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INDUSTRIJA NAFTE, d.d. INDUSTRIJA NAFTE d.d. P.F.Korporativni procesi Corporate Processes Function Sektor istraživanja i razvoja R&D Sector

UVOD Služba Centralni ispitni laboratorij provodi ispitivanja, mjerenja i istraživanja u području zaštite okoliša, zaštite na radu kontrole kvalitete naftnih proizvoda i prirodnog plina, merenja štetnih faktora radne okoline, praćenja tijeka tehnoloških operacija i postupaka, te primjenskih istraživanja.

S CIL provodi istraživanja u području suvremenih analitičkih i drugih tehnika za potrebe istraživanja, proizvodnje i prerade nafte i plina, te skladištenja, transporta i trgovine naftnih derivata. Također provodi razvojno-istraživačke projekte i zadatke u funkciji unapređenja vlastite djelatnosti, a ujedno je i analitička potpora razvojno-istraživačkim projektima unutar INA, d.d.

Kompetentnost stručnog osoblja, laboratorijske opreme i primjenjenih metoda i postupaka mjerenja i ispitivanja potvrđena je i Ovlaštenjima nadležnih tijela državne uprave.

1. Ministarstvo poljoprivrede, šumarstva i vodnog gospodrstva –

Ovlašteni laboratorij za obavljanje poslova uzorkovanja, analize i obradu pokazatelja za otpadne vode. Klasa: UP/Io-034-04/03-01/00031, Ur..br.:525-10/2-15-04-004/005 od 08. studenog 2004.

2. Ministarstvo zaštite okoliša, prostornog uređenja i graditeljstva –

Ovlaštenje za ispitivanje fizikalno-kemijskih svojstava otpada. Klasa: 351-01/05- 012/0123, Ur.br.: 531-08-1-06-3 od 29. kolovoza 2006.

3. Ministarstvo gospodarstva, rada i poduzetništva –

Obavljanje poslova zaštite na radu, ispitivanje fizikalnih i kemijskih čimbenika u radnom okolišu. Klasa: UP/I-116-01/03-03/01, Ur.br.: 526-08-03/2-06-6 od 11. prosinca 2006.


Obavljanje stručnih poslova praćenja kakvoće zraka i emisija u zrak. Klasa: UP/I-351- 02/06-08/00067, Ur.br.: 531-08-2-1-AM-06-04 od 12. srpnja 2006.


Obavljanje stručnih poslova praćenja stanja okoliša (monitoring). Klasa: UP/I-351-02/06- 08/00068, Ur.br.:531-08-2-1-AM-06-04. od 26. svibnja 2006.

Služba centralni ispitni laboratorij od 2002. godine djeluje u sustavu akreditacije prema normi HRN EN ISO/IEC 17025 kojim se potvrđuje tehnička kompetencija laboratorija na razini provođenja samih analitičkih metoda. Potvrdom o akreditaciji i njenim opsegom Služba centralni ispitni laboratorij svrtava se u sam vrh hrvatskih laboratorija vezano uz stručnost, opremljenost i provođenje najstrožijih međunarodnih zahtjeva u poslovanju analitičkih laboratorija.

Hrvatska akreditacijska agencija –

Potvrda o akreditaciji br. 1020 kojom se potvrđuje osposobljenost prema zahtjevima norme HRN EN ISO/IEC 17025:2005 za:

Ispitivanje odabranih značajki kvalitete tekućih naftnih proizvoda, prirodnog plina, površinskih, podzemnih, tehnoloških voda, otpadnih ulja i eluata otpada.

Stručno osoblje, laboratorijska oprema i primijenjena znanja na razini su suvremenih znanja i dostignuća analitičkih laboratorija naftnih kompanija što je rezultat dugogodišnjeg rada u području razvojno-istraživačke djelatnosti INA, d.d.

Uz kontinuiran rad na ispitivanjima i mjerenjima za potrebe INA, d.d., S CIL vrši ispitivanja i za potrebe vanjskih naručitelja – pravnih osoba u okviru raspoloživih mogućnosti.


Služba Centralni ispitni laboratorij princip rada u laboratoriju zasniva na dva osnovna načina:

• ulaz u laboratorij je određeni tip uzorka a izlaz je Izvještaj o ispitivanju (sample oriented)

• ulaz u laboratorij je analitički problem a izlaz je Izvještaj o ispitivanju sa interpretacijom (problem solving oriented)

S CIL organizacijski je ustrojena u tri Odsjeka čija osnovna djelatnst obuhvaća:

• Ekologija (sample oriented)

Analiza voda (površinskih, otpadnih, bušotinskih, geotermalnih, tehnoloških, zdenaca, piezometara)

Analiza opasnog otpada (za trajno odlaganje, spaljivanje i fizikalno-kemijsku obradu)

Analiza tla (organska onečišćenja)

Mikrobiološka ispitivanja

Toksikološka ispitivanja

Mjerenje štetnih faktora radne okoline

• Kontrola kvalitete naftnih proizvoda (sample oriented)

Kontrola kvalitete proizvoda rafinerijske prerade na tržištu

Kontrola kvalitete proizvoda u skladištima i spremnicima

Analize po reklamacijama sa tržišta

Analize prema zahtjevima kontrolnih kuća

• Primijenjena laboratorijska istraživanja (problem solving oriented)

Instrumentalno-analitička ispitivanja plinovitih, tekućih, mazivih i krutih uzoraka u rasponu od mikroanalitičkih određivanja komponenti do spektrometrijskih i kromatografskih ispitivanja sastava nafte i derivata, plinova, polimera, procesnih fluida, te vode i otapala.

Ispitivanja se provode po normiranim ili interno razvijenim metodama. Pri tom se koriste slijedeće instrumentalne tehnike:

Plinska kromatografija

Plinska kromatografija/spektrometrija masa

Tekućinska kromatografija

IR spektrofotometrija

UV/VIS spektrofotometrija

NMR spektrometrija (tekući i kruti uzorci)

Elementarna analiza


Služba Centralni ispitni laboratorij pruža usluge ispitivanja svim naručiteljima unutar INA, d.d. i u okviru svojih mogućnosti i izvan INA, d.d. Usluge se provode za potrebe:

• pridobivanja nafte i plina • transporta nafte i plina • prerade nafte • transporta naftnih proizvoda • veleprodaje naftnih proizvoda • trgovine naftnih proizvoda na benzinskim postajama • zaštite okoliša • zaštite na radu.

Služba Centralni ispitni laboratorij kontinuirano unapređuje svoju djelatnost:

• uvođenjem novih analitičkih metoda i postupaka • stručnim osposobljavanjem zaposlenika • nabavom najsuvremenije laboratorijske opreme • aktivnom suradnjom sa vodećim i međunarodnim stručnim i znanstvenim institucijama • aktivnim sudjelovanjem u tijelima vezanim uz normizacijsku djelatnost • prilagodbom rada laboratorija najsuvremenijim međunarodnim tredovima laboratorijskog poslovanja • održavanjem i proširenjem akreditacije prema normi HRN EN ISO/IEC 17025 • kontinuiranom prilagodbom zahtjevima naručitelja.

INTRODUCTION Central Analytical Laboratory (CAL) performs tests, measurements, and research in the field of environmental protection, occupational safety, quality control of oil products and natural gas, measurement of harmful factors in the work environment, monitoring the course of process operations and procedures, as well as applicational research. CAL research activities are carried out in the field of contemporary analytical and other techniques for the requirements of oil and gas exploration, production and processing, as well as oil product storage, transportation and retail. CAL also implements research and development projects and tasks for the purpose of upgrading its own activity and simultaneously, as analytical support to the research projects within INA d.d. Competence of the expert, professional personnel, state-of-the-art laboratory equipment, and applied methods and procedures of measuring and testing have been confirmed also by the certificates issued by the State Administrative Authorities.

1. Ministry of Agriculture, Forestry, and Water Management –

Certified laboratory for performing the activities of sampling, analysis, and processing of waste water indicators. Class:UP/I°-034-04/03-01/00031, Reg.No.:525-10/2-15-04-004/005 of November 8, 2004

2. Ministry of Environmental Protection, Physical Planning, and Construction –

Certificate for testing the physical and chemical properties of waste. Class: 351-01/05-012/0123, Reg.No.:531-08-1-06-3 of August 29, 2006

3. Ministry of Economy, Labour, and Entrepreneurship –

Performing the activities of occupational safety, testing the physical and chemical factors in the work environment. Class: UP/I-116-01/03-03/01, Reg.No.:526-08-03/2-06-6 of December 11, 2006


Performing the expert activities of monitoring the quality of air and emissions into the air. Class: UP/I-351-02/06-08/00067, Reg.No.:531-08-2-1-AM-06-04 of July 12, 2006


Performing the expert activities of monitoring the state/condition of the environment. Class: UP/I-351-02/06-08/00068, Reg.No.:531-08-2-1-AM-06-04 of May 24, 2006

Since the year 2002, CAL has been functioning within the accreditation system according to the requirements of HRN EN ISO/IEC 17025:2005 Standard confirming the laboratory technical competence on the level of performing the analytical methods themselves. By the Accreditation Certificate and its scope, CAL is ranked on the very top of Croatian laboratories in respect of its expertise/professionalism, equipment, and meeting the strictest international requirements in business activities of analytical laboratories. Croatian Accreditation Agency –

Designating the accreditation No.1020 confirming the competence according to the requirements of the HRN EN ISO/IEC 17025:2005 Standard for: Testing the quality of the selected characteristics of liquid oil products; natural gas; surface, ground, and process water; waste oils, and waste eluates. Expert/professional personnel, laboratory equipment, and the applied expertise on the level of contemporary knowledge and achievements of oil company analytical laboratories, which is the result of working for many years in the field of INA d.d. research and development activities.


In addition to a continuous work on testing and measuring for the requirements of INA d.d., CAL performs tests also for external clients i.e. legal entities, within the free operating capacities.. Central analytical laboratory bases its laboratory work principle on the two essential methods:

• laboratory input is a certain type of sample and output is the Test Report (sample oriented) • laboratory input is an analytical problem and output is the Test Report with Interpretation (problem solving

oriented). The CAL organisational structure consists of the three Departments comprising the following basic activities:

• Ecology (sample oriented)

Water analysis (surface, waste, well, geothermal, process, spring, piezometric)

Hazardous waste analysis (for permanent disposal, incineration, as well as physical and chemical treatment)

Soil analysis (organic pollution)

Microbiological testing

Toxicological testing

Measurement of harmful work environment factors.

● Oil product quality control (sample oriented)

Quality control of the refining products on the market

Quality control of the products in storage facilities and tanks

Analyses per complaint from the market

Analyses according to the requests of inspection agencies ● Applied laboratory research (problem solving oriented) Instrumental and analytical research of gaseous, liquid, lubricant, and solid samples in the range from micro-

analytical determination of components to spectrometric and chromatographic testing of the composition of oil and oil products, gases, polymers, process fluids, as well as water and solvents. Testing is performed according to the standardised or internally developed methods, using the following instrumental techniques:

Gas chromatography

Gas chromatography/mass spectrometry

Liquid chromatography

IR chromatography

UV/VUS spectrometry

NMR spectrometry (liquid and solid samples)

Elementary analysis.


Central analytical laboratory provides testing services to all the clients of INA d.d., and, within the scope of its capabilities, also to those outside of INA d.d. Services are performed for the requirements of:

oil and gas recovery oil and gas transportation oil refining transportation of oil products wholesale of oil products oil product retail at petrol stations environmental protection occupational safety.

CAL continuously upgrades its activities by:

introduction of the new analytical methods and procedures professional training of employees procurement of the state-of-the-art laboratory equipment active cooperation with the leading and international professional and scientific

institutions active participation in the bodies connected with standardisation activities conforming the laboratory work with the best contemporary international trends of

laboratory business maintenance and expansion of accreditation according to the HRN EN ISO/IEC 17025

Standard continuously adjusting to meeting the clients’ requests.

Oznaka CODE

O P I S A N A L I Z A

ANALYSIS DESCRIPTION

STR. page no.

METODE AKREDITIRANE PREMA NORMI HRN EN ISO/IEC 17025 METHODS ACCREDITED ACCORDING TO HRN EN ISO/IEC 17025

11

ANALIZE NAFTNIH PROIZVODA Analyses of petroleum products 11

ANALIZE VODA Water Analysis 13

ANALIZE POLIMERA Polymer analyses ANALIZE PLINA Gas analyses

15

ANALIZE PLINA Gas analyses 15

GA ANALIZE PLINA GAS ANALYSES

16

OPA

ANALIZE NAFTNIH PROIZVODA ANALYSES OF PETROLEUM PRODUCTS

17

WA ANALIZE VODA WATER ANALYSES

23

WstA ANALIZE OTPADA WASTE ANALYSES

30

WstA-1.

ZA FIZIKALNO-KEMIJSKU OBRADU - organski i anorganski otpad FOR PHYSICAL AND CHEMICAL TREATMENT – organic and inorganic waste

30

WstA-2.

ANALIZE OTPADA ZA TERMIČKU OBRADU WASTE ANALYSIS FOR THERMAL TREATMENT

32

WstA-3.

ANALIZE OTPADA ZA TERMIČKU OBRADU WASTE ANALYSIS FOR THERMAL TREATMENT

33

WE ISPITIVANJE ŠTETNIH FAKTORA RADNE OKOLINE TESTING OF HARMFUL EFFECTS IN THE WORKING ENVIRONMENT

35

EA-1.

ELEMENTARNA ANALIZA ELEMENTAR ANALYSIS

38

Oznaka CODE

O P I S A N A L I Z A

ANALYSIS DESCRIPTION

STR. page no.

GC-1. PLINSKA KROMATOGRAFIJA PLINSKA KROMATOGRAFIJA – SPEKTROMETRIJA MASA GAS CHROMATOGRAPHY GAS CHROMATOGRAPHY – MASS SPECTROMETRY

39

HPLC-1.

TEKUĆINSKA KROMATOGRAFIJA VISOKE DJELOTVORNOSTI HIGH PERFORMANCE LIQUID CHROMATOGRAPHY

42

IR/UV-1.

IR I UV/VIS SPEKTROMETRIJA IR AND UV/VIS SPECTROMETRY

38

NMR-1.

NMR SPEKTROMETRIJA NMR SPECTROMETRY

45

S-1.

UZORKOVANJE (operacija) SAMPLING (operation)

47

ISTRAŽIVAČKE STUDIJE / IZVJEŠĆA / UZORKOVANJE RESEARCH STUDIES / REPORTS / SAMPLING

48

RS-1.

ISTRAŽIVAČKE STUDIJE RESEARCH STUDIES

48

R-1.

IZVJEŠĆA REPORTS

48

TUMAČ KRATICA ABBREVIATIONS

49


METODE AKREDITIRANE PREMA NORMI HRN EN ISO/IEC 17025 BACCREDITATION METHODS ACCORDING TO HRN EN ISO/IEC 17025

ANALIZE NAFTNIH PROIZVODA ANALYSES OF PETROLEUM PRODUCTS

Oznaka Code

Vrsta ispitivanja

Property

Metoda ispitivanja

Test method IR/UV-1.01.

Benzen Benzene content

HRN EN 238

OPA-1.06.

Centanski indeks (dizelsko gorivo) Cetane index (diesel fuel)

HRN EN ISO 4264

OPA-1.07.

Destilacija (određivanje karakteristika destilacije kod atmosferskog tlaka) Distillation (determination of distillation characteristic at atmospheric pressure)

HRN ISO 3405

EA-1.01.

Elementarna analiza – CHNS (LECO) Elementar analysis - –HNS (LECO)

ASTM D 5291

OPA-1.12.

Filtrabilnost (CFPP) - –izelsko gorivo Cold filter plugging point – diesel fuel

HRN EN 116

OPA-1.13.

Fizikalno kemijske karakteristike dizelskih goriva; "P„trospec metoda" “Cetanski broj, cetanski indeks, gustoća procjenom, ukupni aromati, PAH, toplinska vrijednost procjenom)Physical and Chemical properties of Diesel fuels; "P„trospec Method" “Cetane number, Cetane index, density by estimation, total aromatic cocntent, PAH, caloric value by estimation)

Interna metoda House Method

OPA-1.14.

Gustoća na 15°C Density at 15°C

HRN ISO 3675 ASTM D-1298

OPA-1.15.

Indeks isparljivosti, VLI Vapour lock index

računski calculation

OPA-1.19.

Kiselost ukupna Total acidity

ASTM D 3242

OPA-1.22.

Korozivnost na Cu-pločici Corrosiveness to copper, Copper-strip test

HRN EN ISO 2160 ASTM D 130

OPA-1.23.

Merkaptanski sumpor Mercaptans

HRN ISO 3012 ASTM D 3227

NMR-1.09.

Određivanje sadržaja benzena i sastava motornih benzina 1H NMR Structural characterization and determination of benzene content in motor gasoline by 1H NMR

Interna metoda House Method Usp. HRN EN 238 i ASTM D 1319 comp.


Oznaka Code

Vrsta ispitivanja Property

Metoda ispitivanja Test method

OPA-1.30.

Plamište, zatvoreno, PM Flash point (PM)

HRN EN 22719 ASTM D 93

OPA-1.31.

Plamište, zatvoreno, TAG Flash point (TAG)

ASTM D 56

HPLC-1.06.

Policiklički aromatski ugljikovodici u dizelskom gorivu, NP-HPLC Polycyclic aromatic hydrocarbons in diesel fuel, NP-HPLC

EN 12916

GC-1.21.

Poliklorirani bifenili (PCB) u loživim, otpadnim i transformatorskim uljima Polychlorinated biphenyls (PCB) in fuel, waste and transformer oils

HRN DIN 51527-1

OPA-1.34.

Smole, postojeće Gum content


OPA-1.35.

Sumpor mikrokulometrijski Sulphur by microculometry

HRN DIN 51400-7

EA-1.11.

Sumpor – valnodisperzivni X-Ray Sulphur – wave dispersive X-Ray

HRN EN SO 20884

OPA-1.37.

Tečenje (stinište) Pour point


OPA-1.40.

Viskoznost, kinematička na određenoj temperaturi Kinematic viscosity at determined temperature


OPA-1.44.

Voda, Karl-Fischer (potenciometrijski – srednji destilati) Water, Karl Fischer titration, (potentiometric titration, middle distillates)

ISO 6296

OPA-1.45.

Zamrzavanje Freezing point

HRN ISO 3013

OPA-1.46.

Zamućenje Cloud point

ISO 3015

ANALIZE VODA

WATER ANALYSES

Oznaka Code

Vrsta ispitivanja Property

Metoda ispitivanja Test method

WA-1.04.

Aluminij (ICP) Aluminium (ICP)

HRN ISO 11885

WA-1.06.

Anion aktivni detergent Anion-active detergent

HRN ISO 7875-1

WA-1.07.

Arsen (ICP) Arsenic (ICP)

HRN EN ISO 11885

WA-1.08.

Bakar (ICP) Copper (ICP)

HRN EN ISO 11885

WA-1.18.

Cink (ICP) Zinc (ICP)

HRN EN ISO 11885

WA-1.20.

Električna vodljivost / električni otpor Electric conductivity / Electric resistance

ISO 7888(E)

WA-1.35.

Kadmij (ICP) Cadmium (ICP)

HRN EN ISO 11885

WA-1.36.

Kalcij (ICP) Calcium (ICP)

HRN EN ISO 11885

WA-1.45.

Kemijska potrošnja kisika (KPK) Chemical oxygen demand (COD), bichromate

HACH, Method 8000

WA-1.48.

Klorid (Cl-) Chloride (Cl-)

HRN ISO 9297

WA-1.52.

Krom (ukupni) (ICP) Chromium, total (ICP)

HRN EN ISO 11885

WA-1.55.

Magnezij (ICP) Magnesium (ICP)

HRN EN ISO 11885

WA-1.57.

Mangan (ICP) Manganese (ICP)

HRN EN ISO 11885

WA-1.61.

Natrij (ICP) Sodium (ICP)

HRN EN ISO 11885

WA-1.63.

Nikal (ICP) Nickel (ICP)

HRN EN ISO 11885

WA-1.64.

Nitrat Nitrate

HACH Method 10020

Oznaka

Code Vrsta ispitivanja

Property Metoda ispitivanja

Test method WA-1.65.

Nitrit Nitrite

HRN EN 26777 The Testing of Water, Merck

WA-1.66.

Određivanje fosfata – spektrometrijsko određivanje Determination of phosphates – spectrometric determination

Interna metoda House method

WA-1.67.

Olovo (ICP) Lead (ICP)

HRN EN ISO 11885

WA-1.69.

pH PH-Value

HRN ISO 10523

WA-1.76.

Stroncij (ICP) Strontium (ICP)

HRN EN ISO 11885

WA-1.79.

Sulfat Sulphate

HRN ISO 9280

WA-1.85.

Suspendirane čestice Suspended particles

HRN ISO 11923

WA-1.94.

Ukupni organski ugljik (TOC) Total organic carbon (TOC)

ISO 8245

WA-1.99.

Željezo (dvovalentno) Iron (bivalent)

HRN ISO 6332

WA-1.100.

Željezo (ukupno) (ICP) Iron, total (ICP)

HRN EN ISO 11885

ANALIZE POLIMERA

POLYMER ANALYSES Oznaka



Test method HPLC-1.07.

Raspodjela molekulskih masa polistirena, HPSEC

Polystyrene molecular mass distribution, HPSEC

ASTM D 5296

ANALIZE PLINA GAS ANALYSES

Oznaka



Test method GC-1.04.

Analiza prirodnog plina (sastav C1-C6+, N2, CO2, toplinska vrijednost, gustoća, relativna gustoća i Wobbeov indeks) Natural gas analysis (composition C1-C6+, N2, CO2, calorific value, density, relative density and Wobbe’s Index)

HRN ISO 6974-4 HRN ISO 6976

GC-1.29.

Ukapljeni naftni plin Liquefied petroleum gas

HRN ISO 7941

GA ANALIZE PLINA GAS ANALYSES

Oznaka Code

Vrste ispitivanja Service Description

Metode ispitivanja Test method

GC-1.04.



GC-1.18. Određivanje pojedinačnih sumpornih spojeva u prirodnom plinu (GC/PFPD) Determination of individual composition of sulphur copmpounds in natural gas (GC/PFPD)

ISO 6326-4

GC-1.19. Određivanje pojedinačnih sumpornih spojeva u ukapljenom naftnom plinu (GC/PFPD) Determination of individual composition of sulphur copmpounds in liquified petroleum gas (GC/PFPD)


EA-1.12. Sumporni spojevi (vodik sulfid, merkaptani, karbonil sulfid) Sulphur compounds (hydrogensulfid, mercaptan sulfur, carbonyl sulfide)

ISO 6326-3

GC-1.29.

Ukapljeni naftni plin Liquefied petroleum gas

HRN ISO 7941

GA-1.01. Živa (uzorkovanje i mjerenje) Mercury (sampling and measurement)

ISO 6978

OPA-1. ANALIZE NAFTNIH PROIZVODA ANALYSES OF PETROLEUM PRODUCTS

Oznaka Code

Vrste ispitivanja Property


OPA-1.01. Aerobni mikroorganizmi u dizelskom gorivu i ekstra lakom loživom ulju Determination of aerobes in diesel fuel and extra-light fuel oil

NF M07-070

OPA-1.02. Aromati, FIA Aromatics content, FIA

ASTM D 1319

IR/UV-1.01.

Benzen Benzene content

HRN EN 238

GC-1.06. Benzini i frakcije - –dređivanje pojedinačnog i grupnog sastava plinskom kromatografijomn (motorni benzini, FCC benzin, katalitički reforming, koking) Gasoline and fractions - –etermination of single and group compounds composition by gas chromatography (motor gasolines, FCC gasolines, catalytic reforming gasoline, cocking gasoline)


OPA-1.03. Boja ASTM (ulja) ASTM colour

ASTM 1500

OPA-1.04. Boja i izgled (vizualno) Colour and Appearance (visual)

OPA-1.05. Boja Saybolt Saybolt colour

ASTM D 156

OPA-1.06.

Centanski indeks (dizelsko gorivo) Cetane index (diesel fuel)

HRN EN ISO 4264

OPA-1.07.

Destilacija (određivanje karakteristika destilacije kod atmosferskog tlaka) Distillation (determination of distillation characteristic at atmospheric pressure)

HRN ISO 3405

OPA-1.08. Dimivost Smoke point


OPA-1.09. Doktor test Doctor test

ASTM D 4952

OPA-1.10. Donja ogrijevna vrijednost Net heat of combustion

ASTM D 3338 ISO 8217

OPA-1.11. Električna provodljivost Electric conductivity

ASTM D 2624

EA-1.01. Elementarna analiza – CHNS (LECO) Elementar analysis - –HNS (LECO)

ASTM D 5291

Oznaka Code



OPA-1.12.

Filtrabilnost (CFPP) - –izelsko gorivo Cold filter plugging point – diesel fuel

HRN EN 116

OPA-1.13.

Fizikalno kemijske karakteristike dizelskih goriva; "P„trospec metoda" “Cetanski broj, cetanski indeks, gustoća procjenom, ukupni aromati, PAH, toplinska vrijednost procjenom) Physical and Chemical properties of Diesel fuels; "P„trospec Method" “Cetane number, Cetane index, density by estimation, total aromatic cocntent, PAH, caloric value by estimation)

Interna metoda House Method

OPA-1.14.

Gustoća na 15°C Density at 15°C

HRN ISO 3675 ASTM D-1298

OPA-1.15.

Indeks isparljivosti, VLI Vapour lock index

računski calculation

OPA-1.16. Indeks viskoznosti Viscosity index

ISO 2909 ASTM D-2270

OPA-1.17. Indikator, kvalitativno, UV/VIS Marker, qualitative

HRN 1110

OPA-1.18. Indikator, kvantitativno, UV/VIS Marker, qualitative, UV/VIS

HRN 1110

GC-1.09. Istraživački oktanski broj benzina iz katalitičkog reforminga (GC) Research octane number of catalytic reforming gasoline by GC

usporedivo sa ASTM D 2699 comp.

GC-1.10. Istraživački oktanski broj FCC benzina (GC) Research octane number of FCC gasoline by GC


NMR-1.03. Istraživački oktanski broj FCC benzina (NMR) Research octane number of FCC gasoline by NMR


NMR-1.04. Istraživački oktanski broj koking benzina (NMR) Research octane numbe rof coking gasoline bv NMR


NMR-1.05. Istraživački oktanski broj benzina iz katalitičkog reforminga (NMR) Research octane number of catalytic reforming gasoline by NMR


OPA-1.19.

Kiselost ukupna Total acidity

ASTM D 3242

EA-1.03. Klor, brom - –varcna cijev Chlorine, bromine content- Quartz tube

IP 244

OPA-1.20.

Koks (Conradson) Carbon residue (Conradson)

HRN ISO 6615

OPA-1.21. Koks, mikrokoks Carbon residue

HRN EN ISO 10370

Oznaka Code



OPA-1.22.

Korozivnost na Cu-pločici Corrosiveness to copper, Copper-strip test


OPA-1.23.

Merkaptanski sumpor Mercaptans


GC-1.13. Metilni esteri masnih kiselina (FAME) – Određivanje sadržaja metanola Fatty Acide Methyl Esters (FAME) – Determination of methanol content

DIN EN 14110

GC-1.14. Metilni esteri masnih kiselina (FAME) – Određivanje sadržaja metilni estera i metilnog estera linolenske kiseline Fatty Acide Methyl Esters (FAME) – Determination of methyl esters and methyl ester of linolenic acid

BS EN 14103

OPA-1.24. Mikroonečišćenja, Milipor laboratorijski Particulate matter

ASTM D 5452

OPA-1.25. Mikroonečišćenja, Milipor u protoku Particulate matter

ASTM D 2276

OPA-1.26. MSEP Microseparometer (MSEP)

ASTM D 3948

OPA-1.27. Naftaleni (mlazno gorivo) UV/VIS Naphthalenes (jet-fuel) UV/VIS

ASTM D 1840

IR/UV-1.06. Određivanje metilnih estera u srednjim destilatima nafte pomoću infracrvene spektrometrije Determination of fatty acid methyl esters (FAME) in middle distillates- Infrared spectroscopy method

HRN EN 14078

GC-1.15. Određivanje oksigenata u bezolovnim motornim benzinima plinskom kromatografijom (MTBE, TAME, metanol) - –C Determination of oxygenates in unleaded motor gasoline s by gas chromatography (MTBE, TAME, methanol) by GC


GC-1.16. Određivanje pojedinačnih sumpornih spojeva u FCC benzinu (GC/PFPD) Determination of individual composition of sulphur copmpounds in FCC gasoline (GC/PFPD)


GC-1.17. Određivanje pojedinačnih sumpornih spojeva u lakom cikličkom ulju (GC/PFPD) Determination of individual composition of sulphur copmpounds in light cyclic oil (GC/PFPD)


NMR-1.09.



Oznaka Code



EA-1.07. Olovo – valnodisperzivni X-Ray Lead – wave dispersive X-Ray

HRN EN ISO 13723

EA-1.08. Pepeo (oksidni i sulfatni) Ash content (oxidated and sulphated)

HRN EN ISO 6245 HRN EN ISO 3987

OPA-1.28 Pepeo (oksidni) – instrumentalna metoda Ash content (oxidated)

HRN EN ISO 6245

IR/UV-1.07. Petroleji za loženje – Određivanje sadržaja aromata Kerosene fuels – determination of aromatic contents

UOP 495

OPA-1.29. Plamište, otvoreno (COC) Flash point (COC)

ASTM 92 ISO 2592

OPA-1.30.

Plamište, zatvoreno, PM Flash point (PM)

HRN EN 22719 ASTM D 93

OPA-1.31.

Plamište, zatvoreno, TAG Flash point (TAG)

ASTM D 56

IR/UV-1.08. Plinska ulja – Infracrveno spektrometrijsko određivanje sadržaja ugljikovodika Gas oils – determination of hydrocarbon contents by infrared spectrometry


HPLC-1.06.

Policiklički aromatski ugljikovodici u dizelskom gorivu, NP-HPLC Polycyclic aromatic hydrocarbons in diesel fuel, NP-HPLC

EN 12916

GC-1.21.

Poliklorirani bifenili (PCB) u loživim, otpadnim i transformatorskim uljima Polychlorinated biphenyls (PCB) in fuel, waste and transformer oils

HRN DIN 51527-1

OPA-1.32. Reakcija s vodom Water reaction


OPA-1.33. Sedimenti Contamination in middle distillates

HRN EN 12662

GC-1.24. Simulirana destilacija (do 260°C) Simulated distillation (to 260°C)

ASTM D-3710


ASTM D-2887

GC-1.26. Simulirana destilacija sumpornih spojeva Simulated distillation of sulphur compounds


OPA-1.34.

Smole, postojeće Gum content


IR/UV-1.14. Spektrometrijsko određivanje plave boje u dizelskom gorivu – EURODIZEL PLAVI UV/VIS spektrometrijom Spectrometric analysis of blue colour in diesel fuel – EURODIESEL BLUE


INDUSTRIJA NAFTE d.d. ZAGREB INDUSTRIJA NAFTE d.d. ZAGREB P.F.Korporativni procesi Corporate Processes Function Sektor istraživanja i razvoja R&D Sector

Oznaka Code



IR/UV-1.15. Spektrometrijsko određivanje policikličkih aromatskih ugljikovodika u dizelskom gorivu Petroleum products-Determination of polycyclic aromatic hydrocarbons-Ultraviolet (UV) spectrometric method

CR 13840

NMR-1.14. Strukturni sastav – benzini, NMR Structural characterisation by NMR – gasoline


NMR-1.16. Strukturni sastav - –oking benzin, NMR Structural characterisation by NMR –coking gasoline

usporedivo sa ASTM D 1319 Comp.

NMR-1.15. Strukturni sastav- dizelsko gorivo, NMR Structural characterisation by NMR – diesel fuel


OPA-1.35.

Sumpor mikrokulometrijski Sulphur by microculometry

HRN DIN 51400-7

EA-1.11. Sumpor – valnodisperzivni X-Ray Sulphur – wave dispersive X-Ray

HRN EN SO 20884

OPA-1.36. Sumpor – energodisperzivni X-Ray Sulphur – energodispersive X-Ray


EA-1.10. Sumpor – energodisperzivni X-Ray Sulfur content – energodispersive X-Ray

HRN EN ISO 8754

OPA-1.37.

Tečenje (stinište) Pour point


OPA-1.38. Tlak para, REID Vapour pressure, REID

ISO 3007 ASTM D 5191

OPA-1.39. Ukupni organski kloridi Total organic chlorides

ASTM D 4929

OPA-1.40.

Viskoznost, kinematička na određenoj temperaturi Kinematic viscosity at determined temperature


OPA-1.41. Voda – destilacijom Water by distillation


OPA-1.42. Voda i sedimenti Water and sediments by centrifuge method

HRN ISO 3734

OPA-1.43. Voda i sedimenti, ogledom Water and sediments, visual

Oznaka Code



OPA-1.44.

Voda, Karl-Fischer (potenciometrijski – srednji destilati) Water, Karl Fischer titration, (potentiometric titration, middle distillates)

ISO 6296

OPA-1.45.

Zamrzavanje Freezing point

HRN ISO 3013

OPA-1.46.

Zamućenje Cloud point

ISO 3015

WA-1.101. Živa (ukupna) Mercury content (total)

Metoda proizvođača LECO LECO Method

WA

ANALIZE VODA WATER ANALYSES

Oznaka Code



WA-1.01. Akutna toksičnost na Daphnia magna Str. Acute toxicity on Daphnia magna Str.

ISO 6341

WA-1.02. Akutna toksičnost s luminiscentnim bakterijama (Vibro fischeri NRRL-B-11177) Acute toxicity with luminescent bacteria (Vibro fischeri NRRL-B-11177)

ISO 11348-1,2,3

WA-1.03. Alkalitet vode (p -,m -) Alkalinity (p-, m-)

Metoda proizvođača METROHM METROHM method

WA-1.04.

Aluminij (ICP) Aluminium (ICP)

HRN ISO 11885

WA-1.05. Amonij (NH4+)

Ammonium (NH4+)

HRN ISO 5664

WA-1.06.

Anion aktivni detergent Anion-active detergent

HRN ISO 7875-1

GC-1.05. Aromatski ugljikovodici (BTX) u vodi – ukupni GC Aromatic hydrocarbon (BTX) in water – total by GC

ISO 11423-2

WA-1.07.

Arsen (ICP) Arsenic (ICP)

HRN EN ISO 11885

WA-1.08.

Bakar (ICP) Copper (ICP)

HRN EN ISO 11885

WA-1.09. Barij (ICP) Barium (ICP)

HRN EN ISO 11885

WA-1.10. Biološka potrošnja kisika (BPK5) Biochemical oxygen demand after 5 days (BOD5)

ISO 5815

WA-1.11. Bor (ICP) Bohr (ICP)

HRN EN ISO 11885

WA-1.12. Broj aerobnih bakterija /220C Count of aerobic bacteria/22°C

ISO 6222

WA-1.13. Broj aerobnih bakterija /370C Count of aerobic bacteria/37°C

ISO 6222

WA-1.14. Broj fekalnih koliforma (E.Coli) Number of faccal coliform (E.Coli)

ISO 9308-2

WA-1.15. Broj ukupnih koliforma Number of coliform organisams )

ISO 9308-1

WA-1.16. Bromid (Br-) Bromide (Br-)

ASTM D 3869


Oznaka Code



WA-1.17. Cijanid (CN-) Cyanide (CN-)


WA-1.18.

Cink (ICP) Zinc (ICP)

HRN EN ISO 11885

WA-1.19. Crpljenje piezometra Piezometer pumping

WA-1.20.


ISO 7888(E)

WA-1.21. Fekalni streptokoki Faecal streptococci

ISO 7899-2

WA-1.22. Filtracijska svojstva vode (membran filter test) Filtration characteristics of water (Membrane filter test)

WA-1.23. Fluorid, (F-) Fluoride, (F-)


WA-1.24. Fosfat Phosphate

ISO 6878

WA-1.25. Glikoli – prprema za ICP analizu Glycols – preparation for ICP analysis


WA-1.26. Gustoća

Density

ASTM D 1429-95

WA-1.27. Hidrogenkarbonat Bicarbonate

HRN ISO 9963-1

WA-1.28. Indeks stabilnosti (Langellier, Stiff) Stability index (Langellier, Stiff)

WA-1.29. Indeks zasićenja (Ryzner) Saturation index (Ryzner)

WA-1.30. Interpretacija podataka analize Interpretation of analysis results

WA-1.31. Ispitivanje učinkovitosti biocida Biocide efficiency testing


WA-1.32. Ispitivanje učinkovitosti inhibitora kamenca Scale-inhibitor efficiency testing


WA-1.33. Izgled, boja, miris Aearance, colour, odour

WA-1.34. Jodid Iodide

ASTM D 3869

Oznaka Code



WA-1.35.

Kadmij (ICP) Cadmium (ICP)

HRN EN ISO 11885

IR/UV-1.03.

Kakvoća vode – Određivanje dušika po Kjeldahlu – Metoda nakon mineralizacije s selenom Water quality- determination of Kjeldahl nitrogen- Method after minerakization with selenium

HRN ISO 5663

GC-1.11. Kakvoća vode – Određivanje uljnog indeksa ugljikovodika (Oil index) Water quality – Determination of hydrocarbon oil index

ISO 9377-2

IR/UV-1.04. Kakvoća vode – Spektrometrijsko određivanje fosfora upotrebom aminijevog molibdata Water quality-Spectrometric determination of phosphorus using ammonium molybdate

HRN EN ISO 6878

WA-1.36.

Kalcij (ICP) Calcium (ICP)

HRN EN ISO 11885

WA-1.37. Kalcijeva tvrdoća Calcium hardness

HRN EN ISO 11885

WA-1.38.

Kalij (ICP)

Potassium (ICP)

HRN EN ISO 11885

WA-1.39. Karbonat Carbonate

HRN ISO 9963-1

WA-1.40. Karbonatna tvrdoća Carbonate hardness

HRN ISO 9963-1

WA-1.41. Kategorizacija otpadnih voda (NN 40/99) Categorisation of wastewater (OG 40/99)

WA-1.42. Kategorizacija voda (NN 77/98) Categorisation of water (OG 77/98)

WA-1.43. Kation aktivni detergent Cation-active detergent

WA-1.44. Kemijska potrošnja kisika (KPK) Chemical oxygen demand (COD)

HRN ISO 6060

WA-1.45.


HACH, Method 8000

WA-1.46. Kisik, otopljeni Oxygen, dissolved

HRN ISO 5813

WA-1.47. Klasifikacija bušotinskih voda (Palmer, Stiff, Tickel, hipotetski sastav) Classification of formation waters (Palmer, Stiff, Tickel)

WA-1.48.

Klorid (Cl-) Chloride (Cl-)

HRN ISO 9297


Oznaka Code



WA-1.49. Klorid (Cl-) Chloride (Cl-)

HACH, Method 8113

WA-1.50. Kobalt (ICP) Cobalt (ICP)

HRN EN ISO 11885

WA-1.51.

Krom (Cr+6) Chromium (Cr+6)

HRN ISO 11083

WA-1.52.

Krom (ukupni) (ICP) Chromium, total (ICP)

HRN EN ISO 11885

WA-1.53. Kronična toksičnost s luminiscentnim bakterijama (Vibro fischeri NRRL-B-11177) Chronic toxicity with luminescent bacteria (Vibro fischeri NRRL-B-11177)

ISO 11348-1,2,3

WA-1.54. Litij (ICP) Lithium (ICP)

HRN EN ISO 11885

WA-1.55.

Magnezij (ICP) Magnesium (ICP)

HRN EN ISO 11885

WA-1.56. Magnezijeva tvrdoća Magnesium hardness

HRN EN ISO 11885

WA-1.57.

Mangan (ICP) Manganese (ICP)

HRN EN ISO 11885

WA-1.58. Međufazna napetost Interfacial tension

ASTM D 1590

HPLC-1.03. Metoda određivanja otopljenih aniona F-, Cl-, NO2-, NO3

-

, Br-, PO43-, SO4

2- u vodama ionskom kromatografijom Method for determination of dissolved anions F-, Cl-, NO2

-, NO3

-, Br-, PO43-, SO4

2- in waters by ion chromatography

HRN EN ISO 10304/1HRN EN ISO 10304/2

HPLC-1.04. Metoda određivanja otopljenih kationa Li+, Na+, NH4+,

K+, Mg2+ i Ca2+ u vodama ionskom kromatografijom Method for determination of dissolved cations Li+, Na+, NH4

+, K+, Mg2+ and Ca2+ in waters by ion chromatography

HRN EN ISO 14911

HPLC-1.05. Metoda određivanja S2- u vodama ionskom kromatografijom Method for determination of S2- in waters by ion chromatography


WA-1.59. Mineralna ulja Mineral oils

DIN 38409-18

WA-1.60. Molibden (ICP) Molybdenum (ICP)

HRN EN ISO 11885


Oznaka Code



WA-1.61.

Natrij (ICP) Sodium (ICP)

HRN EN ISO 11885

WA-1.62. Nekarbonatna tvrdoća Non-carbonate hardness

HRN ISO 9963-1 ASTM D 1067

WA-1.63.

Nikal (ICP) Nickel (ICP)

HRN EN ISO 11885

WA-1.64.

Nitrat Nitrate

HACH Method 10020

WA-1.65.

Nitrit Nitrite

HRN EN 26777 The Testing of Water, Merck

WA-1.66.

Određivanje fosfata – spektrometrijsko određivanje Determination of phosphates – spectrometric determination


WA-1.67.

Olovo (ICP) Lead (ICP)

HRN EN ISO 11885

WA-1.68. Permanganatni indeks Determination of permanganate index

ISO 8467

WA-1.69.

pH pH-value

HRN ISO 10523

WA-1.70. Površinska napetost Surface tension


WA-1.71. Priprema uzorka za analizu Sample preparation


WA-1.72. Pseudomonas aeruginosa

ISO 9308-1 ISO 9308-2

WA-1.73. Salinitet Salinity

HRN ISO 9297 HRN ISO 11885

WA-1.74.

Silicij (ICP) Silica (ICP)

HRN EN ISO 11885

WA-1.75. Silicij (UV/VIS) Silica (UV/VIS)

ASTM D 859

IR/UV-1.13. Spektrofotometrijsko određivanje fenola u vodi Standard Test Method for Phenolic Compounds in Water

ASTM D 1783

WA-1.76.

Stroncij (ICP) Strontium (ICP)

HRN EN ISO 11885

WA-1.77. Studija podudarnosti utisnih i bušotinskih voda Correspondence study of injection and formation water

Oznaka

Code Vrste ispitivanja

Property Metode ispitivanja

Test method


WA-1.78. Suhi ostatak (105ºC) Dry residue (105°C)

Standard Methods for the Examination of Water and Wastewater, 20th Edition, 1999.

WA-1.79.

Sulfat Sulphate

HRN ISO 9280

WA-1.80. Sulfatoreducirajuće bakterije Sulphate-reducing bacteria

Standard Methods for the Examination of Water and Wastewater, 20th Edition, 1999. Part 500 and 502

WA-1.81. Sulfid Sulphide

HACH Method 8131

WA-1.82. Sulfid – jodometrijski Sulphide – iodometric method

Standard Methods for the Examination of Water and Wastewater, 20th Edition, 1999., 4500-S2F

WA-1.83. Sulfitoreducirajuće klostridije Sulphite – reducing bacteria (Clostridia)

ISO 6461-1

WA-1.84. Sumpor (ICP) Sulphur (ICP)

HRN EN ISO 11885

WA-1.85.

Suspendirane čestice Suspended particles

HRN ISO 11923

WA-1.86. Taloživa tvar Settleable matter

Standard Methods for the Examination of Water and Wastewater, 20th Edition, 1999. , 224 F

WA-1.87. Temperatura Temperature

WA-1.88. Ugljik dioksid (otopljeni) Carbon dioxide (dissolved)

APHA Part 111 B

WA-1.89. Ukupna otopljena tvar (180oC) Total dissolved solids dried (180oC)

Standard Methods for the Examination of Water and Wastewater, 20th Edition, 1999.

WA-1.90. Ukupna sadržaj otopljenih soli – ukupna mineralizacijaTotal dissolved mineral content – total mineralization

WA-1.91. Ukupna tvrdoća (Ca + Mg) Total hardness

HRN EN ISO 11885

WA-1.92. Ukupna tvrdoća (izračun) Total hardness (calculation)

Oznaka



Test method


WA-1.93.

Ukupna ulja i masnoće Oil and grease, total

DIN 38409-18

WA-1.94.


ISO 8245

WA-1.95.

Vanadij (ICP) Vanadium (ICP)

HRN EN ISO 11885

WA-1.96. Vodik sulfid (otopljen) Hydrogen sulphide (dissolved)

Standard Methods for the Examination of Water and Wastewater, 20th Edition, 1999. , 4500-S2 F

WA-1.97. Žareni ostatak (550ºC) Ignition residue (550°C)

Standard Methods for the Examination of Water and Wastewater, 20th Edition, 1999. Part 501

WA-1.98. Željezne bakterije Iron bacteria

Standard Methods for the Examination of Water and Wastewater, 20th Edition, 1999. Part 500 and 501

WA-1.99.

Željezo (dvovalentno) Iron (bivalent)

HRN ISO 6332

WA-1.100.

Željezo (ukupno) (ICP) Iron, total (ICP)

HRN EN ISO 11885

WA-1.101. Živa (ukupna) Mercury (total)

Metoda proizvođača “LECO” LECO Method

WstA ANALIZE OTPADA WASTE ANALYSES

WstA

ZA FIZIKALNO-KEMIJSKU OBRADU - organski i anorganski otpad

FOR PHYSICAL AND CHEMICAL TREATMENT – organic and inorganic waste

Oznaka Code



WA-1.17. Cijanid (CN-) – razgradivi

Cyanide (CN-)


WA-1.20.

Električna vodljivost / električni otpor (anorganski otpad) Electric conductivity / Electric resistance (inorganic waste)

ISO 7888(E)

WstA-1.01. Izgled Appearance

EA-1.03. Klor, brom – kvarcna cijev (organski otpad) Chlorine, bromine content- Quartz tube (organic waste)

IP 244

WA-1.51.


HRN ISO 11083

WA-1.65.

Nitrit (anorganski otpad) Nitrite (inorganic waste)

HRN EN 26777 The testing of water Merck

WA-1.69.

pH pH-Value

HRN ISO 10523

WstA-1.02. pH – karakterizacija muljeva pH-Value (sludges characterization)

BS EN 12176

HPLC-1.06.

Policiklički aromatski ugljikovodici u dizelskom gorivu, NP-HPLC (organski otpad) Polycyclic aromatic hydrocarbons in diesel fuel by NP-HPLC method

EN 12916

GC-1.21.

Poliklorirani bifenili (PCB) u loživim, otpadnim i transformatorskim uljima (organski otpad) PCB (Polychlorinated biphenyls) in fuel, waste and transformer oils

HRN DIN 51527-1

WstA-1.03. Priprema uzorka za određivanje teških metala (kruti materijal) Sample preparation for heavy-metal determination (solid material)

US EPA 3050 B

WstA-1.04. Priprema uzorka za određivanje teških metala mikrovalnom digestijom Sample preparation for heavy-metal determination by microwave digestion


Oznaka



Test method

WstA-1.05. Sadržaj ulja Oil content

Standard Methods for the Examination of Water and Wastewater, 20th Edition, 1999. Part 503 A,B

IR/UV-1.13.

Spektrofotometrijsko određivanje fenola u vodi Standard test method for phenolic compounds in water

ASTM D 1783

WstA-1.06. Suha tvar (105oC) Dry matter (105oC)

EN 12880

WstA-1.07. Teški metali - –ojedinačno (Cd, Cr, Ni, Pb, Fe, Zn) Heavy metals – individually (Cd, Cr, Ni, Pb, Fe, Zn)

HRN EN ISO 11885

WA-1.101. Živa ukupna Mercury total


WstA

ANALIZE OTPADA ZA TERMIČKU OBRADU

WASTE ANALYSIS FOR THERMAL TREATMENT

Oznaka Code



EA-1.01.

Elementarna analiza – CHNS (LECO) Elementar analysis - –HNS (LECO)

ASTM D 5291


EA-1.03. Klor, brom - –varcna cijev Chlorine, bromine content- Quartz tube

IP 244

EA-1.08. Pepeo (oksidni i sulfatni) Ash (oxidated, sulfated)


GC-1.21.

Poliklorirani bifenili (PCB) u loživim, otpadnim i transformatorskim uljima PCB (Polychlorinated biphenyls) in fuel, waste and transformer oils

HRN DIN 51527-1

WstA-1.03. Priprema uzorka za određivanje teških metala (kruti materijal, pepeo) Sample preparation for heavy metal determination (solid material, ash)

US EPA 3050 B

WstA-1.04. Priprema uzorka za određivanje teških metala mikrovalnom digestijom Sample preparation for heavy-metal determination by microwave digestion


WstA-1.07. Teški metali - –ojedinačno (Cd, Cr, Ni, Pb, Fe, Zn) – sa pripremom uzorka Heavy metals – individually (Cd, Cr, Ni, Pb, Fe, Zn) – with sample preparation

HRN EN ISO 11885

WstA-1.08. Teški metali – pojedinačno (Na, Ca, Pb, V, Ni, Cu, Cd, Fe) – bez pripreme uzorka Heavy metals individually (Na, Ca, Pb, V, Ni, Cu, Cd, Fe) – without sample preparation

ASTM D 5185 ASTM D 4951

EA-1.13. Toplinska vrijednost Heat content

ASTM D240



WstA-4.

OTPAD ZA TRAJNO ODLAGANJE

WASTE FOR PERMANENT DISPOSAL

Oznaka Code



WA-1.05. Amonij (NH4+)

Ammonium (NH4+)

HRN ISO 5664

WA-1.17. Cijanid (CN-) Cyanide (CN-)


WA-1.20.


ISO 7888(E)

WA-1.23. Fluorid, (F-) Fluoride, (F-)


WstA-1.09. Gubitak žarenjem (550°C) Ignition loss (550°C)

EN 12879


WA-1.44. Kemijska potrošnja kisika (KPK) Chemical oxygen demand (COD)

HRN ISO 6060

WA-1.45.


HACH, Method 8000

WA-1.51.


HRN ISO 11083

WstA-1.10. Mineralna ulja (ukupni ugljikovodici) Mineral oils (total hydrocarbons)

DIN 38409-18

WA-1.65.

Nitrit Nitrite

HRN EN 26777

WA-1.69.

pH pH-Value

HRN ISO 10523

WstA-1.11. pH – karakterizacija muljeva pH-Value (sludges characterization)

BS EN 12176

WstA-1.12. Priprema eluata Eluate preparation

EN 12457

WstA-1.13. Reakcija s vodom Reaction with water

IR/UV-1.13.

Spektrofotometrijsko određivanje fenola u vodi Standard Test Method for Phenolic Compounds in Water

ASTM D1783

WstA-1.06. Suha tvar (105oC) Dry matter (105oC)

EN 12880

Oznaka Code



WstA-1.14. Teški metali-pojedinačno (Cd, Cr, Ni, Pb, As, Zn, Cu) Heavy metals – individually (Cd, Cr, Ni, Pb, As, Zn, Cu)

HRN EN ISO 11885

WA-1.93.

Ukupna ulja i masnoće Oil and grease, total

DIN 38409-18

WA-1.94.


ISO 8245



WE

ISPITIVANJE ŠTETNIH FAKTORA RADNE OKOLINE

TESTING OF HARMFUL EFFECTS IN THE WORKING ENVIRONMENT

Oznaka Code



WE-1.1. Amonijak (do 20 mjerenja po radnom mjestu/iznad 20

mjerenja po radnom mjestu) Ammonia (up to 20 measurements per work-place/over 20 measurements per work-place)

WE-1.2. Buka (frekventna oktavna analiza iznad 85 dB) Noise (frequency octave analysis above 85 dB)

HRN ISO 9612

WE-1.3. Buka (razina buke do 85 dB) Noise (up to 85 dB)

HRN ISO 9612

WE-1.4. Eksplozivnost, donja granica (do 20 mjerenja po radnom mjestu/iznad 20 mjerenja po radnom mjestu) Explosiveness, lower limit (up to 20 measurements per work-place/over 20 measurements per work-place)

WE-1.5. Kapacitet ventilacije digestora - po rešetci Digestor ventilation capacity – per screen

HRN EN 14175-3 DIN EN 14175-4

WE-1.6. Kisik (do 20 mjerenja po radnom mjestu/ iznad 20 mjerenja po radnom mjestu) Oxygen (up to 20 measurements per work-place/over 20 measurements per work-place)

WE-1.7. Koncentracija štetnih plinova - dušik (II) oksid, NO Concentration of harmful gases - nitrogen(II)oxide, NO

Metoda proizvođača DRÄGER DRÄGER Method

WE-1.8. Koncentracija štetnih plinova - dušik (IV) oksid, NO2 Concentration of harmful gases - nitrogen(IV)oxide, NO2


WE-1.9. Koncentracija štetnih plinova - sumporovodik, H2S Concentration of harmful gases - Hydrogen sulphide, H2S


WE-1.10. Koncentracija štetnih plinova - ugljik (II) oksid Concentration of harmful gases - Carbon (II) oxide


WE-1.11. Mikroklima - strujanje zraka (do 20 mjerenja po radnom mjestu/iznad 20 mjerenja po radnom mjestu) Air stream, microclimate (up to 20 measurements per work-place/over 20 measurements per work-place)

HRN EN ISO 7726 HRN EN 13779

WE-1.12. Mikroklima – temperatura (do 20 mjerenja po radnom mjestu/ iznad 20 mjerenja po radnom mjestu) Temperature, microclimate (up to 20 measurements per work-place/over 20 measurements per work-place)


Oznaka Code



WE-1.13. Mikroklima - točka rosišta, mikroklima (do 20 mjerenja

po radnom mjestu/iznad 20 mjerenja po radnom mjestu) Dew point, microclimate (up to 20 measurements per work-place/over 20 measurements per work-place)


WE-1.14. Mikroklima - vlaga (do 20 mjerenja po radnom mjestu/ iznad 20 mjerenja po radnom mjestu) Humidity, microclimate (up to 20 measurements per work-place/over 20 measurements per work-place)


GC-1.20. Određivanje ukupnih ugljikovodika u zraku Determination of total hydrocarbons in air


WE-1.15. Prašina (do 20 mjerenja po radnom mjestu/ iznad 20 mjerenja po radnom mjestu) Dust (up to 20 measurements per work-place/over 20 measurements per work-place)

DIN EN 481

WE-1.16. Razina osvjetljenosti (prosječno osvjetljenje vanjskih prostora iznad cca 250 m2)) Lighting level (average outdoor lighting of areas larger than 250 m2)

ISO/FDIS 8995-2

WE-1.17. Razina osvjetljenosti (unutarnji prostori) 100-250 m2 Lighting level (indoors) 100-250 m2

HRN U.C9.100

WE-1.18. Razina osvjetljenosti (unutarnji prostori) 50-100 m2

Lighting level (indoors) 50-100 m2

HRN U.C9.100

WE-1.19. Razina osvjetljenosti (unutarnji prostori) - iznad 250m2

Lighting level (indoors) - >250 m2

HRN U.C9.100

WE-1.20. Razina osvjetljenosti (unutarnji prostori) - po radnom mjestu Lighting level (indoors) - per work-place

HRN U.C9.100

WE-1.21. Razina osvjetljenosti (unutarnji prostori) 50 m2 Lighting level (indoors) 50 m2

HRN U.C9.100

WE-1.22. Razina osvjetljenosti (vanjski prostori) - po radnom mjestu Lighting level (outdoors) - per work-place

ISO/FDIS 8995-2

WE-1.23. Razina osvjetljenosti (vanjski prostori) prosječno osvjetljenje vanjskih prostora cca 100-250 m2 Lighting level (outdoors), average outdoor lighting of areas aprox. 100-250 m2

ISO/FDIS 8995-2

WE-1.24. Razina osvjetljenosti (vanjski prostori) prosječno osvjetljenje vanjskih prostora cca 50-100 m2) Lighting level (outdoors), average outdoor lighting of areas aprox. 50-100 m2

ISO/FDIS 8995-2

Oznaka Code



WE-1.25. Štetni plinovi i pare (do 20 mjerenja po radnom

mjestu/ iznad 20 mjerenja po radnom mjestu) Harmful gases and vapours (up to 20 measurements per work-place/over 20 measurements per work-place)

FOXBORO Instruction manual MIRAN 1A 001-4136, 1986. Metoda proizvođača DRÄGER DRÄGER Method

WE-1.26. Ugljik (IV) oksid, CO2 (do 20 mjerenja po radnom mjestu/iznad 20 mjerenja po radnom mjestu) Carbon dioxide, CO2 ((up to 20 measurements per work-place/over 20 measurements per work-place)

HRN EN 13779

WE-1.27. Ugljikovodici, ukupni (do 20 mjerenja po radnom mjestu/ iznad 20 mjerenja po radnom mjestu) Hydrocarbons, total (up to 20 measurements per work-place/over 20 measurements per work-place)

Metoda proizvođača PHOTOVAC PHOTOVAC Method

WE-1.28. Ventilacija, efikasnost (kapacitet i broj izmjena zraka) po rešetci Ventilation efficiency (air exchange capacity and number) per screen

HRN EN 13779

EA-1.

ELEMENTARNA ANALIZA ELEMENTAR ANALYSIS

Oznaka



Test method

EA-1.01.

Elementarna analiza – CHNS (LECO) Elementar analysis - CHNS (LECO)

ASTM D 5291

EA-1.02 Klor – valnodisperzivne X-Ray Chlorine – wave dispersive X-Ray

ISO 15597

EA-1.03. Klor, brom - kvarcna cijev Chlorine, bromine content- Quartz tube

IP 244

EA-1.04. Koksni ostatak (Conradson) Carbon residue (Conradson)

HRN ISO 6615

EA-1.05. Ni, V - valnodisperzivni X-Ray Ni, V – wave dispersive X-Ray

ISO 14597

EA-1.06. Ni, V, Cl, Mn, Si - valnodisperzivni X-Ray Ni, V, Cl, Mn, Si - wave dispersive X-Ray

Metoda proizvođača THERMO ARL THERMO ARL Method

EA-1.07. Olovo – valnodisperzivni X-Ray Lead - wave dispersive X-Ray

HRN EN ISO 13723

EA-1.08. Pepeo (oksidni i sulfatni) Ash (oxidated, sulfated)


EA-1.09. Pregled nepoznatog uzorka na prisustvo metala – valnodisperzivni X-Ray Screening of unknown sample on metal presence – wave dispersive X-Ray

EA-1.10. Sumpor – energodisperzivni X-Ray Sulfur content – energodispersive X-Ray

HRN EN ISO 8754

EA-1.11.

Sumpor – valnodisperzivni X-Ray Sulphur – wave dispersive X-Ray

HRN EN SO 20884

EA-1.12. Sumporni spojevi (vodik sulfid, merkaptani, karbonil sulfid) Sulphur compounds (hydrogensulfid, mercaptan sulfur, carbonyl sulfide)

ISO 6326-3

EA-1.13. Toplinska vrijednost Heat content

ASTM D240

GC-1.

PLINSKA KROMATOGRAFIJA

PLINSKA KROMATOGRAFIJA – SPEKTROMETRIJA MASA GAS CHROMATOGRAPHY

GAS CHROMATOGRAPHY – MASS SPECTROMETRY

Oznaka Code



GC-1.01. a-MDEA – analiza plinskom kromatografijom a-MDEA – gas chromatographic analysis

Man. BASF

GC-1.02. Analiza debutaniziranog plina Analysis of debutanized gas

ASTM D 2427

GC-1.03. Analiza mono-, di- i tri-etilenglikola Analysis of mono-, di- and tri-ethyleneglycol


GC-1.04.



GC-1.05. Aromatski ugljikovodici (BTX) u vodi - ukupni GC Aromatic hydrocarbon (BTX) in water - total by GC

ISO 11423-2

GC-1.06. Benzini i frakcije - određivanje pojedinačnog i grupnog sastava plinskom kromatografijomn (motorni benzini, FCC benzin, katalitički reforming, koking) Gasoline and fractions - determination of single and group composition by gas chromatography (motor gasolines, FCC gasolines, catalytic reforming gasoline, cocking gasoline)


GC-1.07 GC/MS – Identifikacija i analiza nepoznatih uzoraka GC/MS – Identification analysis of unknown samples

GC-1.08. GC/MS Određivanje biomarkera (hopani, sterani) Determination of biomarkers (hopanes, steranes) by GC/MS


GC-1.09. Istraživački oktanski broj benzina iz katalitičkog reforminga (GC) Research octane number of catalytic reforming gasoline by GC


GC-1.10. Istraživački oktanski broj FCC benzina (GC) Research octane number of FCC gasoline by GC


GC-1.11. Kakvoća vode – Određivanje uljnog indeksa ugljikovodika (Oil index) Water quality – Determination of hydrocarbon oil index

ISO 9377-2

Oznaka Code



GC-1.12. Ksilen - Određivanje sastava plinskom kromatografijom GC determination of Xylene composition


GC-1.13. Metilni esteri masnih kiselina (FAME) – Određivanje sadržaja metanola Fatty Acide Methyl Esters (FAME) – Determination of methanol content

DIN EN 14110

GC-1.14. Metilni esteri masnih kiselina (FAME) – Određivanje sadržaja metilni estera i metilnog estera linolenske kiseline Fatty Acide Methyl Esters (FAME) – Determination of methyl esters and methyl ester of linolenic acid

BS EN 14103

GC-1.15. Određivanje oksigenata u bezolovnim motornim benzinima (MTBE, TAME, metanol) - GC Determination of oxygenates in unleaded motor gasoline s by gas chromatography (MTBE, TAME, methanol)


GC-1.16. Određivanje pojedinačnih sumpornih spojeva u FCC benzinu (GC/PFPD) Determination of individual composition of sulphur copmpounds in FCC gasoline (GC/PFPD)


GC-1.17. Određivanje pojedinačnih sumpornih spojeva u lakom cikličkom ulju (GC/PFPD) Determination of individual composition of sulphur copmpounds in light cyclic oil (GC/PFPD)


GC-1.18. Određivanje pojedinačnih sumpornih spojeva u prirodnom plinu (GC/PFPD) Determination of individual composition of sulphur copmpounds in natural gas (GC/PFPD)

ISO 6326-4

GC-1.19. Određivanje pojedinačnih sumpornih spojeva u ukapljenom naftnom plinu (GC/PFPD) Determination of individual composition of sulphur copmpounds in liquified petroleum gas (GC/PFPD)


GC-1.20. Određivanje ukupnih ugljikovodika u zraku Determination of total hydrocarbons in air


GC-1.21.

Poliklorirani bifenili (PCB) u loživim, otpadnim i transformatorskim uljima PCB (Polychlorinated biphenyls) in fuel, waste and transformer oils

HRN DIN 51527-1

GC-1.22. Razvoj metode GC Method development by gas chromatography

GC-1.23. Razvoj metode – GC/MS Method development by GC/MS

Oznaka Code




ASTM D-3710


ASTM D-2887

GC-1.26. Simulirana destilacija sumpornih spojeva Simulated distillation of sulphur compounds


GC-1.27. Snimanje kromatograma (ukupne ionske struje), GC/MS GC/MS– chromatogram (Total ion current)

GC-1.28. Snimanje kromatograma, GC Gas chromatography – chromatogram

GC-1.29.

Ukapljeni naftni plin - određivanje sastava Liquefied petroleum gas - determination of composition

HRN ISO 7941

HPLC-1.

TEKUĆINSKA KROMATOGRAFIJA VISOKE DJELOTVORNOSTI

HIGH PERFORMANCE LIQUID CHROMATOGRAPHY

Oznaka Code



HPLC-1.01. Izolacija grupa aromatskih spojeva polupreparativnom NP-HPLC Isolation of aromatic hydrocarbon groups by semi-preparative NP-HPLC


HPLC-1.02. Izolacija zasićenih, aromatskih i polarnih ugljikovodika polupreparativnom NP-HPLC Isolation of saturated, aromatic and polar hydrocarbons by semi-preparative NP-HPLC


HPLC-1.03. Metoda određivanja otopljenih aniona F-, Cl-, NO2-, NO3

-

, Br-, PO43-, SO4

2- u vodama ionskom kromatografijom Method for determination of dissolved anions F-, Cl-, NO2

-, NO3

-, Br-, PO43-, SO4

2- in waters by ion chromatography

HRN EN ISO 10304/1 HRN EN ISO 10304/2

HPLC-1.04. Metoda određivanja otopljenih kationa Li+, Na+, NH4+,

K+, Mg2+ i Ca2+ u vodama ionskom kromatografijom Method for determination of dissolved cations Li+, Na+, NH4

+, K+, Mg2+ and Ca2+ in waters by ion chromatography

HRN EN ISO 14911

HPLC-1.05. Metoda određivanja S2- u vodama ionskom kromatografijom Method for determination of S2- in waters by ion chromatography


HPLC-1.06.

Policiklički aromatski ugljikovodici u dizelskom gorivu, NP-HPLC Polycyclic aromatic hydrocarbons in diesel fuel by NP-HPLC method

EN 12916

HPLC-1.07. Raspodjela molekularnih masa i karakterizacija uzoraka nafte i derivata u niskomolekularnom području, HPSEC Molecular mass distribution and characterization of oil and derivates in low molecular mass rangen, HPSEC


HPLC-1.08.

Raspodjela molekularnih masa polimera, HPSEC Polymer molecular mass distribution, HPSEC

ASTM D 5296

HPLC-1.09. Razvoj metode HPLC Method development by HPLC

IR/UV-1.

IR I UV/VIS SPEKTROMETRIJA

IR AND UV/VIS SPECTROMETRY

Oznaka Code



IR/UV-1.01.

Benzen Benzene

HRN EN 238

IR/UV-1.02. IR spektrometrijska identifikacija i analiza nepoznatih uzoraka organskog i anorganskog porijekla IR spectrometric identification and analysis of unknown samples )inorganic and organic)

IR/UV-1.03.

Kakvoća vode – Određivanje dušika po Kjeldahlu – Metoda nakon mineralizacije s selenom Water quality- determination of Kjeldahl nitrogen- Method after minerakization with selenium

HRN ISO 5663

IR/UV-1.04.

Kakvoća vode - Spektrometrijsko određivanje fosfora upotrebom aminijevog molibdata Water quality-Spectrometric determination of phosphorus using ammonium molybdate

HRN EN ISO 6878

IR/UV-1.05. Medicinski naftalan – UV spektrometrijsko određivanje čistoće Standard Test Method for Evaluation of White Mineral Oil by Ultraviolet Absorption

ASTM D 2269

IR/UV-1.06. Određivanje metilnih estera u srednjim destilatima nafte pomoću infracrvene spektrometrije Determination of fatty acid methyl esters (FAME) in middle distillates- Infrared spectroscopy method

HRN EN 14078

IR/UV-1.07. Petroleji za loženje – Određivanje sadržaja aromata Kerosene fuels – determination of aromatic contents

UOP 495

IR/UV-1.08. Plinska ulja – Infracrveno spektrometrijsko određivanje sadržaja ugljikovodika Gas oils – determination of hydrocarbon contents by infrared spectrometry


IR/UV-1.09. Pregledni spektar - IR IR spectra

IR/UV-1.10. Pregledni spektar - UV/VIS UV/VIS spectra

IR/UV-1.11. Razvoj metode - IR Method development by IR spectrometry

IR/UV-1.12. Razvoj metode - UV/VIS Method development by UV/VIS spectrometry

Oznaka Code



IR/UV-1.13. Spektrofotometrijsko određivanje fenola u vodi Standard test method for phenolic compounds in water

ASTM D 1783

IR/UV-1.14. Spektrometrijsko određivanje plave boje u dizelskom gorivu – EURODIZEL PLAVI UV/VIS spektrometrijom Spectrometric analysis of blue colour in diesel fuel – EURODIESEL BLUE


IR/UV-1.15. Spektrometrijsko određivanje policikličkih aromatskih ugljikovodika u dizelskom gorivu Petroleum products-Determination of polycyclic aromatic hydrocarbons-Ultraviolet (UV) spectrometric method

CR 13840

NMR-1.

NMR SPEKTROMETRIJA NMR SPECTROMETRY

Oznaka



Test method

NMR-1.01. Analiza smjesa ugljikovodika po funkcionalnim grupama 1H NMR Functional group distribution in hydrocarbon mixture by 1H NMR


NMR-1.02. Identifikacija polimernih aditiva i onečišćenja 1H ili 13C NMR Structural determination of polymer additives and impurity by 1H or 13C NMR

Interna metoda

NMR-1.03. Istraživački oktanski broj FCC benzina (NMR) Research octane number of FCC gasoline by NMR


NMR-1.04. Istraživački oktanski broj koking benzina (NMR) Research octane numbe rof coking gasoline bv NMR


NMR-1.05. Istraživački oktanski broj benzina iz katalitičkog reforminga (NMR) Research octane number of catalytic reforming gasoline by NMR


NMR-1.06. Kvantitativni sastav kopolimera 1H NMR Copolymer composition by 1H NMR


NMR-1.07. Kvantitativni sastav smjesa organskih spojeva 1H NMR Composition of organic mixture by 1H NMR


NMR-1.08 NMR - Razvoj metode NMR - Method development

NMR-1.09.



NMR-1.10. Pregledni spektar, 1H ili 13C NMR (do 1 sat snimanja) 1H or 13C NMR spectra (up to 1 hour)


NMR-1.11. Snimanje NMR spektra krutog uzorka (do 3 sata snimanja) Solid state NMR spectra (up to 3 hour)


NMR-1.12. Snimanje NMR spektra krutog uzorka sa interpretacijom (do 3 sata snimanja) Solid state NMR spectrawith interpretation (up to 3 hour)


Oznaka Code



NMR-1.13. Spektar i interpretacija strukture organskih spojeva 1H ili 13C NMR 1H or 13C NMR spectra with interpretation of organic samples


NMR-1.14. Strukturni sastav – benzini, NMR Structural characterisation by NMR – gasoline


NMR-1.15. Strukturni sastav - dizelsko gorivo, NMR Structural characterisation by NMR – diesel fuel


NMR-1.16. Strukturni sastav - koking benzin, NMR Structural characterisation by NMR –coking gasoline


NMR-1.17. Strukturni sastav – plinski kondenzat, NMR Structural characterisation by NMR – gas condensate

usporedivo sa ASTM 2549 (comp).

S-1.

UZORKOVANJE (operacija)

SAMPLING (operation)

S-1.01. Uzorkovanje naftnih proizvoda prema normi HRN EN ISO 3170 Oil products sampling according standard method HRN EN ISO 3170

S-1.02. Uzorkovanje otpada Waste sampling

S-1.03. Uzorkovanje vode Water sampling

Oznaka Code

ISTRAŽIVAČKE STUDIJE / IZVJEŠĆA / ZAPOSLENICI /

UZORKOVANJE RESEARCH STUDIES / REPORTS / EMPLOYEES / SAMPLING

RS-1.

ISTRAŽIVAČKE STUDIJE RESEARCH STUDIES

RS-1.01. Razvojno-istraživačke studije

Research studies

R-1.

IZVJEŠĆA REPORTS

R-1.01. Izvješća do 3 stranice

Reports up to 3 pages

R-1.02. Izvješća više od 4 stranice (s proračunima, komentarima, interpretacijama) Reports over 4 pages (include calculations, comments, /interpretations) do 6 primjeraka uključujući CD sa datotekom up to 6 copies including CD with data files

R-1.03. Dodatni primjerci pod R-1.02. po komadu Additional copies under item R-1.02. per additional copy

R-1.04. Izdavanje izvještaja prema važećim Ovlaštenjima državne uprave (uključuje rezultate ispitivanja i/ili mjerenja)

• do 3 strane • do 10 strana • više od 10 strana

Issuing reports according to the valid accreditations of state authorities (including the testing and/or measurment results)

• up to 3 pages • up to 10 pages • more than 10 pages

R-1.05. Izdavanje zakonom propisanih ovjerenih obrazaca (C2 NN 9/90 i NN

27/96)) po primjerku Issuing forms prescribed by the law (C2 O.G. Nos. 9/90 and 27/96), verified per copy

R-1.06 Izdavanje Uvjerenja o ispitivanju radne okoline (NN 59/96, čl.53 i NN 114/02, čl.17) Issuing Certificates on testing the work environment (O.G. Nos. 59/96, art.53 and 114/02, art.17)

TUMAČ KRATICA ABBREVIATIONS

AA Atomic Absorption a-MDEA

Aktivirana otopina metil-dietanol amina Activated Methyl-Diethanol Amine solution

AP Abel Pensky API American Petroleum Institut APHA American Public Health Association ASTM American Society for Testing and Materials BASF

BASF (naziv njemačke firme) BASF (a German firm)

BPK5

Biološka potrošnja kisika (petodnevna) Biological oxygen demand (5-day)

BTX

benzen, toluen, ksilen Benzene, Toluene, Xylene

C H N S Carbon Hydrogen Nitrogen Sulphur CFPP Cold Filter Plugging Point DIN German standard EN

Europska norma European standard

EA Elemental analysis FCC Fluid Catalytic Cracking FIA Fluorescent Indicator Adsorption GA Gas Analyses GC Gas Cromatography GC/MS Gas Chromatography/Mass Spectrometry HPLC High Performance Liquid Chromatography HPSEC High Performance Size Exclusion Chromatography HRN Hrvatska norma Croatian standard IOB

Istraživački oktanski broj Research Octane number

INA N

INA norma INA standard

IP The Institute of Petroleum IR Infrared ISO International Organization for Standardization KPK Kemijska potrošnja kisika LC Liquid Chromatography MSEP Micro Separation Rating NMR Nuclear Magnetic Resonance OPA Oil Product Analyses PCB

Poliklorirani bifenili Polychlorinated biphenyls

PM Pensky Martens R Reports REID po REID-u RS Research Studies TOC Total Oil Carbon TBN Total Base Number UV/VIS Ultraviolet/Visible VLI Volatile Liquid Index VOC Volatile Organic Carbon UOP Universal Oil Products US EPA United States Environmental Protection Agency WA Water Analyses WstA

Waste Analyses

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