MOSH - MOAHSeminar 27 november 2015

Welkom

Willkommen

Wellcome

Service Based Company

Multi-vendor approach

Solution-driven approach “Think YES”

Short communication lines

Privately owned

GC and GC-Analyzers

small footprint saves bench space

“inert GC” optional

color touch screen display and

interface

High Performance Oven, fast ramping rate 170⁰C/minSet-point resolution: 0.1⁰C, max 450⁰C

High pressure injection portsRange 0–150 psi (10 bar)

Full EFC capabilities- up to 3 modules- 1 back flush option

600 Hz data rate detectors

Simply one of the best platforms

456-Series GC – Largest Oven

Conventional columns used

Easy to install columns, valves

Capacity for several columns

Good access. Oven door easily removed

Capabilities that make a difference

Oven with column bracket

Keeps columns organized

Simplifies making critical connections

Easier column replacement

Easy access to oven

Removable door

FAME Analysis: Superb results

OK System: Theoretical FID resp Actual FID resp

C16:0 (25w%) 24.4 24.4

C18:0 (25w%) 24.8 24.8

C20:0 (25w%) 25.2 25.2

C22:0 (25w%) 25.6 25.6

Phar Eur demands: Increasing from C16 to C22. Diff C22-C16 less than 2.0%

Plug and Play GC for FAME• No adjustments need to achieve recovery of EPA/DHA.

• Install a focus liner, column and parameters given by ISB and get perfect results.

• One of the installed GC’s reported has a rapid method doing the analysis in 12 minutes instead of 35 min.

• All GCs shows acceptable results from injection no 1.

• Special and new tools makes maintenance extremely accurate and easy and make reduce user to user variations.

• This message can be confirmed by lots of customers.

GC TO GC VARIATION ON 3 GCs

SNITT

GC 1 GC 2 GC 3 AREAL% STDAV RSD%

C14:0 5.67 5.62 5.58 5.62 0.04 0.64

C14:1 0.99 0.91 0.90 0.93 0.04 4.33

C16:0 15.40 15.57 15.53 15.50 0.08 0.48

C16:1 4.81 4.84 4.82 4.82 0.01 0.28

C18:0 8.01 8.05 8.06 8.04 0.02 0.27

C18:1n-9 12.82 13.06 13.04 12.97 0.11 0.82

C18:1n-7 3.76 4.01 4.00 3.92 0.12 2.94

C18:2n-6 2.11 2.00 2.00 2.04 0.05 2.40

C18:3n-3 2.06 2.00 1.99 2.01 0.03 1.42

C20:0 1.07 1.02 1.02 1.03 0.02 2.14

C20:1n-9 9.15 9.22 9.24 9.20 0.04 0.40

C20:2n-6 1.02 1.02 1.02 1.02 0.00 0.17

C20:4n-6 3.15 3.10 3.11 3.12 0.02 0.73

C20:3n-3 1.01 0.99 0.98 0.99 0.02 1.53

C20:5n-3 10.33 10.25 10.27 10.28 0.04 0.35

C22:0 1.04 1.02 1.03 1.03 0.01 0.68

C22:1n-9 3.08 3.06 3.08 3.07 0.01 0.20

C24:0 1.06 0.98 0.99 1.01 0.04 3.75

C22:6n-3 12.35 12.25 12.31 12.30 0.04 0.35

C24:1 1.12 1.04 1.06 1.07 0.04 3.32n=6 pr GC total of 18 samples

436-GC PTV

FID

NO ADJUSTMENTS NEEDED

Triple Quadruple Solutions

1. Patented Lens-

Free Optical Path

2. Axial Ion Source

3. Auto-focusing

Heated Curved q0

4. 180 degree

curved collision

cell

1. High sensitivity

2. High sensitivity

3. High sensitivity

Robustness

4. Small bench-

space

Master GC with GCxGC option Master GC-oTOF-MS

Master Static Headspace Sampler

Master Dynamic Headspace and Purge

& Trap Sampler

Digitalizing

human sensing

for trouble free

chromatography

/massspectrometry

Pure Gases Solutions

Hydrogen

Air

Nitrogen

High Purity Gas

Solutions

Super Clean™ H2 filters

with

Indicator

Sample Prep Solutions

Complete Product Line

Robotic Tool Change

for sample preparation include:

in LCMS and GCMS

Robotic Sample Injection

(manual tool change)

Successor of PAL-xt

Liquid Sample Injection

For liquid sample injection &

pick and place application

Complete Product Line and

including a

centrifuge

length up to

160 cmintegrating a

balance

multi vendor

Solutions

by

for trouble free

chromatography

/massspectrometry

Knowledge & Skills

ChromatographyGas chromatography

On-Line GC

HPLC

Mass-spectrometry

Statistics

Safety in the lab

Theory by experts from the field

Hands-on experiments

Independent – not related to 1 vendor

Fun

Knowledge & Skills

MOSH - MOAHSeminar 27 November 2015

Morning Programme

11.00 – 11.15 hrs. Instrumental Solutions by Instrument SolutionsGovert Schröder

11.15 – 11.45 hrs. Chronology and examples of the MOSH-MOAH problem in GermanyThomas Funke

11.45 – 12.15 hrs. Principles of the LC-GC Technique for the analysis of MOAS-MOAHAndreas Bruchmann

12.15 – 12.30 hrs. Break

12.30 – 13.00 hrs. Experiences and examples with MOSH-MOAH in food from acommercial food lab | Erik Becker

MOSH - MOAHSeminar 27 November 2015

Chronology and examples of the MOSH-MOAH problem in Germany

Ing. Thomas FunkeChemie. Ing. - Analytik

MOSH - MOAHSeminar 27 November 2015

Principles of the LC-GC technique forthe analysis of MOSH-MOAH

Dr. Andreas BruchmannGeneral Manager

MOSH - MOAHSeminar 27 November 2015

Experiences and examples with MOSH-MOAH in food from a commercial lab

Eillen Schulz

MOSH - MOAHSeminar 27 November 2015

Afternoon Programme

13.00 – 13.45 hrs. Lunch

13.45 – 14.15 hrs. Legal aspects of MOS-MOAH contamination in food and packagingChristoph Goldbeck

14.15 – 14.45 hrs New applications for the LC-GC Technique | PAHs and SterolsMarco Nestola

14.45 – 15.15 hrs. Questions & Answers | Closure

15.15 – 16.00 hrs. Meet & Greet

MOSH - MOAHSeminar 27 November 2015

Legal aspects of MOSH-MOAH contamination in food and packaging

Dr. Christoph GoldbeckLevensmiddelentechnoloog

MOSH - MOAHSeminar 27 November 2015

New applications for the LC-GC technique | PAHs and Sterols

Marco Nestola, MSc.Levensmiddelentechnoloog