NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea...

24

Transcript of NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea...

Page 1: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)
Page 2: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

NDIP 2014 Andrea Franco 2

Page 3: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

NDIP 2014 Andrea Franco 3

Si–Si bonds in tetrahedral coordination but ordered structure lost at long range

5–20% of atomic hydrogen, for dangling bonds passivation

Bandgap of 1.8 eV

a-Si:H resistivity

(W cm)

Ea (eV)

intrinsic 1010 –1012

(104 for c-Si)

0.7–0.8

n-doped 102 –105

(10-1–10-3 for c-Si)

0.1–0.4

p-doped 104 –106 (1–10-2 for c-Si)

0.3–0.6

Thermally-activated electrical conductivity: 𝜎 = 𝜎0exp −𝐸𝑎

𝑘𝑇

Page 4: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

NDIP 2014 Andrea Franco 4

Hydrogenated amorphous silicon

AMCPs results of electron multiplication

Conclusions and outlook

Page 5: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

NDIP 2014 Andrea Franco 5

a-Si:H with r ≈ 1011 W cm AMCP withstands large bias voltages and provides charge replenishment

a-Si:H PE-CVD vertically integrated AMCP on readout electronics

a-Si:H similar to c-Si channels micromachined with techniques of microelectronics industry, such as deep reactive ion etching (DRIE)

Novel fabrication process: a-Si:H as MCP bulk material

Page 6: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

PE-CVD of layer stack

NDIP 2014 Andrea Franco 6

1.5 mm of SiO2 on 4’’ c-Si wafer

100 nm chromium and patterning

Mesa patterning of layer stack

DRIE of channels

PE-CVD reactor for a-Si:H

20 Å/s deposition rate

120 mm of total a-Si:H

Page 7: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

NDIP 2014 Andrea Franco 7

Three independent electrodes:

<n> mc-Si:H top electrode is biased up to -700 V (~105 V/cm)

<n> mc-Si:H intermediate electrode evacuates the leakage current

Cr anode collects the multiplied electrons

Page 8: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

NDIP 2014 Andrea Franco 8

20 AMCP test structures on 4” wafer

AMCP surface of 0.25, 1 and 4 mm2

G: 5–9 mm

H: 2–7 mm

Channel length 60–100 mm

Aspect ratio (AR) 6:1–12.5:1

Page 9: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

NDIP 2014 Andrea Franco 9

Hydrogenated amorphous silicon

Fabrication of amorphous-silicon-based

microchannel plates (AMCPs)

Conclusions and outlook

Page 10: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

NDIP 2014 Andrea Franco 10

Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

Gain > 30 at -500 V, aspect ratio of 12.5:1

Gain independent on input current enough charge replenishment

Franco et al., Scientific Reports 4, 4597, 2014

Full-field illumination at 254 nm with 16 nm of gold as photocathode

Page 11: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

NDIP 2014 Andrea Franco 11

Franco et al., Scientific Reports 4, 4597, 2014

Gain increases as a function of aspect ratio AMCP proof of concept

Page 12: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

2014 NDIP Andrea Franco 12

Seiler, JAP 54, R1-R18, 1983

Gain depends on the primary electron energy, according to the number of secondary electrons emitted at the first collision.

gain increases by a factor 4 with AMCP tilt of 14°

gain increases by a factor 2 with AMCP tilt of 44°

Page 13: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

NDIP 2014 Andrea Franco 13

First ALD of 5 nm of Al2O3 on AMCP doubled the gain.

Page 14: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

NDIP 2014 Andrea Franco 14

Improved AMCP architecture.

Enhanced sensitivity to electron multiplication.

AMCPs vertically integrated on metallic anodes.

Proven feasibility for AMCP integration on ASIC.

AMCP proof of concept.

Gain increases with the channel aspect ratio.

Enhanced gain with high-emissive SE layer.

Page 15: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

NDIP 2014 Andrea Franco 15

To improve the aspect ratio, 20:1 within immediate reach.

To engineer a funnel structure at the channel entrance.

Vertical integration on ASIC (e.g. Medipix2, Timepix) • Compact and rugged detector

• High spatial resolution (vertical integration)

• High temporal resolution (Dch < 10 mm, conductive bulk)

• AMCP insensitivity to magnetic fields up to a few teslas

• Applications: fast fluorescence imaging, simultaneous PET/MRI,

space missions, neutron detection, …

Page 16: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

NDIP 2014 Andrea Franco 16

Grant 200021_126926/1

PV-Lab:

CSEM:

EPFL CMi:

Sylvain Dunand for helping with the PE-CVD depositions

Jérémie Fonjallaz and Joël Currit for the realization of the UV setup

Pierre-André Clerc for the deep reactive ion etching

Sylviane Pochon for the AMCP bonding

Didier Bouvet for atomic layer deposition

Page 17: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

2014 NDIP Andrea Franco 17

Page 18: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

2014 NDIP Andrea Franco 18

Page 19: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

2014 NDIP Andrea Franco 19

Page 20: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

2014 NDIP Andrea Franco 20

thin gold layer as

photocathode

photolectron

screen

Page 21: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

2014 NDIP Andrea Franco 21

fused silica window + diaphragm

Hg lamp at 254 nm

rod for AMCP tilting

Page 22: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

2014 NDIP Andrea Franco 22

vacuum vessel

UV lamp at 254 nm

LabView routine

turbomolecular pump +

dry rotary pump

vacuum of 10-7 mbar

HV supply lock-in amplifier +

mechanical chopper

anode current

attenuation filter

intensity down to 16%

picoammeters

leakage/anode current

tilting rod

to vary the UV light in channels

temperature controller

TAMCP up to 100 °C

photocathode

16 nm gold on quartz

QE~0.1% at 254 nm

Transmittance~26%

Page 23: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

2014 NDIP Andrea Franco 23

Page 24: NDIP 2014 2 Andrea Francondip.in2p3.fr/.../4Thursday/AM/ID35504_Franco.pdf · NDIP 2014 10 Andrea Franco Electron multiplication increases up to tested voltage of 500 V (7×104 V/cm)

2014 NDIP Andrea Franco 24

Each channel exposed for < 10 ms, exposure rate of 10 Hz

Gain drops after having reached a maximum

charge replenishment ok (Ileak >> Iout)

charging of the decoupling layer surface