Action Level ResultNALED 0.025 ppm 0.5 NDOXAMYL 0.05 ppm 0.5 NDPACLOBUTRAZOL 0.01 ppm 0.1 NDPHOSMET 0.01 ppm 0.2 NDPIPERONYL BUTOXIDE 0.1 ppm 3 NDPRALLETHRIN 0.01 ppm 0.4 NDPROPICONAZOLE 0.01 ppm 1 NDPROPOXUR 0.01 ppm 0.1 NDPYRETHRINS 0.05 ppm 1 NDPYRIDABEN 0.02 ppm 3 NDSPINETORAM 0.02 PPM 3 NDSPIROMESIFEN 0.01 ppm 3 NDSPIROTETRAMAT 0.01 ppm 3 NDSPIROXAMINE 0.01 ppm 0.1 NDTEBUCONAZOLE 0.01 ppm 1 NDTHIACLOPRID 0.01 ppm 0.1 NDTHIAMETHOXAM 0.05 ppm 1 NDTOTAL CONTAMINANT LOAD(PESTICIDES)
0 PPM 20 ND
TOTAL PERMETHRIN 0.01 ppm 1 NDTOTAL SPINOSAD 0.01 ppm 3 NDTRIFLOXYSTROBIN 0.01 ppm 3 ND
Pesticides PASSED
Analyzed by Weight Extraction date Extracted By585 0.9796g 05/28/20 02:05:24 1082
Analysis Method - SOP.T.30.065, SOP.T.40.065 ,SOP.T.30.065, SOP.T40.070Analytical Batch - DA012736PES Reviewed On- 05/28/20 15:30:22Instrument Used : DA-LCMS-001_DER (PES)Batch Date : 05/28/20 09:52:09
Reagent Dilution Consums. ID041420.07 10 280678841052620.R16 76262-590052620.R17052620.R20041720.03
Pesticide screen is performed using LC-MS which can screen down to below single digit ppb concentrationsfor regulated Pesticides. Currently we analyze for 67 Pesticides. (Method: SOP.T.30.060 Sample Preparationfor Pesticides Analysis via LCMSMS and SOP.T40.065 Procedure for Pesticide Quantification Using LCMS). *Volatile Pesticide screening is performed using GC-MS which can screen down to below single digit ppbconcentrations for regulated Pesticides. Analytes marked with an asterisk were tested using GC-MS.
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
06/04/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha LabsDaily 500mg
N/AMatrix : Derivative
Certificate of Analysis PASSEDOrganic scientific llc
7300 n waterway dr. MiamiFl, Usa 33143Telephone: (786) 226-5002Email: [email protected]
Sample : DA00528007-004Harvest/LOT ID: 1Batch# : 1Sampled : 05/27/20Ordered : 05/27/20
Sample Size Received : 120 mlCompleted : 06/04/20Expires: 06/04/21Sample Method : SOP Client Method
Page 3 of 4
Residual Solvents PASSED
Solvent LOD Units ActionLevel(PPM)
Pass/Fail Result
1,1-DICHLOROETHENE 0.8 ppm 8 PASS ND
1,2-DICHLOROETHANE 0.2 ppm 2 PASS ND
2-PROPANOL 50 ppm 500 PASS ND
ACETONE 75 ppm 750 PASS ND
ACETONITRILE 6 ppm 60 PASS ND
BENZENE 0.1 ppm 1 PASS ND
BUTANES (N-BUTANE) 500 ppm 5000 PASS ND
CHLOROFORM 0.2 ppm 2 PASS ND
DICHLOROMETHANE 12.5 ppm 125 PASS ND
ETHANOL 500 ppm 5000 PASS ND
ETHYL ACETATE 40 ppm 400 PASS ND
ETHYL ETHER 50 ppm 500 PASS ND
ETHYLENE OXIDE 0.5 ppm 5 PASS ND
HEPTANE 500 ppm 5000 PASS ND
METHANOL 25 ppm 250 PASS ND
N-HEXANE 25 ppm 250 PASS ND
PENTANES (N-PENTANE) 75 ppm 750 PASS ND
PROPANE 500 ppm 5000 PASS ND
TOLUENE 15 ppm 150 PASS ND
TOTAL XYLENES 15 ppm 150 PASS ND
TRICHLOROETHYLENE 2.5 ppm 25 PASS ND
Residual Solvents PASSED
Analyzed by Weight Extraction date Extracted By850 0.0240g 05/29/20 05:05:14 850
Analysis Method -SOP.T.40.032Analytical Batch -DA012782SOL Reviewed On - 06/04/20 13:37:54Instrument Used : DA-GCMS-002Batch Date : 05/29/20 15:05:44
Reagent Dilution Consums. ID
1 00279984161291-124154107
Residual solvents screening is performed using GC-MS which can detect belowsingle digit ppm concentrations. Currently we analyze for 21 Residualsolvents.(Method: SOP.T.30.032 Residual Solvents Analysis via GC-MS).
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
06/04/2020
___________________Signed On
4131 SW 47th AVENUE SUITE 1408
Kaycha LabsDaily 500mg
N/AMatrix : Derivative
Certificate of Analysis PASSEDOrganic scientific llc
7300 n waterway dr. MiamiFl, Usa 33143Telephone: (786) 226-5002Email: [email protected]
Sample : DA00528007-004Harvest/LOT ID: 1Batch# : 1Sampled : 05/27/20Ordered : 05/27/20
Sample Size Received : 120 mlCompleted : 06/04/20Expires: 06/04/21Sample Method : SOP Client Method
Page 4 of 4
Mycotoxins PASSED
Analyte LOD Units Result Action Level (PPM)AFLATOXIN G2 0.002 ppm ND 0.02AFLATOXIN G1 0.002 ppm ND 0.02AFLATOXIN B2 0.002 ppm ND 0.02AFLATOXIN B1 0.002 ppm ND 0.02OCHRATOXIN A+ 0.002 ppm ND 0.02
Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch -DA012737MYC | Reviewed On - 06/03/20 07:34:49Instrument Used : DA-LCMS-001_DER (MYC)Batch Date : 05/28/20 09:53:28
Analyzed by Weight Extraction date Extracted By585 1g NA NA
Aflatoxins B1, B2, G1, G2, and Ochratoxins A testing using LC-MS. (Method: SOP.T.30.065 forSample Preparation and SOP.T40.065 Procedure for Mycotoxins Quantification Using LCMS. LOQ 1.0ppb). Aflatoxin B1, B2, G1, and G2 must individually be <20ug/Kg. Ochratoxins must be <20µg/Kg.
Microbials PASSED
Analyte ResultASPERGILLUS_FLAVUS not present in 1 gram.ASPERGILLUS_FUMIGATUS not present in 1 gram.ASPERGILLUS_NIGER not present in 1 gram.ASPERGILLUS_TERREUS not present in 1 gram.ESCHERICHIA_COLI_SHIGELLA_SPP not present in 1 gram.SALMONELLA_SPECIFIC_GENE not present in 1 gram.
Analysis Method -SOP.T.40.043 / SOP.T.40.045Analytical Batch -DA012796MIC | Reviewed On - 06/01/20 08:53:48Instrument Used : (Micro) 25-27C IncubatorBatch Date : 06/01/20 08:42:09
Analyzed by Weight Extraction date Extracted By513 1.0001g 06/01/20 09:06:41 513
Reagent Dilution Consums. ID
050520.08 4603475C
914C4-914AK
Consums. ID190611634Microbiological testing for Fungal and Bacterial Identification via Polymerase Chain Reaction (PCR)method consisting of sample DNA amplified via tandem Polymerase Chain Reaction (PCR) as acrude lysate which avoids purification. (Method SOP.T.40.043) If a pathogenic Escherichia Coli,Salmonella, Aspergillus fumigatus, Aspergillus flavus, Aspergillus niger, or Aspergillus terreus isdetected in 1g of a sample, the sample fails the microbiological-impurity testing.
Heavy Metals PASSED
Reagent Reagent Dilution Consums. ID051820.R24052920.R01030920.01052620.R01052620.R02052020.R14
052820.R02052620.R03051820.R06
100 89401-566
Metal LOD Unit Result Action Level (PPM)
ARSENIC 0.02 PPM ND 1.5CADMIUM 0.02 PPM ND 0.5LEAD 0.05 PPM 0.346 0.5MERCURY 0.02 PPM ND 3
Analyzed by Weight Extraction date Extracted By53 0.2677g 05/29/20 01:05:02 457
Analysis Method -SOP.T.40.050, SOP.T.30.052Analytical Batch -DA012779HEA | Reviewed On - 06/01/20 10:34:34Instrument Used : DA-ICPMS-002Batch Date : 05/29/20 13:18:38
Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma – MassSpectrometer) which can screen down to below single digit ppb concentrations for regulated heavymetals using Method SOP.T.30.052 Sample Preparation for Heavy Metals Analysis via ICP-MS andSOP.T.40.050 Heavy Metals Analysis via ICP-MS.
