N/A Matrix : Derivative Certificate Harvest/Lot ID: 8390 of … › wp-content › uploads › 2020...
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This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report is an Kaycha Labs certification. The results relate only to the material or product analyzed. Test results are confidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batch material may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter, ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) and Limit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured by an analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholds for human safety for consumption and/or inhalation Jorge Segredo Lab Director State License # n/a ISO Accreditation # 97164 ___________________ Signature 12/06/2019 ___________________ Signed On Kaycha Labs Full Spectrum Tincture 2000 mg N/A Matrix : Derivative Certificate of Analysis SAMPLE:DA91203008-001 Harvest/Lot ID: 8390 Seed to Sale #N/A Batch#: MDC1-5-1 Sample Size: 30 ml Ordered : 11/29/19 Sampled : 11/29/19 Completed: 12/06/19 Expires: 12/06/20 Sampling Method: SOP Client Method Dec 06, 2019 | Carmens Medicinals 111 E Las Olas Blvd Suite 1140 Fort Lauderdale FL, United States 33301 PASSED Page 1 of 5 PRODUCT IMAGE SAFETY RESULTS MISC. Pesticides PASSED Heavy Metals PASSED Microbials PASSED Mycotoxins PASSED Residuals Solvents PASSED Filth PASSED Water Activity NOT TESTED Moisture NOT TESTED Terpenes TESTED CANNABINOID RESULTS Total THC 0.153% THC/Container :45.90 mg Total CBD 6.913% CBD/Container :2075.74 mg 0.174 % ND 0.095 % ND ND 0.039 % ND ND 6.913 % ND 0.153 % 1.740 mg/g ND 0.950 mg/g ND ND 0.390 mg/g ND ND 69.130 mg/g ND 1.530 mg/g CBC CBGA CBG THCV D8-THC CBDV CBN CBDA CBD THCA D9-THC Cannabinoid Profile Test Analyst Weight Sample Prep : Extracted By : 450 3.0197g 2019-12-03 12:12:16 574 Analysis Method -SOP.T.40.020, SOP.T.30.050 Analytical Batch -DA008396POT Reagent Dilution Consums. ID 400 Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 for sample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L). Filth PASSED Analyte Weight Sample Prep : Extracted By : 584 1g 2019-12-03 03:12:03 584 Analysis Method -SOP.T.40.013 Analytical Batch -DA008408FIL This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing waste and by-products. An SH-2B/T Stereo Microscope is use for inspection.
Transcript of N/A Matrix : Derivative Certificate Harvest/Lot ID: 8390 of … › wp-content › uploads › 2020...
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
12/06/2019
___________________Signed On
Kaycha LabsFull Spectrum Tincture 2000 mg
N/AMatrix : Derivative
Certificateof Analysis
SAMPLE:DA91203008-001Harvest/Lot ID: 8390
Seed to Sale #N/ABatch#: MDC1-5-1
Sample Size: 30 mlOrdered : 11/29/19Sampled : 11/29/19
Completed: 12/06/19 Expires: 12/06/20Sampling Method: SOP Client Method
Dec 06, 2019 | CarmensMedicinals111 E Las Olas Blvd Suite 1140 Fort LauderdaleFL, United States 33301
PASSEDPage 1 of 5
PRODUCT IMAGE SAFETY RESULTS MISC.
PesticidesPASSED
Heavy MetalsPASSED
MicrobialsPASSED
MycotoxinsPASSED
ResidualsSolventsPASSED
FilthPASSED
Water ActivityNOT TESTED
MoistureNOT TESTED
TerpenesTESTED
CANNABINOID RESULTS
Total THC
0.153%THC/Container :45.90 mg
Total CBD
6.913%CBD/Container :2075.74 mg
0.174 % ND 0.095 % ND ND 0.039 % ND ND 6.913 % ND 0.153 %
1.740mg/g ND
0.950mg/g ND ND
0.390mg/g ND ND
69.130mg/g ND
1.530mg/g
CBC CBGA CBG THCV D8-THC CBDV CBN CBDA CBD THCA D9-THC
Cannabinoid Profile TestAnalyst Weight Sample Prep : Extracted By :450 3.0197g 2019-12-03 12:12:16 574
Analysis Method -SOP.T.40.020, SOP.T.30.050Analytical Batch -DA008396POT
Reagent Dilution Consums. ID
400Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method:SOP.T.30.050 for sample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1mg/L).
Filth PASSED
Analyte Weight Sample Prep : Extracted By :584 1g 2019-12-03 03:12:03 584
Analysis Method -SOP.T.40.013Analytical Batch -DA008408FIL
This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing wasteand by-products. An SH-2B/T Stereo Microscope is use for inspection.
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
12/06/2019
___________________Signed On
Kaycha LabsFull Spectrum Tincture 2000 mg
N/AMatrix : Derivative
Certificate of Analysis PASSED
Carmens Medicinals
111 E Las Olas Blvd Suite 1140 FortLauderdaleFL, United States 33301Telephone: (954) 993-8077Email: [email protected]
Sample : DA91203008-001Harvest/LOT ID: 8390
Batch# : MDC1-5-1Sample Size : 30mlOrdered : 11/29/19
Sampled : 11/29/19Completed : 12/06/19 Expires : 12/06/20Sample Method : SOP Client Method
Page 2 of 5
Terpenes TESTED
Terpenes TEST RESULT (%)
ALPHA-CEDRENE NDALPHA-HUMULENE NDALPHA-PINENE NDALPHA-TERPINENE NDBETA-MYRCENE NDBETA-PINENE NDBORNEOL NDCAMPHENE NDCAMPHOR NDCARYOPHYLLENE OXIDE NDCEDROL NDALPHA-BISABOLOL 0.073ISOPULEGOL NDCIS-NEROLIDOL ND3-CARENE NDFENCHYL ALCOHOL NDHEXAHYDROTHYMOL 0.722EUCALYPTOL 0.081ISOBORNEOL NDFARNESENE 0.109FENCHONE NDGAMMA-TERPINENE NDGERANIOL NDGERANYL ACETATE NDGUAIOL NDLIMONENE 0.037LINALOOL NDNEROL NDOCIMENE NDALPHA-PHELLANDRENE NDPULEGONE 0.029SABINENE NDSABINENE HYDRATE ND
Terpenes TEST RESULT (%)
TERPINEOL ND
TERPINOLENE ND
BETA-CARYOPHYLLENE 0.082
TRANS-NEROLIDOL ND
VALENCENE ND
Terpenes TESTED
Analyst Weight Sample Prep : Extracted By :1118 1.0118g 2019-12-03 10:12:17 1118
Analysis Method -SOP.T.40.090Analytical Batch -DA008387TER
Reagent Dilution Consums. ID
10
Terpenoid profile screening is performed using GC-MS with Liquid Injection(Gas Chromatography – Mass Spectrometer) which can screen 38 terpenesusing Method SOP.T.40.091 Terpenoid Analysis Via GC/MS.
Total 1.137
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
12/06/2019
___________________Signed On
Kaycha LabsFull Spectrum Tincture 2000 mg
N/AMatrix : Derivative
Certificate of Analysis PASSED
Carmens Medicinals
111 E Las Olas Blvd Suite 1140 FortLauderdaleFL, United States 33301Telephone: (954) 993-8077Email: [email protected]
Sample : DA91203008-001Harvest/LOT ID: 8390
Batch# : MDC1-5-1Sample Size : 30mlOrdered : 11/29/19
Sampled : 11/29/19Completed : 12/06/19 Expires : 12/06/20Sample Method : SOP Client Method
Page 3 of 5
Pesticides PASSED
Pesticides LOQ Action Level Units ResultCHLORDANE 0.010 0.1 ppm NDCAPTAN 0.100 3 ppm NDBOSCALID 0.010 3 PPM NDDIMETHOATE 0.010 0.1 ppm NDABAMECTIN B1A 0.020 0.3 ppm NDCIS-PERMETHRIN 0.050 1 ppm NDSPINETORAM 0.010 3 PPM NDACEPHATE 0.010 3 ppm NDDIMETHOMORPH 0.005 3 ppm NDETHOPROPHOS 0.010 0.1 ppm NDACEQUINOCYL 0.050 2 ppm NDACETAMIPRID 0.010 3 ppm NDETOFENPROX 0.010 0.1 ppm NDALDICARB 0.020 0.1 ppm NDETOXAZOLE 0.010 1.5 ppm NDAZOXYSTROBIN 0.010 3 ppm NDFENHEXAMID 0.010 3 ppm NDBIFENAZATE 0.010 3 ppm NDFENOXYCARB 0.010 0.1 ppm NDFENPYROXIMATE 0.010 2 ppm NDBIFENTHRIN 0.010 0.5 ppm NDCARBARYL 0.010 0.5 ppm NDFIPRONIL 0.020 0.1 ppm NDFLONICAMID 0.010 2 ppm NDCARBOFURAN 0.010 0.1 ppm NDCHLORANTRANILIPROLE 0.010 3 ppm NDFLUDIOXONIL 0.010 3 ppm NDHEXYTHIAZOX 0.010 2 ppm NDCHLORFENAPYR 0.010 0.1 ppm NDIMAZALIL 0.010 0.1 ppm NDCHLORPYRIFOS 0.010 0.1 ppm NDIMIDACLOPRID 0.010 3 ppm NDCLOFENTEZINE 0.010 0.5 ppm NDKRESOXIM-METHYL 0.010 1 ppm NDCOUMAPHOS 0.005 0.1 ppm NDMALATHION 0.010 2 ppm NDCYPERMETHRIN 0.020 1 ppm NDDAMINOZIDE 0.020 0.1 ppm NDMETALAXYL 0.010 3 ppm ND
Pesticides LOQ Action Level Units ResultDICHLORVOS 0.050 0.1 ppm NDMETHIOCARB 0.010 0.1 ppm NDMETHOMYL 0.010 0.1 ppm NDDIAZANON 0.010 0.2 ppm NDMEVINPHOS 0.010 0.1 ppm NDMYCLOBUTANIL 0.010 3 ppm NDNALED 0.010 0.5 ppm NDOXAMYL 0.010 0.5 ppm NDPACLOBUTRAZOL 0.010 0.1 ppm NDTRANS-PERMETHRIN 0.050 1 ppm NDPHOSMET 0.010 0.2 ppm NDPIPERONYL BUTOXIDE 0.010 3 ppm NDPRALLETHRIN 0.050 0.4 ppm NDPROPICONAZOLE 0.010 1 ppm NDPROPOXUR 0.010 0.1 ppm NDPYRETHRIN I 0.010 1 ppm NDPYRIDABEN 0.010 3 ppm NDSPINOSAD (SPINOSYN A) 0.010 3 ppm NDSPINOSAD (SPINOSYN D) 0.010 3 ppm NDSPIROMESIFEN 0.010 3 ppm NDSPIROTETRAMAT 0.020 3 ppm NDSPIROXAMINE 0.010 0.1 ppm NDTEBUCONAZOLE 0.010 1 ppm NDTHIACLOPRID 0.010 0.1 ppm NDTHIAMETHOXAM 0.010 1 ppm NDTRIFLOXYSTROBIN 0.010 3 ppm ND
Pesticides PASSED
Analyst Weight Sample Prep : Extracted By :585 1.0983g 2019-12-03 12:12:22 1082
Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch - DA008399PES
Reagent Dilution Consums. ID
SOP.T.30.065, SOP.T.40.065
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
12/06/2019
___________________Signed On
Kaycha LabsFull Spectrum Tincture 2000 mg
N/AMatrix : Derivative
Certificate of Analysis PASSED
Carmens Medicinals
111 E Las Olas Blvd Suite 1140 FortLauderdaleFL, United States 33301Telephone: (954) 993-8077Email: [email protected]
Sample : DA91203008-001Harvest/LOT ID: 8390
Batch# : MDC1-5-1Sample Size : 30mlOrdered : 11/29/19
Sampled : 11/29/19Completed : 12/06/19 Expires : 12/06/20Sample Method : SOP Client Method
Page 4 of 5
Residual Solvents PASSED
SOLVENT ACTION LEVEL(PPM)
PASS/FAIL RESULT
PROPANE 2100 PASS ND
BUTANES (N-BUTANE) 2000 PASS ND
ETHYLENE OXIDE 5 PASS ND
METHANOL 250 PASS ND
ETHANOL 5000 PASS ND
PENTANES (N-PENTANE) 750 PASS ND
ETHYL ETHER 500 PASS ND
ACETONE 750 PASS ND
2-PROPANOL 500 PASS ND
ACETONITRILE 60 PASS ND
DICHLOROMETHANE 125 PASS ND
N-HEXANE 250 PASS ND
ETHYL ACETATE 400 PASS ND
BENZENE 1 PASS ND
HEPTANE 500 PASS ND
TOLUENE 150 PASS ND
CHLOROFORM 2 PASS ND
1,2-DICHLOROETHANE 2 PASS ND
TRICHLOROETHYLENE 25 PASS ND
1,1-DICHLOROETHENE 8 PASS ND
TOTAL XYLENES 150 PASS ND
Residual Solvents PASSED
Analyst Weight Sample Prep : Extracted By :850 0.0263g 2019-12-03 03:12:54 850
Analysis Method -SOP.T.40.032Analytical Batch -DA008420SOL
Reagent Dilution Consums. ID
1 00276446161040-124152436
Residual solvents screening is performed using GC-MS which can detect belowsingle digit ppm concentrations. Currently we analyze for 34 Residual solvents.(Method: SOP.T.30.042 Residual Solvents Analysis via GC-MS).
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation
Jorge SegredoLab Director
State License # n/aISO Accreditation # 97164 ___________________
Signature
12/06/2019
___________________Signed On
Kaycha LabsFull Spectrum Tincture 2000 mg
N/AMatrix : Derivative
Certificate of Analysis PASSED
Carmens Medicinals
111 E Las Olas Blvd Suite 1140 FortLauderdaleFL, United States 33301Telephone: (954) 993-8077Email: [email protected]
Sample : DA91203008-001Harvest/LOT ID: 8390
Batch# : MDC1-5-1Sample Size : 30mlOrdered : 11/29/19
Sampled : 11/29/19Completed : 12/06/19 Expires : 12/06/20Sample Method : SOP Client Method
Page 5 of 5
Mycotoxins PASSED
Analyte Result Action Level (PPM)AFLATOXIN G2 NDAFLATOXIN G1 NDAFLATOXIN B2 NDAFLATOXIN B1 NDOCHRATOXIN A+ ND 0.02TOTAL AFLATOXINS ND 0.02
Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch -DA008400
Analyst Weight Sample Prep : Extracted By :585 1g NA NA
Microbials PASSED
Analyte ResultASPERGILLUS_FLAVUS not present in 1 gram.ASPERGILLUS_FUMIGATUS not present in 1 gram.ASPERGILLUS_NIGER not present in 1 gram.ASPERGILLUS_TERREUS not present in 1 gram.ESCHERICHIA_COLI_SHIGELLA_SPP not present in 1 gram.SALMONELLA_SPECIFIC_GENE not present in 1 gram.
Analysis Method -SOP.T.40.043Analytical Batch -DA008414MIC
Analyst Weight Sample Prep : Extracted By :513 1.0951g 2019-12-03 11:12:39 513
Heavy Metals PASSED
Reagent Dilution Consums. ID
112719.R03 50120219.R04112719.R01112119.R02112219.R03111419.R01052419.01
Metal Result Action Level (PPM)
ARSENIC ND 1.5CADMIUM ND 0.5LEAD 0.116 0.5MERCURY ND 3
Analyst Weight Sample Prep : Extracted By :457 0.2662g 2019-12-03 01:12:55 457
Analysis Method -SOP.T.40.050, SOP.T.30.052Analytical Batch -DA008382HEA
Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma – MassSpectrometer) which can screen down to below single digit ppb concentrations for regulated heavymetals using Method SOP.T.30.052 Sample Preparation for Heavy Metals Analysis via ICP-MS andSOP.T.40.050 Heavy Metals Analysis via ICP-MS.
