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Transcript of Translate-1 Overview of Source Rocks and Oils in Indonesia (Robinson
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PROCEEDINGS mDO NESIAN PETROLEUM ASSOCIATION
Sixteenth Annual Convention, October 1987
AN OVERVIEWOF SOURCE ROCKS AND
OILS
IN INDONESIA
Kevin
M.
Robinson *
ABSTRACT
Source rocks in the hydrocarbon productive basins in
Indonesia can be classified as lacustrine, fluvio-deltaic and
marine. Lacustrine source rocks are the most productive,
and have sourced most of the oil in Central Sumatra,
some of the oil in the Sunda Basin and also possibly oil in
the West N atuna Basin. Fluvial-deltaic source rocks are
the most common and widely dispersed and have sourced
oil in the majority of foreland (back-arc) basins of Western
Indonesia. Marine source rocks probably occur in Eastern
Indonesia, bu t are poorly documented. However, they may
have sourced oil in the Salaw ati Basin and eastern Sulawesi.
Positively identified producing source rocks are all Tertiary
in age, although PrsTertiary (Permian/Jurassic) rocks are
suspected to source oil in the Bintuni and Bula (Seram)
Basins and are also a possible source in eastern Sulawesi
and t he Banggai-Sula area east of Sulawesi.
Crude oils in Indonesia can also
I
be characterized as
lacustrine, fluvio-deltaic and marine based on a range of
geochemical p arameters, including pyrolysis-gas chrom ato-
graphy on the oils asphaltene fraction and GC-MS bioma rker
data. Lacustrine oils sourced from non-marine algae are
generally low-medium gravity, waxy, low sulfur oils and
often contain'unusually high concentrations of C3O 4-methyl
steranes. Marine oils derived from marine algae are low-
medium gravity, low w ax, medium-high sulfur oils and con-
tain C27-C29 diasteranes and steran es in relatively high
concentrations compared to other oil types. Fluvio-deltaic
oils
derived from higher plant, terrestrial organic matter are
medium-high gravity, waxy, low sulfur oils. They contain
abundant higher plant resin derived C30 alkanes and low
obviously dependent on the original o
source rock.
The main objectives of this paper are
1)
Categorise the source rocks of the
producing basins of Indonesia int o
ine algal), fluvio-deltaic (terrestrial)
ine algal).
2) Describe the general geochemical ch
different source rock types.
3) Develop a scheme to classify Indone
rine, fluvio-deltaic and marine bas
chemical analyses.
SCOPE
This paper a ttemp ts to cover all the
producing basins of Indonesia (Fig.
1
source rocks within the basins is prima
ously published data and
on
experience
However, source rocks within some
unknown, postulated or unconfirmed by
rock correlation studies. The oil classif
detailed geochemical data
on
one .hu
samples covering all the major hydr
basins of Indones ia (Fig. 1).
SOURCE ROCKS
The major source rocks or suspec
the hydrocarbon productive basins in I
in Table
1
and discussed below by de
ment.
© IPA, 2006 - 16th Annual Convention Proceedings, 1987Disc Contents
Contents
Search
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9
where in Indonesia, particularly in the foreland (back-arc)
basins of Western Indonesia, where rifting occurred in the
Early Tertiary behind a volcanic island arc system.
The deep lacustrine shales of Central Sumatra were de-
posited in subsiding basins, under tropical climatic condit-
ions. The lake had no annual turnover, resulting in anoxic
bottom waters, which favoured preservation of organic mat-
ter rich in non-marine algae (Fig. 3;Williams e tal , 1985).
In shallow rift basins, where subsidence was only equal to
the rate of deposition, humic rich lacustrine shales and
coals wiU have formed instead (Central Sumatra Coal zone,
Table
1).
Deep lacustrine shales are some
of
the most oils'product-
ive source rocks in the world. In Central Sumatra they ac-
coun t f or over half of Indonesia's o il reserves (Woodside,
1984). Immature, lacustrine shales typically contain be-
tween 1.0 to 10.0 total organic carbon and
50
to 100
oil prone, fluorescent non-marine algal derived amorphous
kerogen. The pyrofysis yield (Sl+S2) s variable ranging
from 4.0 to 75.0 mg hydrocarbons/gm rock, but is often
very high. Hydrogen indicies are typically in the 400 o
900 range, wit h elem ental kerogen hydrogen/carbon rat-
ios usually greater tha n 1.4 (Table 2). Specific non mar-
ine algae such as Botrycoccus braunii or the non-marine
planktonic algae
Pediastium
spp can sometimes be ident-
ified in the samples, while inp ut from Botryococcus and
dinoflagellates, can be inferred from GC-MS biomarker
data (Wolf et aL 1986; Brassel et al., 1986,Seifert and
Moldowan, 1980).
Fluvio-DeltaicSource Rocks
Fluvio-deltaic source rocks containing terrestrial
de-
rived kerogen are the m ajor source rocks of m edium gra vity,
waxy crude
oils
in many of the foreland basins of Indo-
nesia. In South Sumatra and N.W. Java (Sunda, Ardjuna,
Jatibarang) Basin, Oligocene Talang Akar coals and shales
have been identified as a major source of the oil, while in
the Malacca Straits of Central Sumatra, Sihapas coals have
generated some of the oil (Table 1 .
In the East Java sea, Oligocene Kudjung I11 coals and
shales and in the Barito Basin, Eocene Tanjung coals and
shales are speculated to be the source of the oil (Tabb
1).
Although neither of these co rrelations are proved in the
well documented geochemically (Com
1978; Durand and Oudin, 1979; Hof
Oudin and Picard,
1982;
Schoell
et
a
aL 1985). The major source rocks be
Miocene Balikpapan Group. It represen
progradation which has continued,
interruptions, through to the present d
card,
1982).
The sediments were depos
flowing river system into a subsid
north-south axis. A full suite of facie
sedimentation were deposited (Fig. 4).
tent is relatively high throughout the
(often
>2. ),
but the best source
delta plain where coals tend to be
5, Thompson,
1985).
Generation of hydrocarbons within
largely controlled by maturity, as thick
rich source rocks are present throughou
basin. The top of the oil window in th
depending on temperature gradient, b
about 2800 - 3000 meters (Schoell e
and Picard
1
982) have demonstrated
may also be important in the hydroc
and type (oil or gas) within the Kutei B
the
oil
window is completely within the
generated oil cannot be expelled and i
s i tu gas. The Kutei Basin hydrocarbon
may also be applicable in the Tarakan
men tation occurred along similar lines.
Fluvio-deltaic coal and shale source r
large volumes of oil in Indonesia and ac
production of hydrocarbons in the A
Basins. Fluvio-de ltaic shale source rock
2.0-10.0 tota l organic carbon with
6.0 to 20.0 mg hydro carbons/gm rock
tain 40.0 o
80.0
total organic carbon
rolysis yields of 150-300 g hydroca
ble 2).
Fluvio-deltaic coals and shales gen
higher plant terrestrially derived organi
predominantly of vitrinite with seco
cutinite and resinite. The total amount
exinitic kerogen is usually in the 10-3
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rocks usually have high pristane/phytane. ratios e 3 . 0 ) due
to deposition in an oxik environment. They
also
have relat-
ively high co ncen trations of waxy n-paraffins and
C30
cyclic alkanes (identifiable b y GC-MS) derived from higher
plants.
Marine Source R ocks
Marine algal rich source rocks are the m ajor source of oil
in the world. But in Indonesia none have been positively
identified in the literature. However, based on crude
oil
characterization a marine carbonate or calcareous shale
source is suspected in the Sala wati Basin of Irian Jaya (Pho a
and Samuel, 198 6; Hughes, 198 4) and in eastern Sulawesi
(Table
1).
Deposition of the source rock would have
occurred under anoxic conditions in a restricted marine
basin. In Salawati a likely source is Early Miocene Klamo-
gun
carbonates and shales (Fig. 6), while in eastern Sula-
wesi Early Miocene shales and carbonates are a possible
source or alternatively Jurassic m arine shales and carb-
onates.
Immature, marine source rocks capable
of
generating
oils in the Salawati Basin and Sulawesi area would typical-
ly be expected to contain 0.5 to 5.0 TOC, moderate to
high
pyrolysis yie lds (2.0-30.0 mg hydrocarbon s/gm rock)
and an orga nic facies comprised mainly of oil prone , mar-
ine, algal derived amorpho us kerogen. Pyrolysis hydrogen
indicies should be
in
the 300-600 range and kerogen ele-
mental hydrogenlcarbon ratios
>
1.2 (Table 2).
Re-T ertiav Source Rocks
All the Indonesian source rocks positively identified
and correlated t o oil accumulations in the published liter-
ature are T ertiaty in age. However, pote ntia l Pre-Tertiary
source rocks have been identified
in
Eastern Indonesia
(Chevallier and Bordenave, 1986) and are related to pre-
break up
of
the Australian Plate
in
the Mid-Jurassic (Peck
and Soulhol, 1986). In the Bintuni Basin
of
Irian Jaya
two PrsTertiary sourced
oil
types possibly exist (Chev-
allier and Bordenave, 1986) The major source of most
of these oils is thought to be Late to Early Permian Aifat
shales with Jurassic Tipuma shales or possibly U pper Permian
Ainim coals acting as a source for the other
oil
type
(Wiriagar oiI).All of the source rocks in theBintu ni Basin are
suspected to contain a predominantly terrestrial organic
ses such as API Gravity, Weight Sulphu
ography, plus, more detailed analyses s
topes, Pyrolysis-GC
on
the oils asphalte
Chromatography-Mass Spectrometry (G
analysis on the saturate fraction of the
o
ics listed are
for oils
generated at norm
levels (Ro 0.5 - 1.0 ) and unaltered
as thermal o r biological degradation o r w
Bulk Data
Bulk Data such as API gravity, we
gasoline range analysis and whole oil/s
chromatography give useful indicators
of an oil, but are not detailed enough
ify its gen etic origin.
Algal sourced oils, marine or no
have low-medium API gravities (20-35O)
tane ratios less than 3.0. Initial differ
marine algal oil from a marine algal
oil
based on sulphur conten t and wax c
oils are typically high wax (C31/C19
(< 0.2 wt ); while marine oils are low
C19), high sulphur >
0.2
wt ). Flu
oils usually are medium -high API grav
sulphur high wax crude
oils
(Table 3). T
have high pristanelphytane ratios 3.0
of the source rock in a n oxic enviro
McKirdy, 1975).
The
n-alkane distribution
of
oils (F
useful in distinguishing different
oil
is far from definitive. Lacustrine
oils
t
modal to broad n-alkane distribution d
C19 and C23-C33 n-alkanes from
(Gelpi eta l,1 97 0; Mol dom eta l., 1985)
tanelnC17 ratios. Marine
oils
usually
concentration of higher molecular wei
wax content) and Pristane/nC17 ratios
taic (terrestrial) oils usually show a broad
ion or a predominance
of
waxy (C2
Pristane/nC17 ratios
> 1.0.
Carbon Isotopes
Carbon isotopes
on
whole
oil,
satu
other fractions of the crude
oil
have
entiate marine oils
from terrestrial
oil
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100
and to some extent experimental technique. The idea
behind the analysis, is th at asphaltene molecules are small
kerogen molecules and representative of the original kero-
gen in the source rock (Pelet
e t
aL, 1986). Pyrolysis-GC of
the asphaltenes can then be used to identify the original
kerogen type of the oil’s source rock, based on the general
distribution of hydrocarbons on the pyrogram. This can
then be used to characterize the
oils
into different oil
types (Fig.
8).
Also the relative n-octene, m+p xylene and
phenol content of the oil’s asphaltenes can be quantified
and plotted on a Ternary diagram. (Fig. 9, modified after
Larter, 1985) to determine oil type and the kerogen type
of the source rock. Th e pyrolysis-GC on the oil’s asphal-
te ni s is performed at 550OC.
A
typical lacustrine
oil
pyrogram (Fig. 8) shows well
developed alkenes/alkanes doublets from C5-C35,with part-
icularly high concentra tions of C15-C30 n-alkenes/n-al-
kenes derived from non-marine algae. Characteristicly
aromatics and phenolic compounds are virtually absent
from the pyrogram.
A
typical marine
oil
asphaltene frac-
tion pyrogram shows a decreasing concentration of
n-al-
keneln-alkane doublets with higher molecular weight and
moderate concentrations of aromatics and phenols.
A
flu-
vio-deltatic oil shows a broad n-alkene/n-alkane distribution
and contains the highest concentration of aromatics and
phenols out of all the
oils.
Prist-l-ene also tends t o be high
in
fluvio-deltaic
oils.
A
plot of the
oil’s
n-octene, m+p xylene and phenol
content (Fig. 9) can clearly distinguish lacustrine oils from
fluvio-deltaic oils. But marine oils, probably due to lack of
data, cannot be distinguished from lacustrine oils. Oils pre-
sumed to be from lacustrine sources in the West Natuna
Basin and some of the oils
in
the Sunda Basin plot away
from the deep lacustrine oils of Central Sumatra. This may
be due to deposition of the
oils’
source rock in a different
lacustrine depositonal environment than that proposed
for Central Sumatra. Possibly it was shallower and/or more
saline?
GC-MS
Biornurker Data
Lacustrine, marine and fluvio-deltaic
oils
in Indonesia
can be distinguished based on Triterpane (m/z 191) and
Sterane content (m/z 217). Other biomarkers can also be
used such as Bicyclics (m/z 123), Isoprenoids (m/z 183),
oils in
Indonesia te nd to have simple
ions containing only pentacyclic 17dh
C35 plus moretanes and little else. The
is maturity and organic facies influen
than 1.5 and Tricyclic Terpanes (not sh
centrations or absent.
Marine
oils
also have relatively sim
retane distributions, but
in
Indonesia
concentrations of C3
1
-C35 hopanes..
to deposition of the source rock in an
environment, with high bacterial acti
tend to range from 3.0 to 1.0. In Ind
is often in relatively high concentratio
derived oils (Phoa and Samuel, 1986).
be due to transportation of resistant
into the marine basin and not indicat
source for the
oil.
Noticeable other
compounds, commonly found in ass
oleanane, are absent or in very low con
oils also tend to have relatively high
tricyclic terpanes.
Fluvio-deltaic oils have very character
tributions with high concentrations of
resin derived cyclic alkanes and the C
oleanane.
This
is in addition t o th e norm
and m oretanes. The C30 derived comp
eristic peaks on the m/z 19 1, 163, 17
mass ion scans (Fig. 11). Tm /Ts ratios
rived lndonesian oils tend to be relati
from 6.0 to
1
O
Steranes mfz 21
7
Steranes relative to hopanes tend to
trations in non-marine oils, whether th
fluvial-deltaic in origin (Table 3). Ty
hopane ratios are <0.2 in non-marin
marine
oils
(Moldowan
etal.,
1985). D
centration of steranes, it can be diffi
sterane (m/z 217) scans in non-marine
column of the GC-MS is overloaded .
Deep lacustrine
oils
usually contain
C27-C29 steranes and diasteranes (Fi
low c oncentrations, and usually have a
centration of C27 and C29 steranes (
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oils around the world. The Salawati Basin oils show similar
Triterpane and Sterane distributions to oils in the Mara-
caibo Basin of Venezuela (Fig. 14). These oils are sourced
from the Cretaceous La Luna Formation which is an or-
ganic rich carbonate (Talukdar etal., 1986). This would
suggest a similar type of source rock may have generated
at least so me, of the Salaw ati Basin
oils
(klamogun carb-
onates and shale?).
Fluvio-deltaic oils have a very characteristic m/z 217
Scan usually containing only C29 steranes and diasteranes
(Fig. 12). The dominant compounds on the scan are C30
resin derived cyclic alkanes, which are also present on the
m/z 191 triterpane scan. A comparison of triterpane and
sterane distributions (Figs. 1 5 and 16) of fluvio-deltaic
oils from South Sumatra, Kutei and Tarakan Basins shows
little variation between them, suggesting the organic facies
and original higher plant input is similar in all these basins.
A plot of C27-C29 sterane composition (Fig. 17) can dif-
ferentiate lacustrine/marine oils from fluvio-deltaic oils,
but cannot seperate lacustrine and marine oils from each
other.
CONCLUSIONS
1) The sou rce rocks of Indonesia can broadly be classi-
fied into lacustrine (non-marine algal), marine (marine
algal)
and fluvio-deltaic (terrestrial). Althou gh signifi-
cantly more oil/source rock correlation work needs to
be done or published to confirm the source rocks of
many Indonesian oils.
2) The identified source rocks are of Tertiary age, although
Pre-Tertiary source rocks are probably generating oil
in some parts of Eastern Icdonesia.
3)
Crude oils can be characterized as lacustrine, marine
or
fluvio-deltaic sourced oils based on a combination of
geochemical data. This includes standard bulk data,
Carbon Isotopes, Pyrolysis-GC of Asphaltenes and GC-
MS biomarker analysis. Lacustrine oils need further
work to subdivide deep, fresh water lacustrine oils from
shallow lsaline lacustrine oils.
4) Suspected Pre-Tertiary sourced oils should be analysed
and classified to see what type of
oils
they are and if
they show any differences, (particularly in biomarker
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TABLE 1
SOURCE ROCKS OF
INDONESIA
HYDROCARBON BASIN* MAJOR SOURCE AGE DEPOSITIONAL ORGANIC GENERAL SO
PRODUCTIVE
TYPE
ENVIRONMENT FACIES OIL TYPE REF
BASINS OF
SOURCE ROCK
North Sumatra Foreland
Foreland
Foreland
Foreland
Foreland
Foreland
Foreland
Cratonic
Foreland
Foreland
Foreland
Inner Arc
Inner Arc
Baong shales? M-L.Miccene
Bampo? )
) - Oligocene-
Bruksah?? ) E.Miocene
Marine
Marine
Marine
Deltaic
Marine algal/
Terrestrial.
Marine
algal/
Terrestrial
Terrestrial/Non
marine algal
Non-marinealgal
Gas/Lght
01
Situ
198
Soe
Kin
Central Sumatra
Pematang Eocene-
Brown shale Oligocene
(major)
Coal zone
(minor)
Sihapas
coal E.Miocene
and coal shale
Pematang brown
Eocene-
shale? Oligocene
Talang
Akar
Late
Oligo-
coals/coaly cene-Early
shales Miocene
Deep Lacustrine G M . Gravity, Will
waxy, L.
198
Sulphur
Condensatel
light oil
M.
Gravity, Ma
zie
sulphur
L-M. Gravity, Lee
waxy, L.sulphur
M-H Gravity
oil,
L-Mod.
waxy, L. sulphur/
condensate
M.
Gravity
M
waxy, L. ,ulphur
Bus
198
M.
Gravity, Gor
waxy, low Wah
sulphur
198
M. Gravity, Soe
mod waxy, low Rus
sulphur Bish
M-H Gravity,
low-mod waxy,
low sulphur
M.
Gravity, Sie
waxy, low sulphur
M.
Gravity, Dun
waxy, low
197
su lph ur Tho
198
M.
Gravity, Sam
waxy, low
sulphur
Poll
Shallow lacus-
trine/marsh-bog
Fluviodeltaic
Terrestrial
Terrestrial
entral Sumatra
(Malacca Straits)
Deep lacustrine
Fluviodeltaic
Non-marlnc algal
Terrestrial
outh Sumatra
N.W. Java
(Sunda)
N.W. Java
(Ardjuna
Jatibarang)
E. Java Sea
Banuwati shales
Early Oli-
Talang
Akar
Oligocene
coals/shales -E. Miocene
TalangAkar Oligocene-
coals/coal y E. Miocene
shales
Kudjung Oligocene
Unit 111 shales
and coals?
Barat shales? Late Oligo-
gocene
cene
Deep lacustrhc
Fluvio-Deltaic
Non marlne algal
Terrestrial
FluvIo-Deltaic
Terrestrial
Fluviatile Terrestrial
West Natuna
Barito
Kutei
Non-marine algal/
bacterial/terres-
trial
Terrestrial
Lacustrine
Tanjung coals?/ Eocene
shales?
Balikpapan Middle
coals and Miocene and
shales and Younger
Younger Deltaics
Latin coals and
M.
Miocene
shales?
Tarakan and Bu- Pliocene
nyu
coals and
shales?
Fluvio-Deltaic
Deltaic Terrestrial
Deltaic
Terrestrial
L-M. Gravity
Low wax, mod-
high sulphur
E. Sulawesi
(Banggai/Sula)
E. Miocene
shales and car-
nonates?
Jurassic shales
and carbonates?
Manusela
carbonateslcalc
Early Miocene Marine Marine
algal
Jurassic Marine
Marine
Marine algal
Marine Akgal?
ula (Seram)
Early Jurassic
Low-M. Gravity O S
low wax, mod-
198
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C E N T R A L S U M A T R A
L A C U S T R I N E SO U RC E R OC K D E P O S I T E D
IN
HALF
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RIFT
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110
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112
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P Y R O L Y S I S
-
G C O F C R U D E OIL A S P H A L T E N E S
n
L A C U S T R I N E OIL
TYPE I KEROGEN
M A R I N E O I L
T Y P E 11 KEROGEN
I 0 n
C
10 ALK ENE
T TOLUENE
X
= m t p XYLENE
Pf
PR lST
-
I
-
EN
P H E N O L S A L K Y L B E N Z E N E S
T 8 X
I \
F L U V I O - D E L T A IC O I L
TYPE 1II KEROGEN
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114
P Y R O L Y S I S - G C C L A S S I F I C A T IO N O F C R U D E OIL A S P H A
USING D I S T R I B U T I O N
O F
N - O C T E N E m
+ p
XYLENE
PHENOL
T Y P E = K E RO
*.
M A R I N E O I L S
( S A L A W A T 1 , S U
N O C T E N E
100 Y o
D e e p
L a c u s t i n e
O i l s
S u n d a B a s i n 1
S h a l l o w
L a c u s t i n e O i l s
( W . N a t u n a / S u n d a B a s in )
F l u v i o - D e l t a i c Oils
[ N W.
Java
,East Java,
K u t e i , T a r ak a n ,
T Y P E 111
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t ti
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6
F L U V l O
-
D E L T A I C O I L S
-
I D E N T I F I C A T I O N O F R E S I N
C 3 0 C Y C L I C A L K A N E S
R
B
C 2 9
2 9
30
M / Z 191
TRITER PANE S
R C 3 0 C Y C L I C A L K A N E S
OL = l a d O L E A N A N E
C 3 0 = H OP A N E S
T s ,T m = C 2 7 H O P A N E S
M / Z
217
STERANES
2 9 -
S T E R A N E S
M / Z 163
M / Z
412
D E R
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118
LACUSTRINE
OIL
*IDENTIFICATION O F
C
30 4-METHY
L
S T E R A N E S F R O M
M / Z
217,231 AND
414
I O N S
ION 217.00
METHYL
ERANES
O N
414 .00
I l l
4oJ
30-
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C OM PA RIS ON O F S T E R A N E S ( M / Z 217) IN S O UT H S U MA T RA , T A R A K
A N D KUTEI B A S I N F L U V I O - D E L T A I C S O U R C E D O I L S
R
M / Z
217
T A R A K A N B A S I N O I L
L E G E N D
C 2 9 S T E R A N E S
C
2 9
I
D I A S T E R A
R
C 3 0 R E S I
C Y CL I C A L
bl/Z
217
R
P
R
c 2 9
ljh
R
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bl/Z
217
R
K U T E I B A S I N O I L
c 2 9
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