UVX/LNLS - sites.ifi.unicamp.br · Vertically collimating mirror (VCM): Water cooled Three stripes,...

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UVX/LNLS 1.37 GeV 4 straight sections: 1 regular Wiggler for PX – MX2 beamline 1 undulator for soft x-rays - PGM beamline Superconducting Wiggler – XDS beamline

Transcript of UVX/LNLS - sites.ifi.unicamp.br · Vertically collimating mirror (VCM): Water cooled Three stripes,...

Page 1: UVX/LNLS - sites.ifi.unicamp.br · Vertically collimating mirror (VCM): Water cooled Three stripes, Si (5-10 keV), Rh (9-20 keV), Pt (14-30 keV). Double Crystal Monochromator (DCM):

UVX/LNLS

1.37 GeV4 straight sections:

1 regular Wiggler for PX – MX2 beamline

1 undulator for soft x-rays - PGM beamline

Superconducting Wiggler – XDS beamline

Page 2: UVX/LNLS - sites.ifi.unicamp.br · Vertically collimating mirror (VCM): Water cooled Three stripes, Si (5-10 keV), Rh (9-20 keV), Pt (14-30 keV). Double Crystal Monochromator (DCM):

Superconducting Wiggler

Manufactured by Budker Institute, Russia

Page 3: UVX/LNLS - sites.ifi.unicamp.br · Vertically collimating mirror (VCM): Water cooled Three stripes, Si (5-10 keV), Rh (9-20 keV), Pt (14-30 keV). Double Crystal Monochromator (DCM):

Only one shot for XAS and XRD, so the beamline must be versatile !

Must be easy to operate, minimum dead time to exchange setups.

The beamline must access a relatively broad energy range (~5-30 keV)

Horizontal focusing:EXAFS community demands DCM with plane crystals, toroidal

focusing mirror, for greater stability and reproducibility.

Diffraction and scattering community demands DCM with sagittal crystals for horizontal focusing, and cylindrical focusing mirror, for control of the horizontal divergence (GID, reflectivity).

Beamline requirements

Page 4: UVX/LNLS - sites.ifi.unicamp.br · Vertically collimating mirror (VCM): Water cooled Three stripes, Si (5-10 keV), Rh (9-20 keV), Pt (14-30 keV). Double Crystal Monochromator (DCM):

Vertically collimating mirror (VCM): Water cooled Three stripes, Si (5-10 keV), Rh (9-20 keV), Pt (14-30 keV).

Double Crystal Monochromator (DCM): First crystals: LN2-refrigerated Si(111) [5-20 keV) and Si(311) [14-30 keV] Second crystals: Plane Si(111), plane Si(311), sagittal Si(111)

Focusing Mirror (VFM) Three stripes: Rh toroidal, Pt toroidal, Rh cylindrical (for use with sagittal

DCM)

Optical Layout

Wiggler

VCM DCM VFM

PtRh

Si

Si(311)

Si(311)

Si(111)

Si(111) sagittal

Si(111) plane

Pt RhRh

Page 5: UVX/LNLS - sites.ifi.unicamp.br · Vertically collimating mirror (VCM): Water cooled Three stripes, Si (5-10 keV), Rh (9-20 keV), Pt (14-30 keV). Double Crystal Monochromator (DCM):
Page 6: UVX/LNLS - sites.ifi.unicamp.br · Vertically collimating mirror (VCM): Water cooled Three stripes, Si (5-10 keV), Rh (9-20 keV), Pt (14-30 keV). Double Crystal Monochromator (DCM):

Optical Hutch

Page 7: UVX/LNLS - sites.ifi.unicamp.br · Vertically collimating mirror (VCM): Water cooled Three stripes, Si (5-10 keV), Rh (9-20 keV), Pt (14-30 keV). Double Crystal Monochromator (DCM):
Page 8: UVX/LNLS - sites.ifi.unicamp.br · Vertically collimating mirror (VCM): Water cooled Three stripes, Si (5-10 keV), Rh (9-20 keV), Pt (14-30 keV). Double Crystal Monochromator (DCM):

Beam shape at focal point (sagittal monochromator)

Observed Simulated (ray-tracing)

E = 11 keV

Page 9: UVX/LNLS - sites.ifi.unicamp.br · Vertically collimating mirror (VCM): Water cooled Three stripes, Si (5-10 keV), Rh (9-20 keV), Pt (14-30 keV). Double Crystal Monochromator (DCM):

Beam shape at focal point (plane DCM, thoroidal M2)

Observed

E = 17 keV

Page 10: UVX/LNLS - sites.ifi.unicamp.br · Vertically collimating mirror (VCM): Water cooled Three stripes, Si (5-10 keV), Rh (9-20 keV), Pt (14-30 keV). Double Crystal Monochromator (DCM):

Energy resolution