Development of 2G HTS wire production at SuperOx · 2018. 11. 21. · 3 2G HTS wire architecture...

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1 19 September 2017 Development of 2G HTS wire production at SuperOx EUCAS-2017, Geneva

Transcript of Development of 2G HTS wire production at SuperOx · 2018. 11. 21. · 3 2G HTS wire architecture...

Page 1: Development of 2G HTS wire production at SuperOx · 2018. 11. 21. · 3 2G HTS wire architecture Hastelloy C276 Al 2 O 3 Y 2 O 3 IBAD - MgO LaMnO 3 CeO 2 (Gd 2 O 3) GdBCO Ag Cold

119 September 2017

Development of 2G HTS wire production at SuperOx

EUCAS-2017, Geneva

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Outline

2G HTS wire productiono Facility expansion

o Quality control

2G HTS wire performanceo Consistent performance without APC

o R&D into APC

HTS device projectso FCL

o Lightweight cable for aircraft

o Horizon 2020: HTS motor for aircraft

o Roebel cables

19 September 2017

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2G HTS wire architecture

Hastelloy C276

Al2O3

Y2O3

IBAD - MgO

LaMnO3

CeO2(Gd2O3)

GdBCO

Ag

Cold rolled & electro polished

(60 or 100 microns)

Sputtering (30-50 nm)

Sputtering (custom thickness)

PLD (1-3 microns)

PLD (100-200 nm)

e-beam IBAD (5-7 nm) + epi (50-150 nm)

Sputtering (30-50 nm)

Sputtering (5-10 nm)

FinishCustomised finish tailored to application

19 September 2017

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Production status and development

Originally: 2011-2015

Moscow Substrate Ag Cu Finish

Tokyo Buffer HTS Ag

At present: 2017

Moscow Substrate Buffer HTS Ag Cu Finish

Tokyo Buffer HTS Ag Cu

Decisions to increase throughput are driven by demand

19 September 2017

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SuperOx Japan LLC: in operation since Nov 2011

Multiprocess one-chamber sputtering/IBAD system

Dual-chamber PLD-HTS system for CeO2 and GdBCO19 September 2017

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Moscow buffer layer line commissioned Jan 2016

e-Polished Hastelloy substrate in

Ready buffered tape with LaMnO3 on top out19 September 2017

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Moscow buffer layer line commissioned Jan 2016

High Ic by PLD-HTS on Moscow buffer

Df (110) LMO < 7oGood IBAD-MgO RHEED patterns

19 September 2017

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Moscow PLD-HTS line commissioned Dec 2016

Wire produced at SuperOx in Moscow

and at SuperOx Japan is of identical high quality19 September 2017

SuperOx production capacity doubled

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Quality control

Substrate Buffer HTS Ag Cu Finish

In-line Optical RHEED Optical

Off-line,

full length

Non-

contact Ic

Non-

contact Ic

Non-

contact Ic

Specific

tests

Off-line,

segmentsAFM XRD

XRD

SEM

EDX

Transport Ic Transport Ic

19 September 2017

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In-line QC in textured template production

• RGB Scan: software for optical detection of various surface defects

o The software collects images from a camera and performs digital

analysis of the tape surface quality

o Several quality parameters are derived from each image

19 September 2017 Poster on Thursday: 4MP7-14

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In-line QC in textured template production

19 September 2017 Poster on Thursday: 4MP7-14

• GreenScan: software for digital analysis of RHEED patterns

o Texture quality is described by a single parameter

o Closed-loop texture quality control is implemented

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Outline

2G HTS wire productiono Facility expansion

o Quality control

2G HTS wire performanceo Consistent performance without APC

o R&D into APC

HTS device projectso FCL

o Lightweight cable for aircraft

o Horizon 2020: HTS motor for aircraft

o Roebel cables

19 September 2017

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2G HTS wire: high Ic over long length

77 K

19 September 2017

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2G HTS wire: consistent performance

Data updated regularly, available for download at

http://www.superox.ru/en/products/974-vtspprovod/

77 K, 1 T

4.2 K

Low angular anisotropy Reproducible lift factors

NO artificial pinning centres, only intrinsic Gd2O3 nanoparticles due to excess Gd

S. Samoilenkov et al., Supercond. Sci. Technol. 29 (2016) 024001

19 September 2017

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2G HTS wire: artificial pinning in high rate PLD

Production rate PLD. Classic nanocolumns of perovskite AP centres.

19 September 2017

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2G HTS wire: artificial pinning in high rate PLD

Less anisotropy and higher min. Ic in field with pinning

19 September 2017

V. Chepikov et al., submitted to SuST special issue

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2G HTS wire: artificial pinning in high rate PLD

Higher Jc/Ic in liquid helium

Next steps:

Optimise for specific T, B

Verify reproducibility in production wires19 September 2017

V. Chepikov et al., submitted to SuST special issue

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2G HTS wire: customisation

Manufacturer Customisation options

Silver Copper

plating

Lamination Surround

polyimide

Polyimide

wrapping

Solder

plating

Tape

stacks

Filaments

AMSC ● ● ●

Fujikura ● ● ●

SuNAM ● ● ● ●

SuperOx ● ● ● ● ● ● ● ●

SuperPower ● ● ● ● ●

Custom copper plating

Custom solder plating

Polyimide deposition

19 September 2017

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2G HTS wire: specifications

Customisation: + Variable silver thickness

+ Variable copper thickness

+ Lamination

+ Insulation

+ Solder plating

+ Low resistance splices

+ Filaments

+ … just ask

Parameter Value

Substrate Thickness 60 or 100 µm

Tape width 4 mm 6 mm 12 mm

Critical Current @ 77K, s.f. 80-150 A 120-200 A 250-500 A

Je at 4.2 K, 20 T > 400 A/mm2 > 400 A/mm2 > 400 A/mm2

Current Uniformity ±10% ±10% ±10%

19 September 2017

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Outline

2G HTS wire productiono Facility expansion

o Quality control

2G HTS wire performanceo Consistent performance without APC

o R&D into APC

HTS device projectso FCL

o Lightweight cable for aircraft

o Horizon 2020: HTS motor for aircraft

o Roebel cables

19 September 2017

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220 kV FCL for Moscow City grid

Scope• First SFCL in Russian Power Grid

• 220 kV – class

• In operation in 2018

• SuperOx manages full project

1. Superconductor

manufacturing

3. Onsite

construction

2. Engineering

and production

19 September 2017 Talk on Monday: 1LO1-02

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3.3 kV DC FCL for railway grid

Specification

Rated voltage 3.3 kV

Rated current Up to 5 kА

Limitation speed 100 ms

Resistance w/o fault 0.001 Ohm

Resistance during fault 1 Ohm

Power consumption < 6 kW

Cryo-systemClosed type,

cryocooler

Dimensions (mm) 800 х 1740 х 2100

Weight, kg 700

▪ Medium-voltage DC

▪ Retrofitted into a standard switchbox

▪Joint project with «NIIEFA-ENERGO», LLC (St.Petersburg)

19 September 2017

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HTS cable system for Airbus

Length (m)

Current (kA)

0,1

1

10

100

10 100

In this area, losses in

HTS cable are lower

than in Al or Cu

19 September 2017

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HTS motor for aircraft. Horizon 2020 consortium

19 September 2017

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Punch-and-Coat: perfect degradation/delamination stability

Coat-and-Punch: delamination on cycling occurs

S. Otten et al., SUST 28 (2015) 065014

2G HTS Roebel cables

19 September 2017

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2G HTS Roebel cables

TapeStar data on individual strand

J. Fleiter et al. CERN Internal Note 2017_15, EDMS: 1757653 35 m cable

now in Feather 2 coil at CERN

4.2 K

19 September 2017

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Outline

2G HTS wire productiono Facility expansion

o Quality control

2G HTS wire performanceo Consistent performance without APC

o R&D into APC

HTS device projectso FCL

o Lightweight cable for aircraft

o Horizon 2020: HTS motor for aircraft

o Roebel cables

19 September 2017

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THANK YOU FOR YOUR ATTENTION

www.superox.ru

19 September 2017