WORK ORDER NUMBER: 17-03-0642 - ElevateBUR.com

WORK ORDER NUMBER: 17-03-0642

Analytical Report ForClient: Andersen Environmental

Client Project Name: Burbank Airport / 9836002041Attention: Brian Martasin

5261 West Imperial HighwayLos Angeles, CA 90045-6231

Approved for release on by:Stephen NowakProject Manager

AIR SOIL WATER MARINE CHEMISTRY

Eurofins Calscience, Inc. (Calscience) certifies that the test results provided in this report meet all NELAC requirements for parameters for which accreditation isrequired or available. Any exceptions to NELAC requirements are noted in the case narrative. The original report of subcontracted analyses, if any, is attached tothis report. The results in this report are limited to the sample(s) tested and any reproduction thereof must be made in its entirety. The client or recipient of thisreport is specifically prohibited from making material changes to said report and, to the extent that such changes are made, Calscience is not responsible, legally orotherwise. The client or recipient agrees to indemnify Calscience for any defense to any litigation which may arise.

04/27/2017

Supplemental Report 1

The original report has been revised toinclude the Level III deliverablespackage.

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mailto:[email protected]

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Contents

7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL: (714) 895-5494 • FAX: (714) 894-7501

Client Project Name: Burbank Airport / 9836002041

Work Order Number: 17-03-0642

1 Work Order Narrative. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

2 Sample Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

3 Detections Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

4 Client Sample Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74.1 ASTM D-2216 (M) Moisture Content (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74.2 EPA 8015B (M) Diesel and Motor Oil Ranges (Solid). . . . . . . . . . . . . . . . . . . . . . . . 84.3 EPA 6010B/7471A CAC Title 22 Metals (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . 104.4 EPA 7471A Mercury (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 164.5 EPA 8082 PCB Aroclors (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 174.6 EPA 8270C SIM PAHs (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20

5 Quality Control Sample Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 255.1 MS/MSD. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 255.2 Sample Duplicate. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 315.3 LCS/LCSD. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32

6 Sample Analysis Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38

7 Glossary of Terms and Qualifiers. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39

8 Chain-of-Custody/Sample Receipt Form. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40

9 Level III Data Package - Case Narrative. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52

9.1 ASTM D-2216 (M) Moisture Content (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58

9.2 EPA 8015 (M) Diesel and Motor Oil Ranges (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . 69

9.3 EPA 6010B Title 22 Metals (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 144

9.4 EPA 7471A Mercury (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 229

9.5 EPA 8082 PCB Aroclors (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 263

9.6 EPA 8270C SIM PAHs (Solid). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 340

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Condition Upon Receipt: Samples were received under Chain-of-Custody (COC) on 03/08/17. They were assigned to Work Order 17-03-0642. Unless otherwise noted on the Sample Receiving forms all samples were received in good condition and within the

recommended EPA temperature criteria for the methods noted on the COC. The COC and Sample Receiving Documents are

integral elements of the analytical report and are presented at the back of the report. Holding Times: All samples were analyzed within prescribed holding times (HT) and/or in accordance with the Calscience Sample Acceptance

Policy unless otherwise noted in the analytical report and/or comprehensive case narrative, if required. Any parameter identified in 40CFR Part 136.3 Table II that is designated as "analyze immediately" with a holding time of <= 15

minutes (40CFR-136.3 Table II, footnote 4), is considered a "field" test and the reported results will be qualified as being

received outside of the stated holding time unless received at the laboratory within 15 minutes of the collection time. Quality Control: All quality control parameters (QC) were within established control limits except where noted in the QC summary forms or

described further within this report. Subcontractor Information: Unless otherwise noted below (or on the subcontract form), no samples were subcontracted. Additional Comments: Air - Sorbent-extracted air methods (EPA TO-4A, EPA TO-10, EPA TO-13A, EPA TO-17): Analytical results are converted from

mass/sample basis to mass/volume basis using client-supplied air volumes. Solid - Unless otherwise indicated, solid sample data is reported on a wet weight basis, not corrected for % moisture. All QC

results are always reported on a wet weight basis.

Work Order Narrative


Work Order: 17-03-0642 Page 1 of 1

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Sample Identification Lab Number Collection Date and Time Number ofContainers

Matrix

D-DU3-S-01-08 17-03-0642-1 02/24/17 14:52 1 Solid

D-DU3-S-02-08 17-03-0642-2 02/28/17 11:44 1 Solid

D-DU3-S-03-08 17-03-0642-3 02/28/17 09:25 1 Solid

D-DU3-S-04-08 17-03-0642-4 02/28/17 10:58 1 Solid

D-DU3-S-05-08 17-03-0642-5 02/28/17 10:00 1 Solid

D-DU3-S-SG-04-08 17-03-0642-6 03/01/17 12:55 1 Solid

D-DU3-S-SG-05-08 17-03-0642-7 03/01/17 14:20 1 Solid

D-DU3-S-06-08 17-03-0642-8 03/01/17 11:07 1 Solid

D-DU3-S-07-08 17-03-0642-9 03/01/17 10:30 1 Solid

D-DU3-S-08-08 17-03-0642-10 03/01/17 09:42 1 Solid

D-DU3-S-09-08 17-03-0642-11 03/01/17 09:12 1 Solid

D-DU3-S-10-8 17-03-0642-12 03/08/17 08:27 1 Solid

D-DU3-S-11-8 17-03-0642-13 03/08/17 14:12 1 Solid

D-DU3-S-12-8 17-03-0642-14 03/08/17 11:15 1 Solid

D-DU3-S-13-8 17-03-0642-15 03/08/17 09:13 1 Solid

D-DU3-S-14-8 17-03-0642-16 03/08/17 07:53 1 Solid

D-DU3-S-15-8 17-03-0642-17 03/08/17 09:50 1 Solid

D-DU3-S-SG-01-8S 17-03-0642-18 03/08/17 13:29 1 Solid

D-DU3-S-SG-02-8S 17-03-0642-19 03/08/17 12:48 1 Solid

D-DU3-S-SG-03-8S 17-03-0642-20 03/08/17 10:15 1 Solid

COMPOSITE 17-03-0642-21 02/24/17 00:00 1 Solid

D-DU3-ISM1-8 17-03-0642-22 02/24/17 00:00 1 Solid

D-DU3-ISM2-8 17-03-0642-23 02/24/17 00:00 1 Solid

D-DU3-ISM3-8 17-03-0642-24 02/24/17 00:00 1 Solid

D-DU3-ISM4-8 17-03-0642-25 02/24/17 00:00 1 Solid

D-DU3-ISM1-8 17-03-0642-26 02/24/17 00:00 1 Solid

D-DU3-ISM2-8 17-03-0642-27 02/24/17 00:00 1 Solid

D-DU3-ISM3-8 17-03-0642-28 02/24/17 00:00 1 Solid

D-DU3-ISM4-8 17-03-0642-29 02/24/17 00:00 1 Solid

D-DU3-ISM1-8 17-03-0642-30 02/24/17 00:00 1 Solid

D-DU3-ISM2-8 17-03-0642-31 02/24/17 00:00 1 Solid

D-DU3-ISM3-8 17-03-0642-32 02/24/17 00:00 1 Solid

D-DU3-ISM4-8 17-03-0642-33 02/24/17 00:00 1 Solid

Sample Summary


Client: Andersen Environmental

5261 West Imperial Highway

Los Angeles, CA 90045-6231

Work Order: 17-03-0642

Project Name: Burbank Airport / 9836002041

PO Number:

Date/TimeReceived:

03/08/17 18:10

Number ofContainers:

33

Attn: Brian Martasin

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D-DU3-ISM1-8 (17-03-0642-26)

Moisture 3.3 BV,BU 0.10 % ASTM D-2216 (M) N/A

Mercury 0.0920 0.0821 mg/kg EPA 7471A EPA 7471A Total

D-DU3-ISM2-8 (17-03-0642-27)


D-DU3-ISM3-8 (17-03-0642-28)


D-DU3-ISM4-8 (17-03-0642-29)


D-DU3-ISM1-8 (17-03-0642-30)

Barium 74.1 0.503 mg/kg EPA 6010B EPA 3050B

Chromium 6.75 0.251 mg/kg EPA 6010B EPA 3050B

Cobalt 5.97 0.251 mg/kg EPA 6010B EPA 3050B

Copper 8.28 0.503 mg/kg EPA 6010B EPA 3050B

Lead 1.85 0.503 mg/kg EPA 6010B EPA 3050B

Nickel 5.21 0.251 mg/kg EPA 6010B EPA 3050B

Vanadium 20.5 0.251 mg/kg EPA 6010B EPA 3050B

Zinc 41.3 1.01 mg/kg EPA 6010B EPA 3050B

D-DU3-ISM2-8 (17-03-0642-31)









D-DU3-ISM3-8 (17-03-0642-32)









Detections Summary







Received: 03/08/17

Attn: Brian Martasin Page 1 of 2

Client SampleID

Analyte Result Qualifiers RL Units Method Extraction

* MDL is shown

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Subcontracted analyses, if any, are not included in this summary.

D-DU3-ISM4-8 (17-03-0642-33)









Detections Summary







Received: 03/08/17

Attn: Brian Martasin Page 2 of 2

Client SampleID

Analyte Result Qualifiers RL Units Method Extraction

* MDL is shown

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Client Sample Number Lab SampleNumber

Date/TimeCollected

Matrix Instrument DatePrepared

Date/TimeAnalyzed

QC Batch ID

D-DU3-ISM1-8 17-03-0642-26-A 02/24/1700:00

Solid N/A 03/09/17 03/09/1721:00

H0309MOIB2

Parameter Result RL DF Qualifiers

Moisture 3.3 0.10 1.00 BV,BU

D-DU3-ISM2-8 17-03-0642-27-A 02/24/1700:00

Solid N/A 03/09/17 03/09/1721:00

H0309MOIB2



D-DU3-ISM3-8 17-03-0642-28-A 02/24/1700:00

Solid N/A 03/09/17 03/09/1721:00

H0309MOIB2



D-DU3-ISM4-8 17-03-0642-29-A 02/24/1700:00

Solid N/A 03/09/17 03/09/1721:00

H0309MOIB2



Method Blank 099-05-014-6733 N/A Solid N/A 03/09/17 03/09/1721:00

H0309MOIB2


Moisture ND 0.10 1.00

Analytical Report


Andersen Environmental



Date Received: 03/08/17


Preparation: N/A

Method: ASTM D-2216 (M)

Units: %

Project: Burbank Airport / 9836002041 Page 1 of 1

RL: Reporting Limit. DF: Dilution Factor. MDL: Method Detection Limit.

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Date/TimeCollected


Date/TimeAnalyzed

QC Batch ID

D-DU3-ISM1-8 17-03-0642-26-A 02/24/1700:00

Solid GC 45 03/09/17 03/11/1711:17

170309B12

Comment(s): - Results are reported on a dry weight basis.

- Motor Oil Range Organics (C17-C44) uses a Diesel Range Organics (C10-C28) standard for quantitation and quality control.


TPH as Diesel ND 5.1 1.00

TPH as Motor Oil ND 5.1 1.00

Surrogate Rec. (%) Control Limits Qualifiers

n-Octacosane 88 61-145

D-DU3-ISM2-8 17-03-0642-27-A 02/24/1700:00

Solid GC 45 03/09/17 03/11/1711:38

170309B12








D-DU3-ISM3-8 17-03-0642-28-A 02/24/1700:00

Solid GC 45 03/09/17 03/11/1712:01

170309B12








Analytical Report







Preparation: EPA 3550B

Method: EPA 8015B (M)

Units: mg/kg



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Date/TimeCollected


Date/TimeAnalyzed

QC Batch ID

D-DU3-ISM4-8 17-03-0642-29-A 02/24/1700:00

Solid GC 45 03/09/17 03/11/1712:44

170309B12








Method Blank 099-14-353-6 N/A Solid GC 45 03/09/17 03/11/1707:21

170309B12

Comment(s): - Motor Oil Range Organics (C17-C44) uses a Diesel Range Organics (C10-C28) standard for quantitation and quality control.






Analytical Report









Units: mg/kg



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Date/TimeCollected


Date/TimeAnalyzed

QC Batch ID

D-DU3-ISM1-8 17-03-0642-30-A 02/24/1700:00

Solid ICP 7300 03/20/17 03/20/1717:26

170320L05


Antimony ND 0.754 1.01

Arsenic ND 0.754 1.01

Barium 74.1 0.503 1.01

Beryllium ND 0.251 1.01

Cadmium ND 0.503 1.01

Chromium 6.75 0.251 1.01

Cobalt 5.97 0.251 1.01

Copper 8.28 0.503 1.01

Lead 1.85 0.503 1.01

Molybdenum ND 0.251 1.01

Nickel 5.21 0.251 1.01

Selenium ND 0.754 1.01

Silver ND 0.251 1.01

Thallium ND 0.754 1.01

Vanadium 20.5 0.251 1.01

Zinc 41.3 1.01 1.01

Analytical Report








Method: EPA 6010B

Units: mg/kg



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Date/TimeCollected


Date/TimeAnalyzed

QC Batch ID

D-DU3-ISM2-8 17-03-0642-31-A 02/24/1700:00

Solid ICP 7300 03/20/17 03/20/1717:27

170320L05




Barium 66.9 0.500 1.00



Chromium 5.74 0.250 1.00

Cobalt 5.25 0.250 1.00

Copper 7.06 0.500 1.00

Lead 1.67 0.500 1.00


Nickel 4.45 0.250 1.00




Vanadium 17.7 0.250 1.00

Zinc 36.1 1.00 1.00

Analytical Report








Method: EPA 6010B

Units: mg/kg



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Date/TimeCollected


Date/TimeAnalyzed

QC Batch ID

D-DU3-ISM3-8 17-03-0642-32-A 02/24/1700:00

Solid ICP 7300 03/20/17 03/20/1717:28

170320L06




Barium 63.5 0.505 1.01



Chromium 5.75 0.253 1.01

Cobalt 4.95 0.253 1.01

Copper 6.79 0.505 1.01

Lead 1.63 0.505 1.01


Nickel 4.35 0.253 1.01




Vanadium 15.8 0.253 1.01

Zinc 32.3 1.01 1.01

Analytical Report








Method: EPA 6010B

Units: mg/kg



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Date/TimeAnalyzed

QC Batch ID

D-DU3-ISM4-8 17-03-0642-33-A 02/24/1700:00

Solid ICP 7300 03/20/17 03/20/1717:29

170320L06




Barium 73.5 0.505 1.01



Chromium 6.70 0.253 1.01

Cobalt 5.95 0.253 1.01

Copper 7.97 0.505 1.01

Lead 1.89 0.505 1.01


Nickel 5.04 0.253 1.01




Vanadium 20.1 0.253 1.01

Zinc 37.5 1.01 1.01

Analytical Report








Method: EPA 6010B

Units: mg/kg



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Date/TimeCollected


Date/TimeAnalyzed

QC Batch ID

Method Blank 097-01-002-24461 N/A Solid ICP 7300 03/20/17 03/20/1717:07

170320L05




Barium ND 0.481 0.962



Chromium ND 0.240 0.962

Cobalt ND 0.240 0.962

Copper ND 0.481 0.962

Lead ND 0.481 0.962


Nickel ND 0.240 0.962


Silver ND 0.240 0.962


Vanadium ND 0.240 0.962

Zinc ND 0.962 0.962

Analytical Report








Method: EPA 6010B

Units: mg/kg



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Date/TimeCollected


Date/TimeAnalyzed

QC Batch ID

Method Blank 097-01-002-24464 N/A Solid ICP 7300 03/20/17 03/20/1717:09

170320L06




Barium ND 0.481 0.962



Chromium ND 0.240 0.962

Cobalt ND 0.240 0.962

Copper ND 0.481 0.962

Lead ND 0.481 0.962


Nickel ND 0.240 0.962


Silver ND 0.240 0.962


Vanadium ND 0.240 0.962

Zinc ND 0.962 0.962

Analytical Report








Method: EPA 6010B

Units: mg/kg



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Date/TimeAnalyzed

QC Batch ID

D-DU3-ISM1-8 17-03-0642-26-A 02/24/1700:00

Solid Mercury 08 03/14/17 03/14/1716:27

170314L01



Mercury 0.0920 0.0821 1.00

D-DU3-ISM2-8 17-03-0642-27-A 02/24/1700:00

Solid Mercury 08 03/14/17 03/14/1716:29

170314L01



Mercury ND 0.0849 1.00

D-DU3-ISM3-8 17-03-0642-28-A 02/24/1700:00

Solid Mercury 08 03/14/17 03/14/1716:31

170314L01




D-DU3-ISM4-8 17-03-0642-29-A 02/24/1700:00

Solid Mercury 08 03/14/17 03/14/1716:38

170314L01




Method Blank 099-16-272-2870 N/A Solid Mercury 08 03/14/17 03/14/1715:52

170314L01



Analytical Report







Preparation: EPA 7471A Total

Method: EPA 7471A

Units: mg/kg



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Date/TimeAnalyzed

QC Batch ID

D-DU3-ISM1-8 17-03-0642-30-A 02/24/1700:00

Solid GC 66 03/13/17 03/16/1703:48

170313L11

Comment(s): - Sample extracted outside recommended holding time.


Aroclor-1016 ND 50 1.00 ET










Decachlorobiphenyl 76 24-168

2,4,5,6-Tetrachloro-m-Xylene 69 25-145

D-DU3-ISM2-8 17-03-0642-31-A 02/24/1700:00

Solid GC 66 03/13/17 03/16/1704:06

170313L11















Analytical Report







Preparation: EPA 3545

Method: EPA 8082

Units: ug/kg



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Date/TimeCollected


Date/TimeAnalyzed

QC Batch ID

D-DU3-ISM3-8 17-03-0642-32-A 02/24/1700:00

Solid GC 66 03/13/17 03/16/1704:24

170313L11















D-DU3-ISM4-8 17-03-0642-33-A 02/24/1700:00

Solid GC 66 03/13/17 03/16/1704:42

170313L11















Analytical Report








Method: EPA 8082

Units: ug/kg



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Date/TimeCollected


Date/TimeAnalyzed

QC Batch ID

Method Blank 099-12-535-4095 N/A Solid GC 66 03/13/17 03/16/1702:37

170313L11


Aroclor-1016 ND 50 1.00

Aroclor-1221 ND 50 1.00

Aroclor-1232 ND 50 1.00

Aroclor-1242 ND 50 1.00

Aroclor-1248 ND 50 1.00

Aroclor-1254 ND 50 1.00

Aroclor-1260 ND 50 1.00

Aroclor-1262 ND 50 1.00

Aroclor-1268 ND 50 1.00




Analytical Report








Method: EPA 8082

Units: ug/kg



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D-DU3-ISM1-8 17-03-0642-26-A 02/24/1700:00

Solid GC/MS AAA 03/10/17 03/13/1718:28

170310L04



Naphthalene ND 0.010 1.00

2-Methylnaphthalene ND 0.010 1.00


Acenaphthylene ND 0.010 1.00

Acenaphthene ND 0.010 1.00

Fluorene ND 0.010 1.00

Phenanthrene ND 0.010 1.00

Anthracene ND 0.010 1.00

Fluoranthene ND 0.010 1.00

Pyrene ND 0.010 1.00

Benzo (a) Anthracene ND 0.010 1.00

Chrysene ND 0.010 1.00

Benzo (k) Fluoranthene ND 0.010 1.00

Benzo (b) Fluoranthene ND 0.010 1.00

Benzo (a) Pyrene ND 0.010 1.00

Indeno (1,2,3-c,d) Pyrene ND 0.010 1.00

Dibenz (a,h) Anthracene ND 0.010 1.00

Benzo (g,h,i) Perylene ND 0.010 1.00


2-Fluorobiphenyl 79 13-127

Nitrobenzene-d5 89 17-137

p-Terphenyl-d14 90 4-160

Analytical Report








Method: EPA 8270C SIM PAHs

Units: mg/kg



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Date/TimeCollected


Date/TimeAnalyzed

QC Batch ID

D-DU3-ISM2-8 17-03-0642-27-A 02/24/1700:00

Solid GC/MS AAA 03/10/17 03/13/1718:47

170310L04

























Analytical Report









Units: mg/kg



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Date/TimeAnalyzed

QC Batch ID

D-DU3-ISM3-8 17-03-0642-28-A 02/24/1700:00

Solid GC/MS AAA 03/10/17 03/13/1719:07

170310L04

























Analytical Report









Units: mg/kg



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Date/TimeCollected


Date/TimeAnalyzed

QC Batch ID

D-DU3-ISM4-8 17-03-0642-29-A 02/24/1700:00

Solid GC/MS AAA 03/10/17 03/13/1719:27

170310L04

























Analytical Report









Units: mg/kg



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Date/TimeCollected


Date/TimeAnalyzed

QC Batch ID

Method Blank 099-14-035-380 N/A Solid GC/MS AAA 03/10/17 03/13/1717:09

170310L04
























Analytical Report









Units: mg/kg



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Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed MS/MSD Batch Number

17-03-0590-25 Sample Solid GC 45 03/09/17 03/11/17 08:46 170309S12

17-03-0590-25 Matrix Spike Solid GC 45 03/09/17 03/11/17 08:03 170309S12

17-03-0590-25 Matrix Spike Duplicate Solid GC 45 03/09/17 03/11/17 08:24 170309S12

Parameter SampleConc.

SpikeAdded

MSConc.

MS%Rec.

MSDConc.

MSD%Rec.

%Rec. CL RPD RPD CL Qualifiers

TPH as Diesel ND 400.0 361.3 90 394.8 99 61-145 9 0-25

Quality Control - Spike/Spike Duplicate










RPD: Relative Percent Difference. CL: Control Limits

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17-03-1188-1 Sample Solid ICP 7300 03/20/17 03/20/17 17:45 170320S05

17-03-1188-1 Matrix Spike Solid ICP 7300 03/20/17 03/20/17 17:46 170320S05

17-03-1188-1 Matrix Spike Duplicate Solid ICP 7300 03/20/17 03/20/17 17:47 170320S05


SpikeAdded

MSConc.

MS%Rec.

MSDConc.

MSD%Rec.


Antimony 0.9236 25.00 10.72 39 11.99 44 50-115 11 0-20 3

Arsenic 1.838 25.00 26.00 97 28.92 108 75-125 11 0-20

Barium 186.3 25.00 205.1 4X 203.1 4X 75-125 4X 0-20 Q

Beryllium 0.5630 25.00 27.08 106 28.63 112 75-125 6 0-20

Cadmium ND 25.00 25.62 102 27.45 110 75-125 7 0-20

Chromium 23.50 25.00 46.98 94 52.70 117 75-125 11 0-20

Cobalt 15.33 25.00 38.82 94 41.44 104 75-125 7 0-20

Copper 30.48 25.00 56.19 103 60.74 121 75-125 8 0-20

Lead 6.808 25.00 31.40 98 34.53 111 75-125 9 0-20

Molybdenum ND 25.00 20.03 80 22.07 88 75-125 10 0-20

Nickel 25.72 25.00 49.98 97 54.35 115 75-125 8 0-20

Selenium 0.8236 25.00 23.79 92 26.76 104 75-125 12 0-20

Silver ND 12.50 12.78 102 11.89 95 75-125 7 0-20

Thallium ND 25.00 16.26 65 23.45 94 75-125 36 0-20 3,4

Vanadium 50.20 25.00 71.16 84 76.62 106 75-125 7 0-20

Zinc 48.96 25.00 82.91 136 85.90 148 75-125 4 0-20 3









Method: EPA 6010B



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17-03-1189-1 Sample Solid ICP 7300 03/20/17 03/20/17 17:47 170320S06

17-03-1189-1 Matrix Spike Solid ICP 7300 03/20/17 03/20/17 17:48 170320S06

17-03-1189-1 Matrix Spike Duplicate Solid ICP 7300 03/20/17 03/20/17 17:49 170320S06


SpikeAdded

MSConc.

MS%Rec.

MSDConc.

MSD%Rec.


Antimony ND 25.00 14.70 59 12.04 48 50-115 20 0-20 3

Arsenic 3.184 25.00 33.40 121 30.64 110 75-125 9 0-20

Barium 361.9 25.00 349.1 4X 351.3 4X 75-125 4X 0-20 Q

Beryllium ND 25.00 30.06 120 27.75 111 75-125 8 0-20

Cadmium 0.8055 25.00 29.31 114 26.55 103 75-125 10 0-20

Chromium 24.87 25.00 47.52 91 45.20 81 75-125 5 0-20

Cobalt 10.62 25.00 37.25 107 34.62 96 75-125 7 0-20

Copper 228.1 25.00 254.2 4X 260.9 4X 75-125 4X 0-20 Q

Lead 16.64 25.00 43.91 109 40.02 94 75-125 9 0-20

Molybdenum 1.212 25.00 28.86 111 25.79 98 75-125 11 0-20

Nickel 26.77 25.00 48.51 87 45.69 76 75-125 6 0-20

Selenium 1.309 25.00 28.97 111 26.10 99 75-125 10 0-20

Silver ND 12.50 13.45 108 13.35 107 75-125 1 0-20

Thallium ND 25.00 25.40 102 22.76 91 75-125 11 0-20

Vanadium 52.06 25.00 73.17 84 71.52 78 75-125 2 0-20

Zinc 581.8 25.00 570.8 4X 517.5 4X 75-125 4X 0-20 Q









Method: EPA 6010B



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17-03-0566-1 Sample Solid Mercury 08 03/14/17 03/14/17 15:57 170314S01

17-03-0566-1 Matrix Spike Solid Mercury 08 03/14/17 03/14/17 15:59 170314S01

17-03-0566-1 Matrix Spike Duplicate Solid Mercury 08 03/14/17 03/14/17 16:02 170314S01


SpikeAdded

MSConc.

MS%Rec.

MSDConc.

MSD%Rec.


Mercury 0.1355 0.8350 0.8591 87 0.8413 85 71-137 2 0-14









Method: EPA 7471A



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D-DU3-ISM1-8 Sample Solid GC 66 03/13/17 03/16/17 03:48 170313S11

D-DU3-ISM1-8 Matrix Spike Solid GC 66 03/13/17 03/16/17 03:13 170313S11

D-DU3-ISM1-8 Matrix Spike Duplicate Solid GC 66 03/13/17 03/16/17 03:31 170313S11


SpikeAdded

MSConc.

MS%Rec.

MSDConc.

MSD%Rec.


Aroclor-1016 ND 100.0 83.00 83 82.50 82 50-135 1 0-20

Aroclor-1260 ND 100.0 84.50 84 85.00 85 50-135 1 0-20









Method: EPA 8082



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17-03-0641-26 Sample Solid GC/MS AAA 03/10/17 03/13/17 19:46 170310S04

17-03-0641-26 Matrix Spike Solid GC/MS AAA 03/10/17 03/14/17 12:30 170310S04

17-03-0641-26 Matrix Spike Duplicate Solid GC/MS AAA 03/10/17 03/13/17 18:08 170310S04


SpikeAdded

MSConc.

MS%Rec.

MSDConc.

MSD%Rec.


Naphthalene ND 0.1000 0.09218 92 0.08516 85 20-150 8 0-33

2-Methylnaphthalene ND 0.1000 0.1045 104 0.09445 94 29-137 10 0-31

1-Methylnaphthalene ND 0.1000 0.09569 96 0.08605 86 34-136 11 0-29

Acenaphthylene ND 0.1000 0.08040 80 0.07537 75 29-131 6 0-32

Acenaphthene ND 0.1000 0.08276 83 0.07798 78 29-137 6 0-28

Fluorene ND 0.1000 0.08493 85 0.07855 79 36-132 8 0-27

Phenanthrene ND 0.1000 0.09732 97 0.09182 92 20-144 6 0-27

Anthracene ND 0.1000 0.1009 101 0.09138 91 26-134 10 0-27

Fluoranthene ND 0.1000 0.09398 94 0.08904 89 20-151 5 0-26

Pyrene ND 0.1000 0.1040 104 0.09233 92 20-150 12 0-32

Benzo (a) Anthracene ND 0.1000 0.09475 95 0.09013 90 24-150 5 0-24

Chrysene ND 0.1000 0.09979 100 0.08850 88 25-145 12 0-28

Benzo (k) Fluoranthene ND 0.1000 0.1023 102 0.09310 93 28-148 9 0-26

Benzo (b) Fluoranthene ND 0.1000 0.08982 90 0.08694 87 21-153 3 0-26

Benzo (a) Pyrene ND 0.1000 0.09441 94 0.08980 90 29-149 5 0-22

Indeno (1,2,3-c,d) Pyrene ND 0.1000 0.08802 88 0.08785 88 20-154 0 0-25

Dibenz (a,h) Anthracene ND 0.1000 0.08938 89 0.08940 89 20-132 0 0-26

Benzo (g,h,i) Perylene ND 0.1000 0.08732 87 0.09140 91 20-148 5 0-27












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Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed Duplicate Batch Number

17-03-0643-29 Sample Solid N/A 03/09/17 00:00 03/09/17 21:00 H0309MOID2

17-03-0643-29 Sample Duplicate Solid N/A 03/09/17 00:00 03/09/17 21:00 H0309MOID2

Parameter Sample Conc. DUP Conc. RPD RPD CL Qualifiers

Moisture 3.300 3.100 6 0-10

Quality Control - Sample Duplicate







Preparation: N/A

Method: ASTM D-2216 (M)



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Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS Batch Number

099-14-353-6 LCS Solid GC 45 03/09/17 03/11/17 07:42 170309B12

Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL Qualifiers

TPH as Diesel 400.0 407.8 102 61-145

Quality Control - LCS











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Total number of LCS compounds: 16

Total number of ME compounds: 0

Total number of ME compounds allowed: 1

LCS ME CL validation result: Pass


097-01-002-24461 LCS Solid ICP 7300 03/20/17 03/20/17 17:08 170320L05

Parameter Spike Added Conc. Recovered LCS %Rec. %Rec. CL ME CL Qualifiers

Antimony 25.00 22.35 89 80-120 73-127

Arsenic 25.00 22.51 90 80-120 73-127

Barium 25.00 24.20 97 80-120 73-127

Beryllium 25.00 23.17 93 80-120 73-127

Cadmium 25.00 23.22 93 80-120 73-127

Chromium 25.00 23.34 93 80-120 73-127

Cobalt 25.00 24.11 96 80-120 73-127

Copper 25.00 23.06 92 80-120 73-127

Lead 25.00 23.73 95 80-120 73-127

Molybdenum 25.00 22.93 92 80-120 73-127

Nickel 25.00 24.17 97 80-120 73-127

Selenium 25.00 22.92 92 80-120 73-127

Silver 12.50 10.79 86 80-120 73-127

Thallium 25.00 23.74 95 80-120 73-127

Vanadium 25.00 22.08 88 80-120 73-127

Zinc 25.00 23.35 93 80-120 73-127









Method: EPA 6010B



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097-01-002-24464 LCS Solid ICP 7300 03/20/17 03/20/17 17:10 170320L06


Antimony 25.00 23.02 92 80-120 73-127

Arsenic 25.00 23.12 92 80-120 73-127

Barium 25.00 24.45 98 80-120 73-127

Beryllium 25.00 23.24 93 80-120 73-127

Cadmium 25.00 23.40 94 80-120 73-127

Chromium 25.00 23.52 94 80-120 73-127

Cobalt 25.00 24.61 98 80-120 73-127

Copper 25.00 23.20 93 80-120 73-127

Lead 25.00 24.06 96 80-120 73-127

Molybdenum 25.00 23.39 94 80-120 73-127

Nickel 25.00 24.65 99 80-120 73-127

Selenium 25.00 23.65 95 80-120 73-127

Silver 12.50 10.96 88 80-120 73-127

Thallium 25.00 24.14 97 80-120 73-127

Vanadium 25.00 22.32 89 80-120 73-127

Zinc 25.00 23.81 95 80-120 73-127









Method: EPA 6010B



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099-16-272-2870 LCS Solid Mercury 08 03/14/17 03/14/17 15:55 170314L01


Mercury 0.8350 0.8050 96 85-121









Method: EPA 7471A



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099-12-535-4095 LCS Solid GC 66 03/13/17 03/16/17 02:55 170313L11


Aroclor-1016 100.0 84.00 84 50-135

Aroclor-1260 100.0 85.00 85 50-135









Method: EPA 8082



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099-14-035-380 LCS Solid GC/MS AAA 03/10/17 03/13/17 17:28 170310L04


Naphthalene 0.1000 0.06679 67 51-129 38-142

2-Methylnaphthalene 0.1000 0.07206 72 50-127 37-140

1-Methylnaphthalene 0.1000 0.06639 66 54-132 41-145

Acenaphthylene 0.1000 0.05763 58 50-123 38-135

Acenaphthene 0.1000 0.05903 59 53-125 41-137

Fluorene 0.1000 0.06071 61 55-127 43-139

Phenanthrene 0.1000 0.07239 72 50-122 38-134

Anthracene 0.1000 0.07105 71 50-132 36-146

Fluoranthene 0.1000 0.07754 78 55-127 43-139

Pyrene 0.1000 0.07831 78 50-134 36-148

Benzo (a) Anthracene 0.1000 0.08311 83 50-133 36-147

Chrysene 0.1000 0.08263 83 51-129 38-142

Benzo (k) Fluoranthene 0.1000 0.08987 90 49-150 32-167

Benzo (b) Fluoranthene 0.1000 0.08263 83 50-142 35-157

Benzo (a) Pyrene 0.1000 0.08523 85 50-134 36-148

Indeno (1,2,3-c,d) Pyrene 0.1000 0.08255 83 50-148 34-164

Dibenz (a,h) Anthracene 0.1000 0.08511 85 50-133 36-147

Benzo (g,h,i) Perylene 0.1000 0.08546 85 50-130 37-143












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Method Extraction Chemist ID Instrument Analytical Location

ASTM D-2216 (M) N/A 1009 N/A 1

EPA 6010B EPA 3050B 935 ICP 7300 1

EPA 7471A EPA 7471A Total 868 Mercury 08 1

EPA 8015B (M) EPA 3550B 972 GC 45 1

EPA 8082 EPA 3545 669 GC 66 1

EPA 8270C SIM PAHs EPA 3545 907 GC/MS AAA 1

Sample Analysis Summary Report



Location 1: 7440 Lincoln Way, Garden Grove, CA 92841

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Qualifiers Definition

* See applicable analysis comment.

< Less than the indicated value.

> Greater than the indicated value.

1 Surrogate compound recovery was out of control due to a required sample dilution. Therefore, the sample data was reported without furtherclarification.

2 Surrogate compound recovery was out of control due to matrix interference. The associated method blank surrogate spike compound wasin control and, therefore, the sample data was reported without further clarification.

3 Recovery of the Matrix Spike (MS) or Matrix Spike Duplicate (MSD) compound was out of control due to suspected matrix interference. Theassociated LCS recovery was in control.

4 The MS/MSD RPD was out of control due to suspected matrix interference.

5 The PDS/PDSD or PES/PESD associated with this batch of samples was out of control due to suspected matrix interference.

6 Surrogate recovery below the acceptance limit.

7 Surrogate recovery above the acceptance limit.

B Analyte was present in the associated method blank.

BU Sample analyzed after holding time expired.

BV Sample received after holding time expired.

CI See case narrative.

E Concentration exceeds the calibration range.

ET Sample was extracted past end of recommended max. holding time.

HD The chromatographic pattern was inconsistent with the profile of the reference fuel standard.

HDH The sample chromatographic pattern for TPH matches the chromatographic pattern of the specified standard but heavier hydrocarbonswere also present (or detected).

HDL The sample chromatographic pattern for TPH matches the chromatographic pattern of the specified standard but lighter hydrocarbons werealso present (or detected).

J Analyte was detected at a concentration below the reporting limit and above the laboratory method detection limit. Reported value isestimated.

JA Analyte positively identified but quantitation is an estimate.

ME LCS Recovery Percentage is within Marginal Exceedance (ME) Control Limit range (+/- 4 SD from the mean).

ND Parameter not detected at the indicated reporting limit.

Q Spike recovery and RPD control limits do not apply resulting from the parameter concentration in the sample exceeding the spikeconcentration by a factor of four or greater.

SG The sample extract was subjected to Silica Gel treatment prior to analysis.

X % Recovery and/or RPD out-of-range.

Z Analyte presence was not confirmed by second column or GC/MS analysis.

Solid - Unless otherwise indicated, solid sample data is reported on a wet weight basis, not corrected for % moisture. All QC results arereported on a wet weight basis.

Any parameter identified in 40CFR Part 136.3 Table II that is designated as "analyze immediately" with a holding time of <= 15 minutes(40CFR-136.3 Table II, footnote 4), is considered a "field" test and the reported results will be qualified as being received outside of thestated holding time unless received at the laboratory within 15 minutes of the collection time.

A calculated total result (Example: Total Pesticides) is the summation of each component concentration and/or, if "J" flags are reported,estimated concentration. Component concentrations showing not detected (ND) are summed into the calculated total result as zeroconcentrations.

Glossary of Terms and Qualifiers



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Number

Lab

ID

Grab

Composite

Water

Soil

Vapor

Other

Cold (4° C)

HNO3

NaHSO4

HCl

Tim

e

1X

XX

2/24

,2/2

8,3/

1,3/

8X

XX

XX

XX

2X

XX

XX

XX

XX

X

3X

XX

XX

XX

XX

X

4X

XX

2/24

,2/2

8,3/

1,3/

8X

XX

XX

XX

5X

XX

2/24

,2/2

8,3/

1,3/

8X

XX

XX

XX

6X

XX

2/24

,2/2

8,3/

1,3/

8X

XX

XX

XX

7X

XX

2/24

,2/2

8,3/

1,3/

8X

XX

XX

XX

8X

XX

2/24

,2/2

8,3/

1,3/

8X

XX

XX

XX

9X

XX

2/24

,2/2

8,3/

1,3/

8X

X

10X

XX

2/24

,2/2

8,3/

1,3/

8X

X

11X

XX

2/24

,2/2

8,3/

1,3/

8X

X

12X

XX

2/24

,2/2

8,3/

1,3/

8X

X

13 14 15 16 17 18 19 20Da

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8/17

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D-D

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3-15

D-D

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2-8

D-D

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D-D

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4-8

D-D

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ERPH, EPA Method 8015M

Composite Hold

4- or 8-ounce Glass

VOA

EZ Draw (EPA 5035)

Lead, EPA Method 6010B

Arsenic, EPA Method 6010B

STLC Lead EPA Method

TCLP Lead EPA Method

PCBs, EPA Method 8082

TPH full chain, EPA Method 8015M

Page

1 o

f 1

Met

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Con

tain

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rnar

ound

Tim

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Job

# 98

3600

2041

VOCs, EPA Method 8260B

PAHs, EPA Method 8270C

Metals, EPA Method 6010B/7470A

Proj

ect M

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B. M

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by:

G. B

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Case Narrative Client Project Name: Burbank Airport / 9836002041


Page 1 of 6

CONDITION UPON RECEIPT:

Eurofins Calscience, Inc. received (20) solid samples on February 24, 28 and March 1, 8, 2017. A total of (20) containers were received in good condition and at temperatures of 3.2oC, 1.8oC, and 2.0oC, which were within the recommended temperature of 0oC – 6oC.

Client Sample ID Lab Sample ID Date & Time Sampled Date & Time Received D-DU3-S-01-08 17-03-0642-1 02/24/17 14:52 03/08/17 18:10 D-DU3-S-02-08 17-03-0642-2 02/28/17 11:44 03/08/17 18:10 D-DU3-S-03-08 17-03-0642-3 02/28/17 09:25 03/08/17 18:10 D-DU3-S-04-08 17-03-0642-4 02/28/17 10:58 03/08/17 18:10 D-DU3-S-05-08 17-03-0642-5 02/28/17 10:00 03/08/17 18:10

D-DU3-S-SG-04-08 17-03-0642-6 03/01/17 12:55 03/08/17 18:10 D-DU3-S-SG-05-08 17-03-0642-7 03/01/17 14:20 03/08/17 18:10

D-DU3-S-06-08 17-03-0642-8 03/01/17 11:07 03/08/17 18:10 D-DU3-S-07-08 17-03-0642-9 03/01/17 10:30 03/08/17 18:10 D-DU3-S-08-08 17-03-0642-10 03/01/17 09:42 03/08/17 18:10 D-DU3-S-09-08 17-03-0642-11 03/01/17 09:12 03/08/17 18:10 D-DU3-S-10-8 17-03-0642-12 03/08/17 08:27 03/08/17 18:10 D-DU3-S-11-8 17-03-0642-13 03/08/17 14:12 03/08/17 18:10 D-DU3-S-12-8 17-03-0642-14 03/08/17 11:15 03/08/17 18:10 D-DU3-S-13-8 17-03-0642-15 03/08/17 09:13 03/08/17 18:10 D-DU3-S-14-8 17-03-0642-16 03/08/17 07:53 03/08/17 18:10 D-DU3-S-15-8 17-03-0642-17 03/08/17 09:50 03/08/17 18:10

D-DU3-S-SG-01-8S 17-03-0642-18 03/08/17 13:29 03/08/17 18:10 D-DU3-S-SG-02-8S 17-03-0642-19 03/08/17 12:48 03/08/17 18:10 D-DU3-S-SG-03-8S 17-03-0642-20 03/08/17 10:15 03/08/17 18:10

COMPOSITE 17-03-0642-21 02/24/17 00:00 03/08/17 18:10 D-DU3-ISM1-8 17-03-0642-22 02/24/17 00:00 03/08/17 18:10 D-DU3-ISM2-8 17-03-0642-23 02/24/17 00:00 03/08/17 18:10 D-DU3-ISM3-8 17-03-0642-24 02/24/17 00:00 03/08/17 18:10 D-DU3-ISM4-8 17-03-0642-25 02/24/17 00:00 03/08/17 18:10 D-DU3-ISM1-8 17-03-0642-26 02/24/17 00:00 03/08/17 18:10 D-DU3-ISM2-8 17-03-0642-27 02/24/17 00:00 03/08/17 18:10 D-DU3-ISM3-8 17-03-0642-28 02/24/17 00:00 03/08/17 18:10 D-DU3-ISM4-8 17-03-0642-29 02/24/17 00:00 03/08/17 18:10 D-DU3-ISM1-8 17-03-0642-30 02/24/17 00:00 03/08/17 18:10 D-DU3-ISM2-8 17-03-0642-31 02/24/17 00:00 03/08/17 18:10 D-DU3-ISM3-8 17-03-0642-32 02/24/17 00:00 03/08/17 18:10


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Page 2 of 6

Client Sample ID Lab Sample ID Date & Time Sampled Date & Time Received D-DU3-ISM4-8 17-03-0642-33 02/24/17 00:00 03/08/17 18:10

DATA SUMMARY:

As per the chain of custody (COC), the samples were analyzed using one or more of the following methodologies:

ASTM D-2216 (M) Moisture Content (Solid) EPA 6010B Title 22 Metals (Solid) EPA 7471A Mercury (Solid) EPA 8015B (M) Diesel and Motor Oil Ranges (Solid) EPA 8082 PCB Aroclors (Solid) EPA 8270C SIM PAHs (Solid)

The samples were analyzed within the suggested EPA holding time for the requested methods unless otherwise noted.

Sample results were reported in the RL format.

The sample data is reported in dry weight. The instrument printouts do not reflect the correction for dry weight.

Any dilutions made to the sample(s) and/or QC will be noted in the following narrative. Reporting limits have been adjusted accordingly.

Manual integrations made to the data will be noted in the following narrative. The before and amended chromatograms have been included in the data package.

All sample and analytical QC are within acceptance criteria unless otherwise noted.

ASTM D-2216 (M) Moisture Content (Solid):

Samples -26 through -29 were analyzed for % Moisture by ASTM D-2216 (M). The samples were prepared and analyzed on 03/09/17 in batch #s H0309MOIB2 / H0309MOID2.

Samples -26 through -29 were analyzed after holding time expired.

Balance Calibration/Verification:

All values were within acceptance criteria.


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Sample and QC:

A sample from a different work order was used as the sample duplicate for quality control. The method blank was non-detect and the duplicate analysis was within acceptance criteria.

EPA 6010B Title 22 Metals (Solid):

Samples -30 through -33 were analyzed for Metals by EPA 6010B. The samples were prepared and analyzed on 03/20/17 in batch #s 170320L05 / 170320S05 and 170320L06 / 170320S06 on ICP 7300.

Initial Calibration, Initial Calibration Verification, and Initial Calibration Blank:


Continuing Calibration Verification and Continuing Calibration Blank:


ICS A/AB:


Sample and QC:

QC Batch #s 170320L05 / 170320S05: (Associated with samples -30 and -31)

The method blank was non-detect and the LCS was within acceptance criteria.

A non-client sample was used for the MS/MSD; refer to the MS/MSD summary form for further information.

QC Batch #s 170320L06 / 170320S06: (Associated with samples -32 and -33)



EPA 7471A Mercury (Solid):

Samples -26 through -29 were analyzed for Mercury by EPA 7471A. The samples were prepared and analyzed on 03/14/17 in batch #s 170314L01 / 170314S01 on Mercury 08.


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Initial Calibration, Initial Calibration Verification, and Initial Calibration Blank:


Continuing Calibration Verification and Continuing Calibration Blank:


Sample and QC:



EPA 8015B (M) Diesel and Motor Oil Ranges (Solid):

Samples -26 through -29 were analyzed for Diesel and Motor Oil Ranges by EPA 8015B (M). The samples were prepared on 03/09/17 and analyzed on 03/11/17 in batch #s 170309B12 / 170309S12 on GC 45.

Initial Calibration and Initial Calibration Verification:

The initial calibration was performed on 12/02/16 on GC 45. The ICAL was within the 20% RSD acceptance criteria and the ICV was within the 30% D acceptance criteria.

For the Diesel and Motor Oil Ranges, Diesel is used for the initial calibration and spiking standards. The surrogate recoveries for the samples and QC were calculated from the 5-point surrogate curve analyzed with the Diesel ICAL.

Continuing Calibration Verification:

All values were within the 20% D acceptance criteria.

Sample and QC:

A sample from a different work order was used for the MS/MSD. The method blank was non-detect; the LCS, MS/MSD, and all surrogate recoveries were within acceptance criteria.


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EPA 8082 PCB Aroclors (Solid):

Samples -30 through -33 were analyzed for Polychlorinated Biphenyls Aroclors by EPA 8082. The samples were prepared on 03/13/17 and analyzed on 03/16/17 in batch #s 170313L11 / 170313S11 on GC 66.

Samples -30 through -33 were extracted outside recommended holding time.


The initial calibration was performed on 02/22/17 on GC 66. The ICAL was within the 20% RSD acceptance criteria and the ICV was within the 15% D acceptance criteria for Aroclors 1016 and 1260. Single point response factors were generated for all other Aroclors.



Sample and QC:

Sample -30 was used for the MS/MSD. The method blank was non-detect; the LCS, MS/MSD, and all surrogate recoveries were within acceptance criteria.

EPA 8270C SIM PAHs (Solid):

Samples -26 through -29 were analyzed for Polynuclear Aromatic Hydrocarbons by EPA 8270C SIM. The samples were prepared on 03/10/17 and analyzed on 03/13/17 in batch #s 170310L04 / 170310S04 on GC/MS AAA.


The initial calibration was performed on 03/13/17 on GC/MS AAA. The ICAL was within the 15% RSD acceptance criteria and the ICV was within the 20% D acceptance criteria.



Tuning Standards:

All instrument tuning standards (DFTPP) were within acceptance criteria.


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Sample and QC:

A sample from a different work order was used for the MS/MSD. The method blank was non-detect; the LCS, MS/MSD, all surrogate and internal standard recoveries were within acceptance criteria.


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WORK ORDER NUMBER: 17-03-0642 - ElevateBUR.com

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Transcript of WORK ORDER NUMBER: 17-03-0642 - ElevateBUR.com