N/A Matrix: Derivative Certificate Harvest/Lot ID: 104 of ...

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This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report is an Kaycha Labs certification. The results relate only to the material or product analyzed. Test results are confidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batch material may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter, ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) and Limit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured by an analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholds for human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty of measurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for the pass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310. Jorge Segredo Lab Director State License # CMTL-0002 ISO Accreditation # 97164 ___________________ Signature 07/08/2020 ___________________ Signed On 4131 SW 47th AVENUE SUITE 1408 DAVIE, FL, 33314, USA Kaycha Labs CBG 700 N/A Matrix: Derivative Certificate of Analysis Sample:DA00623006-004 Harvest/Lot ID: 104 Seed to Sale #N/A Batch Date :N/A Batch#: 4-061620 Sample Size Received: 30 ml gram Retail Product Size: 30 gram Ordered : 06/16/20 Sampled : 06/16/20 Completed: 07/08/20 Expires: 07/08/21 Sampling Method: SOP Client Method Jul 08, 2020 | Flower Child CBD 632 W. Gunnison Ave Grand Junction , CO, 81501, USA PASSED Page 1 of 4 PRODUCT IMAGE SAFETY RESULTS MISC. Pesticides PASSED Heavy Metals PASSED Microbials PASSED Mycotoxins PASSED Residuals Solvents PASSED Filth PASSED Water Activity NOT TESTED Moisture NOT TESTED Terpenes NOT TESTED CANNABINOID RESULTS Total THC 0.012% THC/Container :3.312 mg Total CBD 0.030% CBD/Container :8.289 mg Total Cannabinoids 2.291% Total Cannabinoids/Container :632.316 mg CBC CBGA CBG THCV D8-THC CBDV CBN CBDA CBD D9-THC THCA 0.080% ND 2.167% ND ND ND ND 0.016% 0.016% 0.012% ND 0.800 mg/g ND 21.670 mg/g ND ND ND ND 0.160 mg/g 0.160 mg/g 0.120 mg/g ND LOD 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.0001 0.0001 0.001 % % % % % % % % % % % Cannabinoid Profile Test Analyzed by Weight Extraction date : Extracted By : 450 3.0225g 06/23/20 03:06:11 574 Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 06/24/20 13:02:02 Analytical Batch -DA013350POT Instrument Used : DA-LC-001 Batch Date : 06/23/20 09:32:31 Reagent Dilution Consums. ID 061220.16 400 280670723 031820.R16 918C4-918J 061820.R17 914C4-914AK 061820.R16 929C6-929H 76262-590 Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 for sample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L). Label Claim Analyte LOD Units Result CBG/CONTAINER 0.01 mg 650.099 Filth PASSED Analyzed By Weight Extraction date LOD(ppm) Extracted By 457 1g NA NA Analysis Method -SOP.T.40.013 Batch Date : 06/23/20 10:22:10 Analytical Batch -DA013362FIL Reviewed On - 06/23/20 10:30:11 Instrument Used : Filth/Foreign Material Microscope This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing waste and by-products. An SH-2B/T Stereo Microscope is use for inspection.

Transcript of N/A Matrix: Derivative Certificate Harvest/Lot ID: 104 of ...

Page 1: N/A Matrix: Derivative Certificate Harvest/Lot ID: 104 of ...

This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.

Jorge SegredoLab Director

State License # CMTL-0002ISO Accreditation # 97164 ___________________

Signature

07/08/2020

___________________Signed On

4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, USA

Kaycha LabsCBG 700

N/AMatrix: Derivative

Certificateof Analysis

Sample:DA00623006-004Harvest/Lot ID: 104

Seed to Sale #N/ABatch Date :N/A

Batch#: 4-061620Sample Size Received: 30 ml gram

Retail Product Size: 30 gramOrdered : 06/16/20Sampled : 06/16/20

Completed: 07/08/20 Expires: 07/08/21Sampling Method: SOP Client Method

Jul 08, 2020 | Flower Child CBD632 W. Gunnison AveGrand Junction , CO, 81501, USA

PASSEDPage 1 of 4

PRODUCT IMAGE SAFETY RESULTS MISC.

PesticidesPASSED

Heavy MetalsPASSED

MicrobialsPASSED

MycotoxinsPASSED

ResidualsSolventsPASSED

FilthPASSED

Water ActivityNOT TESTED

MoistureNOT TESTED

TerpenesNOT TESTED

CANNABINOID RESULTS

Total THC

0.012%THC/Container :3.312 mg

Total CBD

0.030%CBD/Container :8.289 mg

Total Cannabinoids

2.291%Total Cannabinoids/Container:632.316 mg

CBC CBGA CBG THCV D8-THC CBDV CBN CBDA CBD D9-THC THCA

0.080% ND 2.167% ND ND ND ND 0.016% 0.016% 0.012% ND

0.800mg/g ND

21.670mg/g ND ND ND ND

0.160mg/g

0.160mg/g

0.120mg/g ND

LOD 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.0001 0.0001 0.001

% % % % % % % % % % %

Cannabinoid Profile TestAnalyzed by Weight Extraction date : Extracted By :450 3.0225g 06/23/20 03:06:11 574

Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 06/24/20 13:02:02Analytical Batch -DA013350POT Instrument Used : DA-LC-001 Batch Date : 06/23/20 09:32:31

Reagent Dilution Consums. ID

061220.16 400 280670723031820.R16 918C4-918J061820.R17 914C4-914AK061820.R16 929C6-929H

76262-590Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 forsample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).

Label ClaimAnalyte LOD Units ResultCBG/CONTAINER 0.01 mg 650.099

Filth PASSED

Analyzed By Weight Extraction date LOD(ppm) Extracted By457 1g NA NA

Analysis Method -SOP.T.40.013 Batch Date : 06/23/20 10:22:10Analytical Batch -DA013362FIL Reviewed On - 06/23/20 10:30:11Instrument Used : Filth/Foreign Material Microscope

This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing wasteand by-products. An SH-2B/T Stereo Microscope is use for inspection.

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This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.

Jorge SegredoLab Director

State License # CMTL-0002ISO Accreditation # 97164 ___________________

Signature

07/08/2020

___________________Signed On

4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, USA

Kaycha LabsCBG 700

N/AMatrix : Derivative

Certificate of Analysis PASSEDFlower Child CBD

632 W. Gunnison AveGrand Junction , CO, 81501, USATelephone: (541) 324-6872Email: [email protected]

Sample : DA00623006-004Harvest/LOT ID: 104Batch# : 4-061620Sampled : 06/16/20Ordered : 06/16/20

Sample Size Received : 30 ml gramCompleted : 07/08/20Expires: 07/08/21Sample Method : SOP Client Method

Page 2 of 4

Pesticides PASSEDPesticides LOD Units Action Level ResultABAMECTIN B1A 0.01 ppm 0.3 NDACEPHATE 0.01 ppm 3 NDACEQUINOCYL 0.01 ppm 2 NDACETAMIPRID 0.01 ppm 3 NDALDICARB 0.01 ppm 0.1 NDAZOXYSTROBIN 0.01 ppm 3 NDBIFENAZATE 0.01 ppm 3 NDBIFENTHRIN 0.01 ppm 0.5 NDBOSCALID 0.01 PPM 3 NDCARBARYL 0.05 ppm 0.5 NDCARBOFURAN 0.01 ppm 0.1 NDCHLORANTRANILIPROLE 0.1 ppm 3 NDCHLORMEQUAT CHLORIDE 0.05 ppm 3 NDCHLORPYRIFOS 0.01 ppm 0.1 NDCLOFENTEZINE 0.02 ppm 0.5 NDCOUMAPHOS 0.01 ppm 0.1 NDDAMINOZIDE 0.01 ppm 0.1 NDDIAZANON 0.01 ppm 0.2 NDDICHLORVOS 0.01 ppm 0.1 NDDIMETHOATE 0.01 ppm 0.1 NDDIMETHOMORPH 0.02 ppm 3 NDETHOPROPHOS 0.01 ppm 0.1 NDETOFENPROX 0.01 ppm 0.1 NDETOXAZOLE 0.01 ppm 1.5 NDFENHEXAMID 0.01 ppm 3 NDFENOXYCARB 0.01 ppm 0.1 NDFENPYROXIMATE 0.01 ppm 2 NDFIPRONIL 0.01 ppm 0.1 NDFLONICAMID 0.01 ppm 2 NDFLUDIOXONIL 0.01 ppm 3 NDHEXYTHIAZOX 0.01 ppm 2 NDIMAZALIL 0.01 ppm 0.1 NDIMIDACLOPRID 0.04 ppm 3 NDKRESOXIM-METHYL 0.01 ppm 1 NDMALATHION 0.02 ppm 2 NDMETALAXYL 0.01 ppm 3 NDMETHIOCARB 0.01 ppm 0.1 NDMETHOMYL 0.01 ppm 0.1 NDMETHYL PARATHION 0.005 ppm 0.1 NDMEVINPHOS 0.01 ppm 0.1 NDMYCLOBUTANIL 0.01 ppm 3 NDNALED 0.025 ppm 0.5 NDOXAMYL 0.05 ppm 0.5 NDPACLOBUTRAZOL 0.01 ppm 0.1 NDPHOSMET 0.01 ppm 0.2 NDPIPERONYL BUTOXIDE 0.1 ppm 3 ND

Pesticides LOD Units Action Level ResultPRALLETHRIN 0.01 ppm 0.4 NDPROPICONAZOLE 0.01 ppm 1 NDPROPOXUR 0.01 ppm 0.1 NDPYRETHRINS 0.05 ppm 1 NDPYRIDABEN 0.02 ppm 3 NDSPINETORAM 0.02 PPM 3 NDSPIROMESIFEN 0.01 ppm 3 NDSPIROTETRAMAT 0.01 ppm 3 NDSPIROXAMINE 0.01 ppm 0.1 NDTEBUCONAZOLE 0.01 ppm 1 NDTHIACLOPRID 0.01 ppm 0.1 NDTHIAMETHOXAM 0.05 ppm 1 NDTOTAL CONTAMINANT LOAD(PESTICIDES)

0 PPM 20 ND

TOTAL PERMETHRIN 0.01 ppm 1 NDTOTAL SPINOSAD 0.01 ppm 3 NDTRIFLOXYSTROBIN 0.01 ppm 3 NDCHLORDANE * 0.01 PPM 0.1 NDPENTACHLORONITROBENZENE(PCNB) *

0.01 PPM 0.2 ND

PARATHION-METHYL * 0.01 PPM 0.1 NDCAPTAN * 0.025 PPM 3 NDCHLORFENAPYR * 0.01 PPM 0.1 NDCYFLUTHRIN * 0.01 PPM 1 NDCYPERMETHRIN * 0.01 PPM 1 ND

Pesticides PASSED

Analyzed by Weight Extraction date Extracted By585 , 1665 1.0346g 06/23/20 12:06:52 1665 , 1665

Analysis Method - SOP.T.30.065, SOP.T.40.065 ,SOP.T.30.065, SOP.T40.070Analytical Batch - DA013370PES , DA013530VOL Reviewed On- 06/23/20 10:30:11Instrument Used : DA-LCMS-001_DER (PES) , DA-GCMS-001Batch Date : 06/23/20 11:46:05

Reagent Dilution Consums. ID041420.09 10 280678841061920.R19 76262-590041720.03061620.R14062320.R20

Pesticide screen is performed using LC-MS which can screen down to below single digit ppb concentrations forregulated Pesticides. Currently we analyze for 67 Pesticides. (Method: SOP.T.30.060 Sample Preparation forPesticides Analysis via LCMSMS and SOP.T40.065 Procedure for Pesticide Quantification Using LCMS). * VolatilePesticide screening is performed using GC-MS which can screen down to below single digit ppb concentrationsfor regulated Pesticides. Analytes marked with an asterisk were tested using GC-MS.

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This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.

Jorge SegredoLab Director

State License # CMTL-0002ISO Accreditation # 97164 ___________________

Signature

07/08/2020

___________________Signed On

4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, USA

Kaycha LabsCBG 700

N/AMatrix : Derivative

Certificate of Analysis PASSEDFlower Child CBD

632 W. Gunnison AveGrand Junction , CO, 81501, USATelephone: (541) 324-6872Email: [email protected]

Sample : DA00623006-004Harvest/LOT ID: 104Batch# : 4-061620Sampled : 06/16/20Ordered : 06/16/20

Sample Size Received : 30 ml gramCompleted : 07/08/20Expires: 07/08/21Sample Method : SOP Client Method

Page 3 of 4

Residual Solvents PASSED

Solvent LOD Units ActionLevel(PPM)

Pass/Fail Result

1,1-DICHLOROETHENE 0.8 ppm 8 PASS ND

1,2-DICHLOROETHANE 0.2 ppm 2 PASS ND

2-PROPANOL 50 ppm 500 PASS ND

ACETONE 75 ppm 750 PASS ND

ACETONITRILE 6 ppm 60 PASS ND

BENZENE 0.1 ppm 1 PASS ND

BUTANES (N-BUTANE) 500 ppm 5000 PASS ND

CHLOROFORM 0.2 ppm 2 PASS ND

DICHLOROMETHANE 12.5 ppm 125 PASS ND

ETHANOL 500 ppm 5000 PASS ND

ETHYL ACETATE 40 ppm 400 PASS ND

ETHYL ETHER 50 ppm 500 PASS ND

ETHYLENE OXIDE 0.5 ppm 5 PASS ND

HEPTANE 500 ppm 5000 PASS ND

METHANOL 25 ppm 250 PASS ND

N-HEXANE 25 ppm 250 PASS ND

PENTANES (N-PENTANE) 75 ppm 750 PASS ND

PROPANE 500 ppm 5000 PASS ND

TOLUENE 15 ppm 150 PASS ND

TOTAL XYLENES 15 ppm 150 PASS ND

TRICHLOROETHYLENE 2.5 ppm 25 PASS ND

Residual Solvents PASSED

Analyzed by Weight Extraction date Extracted By850 0.0203g 06/24/20 03:06:58 850

Analysis Method -SOP.T.40.032Analytical Batch -DA013405SOL Reviewed On - 06/26/20 14:17:36Instrument Used : DA-GCMS-003Batch Date : 06/24/20 14:52:35

Reagent Dilution Consums. ID

1 H2017.07700279984161291-1

Residual solvents screening is performed using GC-MS which can detect belowsingle digit ppm concentrations. Currently we analyze for 21 Residualsolvents.(Method: SOP.T.30.032 Residual Solvents Analysis via GC-MS).

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This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.

Jorge SegredoLab Director

State License # CMTL-0002ISO Accreditation # 97164 ___________________

Signature

07/08/2020

___________________Signed On

4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, USA

Kaycha LabsCBG 700

N/AMatrix : Derivative

Certificate of Analysis PASSEDFlower Child CBD

632 W. Gunnison AveGrand Junction , CO, 81501, USATelephone: (541) 324-6872Email: [email protected]

Sample : DA00623006-004Harvest/LOT ID: 104Batch# : 4-061620Sampled : 06/16/20Ordered : 06/16/20

Sample Size Received : 30 ml gramCompleted : 07/08/20Expires: 07/08/21Sample Method : SOP Client Method

Page 4 of 4

Mycotoxins PASSED

Analyte LOD Units Result Action Level (PPM)AFLATOXIN G2 0.002 ppm ND 0.02AFLATOXIN G1 0.002 ppm ND 0.02AFLATOXIN B2 0.002 ppm ND 0.02AFLATOXIN B1 0.002 ppm ND 0.02OCHRATOXIN A+ 0.002 ppm ND 0.02

Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch -DA013372MYC | Reviewed On - 07/01/20 10:40:59Instrument Used : DA-LCMS-001_DER (MYC)Batch Date : 06/23/20 11:47:25

Analyzed by Weight Extraction date Extracted By585 1g 06/23/20 04:06:02 585

Aflatoxins B1, B2, G1, G2, and Ochratoxins A testing using LC-MS. (Method: SOP.T.30.065 forSample Preparation and SOP.T40.065 Procedure for Mycotoxins Quantification Using LCMS. LOQ 1.0ppb). Aflatoxin B1, B2, G1, and G2 must individually be <20ug/Kg. Ochratoxins must be <20µg/Kg.

Microbials PASSED

Analyte ResultASPERGILLUS_FLAVUS not present in 1 gram.ASPERGILLUS_FUMIGATUS not present in 1 gram.ASPERGILLUS_NIGER not present in 1 gram.ASPERGILLUS_TERREUS not present in 1 gram.ESCHERICHIA_COLI_SHIGELLA_SPP not present in 1 gram.SALMONELLA_SPECIFIC_GENE not present in 1 gram.

Analysis Method -SOP.T.40.043 / SOP.T.40.045Analytical Batch -DA013498MIC | Reviewed On - 06/29/20 23:07:30Instrument Used : (Micro) 25-27C IncubatorBatch Date : 06/27/20 16:33:52

Analyzed by Weight Extraction date Extracted By513 1.0158g NA NA

Reagent Dilution Consums. ID

052620.16 4603475C

914C4-914AK

Consums. ID190827060Microbiological testing for Fungal and Bacterial Identification via Polymerase Chain Reaction (PCR)method consisting of sample DNA amplified via tandem Polymerase Chain Reaction (PCR) as acrude lysate which avoids purification. (Method SOP.T.40.043) If a pathogenic Escherichia Coli,Salmonella, Aspergillus fumigatus, Aspergillus flavus, Aspergillus niger, or Aspergillus terreus isdetected in 1g of a sample, the sample fails the microbiological-impurity testing.

Heavy Metals PASSED

Reagent Reagent Dilution Consums. ID062220.R01030920.02062220.R02061220.R02062220.R04062320.R04

062320.R01062320.R02062320.R03061520.R05

100 89401-566

Metal LOD Unit Result Action Level (PPM)

ARSENIC 0.02 PPM ND 1.5CADMIUM 0.02 PPM ND 0.5LEAD 0.05 PPM ND 0.5MERCURY 0.02 PPM ND 3

Analyzed by Weight Extraction date Extracted By457 0.2673g 06/23/20 12:06:15 1022

Analysis Method -SOP.T.40.050, SOP.T.30.052Analytical Batch -DA013358HEA | Reviewed On - 06/25/20 07:50:10Instrument Used : DA-ICPMS-002Batch Date : 06/23/20 09:48:39

Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma – MassSpectrometer) which can screen down to below single digit ppb concentrations for regulated heavymetals using Method SOP.T.30.052 Sample Preparation for Heavy Metals Analysis via ICP-MS andSOP.T.40.050 Heavy Metals Analysis via ICP-MS.