CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities...

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CITY OF PETALUMA POST OFFICE BOX 61 PETALUMA, CA 94953-0061 Teresa Barrett Mayor D’Lynda Fischer Mike Healy Gabe Kearney Dave King Kevin McDonnell Kathy Miller Councilmembers Public Works & Utilities City Engineer 11 English Street Petaluma, CA 94952 Phone (707) 778-4303 Environmental Services Ellis Creek – Water Recycling Facility 3890 Cypress Drive Petaluma, CA 94954 Phone (707) 776-3777 Fax (707) 656-4067 Parks & Facility Maintenance 840 Hopper St. Ext. Petaluma, CA 94952 Phone (707) 778-4303 Fax (707) 206-6065 Transit Division 555 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546 Fax (707) 206-6034 E-Mail: [email protected] May 6, 2020 To: All Planholders (via email) Petaluma Blvd South Water Main Replacement CITY PROJECT NO. C67401918 ADDENDUM NO. 1 NOTICE INVITING BIDS The following paragraphs of the Notice Inviting Bidswill be modified as described. 1. RECEIPT OF BIDS: Due to the COVID-19 Shelter in Place Order, the bids for this project will be submitted by email before 2:00PM on May 13, 2020. The emailed bid will include all of the completed documents found in the BID FORMS section of the Contract Documents. The bids will be emailed to: [email protected]. The email subject line will be Bid For Petaluma Blvd South Water Main Replacement C67401918. The response email from the City Clerk will indicate the time stamp of the bid receipt. Original copies of the Sealed Bids will be sent by standard United States Postal Service (USPS) mail services and received by the mail clerk at 11 English Street, Petaluma CA 94952. The Sealed Bids will be postmarked at USPS not later than the date of May 13, 2020. Sealed Bids postmarked after May 13, 2020, may not be considered. The Sealed Bids sent via USPS will include all of the original signed and sealed documents included in the Bid Form section of the Contract Documents. This packet will be clearly marked on the outside of the package Sealed Bid for Petaluma Blvd South Water Main Replacement Project C67401918. 2. OPENING OF BIDS: The emailed bids will be opened by the Project Manager and the City Clerk. The bids will be documented on the Bid Result template with the name of the bidding contractor and ranked by the Base Bid dollar amount. The Bid results will be posted on the Citys webpage at https://cityofpetaluma.org/bid- opportunities-2/

Transcript of CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities...

Page 1: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

CITY OF PETALUMA POST OFFICE BOX 61

PETALUMA, CA 94953-0061

Teresa Barrett

Mayor

D’Lynda Fischer Mike Healy

Gabe Kearney Dave King

Kevin McDonnell Kathy Miller

Councilmembers

Public Works & Utilities

City Engineer

11 English Street Petaluma, CA 94952

Phone (707) 778-4303

Environmental Services

Ellis Creek – Water Recycling Facility

3890 Cypress Drive Petaluma, CA 94954

Phone (707) 776-3777 Fax (707) 656-4067

Parks & Facility Maintenance

840 Hopper St. Ext. Petaluma, CA 94952

Phone (707) 778-4303 Fax (707) 206-6065

Transit Division

555 N. McDowell Blvd. Petaluma, CA 94954

Phone (707) 778-4421

Utilities & Field Operations

202 N. McDowell Blvd. Petaluma, CA 94954

Phone (707) 778-4546 Fax (707) 206-6034

E-Mail:

[email protected]

May 6, 2020

To: All Planholders (via email)

Petaluma Blvd South Water Main Replacement

CITY PROJECT NO. C67401918

ADDENDUM NO. 1

NOTICE INVITING BIDS

The following paragraphs of the “Notice Inviting Bids” will be modified as

described.

1. RECEIPT OF BIDS: Due to the COVID-19 Shelter in Place Order, the

bids for this project will be submitted by email before 2:00PM on May

13, 2020. The emailed bid will include all of the completed documents

found in the BID FORMS section of the Contract Documents. The bids

will be emailed to: [email protected]. The email subject

line will be “Bid For Petaluma Blvd South Water Main Replacement

C67401918”. The response email from the City Clerk will indicate the

time stamp of the bid receipt.

Original copies of the Sealed Bids will be sent by standard

United States Postal Service (USPS) mail services and received by

the mail clerk at 11 English Street, Petaluma CA 94952. The

Sealed Bids will be postmarked at USPS not later than the date of

May 13, 2020. Sealed Bids postmarked after May 13, 2020, may

not be considered. The Sealed Bids sent via USPS will include all

of the original signed and sealed documents included in the Bid

Form section of the Contract Documents. This packet will be

clearly marked on the outside of the package “Sealed Bid for

Petaluma Blvd South Water Main Replacement Project

C67401918”.

2. OPENING OF BIDS: The emailed bids will be opened by the

Project Manager and the City Clerk. The bids will be documented

on the Bid Result template with the name of the bidding contractor

and ranked by the Base Bid dollar amount. The Bid results will be

posted on the City’s webpage at https://cityofpetaluma.org/bid-

opportunities-2/

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CHANGES TO BID FORMS

1. A new bid schedule has been created and is part of this addendum. An additional

alternate bid item has been created for disposal of contaminated soil if encountered.

CHANGES TO SECTION IV – TECHNICAL SPECIFICATIONS

2. Refer to Section 85 – Contaminated Soils and Groundwater

Remove – entire specification section. Replace – with updated Section 85 included in this

addendum.

CHANGES TO SECTION V – PROJECT DRAWINGS

1. Refer to SHEET C4 (7 OF 13) of the Contract Drawings.

Remove -At eastern side of the intersection of H Street and Petaluma Blvd South, there is a

proposed 8-inch pipeline connecting an existing 8-inch CI pipe to an existing 4-inch CI pipe,

with construction notes to tie into existing water mains and install an 8-inch PVC PIPE. Replace

– with a 4-inch DI elbow, 4-inch PVC piping, 4-inch gate valve, and tapping sleeve around

existing 8-inch water main. A detail has been created and included with this addendum. This

work shall be included in the lump sum bid item for Tie-ins to existing main.

TECHNICAL CLARIFICATION TO CONTRACTORS – QUESTION AND RESPONSE

Question #1: Is there a geotechnical report available or report showing contaminated soils

extents and approved landfills for disposal?

Response #1: There is no geotechnical report made specifically for this project. A previous

report for a project within the project limits has been included in Appendix A. This report

should be used for informational purposes only. The extent of contaminated soils is unknown,

although historically some areas within the project limits have had contaminated soils. It is the

responsibility of the Contractor to test, store, and dispose of any contaminated soils encountered

within the project work. A new bid schedule has been created for an additional alternate bid

item for the disposal of any contaminated soil encountered during the work.

Question #2: Are the areas where the concrete paving or asphalt paving replacement is known?

Response #2: The drawing details show two methods of trench paving resurfacing, one for

where concrete is encountered, one for where only asphalt is encountered. The limits of

concrete paving are not known. The contractor should assume the concrete paving extends from

lip of gutter on each side of the street.

Page 3: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Question #3: Can the contractor discharge groundwater encountered in the trench work to the

City’s sewer system?

Response #3: The contractor may obtain a discharge permit from the City to discharge to the

sewer system, provided it meets all contaminant limit requirements.

Question #4: Does the abandonment of the 4-inch water main include filling the pipe with grout

or just plugging the ends?

Response #4: The abandonment of the 4-inch water main includes filling the pipe with grout to

the extent possible. The work shall also include removal of valve cans at the pavement level and

backfilling those areas with the appropriate pavement restoration.

SUBMITTAL CLARIFICATION TO CONTRACTORS – QUESTION AND ANSWER

Q: Can I submit the original copies of the sealed bid by FedEx, UPS, courier, other delivery

service or drop the packet off myself?

A: Due to the COVID-19 Shelter in Place Order, the City of Petaluma has closed City Hall to the

general public to continue the practice of “social distancing”. We will only accept the sealed bid

packet by the daily mail delivery of the United States Postal Service (USPS).

Q: What if the USPS delivers my original copies a week, or more, later?

A: As long as the USPS postmark on the exterior of the package shows May 13, 2020, or earlier

we will accept your original copies.

Q: What if my email doesn’t go through the internet system because the attachments have too

many megabytes?

A: You may send multiple emails to [email protected]. All emails and all

attachments must be received and acknowledged by the City Clerk’s response before 2:00PM on

May 13, 2020. All emails must be titled “Bid For Petaluma Blvd South Water Main Replacement

C67401918”.

Q: What attachment file will you accept?

A: .PDF is preferred. Other common file formats are JPG, TIF, DOC, XLS.

Q: Will you video the bid opening?

A: The bid opening will not be video taped.

Q: How am I assured that you are really choosing the lowest bid?

A: The bid packets are kept by the City Clerk for the duration of the project. After the low bid is

posted, if you want to see Bid information please call the project manager.

Q: Why are you doing it this way?

A: Due to the COVID-19 Shelter in Place Order we are trying to minimize person to person

contact as much as possible to keep everyone as healthy as possible.

Q: What if my email goes to the junk or spam folder?

Page 4: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

A: You may send a trial email in advance of the bid submittal date. Please send your email to

[email protected].

This Addendum No. 1 shall become part of the Contract and all provisions of the Contract shall

apply thereto. Bidders shall acknowledge all Addendums in the Bid Schedule.

City of Petaluma

____________________________

Dan Herrera, P.E.

P.E. No. C77596

Page 5: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Petaluma Blvd South Water Main Replacement - City Project No. C67401918

Page 1 of 3 Bid Schedule

BID SCHEDULE

Item No. Description Estimated

Quantity Unit Unit Price Total Price

1 Mobilization 1 LS

2 Traffic Control 1 LS

3 Stormwater Management and Erosion

Control

1 LS

4 Trench Shoring and Bracing 1 LS

5 Potholing 1 LS

6 8-inch C900 Water Main 1500 LF

7 8-inch Gate Valve 7 EA

8 6-inch Gate Valve 1 EA

9 Tie-In to Existing Water Mains 1 LS

10 Water Main Raise/Lower 4 EA

11 1.5-inch Water Service 51 EA

12 2-inch Water Service 31 EA

13 Abandon Existing Water Service 8 EA

14 4-inch Fire Service Assembly 4 EA

15 6-inch Fire Service Assembly 5 EA

16 8-inch Fire Service Assembly 1 EA

17 Remove and Replace Fire Hydrant

Assembly

4 EA

18 12-inch storm drain 100 LF

19 Catch Basin 1 EA

20 Abandon Existing 4” Water Main 1 LS

21 Remove and Replace Sidewalk 500 SF

22 Remove and Replace Curb & Gutter 100 LF

23 Remove and Replace Driveway 2 EA

24 Remove Existing Tree 6 EA

Base Bid $

*Note: In case of error in extension of price into the total price column, the unit price will govern.

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Petaluma Blvd South Water Main Replacement - City Project No. C67401918

Page 2 of 3 Bid Schedule

Total Amount of Bid (written in words) is:

Dollars and

Cents.

In the event of discrepancy between words and figures, the words shall prevail.

$

Figures

Base Bid $

ALTERNATE BID SCHEDULE

Item No. Description Estimated

Quantity Unit Unit Price Total Price

1. Disposal of Contaminated Soil 100 CY

Bid Alternate Total

$

*Note: In case of error in extension of price into the total price column, the unit price will govern.

Total Amount of Alternate Bid (written in words) is:

Dollars and

Cents.

In the event of discrepancy between words and figures, the words shall prevail.

$

Figures

Note: The award of the contract shall be awarded to the lowest price of the total of Base Bid

Page 7: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Petaluma Blvd South Water Main Replacement - City Project No. C67401918

Page 3 of 3 Bid Schedule

Address of Bidder Signature of Bidder

City Name of Bidder (Print)

Telephone Number of Bidder Fax Number of Bidder

Contractor’s License Number License’s Expiration Date

Addendum Acknowledgement

Addendum No. 1 Signature Acknowledging Receipt: Date:

Addendum No. 2 Signature Acknowledging Receipt: Date:

Addendum No. 3 Signature Acknowledging Receipt: Date:

Addendum No. 4 Signature Acknowledging Receipt: Date:

Page 8: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Contaminated Soil and Groundwater Section 85– Technical Specifications

SECTION 85 CONTAMINATED SOILS AND GROUNDWATER

85A. GENERAL

The CONTRACTOR shall be aware the area has a history of contaminated soils within

the project limits.

CONTRACTOR shall take all necessary precautions when working with these materials,

and all waste shall be properly and legally disposed of. The CONTRACTOR is

responsible for all testing, transport, and disposal fees.

Contaminants of concern are total petroleum hydrocarbons as diesel and motor oil,

polychlorinated biphenyls, semi-volatile organics, volatile organic compounds, CAM17

metals, and RCI. The source of petroleum appears to be either adjacent active or former

gasoline stations or surface runoff from the adjacent roadway.

All trench excavation material from trenches shall be the property of the CONTRACTOR

and shall be tested, stored, and disposed of legally. The CONTRACTOR shall dispose of

material in accordance with the applicable conditions.

85B. MEASUREMENT AND PAYMENT

Dispose of Contaminated Soil shall be paid at the bid alternate contract unit price per

Cubic Yard (CY). Payment shall be full compensation for removing, testing, storing and

disposing of contaminated soil, and shall include, but not limited to, excavation, hauling,

storing, permit approval, and any other work and incidentals included in the disposing of

contaminated soils. considered as included in prices paid under various contract items of

work included, and no additional compensation will be allowed therefor.

The actual quantity for this item of work may vary from the quantity listed in the bid

schedule. Provisions for increased or decreased quantity elsewhere in the specifications

shall not apply and no adjustments of the contract price shall be made therefore.

Disposal of Contaminated Groundwater shall be considered as included in prices paid

under various contract items of work included, and no additional compensation will be

allowed therefor.

END OF SECTION

Page 9: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546
Page 10: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

APPENDIX A

Page 11: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

P.O. Box 3039, Rohnert Park, CA 94927 Ph: (707) 792-9500 eddclarkandassociates.com Fax: (707) 792-9504

October 1, 2015 Job No.: 0778,001.15 Sanjay Mishra Senior Civil Engineer City of Petaluma 202 North McDowell Boulevard Petaluma, California 94954 Limited Pre-Construction Soil Assessment - Sewer Trunk Corridor – 2nd Street (between G Street and H Street), H Street (between 2nd Street and Petaluma Boulevard South), and Petaluma Boulevard South (between H Street and Mountain View Avenue) Petaluma, California Dear Mr. Mishra: Edd Clark & Associates, Inc., (EC&A) is pleased to present this summary report for the limited pre-construction soil assessment investigation conducted at the above-referenced corridor (Figure 1). The City of Petaluma (City) is currently designing a sewer trunk replacement for the project alignment and requested a limited pre-construction soil assessment investigation prior to conducting a full scale pre-construction soil assessment investigation. The purpose of the limited soil assessment is as follows:

• To more accurately assess potential disposal costs for bidding purposes before conducting the full pre-construction soil assessment investigation; and

• To identify soil types and possible contaminants that may be encountered during the City’s trenching activities.

EC&A submitted the July 15, 2015 Pre-Construction Soil Assessment Workplan to the City and to the County of Sonoma Department of Health Services (CSDHS) as a required condition for the issuance of a drilling permit. COMPLETED SCOPE OF WORK Work completed for this investigation included the following activities: $ Acquiring a soil boring permit from the CSDHS and an encroachment permit from the City; $ Advancing 11 borings along the project alignment;

Page 12: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

October 1, 2015 Job No.: 0778,001.15

Page 2

$ Collecting soil samples for chemical analysis and evaluation of soil lithology; $ Generating a non-native stratigraphy summary; and $ Preparing this summary report of the work completed. SUMMARY Prior to commencement of the pre-construction soil assessment, EC&A performed a review of available environmental records on the State GeoTracker Internet Database (GeoTracker) for regulated properties in the site vicinity. Based on EC&A’s past experience investigating the project vicinity and a review of information available on GeoTracker, the July 15, 2015, Pre-Construction Soil Assessment Workplan was prepared and submitted to the City and CSDHS. Based on a review of available information and EC&A’s specialized knowledge of the project area, EC&A’s workplan proposed the advancement of 11 exploratory soil borings along the project alignment. The initial alignment as proposed in EC&A’s Pre-Construction Soil Assessment Workplan originally ran from the intersection of 2nd and E Streets at its northwestern end, to the intersection of Rowan Lane and Petaluma Boulevard South at its southeastern end. At the request of the City, the alignment was shortened to run from 2nd and G Streets at its northwestern end to Mountain View Avenue at Petaluma Boulevard South at its southeastern end (Figure 1). On August 11 and 12, 2015, EC&A directed the advancement of 11 exploratory borings, which were predominantly located along the south-western side of the project alignment. Exploratory soil boring B-1 was advanced to 10 feet (ft) below ground surface (bgs), B-2 to nine ft bgs, B-3 to 10 ft bgs, B-4 and B-5 to 10 ft bgs, B-6 to 12 ft bgs, B-7 to 13 ft bgs, B-8 to eight ft bgs, and B-9 through B-11 to six ft bgs. Boring depths were selected based on the anticipated depth of the proposed trench, as provided by the City. A non-native stratigraphy summary is attached as Appendix A. Soil boring logs are included in Appendix B. Groundwater was not encountered in any of the borings advanced during this investigation. EC&A collected four discrete soil samples from each boring; the discrete samples were composited by the laboratory prior to chemical analyses. Based on a review of the laboratory analytical results, and of Bulletin 100 for Republic Services’ Sonoma Central Landfill waste acceptance criteria, if soils encountered during the subsequent proposed full pre-construction soils assessment indicate similar analytical results to those reported herein, EC&A expects that the soils would be eligible for disposal at Republic Services’ Sonoma Central Landfill. REGULATORY FILE REVIEWS Soil Boring Placement A review of available information on GeoTracker, in addition to EC&A’s knowledge of the project vicinity, revealed the following properties as having the potential to impact soil and/or groundwater along the entire project alignment:

Page 13: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

October 1, 2015 Job No.: 0778,001.15

Page 3

• Open Leaking Underground Storage Tank facility (LUST) - Bar Ale Inc., 225 2nd Street; • Open LUST - Former Unocal #6152, 201 Petaluma Boulevard South; • Closed LUST - Hlebackos & Sons Trucking, 1473 Petaluma Boulevard South; • Closed LUST - Lee’s Truck & Auto Repair, 301 2nd Street; • Closed LUST - Petaluma Recycling Center, 315 2nd Street; • Closed LUST - Barber Sign Company, 321 2nd Street; • Closed LUST - D&M Automotive, 210 F Street; • Closed LUST - Metcalf’s Auto Parts, 494 2nd Street; • Closed LUST - Foundry Wharf Business Park, 615 2nd Street; • Open LUST - Andy’s Auto Repair, 619 Petaluma Boulevard South; • Closed Historical-UST - Van Bebber Bros, 729 Petaluma Boulevard South; and • Closed LUST - Mahoney Davison Property, 929 Petaluma Boulevard South.

The information obtained from a review of files for the properties listed above, in addition to the waste acceptance requirements from proposed future landfills was used to design the scope of work. Details of the limited pre-construction soils assessment investigation are presented below. LIMITED PRE-CONSTRUCTION SOILS ASSESSMENT INVESTIGATION Pre-field Activities Prior to drilling activities, EC&A reviewed utility maps provided by the City. Boring locations were based on a thorough review of available information of GeoTracker for LUST sites and other regulated sites in the vicinity of the sewer main alignment. Boring depths were selected based on the anticipated depth of the proposed trench, as provided by the City. The initial alignment as proposed in EC&A’s Pre-Construction Soil Assessment Workplan originally ran from the intersection of 2nd and E Streets at its northwestern end, to the intersection of Rowan Lane and Petaluma Boulevard South at its southeastern end. At the request of the City, the alignment was shortened to run from 2nd and G Streets at its northwestern end to Mountain View Avenue at Petaluma Boulevard South at its southeastern end (Figure 1). With the assistance of the City, proposed boring locations were marked at the site for Underground Service Alert (USA). EC&A contacted Underground Service Alert (USA) at least 48 hours prior to drilling activities to locate underground utilities within the proposed investigation area. EC&A notified the City and CSDHS prior to the start of field work. Boring permit #SR0013004 was obtained from the CSDHS. Encroachment permit #PWEN-15-1183 was obtained from the City. Copies of the permits are included in Appendix C.

Page 14: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

October 1, 2015 Job No.: 0778,001.15

Page 4

Field Activities On August 11 and 12, 2015, EC&A oversaw the advancement of 11 exploratory borings along the project alignment. The locations of the borings are as shown on Figure 1. Exploratory soil boring B-1 was advanced to 10 ft bgs, B-2 to nine ft bgs, B-3 to 10 ft bgs, B-4 to 10 ft bgs, B-5 to 10 ft bgs, B-6 to 12 ft bgs, B-7 to 13 ft bgs, B-8 to eight ft bgs, and B-9, B-10 and B-11 to six ft bgs each. Boring logs describing soil lithology encountered in each well boring are included in Appendix B. Drilling services were provided by Clear Heart Drilling, Inc., of Santa Rosa, California (C-57 license #780357). Soil borings were advanced using a truck-mounted drill rig equipped with GeoProbe™ direct-push drilling equipment. Drilling was performed under the technical direction of an EC&A field geologist who classified the soils encountered, maintained a continuous log of the lithology, and assisted in collecting soil samples. All field work was performed under the supervision of a California registered geologist. EC&A personnel field screened the breathing zone and soil samples for organic vapors with a photoionization detector (PID). As a condition of the encroachment permit and to ensure the safety of all personnel along the project alignment, EC&A contracted with Statewide Traffic Safety & Signs (Statewide) to provide traffic safety services during the field work. Soil In borings B-1, B-2 and B-11, six inches (0.5 feet) of asphalt was observed; no concrete was observed beneath the asphalt layer in these three borings. In the remaining eight borings advanced during this investigation, asphalt was generally observed from the ground surface to a maximum depth of 0.25 ft bgs, underlain by concrete to a maximum depth of 0.58 feet bgs (borings B-3 and B-9). Base rock/fill was observed from approximately 0.5 feet bgs to depths ranging from approximately 0.58 feet bgs to an estimated depth of 2.5 feet bgs (boring B-5). Only a very thin fill layer was observed in boring B-6 (approximately 1 inch from 0.5 to 0.58 feet bgs). Fill was not observed in borings B-7, B-9 and B-10.

Materials observed deeper than the fill consisted of low and high plasticity clays, sandy clays, silty clays, silts, silt with sand, silt with sand and gravel, clayey silt, and silt with gravel. Groundwater Groundwater was not encountered in any of the borings advanced during this investigation; however, groundwater has been measured as shallow as 0.5 ft bgs in monitoring wells at regulated sites located along the project alignment. Soil Sampling Procedures Soil samples were collected from each boring by pushing a sampler lined with a 4-ft-long by 2.125-inch-diameter butyrate sample sleeve into the soil at the bottom of the borehole. Soil samples selected

Page 15: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

October 1, 2015 Job No.: 0778,001.15

Page 5

for laboratory analysis were cut from the butyrate liner, capped, labeled, logged on a chain-of-custody form and placed on ice for transport to McCampbell Analytical, Inc. (MAI) for the required analyses. MAI is a State-certified laboratory located in Pittsburg, California. EC&A collected four discrete soil samples from each of the eleven exploratory soil borings for laboratory analysis. The discrete samples from each boring were composited by the laboratory prior to chemical analyses. Soil Sample Analyses The composited soil samples were analyzed for TPH multi scan with silica gel clean-up by Method 8015B, for volatile organic compounds (VOCs) by Method 8260B, and for LUFT 5 Metals by Method 200.8. Analyses were performed on standard five-day turnaround. Analytical results from composited samples collected from B-1 through B-11 meet Republic Services’ Waste Acceptance Criteria for disposal at Sonoma Central landfill. Soil analytical results are summarized on Tables 1 and 2. Laboratory analytical reports are included in Appendix D. Waste On August 11 and 12, 2015, at the request of the City, EC&A transported one, 55-gallon UN/DOT drum of soil cuttings to their corporate yard and added the soil cuttings to an existing stockpile of soil, pending subsequent profiling and disposal. Disposal documentation will be forwarded upon receipt. CONCLUSIONS None of the constituents of concern detected in the soil samples collected during this limited pre-construction soil assessment exceeded Republic Services’ Sonoma Central Landfill Refuse Bulletin No. 100 Soil Acceptance Criteria (Tables 1 and 2). Based on a review of the laboratory analytical results, and of Bulletin 100 for Republic Services’ Sonoma Central Landfill waste acceptance criteria, if soils encountered during the subsequent proposed full pre-construction soils assessment indicate similar analytical results to those reported herein, EC&A expects that the soils would be eligible for disposal at Republic Services’ Sonoma Central Landfill. The historical releases from LUST facilities along the project alignment investigated during the limited pre-construction soil assessment investigation do not appear to have impacted soils at the boring locations tested and the alignment of the proposed sewer line trench.

Page 16: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546
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Petaluma Blvd South

Explanation

!H Approximate Boring Location

City Proposed Project Alignment

Lee's Truck & Auto Repair (Closed LUST)

301 2nd St

D & M Automotive (Closed LUST)

210 F St

Foundry Wharf Bus. Park (Closed LUST)

615 2nd St

Job Number Reviewed By Date Revised DatePW-478.15 EC&A, KC April 2015

F S

tF S

t

H S

tH

St

I S

tI S

t

K S

tK

St

Mounta

in V

iew

Ave

Mounta

in V

iew

Ave

5th St

5th St

4th St

4th St

2nd St

2nd St

Rovin

a L

nR

ovin

a L

n

MMccNNeeaarr CCiirr

PPeettaalluummaa

RRiivveerr

Petaluma Recycling Center (Closed LUST)315 2nd St

Metcalf's Auto Parts (Closed LUSTs)

494 2nd St

Van Bebber Bros (Closed in-place Hist-UST)

729 Petaluma Blvd S

Mahoney Davison Property (Closed LUST)929 Petaluma Blvd S

Barber Sign Company, Inc. (Closed LUST)

321 2nd St

Andy's Auto Repair (Open LUST)619 Petaluma Blvd S

2nd St

2nd St

D S

tD

St

Bar Ale Inc (Open LUST)225 2nd Street

Sonoma County

Petaluma

Notes:

-Gray label font represents sites that have no associated data.

-B1 through B-4 will be drilled to 16 feet bgs, B-5 through B-7 to 15 feet bgs, B-8 through B-10 to 14 feet bgs, and B-11 to 13 feet bgs.

-Each boring represents 100 cubic yards; the borings shown in in sets of three are approximately 35 feet apart.

-Four discrete samples will be collected from each boring to be lab composited as a four-point sample set representing the full length of each boring.

Gray

Former Unocal #6152 (Open LUST)201 Petaluma Blvd S

G S

tG

St

Hlebakos & Sons Trucking (Closed LUST)1473 Petaluma Blvd S

JOB NUMBER DATE REVISED DATE

FIGURE

EC&A, Kevin CokerREVIEWED BY

July 20150778,001.15

1

SITE MAPwith Boring Locations for City Sewer Line Investigation,

11-12 August 2015Petaluma Blvd South CorridorPetaluma, California

(TR

ACE

#155

5, 0

1 N

ov ‘1

5) EDD CLARK & ASSOCIATES, INC.ENVIRONMENTAL C O N S U L T A N T S

PAGE OF1 1

FIGU

RE

1

PAGE O

F1

1

November 2015

N

0 500

feet(approximate scale)

Notes: Gray label font represents sites that have no associated data. B-1, B-3, B-4 and B-5 were drilled to 10 ft bgs; B-2 to 9 ft bgs, B-6 to 12 ft bgs, B-7 to 13 ft bgs, and B-8 to 8 ft bgs; B-9, B-10 and B-11 to 6 ft bgs. Each boring represents 100 cu.yds; borings shown in sets of three are ~60 ft apart. Four discrete samples were collected from each boring and lab composited as a four-point sample set representing the full length of each boring.

Boring Location (approx.)City Project Alignment (revised)Original City Project Alignment (proposed)

B-1

B-2

B-3

B-10

B-9B-8

B-7

B-6

B-5B-4

B-11

Page 18: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546
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Table 2Petaluma Boulevard S Page 1 of 1

Cadmium Chromium (total) Lead Nickel Zinc

B-1 COMP 08/12/15 ND <0.25 85 6.9 94 55B-2 COMP 08/12/15 ND <0.25 74 5.7 90 39B-3 COMP 08/11/15 ND <0.25 56 6.1 76 31B-4 COMP 08/11/15 ND <0.25 69 10 69 34B-5 COMP 08/11/15 ND <0.25 52 5.5 61 27B-6 COMP 08/11/15 ND <0.25 68 5.6 100 36B-7 COMP 08/11/15 ND <0.25 71 4.5 85 33B-8 COMP 08/11/15 ND <0.25 68 6.3 51 31B-9 COMP 08/12/15 ND <0.25 86 5.9 57 34B-10 COMP 08/12/15 ND <0.25 83 6.4 57 34B-11 COMP 08/12/15 ND <0.25 64 6.7 37 32

100 2,500 350 2,000 5,000

Notes:mg/kg: milligrams per kilogramND: Not detected above the laboratory reporting limitCOMP: Composite. All analyzed soil samples were composites of four separate soil samples collected from

each boring.All samples analyzed by McCampbell Analytical, Inc., Pittsburg, CaliforniaAnalyzed for LUFT 5 metals by Analytical Method SW6020

Sonoma Central = Republic Services' Sonoma Central Landfill Refuse Bulletin No. 100 Soil Acceptance Criteria

Sonoma Central

Mountain View Avenue)

Table 2: Exploratory Soil Boring Analytical Results

2nd Street (between G Street and H Street),

Sample ID Sample Datemilligrams per kilogram (mg/kg)

LUFT 5 MetalsPetaluma Boulevard South Alignment

H Street (between 2nd Street and Petaluma Boulevard South),and Petaluma Boulevard South (between H Street and

Petaluma, California

Page 20: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Appendix A

Non-native Stratigraphy

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´0 500

feet

Ash

lee

Lle

we

llyn

, 4

/7/1

5, S

:\G

IS\P

roje

cts

\Fe

eE

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PW

47

8_

15

Pre

Co

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idP

etB

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S\F

ig1

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RE

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reC

on

Site

Lo

ca

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FIGURE

1

Petaluma Blvd S Corridor

Petaluma, CaliforniaCalifornia

Sonoma County

Petaluma

Site

£¤101

UV116

SITE LOCATION MAP

with Proposed Boring Locations

for Limited Pre-Construction Hazardous Materials Investigation

E S

tE

St

Petaluma Blvd South

Petaluma Blvd South

Explanation

!H Approximate Boring Location

City Proposed Project Alignment

Lee's Truck & Auto Repair (Closed LUST)

301 2nd St

D & M Automotive (Closed LUST)

210 F St

Foundry Wharf Bus. Park (Closed LUST)

615 2nd St

Job Number Reviewed By Date Revised DatePW-478.15 EC&A, KC April 2015

F S

tF S

t

H S

tH

St

I S

tI S

t

K S

tK

St

Mounta

in V

iew

Ave

Mounta

in V

iew

Ave

5th St

5th St

4th St

4th St

2nd St

2nd St

Rovin

a L

nR

ovin

a L

n

MMccNNeeaarr CCiirr

PPeettaalluummaa

RRiivveerr

Petaluma Recycling Center (Closed LUST)315 2nd St

Metcalf's Auto Parts (Closed LUSTs)

494 2nd St

Van Bebber Bros (Closed in-place Hist-UST)

729 Petaluma Blvd S

Mahoney Davison Property (Closed LUST)929 Petaluma Blvd S

Barber Sign Company, Inc. (Closed LUST)

321 2nd St

Andy's Auto Repair (Open LUST)619 Petaluma Blvd S

2nd St

2nd St

D S

tD

St

Bar Ale Inc (Open LUST)225 2nd Street

Sonoma County

Petaluma

Notes:

-Gray label font represents sites that have no associated data.

-B1 through B-4 will be drilled to 16 feet bgs, B-5 through B-7 to 15 feet bgs, B-8 through B-10 to 14 feet bgs, and B-11 to 13 feet bgs.

-Each boring represents 100 cubic yards; the borings shown in in sets of three are approximately 35 feet apart.

-Four discrete samples will be collected from each boring to be lab composited as a four-point sample set representing the full length of each boring.

Gray

Former Unocal #6152 (Open LUST)201 Petaluma Blvd S

G S

tG

St

Hlebakos & Sons Trucking (Closed LUST)1473 Petaluma Blvd S

JOB NUMBER DATE REVISED DATE

FIGURE

EC&A, Kevin CokerREVIEWED BY

July 20150778,001.15

1

SITE MAPwith Boring Locations for City Sewer Line Investigation,

11-12 August 2015Petaluma Blvd South CorridorPetaluma, California

(TR

ACE

#155

5, 0

1 N

ov ‘1

5) EDD CLARK & ASSOCIATES, INC.ENVIRONMENTAL C O N S U L T A N T S

PAGE OF1 1

FIGU

RE

1

PAGE O

F1

1

November 2015

N

0 500

feet(approximate scale)

Notes: Gray label font represents sites that have no associated data. B-1, B-3, B-4 and B-5 were drilled to 10 ft bgs; B-2 to 9 ft bgs, B-6 to 12 ft bgs, B-7 to 13 ft bgs, and B-8 to 8 ft bgs; B-9, B-10 and B-11 to 6 ft bgs. Each boring represents 100 cu.yds; borings shown in sets of three are ~60 ft apart. Four discrete samples were collected from each boring and lab composited as a four-point sample set representing the full length of each boring.

Boring Location (approx.)City Project Alignment (revised)Original City Project Alignment (proposed)

B-1

B-2

B-3

B-10

B-9B-8

B-7

B-6

B-5B-4

B-11

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Appendix D

Laboratory Analytical Reports

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WorkOrder:

Report Created for: Edd Clark & Associates, Inc.

320 Professional Center Ste. 215Rohnert Park, CA 94928

Project Contact: Christopher Houlihan

Project Name: 0778,001.15; Limited Pre-Con Soil AssessmentProject P.O.:

Project Received: 08/12/2015

Analytical Report reviewed & approved for release on 08/19/2015 by:

Angela Rydelius,Laboratory Manager

1508393

The report shall not be reproduced except in full, without the written approval of the laboratory.

The analytical results relate only to the items tested. Results reported conform to the most

current NELAP standards, where applicable, unless otherwise stated in the case narrative.

Analytical Report

1534 Willow Pass Rd. Pittsburg, CA 94565 ♦ TEL: (877) 252-9262 ♦ FAX: (925) 252-9269 ♦ www.mccampbell.comNELAP: 4033ORELAP ♦ ELAP: 1644 ♦ ISO/IEC: 17025:2005 ♦ WSDE: C972-11 ♦ ADEC: UST-098 ♦ UCMR3

McCampbell Analytical, Inc."When Quality Counts"

Page 1 of 40

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Glossary of Terms & Qualifier Definitions

Client: Edd Clark & Associates, Inc.Project: 0778,001.15; Limited Pre-Con Soil AssessmentWorkOrder: 1508393

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Glossary Abbreviation

95% Interval 95% Confident IntervalDF Dilution FactorDI WET (DISTLC) Waste Extraction Test using DI waterDISS Dissolved (direct analysis of 0.45 µm filtered and acidified water sample)DUP DuplicateEDL Estimated Detection LimitITEF International Toxicity Equivalence FactorLCS Laboratory Control SampleMB Method BlankMB % Rec % Recovery of Surrogate in Method Blank, if applicableMDL Method Detection LimitML Minimum Level of QuantitationMS Matrix SpikeMSD Matrix Spike DuplicateN/A Not ApplicableND Not detected at or above the indicated MDL or RLNR Data Not Reported due to matrix interference or insufficient sample amount.PF Prep FactorRD Relative DifferenceRL Reporting Limit (The RL is the lowest calibration standard in a multipoint calibration.)RPD Relative Percent DeviationRRT Relative Retention TimeSPK Val Spike ValueSPKRef Val Spike Reference ValueSPLP Synthetic Precipitation Leachate ProcedureTCLP Toxicity Characteristic Leachate ProcedureTEQ Toxicity EquivalentsWET (STLC) Waste Extraction Test (Soluble Threshold Limit Concentration)

Analytical Qualifiers

e2 diesel range compounds are significant; no recognizable patterne7 oil range compounds are significant

Page 2 of 40

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Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-3 COMP 1508393-001A Soil 08/11/2015 09:05 GC10 108899

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Acetone ND 0.10 1 08/15/2015 00:26tert-Amyl methyl ether (TAME) ND 0.0050 1 08/15/2015 00:26Benzene ND 0.0050 1 08/15/2015 00:26Bromobenzene ND 0.0050 1 08/15/2015 00:26Bromochloromethane ND 0.0050 1 08/15/2015 00:26Bromodichloromethane ND 0.0050 1 08/15/2015 00:26Bromoform ND 0.0050 1 08/15/2015 00:26Bromomethane ND 0.0050 1 08/15/2015 00:262-Butanone (MEK) ND 0.020 1 08/15/2015 00:26t-Butyl alcohol (TBA) ND 0.050 1 08/15/2015 00:26n-Butyl benzene ND 0.0050 1 08/15/2015 00:26sec-Butyl benzene ND 0.0050 1 08/15/2015 00:26tert-Butyl benzene ND 0.0050 1 08/15/2015 00:26Carbon Disulfide ND 0.0050 1 08/15/2015 00:26Carbon Tetrachloride ND 0.0050 1 08/15/2015 00:26Chlorobenzene ND 0.0050 1 08/15/2015 00:26Chloroethane ND 0.0050 1 08/15/2015 00:26Chloroform ND 0.0050 1 08/15/2015 00:26Chloromethane ND 0.0050 1 08/15/2015 00:262-Chlorotoluene ND 0.0050 1 08/15/2015 00:264-Chlorotoluene ND 0.0050 1 08/15/2015 00:26Dibromochloromethane ND 0.0050 1 08/15/2015 00:261,2-Dibromo-3-chloropropane ND 0.0040 1 08/15/2015 00:261,2-Dibromoethane (EDB) ND 0.0040 1 08/15/2015 00:26Dibromomethane ND 0.0050 1 08/15/2015 00:261,2-Dichlorobenzene ND 0.0050 1 08/15/2015 00:261,3-Dichlorobenzene ND 0.0050 1 08/15/2015 00:261,4-Dichlorobenzene ND 0.0050 1 08/15/2015 00:26Dichlorodifluoromethane ND 0.0050 1 08/15/2015 00:261,1-Dichloroethane ND 0.0050 1 08/15/2015 00:261,2-Dichloroethane (1,2-DCA) ND 0.0040 1 08/15/2015 00:261,1-Dichloroethene ND 0.0050 1 08/15/2015 00:26cis-1,2-Dichloroethene ND 0.0050 1 08/15/2015 00:26trans-1,2-Dichloroethene ND 0.0050 1 08/15/2015 00:261,2-Dichloropropane ND 0.0050 1 08/15/2015 00:261,3-Dichloropropane ND 0.0050 1 08/15/2015 00:262,2-Dichloropropane ND 0.0050 1 08/15/2015 00:26

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 3 of 40

Page 47: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-3 COMP 1508393-001A Soil 08/11/2015 09:05 GC10 108899

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

1,1-Dichloropropene ND 0.0050 1 08/15/2015 00:26cis-1,3-Dichloropropene ND 0.0050 1 08/15/2015 00:26trans-1,3-Dichloropropene ND 0.0050 1 08/15/2015 00:26Diisopropyl ether (DIPE) ND 0.0050 1 08/15/2015 00:26Ethylbenzene ND 0.0050 1 08/15/2015 00:26Ethyl tert-butyl ether (ETBE) ND 0.0050 1 08/15/2015 00:26Freon 113 ND 0.0050 1 08/15/2015 00:26Hexachlorobutadiene ND 0.0050 1 08/15/2015 00:26Hexachloroethane ND 0.0050 1 08/15/2015 00:262-Hexanone ND 0.0050 1 08/15/2015 00:26Isopropylbenzene ND 0.0050 1 08/15/2015 00:264-Isopropyl toluene ND 0.0050 1 08/15/2015 00:26Methyl-t-butyl ether (MTBE) ND 0.0050 1 08/15/2015 00:26Methylene chloride ND 0.0050 1 08/15/2015 00:264-Methyl-2-pentanone (MIBK) ND 0.0050 1 08/15/2015 00:26Naphthalene ND 0.0050 1 08/15/2015 00:26n-Propyl benzene ND 0.0050 1 08/15/2015 00:26Styrene ND 0.0050 1 08/15/2015 00:261,1,1,2-Tetrachloroethane ND 0.0050 1 08/15/2015 00:261,1,2,2-Tetrachloroethane ND 0.0050 1 08/15/2015 00:26Tetrachloroethene ND 0.0050 1 08/15/2015 00:26Toluene ND 0.0050 1 08/15/2015 00:261,2,3-Trichlorobenzene ND 0.0050 1 08/15/2015 00:261,2,4-Trichlorobenzene ND 0.0050 1 08/15/2015 00:261,1,1-Trichloroethane ND 0.0050 1 08/15/2015 00:261,1,2-Trichloroethane ND 0.0050 1 08/15/2015 00:26Trichloroethene ND 0.0050 1 08/15/2015 00:26Trichlorofluoromethane ND 0.0050 1 08/15/2015 00:261,2,3-Trichloropropane ND 0.0050 1 08/15/2015 00:261,2,4-Trimethylbenzene ND 0.0050 1 08/15/2015 00:261,3,5-Trimethylbenzene ND 0.0050 1 08/15/2015 00:26Vinyl Chloride ND 0.0050 1 08/15/2015 00:26Xylenes, Total ND 0.0050 1 08/15/2015 00:26

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 4 of 40

Page 48: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-3 COMP 1508393-001A Soil 08/11/2015 09:05 GC10 108899

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Surrogates REC (%) Limits

Analyst(s): KF

Dibromofluoromethane 113 70-130 08/15/2015 00:26Toluene-d8 104 70-130 08/15/2015 00:264-BFB 118 70-130 08/15/2015 00:26Benzene-d6 92 60-140 08/15/2015 00:26Ethylbenzene-d10 106 60-140 08/15/2015 00:261,2-DCB-d4 87 60-140 08/15/2015 00:26

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 5 of 40

Page 49: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-4 COMP 1508393-002A Soil 08/11/2015 10:00 GC10 108899

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Acetone ND 0.10 1 08/15/2015 01:08tert-Amyl methyl ether (TAME) ND 0.0050 1 08/15/2015 01:08Benzene ND 0.0050 1 08/15/2015 01:08Bromobenzene ND 0.0050 1 08/15/2015 01:08Bromochloromethane ND 0.0050 1 08/15/2015 01:08Bromodichloromethane ND 0.0050 1 08/15/2015 01:08Bromoform ND 0.0050 1 08/15/2015 01:08Bromomethane ND 0.0050 1 08/15/2015 01:082-Butanone (MEK) ND 0.020 1 08/15/2015 01:08t-Butyl alcohol (TBA) ND 0.050 1 08/15/2015 01:08n-Butyl benzene ND 0.0050 1 08/15/2015 01:08sec-Butyl benzene ND 0.0050 1 08/15/2015 01:08tert-Butyl benzene ND 0.0050 1 08/15/2015 01:08Carbon Disulfide ND 0.0050 1 08/15/2015 01:08Carbon Tetrachloride ND 0.0050 1 08/15/2015 01:08Chlorobenzene ND 0.0050 1 08/15/2015 01:08Chloroethane ND 0.0050 1 08/15/2015 01:08Chloroform ND 0.0050 1 08/15/2015 01:08Chloromethane ND 0.0050 1 08/15/2015 01:082-Chlorotoluene ND 0.0050 1 08/15/2015 01:084-Chlorotoluene ND 0.0050 1 08/15/2015 01:08Dibromochloromethane ND 0.0050 1 08/15/2015 01:081,2-Dibromo-3-chloropropane ND 0.0040 1 08/15/2015 01:081,2-Dibromoethane (EDB) ND 0.0040 1 08/15/2015 01:08Dibromomethane ND 0.0050 1 08/15/2015 01:081,2-Dichlorobenzene ND 0.0050 1 08/15/2015 01:081,3-Dichlorobenzene ND 0.0050 1 08/15/2015 01:081,4-Dichlorobenzene ND 0.0050 1 08/15/2015 01:08Dichlorodifluoromethane ND 0.0050 1 08/15/2015 01:081,1-Dichloroethane ND 0.0050 1 08/15/2015 01:081,2-Dichloroethane (1,2-DCA) ND 0.0040 1 08/15/2015 01:081,1-Dichloroethene ND 0.0050 1 08/15/2015 01:08cis-1,2-Dichloroethene ND 0.0050 1 08/15/2015 01:08trans-1,2-Dichloroethene ND 0.0050 1 08/15/2015 01:081,2-Dichloropropane ND 0.0050 1 08/15/2015 01:081,3-Dichloropropane ND 0.0050 1 08/15/2015 01:082,2-Dichloropropane ND 0.0050 1 08/15/2015 01:08

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 6 of 40

Page 50: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-4 COMP 1508393-002A Soil 08/11/2015 10:00 GC10 108899

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

1,1-Dichloropropene ND 0.0050 1 08/15/2015 01:08cis-1,3-Dichloropropene ND 0.0050 1 08/15/2015 01:08trans-1,3-Dichloropropene ND 0.0050 1 08/15/2015 01:08Diisopropyl ether (DIPE) ND 0.0050 1 08/15/2015 01:08Ethylbenzene ND 0.0050 1 08/15/2015 01:08Ethyl tert-butyl ether (ETBE) ND 0.0050 1 08/15/2015 01:08Freon 113 ND 0.0050 1 08/15/2015 01:08Hexachlorobutadiene ND 0.0050 1 08/15/2015 01:08Hexachloroethane ND 0.0050 1 08/15/2015 01:082-Hexanone ND 0.0050 1 08/15/2015 01:08Isopropylbenzene ND 0.0050 1 08/15/2015 01:084-Isopropyl toluene ND 0.0050 1 08/15/2015 01:08Methyl-t-butyl ether (MTBE) ND 0.0050 1 08/15/2015 01:08Methylene chloride ND 0.0050 1 08/15/2015 01:084-Methyl-2-pentanone (MIBK) ND 0.0050 1 08/15/2015 01:08Naphthalene ND 0.0050 1 08/15/2015 01:08n-Propyl benzene ND 0.0050 1 08/15/2015 01:08Styrene ND 0.0050 1 08/15/2015 01:081,1,1,2-Tetrachloroethane ND 0.0050 1 08/15/2015 01:081,1,2,2-Tetrachloroethane ND 0.0050 1 08/15/2015 01:08Tetrachloroethene ND 0.0050 1 08/15/2015 01:08Toluene ND 0.0050 1 08/15/2015 01:081,2,3-Trichlorobenzene ND 0.0050 1 08/15/2015 01:081,2,4-Trichlorobenzene ND 0.0050 1 08/15/2015 01:081,1,1-Trichloroethane ND 0.0050 1 08/15/2015 01:081,1,2-Trichloroethane ND 0.0050 1 08/15/2015 01:08Trichloroethene ND 0.0050 1 08/15/2015 01:08Trichlorofluoromethane ND 0.0050 1 08/15/2015 01:081,2,3-Trichloropropane ND 0.0050 1 08/15/2015 01:081,2,4-Trimethylbenzene ND 0.0050 1 08/15/2015 01:081,3,5-Trimethylbenzene ND 0.0050 1 08/15/2015 01:08Vinyl Chloride ND 0.0050 1 08/15/2015 01:08Xylenes, Total ND 0.0050 1 08/15/2015 01:08

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 7 of 40

Page 51: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-4 COMP 1508393-002A Soil 08/11/2015 10:00 GC10 108899

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Surrogates REC (%) Limits

Analyst(s): KF

Dibromofluoromethane 113 70-130 08/15/2015 01:08Toluene-d8 103 70-130 08/15/2015 01:084-BFB 118 70-130 08/15/2015 01:08Benzene-d6 92 60-140 08/15/2015 01:08Ethylbenzene-d10 106 60-140 08/15/2015 01:081,2-DCB-d4 88 60-140 08/15/2015 01:08

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 8 of 40

Page 52: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-5 COMP 1508393-003A Soil 08/11/2015 10:44 GC10 108899

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Acetone ND 0.10 1 08/15/2015 01:49tert-Amyl methyl ether (TAME) ND 0.0050 1 08/15/2015 01:49Benzene ND 0.0050 1 08/15/2015 01:49Bromobenzene ND 0.0050 1 08/15/2015 01:49Bromochloromethane ND 0.0050 1 08/15/2015 01:49Bromodichloromethane ND 0.0050 1 08/15/2015 01:49Bromoform ND 0.0050 1 08/15/2015 01:49Bromomethane ND 0.0050 1 08/15/2015 01:492-Butanone (MEK) ND 0.020 1 08/15/2015 01:49t-Butyl alcohol (TBA) ND 0.050 1 08/15/2015 01:49n-Butyl benzene ND 0.0050 1 08/15/2015 01:49sec-Butyl benzene ND 0.0050 1 08/15/2015 01:49tert-Butyl benzene ND 0.0050 1 08/15/2015 01:49Carbon Disulfide ND 0.0050 1 08/15/2015 01:49Carbon Tetrachloride ND 0.0050 1 08/15/2015 01:49Chlorobenzene ND 0.0050 1 08/15/2015 01:49Chloroethane ND 0.0050 1 08/15/2015 01:49Chloroform ND 0.0050 1 08/15/2015 01:49Chloromethane ND 0.0050 1 08/15/2015 01:492-Chlorotoluene ND 0.0050 1 08/15/2015 01:494-Chlorotoluene ND 0.0050 1 08/15/2015 01:49Dibromochloromethane ND 0.0050 1 08/15/2015 01:491,2-Dibromo-3-chloropropane ND 0.0040 1 08/15/2015 01:491,2-Dibromoethane (EDB) ND 0.0040 1 08/15/2015 01:49Dibromomethane ND 0.0050 1 08/15/2015 01:491,2-Dichlorobenzene ND 0.0050 1 08/15/2015 01:491,3-Dichlorobenzene ND 0.0050 1 08/15/2015 01:491,4-Dichlorobenzene ND 0.0050 1 08/15/2015 01:49Dichlorodifluoromethane ND 0.0050 1 08/15/2015 01:491,1-Dichloroethane ND 0.0050 1 08/15/2015 01:491,2-Dichloroethane (1,2-DCA) ND 0.0040 1 08/15/2015 01:491,1-Dichloroethene ND 0.0050 1 08/15/2015 01:49cis-1,2-Dichloroethene ND 0.0050 1 08/15/2015 01:49trans-1,2-Dichloroethene ND 0.0050 1 08/15/2015 01:491,2-Dichloropropane ND 0.0050 1 08/15/2015 01:491,3-Dichloropropane ND 0.0050 1 08/15/2015 01:492,2-Dichloropropane ND 0.0050 1 08/15/2015 01:49

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 9 of 40

Page 53: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-5 COMP 1508393-003A Soil 08/11/2015 10:44 GC10 108899

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

1,1-Dichloropropene ND 0.0050 1 08/15/2015 01:49cis-1,3-Dichloropropene ND 0.0050 1 08/15/2015 01:49trans-1,3-Dichloropropene ND 0.0050 1 08/15/2015 01:49Diisopropyl ether (DIPE) ND 0.0050 1 08/15/2015 01:49Ethylbenzene ND 0.0050 1 08/15/2015 01:49Ethyl tert-butyl ether (ETBE) ND 0.0050 1 08/15/2015 01:49Freon 113 ND 0.0050 1 08/15/2015 01:49Hexachlorobutadiene ND 0.0050 1 08/15/2015 01:49Hexachloroethane ND 0.0050 1 08/15/2015 01:492-Hexanone ND 0.0050 1 08/15/2015 01:49Isopropylbenzene ND 0.0050 1 08/15/2015 01:494-Isopropyl toluene ND 0.0050 1 08/15/2015 01:49Methyl-t-butyl ether (MTBE) ND 0.0050 1 08/15/2015 01:49Methylene chloride ND 0.0050 1 08/15/2015 01:494-Methyl-2-pentanone (MIBK) ND 0.0050 1 08/15/2015 01:49Naphthalene ND 0.0050 1 08/15/2015 01:49n-Propyl benzene ND 0.0050 1 08/15/2015 01:49Styrene ND 0.0050 1 08/15/2015 01:491,1,1,2-Tetrachloroethane ND 0.0050 1 08/15/2015 01:491,1,2,2-Tetrachloroethane ND 0.0050 1 08/15/2015 01:49Tetrachloroethene ND 0.0050 1 08/15/2015 01:49Toluene ND 0.0050 1 08/15/2015 01:491,2,3-Trichlorobenzene ND 0.0050 1 08/15/2015 01:491,2,4-Trichlorobenzene ND 0.0050 1 08/15/2015 01:491,1,1-Trichloroethane ND 0.0050 1 08/15/2015 01:491,1,2-Trichloroethane ND 0.0050 1 08/15/2015 01:49Trichloroethene ND 0.0050 1 08/15/2015 01:49Trichlorofluoromethane ND 0.0050 1 08/15/2015 01:491,2,3-Trichloropropane ND 0.0050 1 08/15/2015 01:491,2,4-Trimethylbenzene ND 0.0050 1 08/15/2015 01:491,3,5-Trimethylbenzene ND 0.0050 1 08/15/2015 01:49Vinyl Chloride ND 0.0050 1 08/15/2015 01:49Xylenes, Total ND 0.0050 1 08/15/2015 01:49

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 10 of 40

Page 54: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-5 COMP 1508393-003A Soil 08/11/2015 10:44 GC10 108899

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Surrogates REC (%) Limits

Analyst(s): KF

Dibromofluoromethane 113 70-130 08/15/2015 01:49Toluene-d8 101 70-130 08/15/2015 01:494-BFB 109 70-130 08/15/2015 01:49Benzene-d6 90 60-140 08/15/2015 01:49Ethylbenzene-d10 105 60-140 08/15/2015 01:491,2-DCB-d4 86 60-140 08/15/2015 01:49

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 11 of 40

Page 55: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-6 COMP 1508393-004A Soil 08/11/2015 11:58 GC16 108899

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Acetone ND 0.10 1 08/15/2015 05:23tert-Amyl methyl ether (TAME) ND 0.0050 1 08/15/2015 05:23Benzene ND 0.0050 1 08/15/2015 05:23Bromobenzene ND 0.0050 1 08/15/2015 05:23Bromochloromethane ND 0.0050 1 08/15/2015 05:23Bromodichloromethane ND 0.0050 1 08/15/2015 05:23Bromoform ND 0.0050 1 08/15/2015 05:23Bromomethane ND 0.0050 1 08/15/2015 05:232-Butanone (MEK) ND 0.020 1 08/15/2015 05:23t-Butyl alcohol (TBA) ND 0.050 1 08/15/2015 05:23n-Butyl benzene ND 0.0050 1 08/15/2015 05:23sec-Butyl benzene ND 0.0050 1 08/15/2015 05:23tert-Butyl benzene ND 0.0050 1 08/15/2015 05:23Carbon Disulfide ND 0.0050 1 08/15/2015 05:23Carbon Tetrachloride ND 0.0050 1 08/15/2015 05:23Chlorobenzene ND 0.0050 1 08/15/2015 05:23Chloroethane ND 0.0050 1 08/15/2015 05:23Chloroform ND 0.0050 1 08/15/2015 05:23Chloromethane ND 0.0050 1 08/15/2015 05:232-Chlorotoluene ND 0.0050 1 08/15/2015 05:234-Chlorotoluene ND 0.0050 1 08/15/2015 05:23Dibromochloromethane ND 0.0050 1 08/15/2015 05:231,2-Dibromo-3-chloropropane ND 0.0040 1 08/15/2015 05:231,2-Dibromoethane (EDB) ND 0.0040 1 08/15/2015 05:23Dibromomethane ND 0.0050 1 08/15/2015 05:231,2-Dichlorobenzene ND 0.0050 1 08/15/2015 05:231,3-Dichlorobenzene ND 0.0050 1 08/15/2015 05:231,4-Dichlorobenzene ND 0.0050 1 08/15/2015 05:23Dichlorodifluoromethane ND 0.0050 1 08/15/2015 05:231,1-Dichloroethane ND 0.0050 1 08/15/2015 05:231,2-Dichloroethane (1,2-DCA) ND 0.0040 1 08/15/2015 05:231,1-Dichloroethene ND 0.0050 1 08/15/2015 05:23cis-1,2-Dichloroethene ND 0.0050 1 08/15/2015 05:23trans-1,2-Dichloroethene ND 0.0050 1 08/15/2015 05:231,2-Dichloropropane ND 0.0050 1 08/15/2015 05:231,3-Dichloropropane ND 0.0050 1 08/15/2015 05:232,2-Dichloropropane ND 0.0050 1 08/15/2015 05:23

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 12 of 40

Page 56: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-6 COMP 1508393-004A Soil 08/11/2015 11:58 GC16 108899

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

1,1-Dichloropropene ND 0.0050 1 08/15/2015 05:23cis-1,3-Dichloropropene ND 0.0050 1 08/15/2015 05:23trans-1,3-Dichloropropene ND 0.0050 1 08/15/2015 05:23Diisopropyl ether (DIPE) ND 0.0050 1 08/15/2015 05:23Ethylbenzene ND 0.0050 1 08/15/2015 05:23Ethyl tert-butyl ether (ETBE) ND 0.0050 1 08/15/2015 05:23Freon 113 ND 0.0050 1 08/15/2015 05:23Hexachlorobutadiene ND 0.0050 1 08/15/2015 05:23Hexachloroethane ND 0.0050 1 08/15/2015 05:232-Hexanone ND 0.0050 1 08/15/2015 05:23Isopropylbenzene ND 0.0050 1 08/15/2015 05:234-Isopropyl toluene ND 0.0050 1 08/15/2015 05:23Methyl-t-butyl ether (MTBE) ND 0.0050 1 08/15/2015 05:23Methylene chloride ND 0.0050 1 08/15/2015 05:234-Methyl-2-pentanone (MIBK) ND 0.0050 1 08/15/2015 05:23Naphthalene ND 0.0050 1 08/15/2015 05:23n-Propyl benzene ND 0.0050 1 08/15/2015 05:23Styrene ND 0.0050 1 08/15/2015 05:231,1,1,2-Tetrachloroethane ND 0.0050 1 08/15/2015 05:231,1,2,2-Tetrachloroethane ND 0.0050 1 08/15/2015 05:23Tetrachloroethene ND 0.0050 1 08/15/2015 05:23Toluene ND 0.0050 1 08/15/2015 05:231,2,3-Trichlorobenzene ND 0.0050 1 08/15/2015 05:231,2,4-Trichlorobenzene ND 0.0050 1 08/15/2015 05:231,1,1-Trichloroethane ND 0.0050 1 08/15/2015 05:231,1,2-Trichloroethane ND 0.0050 1 08/15/2015 05:23Trichloroethene ND 0.0050 1 08/15/2015 05:23Trichlorofluoromethane ND 0.0050 1 08/15/2015 05:231,2,3-Trichloropropane ND 0.0050 1 08/15/2015 05:231,2,4-Trimethylbenzene ND 0.0050 1 08/15/2015 05:231,3,5-Trimethylbenzene ND 0.0050 1 08/15/2015 05:23Vinyl Chloride ND 0.0050 1 08/15/2015 05:23Xylenes, Total ND 0.0050 1 08/15/2015 05:23

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 13 of 40

Page 57: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-6 COMP 1508393-004A Soil 08/11/2015 11:58 GC16 108899

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Surrogates REC (%) Limits

Analyst(s): KF

Dibromofluoromethane 101 70-130 08/15/2015 05:23Toluene-d8 108 70-130 08/15/2015 05:234-BFB 88 70-130 08/15/2015 05:23Benzene-d6 87 60-140 08/15/2015 05:23Ethylbenzene-d10 93 60-140 08/15/2015 05:231,2-DCB-d4 71 60-140 08/15/2015 05:23

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 14 of 40

Page 58: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-7 COMP 1508393-005A Soil 08/11/2015 13:35 GC18 108899

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Acetone ND 0.10 1 08/18/2015 13:25tert-Amyl methyl ether (TAME) ND 0.0050 1 08/18/2015 13:25Benzene ND 0.0050 1 08/18/2015 13:25Bromobenzene ND 0.0050 1 08/18/2015 13:25Bromochloromethane ND 0.0050 1 08/18/2015 13:25Bromodichloromethane ND 0.0050 1 08/18/2015 13:25Bromoform ND 0.0050 1 08/18/2015 13:25Bromomethane ND 0.0050 1 08/18/2015 13:252-Butanone (MEK) ND 0.020 1 08/18/2015 13:25t-Butyl alcohol (TBA) ND 0.050 1 08/18/2015 13:25n-Butyl benzene ND 0.0050 1 08/18/2015 13:25sec-Butyl benzene ND 0.0050 1 08/18/2015 13:25tert-Butyl benzene ND 0.0050 1 08/18/2015 13:25Carbon Disulfide ND 0.0050 1 08/18/2015 13:25Carbon Tetrachloride ND 0.0050 1 08/18/2015 13:25Chlorobenzene ND 0.0050 1 08/18/2015 13:25Chloroethane ND 0.0050 1 08/18/2015 13:25Chloroform ND 0.0050 1 08/18/2015 13:25Chloromethane ND 0.0050 1 08/18/2015 13:252-Chlorotoluene ND 0.0050 1 08/18/2015 13:254-Chlorotoluene ND 0.0050 1 08/18/2015 13:25Dibromochloromethane ND 0.0050 1 08/18/2015 13:251,2-Dibromo-3-chloropropane ND 0.0040 1 08/18/2015 13:251,2-Dibromoethane (EDB) ND 0.0040 1 08/18/2015 13:25Dibromomethane ND 0.0050 1 08/18/2015 13:251,2-Dichlorobenzene ND 0.0050 1 08/18/2015 13:251,3-Dichlorobenzene ND 0.0050 1 08/18/2015 13:251,4-Dichlorobenzene ND 0.0050 1 08/18/2015 13:25Dichlorodifluoromethane ND 0.0050 1 08/18/2015 13:251,1-Dichloroethane ND 0.0050 1 08/18/2015 13:251,2-Dichloroethane (1,2-DCA) ND 0.0040 1 08/18/2015 13:251,1-Dichloroethene ND 0.0050 1 08/18/2015 13:25cis-1,2-Dichloroethene ND 0.0050 1 08/18/2015 13:25trans-1,2-Dichloroethene ND 0.0050 1 08/18/2015 13:251,2-Dichloropropane ND 0.0050 1 08/18/2015 13:251,3-Dichloropropane ND 0.0050 1 08/18/2015 13:252,2-Dichloropropane ND 0.0050 1 08/18/2015 13:25

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 15 of 40

Page 59: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-7 COMP 1508393-005A Soil 08/11/2015 13:35 GC18 108899

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

1,1-Dichloropropene ND 0.0050 1 08/18/2015 13:25cis-1,3-Dichloropropene ND 0.0050 1 08/18/2015 13:25trans-1,3-Dichloropropene ND 0.0050 1 08/18/2015 13:25Diisopropyl ether (DIPE) ND 0.0050 1 08/18/2015 13:25Ethylbenzene ND 0.0050 1 08/18/2015 13:25Ethyl tert-butyl ether (ETBE) ND 0.0050 1 08/18/2015 13:25Freon 113 ND 0.0050 1 08/18/2015 13:25Hexachlorobutadiene ND 0.0050 1 08/18/2015 13:25Hexachloroethane ND 0.0050 1 08/18/2015 13:252-Hexanone ND 0.0050 1 08/18/2015 13:25Isopropylbenzene ND 0.0050 1 08/18/2015 13:254-Isopropyl toluene ND 0.0050 1 08/18/2015 13:25Methyl-t-butyl ether (MTBE) ND 0.0050 1 08/18/2015 13:25Methylene chloride ND 0.0050 1 08/18/2015 13:254-Methyl-2-pentanone (MIBK) ND 0.0050 1 08/18/2015 13:25Naphthalene ND 0.0050 1 08/18/2015 13:25n-Propyl benzene ND 0.0050 1 08/18/2015 13:25Styrene ND 0.0050 1 08/18/2015 13:251,1,1,2-Tetrachloroethane ND 0.0050 1 08/18/2015 13:251,1,2,2-Tetrachloroethane ND 0.0050 1 08/18/2015 13:25Tetrachloroethene ND 0.0050 1 08/18/2015 13:25Toluene ND 0.0050 1 08/18/2015 13:251,2,3-Trichlorobenzene ND 0.0050 1 08/18/2015 13:251,2,4-Trichlorobenzene ND 0.0050 1 08/18/2015 13:251,1,1-Trichloroethane ND 0.0050 1 08/18/2015 13:251,1,2-Trichloroethane ND 0.0050 1 08/18/2015 13:25Trichloroethene ND 0.0050 1 08/18/2015 13:25Trichlorofluoromethane ND 0.0050 1 08/18/2015 13:251,2,3-Trichloropropane ND 0.0050 1 08/18/2015 13:251,2,4-Trimethylbenzene ND 0.0050 1 08/18/2015 13:251,3,5-Trimethylbenzene ND 0.0050 1 08/18/2015 13:25Vinyl Chloride ND 0.0050 1 08/18/2015 13:25Xylenes, Total ND 0.0050 1 08/18/2015 13:25

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 16 of 40

Page 60: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-7 COMP 1508393-005A Soil 08/11/2015 13:35 GC18 108899

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Surrogates REC (%) Limits

Analyst(s): KF

Dibromofluoromethane 119 70-130 08/18/2015 13:25Toluene-d8 115 70-130 08/18/2015 13:254-BFB 120 70-130 08/18/2015 13:25Benzene-d6 110 60-140 08/18/2015 13:25Ethylbenzene-d10 115 60-140 08/18/2015 13:251,2-DCB-d4 90 60-140 08/18/2015 13:25

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 17 of 40

Page 61: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-8 COMP 1508393-006A Soil 08/11/2015 14:06 GC10 108899

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Acetone ND 0.10 1 08/14/2015 12:50tert-Amyl methyl ether (TAME) ND 0.0050 1 08/14/2015 12:50Benzene ND 0.0050 1 08/14/2015 12:50Bromobenzene ND 0.0050 1 08/14/2015 12:50Bromochloromethane ND 0.0050 1 08/14/2015 12:50Bromodichloromethane ND 0.0050 1 08/14/2015 12:50Bromoform ND 0.0050 1 08/14/2015 12:50Bromomethane ND 0.0050 1 08/14/2015 12:502-Butanone (MEK) ND 0.020 1 08/14/2015 12:50t-Butyl alcohol (TBA) ND 0.050 1 08/14/2015 12:50n-Butyl benzene ND 0.0050 1 08/14/2015 12:50sec-Butyl benzene ND 0.0050 1 08/14/2015 12:50tert-Butyl benzene ND 0.0050 1 08/14/2015 12:50Carbon Disulfide ND 0.0050 1 08/14/2015 12:50Carbon Tetrachloride ND 0.0050 1 08/14/2015 12:50Chlorobenzene ND 0.0050 1 08/14/2015 12:50Chloroethane ND 0.0050 1 08/14/2015 12:50Chloroform ND 0.0050 1 08/14/2015 12:50Chloromethane ND 0.0050 1 08/14/2015 12:502-Chlorotoluene ND 0.0050 1 08/14/2015 12:504-Chlorotoluene ND 0.0050 1 08/14/2015 12:50Dibromochloromethane ND 0.0050 1 08/14/2015 12:501,2-Dibromo-3-chloropropane ND 0.0040 1 08/14/2015 12:501,2-Dibromoethane (EDB) ND 0.0040 1 08/14/2015 12:50Dibromomethane ND 0.0050 1 08/14/2015 12:501,2-Dichlorobenzene ND 0.0050 1 08/14/2015 12:501,3-Dichlorobenzene ND 0.0050 1 08/14/2015 12:501,4-Dichlorobenzene ND 0.0050 1 08/14/2015 12:50Dichlorodifluoromethane ND 0.0050 1 08/14/2015 12:501,1-Dichloroethane ND 0.0050 1 08/14/2015 12:501,2-Dichloroethane (1,2-DCA) ND 0.0040 1 08/14/2015 12:501,1-Dichloroethene ND 0.0050 1 08/14/2015 12:50cis-1,2-Dichloroethene ND 0.0050 1 08/14/2015 12:50trans-1,2-Dichloroethene ND 0.0050 1 08/14/2015 12:501,2-Dichloropropane ND 0.0050 1 08/14/2015 12:501,3-Dichloropropane ND 0.0050 1 08/14/2015 12:502,2-Dichloropropane ND 0.0050 1 08/14/2015 12:50

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 18 of 40

Page 62: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-8 COMP 1508393-006A Soil 08/11/2015 14:06 GC10 108899

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

1,1-Dichloropropene ND 0.0050 1 08/14/2015 12:50cis-1,3-Dichloropropene ND 0.0050 1 08/14/2015 12:50trans-1,3-Dichloropropene ND 0.0050 1 08/14/2015 12:50Diisopropyl ether (DIPE) ND 0.0050 1 08/14/2015 12:50Ethylbenzene ND 0.0050 1 08/14/2015 12:50Ethyl tert-butyl ether (ETBE) ND 0.0050 1 08/14/2015 12:50Freon 113 ND 0.0050 1 08/14/2015 12:50Hexachlorobutadiene ND 0.0050 1 08/14/2015 12:50Hexachloroethane ND 0.0050 1 08/14/2015 12:502-Hexanone ND 0.0050 1 08/14/2015 12:50Isopropylbenzene ND 0.0050 1 08/14/2015 12:504-Isopropyl toluene ND 0.0050 1 08/14/2015 12:50Methyl-t-butyl ether (MTBE) ND 0.0050 1 08/14/2015 12:50Methylene chloride ND 0.0050 1 08/14/2015 12:504-Methyl-2-pentanone (MIBK) ND 0.0050 1 08/14/2015 12:50Naphthalene ND 0.0050 1 08/14/2015 12:50n-Propyl benzene ND 0.0050 1 08/14/2015 12:50Styrene ND 0.0050 1 08/14/2015 12:501,1,1,2-Tetrachloroethane ND 0.0050 1 08/14/2015 12:501,1,2,2-Tetrachloroethane ND 0.0050 1 08/14/2015 12:50Tetrachloroethene ND 0.0050 1 08/14/2015 12:50Toluene ND 0.0050 1 08/14/2015 12:501,2,3-Trichlorobenzene ND 0.0050 1 08/14/2015 12:501,2,4-Trichlorobenzene ND 0.0050 1 08/14/2015 12:501,1,1-Trichloroethane ND 0.0050 1 08/14/2015 12:501,1,2-Trichloroethane ND 0.0050 1 08/14/2015 12:50Trichloroethene ND 0.0050 1 08/14/2015 12:50Trichlorofluoromethane ND 0.0050 1 08/14/2015 12:501,2,3-Trichloropropane ND 0.0050 1 08/14/2015 12:501,2,4-Trimethylbenzene ND 0.0050 1 08/14/2015 12:501,3,5-Trimethylbenzene ND 0.0050 1 08/14/2015 12:50Vinyl Chloride ND 0.0050 1 08/14/2015 12:50Xylenes, Total ND 0.0050 1 08/14/2015 12:50

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 19 of 40

Page 63: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-8 COMP 1508393-006A Soil 08/11/2015 14:06 GC10 108899

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Surrogates REC (%) Limits

Analyst(s): KF

Dibromofluoromethane 114 70-130 08/14/2015 12:50Toluene-d8 99 70-130 08/14/2015 12:504-BFB 115 70-130 08/14/2015 12:50Benzene-d6 90 60-140 08/14/2015 12:50Ethylbenzene-d10 100 60-140 08/14/2015 12:501,2-DCB-d4 79 60-140 08/14/2015 12:50

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

Page 20 of 40

Page 64: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8021B/8015BmUnit: mg/Kg

Gasoline Range (C6-C12) Volatile Hydrocarbons as Gasoline with BTEX and MTBE

B-3 COMP 1508393-001A Soil 08/11/2015 09:05 GC7 108898

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH(g) ND 1.0 1 08/15/2015 00:41MTBE --- 0.050 1 08/15/2015 00:41Benzene --- 0.0050 1 08/15/2015 00:41Toluene --- 0.0050 1 08/15/2015 00:41Ethylbenzene --- 0.0050 1 08/15/2015 00:41Xylenes --- 0.0050 1 08/15/2015 00:41

Surrogates REC (%) Limits

Analyst(s): IA

2-Fluorotoluene 107 70-130 08/15/2015 00:41

B-4 COMP 1508393-002A Soil 08/11/2015 10:00 GC7 108898

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH(g) ND 1.0 1 08/15/2015 02:11MTBE --- 0.050 1 08/15/2015 02:11Benzene --- 0.0050 1 08/15/2015 02:11Toluene --- 0.0050 1 08/15/2015 02:11Ethylbenzene --- 0.0050 1 08/15/2015 02:11Xylenes --- 0.0050 1 08/15/2015 02:11

Surrogates REC (%) Limits

Analyst(s): IA

2-Fluorotoluene 101 70-130 08/15/2015 02:11

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 21 of 40

Page 65: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8021B/8015BmUnit: mg/Kg

Gasoline Range (C6-C12) Volatile Hydrocarbons as Gasoline with BTEX and MTBE

B-5 COMP 1508393-003A Soil 08/11/2015 10:44 GC7 108898

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH(g) ND 1.0 1 08/15/2015 06:09MTBE --- 0.050 1 08/15/2015 06:09Benzene --- 0.0050 1 08/15/2015 06:09Toluene --- 0.0050 1 08/15/2015 06:09Ethylbenzene --- 0.0050 1 08/15/2015 06:09Xylenes --- 0.0050 1 08/15/2015 06:09

Surrogates REC (%) Limits

Analyst(s): IA

2-Fluorotoluene 107 70-130 08/15/2015 06:09

B-6 COMP 1508393-004A Soil 08/11/2015 11:58 GC7 108898

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH(g) ND 1.0 1 08/15/2015 05:40MTBE --- 0.050 1 08/15/2015 05:40Benzene --- 0.0050 1 08/15/2015 05:40Toluene --- 0.0050 1 08/15/2015 05:40Ethylbenzene --- 0.0050 1 08/15/2015 05:40Xylenes --- 0.0050 1 08/15/2015 05:40

Surrogates REC (%) Limits

Analyst(s): IA

2-Fluorotoluene 105 70-130 08/15/2015 05:40

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 22 of 40

Page 66: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW5030BAnalytical Method: SW8021B/8015BmUnit: mg/Kg

Gasoline Range (C6-C12) Volatile Hydrocarbons as Gasoline with BTEX and MTBE

B-7 COMP 1508393-005A Soil 08/11/2015 13:35 GC7 108898

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH(g) ND 1.0 1 08/15/2015 04:10MTBE --- 0.050 1 08/15/2015 04:10Benzene --- 0.0050 1 08/15/2015 04:10Toluene --- 0.0050 1 08/15/2015 04:10Ethylbenzene --- 0.0050 1 08/15/2015 04:10Xylenes --- 0.0050 1 08/15/2015 04:10

Surrogates REC (%) Limits

Analyst(s): IA

2-Fluorotoluene 105 70-130 08/15/2015 04:10

B-8 COMP 1508393-006A Soil 08/11/2015 14:06 GC7 108898

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH(g) ND 1.0 1 08/15/2015 04:40MTBE --- 0.050 1 08/15/2015 04:40Benzene --- 0.0050 1 08/15/2015 04:40Toluene --- 0.0050 1 08/15/2015 04:40Ethylbenzene --- 0.0050 1 08/15/2015 04:40Xylenes --- 0.0050 1 08/15/2015 04:40

Surrogates REC (%) Limits

Analyst(s): IA

2-Fluorotoluene 104 70-130 08/15/2015 04:40

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

Page 23 of 40

Page 67: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW3050BAnalytical Method: SW6020Unit: mg/Kg

LUFT 5 Metals

B-3 COMP 1508393-001A Soil 08/11/2015 09:05 ICP-MS1 108846

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Cadmium ND 0.25 1 08/15/2015 02:19Chromium 56 0.50 1 08/15/2015 02:19Lead 6.1 0.50 1 08/15/2015 02:19Nickel 76 0.50 1 08/15/2015 02:19Zinc 31 5.0 1 08/15/2015 02:19

Surrogates REC (%) Limits

Analyst(s): DB

Terbium 105 70-130 08/15/2015 02:19

B-4 COMP 1508393-002A Soil 08/11/2015 10:00 ICP-MS1 108846

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Cadmium ND 0.25 1 08/15/2015 02:25Chromium 69 0.50 1 08/15/2015 02:25Lead 10 0.50 1 08/15/2015 02:25Nickel 69 0.50 1 08/15/2015 02:25Zinc 34 5.0 1 08/15/2015 02:25

Surrogates REC (%) Limits

Analyst(s): DB

Terbium 104 70-130 08/15/2015 02:25

B-5 COMP 1508393-003A Soil 08/11/2015 10:44 ICP-MS1 108846

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Cadmium ND 0.25 1 08/15/2015 02:31Chromium 52 0.50 1 08/15/2015 02:31Lead 5.5 0.50 1 08/15/2015 02:31Nickel 61 0.50 1 08/15/2015 02:31Zinc 27 5.0 1 08/15/2015 02:31

Surrogates REC (%) Limits

Analyst(s): DB

Terbium 101 70-130 08/15/2015 02:31

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 24 of 40

Page 68: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15

WorkOrder: 1508393Extraction Method: SW3050BAnalytical Method: SW6020Unit: mg/Kg

LUFT 5 Metals

B-6 COMP 1508393-004A Soil 08/11/2015 11:58 ICP-MS1 108846

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Cadmium ND 0.25 1 08/15/2015 02:50Chromium 68 0.50 1 08/15/2015 02:50Lead 5.6 0.50 1 08/15/2015 02:50Nickel 100 0.50 1 08/15/2015 02:50Zinc 36 5.0 1 08/15/2015 02:50

Surrogates REC (%) Limits

Analyst(s): DB

Terbium 103 70-130 08/15/2015 02:50

B-7 COMP 1508393-005A Soil 08/11/2015 13:35 ICP-MS1 108846

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Cadmium ND 0.25 1 08/15/2015 02:56Chromium 71 0.50 1 08/15/2015 02:56Lead 4.5 0.50 1 08/15/2015 02:56Nickel 85 0.50 1 08/15/2015 02:56Zinc 33 5.0 1 08/15/2015 02:56

Surrogates REC (%) Limits

Analyst(s): DB

Terbium 104 70-130 08/15/2015 02:56

B-8 COMP 1508393-006A Soil 08/11/2015 14:06 ICP-MS1 108846

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Cadmium ND 0.25 1 08/15/2015 03:02Chromium 68 0.50 1 08/15/2015 03:02Lead 6.3 0.50 1 08/15/2015 03:02Nickel 51 0.50 1 08/15/2015 03:02Zinc 31 5.0 1 08/15/2015 03:02

Surrogates REC (%) Limits

Analyst(s): DB

Terbium 104 70-130 08/15/2015 03:02

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

Page 25 of 40

Page 69: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15-8/14/15

WorkOrder: 1508393Extraction Method: SW3550B/3630CAnalytical Method: SW8015BUnit: mg/Kg

Total Extractable Petroleum Hydrocarbons with Silica Gel Clean-Up

B-3 COMP 1508393-001A Soil 08/11/2015 09:05 GC9a 108896

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH-Diesel (C10-C23) ND 1.0 1 08/14/2015 16:11TPH-Motor Oil (C18-C36) ND 5.0 1 08/14/2015 16:11

Surrogates REC (%) Limits

Analyst(s): TK

C9 93 70-130 08/14/2015 16:11

B-4 COMP 1508393-002A Soil 08/11/2015 10:00 GC9a 108896

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH-Diesel (C10-C23) ND 1.0 1 08/14/2015 17:23TPH-Motor Oil (C18-C36) ND 5.0 1 08/14/2015 17:23

Surrogates REC (%) Limits

Analyst(s): TK

C9 102 70-130 08/14/2015 17:23

B-5 COMP 1508393-003A Soil 08/11/2015 10:44 GC9a 108896

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH-Diesel (C10-C23) ND 1.0 1 08/14/2015 18:34TPH-Motor Oil (C18-C36) ND 5.0 1 08/14/2015 18:34

Surrogates REC (%) Limits

Analyst(s): TK

C9 103 70-130 08/14/2015 18:34

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 26 of 40

Page 70: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/12/15 18:00Date Prepared: 8/13/15-8/14/15

WorkOrder: 1508393Extraction Method: SW3550B/3630CAnalytical Method: SW8015BUnit: mg/Kg

Total Extractable Petroleum Hydrocarbons with Silica Gel Clean-Up

B-6 COMP 1508393-004A Soil 08/11/2015 11:58 GC9b 108896

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH-Diesel (C10-C23) ND 1.0 1 08/14/2015 19:46TPH-Motor Oil (C18-C36) ND 5.0 1 08/14/2015 19:46

Surrogates REC (%) Limits

Analyst(s): TK

C9 104 70-130 08/14/2015 19:46

B-7 COMP 1508393-005A Soil 08/11/2015 13:35 GC11A 108896

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH-Diesel (C10-C23) ND 1.0 1 08/18/2015 20:54TPH-Motor Oil (C18-C36) ND 5.0 1 08/18/2015 20:54

Surrogates REC (%) Limits

Analyst(s): TK

C9 102 70-130 08/18/2015 20:54

B-8 COMP 1508393-006A Soil 08/11/2015 14:06 GC2A 108934

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH-Diesel (C10-C23) 2.3 1.0 1 08/17/2015 12:06TPH-Motor Oil (C18-C36) 15 5.0 1 08/17/2015 12:06

Surrogates REC (%) Limits

Analytical Comments: e7,e2Analyst(s): TK

C9 94 70-130 08/17/2015 12:06

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

Page 27 of 40

Page 71: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Quality Control Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Analyzed: 8/13/15Date Prepared: 8/13/15

WorkOrder: 1508393BatchID: 108899

Analytical Method: SW8260BUnit: mg/KgSample ID: MB/LCS-108899

1508393-006AMS/MSD

Instrument: GC10Matrix: Soil

Extraction Method: SW5030B

QC Summary Report for SW8260B

Analyte MB

Result

LCS

Result

RL SPK

Val

MB SS

%REC

LCS

%REC

LCS

Limits

Acetone ND - 0.10 - - - -tert-Amyl methyl ether (TAME) ND 0.0390 0.0050 0.050 - 78 53-116Benzene ND 0.0453 0.0050 0.050 - 91 63-137Bromobenzene ND - 0.0050 - - - -Bromochloromethane ND - 0.0050 - - - -Bromodichloromethane ND - 0.0050 - - - -Bromoform ND - 0.0050 - - - -Bromomethane ND - 0.0050 - - - -2-Butanone (MEK) ND - 0.020 - - - -t-Butyl alcohol (TBA) ND 0.177 0.050 0.20 - 89 41-135n-Butyl benzene ND - 0.0050 - - - -sec-Butyl benzene ND - 0.0050 - - - -tert-Butyl benzene ND - 0.0050 - - - -Carbon Disulfide ND - 0.0050 - - - -Carbon Tetrachloride ND - 0.0050 - - - -Chlorobenzene ND 0.0463 0.0050 0.050 - 93 77-121Chloroethane ND - 0.0050 - - - -Chloroform ND - 0.0050 - - - -Chloromethane ND - 0.0050 - - - -2-Chlorotoluene ND - 0.0050 - - - -4-Chlorotoluene ND - 0.0050 - - - -Dibromochloromethane ND - 0.0050 - - - -1,2-Dibromo-3-chloropropane ND - 0.0040 - - - -1,2-Dibromoethane (EDB) ND 0.0432 0.0040 0.050 - 86 67-119Dibromomethane ND - 0.0050 - - - -1,2-Dichlorobenzene ND - 0.0050 - - - -1,3-Dichlorobenzene ND - 0.0050 - - - -1,4-Dichlorobenzene ND - 0.0050 - - - -Dichlorodifluoromethane ND - 0.0050 - - - -1,1-Dichloroethane ND - 0.0050 - - - -1,2-Dichloroethane (1,2-DCA) ND 0.0433 0.0040 0.050 - 87 58-1351,1-Dichloroethene ND 0.0434 0.0050 0.050 - 87 42-145cis-1,2-Dichloroethene ND - 0.0050 - - - -trans-1,2-Dichloroethene ND - 0.0050 - - - -1,2-Dichloropropane ND - 0.0050 - - - -1,3-Dichloropropane ND - 0.0050 - - - -2,2-Dichloropropane ND - 0.0050 - - - -1,1-Dichloropropene ND - 0.0050 - - - -

QA/QC OfficerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

(Cont.)

Page 28 of 40

Page 72: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Quality Control Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Analyzed: 8/13/15Date Prepared: 8/13/15

WorkOrder: 1508393BatchID: 108899

Analytical Method: SW8260BUnit: mg/KgSample ID: MB/LCS-108899

1508393-006AMS/MSD

Instrument: GC10Matrix: Soil

Extraction Method: SW5030B

QC Summary Report for SW8260B

Analyte MB

Result

LCS

Result

RL SPK

Val

MB SS

%REC

LCS

%REC

LCS

Limits

cis-1,3-Dichloropropene ND - 0.0050 - - - -trans-1,3-Dichloropropene ND - 0.0050 - - - -Diisopropyl ether (DIPE) ND 0.0435 0.0050 0.050 - 87 52-129Ethylbenzene ND - 0.0050 - - - -Ethyl tert-butyl ether (ETBE) ND 0.0422 0.0050 0.050 - 84 53-125Freon 113 ND - 0.0050 - - - -Hexachlorobutadiene ND - 0.0050 - - - -Hexachloroethane ND - 0.0050 - - - -2-Hexanone ND - 0.0050 - - - -Isopropylbenzene ND - 0.0050 - - - -4-Isopropyl toluene ND - 0.0050 - - - -Methyl-t-butyl ether (MTBE) ND 0.0425 0.0050 0.050 - 85 58-122Methylene chloride ND - 0.0050 - - - -4-Methyl-2-pentanone (MIBK) ND - 0.0050 - - - -Naphthalene ND - 0.0050 - - - -n-Propyl benzene ND - 0.0050 - - - -Styrene ND - 0.0050 - - - -1,1,1,2-Tetrachloroethane ND - 0.0050 - - - -1,1,2,2-Tetrachloroethane ND - 0.0050 - - - -Tetrachloroethene ND - 0.0050 - - - -Toluene ND 0.0464 0.0050 0.050 - 93 76-1301,2,3-Trichlorobenzene ND - 0.0050 - - - -1,2,4-Trichlorobenzene ND - 0.0050 - - - -1,1,1-Trichloroethane ND - 0.0050 - - - -1,1,2-Trichloroethane ND - 0.0050 - - - -Trichloroethene ND 0.0435 0.0050 0.050 - 87 72-132Trichlorofluoromethane ND - 0.0050 - - - -1,2,3-Trichloropropane ND - 0.0050 - - - -1,2,4-Trimethylbenzene ND - 0.0050 - - - -1,3,5-Trimethylbenzene ND - 0.0050 - - - -Vinyl Chloride ND - 0.0050 - - - -Xylenes, Total ND - 0.0050 - - - -

QA/QC OfficerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

(Cont.)

Page 29 of 40

Page 73: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Quality Control Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Analyzed: 8/13/15Date Prepared: 8/13/15

WorkOrder: 1508393BatchID: 108899

Analytical Method: SW8260BUnit: mg/KgSample ID: MB/LCS-108899

1508393-006AMS/MSD

Instrument: GC10Matrix: Soil

Extraction Method: SW5030B

QC Summary Report for SW8260B

Analyte MB

Result

LCS

Result

RL SPK

Val

MB SS

%REC

LCS

%REC

LCS

Limits

Surrogate Recovery

Dibromofluoromethane 0.139 0.141 0.12 111 113 70-130Toluene-d8 0.128 0.129 0.12 102 103 70-1304-BFB 0.0144 0.0144 0.012 116 116 70-130Benzene-d6 0.0917 0.0933 0.10 92 93 60-140Ethylbenzene-d10 0.110 0.116 0.10 110 116 60-1401,2-DCB-d4 0.0826 0.0842 0.10 83 84 60-140

Analyte MS

Result

MSD

Result

SPK

Val

SPKRef

Val

MS

%REC

MSD

%REC

MS/MSD

Limits

RPD RPD

Limit

tert-Amyl methyl ether (TAME) 0.0349 0.0360 0.050 ND 70 72 70-130 3.14 20Benzene 0.0446 0.0456 0.050 ND 89 91 70-130 2.26 20t-Butyl alcohol (TBA) 0.149 0.157 0.20 ND 75 79 70-130 5.27 20Chlorobenzene 0.0431 0.0444 0.050 ND 86 89 70-130 3.06 201,2-Dibromoethane (EDB) 0.0384 0.0402 0.050 ND 77 80 70-130 4.53 201,2-Dichloroethane (1,2-DCA) 0.0418 0.0425 0.050 ND 84 85 70-130 1.65 201,1-Dichloroethene 0.0427 0.0434 0.050 ND 85 87 70-130 1.80 20Diisopropyl ether (DIPE) 0.0412 0.0420 0.050 ND 83 84 70-130 1.83 20Ethyl tert-butyl ether (ETBE) 0.0388 0.0399 0.050 ND 78 80 70-130 2.72 20Methyl-t-butyl ether (MTBE) 0.0384 0.0396 0.050 ND 77 79 70-130 3.12 20Toluene 0.0427 0.0441 0.050 ND 85 88 70-130 3.32 20Trichloroethene 0.0477 0.0458 0.050 ND 95 92 70-130 4.02 20

Surrogate Recovery

Dibromofluoromethane 0.145 0.145 0.12 116 116 70-130 0 20Toluene-d8 0.125 0.126 0.12 100 101 70-130 0.730 204-BFB 0.0147 0.0143 0.012 118 114 70-130 3.03 20Benzene-d6 0.0937 0.0962 0.10 94 96 60-140 2.65 20Ethylbenzene-d10 0.106 0.112 0.10 107 112 60-140 4.77 201,2-DCB-d4 0.0825 0.0827 0.10 83 83 60-140 0 20

QA/QC OfficerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

Page 30 of 40

Page 74: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Quality Control Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Analyzed: 8/14/15Date Prepared: 8/13/15

WorkOrder: 1508393BatchID: 108898

Analytical Method: SW8021B/8015BmUnit: mg/KgSample ID: MB/LCS-108898

1508392-006AMS/MSD

Instrument: GC19Matrix: Soil

Extraction Method: SW5030B

QC Summary Report for SW8021B/8015Bm

Analyte MB

Result

LCS

Result

RL SPK

Val

MB SS

%REC

LCS

%REC

LCS

Limits

TPH(btex) ND 0.481 0.40 0.60 - 80 70-130MTBE ND 0.0869 0.050 0.10 - 87 70-130Benzene ND 0.108 0.0050 0.10 - 108 70-130Toluene ND 0.110 0.0050 0.10 - 110 70-130Ethylbenzene ND 0.113 0.0050 0.10 - 113 70-130Xylenes ND 0.369 0.0050 0.30 - 123 70-130

Surrogate Recovery

2-Fluorotoluene 0.118 0.115 0.10 119 115 70-130

Analyte MS

Result

MSD

Result

SPK

Val

SPKRef

Val

MS

%REC

MSD

%REC

MS/MSD

Limits

RPD RPD

Limit

TPH(btex) 0.513 0.501 0.60 ND 85 83 70-130 2.35 20MTBE 0.0918 0.0935 0.10 ND 92 94 70-130 1.87 20Benzene 0.101 0.101 0.10 ND 101 101 70-130 0 20Toluene 0.103 0.104 0.10 ND 103 104 70-130 0.596 20Ethylbenzene 0.106 0.107 0.10 ND 106 107 70-130 0.385 20Xylenes 0.341 0.346 0.30 ND 114 115 70-130 1.39 20

Surrogate Recovery

2-Fluorotoluene 0.108 0.109 0.10 108 109 70-130 0.569 20

QA/QC OfficerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

Page 31 of 40

Page 75: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Quality Control Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Analyzed: 8/13/15Date Prepared: 8/12/15

WorkOrder: 1508393BatchID: 108846

Analytical Method: SW6020Unit: mg/KgSample ID: MB/LCS-108846

1508336-012AMS/MSD

Instrument: ICP-MS2Matrix: Soil

Extraction Method: SW3050B

QC Summary Report for Metals

Analyte MB

Result

LCS

Result

RL SPK

Val

MB SS

%REC

LCS

%REC

LCS

Limits

Cadmium ND 48.4 0.25 50 - 97 75-125Chromium ND 47.6 0.50 50 - 95 75-125Lead ND 49.9 0.50 50 - 100 75-125Nickel ND 48.2 0.50 50 - 96 75-125Zinc ND 497 5.0 500 - 99 75-125

Surrogate Recovery

Terbium 539 520 500 108 104 70-130

Analyte MS

Result

MSD

Result

SPK

Val

SPKRef

Val

MS

%REC

MSD

%REC

MS/MSD

Limits

RPD RPD

Limit

Cadmium 50.7 50.7 50 0.8656 100 100 75-125 0 20Chromium NR NR 50 68.53 NR NR 75-125 NR 20Lead NR NR 50 278.1 NR NR 75-125 NR 20Nickel NR NR 50 60.05 NR NR 75-125 NR 20Zinc NR NR 500 1638 NR NR 75-125 NR 20

Surrogate Recovery

Terbium 552 541 500 110 108 70-130 1.88 20

QA/QC OfficerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

Page 32 of 40

Page 76: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Quality Control Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Analyzed: 8/14/15Date Prepared: 8/13/15

WorkOrder: 1508393BatchID: 108896

Analytical Method: SW8015BUnit: mg/KgSample ID: MB/LCS-108896

1508391-008AMS/MSD

Instrument: GC11AMatrix: Soil

Extraction Method: SW3550B/3630C

QC Report for SW8015B with Silica Gel Clean-Up

Analyte MB

Result

LCS

Result

RL SPK

Val

MB SS

%REC

LCS

%REC

LCS

Limits

TPH-Diesel (C10-C23) ND 40.0 1.0 40 - 100 70-130TPH-Motor Oil (C18-C36) ND - 5.0 - - - -

Surrogate Recovery

C9 23.3 23.7 25 93 95 62-139

Analyte MS

Result

MSD

Result

SPK

Val

SPKRef

Val

MS

%REC

MSD

%REC

MS/MSD

Limits

RPD RPD

Limit

TPH-Diesel (C10-C23) 40.0 39.7 40 ND 98 97 70-130 0.941 30

Surrogate Recovery

C9 23.9 23.7 25 96 95 70-130 0.908 30

QA/QC OfficerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

(Cont.)

Page 33 of 40

Page 77: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Quality Control Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Analyzed: 8/14/15Date Prepared: 8/13/15

WorkOrder: 1508393BatchID: 108934

Analytical Method: SW8015BUnit: mg/KgSample ID: MB/LCS-108934

1508432-013AMS/MSD

Instrument: GC11BMatrix: Soil

Extraction Method: SW3550B/3630C

QC Report for SW8015B with Silica Gel Clean-Up

Analyte MB

Result

LCS

Result

RL SPK

Val

MB SS

%REC

LCS

%REC

LCS

Limits

TPH-Diesel (C10-C23) ND 40.4 1.0 40 - 101 70-130TPH-Motor Oil (C18-C36) ND - 5.0 - - - -

Surrogate Recovery

C9 25.8 26.5 25 103 106 62-139

Analyte MS

Result

MSD

Result

SPK

Val

SPKRef

Val

MS

%REC

MSD

%REC

MS/MSD

Limits

RPD RPD

Limit

TPH-Diesel (C10-C23) 39.8 40.4 40 ND 99 101 70-130 1.64 30

Surrogate Recovery

C9 26.5 26.5 25 106 106 70-130 0 30

QA/QC OfficerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

Page 34 of 40

Page 78: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

McCampbell Analytical, Inc.1534 Willow Pass RdPittsburg, CA 94565-1701(925) 252-9262

CHAIN-OF-CUSTODY RECORD Page

Lab ID Matrix Collection Date Hold

Requested Tests (See legend below)

Report to:

Christopher Houlihan

320 Professional Center Ste. 215Rohnert Park, CA 94928(707) 792-9500 FAX: (707) 792-9504

PO:

08/19/2015

Client ID

ProjectNo: 0778,001.15; Limited Pre-Con Soil Assessment

WorkOrder: 1508393

1 of 1

Date Printed:

Date Received: 08/12/2015

1 2 3 4 5 6 7 8 9 10 11 12

Edd Clark & Associates, Inc.

Bill to:

Accounts PayableEdd Clark & Associates, Inc.320 Professional Center Ste.215Rohnert Park, CA 94928

Requested TAT: 5 days;

ClientCode: ECAR

Email: [email protected]

EDF EQuIS Email HardCopy ThirdParty

[email protected]

Excel J-flagWriteOn

cc/3rd Party:

WaterTrax

A1508393-001 Soil 8/11/2015 9:05B-3 COMP A A AA1508393-002 Soil 8/11/2015 10:00B-4 COMP A A AA1508393-003 Soil 8/11/2015 10:44B-5 COMP A A AA1508393-004 Soil 8/11/2015 11:58B-6 COMP A A AA1508393-005 Soil 8/11/2015 13:35B-7 COMP A A AA1508393-006 Soil 8/11/2015 14:06B-8 COMP A A A

Prepared by: Maria Venegas

NOTE: Soil samples are discarded 60 days after results are reported unless other arrangements are made (Water samples are 30 days). Hazardous samples will be returned to client or disposed of at client expense.

Comments: For Soil Vapor Samples ALWAYS report in ug/L AND nL/L per Brian

8260B_S G-MBTEX_S LUFTMS_6020_S TPH(DMO)WSG_S1 2 3 4 5

6 7 8 9 10

Test Legend:

11 12

The following SampIDs: 001A, 002A, 003A, 004A, 005A, 006A contain testgroup.

Page 35 of 40

Page 79: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Lab ID Client ID Collection Date

& Time

Date Received:

TATMatrix Test Name Containers

/Composites

WORK ORDER SUMMARY

Work Order: 1508393

Comments: For Soil Vapor Samples ALWAYS report in ug/L AND nL/L per Brian

Client Name: EDD CLARK & ASSOCIATES, INC.Project: 0778,001.15; Limited Pre-Con Soil Assessment

QC Level: LEVEL 2

HoldDe-

chlorinated

SubOutBottle & Preservative

8/12/2015

Sediment

Content

EDF Fax Email HardCopy ThirdPartyExcel J-flagWriteOn

Christopher HoulihanClient Contact:

[email protected]'s Email:

WaterTrax

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

1508393-001A B-3 COMP 8/11/2015 9:05 5 daysSoil SW6020 (LUFT) 4 / (4:1) Acetate Liner

5 daysMulti-Range TPH(g,d,mo) w/ S.G. Clean-Up

5 daysSW8260B (VOCs)

1508393-002A B-4 COMP 8/11/2015 10:00 5 daysSoil SW6020 (LUFT) 4 / (4:1) Acetate Liner

5 daysMulti-Range TPH(g,d,mo) w/ S.G. Clean-Up

5 daysSW8260B (VOCs)

1508393-003A B-5 COMP 8/11/2015 10:44 5 daysSoil SW6020 (LUFT) 4 / (4:1) Acetate Liner

5 daysMulti-Range TPH(g,d,mo) w/ S.G. Clean-Up

5 daysSW8260B (VOCs)

1508393-004A B-6 COMP 8/11/2015 11:58 5 daysSoil SW6020 (LUFT) 4 / (4:1) Acetate Liner

5 daysMulti-Range TPH(g,d,mo) w/ S.G. Clean-Up

5 daysSW8260B (VOCs)

1508393-005A B-7 COMP 8/11/2015 13:35 5 daysSoil SW6020 (LUFT) 4 / (4:1) Acetate Liner

5 daysMulti-Range TPH(g,d,mo) w/ S.G. Clean-Up

5 daysSW8260B (VOCs)

1 of 2Page

- STLC and TCLP extractions require 2 days to complete; therefore, all TATs begin after the extraction is completed (i.e., One-day TAT yields results

in 3 days from sample submission).

NOTES:

- MAI assumes that all material present in the provided sampling container is considered part of the sample - MAI does not exclude any material from

the sample prior to sample preparation unless requested in writing by the client.

Page 36 of 40

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Lab ID Client ID Collection Date

& Time

Date Received:

TATMatrix Test Name Containers

/Composites

WORK ORDER SUMMARY

Work Order: 1508393

Comments: For Soil Vapor Samples ALWAYS report in ug/L AND nL/L per Brian

Client Name: EDD CLARK & ASSOCIATES, INC.Project: 0778,001.15; Limited Pre-Con Soil Assessment

QC Level: LEVEL 2

HoldDe-

chlorinated

SubOutBottle & Preservative

8/12/2015

Sediment

Content

EDF Fax Email HardCopy ThirdPartyExcel J-flagWriteOn

Christopher HoulihanClient Contact:

[email protected]'s Email:

WaterTrax

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

1508393-006A B-8 COMP 8/11/2015 14:06 5 daysSoil SW6020 (LUFT) 4 / (4:1) Acetate Liner

5 daysMulti-Range TPH(g,d,mo) w/ S.G. Clean-Up

5 daysSW8260B (VOCs)

2 of 2Page

- STLC and TCLP extractions require 2 days to complete; therefore, all TATs begin after the extraction is completed (i.e., One-day TAT yields results

in 3 days from sample submission).

NOTES:

- MAI assumes that all material present in the provided sampling container is considered part of the sample - MAI does not exclude any material from

the sample prior to sample preparation unless requested in writing by the client.

Page 37 of 40

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Page 38 of 40

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Page 39 of 40

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Sample Receipt Checklist

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client Name: Edd Clark & Associates, Inc.

WorkOrder №: 1508393

Date and Time Received: 8/12/2015 6:00:00 PM

LogIn Reviewed by: Maria Venegas

Matrix: Soil Carrier: Bernie Cummins (MAI Courier)

Shipping container/cooler in good condition? Yes No

Custody seals intact on shipping container/cooler? Yes No NA

Samples Received on Ice? Yes No

Chain of custody present? Yes No

Chain of custody signed when relinquished and received? Yes No

Chain of custody agrees with sample labels? Yes No

Samples in proper containers/bottles? Yes No

Sample containers intact? Yes No

Sufficient sample volume for indicated test? Yes No

All samples received within holding time? Yes No

NASample/Temp Blank temperature

Yes No NAWater - VOA vials have zero headspace / no bubbles?

pH acceptable upon receipt (Metal: <2; 522: <4; 218.7: >8)? Yes No NA

* NOTE: If the "No" box is checked, see comments below.

Temp: 4.5°C

Chain of Custody (COC) Information

Yes NoSample IDs noted by Client on COC?

Yes NoDate and Time of collection noted by Client on COC?

Yes NoSampler's name noted on COC?

Sample Receipt Information

Sample Preservation and Hold Time (HT) Information

Sample labels checked for correct preservation? Yes No

Project Name: 0778,001.15; Limited Pre-Con Soil Assessment

(Ice Type: WET ICE )

Comments:

Total Chlorine tested and acceptable upon receipt for EPA 522? Yes No NAUCMR3 Samples:

Free Chlorine tested and acceptable upon receipt for EPA 218.7, 300.1, 537, 539?

Yes No NA

Page 40 of 40

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WorkOrder:

Report Created for: Edd Clark & Associates, Inc.

320 Professional Center Ste. 215Rohnert Park, CA 94928

Project Contact: Christopher Houlihan

Project Name: 0778,001.15; Limited Pre-Con Soil AssessmentProject P.O.:

Project Received: 08/13/2015

Analytical Report reviewed & approved for release on 08/20/2015 by:

Angela Rydelius,Laboratory Manager

1508465

The report shall not be reproduced except in full, without the written approval of the laboratory.

The analytical results relate only to the items tested. Results reported conform to the most

current NELAP standards, where applicable, unless otherwise stated in the case narrative.

Analytical Report

1534 Willow Pass Rd. Pittsburg, CA 94565 ♦ TEL: (877) 252-9262 ♦ FAX: (925) 252-9269 ♦ www.mccampbell.comNELAP: 4033ORELAP ♦ ELAP: 1644 ♦ ISO/IEC: 17025:2005 ♦ WSDE: C972-11 ♦ ADEC: UST-098 ♦ UCMR3

McCampbell Analytical, Inc."When Quality Counts"

Page 1 of 37

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Glossary of Terms & Qualifier Definitions

Client: Edd Clark & Associates, Inc.Project: 0778,001.15; Limited Pre-Con Soil AssessmentWorkOrder: 1508465

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Glossary Abbreviation

95% Interval 95% Confident IntervalDF Dilution FactorDI WET (DISTLC) Waste Extraction Test using DI waterDISS Dissolved (direct analysis of 0.45 µm filtered and acidified water sample)DUP DuplicateEDL Estimated Detection LimitITEF International Toxicity Equivalence FactorLCS Laboratory Control SampleMB Method BlankMB % Rec % Recovery of Surrogate in Method Blank, if applicableMDL Method Detection LimitML Minimum Level of QuantitationMS Matrix SpikeMSD Matrix Spike DuplicateN/A Not ApplicableND Not detected at or above the indicated MDL or RLNR Data Not Reported due to matrix interference or insufficient sample amount.PF Prep FactorRD Relative DifferenceRL Reporting Limit (The RL is the lowest calibration standard in a multipoint calibration.)RPD Relative Percent DeviationRRT Relative Retention TimeSPK Val Spike ValueSPKRef Val Spike Reference ValueSPLP Synthetic Precipitation Leachate ProcedureTCLP Toxicity Characteristic Leachate ProcedureTEQ Toxicity EquivalentsWET (STLC) Waste Extraction Test (Soluble Threshold Limit Concentration)

Analytical Qualifiers

e2 diesel range compounds are significant; no recognizable pattern

Quality Control Qualifiers

F1 MS/MSD recovery and/or RPD was out of acceptance criteria; LCS validated the prep batch.

Page 2 of 37

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Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/14/15

WorkOrder: 1508465Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-9 COMP 1508465-001A Soil 08/12/2015 08:45 GC10 108968

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Acetone ND 0.10 1 08/17/2015 15:14tert-Amyl methyl ether (TAME) ND 0.0050 1 08/17/2015 15:14Benzene ND 0.0050 1 08/17/2015 15:14Bromobenzene ND 0.0050 1 08/17/2015 15:14Bromochloromethane ND 0.0050 1 08/17/2015 15:14Bromodichloromethane ND 0.0050 1 08/17/2015 15:14Bromoform ND 0.0050 1 08/17/2015 15:14Bromomethane ND 0.0050 1 08/17/2015 15:142-Butanone (MEK) ND 0.020 1 08/17/2015 15:14t-Butyl alcohol (TBA) ND 0.050 1 08/17/2015 15:14n-Butyl benzene ND 0.0050 1 08/17/2015 15:14sec-Butyl benzene ND 0.0050 1 08/17/2015 15:14tert-Butyl benzene ND 0.0050 1 08/17/2015 15:14Carbon Disulfide ND 0.0050 1 08/17/2015 15:14Carbon Tetrachloride ND 0.0050 1 08/17/2015 15:14Chlorobenzene ND 0.0050 1 08/17/2015 15:14Chloroethane ND 0.0050 1 08/17/2015 15:14Chloroform ND 0.0050 1 08/17/2015 15:14Chloromethane ND 0.0050 1 08/17/2015 15:142-Chlorotoluene ND 0.0050 1 08/17/2015 15:144-Chlorotoluene ND 0.0050 1 08/17/2015 15:14Dibromochloromethane ND 0.0050 1 08/17/2015 15:141,2-Dibromo-3-chloropropane ND 0.0040 1 08/17/2015 15:141,2-Dibromoethane (EDB) ND 0.0040 1 08/17/2015 15:14Dibromomethane ND 0.0050 1 08/17/2015 15:141,2-Dichlorobenzene ND 0.0050 1 08/17/2015 15:141,3-Dichlorobenzene ND 0.0050 1 08/17/2015 15:141,4-Dichlorobenzene ND 0.0050 1 08/17/2015 15:14Dichlorodifluoromethane ND 0.0050 1 08/17/2015 15:141,1-Dichloroethane ND 0.0050 1 08/17/2015 15:141,2-Dichloroethane (1,2-DCA) ND 0.0040 1 08/17/2015 15:141,1-Dichloroethene ND 0.0050 1 08/17/2015 15:14cis-1,2-Dichloroethene ND 0.0050 1 08/17/2015 15:14trans-1,2-Dichloroethene ND 0.0050 1 08/17/2015 15:141,2-Dichloropropane ND 0.0050 1 08/17/2015 15:141,3-Dichloropropane ND 0.0050 1 08/17/2015 15:142,2-Dichloropropane ND 0.0050 1 08/17/2015 15:14

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 3 of 37

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Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/14/15

WorkOrder: 1508465Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-9 COMP 1508465-001A Soil 08/12/2015 08:45 GC10 108968

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

1,1-Dichloropropene ND 0.0050 1 08/17/2015 15:14cis-1,3-Dichloropropene ND 0.0050 1 08/17/2015 15:14trans-1,3-Dichloropropene ND 0.0050 1 08/17/2015 15:14Diisopropyl ether (DIPE) ND 0.0050 1 08/17/2015 15:14Ethylbenzene ND 0.0050 1 08/17/2015 15:14Ethyl tert-butyl ether (ETBE) ND 0.0050 1 08/17/2015 15:14Freon 113 ND 0.0050 1 08/17/2015 15:14Hexachlorobutadiene ND 0.0050 1 08/17/2015 15:14Hexachloroethane ND 0.0050 1 08/17/2015 15:142-Hexanone ND 0.0050 1 08/17/2015 15:14Isopropylbenzene ND 0.0050 1 08/17/2015 15:144-Isopropyl toluene ND 0.0050 1 08/17/2015 15:14Methyl-t-butyl ether (MTBE) ND 0.0050 1 08/17/2015 15:14Methylene chloride ND 0.0050 1 08/17/2015 15:144-Methyl-2-pentanone (MIBK) ND 0.0050 1 08/17/2015 15:14Naphthalene ND 0.0050 1 08/17/2015 15:14n-Propyl benzene ND 0.0050 1 08/17/2015 15:14Styrene ND 0.0050 1 08/17/2015 15:141,1,1,2-Tetrachloroethane ND 0.0050 1 08/17/2015 15:141,1,2,2-Tetrachloroethane ND 0.0050 1 08/17/2015 15:14Tetrachloroethene ND 0.0050 1 08/17/2015 15:14Toluene ND 0.0050 1 08/17/2015 15:141,2,3-Trichlorobenzene ND 0.0050 1 08/17/2015 15:141,2,4-Trichlorobenzene ND 0.0050 1 08/17/2015 15:141,1,1-Trichloroethane ND 0.0050 1 08/17/2015 15:141,1,2-Trichloroethane ND 0.0050 1 08/17/2015 15:14Trichloroethene ND 0.0050 1 08/17/2015 15:14Trichlorofluoromethane ND 0.0050 1 08/17/2015 15:141,2,3-Trichloropropane ND 0.0050 1 08/17/2015 15:141,2,4-Trimethylbenzene ND 0.0050 1 08/17/2015 15:141,3,5-Trimethylbenzene ND 0.0050 1 08/17/2015 15:14Vinyl Chloride ND 0.0050 1 08/17/2015 15:14Xylenes, Total ND 0.0050 1 08/17/2015 15:14

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 4 of 37

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Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/14/15

WorkOrder: 1508465Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-9 COMP 1508465-001A Soil 08/12/2015 08:45 GC10 108968

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Surrogates REC (%) Limits

Analyst(s): KF

Dibromofluoromethane 115 70-130 08/17/2015 15:14Toluene-d8 99 70-130 08/17/2015 15:144-BFB 107 70-130 08/17/2015 15:14Benzene-d6 89 60-140 08/17/2015 15:14Ethylbenzene-d10 99 60-140 08/17/2015 15:141,2-DCB-d4 82 60-140 08/17/2015 15:14

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 5 of 37

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Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/14/15

WorkOrder: 1508465Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-10 COMP 1508465-002A Soil 08/12/2015 09:45 GC18 108968

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Acetone ND 0.10 1 08/18/2015 14:43tert-Amyl methyl ether (TAME) ND 0.0050 1 08/18/2015 14:43Benzene ND 0.0050 1 08/18/2015 14:43Bromobenzene ND 0.0050 1 08/18/2015 14:43Bromochloromethane ND 0.0050 1 08/18/2015 14:43Bromodichloromethane ND 0.0050 1 08/18/2015 14:43Bromoform ND 0.0050 1 08/18/2015 14:43Bromomethane ND 0.0050 1 08/18/2015 14:432-Butanone (MEK) ND 0.020 1 08/18/2015 14:43t-Butyl alcohol (TBA) ND 0.050 1 08/18/2015 14:43n-Butyl benzene ND 0.0050 1 08/18/2015 14:43sec-Butyl benzene ND 0.0050 1 08/18/2015 14:43tert-Butyl benzene ND 0.0050 1 08/18/2015 14:43Carbon Disulfide ND 0.0050 1 08/18/2015 14:43Carbon Tetrachloride ND 0.0050 1 08/18/2015 14:43Chlorobenzene ND 0.0050 1 08/18/2015 14:43Chloroethane ND 0.0050 1 08/18/2015 14:43Chloroform ND 0.0050 1 08/18/2015 14:43Chloromethane ND 0.0050 1 08/18/2015 14:432-Chlorotoluene ND 0.0050 1 08/18/2015 14:434-Chlorotoluene ND 0.0050 1 08/18/2015 14:43Dibromochloromethane ND 0.0050 1 08/18/2015 14:431,2-Dibromo-3-chloropropane ND 0.0040 1 08/18/2015 14:431,2-Dibromoethane (EDB) ND 0.0040 1 08/18/2015 14:43Dibromomethane ND 0.0050 1 08/18/2015 14:431,2-Dichlorobenzene ND 0.0050 1 08/18/2015 14:431,3-Dichlorobenzene ND 0.0050 1 08/18/2015 14:431,4-Dichlorobenzene ND 0.0050 1 08/18/2015 14:43Dichlorodifluoromethane ND 0.0050 1 08/18/2015 14:431,1-Dichloroethane ND 0.0050 1 08/18/2015 14:431,2-Dichloroethane (1,2-DCA) ND 0.0040 1 08/18/2015 14:431,1-Dichloroethene ND 0.0050 1 08/18/2015 14:43cis-1,2-Dichloroethene ND 0.0050 1 08/18/2015 14:43trans-1,2-Dichloroethene ND 0.0050 1 08/18/2015 14:431,2-Dichloropropane ND 0.0050 1 08/18/2015 14:431,3-Dichloropropane ND 0.0050 1 08/18/2015 14:432,2-Dichloropropane ND 0.0050 1 08/18/2015 14:43

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 6 of 37

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Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/14/15

WorkOrder: 1508465Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-10 COMP 1508465-002A Soil 08/12/2015 09:45 GC18 108968

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

1,1-Dichloropropene ND 0.0050 1 08/18/2015 14:43cis-1,3-Dichloropropene ND 0.0050 1 08/18/2015 14:43trans-1,3-Dichloropropene ND 0.0050 1 08/18/2015 14:43Diisopropyl ether (DIPE) ND 0.0050 1 08/18/2015 14:43Ethylbenzene ND 0.0050 1 08/18/2015 14:43Ethyl tert-butyl ether (ETBE) ND 0.0050 1 08/18/2015 14:43Freon 113 ND 0.0050 1 08/18/2015 14:43Hexachlorobutadiene ND 0.0050 1 08/18/2015 14:43Hexachloroethane ND 0.0050 1 08/18/2015 14:432-Hexanone ND 0.0050 1 08/18/2015 14:43Isopropylbenzene ND 0.0050 1 08/18/2015 14:434-Isopropyl toluene ND 0.0050 1 08/18/2015 14:43Methyl-t-butyl ether (MTBE) ND 0.0050 1 08/18/2015 14:43Methylene chloride ND 0.0050 1 08/18/2015 14:434-Methyl-2-pentanone (MIBK) ND 0.0050 1 08/18/2015 14:43Naphthalene ND 0.0050 1 08/18/2015 14:43n-Propyl benzene ND 0.0050 1 08/18/2015 14:43Styrene ND 0.0050 1 08/18/2015 14:431,1,1,2-Tetrachloroethane ND 0.0050 1 08/18/2015 14:431,1,2,2-Tetrachloroethane ND 0.0050 1 08/18/2015 14:43Tetrachloroethene ND 0.0050 1 08/18/2015 14:43Toluene ND 0.0050 1 08/18/2015 14:431,2,3-Trichlorobenzene ND 0.0050 1 08/18/2015 14:431,2,4-Trichlorobenzene ND 0.0050 1 08/18/2015 14:431,1,1-Trichloroethane ND 0.0050 1 08/18/2015 14:431,1,2-Trichloroethane ND 0.0050 1 08/18/2015 14:43Trichloroethene ND 0.0050 1 08/18/2015 14:43Trichlorofluoromethane ND 0.0050 1 08/18/2015 14:431,2,3-Trichloropropane ND 0.0050 1 08/18/2015 14:431,2,4-Trimethylbenzene ND 0.0050 1 08/18/2015 14:431,3,5-Trimethylbenzene ND 0.0050 1 08/18/2015 14:43Vinyl Chloride ND 0.0050 1 08/18/2015 14:43Xylenes, Total ND 0.0050 1 08/18/2015 14:43

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 7 of 37

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Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/14/15

WorkOrder: 1508465Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-10 COMP 1508465-002A Soil 08/12/2015 09:45 GC18 108968

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Surrogates REC (%) Limits

Analyst(s): KF

Dibromofluoromethane 119 70-130 08/18/2015 14:43Toluene-d8 114 70-130 08/18/2015 14:434-BFB 117 70-130 08/18/2015 14:43Benzene-d6 110 60-140 08/18/2015 14:43Ethylbenzene-d10 115 60-140 08/18/2015 14:431,2-DCB-d4 87 60-140 08/18/2015 14:43

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 8 of 37

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Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/14/15

WorkOrder: 1508465Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-11 COMP 1508465-003A Soil 08/12/2015 10:22 GC16 108968

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Acetone ND 0.10 1 08/18/2015 00:28tert-Amyl methyl ether (TAME) ND 0.0050 1 08/18/2015 00:28Benzene ND 0.0050 1 08/18/2015 00:28Bromobenzene ND 0.0050 1 08/18/2015 00:28Bromochloromethane ND 0.0050 1 08/18/2015 00:28Bromodichloromethane ND 0.0050 1 08/18/2015 00:28Bromoform ND 0.0050 1 08/18/2015 00:28Bromomethane ND 0.0050 1 08/18/2015 00:282-Butanone (MEK) ND 0.020 1 08/18/2015 00:28t-Butyl alcohol (TBA) ND 0.050 1 08/18/2015 00:28n-Butyl benzene ND 0.0050 1 08/18/2015 00:28sec-Butyl benzene ND 0.0050 1 08/18/2015 00:28tert-Butyl benzene ND 0.0050 1 08/18/2015 00:28Carbon Disulfide ND 0.0050 1 08/18/2015 00:28Carbon Tetrachloride ND 0.0050 1 08/18/2015 00:28Chlorobenzene ND 0.0050 1 08/18/2015 00:28Chloroethane ND 0.0050 1 08/18/2015 00:28Chloroform ND 0.0050 1 08/18/2015 00:28Chloromethane ND 0.0050 1 08/18/2015 00:282-Chlorotoluene ND 0.0050 1 08/18/2015 00:284-Chlorotoluene ND 0.0050 1 08/18/2015 00:28Dibromochloromethane ND 0.0050 1 08/18/2015 00:281,2-Dibromo-3-chloropropane ND 0.0040 1 08/18/2015 00:281,2-Dibromoethane (EDB) ND 0.0040 1 08/18/2015 00:28Dibromomethane ND 0.0050 1 08/18/2015 00:281,2-Dichlorobenzene ND 0.0050 1 08/18/2015 00:281,3-Dichlorobenzene ND 0.0050 1 08/18/2015 00:281,4-Dichlorobenzene ND 0.0050 1 08/18/2015 00:28Dichlorodifluoromethane ND 0.0050 1 08/18/2015 00:281,1-Dichloroethane ND 0.0050 1 08/18/2015 00:281,2-Dichloroethane (1,2-DCA) ND 0.0040 1 08/18/2015 00:281,1-Dichloroethene ND 0.0050 1 08/18/2015 00:28cis-1,2-Dichloroethene ND 0.0050 1 08/18/2015 00:28trans-1,2-Dichloroethene ND 0.0050 1 08/18/2015 00:281,2-Dichloropropane ND 0.0050 1 08/18/2015 00:281,3-Dichloropropane ND 0.0050 1 08/18/2015 00:282,2-Dichloropropane ND 0.0050 1 08/18/2015 00:28

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 9 of 37

Page 93: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/14/15

WorkOrder: 1508465Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-11 COMP 1508465-003A Soil 08/12/2015 10:22 GC16 108968

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

1,1-Dichloropropene ND 0.0050 1 08/18/2015 00:28cis-1,3-Dichloropropene ND 0.0050 1 08/18/2015 00:28trans-1,3-Dichloropropene ND 0.0050 1 08/18/2015 00:28Diisopropyl ether (DIPE) ND 0.0050 1 08/18/2015 00:28Ethylbenzene ND 0.0050 1 08/18/2015 00:28Ethyl tert-butyl ether (ETBE) ND 0.0050 1 08/18/2015 00:28Freon 113 ND 0.0050 1 08/18/2015 00:28Hexachlorobutadiene ND 0.0050 1 08/18/2015 00:28Hexachloroethane ND 0.0050 1 08/18/2015 00:282-Hexanone ND 0.0050 1 08/18/2015 00:28Isopropylbenzene ND 0.0050 1 08/18/2015 00:284-Isopropyl toluene ND 0.0050 1 08/18/2015 00:28Methyl-t-butyl ether (MTBE) ND 0.0050 1 08/18/2015 00:28Methylene chloride ND 0.0050 1 08/18/2015 00:284-Methyl-2-pentanone (MIBK) ND 0.0050 1 08/18/2015 00:28Naphthalene ND 0.0050 1 08/18/2015 00:28n-Propyl benzene ND 0.0050 1 08/18/2015 00:28Styrene ND 0.0050 1 08/18/2015 00:281,1,1,2-Tetrachloroethane ND 0.0050 1 08/18/2015 00:281,1,2,2-Tetrachloroethane ND 0.0050 1 08/18/2015 00:28Tetrachloroethene ND 0.0050 1 08/18/2015 00:28Toluene ND 0.0050 1 08/18/2015 00:281,2,3-Trichlorobenzene ND 0.0050 1 08/18/2015 00:281,2,4-Trichlorobenzene ND 0.0050 1 08/18/2015 00:281,1,1-Trichloroethane ND 0.0050 1 08/18/2015 00:281,1,2-Trichloroethane ND 0.0050 1 08/18/2015 00:28Trichloroethene ND 0.0050 1 08/18/2015 00:28Trichlorofluoromethane ND 0.0050 1 08/18/2015 00:281,2,3-Trichloropropane ND 0.0050 1 08/18/2015 00:281,2,4-Trimethylbenzene ND 0.0050 1 08/18/2015 00:281,3,5-Trimethylbenzene ND 0.0050 1 08/18/2015 00:28Vinyl Chloride ND 0.0050 1 08/18/2015 00:28Xylenes, Total ND 0.0050 1 08/18/2015 00:28

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 10 of 37

Page 94: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/14/15

WorkOrder: 1508465Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-11 COMP 1508465-003A Soil 08/12/2015 10:22 GC16 108968

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Surrogates REC (%) Limits

Analyst(s): KF

Dibromofluoromethane 100 70-130 08/18/2015 00:28Toluene-d8 106 70-130 08/18/2015 00:284-BFB 88 70-130 08/18/2015 00:28Benzene-d6 89 60-140 08/18/2015 00:28Ethylbenzene-d10 92 60-140 08/18/2015 00:281,2-DCB-d4 69 60-140 08/18/2015 00:28

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 11 of 37

Page 95: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/14/15

WorkOrder: 1508465Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-2 COMP 1508465-004A Soil 08/12/2015 11:28 GC16 108968

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Acetone ND 0.10 1 08/18/2015 01:10tert-Amyl methyl ether (TAME) ND 0.0050 1 08/18/2015 01:10Benzene ND 0.0050 1 08/18/2015 01:10Bromobenzene ND 0.0050 1 08/18/2015 01:10Bromochloromethane ND 0.0050 1 08/18/2015 01:10Bromodichloromethane ND 0.0050 1 08/18/2015 01:10Bromoform ND 0.0050 1 08/18/2015 01:10Bromomethane ND 0.0050 1 08/18/2015 01:102-Butanone (MEK) ND 0.020 1 08/18/2015 01:10t-Butyl alcohol (TBA) ND 0.050 1 08/18/2015 01:10n-Butyl benzene ND 0.0050 1 08/18/2015 01:10sec-Butyl benzene ND 0.0050 1 08/18/2015 01:10tert-Butyl benzene ND 0.0050 1 08/18/2015 01:10Carbon Disulfide ND 0.0050 1 08/18/2015 01:10Carbon Tetrachloride ND 0.0050 1 08/18/2015 01:10Chlorobenzene ND 0.0050 1 08/18/2015 01:10Chloroethane ND 0.0050 1 08/18/2015 01:10Chloroform ND 0.0050 1 08/18/2015 01:10Chloromethane ND 0.0050 1 08/18/2015 01:102-Chlorotoluene ND 0.0050 1 08/18/2015 01:104-Chlorotoluene ND 0.0050 1 08/18/2015 01:10Dibromochloromethane ND 0.0050 1 08/18/2015 01:101,2-Dibromo-3-chloropropane ND 0.0040 1 08/18/2015 01:101,2-Dibromoethane (EDB) ND 0.0040 1 08/18/2015 01:10Dibromomethane ND 0.0050 1 08/18/2015 01:101,2-Dichlorobenzene ND 0.0050 1 08/18/2015 01:101,3-Dichlorobenzene ND 0.0050 1 08/18/2015 01:101,4-Dichlorobenzene ND 0.0050 1 08/18/2015 01:10Dichlorodifluoromethane ND 0.0050 1 08/18/2015 01:101,1-Dichloroethane ND 0.0050 1 08/18/2015 01:101,2-Dichloroethane (1,2-DCA) ND 0.0040 1 08/18/2015 01:101,1-Dichloroethene ND 0.0050 1 08/18/2015 01:10cis-1,2-Dichloroethene ND 0.0050 1 08/18/2015 01:10trans-1,2-Dichloroethene ND 0.0050 1 08/18/2015 01:101,2-Dichloropropane ND 0.0050 1 08/18/2015 01:101,3-Dichloropropane ND 0.0050 1 08/18/2015 01:102,2-Dichloropropane ND 0.0050 1 08/18/2015 01:10

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 12 of 37

Page 96: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/14/15

WorkOrder: 1508465Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-2 COMP 1508465-004A Soil 08/12/2015 11:28 GC16 108968

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

1,1-Dichloropropene ND 0.0050 1 08/18/2015 01:10cis-1,3-Dichloropropene ND 0.0050 1 08/18/2015 01:10trans-1,3-Dichloropropene ND 0.0050 1 08/18/2015 01:10Diisopropyl ether (DIPE) ND 0.0050 1 08/18/2015 01:10Ethylbenzene ND 0.0050 1 08/18/2015 01:10Ethyl tert-butyl ether (ETBE) ND 0.0050 1 08/18/2015 01:10Freon 113 ND 0.0050 1 08/18/2015 01:10Hexachlorobutadiene ND 0.0050 1 08/18/2015 01:10Hexachloroethane ND 0.0050 1 08/18/2015 01:102-Hexanone ND 0.0050 1 08/18/2015 01:10Isopropylbenzene ND 0.0050 1 08/18/2015 01:104-Isopropyl toluene ND 0.0050 1 08/18/2015 01:10Methyl-t-butyl ether (MTBE) ND 0.0050 1 08/18/2015 01:10Methylene chloride ND 0.0050 1 08/18/2015 01:104-Methyl-2-pentanone (MIBK) ND 0.0050 1 08/18/2015 01:10Naphthalene ND 0.0050 1 08/18/2015 01:10n-Propyl benzene ND 0.0050 1 08/18/2015 01:10Styrene ND 0.0050 1 08/18/2015 01:101,1,1,2-Tetrachloroethane ND 0.0050 1 08/18/2015 01:101,1,2,2-Tetrachloroethane ND 0.0050 1 08/18/2015 01:10Tetrachloroethene ND 0.0050 1 08/18/2015 01:10Toluene ND 0.0050 1 08/18/2015 01:101,2,3-Trichlorobenzene ND 0.0050 1 08/18/2015 01:101,2,4-Trichlorobenzene ND 0.0050 1 08/18/2015 01:101,1,1-Trichloroethane ND 0.0050 1 08/18/2015 01:101,1,2-Trichloroethane ND 0.0050 1 08/18/2015 01:10Trichloroethene ND 0.0050 1 08/18/2015 01:10Trichlorofluoromethane ND 0.0050 1 08/18/2015 01:101,2,3-Trichloropropane ND 0.0050 1 08/18/2015 01:101,2,4-Trimethylbenzene ND 0.0050 1 08/18/2015 01:101,3,5-Trimethylbenzene ND 0.0050 1 08/18/2015 01:10Vinyl Chloride ND 0.0050 1 08/18/2015 01:10Xylenes, Total ND 0.0050 1 08/18/2015 01:10

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 13 of 37

Page 97: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/14/15

WorkOrder: 1508465Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-2 COMP 1508465-004A Soil 08/12/2015 11:28 GC16 108968

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Surrogates REC (%) Limits

Analyst(s): KF

Dibromofluoromethane 101 70-130 08/18/2015 01:10Toluene-d8 106 70-130 08/18/2015 01:104-BFB 91 70-130 08/18/2015 01:10Benzene-d6 90 60-140 08/18/2015 01:10Ethylbenzene-d10 93 60-140 08/18/2015 01:101,2-DCB-d4 72 60-140 08/18/2015 01:10

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 14 of 37

Page 98: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/14/15

WorkOrder: 1508465Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-1 COMP 1508465-005A Soil 08/12/2015 12:14 GC16 108968

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Acetone ND 0.10 1 08/18/2015 01:53tert-Amyl methyl ether (TAME) ND 0.0050 1 08/18/2015 01:53Benzene ND 0.0050 1 08/18/2015 01:53Bromobenzene ND 0.0050 1 08/18/2015 01:53Bromochloromethane ND 0.0050 1 08/18/2015 01:53Bromodichloromethane ND 0.0050 1 08/18/2015 01:53Bromoform ND 0.0050 1 08/18/2015 01:53Bromomethane ND 0.0050 1 08/18/2015 01:532-Butanone (MEK) ND 0.020 1 08/18/2015 01:53t-Butyl alcohol (TBA) ND 0.050 1 08/18/2015 01:53n-Butyl benzene ND 0.0050 1 08/18/2015 01:53sec-Butyl benzene ND 0.0050 1 08/18/2015 01:53tert-Butyl benzene ND 0.0050 1 08/18/2015 01:53Carbon Disulfide ND 0.0050 1 08/18/2015 01:53Carbon Tetrachloride ND 0.0050 1 08/18/2015 01:53Chlorobenzene ND 0.0050 1 08/18/2015 01:53Chloroethane ND 0.0050 1 08/18/2015 01:53Chloroform ND 0.0050 1 08/18/2015 01:53Chloromethane ND 0.0050 1 08/18/2015 01:532-Chlorotoluene ND 0.0050 1 08/18/2015 01:534-Chlorotoluene ND 0.0050 1 08/18/2015 01:53Dibromochloromethane ND 0.0050 1 08/18/2015 01:531,2-Dibromo-3-chloropropane ND 0.0040 1 08/18/2015 01:531,2-Dibromoethane (EDB) ND 0.0040 1 08/18/2015 01:53Dibromomethane ND 0.0050 1 08/18/2015 01:531,2-Dichlorobenzene ND 0.0050 1 08/18/2015 01:531,3-Dichlorobenzene ND 0.0050 1 08/18/2015 01:531,4-Dichlorobenzene ND 0.0050 1 08/18/2015 01:53Dichlorodifluoromethane ND 0.0050 1 08/18/2015 01:531,1-Dichloroethane ND 0.0050 1 08/18/2015 01:531,2-Dichloroethane (1,2-DCA) ND 0.0040 1 08/18/2015 01:531,1-Dichloroethene ND 0.0050 1 08/18/2015 01:53cis-1,2-Dichloroethene ND 0.0050 1 08/18/2015 01:53trans-1,2-Dichloroethene ND 0.0050 1 08/18/2015 01:531,2-Dichloropropane ND 0.0050 1 08/18/2015 01:531,3-Dichloropropane ND 0.0050 1 08/18/2015 01:532,2-Dichloropropane ND 0.0050 1 08/18/2015 01:53

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 15 of 37

Page 99: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/14/15

WorkOrder: 1508465Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-1 COMP 1508465-005A Soil 08/12/2015 12:14 GC16 108968

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

1,1-Dichloropropene ND 0.0050 1 08/18/2015 01:53cis-1,3-Dichloropropene ND 0.0050 1 08/18/2015 01:53trans-1,3-Dichloropropene ND 0.0050 1 08/18/2015 01:53Diisopropyl ether (DIPE) ND 0.0050 1 08/18/2015 01:53Ethylbenzene ND 0.0050 1 08/18/2015 01:53Ethyl tert-butyl ether (ETBE) ND 0.0050 1 08/18/2015 01:53Freon 113 ND 0.0050 1 08/18/2015 01:53Hexachlorobutadiene ND 0.0050 1 08/18/2015 01:53Hexachloroethane ND 0.0050 1 08/18/2015 01:532-Hexanone ND 0.0050 1 08/18/2015 01:53Isopropylbenzene ND 0.0050 1 08/18/2015 01:534-Isopropyl toluene ND 0.0050 1 08/18/2015 01:53Methyl-t-butyl ether (MTBE) ND 0.0050 1 08/18/2015 01:53Methylene chloride ND 0.0050 1 08/18/2015 01:534-Methyl-2-pentanone (MIBK) ND 0.0050 1 08/18/2015 01:53Naphthalene ND 0.0050 1 08/18/2015 01:53n-Propyl benzene ND 0.0050 1 08/18/2015 01:53Styrene ND 0.0050 1 08/18/2015 01:531,1,1,2-Tetrachloroethane ND 0.0050 1 08/18/2015 01:531,1,2,2-Tetrachloroethane ND 0.0050 1 08/18/2015 01:53Tetrachloroethene ND 0.0050 1 08/18/2015 01:53Toluene ND 0.0050 1 08/18/2015 01:531,2,3-Trichlorobenzene ND 0.0050 1 08/18/2015 01:531,2,4-Trichlorobenzene ND 0.0050 1 08/18/2015 01:531,1,1-Trichloroethane ND 0.0050 1 08/18/2015 01:531,1,2-Trichloroethane ND 0.0050 1 08/18/2015 01:53Trichloroethene ND 0.0050 1 08/18/2015 01:53Trichlorofluoromethane ND 0.0050 1 08/18/2015 01:531,2,3-Trichloropropane ND 0.0050 1 08/18/2015 01:531,2,4-Trimethylbenzene ND 0.0050 1 08/18/2015 01:531,3,5-Trimethylbenzene ND 0.0050 1 08/18/2015 01:53Vinyl Chloride ND 0.0050 1 08/18/2015 01:53Xylenes, Total ND 0.0050 1 08/18/2015 01:53

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 16 of 37

Page 100: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/14/15

WorkOrder: 1508465Extraction Method: SW5030BAnalytical Method: SW8260BUnit: mg/kg

Volatile Organics by P&T and GC/MS (Basic Target List)

B-1 COMP 1508465-005A Soil 08/12/2015 12:14 GC16 108968

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Surrogates REC (%) Limits

Analyst(s): KF

Dibromofluoromethane 100 70-130 08/18/2015 01:53Toluene-d8 106 70-130 08/18/2015 01:534-BFB 90 70-130 08/18/2015 01:53Benzene-d6 93 60-140 08/18/2015 01:53Ethylbenzene-d10 98 60-140 08/18/2015 01:531,2-DCB-d4 73 60-140 08/18/2015 01:53

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

Page 17 of 37

Page 101: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/17/15-8/18/15

WorkOrder: 1508465Extraction Method: SW5030BAnalytical Method: SW8021B/8015BmUnit: mg/Kg

Gasoline Range (C6-C12) Volatile Hydrocarbons as Gasoline with BTEX and MTBE

B-9 COMP 1508465-001A Soil 08/12/2015 08:45 GC19 109095

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH(g) ND 1.0 1 08/19/2015 12:04MTBE --- 0.050 1 08/19/2015 12:04Benzene --- 0.0050 1 08/19/2015 12:04Toluene --- 0.0050 1 08/19/2015 12:04Ethylbenzene --- 0.0050 1 08/19/2015 12:04Xylenes --- 0.0050 1 08/19/2015 12:04

Surrogates REC (%) Limits

Analyst(s): IA

2-Fluorotoluene 102 70-130 08/19/2015 12:04

B-10 COMP 1508465-002A Soil 08/12/2015 09:45 GC7 109023

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH(g) ND 1.0 1 08/18/2015 16:28MTBE --- 0.050 1 08/18/2015 16:28Benzene --- 0.0050 1 08/18/2015 16:28Toluene --- 0.0050 1 08/18/2015 16:28Ethylbenzene --- 0.0050 1 08/18/2015 16:28Xylenes --- 0.0050 1 08/18/2015 16:28

Surrogates REC (%) Limits

Analyst(s): IA

2-Fluorotoluene 98 70-130 08/18/2015 16:28

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 18 of 37

Page 102: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/17/15-8/18/15

WorkOrder: 1508465Extraction Method: SW5030BAnalytical Method: SW8021B/8015BmUnit: mg/Kg

Gasoline Range (C6-C12) Volatile Hydrocarbons as Gasoline with BTEX and MTBE

B-11 COMP 1508465-003A Soil 08/12/2015 10:22 GC7 109023

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH(g) ND 1.0 1 08/18/2015 17:00MTBE --- 0.050 1 08/18/2015 17:00Benzene --- 0.0050 1 08/18/2015 17:00Toluene --- 0.0050 1 08/18/2015 17:00Ethylbenzene --- 0.0050 1 08/18/2015 17:00Xylenes --- 0.0050 1 08/18/2015 17:00

Surrogates REC (%) Limits

Analyst(s): IA

2-Fluorotoluene 102 70-130 08/18/2015 17:00

B-2 COMP 1508465-004A Soil 08/12/2015 11:28 GC7 109023

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH(g) ND 1.0 1 08/18/2015 18:02MTBE --- 0.050 1 08/18/2015 18:02Benzene --- 0.0050 1 08/18/2015 18:02Toluene --- 0.0050 1 08/18/2015 18:02Ethylbenzene --- 0.0050 1 08/18/2015 18:02Xylenes --- 0.0050 1 08/18/2015 18:02

Surrogates REC (%) Limits

Analyst(s): IA

2-Fluorotoluene 90 70-130 08/18/2015 18:02

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 19 of 37

Page 103: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/17/15-8/18/15

WorkOrder: 1508465Extraction Method: SW5030BAnalytical Method: SW8021B/8015BmUnit: mg/Kg

Gasoline Range (C6-C12) Volatile Hydrocarbons as Gasoline with BTEX and MTBE

B-1 COMP 1508465-005A Soil 08/12/2015 12:14 GC19 109023

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH(g) ND 1.0 1 08/17/2015 22:53MTBE --- 0.050 1 08/17/2015 22:53Benzene --- 0.0050 1 08/17/2015 22:53Toluene --- 0.0050 1 08/17/2015 22:53Ethylbenzene --- 0.0050 1 08/17/2015 22:53Xylenes --- 0.0050 1 08/17/2015 22:53

Surrogates REC (%) Limits

Analyst(s): IA

2-Fluorotoluene 112 70-130 08/17/2015 22:53

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

Page 20 of 37

Page 104: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/14/15

WorkOrder: 1508465Extraction Method: SW3050BAnalytical Method: SW6020Unit: mg/Kg

LUFT 5 Metals

B-9 COMP 1508465-001A Soil 08/12/2015 08:45 ICP-MS1 108956

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Cadmium ND 0.25 1 08/17/2015 19:30Chromium 86 0.50 1 08/17/2015 19:30Lead 5.9 0.50 1 08/17/2015 19:30Nickel 57 0.50 1 08/17/2015 19:30Zinc 34 5.0 1 08/17/2015 19:30

Surrogates REC (%) Limits

Analyst(s): DB

Terbium 109 70-130 08/17/2015 19:30

B-10 COMP 1508465-002A Soil 08/12/2015 09:45 ICP-MS1 108956

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Cadmium ND 0.25 1 08/17/2015 19:36Chromium 83 0.50 1 08/17/2015 19:36Lead 6.4 0.50 1 08/17/2015 19:36Nickel 57 0.50 1 08/17/2015 19:36Zinc 34 5.0 1 08/17/2015 19:36

Surrogates REC (%) Limits

Analyst(s): DB

Terbium 108 70-130 08/17/2015 19:36

B-11 COMP 1508465-003A Soil 08/12/2015 10:22 ICP-MS1 108956

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Cadmium ND 0.25 1 08/17/2015 19:42Chromium 64 0.50 1 08/17/2015 19:42Lead 6.7 0.50 1 08/17/2015 19:42Nickel 37 0.50 1 08/17/2015 19:42Zinc 32 5.0 1 08/17/2015 19:42

Surrogates REC (%) Limits

Analyst(s): DB

Terbium 109 70-130 08/17/2015 19:42

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 21 of 37

Page 105: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/14/15

WorkOrder: 1508465Extraction Method: SW3050BAnalytical Method: SW6020Unit: mg/Kg

LUFT 5 Metals

B-2 COMP 1508465-004A Soil 08/12/2015 11:28 ICP-MS1 108956

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Cadmium ND 0.25 1 08/17/2015 19:49Chromium 74 0.50 1 08/17/2015 19:49Lead 5.7 0.50 1 08/17/2015 19:49Nickel 90 0.50 1 08/17/2015 19:49Zinc 39 5.0 1 08/17/2015 19:49

Surrogates REC (%) Limits

Analyst(s): DB

Terbium 110 70-130 08/17/2015 19:49

B-1 COMP 1508465-005A Soil 08/12/2015 12:14 ICP-MS1 108956

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

Cadmium ND 0.25 1 08/17/2015 19:55Chromium 85 0.50 1 08/17/2015 19:55Lead 6.9 0.50 1 08/17/2015 19:55Nickel 94 0.50 1 08/17/2015 19:55Zinc 55 5.0 1 08/17/2015 19:55

Surrogates REC (%) Limits

Analyst(s): DB

Terbium 111 70-130 08/17/2015 19:55

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

Page 22 of 37

Page 106: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/14/15

WorkOrder: 1508465Extraction Method: SW3550B/3630CAnalytical Method: SW8015BUnit: mg/Kg

Total Extractable Petroleum Hydrocarbons with Silica Gel Clean-Up

B-9 COMP 1508465-001A Soil 08/12/2015 08:45 GC2A 108934

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH-Diesel (C10-C23) 1.9 1.0 1 08/15/2015 23:23TPH-Motor Oil (C18-C36) ND 5.0 1 08/15/2015 23:23

Surrogates REC (%) Limits

Analytical Comments: e2Analyst(s): TK

C9 91 70-130 08/15/2015 23:23

B-10 COMP 1508465-002A Soil 08/12/2015 09:45 GC2A 108934

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH-Diesel (C10-C23) ND 1.0 1 08/15/2015 20:51TPH-Motor Oil (C18-C36) ND 5.0 1 08/15/2015 20:51

Surrogates REC (%) Limits

Analyst(s): TK

C9 91 70-130 08/15/2015 20:51

B-11 COMP 1508465-003A Soil 08/12/2015 10:22 GC2A 108934

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH-Diesel (C10-C23) ND 1.0 1 08/15/2015 19:34TPH-Motor Oil (C18-C36) ND 5.0 1 08/15/2015 19:34

Surrogates REC (%) Limits

Analyst(s): TK

C9 91 70-130 08/15/2015 19:34

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP(Cont.)

Page 23 of 37

Page 107: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Analytical Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Received: 8/13/15 15:50Date Prepared: 8/14/15

WorkOrder: 1508465Extraction Method: SW3550B/3630CAnalytical Method: SW8015BUnit: mg/Kg

Total Extractable Petroleum Hydrocarbons with Silica Gel Clean-Up

B-2 COMP 1508465-004A Soil 08/12/2015 11:28 GC2A 108934

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH-Diesel (C10-C23) 1.1 1.0 1 08/15/2015 18:16TPH-Motor Oil (C18-C36) ND 5.0 1 08/15/2015 18:16

Surrogates REC (%) Limits

Analytical Comments: e2Analyst(s): TK

C9 92 70-130 08/15/2015 18:16

B-1 COMP 1508465-005A Soil 08/12/2015 12:14 GC2A 108934

Analytes Result DF Date AnalyzedRL

Client ID Lab ID Matrix Date Collected Instrument Batch ID

TPH-Diesel (C10-C23) 1.0 1.0 1 08/15/2015 15:41TPH-Motor Oil (C18-C36) ND 5.0 1 08/15/2015 15:41

Surrogates REC (%) Limits

Analytical Comments: e2Analyst(s): TK

C9 92 70-130 08/15/2015 15:41

Angela Rydelius, Lab ManagerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

Page 24 of 37

Page 108: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Quality Control Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Analyzed: 8/15/15Date Prepared: 8/14/15

WorkOrder: 1508465BatchID: 108968

Analytical Method: SW8260BUnit: mg/KgSample ID: MB/LCS-108968

1508433-017AMS/MSD

Instrument: GC10Matrix: Soil

Extraction Method: SW5030B

QC Summary Report for SW8260B

Analyte MB

Result

LCS

Result

RL SPK

Val

MB SS

%REC

LCS

%REC

LCS

Limits

Acetone ND - 0.10 - - - -tert-Amyl methyl ether (TAME) ND 0.0361 0.0050 0.050 - 72 53-116Benzene ND 0.0463 0.0050 0.050 - 93 63-137Bromobenzene ND - 0.0050 - - - -Bromochloromethane ND - 0.0050 - - - -Bromodichloromethane ND - 0.0050 - - - -Bromoform ND - 0.0050 - - - -Bromomethane ND - 0.0050 - - - -2-Butanone (MEK) ND - 0.020 - - - -t-Butyl alcohol (TBA) ND 0.168 0.050 0.20 - 84 41-135n-Butyl benzene ND - 0.0050 - - - -sec-Butyl benzene ND - 0.0050 - - - -tert-Butyl benzene ND - 0.0050 - - - -Carbon Disulfide ND - 0.0050 - - - -Carbon Tetrachloride ND - 0.0050 - - - -Chlorobenzene ND 0.0460 0.0050 0.050 - 92 77-121Chloroethane ND - 0.0050 - - - -Chloroform ND - 0.0050 - - - -Chloromethane ND - 0.0050 - - - -2-Chlorotoluene ND - 0.0050 - - - -4-Chlorotoluene ND - 0.0050 - - - -Dibromochloromethane ND - 0.0050 - - - -1,2-Dibromo-3-chloropropane ND - 0.0040 - - - -1,2-Dibromoethane (EDB) ND 0.0420 0.0040 0.050 - 84 67-119Dibromomethane ND - 0.0050 - - - -1,2-Dichlorobenzene ND - 0.0050 - - - -1,3-Dichlorobenzene ND - 0.0050 - - - -1,4-Dichlorobenzene ND - 0.0050 - - - -Dichlorodifluoromethane ND - 0.0050 - - - -1,1-Dichloroethane ND - 0.0050 - - - -1,2-Dichloroethane (1,2-DCA) ND 0.0438 0.0040 0.050 - 88 58-1351,1-Dichloroethene ND 0.0449 0.0050 0.050 - 90 42-145cis-1,2-Dichloroethene ND - 0.0050 - - - -trans-1,2-Dichloroethene ND - 0.0050 - - - -1,2-Dichloropropane ND - 0.0050 - - - -1,3-Dichloropropane ND - 0.0050 - - - -2,2-Dichloropropane ND - 0.0050 - - - -1,1-Dichloropropene ND - 0.0050 - - - -

QA/QC OfficerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

(Cont.)

Page 25 of 37

Page 109: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Quality Control Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Analyzed: 8/15/15Date Prepared: 8/14/15

WorkOrder: 1508465BatchID: 108968

Analytical Method: SW8260BUnit: mg/KgSample ID: MB/LCS-108968

1508433-017AMS/MSD

Instrument: GC10Matrix: Soil

Extraction Method: SW5030B

QC Summary Report for SW8260B

Analyte MB

Result

LCS

Result

RL SPK

Val

MB SS

%REC

LCS

%REC

LCS

Limits

cis-1,3-Dichloropropene ND - 0.0050 - - - -trans-1,3-Dichloropropene ND - 0.0050 - - - -Diisopropyl ether (DIPE) ND 0.0426 0.0050 0.050 - 85 52-129Ethylbenzene ND - 0.0050 - - - -Ethyl tert-butyl ether (ETBE) ND 0.0404 0.0050 0.050 - 81 53-125Freon 113 ND - 0.0050 - - - -Hexachlorobutadiene ND - 0.0050 - - - -Hexachloroethane ND - 0.0050 - - - -2-Hexanone ND - 0.0050 - - - -Isopropylbenzene ND - 0.0050 - - - -4-Isopropyl toluene ND - 0.0050 - - - -Methyl-t-butyl ether (MTBE) ND 0.0404 0.0050 0.050 - 81 58-122Methylene chloride ND - 0.0050 - - - -4-Methyl-2-pentanone (MIBK) ND - 0.0050 - - - -Naphthalene ND - 0.0050 - - - -n-Propyl benzene ND - 0.0050 - - - -Styrene ND - 0.0050 - - - -1,1,1,2-Tetrachloroethane ND - 0.0050 - - - -1,1,2,2-Tetrachloroethane ND - 0.0050 - - - -Tetrachloroethene ND - 0.0050 - - - -Toluene ND 0.0458 0.0050 0.050 - 92 76-1301,2,3-Trichlorobenzene ND - 0.0050 - - - -1,2,4-Trichlorobenzene ND - 0.0050 - - - -1,1,1-Trichloroethane ND - 0.0050 - - - -1,1,2-Trichloroethane ND - 0.0050 - - - -Trichloroethene ND 0.0449 0.0050 0.050 - 90 72-132Trichlorofluoromethane ND - 0.0050 - - - -1,2,3-Trichloropropane ND - 0.0050 - - - -1,2,4-Trimethylbenzene ND - 0.0050 - - - -1,3,5-Trimethylbenzene ND - 0.0050 - - - -Vinyl Chloride ND - 0.0050 - - - -Xylenes, Total ND - 0.0050 - - - -

QA/QC OfficerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

(Cont.)

Page 26 of 37

Page 110: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Quality Control Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Analyzed: 8/15/15Date Prepared: 8/14/15

WorkOrder: 1508465BatchID: 108968

Analytical Method: SW8260BUnit: mg/KgSample ID: MB/LCS-108968

1508433-017AMS/MSD

Instrument: GC10Matrix: Soil

Extraction Method: SW5030B

QC Summary Report for SW8260B

Analyte MB

Result

LCS

Result

RL SPK

Val

MB SS

%REC

LCS

%REC

LCS

Limits

Surrogate Recovery

Dibromofluoromethane 0.138 0.141 0.12 110 113 70-130Toluene-d8 0.133 0.127 0.12 106 101 70-1304-BFB 0.0150 0.0138 0.012 120 110 70-130Benzene-d6 0.0979 0.0936 0.10 98 94 60-140Ethylbenzene-d10 0.120 0.114 0.10 120 114 60-1401,2-DCB-d4 0.0886 0.0835 0.10 89 84 60-140

Analyte MS

Result

MSD

Result

SPK

Val

SPKRef

Val

MS

%REC

MSD

%REC

MS/MSD

Limits

RPD RPD

Limit

tert-Amyl methyl ether (TAME) 0.0309 0.0317 0.050 ND 62,F1 63,F1 70-130 2.39 20Benzene 0.0382 0.0394 0.050 ND 76 79 70-130 3.14 20t-Butyl alcohol (TBA) 0.134 0.138 0.20 ND 67,F1 69,F1 70-130 2.94 20Chlorobenzene 0.0381 0.0392 0.050 ND 76 78 70-130 2.84 201,2-Dibromoethane (EDB) 0.0342 0.0354 0.050 ND 69,F1 71 70-130 3.36 201,2-Dichloroethane (1,2-DCA) 0.0366 0.0376 0.050 ND 73 75 70-130 2.57 201,1-Dichloroethene 0.0360 0.0382 0.050 ND 72 76 70-130 6.08 20Diisopropyl ether (DIPE) 0.0359 0.0371 0.050 ND 72 74 70-130 3.10 20Ethyl tert-butyl ether (ETBE) 0.0342 0.0350 0.050 ND 68,F1 70 70-130 2.15 20Methyl-t-butyl ether (MTBE) 0.0337 0.0348 0.050 ND 67,F1 70 70-130 3.40 20Toluene 0.0377 0.0387 0.050 ND 75 77 70-130 2.77 20Trichloroethene 0.0392 0.0406 0.050 ND 79 81 70-130 3.24 20

Surrogate Recovery

Dibromofluoromethane 0.145 0.144 0.12 116 115 70-130 0.510 20Toluene-d8 0.125 0.125 0.12 100 100 70-130 0 204-BFB 0.0144 0.0135 0.012 115 108 70-130 6.07 20Benzene-d6 0.0798 0.0813 0.10 80 81 60-140 1.79 20Ethylbenzene-d10 0.0903 0.0919 0.10 90 92 60-140 1.74 201,2-DCB-d4 0.0658 0.0670 0.10 66 67 60-140 1.74 20

QA/QC OfficerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

Page 27 of 37

Page 111: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Quality Control Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Analyzed: 8/17/15Date Prepared: 8/17/15

WorkOrder: 1508465BatchID: 109023

Analytical Method: SW8021B/8015BmUnit: mg/KgSample ID: MB/LCS-109023

1508469-056AMS/MSD

Instrument: GC7Matrix: Soil

Extraction Method: SW5030B

QC Summary Report for SW8021B/8015Bm

Analyte MB

Result

LCS

Result

RL SPK

Val

MB SS

%REC

LCS

%REC

LCS

Limits

TPH(btex) ND 0.502 0.40 0.60 - 84 70-130MTBE ND 0.111 0.050 0.10 - 111 70-130Benzene ND 0.107 0.0050 0.10 - 107 70-130Toluene ND 0.106 0.0050 0.10 - 106 70-130Ethylbenzene ND 0.112 0.0050 0.10 - 112 70-130Xylenes ND 0.348 0.0050 0.30 - 116 70-130

Surrogate Recovery

2-Fluorotoluene 0.112 0.115 0.10 112 115 70-130

Analyte MS

Result

MSD

Result

SPK

Val

SPKRef

Val

MS

%REC

MSD

%REC

MS/MSD

Limits

RPD RPD

Limit

TPH(btex) NR NR 0.75 NR NR - NRMTBE NR NR ND NR NR - NRBenzene NR NR 0.0061 NR NR - NRToluene NR NR 0.034 NR NR - NREthylbenzene NR NR 0.0081 NR NR - NRXylenes NR NR 0.12 NR NR - NR

Surrogate Recovery

2-Fluorotoluene NR NR NR NR - NR

QA/QC OfficerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

(Cont.)

Page 28 of 37

Page 112: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Quality Control Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Analyzed: 8/19/15Date Prepared: 8/18/15

WorkOrder: 1508465BatchID: 109095

Analytical Method: SW8021B/8015BmUnit: mg/KgSample ID: MB/LCS-109095

1508583-029AMS/MSD

Instrument: GC3Matrix: Soil

Extraction Method: SW5030B

QC Summary Report for SW8021B/8015Bm

Analyte MB

Result

LCS

Result

RL SPK

Val

MB SS

%REC

LCS

%REC

LCS

Limits

TPH(btex) ND 0.662 0.40 0.60 - 110 70-130MTBE ND 0.107 0.050 0.10 - 107 70-130Benzene ND 0.118 0.0050 0.10 - 118 70-130Toluene ND 0.123 0.0050 0.10 - 123 70-130Ethylbenzene ND 0.117 0.0050 0.10 - 117 70-130Xylenes ND 0.358 0.0050 0.30 - 119 70-130

Surrogate Recovery

2-Fluorotoluene 0.103 0.106 0.10 103 106 70-130

Analyte MS

Result

MSD

Result

SPK

Val

SPKRef

Val

MS

%REC

MSD

%REC

MS/MSD

Limits

RPD RPD

Limit

TPH(btex) NR NR 8.2 NR NR - NRMTBE NR NR ND NR NR - NRBenzene NR NR 0.49 NR NR - NRToluene NR NR 0.11 NR NR - NREthylbenzene NR NR 0.76 NR NR - NRXylenes NR NR 1.7 NR NR - NR

Surrogate Recovery

2-Fluorotoluene NR NR NR NR - NR

QA/QC OfficerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

Page 29 of 37

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Quality Control Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Analyzed: 8/14/15Date Prepared: 8/14/15

WorkOrder: 1508465BatchID: 108956

Analytical Method: SW6020Unit: mg/KgSample ID: MB/LCS-108956

1508458-001AMS/MSD

Instrument: ICP-MS1Matrix: Soil

Extraction Method: SW3050B

QC Summary Report for Metals

Analyte MB

Result

LCS

Result

RL SPK

Val

MB SS

%REC

LCS

%REC

LCS

Limits

Cadmium ND 49.6 0.25 50 - 99 75-125Chromium ND 51.8 0.50 50 - 104 75-125Lead ND 49.8 0.50 50 - 100 75-125Nickel ND 51.0 0.50 50 - 102 75-125Zinc ND 523 5.0 500 - 105 75-125

Surrogate Recovery

Terbium 496 500 500 99 100 70-130

Analyte MS

Result

MSD

Result

SPK

Val

SPKRef

Val

MS

%REC

MSD

%REC

MS/MSD

Limits

RPD RPD

Limit

Cadmium 48.5 48.3 50 0.2916 96 96 75-125 0 20Chromium NR NR 50 58.24 NR NR 75-125 NR 20Lead 71.9 80.1 50 28.40 87 103 75-125 10.8 20Nickel 99.2 90.5 50 44.99 108 91 75-125 9.20 20Zinc 563 567 500 84.26 96 97 75-125 0.761 20

Surrogate Recovery

Terbium 503 495 500 101 99 70-130 1.60 20

QA/QC OfficerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

Page 30 of 37

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Quality Control Report

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client: Edd Clark & Associates, Inc.

Project: 0778,001.15; Limited Pre-Con Soil Assessment

Date Analyzed: 8/14/15Date Prepared: 8/13/15

WorkOrder: 1508465BatchID: 108934

Analytical Method: SW8015BUnit: mg/KgSample ID: MB/LCS-108934

1508432-013AMS/MSD

Instrument: GC11BMatrix: Soil

Extraction Method: SW3550B/3630C

QC Report for SW8015B with Silica Gel Clean-Up

Analyte MB

Result

LCS

Result

RL SPK

Val

MB SS

%REC

LCS

%REC

LCS

Limits

TPH-Diesel (C10-C23) ND 40.4 1.0 40 - 101 70-130TPH-Motor Oil (C18-C36) ND - 5.0 - - - -

Surrogate Recovery

C9 25.8 26.5 25 103 106 62-139

Analyte MS

Result

MSD

Result

SPK

Val

SPKRef

Val

MS

%REC

MSD

%REC

MS/MSD

Limits

RPD RPD

Limit

TPH-Diesel (C10-C23) 39.8 40.4 40 ND 99 101 70-130 1.64 30

Surrogate Recovery

C9 26.5 26.5 25 106 106 70-130 0 30

QA/QC OfficerCDPH ELAP 1644 ♦ NELAP 4033ORELAP

Page 31 of 37

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McCampbell Analytical, Inc.1534 Willow Pass RdPittsburg, CA 94565-1701(925) 252-9262

CHAIN-OF-CUSTODY RECORD Page

Lab ID Matrix Collection Date Hold

Requested Tests (See legend below)

Report to:

Christopher Houlihan

320 Professional Center Ste. 215Rohnert Park, CA 94928(707) 792-9500 FAX: (707) 792-9504

PO:

08/20/2015

Client ID

ProjectNo: 0778,001.15; Limited Pre-Con Soil Assessment

WorkOrder: 1508465

1 of 1

Date Printed:

Date Received: 08/13/2015

1 2 3 4 5 6 7 8 9 10 11 12

Edd Clark & Associates, Inc.

Bill to:

Accounts PayableEdd Clark & Associates, Inc.320 Professional Center Ste.215Rohnert Park, CA 94928

Requested TAT: 5 days;

ClientCode: ECAR

Email: [email protected]

EDF EQuIS Email HardCopy ThirdParty

[email protected]

Excel J-flagWriteOn

cc/3rd Party:

WaterTrax

A1508465-001 Soil 8/12/2015 8:45B-9 COMP A A AA1508465-002 Soil 8/12/2015 9:45B-10 COMP A A AA1508465-003 Soil 8/12/2015 10:22B-11 COMP A A AA1508465-004 Soil 8/12/2015 11:28B-2 COMP A A AA1508465-005 Soil 8/12/2015 12:14B-1 COMP A A A

Prepared by: Maria Venegas

NOTE: Soil samples are discarded 60 days after results are reported unless other arrangements are made (Water samples are 30 days). Hazardous samples will be returned to client or disposed of at client expense.

Comments: For Soil Vapor Samples ALWAYS report in ug/L AND nL/L per Brian

8260B_S G-MBTEX_S LUFTMS_6020_S TPH(DMO)WSG_S1 2 3 4 5

6 7 8 9 10

Test Legend:

11 12

The following SampIDs: 001A, 002A, 003A, 004A, 005A contain testgroup.

Page 32 of 37

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Lab ID Client ID Collection Date

& Time

Date Received:

TATMatrix Test Name Containers

/Composites

WORK ORDER SUMMARY

Work Order: 1508465

Comments: For Soil Vapor Samples ALWAYS report in ug/L AND nL/L per Brian

Client Name: EDD CLARK & ASSOCIATES, INC.Project: 0778,001.15; Limited Pre-Con Soil Assessment

QC Level: LEVEL 2

HoldDe-

chlorinated

SubOutBottle & Preservative

8/14/2015

Sediment

Content

EDF Fax Email HardCopy ThirdPartyExcel J-flagWriteOn

Christopher HoulihanClient Contact:

[email protected]'s Email:

WaterTrax

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

1508465-001A B-9 COMP 8/12/2015 8:45 5 daysSoil SW6020 (LUFT) 4 / (4:1) Acetate Liner

5 daysMulti-Range TPH(g,d,mo) w/ S.G. Clean-Up

5 daysSW8260B (VOCs)

1508465-002A B-10 COMP 8/12/2015 9:45 5 daysSoil SW6020 (LUFT) 4 / (4:1) Acetate Liner

5 daysMulti-Range TPH(g,d,mo) w/ S.G. Clean-Up

5 daysSW8260B (VOCs)

1508465-003A B-11 COMP 8/12/2015 10:22 5 daysSoil SW6020 (LUFT) 4 / (4:1) Acetate Liner

5 daysMulti-Range TPH(g,d,mo) w/ S.G. Clean-Up

5 daysSW8260B (VOCs)

1508465-004A B-2 COMP 8/12/2015 11:28 5 daysSoil SW6020 (LUFT) 4 / (4:1) Acetate Liner

5 daysMulti-Range TPH(g,d,mo) w/ S.G. Clean-Up

5 daysSW8260B (VOCs)

1508465-005A B-1 COMP 8/12/2015 12:14 5 daysSoil SW6020 (LUFT) 4 / (4:1) Acetate Liner

5 daysMulti-Range TPH(g,d,mo) w/ S.G. Clean-Up

5 daysSW8260B (VOCs)

1 of 2Page

- STLC and TCLP extractions require 2 days to complete; therefore, all TATs begin after the extraction is completed (i.e., One-day TAT yields results

in 3 days from sample submission).

NOTES:

- MAI assumes that all material present in the provided sampling container is considered part of the sample - MAI does not exclude any material from

the sample prior to sample preparation unless requested in writing by the client.

Page 33 of 37

Page 117: CITY OF PETALUMA - storage.googleapis.com€¦ · Petaluma, CA 94954 Phone (707) 778-4421 Utilities & Field Operations 202 N. McDowell Blvd. Petaluma, CA 94954 Phone (707) 778-4546

Lab ID Client ID Collection Date

& Time

Date Received:

TATMatrix Test Name Containers

/Composites

WORK ORDER SUMMARY

Work Order: 1508465

Comments: For Soil Vapor Samples ALWAYS report in ug/L AND nL/L per Brian

Client Name: EDD CLARK & ASSOCIATES, INC.Project: 0778,001.15; Limited Pre-Con Soil Assessment

QC Level: LEVEL 2

HoldDe-

chlorinated

SubOutBottle & Preservative

8/14/2015

Sediment

Content

EDF Fax Email HardCopy ThirdPartyExcel J-flagWriteOn

Christopher HoulihanClient Contact:

[email protected]'s Email:

WaterTrax

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

2 of 2Page

- STLC and TCLP extractions require 2 days to complete; therefore, all TATs begin after the extraction is completed (i.e., One-day TAT yields results

in 3 days from sample submission).

NOTES:

- MAI assumes that all material present in the provided sampling container is considered part of the sample - MAI does not exclude any material from

the sample prior to sample preparation unless requested in writing by the client.

Page 34 of 37

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Page 36 of 37

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Sample Receipt Checklist

McCampbell Analytical, Inc.1534 Willow Pass Road, Pittsburg, CA 94565-1701

Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269http://www.mccampbell.com / E-mail: [email protected]"When Quality Counts"

Client Name: Edd Clark & Associates, Inc.

WorkOrder №: 1508465

Date and Time Received: 8/13/2015 3:50:00 PM

LogIn Reviewed by: Maria Venegas

Matrix: Soil Carrier: Bernie Cummins (MAI Courier)

Shipping container/cooler in good condition? Yes No

Custody seals intact on shipping container/cooler? Yes No NA

Samples Received on Ice? Yes No

Chain of custody present? Yes No

Chain of custody signed when relinquished and received? Yes No

Chain of custody agrees with sample labels? Yes No

Samples in proper containers/bottles? Yes No

Sample containers intact? Yes No

Sufficient sample volume for indicated test? Yes No

All samples received within holding time? Yes No

NASample/Temp Blank temperature

Yes No NAWater - VOA vials have zero headspace / no bubbles?

pH acceptable upon receipt (Metal: <2; 522: <4; 218.7: >8)? Yes No NA

* NOTE: If the "No" box is checked, see comments below.

Temp: 1°C

Chain of Custody (COC) Information

Yes NoSample IDs noted by Client on COC?

Yes NoDate and Time of collection noted by Client on COC?

Yes NoSampler's name noted on COC?

Sample Receipt Information

Sample Preservation and Hold Time (HT) Information

Sample labels checked for correct preservation? Yes No

Project Name: 0778,001.15; Limited Pre-Con Soil Assessment

(Ice Type: WET ICE )

Comments:

Total Chlorine tested and acceptable upon receipt for EPA 522? Yes No NAUCMR3 Samples:

Free Chlorine tested and acceptable upon receipt for EPA 218.7, 300.1, 537, 539?

Yes No NA

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