TECHNICAL MEMORANDUM NO. 3 FOR REMEDIAL … · facility Sample Point Date Time Hours Swep T Davis...

A p f\ K a- * - ^. t_- (.' o </

PELA——L'

TECHNICAL MEMORANDUM NO. 3

FOR REMEDIAL INVESTIGATION/FEASIBILITY STUDY

CITY DISPOSAL CORPORATION LANDFILL

(DUNN LANDFILL)

{PELA Reference No. 495201)

Appendix B.

Results of Analyses of Soil Samples and

Ground-Water Samples - Summary Package C

CA1889-CA1892, CA1907-CA1908

CA1910, CA2144-CA2148

CA2152-CA2153, CA2266, CA2P82

February, 1990

P. E. LaMc^eaux & Associates, Inc.

Summary Package

for

CITY DISPOSAL CORPORATION LANDFILL

Chain ol Custody Data Required tor ETC Data Management Summary Reports

CA1889-CA1892.CA1907-CA1908, WASTE MANAGEMENT, INC 405CA19.10.CA2I44-CA2I48CA2I52-CA2I53,CA2266,CA2282ETC Sample No. Company

Elapsedfacility Sample Point Date Time Hours

Swep T Davis

President

This Technical fi-spart is an INCITE1" *»rvi-:» !*•*.+, •,•*$ fry LODESTdC'" C'aia Mar,a.3*m*r,t i.r I

ETC

CASE NARRATIVE

This technical report submitted by ETC Corporation contains theanalytical results and required deliverables for Waste Management,Inc. site 405 samples as identified below:

ETC IDCA1889CA1890CA1891CA1892CA1907CA1908CA1910CA2144

CLIEMT IPBLSWIHLADUP03FB03TB1GWF5A

ETC IPCA2145CA2146CA2147CA2148CA2152CA2153CA2266CA2282

CLIENT IP1GWP8A1GWP10A1GWP9A1GWB18RR03FB03TB1GWB18RR1GWP1B

During the preparation and analysis of these samples, the followingwas observed:

fOV7QQ851!Sample CA2144 required dilution which resulted in elevated methoddetection limits.

ACID /BASE /NEUTRAL

The acid surrogate recoveries for sample CA2147 did not meet QCcriteria in the original analysis. Surrogate recoveries wereconfirmed by the results of the repeat analysis. The data for therepeat analysis are included in this report.

The base/neutral surrogate recoveries and internal standard areacounts for sample CA2148 did not meet QC criteria in the originalanalysis. Reinjection of the extract confirmed the initialresults. The laboratory attempted to reextract the sample toconfirm matrix interference on the surrogate compounds. However,the sample was lost in a laboratory accident and analysis of asecond extract could not be performed. The results from theoriginal analysis have been reported.

ETC

Surrogate and internal standard criteria for sample CA2271were not satisfied. Reinjection of the sample extract yieldedsimilar results. Since sample CA2271 was a laboratory generatedsample for QC purposes, it was not reextracted. The data fromCA2271 was utilized in conjunction with the HS/MSD data whichdemonstrated acceptable spike recoveries and RPD. The reinjectiondata and forms are not provided because CA2 271 was not a cl ientsample.

The surrogate recoveries for samples CA2145 and CA2146 did not meetQC criteria. Surrogate recoveries were confirmed by the resul.tsof the repeat analysis. The data for the repeat analysis areincluded in this report.

fQG7QQ3Ql:Primary Analysis: Instrument JA: 6'x4 mm ID 1.5%SP2250/1.95%SP240lConfirmation Analysis: Instrument KB: 6'x2 mm ID 3% SP2100

The-confirmation analysis was performed outside of analysis holdtine. However, quantitation was performed from the primaryanalysis only.

fOG700491!Primary Analysis: Instrument KB: 6'x2 mm ID 3% SP2100Confirmation Analysis: Not Required

There were no surrogate recoveries for samples CA2147, CA2148, theBlank and the Matrix Spike which may have resulted from aninterfering component introduced during the alumina cleanup.

The Matrix Spike and the Matrix Spike Duplicate spike recoveriesdid not meet QC criteria. However, spike recoveries are advisoryonly.

fQG7QQ5Ql!Primary Analysis: Instrument HA: 6'x4 mm ID 1.5%SP2250/l.95%SP240lConfirmation Analysis: Instrument KB: 6'x2 mm ID 3% SP2100

The surrogate recoveries for samples CA1889, CA1890, CA1892, andCA2152 exceeded QC criteria. However,' surrogate criteria isadvisory only.The confirmation analysis was performed outside of analysis holdtime. However, quantitation was performed from the primaryanalysis only.

File I 000022

Release of the data contained in this hardcopy data packagebeen authorized by the following signature.

has

Ken/Hebe1Viae President of Operations

Date

File I 000022

1AUOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO,

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: (soil/water) WATER

Sample ut/vol: 5.0 Cg/mL) ML

Level: (low/mod) LOW

S Moisture: not dec.

Column: (pack/cap) PACK

Cont rac t :

SAS No.: SDG No.i

Lab Sample ID: CA1889U

Lab File ID: >C7409

Date Received: 10/07/39

Date Analyzed: 10/16/89

Dilution Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) UG/L

74-87-3---------Chlorome thane_____________I 1074-83-9---------Bromomethane______________| 1075-01-4---- ———— Yinyl Chloride_____________I 1075-00-3- ——————— Ch I o roe thane______________I 1075-09-2----- —— -Methylene Chloride_________1567-64-1- ——— ----Acetone___________________I 1075-15-0- —— -----Carbon Disulf ide___________1575-35-4-- —— ———1,1-Dichloroethene_________1575-34-3--------- 1,1-Oichlo roe thane_________15540-59-0 ——————— l,2-0ichlor«thene (total )__1567-66-3- ———— ---Chloroform_________________15107-06-2- — ——— -1,2-Dichlo roe thane_________1578-93-3 — -- —— --2-Butanone________________I 1071-55-6————————1,1,1-Trichlo roe thane______1556-23-5 — - — -- — Carbon Tet rachlor ide_______!5109-05-4——————Uinyl Acetate_____________I 1075-27-4---------Bromodich loromethane_______I 579-87-5 —— —— —— 1,2-Dichloropropane________1510061-01-5— — — ci*-l,3-Dichloropropene____1579-01-6——— — — -Tr ichloroethene___________15124-48-1- —— ----Oibromoch lorome thane_______I 579-00-5————————1,1,2-Trichloroethane______1571-43-2————————Benzene__________________.1510061-02-6—————tran»-l, 3-D ich loropropene__1575-25-2- —— — ---Bromof orm_________________I 5108-10-1 ——— ——— 4-Methyl-2-Pentanone_______I 10591-79-6 ——————— 2-Hexanone________________I 10127-19-4———————Tetrach loroethene__________1579-34-5---------1,1,2,2-Tetrachloroethane__15108-88-3 ——————— Toluene___________________15108-90-7--- — ---Chlorobenzene_____________15100-41-4- ———— --Ethyl benzene_______________15100-42-5---- ——— Styrene____________________151330-20-7——————Xylene (total)___________15

IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM I UQA l/e7 Rev

\

vounu

L09-99-9 Tetrahydrofuran

row x

IEVOLATILE ORGAN ICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

Lab Name:ETCNJ

Lab Code: Case No.:

Mat r ix: (so i 1/wateDUATER

Sample ut/vol : 5.0 (g/mL)ML

Level: (low/med) LQU

\ Moisture: not dec._____

Column: (pack/cap)

Number TICa found:

Cont ract:

SAS No.: SDG No.:

Lab Sample ID:

Lab File ID: >C7409



Dilution Factor: 1

CONCENTRATION UNITS:Cug/L or ug/Kg)UG/L

CAS NUMBER

01. •

COMPOUND NAME

CARBON DIOXIDE

.

FORM I UQA-TIC

RT

1.53

EST. CONC

460

i/e;

Q*w

' Rev.

6


SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

Mat r ix : (.so i 1/water ) UIATER

Sample wt /vo l : 5.0 (g/mL) ML

Level: ( low/med) LQUI

H Moisture: not dec.


Cont rac t:

5AS No.:

CAS NO. COMPOUND

SDG No.:

Lab Sample 10: CA139QU

Lab File ID: >C741Q


Date Analyzed: 10/16-''89

Di lut ion Factor: 1

CONCENTRATION UNITS:Cug/L or ug/Kg) UG/L

74-87-3- —— ——— -Ch lorome thane_____74-83-9---------Bromomethane_____75-01-4--- —— ---"Jinyl Chloride____75-00-3 — - —— — -Chloroe thane_____75-09-2——------Methylene Chloride.67-64-1 —— ———— -Acetone___________75-15-0————— •Carbon Disu1fide.75-35-4-——-—-1,1-Dichloroethene______75-34-3- —— - — —1,1-Dichloroe thane______540-59-0—————1,2-Dichlorethene (total),67-66-3- ——— ——— Chloroform______________107-06-2- — - — —1,2-Dichloroe thane___78-93-3—---—--2-Butanone__________71-55-6- —— --——1, 1,1-Trichloroethane,56-23-5---------Carbon Tetrachlor ide_108-05-4———— •Uinyl Ace ta te .75-27-4---------Bromod ichloromethane___78-87-5 ———————— 1,2-Dichloropropane___10Q61-01-5"-----cis-l»3-Dichloropropene.79-01-6 —— — -——Tr ichloroethene_______124-48-1---—---Dibromochloromethane_____79-00-5————————1,1,2-Tr ich loroethane___71-43-2————————Benzene________________10061-02-6—————tr*ns-l,3-Dichloropropene.75-25-2 —— - ———— Brotnof orm______________108-10-1————591-78-6————

•4-Methyl-2-Pentanone.•2-Hexanone_________

108-88-3 —————— -Toluene._______108-90-7----—--Chlorobenzene_100-41-4——— — — Ethyl benzene__10Q-42-5--——---Styrene_______1330-20-7——————Xylene C total)

IIUIIIIUIUI13IUtuI UIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM 1 UQA 1/87

votMtuiu Ajuartu cm UN** NO

t1

.1

Matrix i (M<€/MU MC

(>Mfe/«M)

109-99-9 Tetranydrofuran

u» ru* t»i

u

I

U

8



ERA SAMPLE NO.

Lab NamesETCNJ

Lab Code: Case No.:

Matr ix: (soi1-'water)WATER

Sample wt/vol : 5.0 Cg/mLJML

Level: (low/med) LOW


Column: (pack/cap)

Number TICs found:

Cont rac t:

SAS No.: SDG No.:


Lab File ID: >C74lO

Date Recalled: 10/07/89


Dilution Factor: I


CAS NUMBER

01.a .3.

COMPOUND NAME

CARBON DIOXIDE"TV"! \rf\ \e\t Jfti t ffin rvi *in/^n<TV1! i-viJ-^-flr i| — 5 " , \nr~\rt \

.

FORM I UOA-TIC

RT

1.53

PI. 1*5

EST. CONC

370l"ltO

i/a;

Q

0J ^1-

3-

? Rev.

9


EPA SAMPLE NO

Lab Name: ETC Corp.

Lab Cods: Case No.:

Matrix: (so i 1/uater) WATER

Sample wt/vol: 5.0 (g/mL) ML

Level: (low/mod) LQU

\ Moisture: not dec.


Cont ract

SAS No. ; SDG No.:

Lab Sample ID: CA1S91U

Lab File ID: >D8043/r

Date Received: 10/MJ/89

Date Analyzed: 10/17/89^7-

Dilut ion Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) UG/L Q

74-87-3 —— ——74-83-9 ------75-01-4 — — —75-00-3 ------75-09-2 ------67-64-1 ------75-15-0 —— ——75-35-4 —————75-34-3 —————540-59-0 -----67-66-3 —— ——107-06-2 ————78-93-3 ------71-55-6 ------56-23-5 —————108-05-4 — ——75-27-4 — — —78-87-5 —————10061-01-5 ——79-01-6 —————

79-00-5 —————71-43-2 —————10061-02-6 ——75-25-2 —————108-10-1 -----591-78-6 -----1 77-1 fl_A_-- _

79-34-5- -----108-88-3 -----108-90-7 -----100-41-4 -----100-42-5 — ——1330-20-7 —— -

---Chlorome thane---Bro mo me thane---Uinyl Ch lor ide---Chloroethane---Methv-lene Ch lor ide---Acetone---Carbon Disul f ide---1 r 1-Dich loroe the ne---1 . 1-Dich loroethane—— 1 ,2-Dichlorethene (total ) __— -Ch lorof orm---1 ,2-Dich loroethane---2-Butanone---1 .1.1-Trich loroethane---Carbon Tetrachloride—— Uinol Acetate---Bromodichlarome thane——— 1 r2-Dich lornprooane- — e i»-l r3-DichloroproQene— .-Trichloroethene---Dibrnmoehloromathana. —— I,lr2-Trichio roe thane—— Benzene---trans-l,3-Dichloropropene— -Bromoform ,_ „ _

2 Haxanone---Tatraehloroethene---1,1,2,2-Tet rach loroe thane __---To luene---Chlorobenzene---Ethyl benzene---Styrene——— Xylena Ctntal)

FORM I vOAV

N

i110110110110171101515151515151101515110151515151515151515110110151515151515151

1IUIUIUIU1IUIUIUIUIUIUtuIUIUIUIUIUIUIUIUtuIUIUIUIUIUtuIUIUtuIUIUIUIU1

• 0/87 Rev

109-99-9 Tetraftydrofuran

I/IT

11


TENTATIUELY IDENTIFIED COMPOUNDS

ERA SAMPLE NO.

Lab Name:ETC Corp.

Lab Code: Case No.:

Matr ix: (soi1/water)WATER

Sample wt/vol: 5.0 (g/mL)ML

Level : ( low/med) LOUI


Column: (pack/cap)

Number TICs found:

Cont ract:

SAS No.: SDG No.:


Lab File ID: >D8Q43

Date Received: 10/1-9/89


Dilution Factor: /


CAS NUMBER COMPOUND NAME

yt*™- ^^t^^j

FORM I UOA-TIC

RT EST. CONC

1/9;

Q

' Rev.

12

1AVOLATILE QRGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: (so i1/water) WATER

Sample wt/vol: 5.0 Cg/mL) ML

Leve 1: C low/mod ) LOUI

\ M o i s t u r e : not dec.

Column: tpack/cap) PACK

CAS NO. COMPOUND

Cont rac t :

SAS No.: SDG No.:


Lab F i l e ID: >C7411


Date Analyzed: 10/16'-"89

Oilu tion Fac tor: 1

CONCENTRATION UNITS:Cug/L or ug/Kg) UG/L Q

74-87-3 ———74-83-9 ——— -75-01-4 ——— .75-00-3 ——— -75-09-2 ——— •67-64-1 ——— -75-15-0 —— -•75-35-4 ——— -75-34-3 ——— •540-59-0 —— -67-66-3 ——— -107-06-2 —— -78-93-3 ———71-55-6 ——— -56-23-5 ———108-05-4 —— -75-27-4 ——— -78-87-5 ——— -10Q61-01-5--79-01-6 ——— -124-48-1 —— •79-00-5 ——— -71-43-2 ———10061-02-6—75-25-2 ———108-10-1 —— -591-78-6 ——127-18-4 —— -79-34-5 ———108-88-3 ——108-90-7 ——100-41-4 ——100-42-5 ——1330-20-7--

-----Chloro me thane-----Bromo me thane-----Uinyl Chloride-----Chloroethane-----Mettrjlene Ch lor ide-----Ace tone-----Carbon Disulfide-----1 ,1-Dichloroethene-----1 Pl-Dichloroe thane-- — -1,2-Dichlorethene C total ) __----- Ch loroform-----1 .2-Dich lor oe thane-----2-Butanone-----1 .1 .1-Trichloroathane-----Carbon Tetrachloride_____ginyl Acetate .-----Bromodiehloro me thane-----1 .2-Dichloronronane-----ci»-l,3-Dich loropropene ____-- — --Triehloroethene-----Dibromoeh lorn me thane- — --lTlf2-Trich loroe thane._ — -Benzene-----trans-l,3-Dich loropropene. — --Bromoform-----A-MBthyl-^-Pentanone-----2-Hexanone__-__TBtrachlorQ«thene-- —— 1,1,2 ,2-Tet rach loroe thane __-----To luene_____Chlorobenzene____-Ethylh*nzene-----St>jrene--'---Xy lane (total )

I1101101101101511015151515151511015151 101515151515151515151 10110151515151515151

1IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1UIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

FORM I UOA

vourxu o«Mirtc« Aiutms

Ub rll« XOt S r>

OUMiM rMttt:

109-99-9 Tetrahydrofuran. . . . . . . . . . . . . . . . . . .1,

i!

X VQA I/IT R«v

14

IEVOLATILE ORGANICS ANALYSIS DATA SHEET


ERA SAMPLE NO.

Lab Name:ETCNJ

Lab Code: Case No.:

Mat P ix: (so i 1/wa te r )LJATER

Sample wt/vol: 5.0 (g/mDML

Level: Clow/med) LOU


Column: (pack/cap) "pACK

Number TICs found: .3-

Con t ract:

SAS No.: SDG No.:


Lab File ID: >C7411

Date Received: 10 07/89


Dilution Factor: 1

CONCENTRATION UNITS:(ug/L or ug^Kg)UG/L

CAS NUMBER

01.02.

COMPOUND NAME

CARBON DIOXIDEUNKNOWN

RT

1.571.30

EST. CONC

45024

Q

Z«L'93 LV

FORM I UQA-TIC 1/87 Rev,

15

1AUQLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO,

Lab Name: ETCNJ

Lab Code: Case No.:

Cont rac t

SAS No.

Matrix: (soil/water) LJATER


Level: (low/med) LOU

% Moisture: not dec.


SDG No.:

Lab Sample ID: CA19Q7U

Lab File ID: >C7412



Dilution Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) UG'L

74-87-3 — - — ----Ch lorome thane_____________I 1074-83-9 — - — -- — Bromome thane______________11075-01-4————————Umyl Chloride____________I 1075-00-3 ———————— Chloroe thane_______________I 1075-09-2- ———— ---Methylene Chloride_________1567-64-1 ———————— Acetone____________________I 1075-15-0- —— —— --Carbon Disulf ide___________1575-35-4— —— — "I > 1-Dichloroethene_________1575-34-3————————1,1-0ich loroethane_________15540-59-0—---—-1,2-Dichlorethene (total)__1567-66-3- —————— -Chloroform_________________15107-06-2- — - — —1,2-Dich loroe thane_________1578-93-3- —— ———— 2-Butanone________________1 1071-55-6-- —— ——1,1,1-TP ich loroe thane______1556-23-5 — - ——— —Carbon Tet rach lor ide_______15108-05-4———————vinyl Acetate_____________I 1075-27-4----- — --Bromod ich lorome thane_______I 578-87-5 — - — — — 1,2-Dichloropropane________1510061-01-5—————cis-l,3-Dichloropropene____1579-01-6 — - — -- — Tr ich loroe thene___________15124-48-1- —— ----Dibromoch lorome thane_______I 579-00-5————————1,1,2-Tr ich loroe thane______1571-43-2————————B«nzen«___________________1510061-02-6—————tr«ns-l,3-Dichloropropene__1575-25-2— ———— --Bromof orm_________________1 5108-10-1- —————— 4-Methyl-2-Pentanone_______I 10591-78-6 ——————— 2-Hexenone________________I 10127-18-4——— —— -Tet rach loroe thene__________1579-34-5————————1,1,2,2-Tet rach loroe thane__15108-88-3 ——————— Toluene___________________15108-90-7——- ——— Chlorobenzene_____________15100-41-4------—Ethyl benzene_______________15100-42-5 ——————— Styrene____________________151330-20-7——————Xylene (total )___________15

Q

IIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUI

FORM I UOA 1 6tt/87 Rev

\

uWUT?U OiOMtlCS AJULTtXS QAffc

109-99-9 Tetrahydrocuran

17

IEVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

ERA SAMPLE NO.

Lab Name:ETCNJ

Lab Code: Case No.:

Matr ix: (3011/water)WATER

Sample w t / vo l : 5.0 CgxmDML


S Moisture: not dec._____

Column: Cpack/cap)

Number TICa found:

Cont rac t :

SAS No.: SDG No.:


Lab File ID: >C7412

Date Recei^ed: 10/07/89


Dilution Factor: _I___

CONCENTRATION UNITS:(ug/L or ug/Kg)UG/L

CAS NUMBER

01. "

COMPOUND NAME

CARBON DIOXIDE

RT

1.54

EST. CONC

620

Q

W'

FORM I "JOA-TIC 1/97 Rev.

8


EPA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

MatP ixi (so i1/water) UATER


Level: (low/mad) LOUI

\ M o i s t u r e ; not dec.

Co lumn: (pack/cap) PACK

CAS NO. COMPOUND

Cont rac t:

SWS No.: SDG No.:

Lab Samp Ie ID: CA19090

Lab File ID: >C74l3

Date Raceived: 10/07/89


Di lut ion Fac tor: 1

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

74-97-3 —————74-83-9 —————75-01-4 —————75-00-3 ----- -75-09-2 —————67-64-1 —————75-15-0 ------75-35-4 —————75-34-3 ------540-59-0 ————67-66-3 ------107-06-2 -----78-93-3 ------71-55-6 -----56-23-5 —— ---108-05-4 —— —75-27-4 ------78-87-5 ------10061-01-5 — -79-01-6 —————124-48-1 -----79-00-5 —————71-43-2 —————10061-02-6 ——75-25-2 —————ioa-io-1 ———591-78-6 ——— -127-18-4 -----79-34-5 ------1Q8-B8-3 ————108-90-7 — — -100-41-4 -----100-42-5 ————1330-20-7 ———

---Chlorome thane---Bromome thane---Uinyl Chloride---Chloroethane---Methvlene Ch lor ide---Acetone---Carbon Disulfide---lrl-Dichlaroethene---1 rl-Dichloroethane— -1,2-Dichlorethene (total ) __---Ch lorof arm---1 f2-Dichloroe thane---2-Butanone---1 .1 .1-Trichloroe thane---Carbon Tetrachloride---Uinyl Acetate---Bromodichloro me thane---1.2-Dichloropropane---cis-l,3-Dich loropropene ____---Triehloroethene---Dibromochloro me thane— -1.1 .2-Tr ichloroe thane---Benzene---trans-1 ,3-Dich loropropene- — -Brnmoform——— 4-M«thyl-'2-PantanQne---2-Hexanone---TatraehlnrQBthane---1, 1,2,2- Tetrach lo roe thane __---To luene---Chlorobenzene---Ethylbenzene---Styrene——— Xylena (total )

11101101101101811015151515151511015151101515151515151515151 101 10151515151515151

1IUIUIUIU1IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

FORM I UOA Rev.

1AOMMHCi AIULTSX* MX*

SAI9U NO.

POM t

20

IEVOLATILE ORGAN1CS ANALYSIS DATA SHEET


EPA SAMPLE NO.

Lab Name:ETCNJ

Lab Code: Case No.:

Matrix: (soil/water)WATER

Sample wt/vol: 5.0 tg/mL)ML


S Moisture: not dec._____

Column: (pack/cap)

Number TICs found:

Cont ract :

SAS No.: SDG No.:


Lab File ID: >C7413



Dilution Factor: 1


CAS NUMBER

01.02.

COMPOUND NAME


1

RT

1.581.27

EST. CONC

11028

Q

^0 A90 iA •

FORM I UOA-TIC 1/87

21

1AVOLATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO.

Lab Name: ETCNO

Lab Code: Case No.:

M a t r i x : ( s o i l / w a t e r ) WATER

Sample wt/vo 1 : 5.0 Cg/mL) ML

Leve1: Clow/med) LOW

X M o i s t u r e : not dec.


CAS NO. COMPOUND

Cont rac t:

SAS No.: SDG No.:


Lab Fi la ID: >C74l4


Date Analyzed: 10/16''89



74-87-3- — --- —— Chlorome thane_____________I 1074-83-9 ————— —— Bromome thane______________11075-Ql-4---------Uinyl Chloride_____________I 1075-00-3 ———————— Chloroe thane______________I 1075-09-2---------Methylene Chloride_________1567-64-1-- ———— — Acetone____________________I 1075-15-0 ———————— Carbon Oisulf ide___________1575-35-4- —————— -1,1-Dichloroethene_________1575-34-3————————1,1-Dichloroc thane_________15540-59-0--———-1,2-Dichlorethene Ctotal)__1567-66-3 ———————— Chloroform_________________15107-06-2 —— -----1,2-Dichloroe thane_________1578-93-3-- — - — --2-Butanone_________________I 1071-55-6————————1,1,1-Tr ichloroe thane______1556-23-5--- — - — -Carbon Te t rach lor ide_______15108-05-4———————Uinyl Acetate_____________1 1075-27-4---------Bromodichlorome thane_______I 578-87-5- —— — ——1,2-0 ich lor op ropane________1510061-01-5 ——— — cis-1,3-Dichloropropene____1579-01-6———————Tri chloroe thane____________15124~48-l--------Dibromoch loro me thane_______I 579-00-5————————1,1,2-Tri chloroe than*______1571-43-2 ————— —— Benzene___________________1510061-02-6-*----trans-1,3-Dichloropropene__1575-25-2 — ————— -Bromoform_________________15108-10-1———————4-Methyl-2-Pentanone_______I 10591-78-6 ——————— 2-Hexanone________________I 10127-18-4- —— ——— Tat rach loroe thane__________1579-34-5----- —— -1,1,2,2-Tetrachloroe thane__15109-88-3 ——————— Toluene___________________15108-90-7———— — -Chlorobenzene_____________15100-41-4———————Ethyl benzene______________15100-42-5 ——————— Styrene____________________151330-20-7---- —— Xylene Ctotal)___________.15

__I__

Q

IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1UIUiuIUIUIUIUIUIUIUIUIUIUIU

FORM I UQA 22 1/87 Rev

IAVOLA17U

X VOA

23

IEVOLATILE ORGAN ICS ANALYSIS DATA SHEETTENTATIUELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

Lab NameiETCNJ

Lab Code : Case No . :

Mat r ix: Csoi 1 /water )UATER

Samp le wt/vol : 5.0 (g/mL)ML

Level: C low/mod) LOW

% Moisture: not dec. _____

Column: (pack/cap)

Cont ract:

SAS No.: SDG No.:


Lab File ID: >C7414


Date Analyzed: 10••'16/39

Dilution Factor: I

Number TIC* found: \CONCENTRATION UNITS:(ug/L or ug/Kg)UG/L

CAS NUMBER

01.

COMPOUND NAME

CARBON DIOXIDE

FORM I UQA-TIC

RT

1.57

EST. CONC

110

i/a;

Q

B J w

> Rev.

24

1AVOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Name: ETC Corp.

Lab Code: Case No.:


Sample wt/vol: .0^ (g/mL) ML




Contract

SAS No.:: SDG No.:

Lab Sample ID: CA2144V

Lab File ID: >I8252

Date Received: 10/W/89


Dilution Factor:

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

74-87-3 —————74-83-9 —————75-01-4 —————75-00-3 —————75-09-2 ------67-64-1-- ———75-15-0 —————75-35-4 ------75-34-3——-———* tJ J T **

540-59-0 -----67-66-3 —— ——107-06-2 —— —

71-55-6 —— ——56-23-5 -----108-05-4 ————T^ ^^ A75—27—4™———

10061-01-5 ——

79-00-5 —————14 f 1 f\

10061-02-6 ——

108-10-1 ————

127-18-4™———7Q-34-5—— ————* *f -rf

100-41-4 ————100-42-5 ————1330-20-7 ———

—— Chloromethane—— Bromomethane—— Vinyl Chloride— — Chloroethane—— Methylene Chloride—— Acetone—— Carbon Disulfide—— 1 , 1-Dichloroethene—— 1 , 1-Dichloroethane—— 1,2-Dichlorethene (total) __— -Chloroform—— 1 , 2-Dichloroethane—— 2-Butanone—— 1 , 1 , l-Trichloroethane—— Carbon Tetrachloride—— Vinyl Acetate—— Bromodichl orome thane—— 1 . 2-DichloroDrooane—— cis-l , 3-Dichloropropene ____—— Tr ich 1 oroethene- — D i bromoch 1 orome thane—— 1 , 1 . 2-Trichloroethane——Benzene— — trans-1 , 3-Dichloropropene __—— Bromofonn—— 4-Methyl-2-Pentanone—— 2-Hexanone—— Tetrachloroethene—— 1 ,1,2, 2-Tetrachloroethane __—— Toluene—— Chlorobenzene—— Ethvlbenzene- — Stvrene—— Xylene ( total)

i1000100010001000110017001000500500

100026001000500320100050050050050050050050050050010001000500500500500500500500

ju -uuju!uujriu

1°uruuuuuruuuuriuuuuur!u—— i —— i

VOIATXXJ

109.99-9 Tetrahydroturan

26

"OLATILI OMAWXCS ANALYSIS DATA SHUTTMTATIVEU IDENTIFIED COMPOUNDS

Lab Naaa:Lab Codat Caaa No.:

Contract:SAS No.:

Matrix: (»oil/vatar)

Saapla vt/vol:Laval: (lov/aed)% Moiatura: not decColumn: (pack/cap)

Number TIC* found:

SDG No.:

Lab Saapla ID: _e.Lab FiU IDs _^Data Xacaivad: n.Data Analytad:Dilution Factor:

1C

100.

CONCXHT1UTXOII WITSt(U9/L or

x VO*-KC 1/17

27

1AUOLAJ:LE ORGANics ANALYSIS DATA SHEET EPA SAMPLE NQ

Lab Name: ETC Corp.

Lab Code: Case No.:



Level: (low/mod) LOU

H Moisture: not dec.


Cont rac t :

SAS No.: SDG No.:


Lab File ID: >D8044

Date Received: 10/W/89



CAS NQ. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

74-87-3 ————— ---Ch lorome thane_____________I 1074-83-9———————-Bromome thane______________I 1075-01-4————————Uinyl Chloride_____________11075-00-3 ———————— Chlo roe thane______________11075-09-2 ———————— Methylene Chloride_________1767-64-1- ——— — — Acetone___________________1875-15-0- ———— —— Carbon Disulf ide___________1575-35-4———————1,1-Dichloroetnene_________1575-34-3-- ——— —— 1,1-Di chlo roe thane_________144540-59-0 —— ———— 1,2-Dichlorethene (total)__12267-66-3 ———————— Chloroform________________15107-06-2———————1,2-Dichloroe thane_________1578-93-3 ——— - — — 2-Butanone________________! 1071-55-6————————1,1,1-Tri chlo roe thane______1556-23-5————— —— Carbon Tet rach lor ide_______15108-05-4———————Uinyl Acetate______________I 1075-27-4---------Bromodich lorome thane_______I 578-87-5————————1,2-Dichloropropane________1510061-01-5—————cia-1,3-Dich loropropene____1579-01-6—.—————— Tri chlo roe thane____________121124-48- l--------Dibromoch lorome thane_______I 579-00-5————————1,1,2-Trichloroe thane______1571-43-2 ———————— Benzene___________________I 110061-02-6————trans-1,3-Dichloropropene__1575-25-2 ———————— Bromoform_________________15108-10-1———————4-Methyl-2-Pentanone_______I 10591-78-6———————2-Hexanone________________I 10127-18-4———————Tat rach loroethene__________I 12079-34-5 — - —— —— 1,1,2 ,2-Tet rach lo roe thane__15108-88-3-———————Toluene___________________15108-90-7——————Chlorobenzene_____________15100-41-4——— —— -Ethyl benzene______________15100-42-5 ——————— Styrene___________________151330-20-7———----Xylene (total)____________15

Q

IUIUIUIUIIJIUIUIIIUIUIUIUIUIUIUIUIU1IUIUIJIUIUIUIU1IUIUIUIUIUIU

FORM I UOA 1/87



ERA SAMPLE NO.

Lab Name:ETC Corp.

Lab Code: Case No.:

Mat r ix: (so iI/water>WATER

Sample ut/^ol: 5.0 (g/mL)ML

Le^el: ( loui /med> LQLJ

% Mo la ture: not dec. _____

Column: (pack/cap)

Number TICs found:

Cont rac t :

SAS No.: SDG No.:


Lab F i l e ID: >D8044//

Date Recewed: 10/-HJ/89


Di lut ion Factor: '


CAS NUMBER

01. 75-43-402. 75-71-9

COMPOUND NAME

Methane, dichlorofluoro- CSCMethane, dichlorodifluoro- C

RT

8.395.25

-

EST. CONC

1711

Q

3J

FORM t UOA-TIC 1/87 Rev

30


EPA SAMPLE NO.

Lab Name: ETC Corp. Contract:

Lab code: Case No.: SAS Mo.:

Matrix: (soil/water) HATER

Sample vt/vol: 5.0 (g/mL) ML



SDG Ho


GAS NO COMPOUND

Dilution Factor:

CONCENTRATION OMITS:(ug/L or ug/Kg) UG/L

146V

74-87-3———————Chlorome thane____________74-83-9-—-———Bromomethane____________75-01-4——————Vinyl Chloride__________75-00-3——————Chloroethane___________75-09-2——————Methylene Chloride "*""67-64-1—— --——Acetone ______________75-15-0——————Carbon Disulfide

5-4——————l, 1-Dichloroethene_______'5-34-3——————l, 1-Dichloroethane_______

59-0—————1,2-Dichlorethene (total)__r^66-3————-—-Chloroform_____________

107-06-2—————l, 2-Dichloroethane_______7B-93-3——————2-Butanone_____________71-55-6——————l, l, 1-Trichloroethane_____56-23-5-—-———Carbon Tetrachloride______108-05-4——————Vinyl Acetate___________75-27-4———————Bromodichlorome thane______78-87-5———————1 , 2-Dichloropropane_______10061-01-5———-cis-1,3-Dichloropropene____79-01-6——————Trichloroethene_________124-48-1—————Dibromochlorome thane_____79-00-5——————1,1,2-Trichloroethane_____71-43-2——————Benzene _____________10061-02-6————trans-1.3-Dicnloropropene75-25-2——————Bromoform_____________108-10-1—————4-Methyl-2-Pentanone_____591-78-6—————2-Hexanone_____________127-18-4——————Tetrachloroethene________m79-34-5———————1,1,2,2-Tetrachloroetnane__108-88-3—————Toluene________________108-90-7—————Chlorobenzene_________ •100-41-4—————Ethylbenzene___________100-42-5—————Styrene_______________1330-20-7—————Xylene (total)___________«—__—___^__—,_____.______,——————————i

101010105105555551055105555552551010

55

uuuuuuuuuuuuuuuuuuus5uuuusuDuuu

SMVU HO.

32


Contract:

SAS No.:

EPA SAMPLE NO.

Lab Name:ETC Corp. [ tahargfeory

Lab code: Case No.:

Matrix: (soil/water)WATERSample wt/vol: 5.0 (g/mL)ML


% Moisture: not dec. _

Column: (pack/cap)

Number TICs found: /

DateDilution Factors I

COflCBNTJtATiaN UNITS:(ug/L or ug/Kg)UC/L

CAS NUMBER

01. 60-29-7

COMPOUND NAME

Ethyl ether (SCI)EST. COMC

11

FORM I VOA-TIC 33 1/87 Rev,


EPA SAMPLE NO.

Lab Name: ETC Corp. Contract: ]_______

Lab Code: Case No.: SAS No.: SDG No.:

Matrix: (soil/water) WATER Lab Sample ID: CA2147V

Sample wt/vol: 5.0 (g/mL) ML Lab File ID: >I8250

Level: (low/med) LOW Date Received: lO/itf/89

% Moisture: not dec. Date Analyzed: 10/19/89

Column: (pack/cap) PACK Dilution Factor: i


74-87-3———————Chloromethane____________ 10 u74-83-9———————Broraomethane____________ 10 u75-01-4———————Vinyl Chloride___________ 10 U75-00-3———————Chloroethane_____________ 10 U75-09-2———————Methylene Chloride _____ 767-64-1———————Acetone_________________ 10 U75-15-0———————Carbon Disulfide_________ 10 U75-35-4———————1,1-Dichloroethene________ 5 U75-34-3———————i, l-Dichloroethane________ 5 U540-59-0——————1,2-Dichlorethene (total)__ 5 U67-66-3——————chloroform_____________ 10 u107-06-2 —————— 1,2-Dichloroethane________ 5 U78-93-3———————2-Butanone______________ 10 U71-55-6———————i, 1,1-Trichloroethane_____ 5 U56-23-5———————Carbon Tetrachloride______ 5 U108-05-4——————Vinyl Acetate____________ 10 U75-27-4———————Bromod ichlororae thane______ 5 U78-87-5———————1,2-Dichloropropane_______ 5 U10061-01-5————cis-l,3-Dichloropropene____ 5 U79-01-6———————Trichloroethene__________ 5 u124-48-1-—————Dibromochloromethane______ 5 U79-00-5———————1,1,2-Trichloroethane_____ 5 U71-43-2——————Benzene_______________ 5 u10061-02-6--———trans-1,3-Dichloropropene__ 5 U75-25-2———————Bromoform_______________ 5 U108-10-1——————4-Methyl-2-Pentanone______ 10 U591-78-6——————2-Hexanone_______________ 10 U127-18-4——————Tetrachloroethene________ 5 U79-34-5———————1,1,2,2-Tetrachloroethane__ 5 U108-88-3———————Toluene___________________ 5 U108-90-7——————Chlorobenzene____________ 5 U100-41-4——————Ethylbenzene____________ 5 U100-42-5——————Styrene________________ 5 U1330-20-7—————Xylene (total)__________ 5 U______________________________.———— i ——————————— ( —

vaunt!

109-99-9 Tetrahydrofuran...................1 to

VOLATi r t OPCA^ICS AWAUSIS DATA SHEETWWTIfXIO COMPOUNDS

-'A . r ,

Ub Na»o:Lab Cod«:Matrix: (•oil/w*t«r)

vt/vol:

Caso No.

Contrtet:SAS NO. :

I

% Moisturo: not doe.Coluan: (pack/cap)

_____ SDG No.:

Lab s«»pl« XDi _Ub fil« 10:

D«t« Metivtd:

Dftto An*lyt«4:Dilution rtetor:

CONCBmUTXON UNITS:or u«/K«) "NumJ»«r TZC« found:

row i VC*-TXC 1/17

36


EPA SAMPLE NO

Lab Name: ETC Corp.

Lab Code: Case No.:

M a t r i x : Csoil/water) LJATER


Level: (lou/med) LOW



Cont rac t :

SAS No.: SDG No.:


Lab F i l e ID: >D8045/t

Date Received: 10/J-flV89


Di lu t ion Fac to r ; 1


1 I) 74-87-3——------Chlorome thane_____________11074-83-9————————Bromome thane______________I 1075-01-4————————vinyl Chloride_____________I 1075-00-3- —— - —— -Chloroethane______________I 1075-09-2 ———————— Methylene Chloride_________I 1167-64-1 —————— --Acetone___________________1975-15-0----- ——— Carbon Disulf ide___________1575-35-4—— ———— -1,1-Dichloroethene_________1575-34-3————————1,1-Di Chloroethane_________15540-59-0———————1,2-D ichl ore t none (total )__1567-66-3 —————— --Chloroform_________________15107-06-2 ————— — 1,2-Di Chloroethane_________1578-93-3 — ——-----2-Butanone________________I 1071-55-6---------l,l,l-Trichloroe thane______I 556-23-5-- ——— — -Carbon Tet rach lor ide_______15108-05-4———————Uinyl Acetate_____________11075-27-4---------Bromodich lorome thane_______I 578-87-5 ——— - — — 1,2-Dichloropropane_______.1510061-01-5-- —— -cia-l,3-Dichloropropene____1579-01-6—f—- ——— Tr ichloroethene____________15124-48-l--------Dibromoch lorome thane_______I 579-00-5————————1,1,2-Tri Chloroethane______1571-43-2————————Benzene___________________1510061-02-6-—---trana-1,3-Dichloropropene__1575-25-2————————Bromoform_________________15108-10-1———————4-M«thyl-2-Pentanone_______I 10591-78-6--------2-Hexenona________________110127-18-4———————Tetrachlo roe thene__________1579-34-5————————1,1,2,2-Tet rach loroe thane__15108-88-3———————Toluene___________________15108-9Q-7--------Ch loro benzene_____________15100-41-4———----Ethyl benzene______________15100-42-5 ——————— Styrene___________________151330-20-7——————Xylene (total)____________15

IUIUIUIU1IJIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM I UQA 37 1/87 Rev.

PAJ9U MOOMMTXCi AJULTf It

109-99-9 Tetrahydrofuran

X V04

38

IEUOLATILE ORGAN ICS ANALYSIS DATA SHEET


ERA SAMPLE NO.

Lab Name:ETC Corp.


M a t r i x : (so i I' water ) WATER


Level: C law/med) LOW

\ Moisture: not dec. _____

Column: (pack/cap)

Cont rac t:

SAS No.: SDG No. :


Lab File ID: >DSQ45

Date Rece ived: 10/iff/89


D i l u t i o n Factor: A

Number TICs found; /CONCENTRATION UNITS:lug/L or ug/Kg)UG/L

CAS NUMBER

01.

COMPOUND NAME

UNKNOWN

_

FORM I UOA-TIC

RT

22.33

EST. CONC

4

i/a;

Q

3

' Rev.

59

1AVOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE MC.

Lab Name: ETC Corp.

Lab Code: Case No.:

Mat r ix : t so i 1 / w a t e r ) WATER

Samp 1 e wt/vo i: 5.0 Cg/mLJ ML

Level: Uow/med) LOW

\ M o i s t u r e : not dec.


Lon t rac t

SAS No. : SDG No . :


Lab File ID: >D8046/>

Date Received: LQ/-HJ/89


D i l u t i o n Fac tor : 1

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L 0

**'

74-87-3 ----74-83-9 ——— -75-01-4 ——— -75-00-3 ——— -75-09-2 ——— -67-64-1 ——— -75-15-0 ——— -75-35-4 ——— -75-34-3 ——— -540 59-0---.67-66-3 ——— -107-06-2 —— -78-93-3 ——— -71-55-6 ——— -56-23-5 ——— -108-05-4 —— -75-27-4 ——— -78-87-5 ——— -10Q61-01-5--79-01-6--.---124-48-1 —— -79-00-5 ——— -71-43-2 ——— -10061-02-6—75-25-2 ——— -

591-78-6 —— -127-18-4 —— -79-34-5 ——— .108-88-3- —— -108-90-7 —— -100-41-4 —— -100-42-5 —— -1330-20-7---

-----Ch lorome thane-----Bro mo me thane-----ijinvjl Chlor ide-----Chloroethane-----Methvlene Ch lor ide-----Acetone-----Carbon Disulfide.____! 1-Dichloroethene-----1 .1-Dichloroe thane--- — 1,2-Dichlorethene (total)-----Ch 1 oro f arm.____! r2-Dich laraethane-----2-Butanone-----1 .1 .1-Triehloroethane-----Carbon Tetrachloride.----ijinyl Acetate-----Bromodich lorome thane-----1,.2-DichloroDraDane-----cis-l,3-Dich loropropene ____-----Trichloroethena ,-----Dibromoch lorome thane-----lrl .2-Trichloroethane-_*__BenzenB-----trana-1 ,3-Dich loropropene __— ---Bromofnrm—— --4-Mathol-2-Pentanone-----2-Hax*non«-----Tatrachlopoethene-- —— 1,1,2,2-Tetrachloroethana-----To luene-----Ch lor oh an zane-____Ethy Ihanzena^ ,._ , „-----Styrane.-j.__Xylan« ( total )

1110110110tio1101915151515151511015151101515151515151515151101 10151515151515151

1IUIUIUIUtIJIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

FORM I UOA Rev.

1AOMMRGi AJULTt" Uffc

CM UOU NQ,

x VOA

41

IEVOLATILE ORGANICS ANALYSIS DATA SHEET


ERA SAMPLE NO.

Lab Name:ETC Corp. Contract:

Lab Code: Case No,: SAS No.:

hatrix: Iso i1/water)WATER

Sample wt/vol: 5.0 Cg/mL)ML

Le^el: f l o w / m e d ) LOW

S M o i s t u r e : not dec._____

Column: Ipack/cap)

Number TICa found: _'_

SDG No.:


Lab F i l e ID:



D i l u t i o n Factor: /

>D8046ft

CONCENTRATION UNITS:

CAS NUMBER

01.

11

COMPOUND NAME

UNKNOWN

FORM I UQA-TIC

RT

22.32

EST. CONC

4

i/a;

42

IQ 1

J 1iittiiiiii

iiitiii

i*

iiiiiiii

7 Rev .


ERA SAMPLE NO

Lab Name: ETC Corp.

Lab Code: Case No.:


Samp 1e wt/vo1: .3 (g/mL) ML

Leve1: (low/mod) LOW



Cont ract

SAS No. SDG No . :


Lab File ID: >C7534

Date Received:


Dilution Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:<ug/L or ug/Kg) UG/L

I I74-87-3 — ---- —— Chl orome thane______________1200 IU74-83-9-—• ——— --Bromomethane______________I 200 IU75-01-4————————Uinyl Chloride_____________1200 IU75-00-3 ———————— Ch loroe thane______________1200 IU75-09-2—-------Methylene Chloride_________163" ]<•67-64-1 ———————— Acetone___________________15254 I75-15-0 ———————— Carbon Disulfide___________1100 IU75-35-4—-- —— —1 .1-Dichloroethena ______I 100 IU75-34-3————————1,1-Dich loroe thane_________I 100 IU540-59-0———————1,2-Dichlorethene (total)__1150 I67-66-3 ———————— Chloroform________________I 100 IU107-06-2———————1,2-Dich loroe thane_________I 100 IU78-93-3 — —— - —— 2-Butanone________________ I 2*-4WW 2-£/T7 I71-55-6 ——— — ——1,1,1-Trichloroethane______I 100 /*» .... IU56-23-5 ———————— Carbon Tet rach lor ide_______1100 W////?/VJ m108-05-4———————Uinyl Acetate_____________1200 ' IU75-27-4—- ———— -Bromodi chl orome thane_______I 100 IU78-87-5————————1,2-Dichloropropane________I 100 tU10061-01-5 ————— cis-1,3-D ich loropropene____ I 100 iU79-01-6 ———————— Trich loroe thene____________I 100 IU124-48-1 ——————— Dibromoch 1 orome thane_______I 100 IU79-00-5 ———————— 1,1,2-Trichloroethane______I 100 IU71-43-2————————Benzene___________________I 100 IU10061-02-6—————trana-1,3-Dichloropropene__I 100 tU75-25-2————————Bromoform_________________I 100 IU108-10-1 —————— -4-Methyl-2-Pentanone_______1200 iU591-78-6 ——————— 2-Hexanone________________1200 tU127-18-4———————Tetrachloroethene__________I 100 IU79-34-5————————1,1,2,2-Tet rach loroe thane__I 100 IU108-88-3 ——————— Toluene___________________15191 I108-90-7———————Chlorobenzene______________1100 IU100-41-4———————Ethylbenzene______________11100 I100-42-5———————Styrene___________________I 100 IU1330-20-7——————Xylene (total)____________1

_____________I

FORM I UOA 1/87 Rev.

CMMRCi MHOXS1*

109-99-9 Tetrahydrof uran.................. .JM^MMM^S»

1/17

44

Ub Hw«:Ub CodatMatrix: (aoil/vataf)

wt/vol:(Xow/aad)

I Moisturai not dacColumn: (pack/cap)

Mumtoar TIC« found:

VOLATILE OPGAXICS X H A L Y S I 5 DAT* .TINTATIVtU IDCXTirilO COMPOUXD4

__ Contract:SAJ Mo.:C*»« MO

Data Analytod:Dilution Factor:

1/17

45

1AUQLATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO,

Lab Name: ETC Corp.

Lab Code: Case No.:

Mat r ix: (so i I/water) UIATER


Level: C low/mod) LQUI



Cont ract:

SAS No.: SDG No.:


Lab File ID: >C7524

Date Received:


Di lution Factor: 1


74-87-3 — — —74-83-9 - —— —75-01-4 ------75-00-3 ——— —75-09-2 — — --67-64-1 ------75-15-0 -----75-35-4 ------75-34-3 ------540-59-0 -----67-66-3 — — —107-06-2 —— —78-93-3 ------71-55-6 -----56-23-5 — —— -108-05-4 -----75-27-4 ——— —78-87-5 ------10061-01-5---79-01-6 —————124-49-1 ————79-00-5 —————71-43-2 ------10061-02-6 ——75-25-2 —————108-10-1 ————591-78-6 ————127-18-4 ————79-34-5 ------108-88-3 —— —108-90-7 ————100-41-4 ————100-42-5 ————1330-20-7 — —

---Ch lorome thane---Bro mome thane—— "Jin-jl Chloride---Ch loroe thane---Methvlene Ch lor ide---Acetone---Carbon Disu 1 f ide---1 ,1-Dichloroethene---1 . 1-Dich loroe thane— -1,2-Dichlorethene Ctotal)---Chloroform,---1 r2-0ieh loroe thane ,.---2-Butanone---1 .1 .1-Trichloroathan*---Carbon Tat rach lor i da---Oinyl Acetate---Bromod ich lorome thane---1 r2-Dieh lorapropane---cia-l,3-0ich loropropene---Trichloroethene,---Dibromoch lorome thane---1 . 1 r2-Tr iehloroethane— -Banzen*---t rans-1 , 3-D ich loropropene __---Bromof orm_ — 4-MBthyI-2-Pent»none---2-Hexanone---Tet rachloroethena . , ,---1,1, 2, 2- Tet rach loroe thane __---To luene---Ch lorohenzene---Ethy Ibenzane MI

---Styrene _---Xylene (total )

11101101101331811015151461715151101171511015151518515151215151101101471515151515151

1IUIUIU1 /i* >UIUIUIU11IUIUIU1IUIUIUIUIU1IUIUIJIUIUIUIU1IUIUIUIUIU AIU t-\ 6

1 /Q-7 O*.

VOURU OMMRCi

109-99-9 Tetrahydrofuran,

X ¥0*

47

VOLATILE ORCA/UC3 ANALYSIS DAT*TEMTATIVIU XOCMTXmO COHJCUXD*

N4MI

CAM HO.!

Matrix:Saaplo vt/vol:UvoX: (Xov/B«d)% Moisturo: not doc.Column: (pack/cap)

Huabor TICo found:

Contract: _._____. I ——SAS Mo.: _____ WO »o.:

Ub StapXo ID:ub mo xotDoto Itoeoivod:

Doto AnaXyxod:Dilution factort

COMCWTHATIOH UNITS:<uf/l or uf/Xf),

1/17

48

IBSEMIUOLATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: ' Case No.:

Matrix: Csoil/water) WATER

Sample ut/woli 910.0 Cg/mL) ML

Level: (low/med) LOLJ

S M o i s t u r e : n o t d e c . dec.

Extract ion: (SepF/Cont/Sonc) CONT

GPC Cleanup: (Y/N) N PH:

Cant ract:

SAS No.: SDG No.:

Lab Sample ID: CA1889C

Lab File ID: >G9052

Date Received:

Date Extracted: 10/12/89


Dilution Factor: 1


108-95-2———————Phenol____________________111-44-4- —————— bis(2-Chloroethyl )ether____95-57-8————————2-Chlorophenol____________541-73-1------—1,3-Dichlorobenzene________106-46-7———————1,4-0ich lorobenzene________100-51-6———————Benzyl alcohol____________95-50-1———— ——— 1,2-Dichlorobenzene________95-48-7————————2-Methylphenol____________108-60-1———————biaC2-Chloroisopropyl )ether_106-44-5 ——————— 4-Methylphenol____________621-64-7--------N-Nitroso-d i-n-propy lamme_67-72-l---------Hexachloroethane___________98-95-3 —————— — Nitrobenzene______________79-59-1---------Isophorone________________88-75-5-———————2-Nitrophenol_____________105-67-9 ——————— 2 ,4-Di methyl phenol_________65-85-0----- — --Benzoic ac id______________111-91-1 ——————— b is C2-Chlo roe thoxy)me thane_120-83-2———————2,4-Dichlorophenol_________120-82-1———————1 ,2,4-Tr ich lorobenzene_____91-20-3————————Naphthalene________________106-47-8—-————4-Chloroani 1 ine___________87-68-3-—-———-H«xachlorobutadiene________59-50-7————-——4-Chloro-3-methy Ipheno 1____91-57-6————————2-Methylnaphtha lane________77-47-4-- — - — --Hexachlorocyc1 open tadlene__88-06-2————————2,4,6-Trichlorophenol______95-95-4————————2,4,5-Trichlorophenol______91_5g_7—————— — 2-Ch loronaphthe lene________88-74-4———— ——— 2-Nitroani 1 ine____________131-11-3 ——————— Dimethylphthalate__________208-96-B ——— ——— Acenaph thy lene____________606-20-2—————2,6-Dinitrotoluene_________

111111111111111111111111111111115511111111111111111111551155111111

IUIIIIUIUtuIUtuIUIU1UIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI

FORM I SO -149

1/87 Rev

1CSEMIUOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Ma t P i x i (soil /wa tar) WATER



X hoi»ture: not dec. dec.

Extraction: (SepF/Cont/Sonc) CONT


Contract:

SAS No.: SDG No.:


Lab Fila ID: >G9052

Date Received: t

Data Extracted: 10/12/89


Dilution Factor: 1


99-09-2 ———————— 3-Nitroani 1 ine_____________15583-32-9————————Acenaphthene______________I 1151-28-5————————2,4-Dinitrophenol__________155100-02-7———————4-Nitrophenol______________155132-64-9———————Dibenzofuran________:______111121-14-2 ——————— 2.4-Dinitrotoiuena _____11184-66-2 ———————— Diethylphthalate___________1117005-72-3 —————— 4-Chlorophanyl-phenylethar_I 1186-73-7————————Fluorena__________________I 11100-01-6 ————— — 4-Nitroani 1 ine_____________155534-52-1 —— ———— 4,6-Dinitro-2-methylphenol_15586-30-6 ———————— N-Nitrosodi phony lamina (1)_I 11101-55-3 ——————— 4-Bromophenyl-phenylether__I 11118-74-1 ——————— Hexachlorobenzene__________I 1187-86-5 ———————— Pentachlorophenol__________15585-01-8————————Phenanthrene______________111120-12-7———————Anthracene________________11184-74-2————————Di-n-butylphthalate________111206-44-0——————F luoranthene_____________111129-00-0———————Pyrene____________________11185-68-7————————Butyl banzylph the late_______11191-94-1———-----3,3'-Oichlorobenzidine_____12256-55-3—-CC TI—Sanzo (a) anthracene________111218-01-9—-^——Chry»ana__________________I 11117-81-7---^^-—bi»(2-Ethylhaxy Dphtha late_111117-84-0——-———Di-n-octylph thai ate_______111205-99-2 ——————— Benzo(b)fluoranthene_______111207-08-9———————Benzo(k)fluoranthene_______11150-32-8————————Benzo(a>pyrene_____________111193-39-5———————IndenoU,2,3-cd)pyrene_____11153-70-3————————Dibenz(a,h)anthracene______111191-24-2---- — --Benzo Cg,h , i )pery lene_______111

I_________________________________________I__(1) - Cannot be separated from Diphenylamina

FORM I SU -2

IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUiuIUIUIUIUIU

.1

1/07 Rev.

50

IFSEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET


EPA SAMPLE NO.

Lab Name:ETCNJ . Contract:

Lab Code: Case No.: SAS No.:

Ma t r i x: (soil/wa tar)UATER

Sample wt/vol: 910,0 <g/mL)ML

Level: Clow/med) LOW

H Moisture: not dec. _. ._ dec.

Extract ion: CSepF/Cont/Sonc) CONT

GPC Cleanup: (Y/N) N pH:___

i

Number TICa found:

SDG No.:


Lab File ID:- >G9052

Date Received:

Date Extracted:10/12/89


Dilution Factor: ___f


CAS NUMBER

01. 141-78-602.03.04. 10574-37-5

-

"

COMPOUND NAME

Acetic acid, ethyl ester •ACETONE DIMERUNKNOWN2-Pentene, 2 , 3-d i methyl-

.

RT

5.166.427.865.24

EST. CONC

690772211

Q

BJ i/1sb ^0

;\<"V"

FORM I SU-TIC51

1/87 Rev.

IBSEMI VOLATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO,

Lab Name: ETCNJ

Lab Code:

Cont ract:

Case No.:

Matrix: Csoi1/water) WATER



HMoisture:notdec.. dec.


GPC Cleanup: (Y/N) N pH:

CAS NO. COMPOUND

SAS No.: SOG No.:

Lab Sample ID: CA1S90C

Lab File ID: >G9Q53

Date Received:



Dilution Factor: 1

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L Q

108-95-2———————Phenol____________________1.11-44-4———————bi»(2-Chloroethyl )ether____95-57-8————————2-Chlorophenol_____________541-73-1———————l,3-Dichlorobenzene_______106-46-7———————1,4-Dichlorobenzene________100-51-6———————Benzyl alcohol_____________95-50-1————————1,2-Dichlorobenzene________95-48-7————————2-Me thy! phenol_____________108-60-1 ——————— bis(2-Chloroisopropy1 )ether_106-44-5 ——————— 4-tlethyl phenol_____________621-64-7--------N-Nit roao-di-n-propy lamine_67-72-1----—---Hexachloroethane___________98-95-3 ———————— Nitrobenzene______________78-59-1————————Isophorone________________88-75-5 ———— ——— 2-Nitrophenol______________105-67-9 —— ————2 ,4-Dimethylphenol_________65-85-0———————Benzoic acid_____________111-91-1 ——————— b is(2-Ch loroethoxy )methane_120-83-2-——————2,4-Dichlorophenol_________120-82-1-"--;——1,2,4-Tr ich lorobenzene_____91-2 0- 3-«*^--—N«ph t ha 1 ene_______________1Q6-47-8-"'-'--—4-Chloro«ni 1 ine____________S7-68-3-^*'f^--—Hejxechlorobutad iene________59-50-7-—~^—--4-Chloro-3-me thy 1 phenol____91-57-6———————2-Methylnaphtha Iene_______77-47-4————————Hexach lorocycl open tad iene__88-06-2————————2,4,6-Trichlorophenol______99-99-4————————2,4,5-Tr ich loropheno 1______91-58-7———————2-Chloronaphthalene________88-74-4————————2-Nitroani 1 ine_____________131-11-3———————Dimethylphthalate__________208-96-8 ——————— Acenaph thy lane_____________606-20-2 ——————— 2,6-Dinitrotoluene_________

111111111111111111111111111111115411111111111111111111541154111111

IIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUI

FORM I S"J -1 52

' 1CSEMIUOLATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Cont ract:

SAS No.:

Matrix: (soil/water) UATER


Level: ( lou/med) LOLJ

SDG No . :

Lab Sample 10: CA1890C

Lab Fi le ID: >G9Q53

Date Received:

S M o i s t u r e : n o t d e c dec

Extraction: (SepF/Cont/Sonc ) CONT




Di lut ion Factor : 1


99-09-2 ——————— 3-Nitroanil ina___________83-32-9————————Acanaph thane______________5.1-28-5————————2,4-Dinitrophenol__________100-02-7———————4-Nitrophenol______________132-64-9———————Dibenzofgren________;______121-14-2———————2,4-Dinitrotoluene_________84-66-2————————Dietnylphthalete___________7005-72-3——————4-Chlorophenyl-phenylether_86-73-7————————Fluorena__________________100-01-6- ————— 4-Nitroanil ina___________534-52-1 ——————— 4,6-Dinit ro-2-methy Ipheno I_86-30-6------ — -N-Ni trosod iphanylamina C1)_101-55-3-—--—-4-8romopheny1-phenylether__118-74-1———————Hexachlorobanzene__________87-96-5 ———————— Pentachlorophenol__________85-01-8————————Phenanthrane______________120-12-7———————Anthracene________________84-74-2————————Oi-n-butylphthalat»________206-44-0———————Fluoran thane______________129-00-0——————Pyr«n«__________________85-68-7-——*~———Butylbanzylphthe late_______91-94-1—«-^rr——3,3'-Dichlorobenzidine_____56-55-3'i '"ft""'.——B«nzo(a)anthracane_________218-01-9V«foLii...——Chryaene__________________117-81-7*—^-———bi»(2-Ethylnexyl )phthe late_117-84-0———————Oi-n-octylphthe late________205-99-2 ——————— BanzoCb )f luoranthena_______207-08-9—-————Benzo(k)fluoranthane_______50-32-8———————Benzo(a)pyrene_____________193-39-5———————IndenoCl,2,3-cd)pyrene_____53-70-3--—-----Oibenz(a,h)anthracene______191-24-2 ——————— Benzo(g,h, i )perylene_______

5411545411111111115454111111541111111111112211111111111111111111

(1) - Cannot be separated from Oiphenylamine

FORM I SU -2

Q

IIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUI

1/87 Rev.

53

IFSEMIUOLATTLE ORGAN ICS ANALYSIS DATA SHEET


ERA SAMPLE NO.


Lab Code: Casa No.: SAS No.:

Matrix: (aoi1/water)WATER

Sample ut/vol: 920.0 (g/mL)ML

Level: Clow/mad) LOW

H Moisture: not dec ._____ dec . _____

Extraction: <SepF/Cont/Sonc) CONT


SDG No.:

Lab Sample ID: CA189QC

Lab Fila ID: >G9053

Data Received: /0/



Dilution Factor: /

Number TICs found:CONCENTRATION UNITS:Cug/L or ug/Kg)UG/L

CAS NUMBER

01. 141-78-602.03.

COMPOUND NAME

Acetic acid, ethyl ester •ACETONE DIMERUNKNOUN

RT

5.116.568.04

EST. CONC

4008914

Q

ja6 »A^J J

FORM I SiJ-TIC /87 Rev


EPA SAP1PLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Ma t r i x: (soil/u« t e r) WATER


Level: Clow/mod) LOW

HMoisture: not dec. dec.

Extraction: (SepF/Cont/Sonc) CQNT

GPC Cleanup: <Y/N> N pH:

Contract:

SAS No.: SDG No.:


Lab File ID: >G9Q61

Date Received: /





108-95-2 ——————— Phenol____________________110111-44-4———————bis(2-Chloroethyl )ether____11095-57-8————————2-Chlorophenol_____________110541-73-1———————1,3-Dichlorobenzene^______I 10106-46-7———————1,4-Dichlorobenzene^______110100-51-6 ——————— Benzyl alcohol_____________11095-50-1 ———————— 1,2-Dichlorobenzene________I 1095-48-7————————2-Methylphenol_____________I 10108-60-1———————bis(2-Chloroisopropyl )ether_l10106-44-5 ——————— 4-Methyl phenol_____________I 10621-64-7------ — N-Nitroso-d i-n-propy lamine_I 1067-72-1 —————— — Hexachloroe thane___________1 1098-95-3————————Nitrobenzene______________I 1078-59-1———————— Isophorone________________I 1088-75-5————————2-Nitrophenol______________I 10105-67-9 ——————— 2,4-Dimethylphenol_________11065-85-0— —————— Benzoic ecid______________152111-91-1 ——————— bi»C2-Chloroethoxy)methane_HO120-83-2———————2,4-Dichlorophenol_________HO120-82-1———————1,2,4-Trichlorobenzene_____I 1091-20-3————————Naphthalene_______________I 10106-47-8—•«-——4-Chloroani 1 ine______;_____I 1087-68-3—«—-——Hexachlorobutad iene________11059-50-7————————4-Chloro-3-methylphanol____I 1091-57-6————————2-Methylneph thai one________I 1077-47-4- —— - — --Hexachlorocyc1 open tadiene__11088-06-2————————2,4,6-Tr ich loropheno 1______t 1095-95-4————————2,4,5-Trichlorophenol______15291-58-7————————2-ChloronaphthaIene________11088-74-4————————2-Nitroani 1 ine_____________152131-11-3 ——————— Dimethylphthalate_______. I 10208-96-8- —— ——— Acenaph thy Iene_____________110606-20-2 ——————— 2,6-Dinitrotoluene_________t 10_________ ____ _______ I__

IUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI

FORM I SlJ -1 5587 Rev

1CSEMI VOLATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO,

Lab Name: ETCNJ

Lab Code: Case No.:

Cont ract

SAS No.

Matrix: (soi1/water) WATER




Extraction: CSepF/Cont/Sonc) CONT

GPC Cleanup: CY/N) N pH:

SDG No.:


Lab Fil e ID: >G9061

Date Received:



Dilut ion Factor: 1


99-09-2 ———————— 3-Nitroanil ine_____________83-32-9 ———————— Acenaphthene______________51-28-5 ———————— 2,4-Oinitrophenol__________100-02-7———————4-Nitrophenol______________132-64-9 ——————— Oibenzofuran________;______121-14-2 ——————— 2,4-Dinitrotoluene_________84-66-2 ——— ———— Oiethylphthalate___________7005-72-3——————4-Chlorophenyl-phenylether_86-73-7————————Fluorene__________________100-01-6———————4-Nitroani 1 ine_____________534-52-1 ——————— 4,6-Dini t ro-2-methy Ipheno 1_66-30-6---------N-Ni t rosodiphenylamine (1)_101-55-3--------4-Bromopheny1-phenylether__118-74-l--------Hexachlorobenzene_87-86-5 ———————— Pentach loropheno 1__________85-01-8 ———————— Phenanthrene______________120-12-7—————-Anthracene_______________94-74-2 ——— ——— Di-n-butylphthalate_______206-44-0———————Fluor an thene______________129-00-0———————Pyrene____________________85-68-7———-————Butylbanzylphthalate_______91-94-1——'--—~3,3'-Dichlorobenzidine_____56-55-3————————B«nzo(«)anthracene_________218-01-9--————Chry»en»_______________117-81-7———————bi»(2-Ethylhexyl )phthalate_117-84-0———————Di-n-octylph thai ate________205-99-2———————Benzo(b)fluo ran thene_______207-08-9——— ——— Benzo(k)f luoranthene_______50-32-8 ——— - —— -BenzoCa)pyrene_____________193-39-5—————— Indenod ,2 ,3-cd )pyrene_____53-70-3 —————— — Dibenz(a,h>anthracene______191-24-2———————Benzo(g,h, i >perylene_______

152110152152110110110110110152152101010521010101010102110101010101010101010

Q

IIU1UIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUI

(1) - Cannot be separated from Dipheny lamine

FORM I SU -2 1/87 Rev,

IFSEMI VOLATILE ORGAN ICS ANALYSIS DATA SHEET


EPA SAMPLE NO.

Lab Naroe:ETCNJ

Lab Code: Case No.:

Matrix: (soi 1/water )UIATER

Sample wt/vol: 960.0 (g/mDML


% Moisture: not dec. dec..___


GPC Cleanup: CY/N) N oH:

.1Number TICs found:

Cont ract:

SAS No.: SDG No.:


Lab File ID: >G9061

Date Received:


Date Analyzed:

Di lut ion Factor:


CAS NUMBER

01. 141-78-602.03.04.

-JJ

COMPOUND NAME

Acetic acid, ethyl ester •ACETONE DIMERUNKNOWNUNKNOWN

•--

RT

5.046.437.838.88

EST. CONC

330911111

Q

90 VBJ >/-

FORM I SU-T1C 57 1/87 Rev.


ERA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: Caoi 1/water) CJATER


Level: <low/mod) LOU

% Moisture: not dec. dec.


GPC Cleanup: (Y/N) N pHi

Contract:

SAS No.: SDG No.:


Lab File ID: >G9054

Date Received:





108-95-2 ——————— Phenol____________________111-44-4———————bis(2-Chloroethyl )ether____95-57-8————————2-Chlorophenol_____________541-73-1———————l,3-Dichlorobenzene_;______106-46-7—---—-1,4-Dichlorobenzene________100-51-6———————Benzyl alcohol_____________95-50-1————————1,2-0ich lorobenzene________95-48-7————————2-Methylphenol_____________108-60-1——————bis(2-Chloroisopropyl>ether_106-44-5———————4-Mathylphenol_____________621-64-7--------N-N1troso-di-n-propy lamine_67-72-1-------—Hexachloroethane___________98-95-3 ———————— Nitrobenzene______________78-59-1--- — - — - Isophorone________________88-75-5————————2-Nitrophenol______________105-67-9———————2 ,4-Di methyl phenol_________65-85-0————————Benzoic acid_______________111-91-1———————bis(2-Ch loroe thoxyJme thane_120-83-2———————2,4-Dichlorophenol_________120-82-1 ——————— 1,2,4-Tr ich lorobenzene_____91-20-3————————Naphthalene_______________106-47-8-————4-Chloroani 1 ine__________87-68-3————————H»xachlorobutad iene________59-50-7——-————4- Chloro-3-methyl phenol____91-57-6————————2-Methylnaphtha Iene________77-47-4-- — -----Hexachloroeyclopentad iene__88-06-2————————2,4,6-Tr ich loropheno 1______95-95-4————————2 ,4,5-Tr ich loropheno 1______91-58-7————————2-Chloronaphthalene________88-74-4————————2-Nitroani 1 ine_____________131-11-3 ——————— Dimethylphthalate__________208-96-8----———AcenaphthyIene_____________606-20-2 ——— ——— 2,6-Dinitrotoluene_________

111111111111111111111111111111115411111111111111111111541154111111

IUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI

58FORM I SU -1 1/87 Rev


ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:



Level: Clow/mod) LOU

H Mo i sture: not dec. dec.

Extraction: (SepF/Cont/Sane) CQNT


Contract:

SAS No.: SOG No.:


Lab Fila ID: >G9Q54

Date Received:

Date Extracted: 10x12/89


Dilut ion Factor: 1


99-09-2 ———————— 3-Nitroani 1 ine_____________83-32-9 ———————— Acenaphthene______________„51-28-5————————2,4-Oinitrophenol__________100-02-7———————4-Nitrophenol______________132-64-9 ——————— Dibenzofuran________;______121-14-2 ——————— 2,4-Dinitrotoluene_________84-66-2 —————— — Diethylphthalate___________7005-72-3——————4-Chlorophenyl-phenylether_86-73-7---------Fluorene ________ ______100-01-6 —— ———— 4-Nitroani 1 me_____________534-52-1 ——————— 4,6-Dinitro-2-methylphenol_86-30-6---------N-Nitrosodiphenylamine (1)_101-55-3--------4-Bromopheny1-phenylether__118-74-1------—Hexachlorobenzene__________87-86-5 —— ————— Pentachlorophenol__________85-01-8 ———————— Phanan throne______________120-12-7——————-Anthracene________________84-74-2-———————Di-n-butylph thai ate________206-44-0 ——————— Fluoranthene______________129-00-0———————Pyrane____________________85-68-7————————Butylbenzylph thai ate_______91-94-1 ———————— 3,3 '-Oichlorobenzidine_____56-55-3——•—————Benzo (a) anthracene_________218-01-9———————Chrysene__________________117-81-7———————bi»(2-Ethylhexyl Jphthalate_117-84-0———————Di-n-octylphthalate________205-99-2 ——————— Benzo Cb ) f luoranthena_______207-08-9 ——————— BonzoCk ) f luoranthene_______50-32-8---------Benzo(aIpyrene_____________193-39-5——————— IndenoCl ,2 ,3-cd >pyrene_____53-70-3 — ——————Dibenz(a,h) anthracene______191-24-2--------Benzo(g,h,i)peryl

5411545411111111115454111111541111111111112211111111111111111111

IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIU1UIUIUIUIUIUIUIUIUIUIUI

(1) - Cannot be separated from Diphenylamine

FORM I SU -2 Rev

IFSEMIUOLATJLE ORGAN ICS ANALYSIS DATA SHEET


ERA SAMPLE NO.

Lab NameiETCNJ . Contract:


Matrix: tsoi1/water)WATER


Level: C low/mod) LOLJ

S Moisture: not dec . ____ dec _



Number TICs found: 6

SDG No . :


Lab Fi le ID: >G9054

Date Received: /



Dilution Factor: '

CONCENTRATION UNITS:(ug/L 'or ug/Kg)UG/L

CAS NUMBER

01. 141-78-602.03.04. 108-88-305.

COMPOUND NAME

Acetic acid, ethyl ester •ACETONE DIMERUNKNOWNBenzene, methyl-UNKNOWN

RT

5.126.509.004.357.95

EST. CONC

46085251211

Q

Jp/jlKT

FORM I SU-TIC 60 1/87 Rev.


ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: Csoi 1 /water) WATER

Sample ut/vol: 940.0 (g/mL) ML

Level : ( low/med) LOU

Cont rac t:

SAS No.: SDG No.:


Lab File ID: >G9Q78

Date Recei ved:

HM o i s t u r e : n o t d e c . dec.

Extraction: (SepF/Cont/Sonc ) CONT




Dilution Factor: 1


I108-95-2 ——————— Phenol____________________111111-44-4———————bis(2-Chloroethyl )ether____11195-57-8————————2-Chlorophenol____________111541-73-1———————1,3-Dichlorobenzene________111106V46-7———————1,4-Dichlorobenzene________111100-51-6 ——————— Benzyl alcohol____________11195-50-1————————1,2-Dichlorobenzene________11195-48-7————————2-Methyl phenol_________ 111108-60-1 ——————— bis(2-Chloroisopropy1 )ether_J 11106-44-5———————4-Methylphenol____________I 11621-64-7--------N-N11 roso-di-n-propy lamine_I 1167-72-1 ———— ——— Hexachloroe thane___________ I 1198-95-3 ———————— Nitrobenzene______________I 1178-59-1———————— Isophorone________________I 1188-75-5————————2-Nitrophenol_____________I 11105-67-9- —————— 2,4-Di methyl phenol_________11165-85-0 ——— ————Benzole acid______________(53111-91-1- —————— b is (2-Chloroe thoxy) me thane_I 11120-83-2———————2,4-Dichlorophenol_________I 11120-82-1———————1,2,4-Trichlorobenzene_____11191-20-3————————Naphthalene_______________I 11106-47-8———————4-Chloroani 1 ine___________I 1187-68-3————————Hexachlorobutadiene________I 1159-50-7————————4-Chloro-3-methyl phenol____I 1191-57-6————————2-Me thy! naphthalene________I 1177-47-4---- — ---Hexachlorocyc1 open tad iene__I 1188-Q6-2--——————2,4,6-Trichlorophenol______I 1195-95-4————----2,4,5-Trichlorophenol______15391-58-7————————2-Chloronaphthalene________I 1188-74-4————————2-Nitro«ni 1 ine____________153131-11-3 ——————— Dimethylphthalate__________I 11208-96-8 ——————— Acenaph thy Iene____________I 11606-20-2 —— ————2,6-Dinitrotoluene_________HI

_____________• __ __ I

Q

IIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIU

FORM I SO -1 1/87 Rev,

(oO.I

ETC

END OF PAGE INSERTION,

1CSEMIUOLATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAHPLE NO

Lab Name: ETCNJ . '

Lab Code: Case No. '•

Matrix: CsoiI/water) WATER

Sample wtxvol: 940.0 Cg/mL) ML

Level: (low/mod) LOU)

HMo is tu re : not dec. dec.

Extrac t ion: (SepF/Cont/Sonc> CONT


Cont ract:

SAS No.: SDG No.:


Lab File ID: >G9078

Date Received: /j/tf?//?

Date Extracted: 10/li/89

Date Analyzed: 11x16/89

Dilution Factor: 1


99-09-2 ————83-32-9 ————51-28-5 ————100-02-7 ———13-2-64-9 ———121*14-2 ———84-66-2 ———— •7005-72-3 —— -86-73-7 ———— -100-01-6 ———534-52-1 ———86-30-6 ————101-55-3 ———118-74-1 ———87-86-5 ————85-01-8 ————120-12-7 ———84-74-2 ————206-44-0 ———129-00-0 ———85-68-7 ————91-94-1 ————56-55-3 ————218-01-9 ———117-81-7 ———117-84-0 ———205-99-2 ———207-08-9 ———50-32-8 ————193-39-5 ———53-70-3 ————191-24-2 ———

1----3-Ni t roan t 1 in* I----Acenaph thane 1— --2 .4-Dini t rooheno 1 1. — -4-Ni t ro phenol 1----Dibenzofuran 1- — -2.4-Dinitroto 1 Liana 1——— Diethylphthalate 1._-_4_Ch loropheny 1-pheny let her _ 1- — --Fluorene 1----4-Ni t roan i 1 ina 1----4,6-Oini tr o-2 -methyl phenol _ I----N-Ni t rosod iphenylamine C 1) _ 1— --4-Bromopheny 1-pheny let her __ 1----Hexachlorobenzene 1— --Pentachlorophanol 1----Phananthrsne 1- — -Anthracene 1——— Di-n-butylphthalate 1----Fluoranthene 1----Pyrana rai _. 1—— -Butulfaanzulohtha late 1----3.3'-Dichlorobenridine 1— ~-Banza(a >anthracana. , , , 1--~-Chry»ene_ ,.., 1——— bi»(2-Ethylhexyl )phthalate I— *-Di-n-oct«jlohtha late 1----Banzo(b) f luo ran thane 1----Banzo(k)fluoranthana 1----Banro (a Ipyrena _ _ , 1----Indano(1.2.3-cd)purene 1____OihBn» (a rh) anthracene 1----BanzQ(g.hri)pap>jlana 1

1

5311535311111111115353111111531111111111112111111111111111111111

1IUIUIUtuIUIU- -IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1


FORM I SV -2 1/87 Rev

61



EPA SAhPLE NO.



Ma t r i x: (soil/ua t a r)WATER



\ Moisture: not dec ._____ dec .____„

Ext ract ion: CSepF/Cont/Sonc) CONT


Number TICs found: "7

SDG No.:

Lab Sample ID: CA19Q7C

Lab File ID: >G9078

Date Received:



Dilution Factor: ../


CAS NUMBER

01.02. >03.04.05.06. 141-78-607. 141-79-7

COMPOUND NAME

UNKNOWNACETONE DIMERUNKNOWNUNKNOWNUNKNOWNAcetic acid, ethyl ester3-Penten-2-one , 4- me thy 1-

RT

10.896.41

15.3222.1011.844.935. 15

EST. CQNC

2301305181332712

Q

i/jn*jjj^ \A-j

FORM I SU-TIC 1/87 Rev

62


ERA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

Cont ract

SAS No.

Matrix: (soi I/water) LJATER

Sample wt/vol: 850.0 (g/mL> ML

Level: C low/med) LOW

S Moisture: not dec. dec .



SDG No.:


Lab F i l e ID: >G9055

Date Received: f»/



Dilution Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) UG/L Q

108-95-2 ———111-44-4 ———OK C~J Q

541-73-1 ———106-46-7 ———100-51-6 ———95-50-1 ————95-48-7 ————108-60-1 ———106-44-5 ———621-64-7 ———67-72-1 ————98-95-3 ————78-59-1 ————88-75-5 ————105-67-9 ———65-85-0 ————111-91-1 ———

91-20-3 ————106-47-8 ———

59-50-7 ————91-57-6 ————77-47-4 ————

95-95-4 ————91-58-7 ————88-74-4 ————131-11-3 ———208-96-8 ———606-20-2 ———

1-- — Phenol 1- —— bis(2-Chloroethyl )ether ____ 1----2-Chlorophenol 1----1,.3-Dichlarobenzene • 1----1,4-Dichlorobenzena 1----Benzyl alcohol 1----1 .2-Dich lorobanzene 1----2-Methylphenol 1~---bis(2-Chloro i sop ropy 1 )ether_l----4-Methylpheno 1 1----N-Ni t roso-d i-n-propy lamine _ I----Hexaehlornethane 1----Ni t robenzene 1---- laophoron* . ., ._ 1----2-Nit rophanol 1—— -2r4-Dimethulphanol 1— — Benzoie acid 1-- — b is (2-Chlo roe thoxy )me thane _ 1- —— 2 r4-Oieh loroohano 1 1——— -1 j.2 r4-Tr ieh lornbenzane 1_ — -Naphthalene _._ ,., 1----4-Chloroaniline _ 1— --Haxaeh lorobutad iane t— --4-Ch loro-3-methy 1 phenol ____ 1———— 9-M«thylnaphth«l«ne _ 1— --Hexach lorocyc 1 open tad iene __ t—— --9 j4j.A-Tr iehlorophenn 1 1----2 .4T5-Tr ichloropheno 1 t———— 9-r:h]nron«phth«lan* .. ..., .. I----2-Ni t rnan i 1 ina ,_ 1———— Dimathylphthalate 1----Acenaphthylene „ 1----2r6-Dinitroto luena t

1

121212121212121212121212121212125912121212121212121212591259121212

1IIIIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI

FORM I SU -1 87


ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:


Sample wt/vol: 850.0 <g/mD ML

Level: C low/mod) LQU1

X Moisture: not dec. dec.

Extract ion: (SepF/Cont/Sonc) CQNT

GPC Cleanup: <Y/N> N pH:

Cont ract:

SAS No.:

II

SDG No.:


Lab File ID: >G9055

Date Received: /ff/



D ilut i on Fac tor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:<ug/L or ug/Kg) UG/L

99-09-2 ——— -83-32-9 ——— -51-28-5 ——— -100-02-7 —— -132-64-9 —— •121-14-2 —— -84-66-2 ———7005-72-3---86-73-7 ———100-01-6 ——534-52-1 ——86-30-6 ———101-55-3 ——118-74-1 ——87-86-5 ———85-01-8 ———120-12-7 ——84-74-2 ———206-44-0 ——129-00-0 ——85-68-7 ———91-94-1 ———56-55-3 ———218-01-9 ——117-81-7 ——117-84-0 ——205-99-2 ——207-08-9 ——50-32-8 ———193-39-5 ——53-70-3 ———191-24-2 ——

-----3-Nitroanilina-----Acenaphthene— _ — 2 ,4-Din i t ropheno 1___,_4_Ni t ropheno 1— — -Dibenzof uran• —— -2 . 4-Din 1 1 roto luene———— Diethvlphthalate_____4_Cn lorophenyl-phenylether _-----Fluorena-----4-Nitroani 1 me-----4,6-Dinit ro- 2 -me thy Ip he no 1 _-----N-Ni t roaodipheny lamina Cl ) __ — --4-Bromophenyl-pheny lather— ---Hexach lorobenzane-----Pentach lorophano 1-----Phenanthrana-----Anthracene-----Di-n-butulohthalate-- — -Fluo ran thane- ——— -Pyrena-.-- -Butyl ban zy Iphtha lata- ——— 3 .3 '-Dich lorahnnz idine, ——— -BenzaCa )anthracene———— Chry&ena———— bi»(2-Ethylhexyl )phthalate_--__Di-n-octy Iphtha late_ — --Banza Ch)fluoranthana-----Benzo(k)fluoranthena. — --BenzoCa Jpyrena _----- IndenoC 1 r2 .3-cd )o*urana-----DibanzCa Th ) anthracene_- ——— Banzo tq .h r i Jperulana

5912595912121212125959121212591212121212122412121212121212121212

1IUtuIUIUIUtutuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1


FORM I SV -2 1/87 Rev,

64

IFSEMIVOLATILE QRGANICS ANALYSIS DATA SHEET


ERA SAMPLE NO.

Lab Name:ETCNJ

Lab Code: Case No.:

Ma t r i x : (soil /wa t e r ) U1ATER



\ Moisture: not dec._____ dec.___



Number TICs found: 5

Cont ract :

SAS No.: SDG No.:

Lab Sample ID: CA19QSC

Lab File ID: >G9Q55

Date Received:



Dilution Factor: /.._

CONCENTRATION UNITS:(ug/L or ug/Kg>UG/L

CAS NUMBER

01. 141-78-602.03.04.05. 108-88-3

COMPOUND NAME

Acetic acid, ethyl esterACETONE DIMERUNKNOWNUNKNOWNBenzene, methyl-

RT

5.176.457.868.894.34

EST. CQNC

810150231915

Q

J

FORM 1 SO-TIC £ C 1/87 Rev,

IBSEHIUQLATILE ORGAN 1CS ANALYSIS DATA SHEET

EPA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No. :

Matrix: Csoi 1 /water) WATER

Sample wt/vol: 950. 0 (g/mL) ML

Level : C low/med) LOU

Contract:

SAS No.: SDG No.:


Lab F i l a ID: >G9064

Da te Rece wed : /,

tto i sture : not dec. dec.

Extraction: (SepF/Cont /Sane ) CONT




Dilut ion Factor: 1


I108-95-2 ——————— Phenol____________________154111-44-4———————bis (2-Ch loroethyl ) ether____I 1195-57-8 ———————— 2-Ch loropheno 1_____________I 1154L-73-1———————1,3-Dich lorobenzene________111106-46-7———————1,4-Dich lorobenzene________111100-51-6———————Benzyl alcohol_____________11195-50-1- — ———— -1,2-Dichlorobenzene________I 1195-48-7————————2-Methyl phenol_____________I 11108-60-l--------bis(2-Chloro isopropy 1)ether_l11106-44-5 ——————— 4-Methylphenol_____________197621-64-7--------N-Ni t roso-d i-n-propylamina_I 1167-72-1-———————Hexaehloroethane___________I 1198-95-3 ———————— Nitrobenzene_______________I 1178-59-1--------- Isophorone________________I 1188-75-5 ———————— 2-Ni t ropheno 1______________I 11105-67-9- —————— 2,4-Di methyl phenol_________I 1165-85-0————————Benzoic acid_______________1390111-91-1 ——————— b is (2-Chlo roe thoxy) me thane_til120-83-2———————2,4-Dichlorophenol_________I 11120-82-1———————1,2,4-Trich lorobenzene_____I 1191-20-3- ———— --Naphthalene.______________111106-47-8———————4-Chloroani 1 ine____________I 1187-68-3————•———Haxachlorobutadiene________11159-50-7————————4-Chloro-3-methylphenol____I 1191-57-6————————2-Methyl naphtha lene________I 1177-47-4— — ---—Hexachlorocyclopen tadlene__I 1188-06-2 ———————— 2,4,6-Tr ichloropheno 1______11195-95-4—— ———— -2,4,5-Tr ich lo ropheno 1______15391-58-7————————2-Ch loronaph thai one________I 1188-74-4————————2-Nitroani 1 me_____________153131-11-3 ——————— Dime thylpht ha late__________111208-96-8 —— ——— -Acenaph thy lene_____________I 11606-20-2 —— - ——— 2,6-Dinitro toluene_________I 11

IUIUIUIUIUIUIUIU1IUIUIUIUIUIU1IUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIU1

FORM I SU -1 66l/87 Rev.

\

' 1CSEMIUOLATILE ORGANICS ANALYSIS DATA SHEET

ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: Csoi 1/water) LJATER


Contract: I_______

SAS No.: SDG No.:


Lab F i l e ID: >G9Q64

Level: Clow/mod) LOU

% Moisture: not dec. dec

Ex tract ion: (SepF/Cont/Sonc) CONT


Date Rece ived: /O ////,



Dilut ion Factor: 1


CD - Cannot be separated from Diphenylamine

FORM I SU -2

Q

QQ no o83-32-9 ———— -51-28-5 ————100-02-7 ——— -132-64-9 ———121-14-2 ——— -84-66-2 ————7005-72-3 —— -86-73-7 ————100-01-6 ——— -534-52-1 ——— •86-30-6 ———— -101-55-3 ———119-74-1 ——— -87-86-5 ———— -85-01-8 ———— -120-12-7 ———84-74-2 ———— -206-44-0 ———129-00-0 ——— -85-68-7 ————91-94-1 ———— -56-55-3 ————218-01-9 ——— -117-81-7 ———117-84-0 ——— -205-99-2 ———207-08-9 ——— -50-32-8 ————193-39-5 ——— -53-70-3 ————191-24-2 ———

----3-Nit roani 1 me----Acenaphthene----2,4-Dinitrophenol——— 4-Ni t rophenol----Dibenzof uran , ,..— --2 , 4-Din i t roto luena—— -Diethylphthalate----4-Ch loropheny 1-pheny I ether _----Fluorene____4_N j t roam 1 me----4, 6- Din i t ro-2-methy Ipheno 1 _----N-Nitroaodiphenylamine (1 )___- — -4-6romopheny 1-pheny lather __----Hexach lorobenzene----Pentach loropheno 1----Phenan throne----Anthracene----Di-n-but-jlohtha late----Fluoranthene ,_—— -Pyrane----But'jlbanzvlohtha late— --3 P3 ' -Dich lorobenz id me— --BenzoCa ) anthracene----Chrymane——— bi»C2-Ethylhexyl )phthalata----Di-n-oet-jlphthalate----BanzoChlf luoranthena----Benzo(k)fluoranthene----Benza (a Jpyrane-- — Indeno(lr2r3-cd Ipurene---~Dihan2<arh)anthraeena----RanzaCg rh f i Jparulane

11531111531531111111111111111531531111111 11153111til1111111111111211111111111111111111111111111111

1IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIU1 I

1/87 Rev,

67

IFSEMIUQLATLLE ORGAN ICS ANALYSIS DATA SHEET


ERA SAMPLE NO.

Lab Name:ETCNJ

Lab Code: Case No.:

Contrac t

SAS No.:

Matrix: Csoi I /water >CJATER

Sample wt/vol: 950.0

Love 1 : (I ow/med ) LOLJ


Cg/mDML

dec.

Ex t r ac t i on: C SepF/Con t/Sonc) CONT

GPC Cleanup: CY/N) N PH:___

•*• _ jNumber TICs found:

SDG No.:


Lab File ID: >G9064

Date Received: /0//



Dilution Factor: t


CAS NUMBER

01. 97-61-002.03.04. 4536-23-605. 107-92-606. 142-62-107.08.09. 98-89-510. 79-09-411. 79-31-212.13.14.15.16. 7"? 09 4 ———17. 111-14-818.19. 98-89-520. 501-52-021. 79-31-222. 108-94-123. 98-89-524. 108-10-125. 4536-23-6

11 COMPOUND NAME

IPentanoic acid, 2-methyl-1 UNKNOUN1 UNKNOUNIHexanoic acid, 2-methyl-IButanoic acidIHexanoic acid1 UNKNOUN1 UNKNOUNt Cyc lohexanecarboxy 1 ic ac idIPropanoic acidIPropanoic acid, 2-methyl-1 UNKNOUN1 UNKNOUN1 UNKNOUN(ACETONE DIMER

IHvptanoic acid1 UNKNOUNICyc lohexanecarboxy 1 ic ac id(Banzanapropanoic ac idIPropanoic acid, 2-methyl-1 Cyc lohexanoneICyc lohexanecarboxy 1 ic ac id12-Pantanone, 4-methyl-IHexanoic acid, 2-methyl-111111

RT

11.259.2516.4012.698.9011.6910.8011.3714.126.676.859.508.077.977.07

——— BiTU — 113.2011.8213.8517.667.017.8914.183.74

12.31

EST. CONC

4025220210201816141201312121088

6565878643944

11 Q

\J1 JtJ1 JIJ1 J1 J1 JIJIJ1 JIJIJ1 J ,W^1 JIJI JI JIJIJ1 J1 J1 J111111

FORM I SU-TIC68

1/87 Rev,

18SEMI VOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:




M Moisture: not dec. dec.



Con t rac t :

SAS No.: SDG No.:


Lab File ID: >G9Q65

Date Received: (&I



Dilut ion Factor : 1


108-95-2 ——————— Phenol____________________111-44-4————— — bia(2-Chloroethyl )ether____95-57-8 ———————— 2-Chlorophenol_____________541-73-1———————1,3-Dichlorobenzene________106-46-7———————1,4-Oichlorobenzene________100-51-6- — - ——— Benzyl alcohol_____________95-50-1 ———— - —— 1,2-Dichlorobenzene________95-48-7———————-2-Methyl phenol_____________108-60-1——————bis(2-Chloroisopropyl)ether_106-44-5---———-4-Methylphenol_____________621-64-7--------N-Nitroso-di-n-propylamina_67-72-l---------Hexachloroe thane___________98-95-3 ——————— -Ni t robenzene_______________78-59-1---------Isophorone________________88-75-5 ———————— 2-Nitrophenol______________105-67-9--- ———— 2,4-Dimethyl phenol_________65-85-0-—--———Benzole acid_______________111-91-1- ————— -bis(2-Chloroethoxylmethane_120-83-2 ——————— 2,4-Dichlorophenol_________120-82-1———————1,2,4-Tr ich lorobenzene_____91-20-3————————Naphthalene ____________.106-47-8 ——————— 4-Chloroani 1 me____________87-68-3--—--——Hexachlorobutadiene________59-50-7————————4-Chloro-3-methyl phenol____91-57-6 —————— — 2-Methyl naphtha lene________77-47-4---------Hexachlorocyc1 open tadiene__gg_Q6-2---------2,4,6-TrichlorophenoI______95-95-4---------2,4,5-Trichloropheno1______91-58-7-———————2-Chloronaphthalene________88-74-4——-- —— -2-Nitroani 1 me_____________131-11-3---————Oimethylphthalate__________208-96-8 — -——,— Acenaph thy lene_____________606-20-2 — -- ——— 2,6-Dmi t rotoluene._________

111111111111111111111111111111115711111111111111111111571157111111

Q

FORM I SU -1 69

IUIDIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

1/87 Rev

1CSEMIUOLATILE ORGANICS ANALYSIS DATA SHEET

ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: Csoi1/water) UATER

Sample wt/vol: 8BO.O Cg/mL) ML


H Mois ture: not dec. dec.

Ex tract ion: CSepF/Cont/Sonc) CONT


Cont rac t:

SAS No.: SDG No.:


Lab File ID: >G9Q65

Date Received: /9f





99-09-2 ———— - — -3-Nitroanil me_____________83-32-9 ———— ——— Acenephthene_______________51-28-5-- —————— 2,4-Dinitrophenol__________100-02-7- — ———— 4-Nitrophenol______________132-64-9- —————— Dibenzofuran_______________121-14-2——————-2,4-Dinitrotoluene_________84-66-2--—-----Diethylphthalate___________7005-72-3—————4-Chiorophenyl-phenylether_86-73-7---------Fluorene__________________100-01-6 —— - ——— 4-Nitroanil me_____________534-52-1-————4,6-Dinitro-2-methylpheno1_86-30-6---------N-Ni trosodipheny1amine C1)_101-55-3--------4-Bromopheny1-phenylether__118-74-l--------Hexachlorobenzene______„___87-86-5---------Pentachloropheno 1 __ _____85-01-8 ————— - — Phenan throne_______________120-12-7———————Anthracene________________84-74-2- —————— -Di-n-butylphthalate________206-44-0———————Fluor ant hone_______________129-00-0 ——————— Pyrena____________________85-68-7————————Butyl benzyl ph thai ate_______91-94-1 ———————— 3,3 '-Dichlorobenzidine_____56-55-3----—---BenzoCa)anthracene_________218-01-9———————Chryaene________,__________117-81-7———————bi»(2-Ethylhexyl )ph thai ate_117-84-0———————Di-n-octylphthalate________205-99-2---————BenzoCb)fluoranthene_______207-08-9----———Benzo(k)fluoranthene_______50-32-8—--———Benzo(a)pyrene_____________193-39-5 — ————— Indeno< 1,2 ,3-cd)pyrene_____53-70-3 ————— - — Dibenz(a,h>anthracene______191-24-2 ——————— BenzoCg ,h, i Jperylene_______

(1) - Cannot be separated from Diphenylamtne

FORM I SU -2

5711575711111111115757111111571111.111111112311111111111111111111

IUIUIUtuIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI

1/87 Rev,

70

IFSEMIUOLATtLE ORGANICS ANALYSIS DATA SHEET


ERA SAMPLE NO.

Lab Name:ETCNJ

Lab Code: Case No.:

Mat r ix: (so i 1/water )LJATER


Leve1: (low/med) LQU

\ Moisture: not dec. _____ dec . ___



Number TICs found: y___

Cont rac t:

SAS No.: SDG No.:


Lab File ID: >G9065

Date Received: /£////*/



D i l u t i o n Factor: /


CAS NUMBER

01. 141-78-602.03. 127-18-404.05. 108-88-306.

COMPOUND NAME

Acetic acid, ethyl esterACETONE DIMEREthene , tetrachloro-UNKNOUNBenzene, methyl-UNKNOWN

RT

5.056.455.508.934.388.36

EST. CONC

2608256471312

Q

JJ

FORM I SU-TIC 711/87 Rev

IBSEMIUOLATILE ORGANICS ANALYSIS DATA SHEET

ERA SAttPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: tsoiI/water) UATER



H Moisture: not dec. dec.



Cont ract :

SAS No.: SDG No.:


Lab File ID: >G9Q66

Date Received: /#////S?7



Oilut ion Factor: 1


108-95-2 ——————— Phenol____________________111-44-4———————bis(2-Chloroethyl )ether____95-57-8 ———————— 2-Chlorophenol_____________541-73-1--————-1,3-Dichlorobenzene________106-46-7————— — 1,4-Dichlorobenzene________100-51-6 ————— — Benzyl alcohol_____________95-50-1 ——— — ——1,2-Oichlorobenzene________95-48-7————————2-Methyl phenol_____________108-60-1—-————bis(2-Chloroisopropyl)ether_106-44-5 ——————— 4-Methy Ipheno 1_____________621-64-7--------N-Nitroso-d i-n-propylamine_67-72-1—---———Hexachloroethane___________98-95-3 —————— --Nitrobenzene_______________78-59-1--------- Isophorone________________88-75-5--- ————— 2-Nitrophenol______________105-67-9 ——— ——— 2,4-Dimethyl phenol_________65-85-0---------Benzole ac id ____________111-91-1 ——————— bia(2-Chloroethoxy)methane_120-83-2 ———— "-2,4-Dichlorophenol_________120-82-l--------l,2,4-Trichlorobenzene_____91-20-3————————Naphthalene_______________106-47-8——.————4-Chloroani 1 me____________87-68-3*———---Hexachlorobutadlene________59-50-7————————4-Chloro-3-methyl phenol____91-57-6- ——————— 2-Methyl naphtha lene________77-47-4---------Hexachlorocyclopentad iene__8S-Q6-2---------2,4,6-Trichloropheno1.______95-95-4---------2,4,5-Trichloropheno1______91-58-7--—————-2-Chloronaphthalene________88-74-4——-- ——— 2-N it roan i 1 ine_____________131-11-3----- —— Dimethylphthai ate__________208-96-9-———-—Acenaphthylene_____________606-20-2—-———-2,6-Dinitrotoluene_________

111111111111111111111111111111115611111111111111111111561156111111

Q

IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM I SY -1 7 2


EPA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Cont ract:

SAS No.:


Sample ut/vol: 900.0 (g/mL) ML

Level : C low/med) LOLJ

S Mo ist ure: not dec. dec.


GPC Cleanup: <Y/N) N pH:

CAS NO. COMPOUND

SOG No.:


Lab File ID: >G9Q66

Date Received: /ff y ///J?f



Oi lut ion Factor: 1


99-09-2 ———— -83-32-9 ———— -51-28-5 ———— -100-02-7 ——— -132-64-9 ——— -121-14-2 ——— -84-66-2 ———— -7005-72-3 —— -86-73-7 ———— -100-01-6 ——— -534-52-1 ——— -86-30-6 ———— -101-55-3 ——— -118-74-1 ——— -87-86-5 ———— -85-01-8 ———— -120-12-7 ——— •84-74-2 ———— -206-44-0 ———129-00-0 ——— •85-68-7 ———— -91-94-1 ————56-55-3 ————218-01-9 ——— •117-81-7 ——— -117-84-0 ——— -2Q5-99-2 ——— -207-08-9 ——— -50-32-8 ————193-39-5 ———53-70-3 ————191-24-2 ———

----3-Ni troani 1 ine----Acenaphthene- — -2.4-Dinitrcmhenol----4-Nitrophenol----Dibenzof uran----2 .4-Dinitroto luena- —— Die thy Iph thai ate----4-Chloropheny l-pheny 1 ether _----Fluorene ,,„_----4-Nitroani 1 ine- — -4 ,6-Dini t ro-2-methy Ipheno 1 _----N-Nitrosodiphenylamine Cl ) _----4-Bromopheny 1-pheny let her __----Hexach lorobenzene----Pantaehloraphenol----Phenanthrene----Anthracene.---Di-n-butylphthalate----Fluor an thane----Pyrena— --Butulhanzulphtha late----3 f3 '-Dichlorobenzidine— -~Banzo(a)anthracene——— Chrysene—— bia(2-Ethylh«xyl Jphthalate _----Di-n-oetylphthalate----BanTQ th)fluoranthena----Benzo(k)fluoranthene----Benzo (a )pyrene ,---- Indano C 1 ,.2 f 3-cd ) pur one_---Dibenz(arh 1 anthracene-__-R«nTQ{g fh ri Iparylene

5611565611111111115656111111561111111111112211111111111111111111

1IDIUtuIUIUIUIUIUIUIUIUIUIU

- IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1U1

(1) - Cannot be separated from Diphenylamina

FORM I SU -2 731/87 Rev



ERA SAMPLE NO.

Lab Name:ETCNJ

Lab Code: Case No.:

Matrix: Csoi1/water)WATER



S Moisture: not dec. _____ dec .___.


GPC Cleanup: CY/N) N pH:___

Number TICs found: j_

Cent ract:

SAS No.: SDG No.:


Lab File ID: >G9066

Date Received: tol



Dilution Factor: /


CAS NUMBER

01. 141-78-602.03.04. 96-48-005.

COMPOUND NAME

Acetic acid, ethyl esterACETONE DIMERUNKNOUNButyro lactoneUNKNOUN

RT

5.066.428.908.239.84

EST. CONC

26067382520

Q

JJ

FORM I SO-TIC 741/87 Rev


ERA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

M a t r i x : (so: 1/water) UIATER

Sample iot/vol: 8 9 0 . 0 Cg/mL) ML

Level: ( lou/med) LOU

S M o i s t u r e : not dec. dec.

E x t r a c t i o n : (SepF/Cont/Sonc) SERF


Cont ract:

SAS No.: . SDG No.:

Lab Sample ID: CA21<*7C





Di lution Factor: 1


108-95-2 ——————— Phenol____________________111-44-4-----——bis(2-Chloroethyl)ether____95-57-8 ———— - — -2-Chlorophano 1_____________541-73-1- —- —— 1,3-Dich lorobenzene________106-46-7——-——1,4-Dichlorobenzene________100-51-6---- —— -Benzyl alcoho 1_____________95-50-1—-———l,2-0ichlorob»nzene________95-48-7————————2-Methylphenol_____________108-60-1—————bis(2-Chloroisopropyl)ether_106-44-5—-———-4-Methylphenol_____________621-64-7--------N-Nit roso-d i-n-propylam me__67-72-l---------Hexachloroe thane___________98-95-3-----—--Nitrobenzene______________78-59-1---------Isophorone________________88-75-5———---—2-Nitrophenol_____________105-67-9 — ------2,4-Dimethyl phenol_________65-85-0-————--Benzoic acid______________111-91-1--—————bis(2-Chloroethoxy)methane_120-83-2 ———— —— 2,4-Dich loropheno 1_________120-82-1 ———————1,2,4-Trich lorobenzene_____91-20-3—————*——Naphtha lene_______________106-47-8 ——————— 4-Chloroani 1 me____________87-68-3——---—-Hexachlorobutadlene________59-50-7- ——————— 4-Chloro-3-methylpheno 1____91-57-6————————2-Methylnaphtha lene________77-47-4---------Hexachlorocyclopentadlane__88-06-2---———--2,4,6-Trichloropheno1______95-95-4----—-—2,4,5-Trichloropheno1______91-58-7-—————2-Chlbronaphthalene________88-74-4----—-—2-Nitroani1ine_____________131-11-3—------Dimethylphthalate__________208-96-8-————-Acenaphthylene_____________606-20-2- —— —— -2,6-Dmitroto luene_________

111111111111111111111111111111115611111111111111111111561156111111

Q

IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM I SO -1 75 1/87 Rev.

. 1CSEMIUOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

Cont ract:

SAS No.:

Matrix: Csoi1/water) UJATER

Sample wt/vol: 890.0 <g/mL> ML

Level: Clow/med) LOW


Extraction: CSepF/Cont/Sonc) SERF


SDG No.:


Lab File ID: >G9071






99-09-2 ———————— 3-Nitroani 1 me_____________ 5683-32-9 ——— ——— -Acenaphthene______________ 1151-28-5--- —— - — 2,4-Dinitrophenol__________ 561-00-02-7—------4-Nit rophenol______________ 56132-64-9---- — — Dibenzofuran_______________ 11121-14-2-- — - — -2,4-Dmitroto luene_________ 1184-66-2- —— — -- -D i e thy Iph thai ate___________ 117005-72-3--——--4-Chlorophanyl-phenylether_ 1186-73-7————————Fluorene__________________ 11100-01-6 ——— - — -4-Nitroanil ine_____________ 56534-52-1 ——— - — -4,6~Dmitro-2-methylphenol_ 5686-30-6-----—--N-Nitrosodiphenylamine (1)_ 11101-55-3--------4-Bromophenyl-phenyle ther__ 11118-74-1--------Hexach lorobenzene__________ 1187-86-5- — - — — -Pentach loropheno 1__________ 5635-01-8---- — - — Phenanthrene______________ 11120-12-7——- —— -Anthracene________________ 1184-74-2 — -------Di-n-butylphthalate________ 11206-44-0-- ———— -Fluoranthene_______________ 11129-00-0 ——————— Pyrene____________________ 1185-68-7————————Butylbenzylphthalate_______ 1191-94-1-- — —•—-3,3 '-Dichlorobenzidme_____ 2256-55-3 —— -- — --Benzo(a )anthracene_________ 11218-01-9 ——————— Chryaene__________________ 11117-81-7———————bia(2-Ethylhexyl Jphthalate_ 11117-84-0- ———— — Di-n-octylphthalate________ 29205-99-2 — ——— — Benzo(b )f luoranthene_______ 11207-08-9 —— - — --BenzoCk )f luoranthene_______ 1150-32-8---------Benzo (a )pyrene_____________ 11193-39-5———————Indeno(l,2,3-cd)pyrene_____ 1153-7Q-3---------Dibenz(a,h)anthracene______ 11191-24-2 — -- — --Benzo(g,h,i Jperylene_______ 11


FORM I SU -2

IIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIIUIUIUIUIUIUI

1/87 Rev

76

IFSEMIUOLATI.LE ORGAN ICS ANALYSIS DATA SHEET

TENTATIUELY IDENTIFIED COtlPOUNDS

EPA SAMPLE NO.



Matr ix : (so i1/water)UATER

Sample wt/vo1: 890.0 (g/mL)ML

Lave I: (low/mod) LQU

S Moisture: not dec. _____ dec . ____

Extraction: (SepF/Cont/Sonc> SEPF

GPC Cleanup: (Y/N) N pH:____

Number TICs found: ?

SDG No.:


Lab Fi le ID: >G9Q71

Date Received: 10/12-'39

Date Extracted:10/13x89


Dilution Factor: _._./


t CAS NUMBER

01,02.03.OA. 541-05-905. 5429-56-106. 541-02-607.08.

COMPOUND NAME

ALKENEACETONE DIMERUNKNOUNCyclotrisi loxane, hexamethyl2-Propenoic acid, 2-CacetylaCyclopentasi loxane, decamethUNKNOWNUNKNOUN

•

RT

5.526.544.206.195.8114. 024.2625.72

EST. CQNC

50050302616201029

" aAJB J JJJJJJ

FORM I SU-TIC 7 Rev

IBSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

ERA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:




H Mo i store: not dec. dec.

Extraction: (SepF/Cont/Sonc) SERF


Cont ract :

SAS No.: SDG No.:

Lab Sample 10: CA2148C





D i l u t i o n Factor : 1


108-95-2 ——————— Phenol_____________________111-44-4———————bis(2-Chloroethyl )ether____95-57-8----——--2-Chlorophenol_____________541-73-1--—-—-1,3-Dichlorobenzene________106-46-7- — - ——— 1,4-Dichlorobenzene________100-51-6--- —— --Benzyl alcoho 1_____________95-50-1-----—--1,2-Oichlorobenzene________95-48-7- — -- ——— 2-Methyl phenol_____________108-60-1——————bis(2-Chloroisopropy1)eth«r_106-44-5--------4-Methylphenot_____________621-6 A-7--------N-Nitroso-di-n-propy lamine__67-72-1---------Hexachloroe thane___________9Q-95 _3 —————— --Nitrobenzene_______________78-59-1--------- I sophorone_________________88-75-5——--—-2-Nitrophenol______________105-67-9--------2,4-01me thyIpheno1_________65-85-0-—---—-Benzoic acid______________111-91-1-—————bis(2-Chloroethoxy)methane_120-83-2-—————2,4-OichlorophenoI_________120-82-1 — ————— 1,2,4-Tr ich lorobenzene_____91-20-3—————*——Naphthalene_______________106-47-8 ——————— 4-Chloroani 1 me____________87-68-3---------Hexachlorobutadlene________59-50-7—-————-4-Chloro-3-methyIpheno1____91-57-6————————2-Methylnaphtha lene________77-47-4---------Hexachlorocyclopentadlene__88-06-2- ———— —— 2,4,6-Tr ichlorophenol______95-95-4——-——--2,4,5-Trichloropheno1______91-58-7————-- — 2-Chloronaphthai one________88-74-4---- —— --2-Nitroam 1 ine_____________131-11-3-- ——— — Dimethylphtha late__________208-96-8——- —— -Acenaphthylene_____________606-20-2 — -- — --2,6-Dimtroto luene_________

1011111111111121112501111111111115011111118111111111111561156111111

Q

I JIUtu1UIUIUIUIIUIIUIUIUIUIUIUIJIUIUIUIIUIUIUIUIUIUIUIUIUIUIUIUI

FORM I SU -1 78 1/87 Rev.

. 1CSEMI VOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO

Lab Name: ETCNO

Lab Code: Case No.'

Cont ract

SAS No.



Leve 1 : ( low/med ) LOLJ

S Moisture: not dec dec

Extraction: (SepF/Cont/Sonc) SEPF


SDG No.:






Di lu tion Fac tor: 1

CAS NO, COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

99-09-2- —— -----3-Nitroani 1 me_____________15683-32-9 — --- — --Acenaphthene______________t 1151-28-5- ———— ---2,4-Dinitrophenol__________156100-02-7——- —— -4-Ni trophenol______________156132-64-9 ——————— Dibenzofuran______________I 1112 1-14-2-- — —— -2,4-Omitro toluene_________I 1184-66-2--- ————— Die thy Ipht ha late___________I 1170Q5-72-3-- —— --4-Chlorophenyl-phenylether_I 1186-73-7- ——— ----Fluorene__________________I 111QO-01-6-- — - —— 4-Nitroanil in«_____________156534-52-1———--—4,6-Dinitro-2-methylphenol_15686-30-6- — —— - — N-Nitrosodiphenylamme (1)_I 11101-55-3-- ——— --4-Bromophenyl-phenylet her__I 11118-74-l--------Hexach lorobenzene__________t 1187_86-5---------Pentach lorephcno 1__________I 5685-01-8--- — - —— Phenan throne______________1 11120-12-7——-----Anthracene________________I 1184-74-2--- — —— -Di-n-buty Ipht ha late________t 112Q6-44-0 —— -- —— Fluoranthene_______________I 11129-00-0———————Pyrene____________________I 1135-68-7———————Butylbenzy Ipht ha late_______I 1191-94-1—————^"---3l3'-Dichlorobenzidine_____12256-55-3---- — ---BenzoCa ) anthracene_________I 11218-01-9 ————— — Chrysene__________________I 11117-81-7———————bia(2-Ethylhexyl )phthalate_I 11117-84-0———————Di-n-octy Ipht ha late________I 11205-99-2 ———— - — 8enzo(b)f luoranthene_______I 11207-08-9 —— - ——— BenzoCk)f luoranthene_______I 1150-32-8 —— — —— -BenzoCa)pyrene_____________I 11193-39-5———————Indeno(l,2,3-cd)pyrene_____I 1153-70-3- — ————— Dibenz Ca,h) anthracene______I 11191-24-2--------Benzo(g,h,i Jperylene_______I 11

__________________________________________I__C1) - Cannot be .separated from Diphenylamine

FORM I SU -2

Q

IIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIU

1/87 Rev

79

IFSEMlUOLATfLE ORGAN ICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COflPQUNDS

EPA SAHPLE NO,

Lab Name:ETCNO

Lab Code:

Cont ract:

Case No.:

hatrix: (sot 1/water)WATER

Sample wt/vol: 900.0 (g/mLJML


S Moisture: not dec. _____ dec . ____


GPC Cleanup: CY/N) N pH:___

Numbor TICs found: ~b

SAS No.: SDG No.:






Dilution Factor: f


CAS

01.02.03.04.05.06.07.08.09.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.

NUMBER

928-94-9108-88-395-47-6100-41-4

541-02-6541-05-9

873-94-9

108-10-133467-74-2

540-97-6622-45-7611-14-3620-14-4

591-34-42050-24-0103-82-2

11 COMPOUND NAME

1 ALKENE12-Hexen-l-ol , (2)-1 Benzene, me thy 1-1 Benzene , 1,2-dimethyl-IBenzene, ethyl-1 UNKNOWN1 Cyc 1 op ent as i loxane, decameth1 Cyc l o t r i s i loxane , hexamethyl1 UNKNOWNICyclohexanone, 3,3,5-trimeth1 ACETONE DIMER1 UNKNOWN1 2-Pentanjone , 4- me thy 1-1 3-Hexen-l-o 1 , propanoate, CZ1 UNKNOWN1 UNKNOWN1 UNKNOWN1 Cyc lohexas i loxane , dodecametlAcetic acid, cyclohexyl este1 Benzene , l-ethyl-2-methyl-1 Benzene, l-ethyl-3-methyl-1 UNKNOWN1 UNKNOWNiPropanoic acid, 1-methylprop1 Benzene, l,3-diethyl-5-methyiBenzeneacetic acid11111

RT EST. CQNC

5.61 1907.97 1504.65 1307.38 1107.09 1 5517.14 1 27014. 106.264.2411.446.6919.303.94

13.5525.7719.9427.4617.3611.509.6110.368. 0521.536.9313.7316.02

220181717171108669782754844333832020

l l1 ' Q 1. |..... |

1 J 11 J 11 J 11 J 11 J 11 J 11 J 1! J 11 J 11 J, 1I£J<A- ii j ii j ii j ii j ii j ii j ii j ii j ii j ii j ii j ii j ii j ii j ii j ii i1 1I :i li i

T

FORM I SU-TIC Rev.

IBSEMIUQLATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: CsoiI/water) WATER



S Mo i sture: not dec. dec.



CAS NO. COMPOUND

Con t ract :

SAS No.: SDG No.:


Lab File ID: >G9067

Date Received: /0/ll(f



Di lution Factor: 1

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

I108-95-2 ——————— Phenol____________________I 11111-44-4———————bis(2-Chloroethyl )ether____I 1195-57-8 ———————— 2-Chlorophenol_____________I 11541-73-1 ——————— 1,3-Dichlorobenzene________111106-46-7- ————— -1,4-Dichlorobenzene________I 11100-51-6 ——————— Benzyl alcohol_____________I 1195-50-1 — -------1,2-Dichlorobenzene________I 1195-48-7- —— ———— 2-Methyl phenol_____________I 11108-60-1 ——————— bia(2-Chloroisopropy 1 )ether_l 11106-44-5 ———— - — 4-Methyl phenol_____________I 11621-64-7--------N-Nitroso-d i-n-propylamine_I 1167-72-1------ —— Hexach loroethane___________I 1198-95-3————————Nitrobenzene_______________I 1178-59-1- —— —— — Isophorone________________I 1188-75-5 ——— --- — 2-Nitrophenol______________I 11105-67-9 — — ——— 2,4-Dimethylpheno 1_________I 1165-85-0---------Benzo ic ac id_______________I 57111-91-1-- — ——— bis(2-ChloroethoxyJmethane_I 1112 0-83-2-- ————— 2,4-Dichlorophenol_________I 11120-82-1- — ———— 1,2,4-Tr ich lorobenzene_____I 1191-20-3 — —— —— -Naphthalene_______________.1 11106-47-8 ——————— 4-Chloroani 1 me______;_____I 1187-68-3 ———————— Hexach lorobutad iene________I 1159-50-7————————4-Chloro-3-methylphenol____I 1191-57-6——— ———— 2-Methylnaphtha lane________I 1177_47_4_-_------Hexachlorocyc1 opentadlene__I 1188-06-2----- —— -2,4,6-Trichlorophenol______I 1195-95-4——— ——— -2,4,5-Tr ich loropheno 1______15791-58-7—————---2-Chloronaphthalene________I 1188-74-4---- —— --2-Ni troam 1 me_____________157131-11-3------ — Oimethylphthalate__________t 11208-96-8 — -- ——— Acenaph thy lene_____________I 11606-20-2- —— — --2,6-Dmitroto luene_________I 11

I

Q

IIUtuIUIUtutuIUIUIUIU1UIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI

FORM I SU -1 /87 Rev.

• icSEMIUOLATILE ORGANICS ANALYSIS DATA SHEET

ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Coda : Case No.:

Matrix: (so:1/water) WATER



S Mo i st ure: not dec. dec.



Cont rac t:

SAS No.: SDG No.:


Lab File ID: >G9067

Date Received: (O



Di1u tion Fac tor: 1


99-09-2 ———————— 3-Nitroani 1 ine_____________83-32-9 —— —— - — Acenaphthene_______________51-28-5 ———————— 2,4-Oinitropheno 1__________10 0-02- 7—————--4-Nitrophenol______________132-64-9———————Dibenzofuran_______________121-14-2--- —— — 2,4-Dini trotoluene_________84-66-2 ——————— -Diethylphthalate___________7005-72-3 —— ——— 4-Chloropheny1-phenylet her_86-73-7————————Fluorene__________________100-01-6- ————— -4-Nitroani 1 ine_____________534-52-1--—--—4,6-Dinitro-2-methylphenol_86-30-6---------N-Nitrosodiphenylamine (I)_101-55-3--------4-Bromopheny1-phenylet her__118-74-1--------Hexachlorobenzene _______87-86-5---------Pentachloropheno1__________85-01-8- — - ———— Phenanthrene_______________120-12-7—— ——— -Anthracene________________84-74-2---————-Di-n-butylphthalate________206-44-0———--—Fluoranthene_______________129-00-0 ———— —— Pyrene_____________________85-68-7---------Butyl benzylphtha late_______91-94-1 — —————— 3,3 '-Dichlorobenzidine_____56-55-3---------Benzo<a)anthracene_________218-01-9 ———— —— Chrysene__________________117-81-7———————bisC2-Ethylhexyl iphthalate_117-84-0-—————Di-n-octylphthalate________205-99-2——--—-BenzoCb)fluoranthene_______207-08-9————Benzo(k)fluoranthene_______50-32-8---------Benzo(a)pyrene_____________193-39-5 —— ———— Indenod ,2 ,3-cd)pyrene_____53-7Q-3---------Dibenz(a,h)anthracene______191-24-2--——-—BenzoCg,h,i)perylene_______


FORM I SV -2

5711575711111111115757111111571111111111112311111111111111111111

IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

1/87 Re-

82

IFSEMIUOLATI-LE ORGAN ICS ANALYSIS DATA SHEET


ERA SAMPLE NO.

Lab Name:£TCNJ

Lab Code: Case No.:

Matrix: (soi 1/wa ter JUJATER

Sample wt/vol: 870.Q (g/mL)ML


\ Moisture: not dec. _____ dec . ___



Number TICs found: ^

Cont ract:

SAS No.: SOG No.:


Lab File ID: >G9Q67

Date Received: /Otffff



Dilution Factor: /


CAS NUMBER

01. 141-78-602.03.

COMPOUND NAME

Acetic acid, ethyl esterACETONE DIMERUNKNOUN

RT

5.076.428.90

EST. CONC

3606646

Q

^ w

FORM I SV-TIC 8r387 Rev,

IDPESTLCIDE ORGAN1CS HNALYSIS DATA SHEET

EPtt SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

(la t r i x : '.soil /wa t e r ) WATER

Sample wt/vol: 920.0 Cg'mL) ML

Level: 'low/mod) LOW

% M o i s t u r e : not dec. dec.

Extraction: (SepF''Cont/Sonc;( 3EPF

GPC Cleanup: (Y/NJ N pH:

Con t rac t:

No.: SOG No.:

Lab Sample ID: CH1S39G

Lab File ID: -HA547

Date Received: *o/o-( /J^

Date Extracted: 10-'12 '8

Date Analyzed: 11-15/39

D i lu t ion Fac tor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:lug/L or ug--'Kg) UG--'L

319-64-6 ———— —— alpha-BHC________319-65-7——————beta-BHC__________319-36-8 ——————— delta-BHC________58-89-9---------gamma-BHC(Lindane J.76-44-8-~-------Heptachlor________309-QO-2--------AIdrin____________1024-57-3-------Heptachlor epoxide.959-98-8-- ————— Endosulfan I______60-57-1----———--Dieldrin___________72-55-9 ———— - —— 4,4'-DDE__________72-20-8--- —----Endr in____________33213-65-9------Endosulfan I I_____72-54-8-- ————— -4, 4'-ODD__________1031-07-8-------Endosulfan sulfate.50-29-3———————-4,4'-DOT__________72-43-5------- — Methoxyen lor______53494-70-5----—Endrin ketone_____5103-71-9 —————— alpha-Chlordane__5103-74-2-------gamma-Chlordane___8001-35-2-------Toxaphene_________12674-11-2 ————— Aroc lor-10 16______11104-28-2 ————— Aroc lor-1221______11141-16-5 ————— Aroc lor-1232______53469-21-9 ————— Aroc lor-1242______12672-29-6 ————— Aroc I or-1248______11097-69-1------Aroclor-1254______11096-32-5------Aroclor-1260______

. 054

. 054

.054

. 054

.054

. 054

.054

. 054

. 110

.110

.110

. 110

. 110

. 110

. 110

.540

.110

. 054

. 0542.200

.540

.540

.540

.5401. 1001. 100

Q

IDIUIUIUtuIUIUIUIUIUI UIUIUIUIU1UIUIUtutuIUIUIUIUIUIUIU

FORM I PEST

84

IDPESTICIDE ORGANICS ANALYSIS DATA SHEET

ERA SAMPLE NO.

Lab Name: ETCNJ


Matrix: (.so i 1 .'water ) UATER

Sample wt'vol: 970.0 Cg/'mLJ ML

Lave 1 : ( la warned ) LOW

S Mo i 5 t ure; not dec. dec.

Ex t rac t ion : tSepF--'Con t -'Sonc ) SEPF

GPC Cleanup: (Y,-N' N pH:

Lon tract:

No.: SQ£ ho . :

uab Sample ID: CAi39Qb

Lab File ID: --Hm54S

Date Received: io/c,7 / ?7

Date Extract«d: 10--'12--aa

Date Analyzed: ll'15--89

D i l u t i o n Fac tor: 1

GAS NO, COMPOUNDCONCENTRATION UNITS:tug''L or ug-'Kg > UG-'L

319-64-6--------alpha-BHC________319-65-7———————beta-BHC_________319-86-8——— ——— delta-BHC________58-39-9-----—--gamma-BHCCLindane).76_44-8---------Heptachlor________309-00-2--------AIdrin____________1024-57-3-------Heptachlor e p o x i d e .959-98-8--------Endosulfan I______60-57-1—-—----DieIdrin__________72-55-9-- ———— --4 ,4'-ODE__________72-2Q-3---------Endrin___________33213-65-9———--Endosulfan 11_____72-54-8 ——————— -4,4'-ODD__________1031-07-8----—-Endosulfan sulfate.50-29-3 ———————— 4 ,4'-DOT__________72-43-5---------Methoxychlor______53494-70-5------Endrin ketone_____5103-71-9—-——-alpha-Chlordane___5 1 03-74-2-------gamma-Ch1ordane___8001-35-2--—---Toxaphene_________12674-11-2 ————— Aroclor-1016______11104-28-2 ————— Aroc lor-1221______11141-16-5 ————— Aroc lor-1232______53469-21-9--———Aroclor-1242______12672-29-6 ————— Aroc I or-1248______11097-69-1-———-Aroclor-1254______11096-82-5--———Aroclor-1260______

. 054

. 054

. 054

. 054

. 054

. 054

. 054

. 054

. 110

. 110

. 110

. 110

. 110

. 110

. 110

. 0

. 110

. 054

. 0542.20 0

.5*01. 1001. 10G

Q

FORM I PEST

85

IDPESTICIDE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO

Lab Name: ETCNJ

LabCode: Case No.:

hat r ix : '. so i 1/'water ; WATER

Sample wt/vo1: 8?0 . 0 tg^mL) ML

Leve 1 '• C 1 ow/med ) LOU

^Moisture: not dec. dec.

Extraction: '. SepF/Con t --'Sonc ) SERF

GPC Cleanup: f,Y--'NJ N pH:

Con t r a c t : I ___

SAS No.: SDG No.:

Lab Sample ID: C

Lab F i l e ID:

Date Received: 10 /u /tf^

Date Ext r acted: 10 "12 3

Date Analyzed: 11 1?- 59

D i l u t i o n Factor: 1

CrtS NO. COMPOUNDCONCENTRATION UNITS:lug-'L or ug-'KgJ UG--'L

319-64-6 ——————— alpha-BHC_________719-65-7- —————— beta-BHC_________319-86-3——————— delta-BHC_________58-89-9---------gamma-BHC(Lmdane J.76-44-8----—---Heptachlor________309-00-2--------Aldrin___________1024-57-3-------Heptachlor epoxide.959-93-8--------EndosuIfan I______60-57-1----—---Dieldrin__________72-55-9-- —— - —— 4, 4 '-DDE_________72-20-a-------~-Endrin_____________?3213-65-9------EndosuIf an I I_____72-54-8---------4,4'-ODD__________1031-07-8-------EndosuIf an sulfate.50-29-3—-------4,4'-DOT__________72-43-5---------Methoxychlor______<?3494-70-5------Endr in ketone_____5103-71-9 —— ———aipha-Chlordane___5103-74-2-------gamma-Ch1ordane___8001-35-2-—--—Toxaphene_________12674-11-2 ————— Aroclor-1016______11104-28-2 ————— Aroc lor- 1221______11141-16-5 ————— Aroc lor-1232______53469-21-9 ————— Aroc lor-1242______12672-29-6------Aroclor-1243______11097-69-1------Aroclor-1254______11096-82-5------rtroclor-1260______

.060

.060

. 060

.060

. 060

. 060

. 060

. 060

. 120

. 120

. 120

. 120

. 120

. 120

. 120

. 600

. 120

. 060

. U 6 02 . 400.600. 600.600. 600. oOO1.2001.200

Q

IIIIUIUIUIUIUIUIUIUIUtuIUIUIUIUIU• uIUIUiUIU1'JIUIUIUIUIU

FORM I PEST 1 37 Rev.

86

IDPESTTCIDE ORGANICS ANALYSIS DATA SHEET

ERA SHMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

Matr ix: laai1/water) WATER

Samp 1e wt/vo1: 9^0.0 t g

Leve 1 : f. low/med ) LOLJ

S M o i s t u r e : no t d ec .

Contract:

SAS No . :

ML

dec.

Ext pact ion: (SepF/Con t/Sonc) SEPF

GPC Cleanup: CY/N) N pH:'

SDG No.:

Lab Sample ID: CA1992G

Lab File ID: >HA549

Date Received: 10/01 / 99

Date Extracted: 10--'12'S9

Date Ana 1 yred: 11-- 15-'6^

D i 1 u t ion Fac tor: 1

CAS NO. COMPOUNDCONCENTRATION UNITSC ug -'L or ug/Kg ) UGX

3.19-64-6-——————alpha-BHC_________319-65-7———————beta-BHC__________319-36-8——————-delta-BHC________58-89-9---------gamma-BHC(Lindane ).76-44-8------—-Heptachlor_______309-00-2--------AIdrin___________1024-57-3-------Heptachlor epoxide959-98-8-——————Endosulfan I______60-57-l---------Oieldrin__________72-55-9 ———— ——— 4 ,4'-DDE__________72-20-8--—---—Endrin____________33213-65*9———--Endosulfan I I_____72-54-8-—---—-4,4'-ODD__________1031-07-8-------Endosulfan sulfate.50-29-3 ———————— 4,4'-DOT__________72-43-5--—-----Methoxychlor______53494-70-5—-——Endrin ketone____5103-71-9—-----alpha-Chlordane___51Q3-74-2-------gamma-Chlordane___8001-35-2---—--Toxaphene________12674-11-2————-Aroclor-1016______11104-28-2 ————— Aroc lor-1221______11141-16-5 ————— Aroc lor-1232______53469-21-9 ————— Aroclor-1242_____•_12672-29-6 ————— Aroc I or-1248______11097-69-1 ————— Aroc lor-1254______11 096-82-5------Aroclor-1260______

.053

. 053

.053

. 053

.053

.053

.053

. 053

. 110

. 110

. 110

. 110

. 110

. 110

. 110

.530

. 110

. 0532. 100.530.530.530,530.5301. 1001.100

IUIUIUIUIUIUIDIUIUIUIUIUIUIUIUIUiuIUIUIUIUI UIUIUIUIUI UI

FORM I PEST

37


ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No. :

M a t r i x : (soil/waterj WATER

Sample ui t / v o l : 940.0 Ig/mL) ML

Leve1: Ilow/med) LOW

^ M o i s t u r e : not dec. dec.

E x t r a c t i o n : (SepF/Cont/Sonc) SEPF

GPC Cleanup: CY/N) N ph:

Con t rac t '

No.: SDG No.:

Lab Sample ID: CA1907G

Lab F i l e ID: >OA*98

Date Received: lo/e>"7/S^>o / •-Jit*

Date Extracted: 0?'in.r''Q9



CAS NO. COMPOUNDCONCENTRATION UNITS:tugxL or ug/KgJ UG-'L

319-64-6 ——————— alpha-BHC________319-65-7-----——beta-BHC_________319-86-3 ——————— delta-BHC________58-e9-9---------gamma-BHCCLmdane ).76-44-8---------Heptachlor_______309-00-2 ——————— A l d r in____________1024-57-3---——Heptach lor epoxide.959-98-8 ——————— E n d o s u l f a n I______60-57-1—----—-Dieldrin__________72-55-9 —— ————— 4, 4'-DDE__________72-20-8————————Endr in____________33213-65-9 ———— -Endosulfan I I_____72-54-8 ———————— 4,4'-DDD__________1031-07-8——----Endosulfan sulfate.50-29-3--———————4,4'-DOT_________72-43-5------——Methoxychlor______53494-70-5—• ——— Endrin ketone____5103-71-9 —————— alpha-Chlordane___5103-74-2 —————— gamma-Ch lordane___8001-35-2———--Toxaphene________12674-11-2 ————— Aroclor-1016_____11104-28-2 ————— Aroc lor-1221______11141-16-5—————Aroc lor-1232______53469-21-9------Aroclor-1242______12672-29-6 ————— Aroc lor-1243______11097-69-1———--Aroclor-1254______11096-82-5 ————— Aroc lor-1260______

.053

. 053

.053

.053

.053

. 053

.053

. 053

. 110

. 110

.110

. 110

.110

.110

.110

.530

. 110

.053

. 0532.100.530.530.530.530.5301. 1001.100

Q

IUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUtuIU!UIUIU

FORM I PEST 1/87 Rev.


EPA SAMPLE NO

Lab Name: ETCNJ

Lab Code : Case No. :



Leve 1 : C low^'med ) LQU

S Mois t ure : not dec. dec.

Extraction: ( SepF^Con t /Sonc ) SERF


Cont ract:

SAS No.: SDG No.:

Lab Sample ID: CA19Q8G

Lab Fi le ID: >Hrt55G

Date Received: Iw/o ~i

Date Extracted: 10-'12- 3-9

Date Ana lyzed: II''15-39


CAS NO. COMPOUNDCONCENTRATION UNITS:tug-'L or ug--KgJ UG-'"L Q

319-64-6 -----519-65-7 -----319-86-3 -----58-89-9 ------76-4a-8-- — —309-OQ-2 -----1024-57-3 - ——959-98-8-----60-57-1 ------72-55-9 ------72-20-8 ———— -33213-65-9 ——72-54-8 ----- -1031-07-8 ----50-29-3 ----- -72-43-5 ------53494-70-5 - —5103-71-9 ----5103-74-2 ———8001-35-2 ———12674-11-2 ——11104-28-2 ——11141-16-5 ——57469-21-9 ——12672-29-6 ——11097-69-1---11096-82-5 ——

—— aloha-BHC---beta-BHC—— delta-BHC---oamma-BHCC Li ndane i---Hep tach 1 o r---Aldr in---Heptachlor epoxide---Endosu 1 f an I---D ie Idr in—— 4.4h-DDE---Endr in---Endosu 1 fan II—— 4.4'-DDD---Endosulfan sulfate- — 4.4--DDT---Methoxych lor---Endr in ketone---alpha-Chlordane---gamma-Ch lordane---Toxaphene_ — Aroclor-1016---Aroc lor-1221—— Aroclor-1232---Aroc lor-1242---Aroc lor-1248---Aroclor-1'^54---Aroc lor-1260

.059

. 059

.059

. 059

. 059

. 059

. 059

. 059

. 120

. 120

. 120

. 120

. 120

. 120

. 120

.590

. 120

. 059

. 0592.400.590.590.590.5^0.5901.2001.200

1IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1 UIUIUIUIUIU1 UIU•U1

FORM I PEST 1 3

39


EPM SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

Mat r ix : ', so i I/water ) UATER

Sample wt/vo1:970.0 Cg^mLJ ML

Level: Clow/medJ LQU)

*i Moisture: not dec, dec.

Ex t rac t ion : ( SepF/Cont --'Sonc ) SEPF

GPC Cleanup: (,Y.-'Nj N pH:

Con tract:

No.: SOG No.:

Lab Sample ID: CA21j4**b

Lab F i l e ID: ^Hrt559

Date Rece i^ed : io/" J&c\

Date Extracted: lu'12 3°

Date Ana lyzed: II I1? 39


NO. COMPOUNDCONCENTRATION UNITS:(ug--''L or ug/Kgi LJG.-L

319-64-6--——---alpha-BHC_________319-6?-?----——-beta-BHC_________319-86-8 ——————— delta-BHC________58-89-9---------gamma-BHC(Lindane ),76-44-3----—---Heptachlor________309-00-2-- ——— --Aid pin____________1024-57-3--—---Heptachlor epoxide.9?9-93-8--------Endosulfan I______60-57-l---------Dieldrin__________72-55-9---- ——— -4, 4'-DDE__________72-20-8---------Endrin____________33213-65-9 —— ---Endosulfan I I_____72-54-3 ———— ——— 4,4' -DDD__________l031-Q7-8-------Endosulfan au 1 fate.50-29-3 ———————— 4,4'-DDT__________72-43-5---—----Methoxychlor______53494-70-5------Endrin ketone_____5103-71-9 —————— alpha-Chlordane___5103-74-2-------gamma-Chlordane___8001-35-2-—-——Toxaphene________12674-11-2 ————— Apoclor-1016_____11104-28-2 ————— Aroc lor-1221______11141-16-5 ————— APQC lor-1232_____57469-21-9 ————— Aroc lor-1242______12672-29-6 ————— Aroc lor- 12*3______I 1097-69-1 ————— -Aroclor-125*______II 096-82-5------Aroclor-1260______

. 052

. 052

.052

. 052

.052

.052

.052

. 052

.100

. 100

. 100

. 100

. 100

. 100

. 100

.520

. 100

. 052

.0522.100.520.520.520.520.52011

Q

1UIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM I PEST 1 37

90

IDPESTfCIDE ORGAN IC3 ANALYSIS DATA SHEET

ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Matr ix: iso i1/water) WATER

Sample wt/vol: 890.0 Cg.-mL) ML

Leve1: t low/med) LOW

% Moisture: not dec. dec.

Extraction: (SepF/Cont ''Sonc ) SEPF


Con t rac t:

S*S No.: 5DG No.;

Lab Samp le ID: CnS i45G

Lab F i l e ID: >HH5oO

Date Received: io/n /2 9

Date Extracted: 1 0 -•' 12 89

Date Analyzed: ll-'15/39

0ilut ion Fac tor: 1

CrtS NO. COMPOUNDCONCENTRATION UNITS:tug/L or ug-"Kg) UG/L

3.19-64-6 ——————— alpha-BHC________319-65-7- —————— beta-BHC_________319-86-8 ——————— delta-BHC________58-89-9-—------gamma-BHC(Lindane).76-44-8---------Heptachlor________309-00-2----—--Aldrin___________1024-57-3-——---Heptachlor epoxide.959-98-8--------EndosuIfan I______60-57-1 ——— ———— Dieldr in__________72-55-9 ——————— -4, 4'-DDE__________72-20-8——------Endrin____________33213-65-9 ————— Endosu If an I I____72-54-8 ———————— 4,4'-DDD__________1031-07-8-------£ndosulfan su If ate,50-29-3 ———————— 4,4'-DDT__________72-43-5----——--Methoxychlor______53494-70-5-————Endrin ketone_____5103-71-9————alpha-Chlordane___51Q3-74-2-------gamma-Chlordane___8001-35-2-—-—-Toxaphene_________12674-11-2—————Aroclor-1016_____11104-28-2 ————— Aroc lor-1221_____11141-16-5—————Aroclor-1232______53469-21-9------Aroclor-1242______12672-29-6 ————— Aroc lor-1248______11097-69-1------Aroclor-1254______11096-82-5------Aroclor-1260______

.056

.056

.056

.056

.056

. 056

. 056

.056

.110

. 110

. 110

. 110

. 110

. 110

.110

.5oO

.110

.056

.0562.200.560. 56 0.560.5&0.5601. 1001. 100

tuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM I PEST 1--37

91

10PESTICIDE ORGANICS ANALYSIS DATA SHEET

ERA NO.

Lab Name: ETCN4

Lab Code: Case No.:

M a t r i x : ( s o i l / w a t e r ) WATER

Samp le uif^o 1 : 9 0 0 . 0 Cg -'mL ) ML

Level: ( l ow /med) LQU

\ Moisture: not dec. dec.

Extraction: (.SepF/Cont 'SoncJ 3EPF

GPC Cleanup: C'ixN) N pH:

Con t rac t:

SrtS No . : SD£ Nc.:

Lab Sample ID: Ch2 I'+c'j

Lab F i l e ID: -HA5ol

Date Received: (^/"/?1

Date Extracted: 10 -'II 1 5

Date nnalyzsd: II 15-39


CMS NO. COMPOUNDCONCENTRATION UNITS:'.ug--'L or ug--'Kgj UG.-'L

319-64-6-——----alpha-BHC_________319-65-7--------beta-BHC__________319-86-8 ——————— delta-BHC________5S-89-9-—------gamma-BHC(Lindane).76-44-8---——-—Heptachlor________309-00-2 ——————— A l d r in____________1024-57-3————-Heptachlor epoxide.959-98-8——————— Endosulfan I_____60-57-1 ———————— D i e l d r in_________72-55-9 ———— ——— 4 ,4'-DDE__________72-20-8---—----Endrin____________33213-65-9- ——— -Endosulfan I I____72-54-3 ———————— 4,4'-DDD__________1031-07-8----J--Endosulfan sulfate50-29-3 ———————— 4,4'-DOT__________72-43-5-----—--Methoxychlor_____53494-70-5--—--Endrin ketone____5103-71-9—-----alpha-Chlordane__5103-74-2-------gamma-Chlordane___3001-35-2-——---Toxaphene________12674-11-2————-Aroclor-1016______11104-28-2 ————— Aroc lor-1221_____11141-16-5 ————— Aroc lor-1232______53469-21-9 ————— Aroc lor-1242______12672-29-6————-Aroc1 or-1248_____11097-69-1 ————— Ar odor-125 4______11096-82-5--———Aroclor-1260______

0560560560560560560560561101101101101101101105601100*6056. 2 0 05605bO

.560

.5601.1001. 100

c

IUIIIIUIUIUIUIUIUiljIUillIUIUIUmI UiUIUiUI UIUI U'UIUIUIUt u

FORM I PEST

92


ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Ma t r i x : (.soil -''wa t e r ) WATER

Sample wt'vol: 910.0 (g/mL.) ML

Leve 1 : (. 1 ow/med ) LQU

S Mo i s tu re : not dec. dec.


GPC Cleanup: <Y/N) N pH:

Cont rac t:

SnS No.: SDG No.:

Lab Samp 1e ID: CA2147G

Lab File ID: >KB102

Date Received: iO'12/99

Date Extracted: 10/13-'99


Di 1 u t ion Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:<ug/L or ug/Kg) UG/L Q

319-64-6 ————319-65-7 -----319-86-8 ————58-89-9 ------76-44-8 —————309-00-2 -----1024-57-3 ———959-98-8- ———60-57-1 —————72-55-9 ———— -72-20-8 —— ——33213-65-9 ——72-54-8 ------1031-07-8 ———5Q-29-3 ------72-43-5 —————53494-70-5 ——5103-71-9 ———5103-74-2 ———8001-35-2 ———12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 — -11096-82-5 ——

— -aloha-BHC—— beta-BHC—— delta-BHC---qatnma-BHCCL indane )---Hept ach lor---Aldr in---Heptachlor epoxide---Endoau 1 fan I---Die Idr in---4.4'-DDE---Endr i n---Endoau 1 fan I I—— 4.4(-DDD---Endosu 1 f an sulfata—— 4.4'-DDT---Methoxych lor---Endrin katana^.---a Ipha-Ch lardane---gamma-Ch lordane---Toxaphene—— Aroclor-1016—— Aroc lor-1221——— Aroclor-1232——— Aroelor-1242——— Arnclor-1248—— Aroclor-1254---Aroclor-12eiO

.055

.055

.055

.055

.055

.055

.055

.055

.110

.110

. 110

. 110

.110

.110

.110

.550

. 110

.550

.5502.200.550.550.550.550.5501. 1001. 100

IIUIUIUtuIUIUIUIUIUIUIUIUIUiUIUIUIUIUIUIUIUIUIUIUIUIUIU1

FORM I PEST 1/37 Rev

93

IDPESTICIDE GRGHNICS ANALYSIS DATA SHEET

ERA NO

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: ( so i 1''water ) WATER

Sample wt/wol: 930.0 tg-"mL) ML

Level: (low/med) LQw

\ M o i s t u r e : not dec. dec.

E x t r a c t ion: (SepF/Cont/Sonc) SERF


Contract:

SnS No . : SDG. Mo . :

Lab Sample ID: Cn2l43G

Lab Fi le ID: >k.B103

Date Rece ived: IQ/IC-'S0

Date Extracted: 10 --'13 -89

Date Analyzed: 11--' 16-39

D i l u t i o n Fac tor : 1

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L Q

•319-64-6 ————319-65-7 — ——319-86-8 -----58-89-9 - — ——76-44-3 ———— -309-00-2 -----1024-57-3 —— -959-98-8 ————6Q-57-1 ------72-55-9 — —— -72-20-8 ------33213-65-9 ——72-54-8 ------1031-07-3 ———50-29-3-- ———72-43-5 ------53494-70-5 ——5103-71-9 ———5103-74-2 ———8001-35-2 —— -12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ——12672-29-6 ——11097-69-1 ——11096-82-5 ——

---aloha-BHC---beta-BHC—— delta-BHC---aamma-BHCCLindane )---Heot ach lor---A Idr in---Heptachlor epoxide---Endosu 1 1 an I---Die 1 dr i n—— 4.4'-DDE---Endr in---Endosu 1 fan II---4.4'-DDO---Endoaulfan aulfate—— 4.4'-DDT---Methoxychlor---Endrin ketona---alpha-Chlordane---qamma-Ch lordane ...---Toxaphene.,—— Aroclor-1016—— ArQclor-1221---Aroclor-1232—— Aroclor-1242——— Ardclor-1249- — Aroc lor-1254___Aroclor-126Q

.054

. 054

.054

. 054

.054

. 054

.054

. 054

. 110

. 110

. 110

. 110

. 110

. 110

.110

.540

. 110

.540

.5402.200.540.540.540.540.5*01.1001. 100

1IUIUIUIUIUIUIUIUIUIUIU!UIUIUIUtuIU!UIUIUIUIUIUIUIUtuIU1

FORM I PEST 1 -87 Re ,.

94

IDPESTICIDE QRGANICS ANALYSIS DATA SHEET

EPtt SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: Csoi1/water ) WATER

Samp le uit /^o 1 : 800,0 Cg/mL J ML

Leve1: (law/Tned) LOW

^ M o i s t u r e : not dec. dec.

Ex t r*c t i on : (SepF/Con t/Sonc) SEPF

GPC C l e a n u p : IY/NJ N pH:

Con t rac t :

SAS No.: SDG No,:

Lab Sample ID: CA2152

Lab F i l e ID: >HM5e.2

Date Received: \o/n

Date Extracted: 1G -' 12 • d'

Date Ana lyzed: 11 -'I1? 39


CAS NO. COMPOUNDCONCENTRATION UNITS:tug /L or ug -''Kg ; UG -"U

319-64-6--------alpha-BHC_________3.19-65-7-----—— beta-BHC_________? 19-36-8 ——————— delta-BHC________58-89-9---- — ---gamma-BHCCLindane >.76-44-8 — -- —— --Heptachlor_______309-00-2- —————— Aldrin____________1024-57-3-------Heptachlor epoxide.959-98-8--------Endosulfan I______60-57-1 ———————— O i e l d r in__________72-55-9- ——— ——— 4,4'-DDE_________72-20-8--——--—Endrin____________33213-65-9 ————— Endosulfan II____72-54-8 ———————— 4,4(-DDD__________1031-07-8----—-Endoaulfan s u l f a t e5Q-29-3 ———————— 4,4'-DOT_________72-43-5 ———————— nethoxychlor______53494-70-5————Endrin ketone____5103-71-9 —————— alpha-Chlordane___5103-74-2- ————— gamma-Chlordane___8001-35-2 ——— - — Toxaphena________12674-11-2—————Aroc lor-1016_____11104-28-2 ————— Aroc lor-1221______11141-16-5—————Aroc I or-1232____•__53469-21-9 ————— Aroc lor-1242_____12672-29-6—————Aroc lor-1248______11097-69-1 ————— Aroc lor-1254______11096-82-5—————Aroc lor-1260______

.062

.062

. 062

. Ob2

. 062

. 062

.062

. 062

.120

. 120

.120

.120

. 120,120.120,630. 120.062, 0622.500.630.630.630.630.o3Q1.3001.300

0

IUIDIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM I PEST 1--37 Pe-

95

Lab Name: ETCNJ

Lab Code:

2AWATER VOLATILE SURROGATE RECOVERY

Cont rect:

Case No.: SAS No.: SOG No

EPASAMPLE NO.

QC70082UCA1889UCA1890UCA1892UCA1907UCA1908UCA1910UCA2049U

SICTOLJ*

100991001001009999100

52CBFB)*

98989910099999999

.

S3CDCE)#

100100103104102107109107

OTHER TOTOUT

00000000

010203040506070809101112131415161718192021222324252627282930

page 1 of

51 CTOL) - Toluene-d852 CBFB) - Bromofluorobenzene53 CDCE) - l,2-Dichloroethane-d4

QC LtttlTS(88-110)(86-115)(76-114)

Column to be used to flagValues outside QC limitsSurrogates diluted out

recovery values

FORM I I UOA -1 1/87 Rev

96

2AHATER VOLATILE SURROGATE RECOVERY

Lab Nama: ETC Corp. Contract:

Lab Coda: Caaa No.: SAS No.: SDG No

paga 1 of

010203040306070809101112"1415161718192021222324252627282»301

EPASAMPLE NO.

QC70083VCA2141VCA2142VCA2143VCA2149VCA2151VCA1891VCA2145VCA2152VCA2153V

————————————————————————————————————————

————————————————————————————————————————————————————————————

ite=^ ^ R£ I£^ ^ E ^ _

si(TOL)*

991001001001019796969797

32(BPB)f

1021011071021039899105102101

—————

S3(DCE)|

95939599104100978999100

OTHER

—————

TOTOUT

0000000000

—— 1

31 (TOL) - Toluana-d832 (BFB) - Bromofluorobanzana33,<DCE) - 1,2-Dlchloroathana-d4

QC LIMITS(88-110)(86-115)(76-114)

/ Column to ba uaad to flag racovary valuaa* valuaa outaida QC HaltsD Surrogataa dllutad out

FORK II VOA -1 97 1/87 Rav,

2AWATER VOLATILE SURROGATE RECOVERY

Lab Name: ETC Corp. j Laboratory Contract:

Lab Code: Case No.: SAS No.: SDG No

! EPASAMPLE NO.

01JQC70085V02 QC70085V03 CA2150V04 CA2147V05 CA2144V06070809!10!1112131415161718192021222324252627282930 !

SI(TOL)f

104105102104101

———————————————

—————

——————————

—————

S2(BFB)#

98102999291

.—————

.........

———————————————

—————

——————————

—————

—————_____

S3(DCE)|

104113105101114

—————1

'—————

—————

—————

— ... ———

—————

OTHER

... ..

•

—————

—————

TOTOUT

00000

—11

SI (TOL) - Toluene-d832 (BFB) - BromofluorobenzeneS3 (DCE) - l,2-Dichloroethane-d4

QC LIMITS(81-117)(74-121)(70-121)

i Column to be used to flag recovery values* Values outside QC limitsD Surrogates diluted out

page 1 ofFORM II VGA -1

981/87 Rev,

2AHATER VOLATILE SURROGATE RECOVERY

Lab Nane: ETC Corp. | LabuiaLury Contract:

Lab Code: Case No.: SAS No.: SOG No.

010203040506070809101112131415161718192021222324252627282930

EPASAMPLE NO.

QC70088VCA2146V

———————————

SI(TOL)|

9898

— — ___

S2(BPB)f

9894

—— . —— —

S3(PCH)*

102101

-

•*rt£ivi

page 1 of

51 (TOL) - Toluene-d852 (BFB) - BroBOfluorobcnzena53 (DCE) - 1,2*Dichloro«than*-d4

QC LIMITS(88-110)(86-115)(76-

I Column to b« u««d to flag recovery values* Value* outside QC limitsD Surrogates diluted out

FORM II VOA -199

1/87 Rev.

2AUATER UOLATILE SURROGATE RECOVERY

Lab Name: ETC Corp. I Laboratory Contract:

Lab Code: Case No.: SAS No.: SDG No

1 ERA1 SAMPLE NO.

01IQC7Q090U02ICA2282003ICA2292US04ICA2282UR05ICA2266Y06ICA2266U071OS)091101lit121131141151161171181191201211221231241251261271281291301

SI(TOD*

999999999799

S2(BFB)*

9799999910094

S3(DCE)*

10110710410910698

OTHER TOTOUT

000000

....

51 CTOL) - Toluene-d852 CBFB) - Bromofluorobanzena53 COCE) - l,2-Dichloroethene-d4

QC LIMITS(88-110)(86-115)(76-114)

* Column to ba used to flag* Ualues outside QC l i m i t sD Surrogates d i l u t e d out

recovery values 100

page 1 of

Lab Name: ETCNJ

Lab Code:

WATER SEMI <JOLATILE SURROGATE RECOVERY

Contract:

Case No.: SAS No.: SDG No

1 ERA1 SAHPLE NO.|. ...........1QC70087CICA1907CRICA2139C1CA19Q7CSICA1907C:CA2140C1!

11

1i

1!

11 —————— * —————————11

1i!11

1IIr:

SICNB2)*

849082837976

S2(FBP)*

823883757070

S3(TPH)#

13312678125129104

S4( PHL ) #

66604 *717560

35(2FP>#

74631 »

757561

S6(TBP)#

61630 *787659

u: HER TO 1

OUT

' 003000

..

010203040506070809101112131415161718192021

23241

2627282930

p a g o 1 of

51 (NBZ)52 CFBP)53 CTPH)54 (PHL)35 (2FP)36 CTBP)

Nit pobenzene-d52-FluorobiphenylTarphenyl-d!4Phenol-d52-Fluoropheno12,4,6-Tribromophenol

QC LI PI ITS(35-114)(43-116)(33-141)(10- 94)(21-100'(10-123)

Column'Ja lues

to be usedoutside QC

to flagl i m i t s

recovery values

Surrogates diluted out

FORM II SU -1 1/87

101

Lab Name: ETCNJ

Lab Code:

2CUATER SEMIUQLATILE SURROGATE RECOVERY

Contract:

Casa No.: SAS No.: SDG No

1 ERAt SAMPLE NO.

01IQC87921C02ICA2139C03ICA2273C04ICA2273CS05ICA2273CR061071081091101111121131141151 >161171181191201211221231241251261271281291301

SI(NBZ)*

7674767681

S2C FBP ) *

7975727975

S3(TPH)#

114109113105110

54C PHL ) *

390 •343636

35C2FP)*

561 •474549

•

S6CT8P)#

7720646675

OTHER TOTOUT

02000

-* 1

page 1 of

51 (NBZ) - Nitrobenzene-d552 (FBP) • 2-Fluorobiphenyl53 CTPH) - Tarphanyl-dl454 (PHL) - Phanol-d555 C2FP) - 2-Fluorophenol56 CTBP) " 2,4,6-Tribromophenol

QC LIMITS(35-114)(43-116)(33-141)(10- 94)(21-100)(10-123)

* Column to be used to flag* Ualuea outside QC limitsD Surrogates diluted out

recovery values

102

FORM II SU -1 1/87 Rev

Lab Name: ETCNJ

Lab Coda:

2CWATER SEMIUOLATILE SURROGATE RECOVERY

Cont ract:

Case No.: SAS No.: SOG No

1 EPA1 SAMPLE NO.

01 IQC87921C02ICA2147C03 104105 f06107108109110111112113114115116117118 I19120121!221231241251261271281291301

SICNBZ)*

7676

S2(F8P)#

7974

S3(TPH)#

114112

S4(PHD*

391 »

S5C2FPJ*

562 •

S6(T8P)#

7712

OTHER TOTOUT

02

page 1 of

51 CNBZ) • Nitrobenzene-d552 (FBP) - 2-Fluorobiphenyl53 CTPH) - Terphenyl-dl454 (PHD - Phenol-d535 (2FP) - 2-FIuorophenolS6 (TBP) • 2,4,6-Tribromophenol

QC LIMITS(35-114)(43-116)(33-141)(10- 94)(21-100)(10-123)

t Column to be used to flag* Oalues outside QC l i m i t sD Surrogates diluted out

recovery values

103

FORM II SU -1 1/87 Rev.

2CWATER SEhIVOLATILE SURROGATE RECOVERY

Contract:

SAS No.i SOS No

1 EPA1 SAMPLE NO.

01IQC87921C02ICA2145C03ICA2146C04ICA2273C05ICA2273CS06ICA2273CR071oat0911011111211311411511611711BI191201211221231241251261271281291•501 -iUrti

SI(N8Z>*

767881767681

1 Taa» -r-Ks^atv,

52(FBP)*

797676727975

.

R&h

S3CTPH)#

114112105113105110

54(PHD*

390 »0 »343636

S5(2FP)#

560 "0 »474549

56(TBP)#

770 »0 »646675

L.

OTHER TOTOUT

033000

ff-'f

..

robanzana-d5luorobiphanyl

T«rphanyl-dl454 CPHL) - Phanol-d?S9 C2FP) - 2-FluorophanolS6 (TBP) " 2,4,6-Tribromophanol

QC LIMITS(35-114)(43-116)(33-141)(10- 94)(21-100)(10-123)

4 Column to bo u*od to flag* Ualuas outsida QC limitsD Surrogates dilutad out

racovary valuas

paga 1 of

FORM II SU -1

104

1/87 Rav.

Lab Name: ETCNJ

Lab Code:

2CWATER SEMIUOLATILE SURROGATE RECOUERY

Cont ract:


I EPAI SAMPLE NO.

01IQC70091C02 ICA2271CRG3ICA2147C04ICA2148C05 ICA2271C06 ICA2271CS07108109110111112113114115116 117118119 120121122f231241251261271281291301

SICNBZ)#

726779766787

I

S2(FBP)*

736692146 *194 •78

S3CTPH)*

104100122184 »195 »136

S4(PHD*

34367 »

452340

S5(2FP)*

555415 *519352

S6(TBP)*

647343

165 -240 •97

OTHER TOTOUT

002330

page 1 of

51 CNBZ) • Nitrobenzene-d552 (FBP) - 2-Fluorobiphenyl53 (TPH) - Terphenyl-dl454 CPHL) - Phenol-d555 C2FP) - 2-Fluorophenol56 (TBP) - 2,4,6-Tribromophenol

QC LIMITS(35-114)(43-116)(33-141)(10- 94)(21-100)(10-123)

* Column to be used to flag* Ualues outside QC l i m i t sD Surrogates d i luted out

recovery values

FORM II SO -1 „ 1/87105

Rev

Lab Name: ETCNJ

Lab Code:

2C• WATER SEMI VOLATILE SURROGATE RECOVERY

Contract:


ERASAMPLE NO.

QC70092CCA1889CCA1890CCA1892CCA1908CCA2141CCA2142CCA2143CCA2149CCA2151CCA1891CCA2144CCA2145CCA2146CCA2152C

SI(N82)*

716773778870669081717673797677

S2< FBP ) *

656369748964598875707373807877

S3(TPH)#

1181161181131411129997106107112977888114

34(PHL)#

6874716573746662717136552 *4 *76

S5(2FP)#

7069716378777065707641630 »1 »

80

S6CTBP)*

5056575548546655526133700 •0 *

58

OTHER

..

TOTOUT

000000000000330

010203040506070809101112131415161718192021222324252627282930

page 1 of

51 (NBZ) - Nitrobanzana-d552 (FBP) - 2-Fluorobiphenyl53 CTPH) - Tarphenyl-dl454 CPHL) - Phenol-d555 C2FP) - 2-Fluorophenol56 CTBP) • 2,4,6-Tnbromophenol

QC LIMITS(35-114)(43-116)(33-141)(10- 94)(21-100)(10-123)

# Column to ba used to flag* Values outside QC l i m i t sD Surrogates diluted out

recovery va lues

FORM II SU -1 106 1/87 Rev

Lab Name: ETCNJ

Lab Code:

2EWATER PESTICIDE SURROGATE RECOVERY

Cont rac t:

Case No.: SAS No,: SDG No

1 EPA1 SAMPLE NO.

01IQC70Q30G02ICA1907G03ICA1907GS04ICA1907GR05ICA2139G06ICA2140G07108109110111112113114'l1511611711811912012112212312412512612712ft 1

3QI

SI( DBC ) *

956187777063

OTHER

. •

TOTOUT

000000

51 CD8C) • Dibutylchlorendate

ADVISORYQC LIMITS(24-154)

* Column to be used to flag* U«lu«» out»id« QC limitsD Surrogatas diluted out

r«cov«ry values

pag« 1 of

FORM II PEST-1 1/87 Rev

107

Lab Name: ETCNJ

Lab Code:

2EIJATER PESTICIDE SURROGATE RECOUERY

Cont rac t :


1 EPA1 SAMPLE NO.

Q1IQC7Q049G02ICA2271GS03ICA2271GR04ICA2147G05ICA2148G06107108109 1101111121131141151161171181191201211221231241251261271281291301

SIC DBC 5 *

210 *0 »

1450 *0 »

OTHER TOTOUT

11011

SI (DBC) - Dibutylchlorendate

ADVISORYQC LIMITS(24-154)

#-Column to be used to flag* Ualues outside QC limitsD Surrogates diluted out

recovery values

page 1 of

FORM II PEST-1 1x87 Rev,

108

Lab Name: ETCNJ

Lab Code:

2EWATER PESTICIDE SURROGATE RECOUERY

Cont rac t :

Caae No . : SAS No . : SDG No

1 ERA1 SAMPLE NO.

01 IQC70Q50GQ2ICA1889G03 1CA189QG04ICA1892G05 ICA1908G06ICA2141G071CA2142G08ICA2143G09 ICA2149G1QICA2151G11 ICA1891G12ICA2144G13ICA2145G14ICA2146G15ICA2152G16 117118119120121122123124125126127129 1291301

SIC DBC ) *

253 *258 *295 *253 *3190

284 *104413 «1001129314987

354 »

OTHER TOTOUT

11110010100Q001

51 <DBC) • Dibuty lchlorendate

rtOUISQRYQC LIMITS

12^-154)

page 1 of

4 Column to be used to flag recovery values* Ualues outside QC 1 i m i t sD Surrogates diluted out

FORM II PEST-1

109

3AWATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Lab Name: ETC Corp. I Laboratory Contract:


Matrix Spike - EPA Sample No.: CA2282US

COMPOUND

1 t 1-Dich loroathanaTr ichloroethena .,BanzanaTo luene , ,Ch lorohenzane

SPIKEADDEDCug/L)

90. 00050.00050,00090.00090.000

SAMPLECONCENTRATION

Cug/L)

0.00084.8911.8170.0000.000

MSCONCENTRATION

Cug/L)

40.093~ 120.641

43.10443.12147.634

MS 1 QC% ILIMITSREC *l REC.

80 161-14971 171-12083 176-12786 176-12999 179-130

1

COMPOUND

1 ,1-DichlopoethenaTr ich laroethena „Benzene ,To luaneCh lorobenzene

SPIKEADDEDCug/L)

50.00090.00090.00090.00050.000

MSDCONCENTRATION

Cug/L)

39.660117.48341.48441.61849.894

.MSDS

REC *

7969 *798392

* -RPD *

19444

\ QC LIMITSRPD 1 REC.

14 161-14914 171-12011' 176-12713 176-12513 179-130

1

# Column to be used to flag recovery and RPD values with an asterisk

* Ualues outside of 1'imits

3PD: Q out of 9 outside limitsSpike Recovery: 1 out of 10 outside limits

Comments:

FORM III VGA -1 1/87 Rev.

3CWATER SEMI VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Lab Name: ETCNJ . Contract:

Lab Code: ,i| Case No.: SAS No.: SOG No.:

Matrix Spike - EPA Sample No.: CA1907C#

COMPOUND

Phenol2-Ch loropheno 1I , 4-Dich lorobenzene ____N-Nitroso-di-n-prop. ( 1 )_1,2, 4-Tr ich lorobenzene _4-Ch loro-3-methylpheno 1_Acenapnthene4-Ni t ropheno 12,4-DinitrotoluenePentach loropheno 1P-jrene

- ——— ~_ ———— * ——————— . —————

SPIKEADDED(ug/L)

208.333208.333104.167104. 167104. 167208.333104.167208.333104. 167208.333104. 167

SAMPLECONCENTRATION

Cug/L)

0. 0000.0000. QOO0.000Q. 0000.0000. QOO0.0000.0000.0000. 000

MS 1 ^!SCONCENTRATION! S

(ug/L) *EC

142.452 68161.713 7879.315 7687.080 1 8479.^50 1 77164.261 7987.149 84100.578 4874.841 72157.179 7581.310 78

1

i QC '(LIMITS!

*i REC.

i 12- 3'- '127-123 1136- 9141-1161! 39- 9:-: :123- 971146-113 :110- 80 1124- 96:1 9-1031

-126-12"-'!-1, 1

COMPOUND

Phenol2-Ch 1 oropheno 11 ,4- D ich 1 orobenzeneN-Nitroso-di-n-prop. C 1 )_I ,2 ,4-Tr ich lorobenzene _4-Ch loro-3-methylphenol_Acenapht hene4-N i t ropheno 12 ,4-Din i t rotolu*n*Pent ach lorophanhl. _..Pvrene

SPIKEADDED(ug/L)

208.333208.333104.167104.167104.167208.333104.167208.333104.167208.333104.167

MSDCONCENTRATION

Cug/L)

134.212138.87481.13871.57084.395132.13189.25397.37567.66984.37682.941.

MSD t\ t SREC #1 RPD #

64 1 667 t 1578 1 269 1 2081 1 663 1 2286 1 247 1 365 1 1041 1 60 »80 1 2

QC LRPD

4240283828423150385031

1MITS '•RtC. 1

12- 8V I27-12 '36- 97141-116 ;39- 98!23- 9 "46-118 110- y: :24- 96 !9 - 1 0 '< :

26-1271'

C1) N-Nitroso-di-n-propylamine

# Column to be used to flag recovery and RPD values with an asterisk

* Ualues outside of limits

RPD: 1 out of 11 outside l i m i t sSp:ke Recovery: 0 out of 22 outside limits

Comment s:

FORM III SU -1

LJATER SEMIUOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOUERY



Matrix Spike - ERA Sample No.: CA2271CS

COMPOUND

Pheno 12-Ch loropheno 11 ,4-Dich lorobenzene ____N-Nitroso-di-n-prop. ( 1 )_1,2,4-Trich lorobenzene _4-Chloro-3-methylpheno 1_Acenaphthene4-Ni t ropheno 12 ,4-Dini-trotoluenePentach loropheno 1Purene

SPIKEADDED(ug/L)

200. 000200.000100.000100. 000100.000200.000100.000200.000100.000200.000100.000

SAMPLECONCENTRATION

(ug/L)

0. 0000. 000O.OQO0. 000O.OQO .0. 0000. 0000.0000.0000.0000. 000

MSCONCENTRATION

(ug/L)

75.569161.64769.82387.66974.115154.80081.15168.03595.149151.75177.681

MSX

REC ft

3881708874778134957678

QCLIMITSREC.

12- 8927-12336- 9741-11639- 9323- 9746-11810- 9024- 969-10326-127

COMPOUND

Pheno 12-Ch loropheno 11 , 4-0 i ch 1 orobenzene ____N-Nitroso-di-n-prop. ( 1 )_1 ,2 ,4-Tr ich lorobenzene __4-Ch loro-3-methy Ipheno 1_Acenaph t hene4-Ni t ropheno 12 f4-Dinitroto luenePen taeh lorophenol ,,Pvrene

SPIKEADDED(ug/L)

200.000200.000100.000100.000100.000200.000100. 000200.000100.000200.000100.000

MSDCONCENTRATION

(ug/L)

73.911158.42763.21272,41062.627154.85370.33754. 05964. 110116. 14673.125

USD i• \ t \REC ft RPD *

37 1 279 1 263 1 1072 1 1963 t 1777 1 070 1 1427 1 2364 I 3958 1 2773 1 6

QC LRPD

4240283828423150385031

iMITS :REC. i

12- 8*'27-12 ' '36- «'.41-11-39- JH23- •>46- lltt10- >•2**- **>9- ii. '

26-12-1

(1) N-Nitroso-di-n-propyl«mine

If Column to be used to flag recovery and RPD values with an asterisk

* Ualues outside of l i m i t s

RPD: 0 out of 11 outside l i m i t sSpike Recovery: Q out of 22 outside l i m i t s 1 12Comments:

FORM III Sv1 -1 1/87 Rev.

3EWATER PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOUERY

Lab Name: ETCNJ Contract:


Matrix Spike - EPA Sample No.: CA1907GS

COMPOUND

qamma-BHCCL indane )Heptachlor ._ „ „Aldr inDieldrinEndr in4. 4 '-DOT

SPIKEADDEDCug/L)

.213

.213

.213

.532

.532

.532

SAMPLECONCENTRATION

<ug/L)

O.OOQ0.0000.0000.0000.0000.000

MSCONCENTRATION

Cug/L)

.187

.173

.192

.487

.369

.520

MS t QC 1% ILIMITSI

REC *l REC. 1

88 154-123181 140-131190 140-120192 J52-126169 156-121198 138-1271

1 1

COMPOUND

qamma-BHC(L indane )Heptach lorAldrinDialdrinEndr in4. 4 '-DOT

SPIKEADDEDCug/L)

.213

.213

.213

.532

.532

.532

MSDCONCENTRATION

(ug/L)

.183

.169

.191,447.376.489

MSD\

REC *

867990847192

HRPD *

221926

QC LIMITSRPD 1 REC.

15 156-12320 140-13122 140-12018 152-12621 156-12127 138-127

1

# Column to be useel to flag recovery and RPD values with an asterisk

* Ualues outside of l i m i t s

RPD: 0 out of 6 outside l i m i t sSpike Recovery: 0 out of 12 outside limits

Comments•

FORM III PEST-1 1/87 Rev.

1 1 3

3EWATER PESTICIDE MATRIX SPIKE-"MATRIX SPIKE DUPLICATE RECOVERY



Matrix Spike - EPA Sample No.: CA2271GS

COMPOUND

qamma-BHC (Lindane )Heptach lorAtdr inDieldr inEndr i n4.4--DDT

SPIKEADDED(ug/L)

.200

.200

.200

.500

.500

.500

SAMPLE 1 MSCONCENTRAT I ON 1 CONCENTRAT I ON

(ug/L) 1 lug/L)............. |..... ........

O.OOQ ! .3420.000 1 .27B0.000 1 .3050.000 1 .9700.000 1 .8960.000 I 1.098

1

MSH

REC #

171 »139 •152 *194 »179 »220 »

QCLIMITSREC.

56-12340-13140-12052-12656*12138-127

COMPOUND

qamma-BHCCL indane )Hept ach lorAldnnD i e Idr inEndr in4.4'-DDT

SPIKEADDED(ug/L)

.200

.200

.200

.500

.500

.500

MSDCONCENTRATION

Cug/L)

.266

.240

.251

.758

.730

.837

MSD\

REC #

133 -120125 *152 «146 *167 »

SRPD *

25 •152025 *2027

QC LRPD

152022182127

[HITSREC.

56-12340-13140-12052-12656-12138-127

1

tt Column to be used to flag recovery and RPD values with an asterisk

* Ualues outside *f limits.•*"•

RPD: 2 out of £ outside l i m i t sSpike Recovery: 11 out of 12 outside lim i t s

Comments:

FORM III PEST-1 1/87 Rev.

114

4AUOLATILE METHOD BLANK SUMMARY

Lab Name: ETCNJ

Lab Code: Case No.:

Lab File ID: >C7407

Date Analyzed 10/16/89


Instrument ID: GC/MS C

THIS METHOD BLANK APPLIES TQ THE FOLLOWING SAMPLES, MS AND MSD:

Cont rac t:

SAS No.: SDG No.:

Lab Sample ID: QC70082U

Time Analyzed: 1141

1:(lou/med) LOW

Common t s:

page 1 of

01020304050607oe09101112131415161718192021222324252627282930

EPASAMPLE NO.

LABSAMPLE ID

CA1889UCA1890UCA1892UCA1907YCA1908UCA1910YCA2049U

LABFILE ID

>C7409>C741Q>C7411>C7412>C7413>C7414>C7415

TIMEANALYZED

1458155416491745184119372032

FORM IU UOA 1/87 Rev

115

4AVOLATILE METHOD BLANK SUMMARY

Lab Name: ETC Corp.

Lab Code: Case No.:

Lab File ID: >C7502




THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:

Contract:

SAS No.: SDG No.;

Lab Sample ID: QC70088V

Time

LevelJ(

Comments :

page l of

010203040506070809101112131415161718192021222324252627282930

_L-

EPASAMPLE NO.

— —— — . —— _—

——————————————————————

——————————————————————————————————————————————————————————————————

———————————

————————————————————————————————————————————

———————————

- _ - — — —— - —— — .

-_._ -.. —— - —— .

LABSAMPLE ID

CA2146VCA2146V

—————————————

——————————————————————————

FORM IV

LABFILE ID

>C7503>C7505

—————————————

——————————————————————————

VOA

! TIMEANALYZED

12071430

—————————_ ...

——————————————————

———————————————————————————-—————————

—————————

-

• -~ j;

:-tlj|-"**?H

1/87 Rev

116


Lab Name: ETC Corp.

Lab Code: Case No.:

Lab File ID: >C752Q


Matrix: (soiI/water) WATER



Cont rac t:

SAS No.: SDG No.:

Lab Sample ID: QC70Q90U

Time Analyzed: 1750

Leve1:C1ow/med) LOW

1 EPA1 SAMPLE NO.

Oil021031041051061071031091101111121131141151161171191191201211221231241251261271281291301

LABSAMPLE ID

CA2282UCA2282USCA2266U

LABFILE ID

>C7524>C7525>C7528

TIMEANALYZED

213222270114

Comment s'

.age 1 ofFORM IU UOA 1/87 Rev

1 1 7

\

Lab Naa«:

Lab Cod*:

4AVOLATILE KETHOD BLANK SUMMARY

ETC Corp. . Contract:

SAS No.:Cast No.:

Lab Fila ID: _

Dat« Analyzed:

Matrix: (soil/water)

Instruacnt ID:

/£>/*}{*<?

SDG Ho

ID: _

Analyzed:

:(low/»«d)

c

THIS METHOD BI^HC APPLIES TO THE fOIM«lW SAMPLES. MS AND MSD

COMMENTS:

pag« J_ of 4.


Lab Name: ETC Corp.

Lab Coda:

Lab File ID: >D8036

Date Analyzed

Case No.Contract:

SAS No.: SDG No.:


Time Analyzed: 1444

Level:(low/med) LOW

10/17/89


Instrument ID: GC/MS D


Comments:

page 1 of

010203040506070809101112131415161718192021222324252627282930

EPASAMPLE NO.

*

•aftfe.-Ammmifeift-"" mmrnEL-" mmm 1mm

—— = ——————

LABSAMPLE ID

CA2141VCA2142VCA2143VCA2149VCA2151VCA1891VCA2145VCA2152VCA2153V————————————

" ————— .

LABFILE ID

>D8038>D8039>D8040>D8041>D8042>D8043>D8044>D8045>D8046

—— . ——————————

TIME |ANALYZED

163517271816190719582048213922302320

—————————

FORM IV VOA 1/87 Rev,

1 19


Lab Name: ETC Corp.

Lab Code: Case No.:

Lab File ID: >I8246



Instrument ID: GC/MS I


Contract:

SAS No.: SDG No.:


Time Analyzed: 2331

Level:(low/med) LOW

010203040506070809101112131415161718192021222324252627282930

EFASAMPLE NO.

———————————

——————————————————————

———————————

———————————

———————————

———————————

LABSAMPLE ID

CA2150VCA2147VCA2144V

———————————————————————————————————————

—————————————

—————————————

—————————————

LABFILE ID

>I8248>I8250>I8252

—————————————

——————————————————————————

—————————————

————————————————————————————————————————————————————

—————————————

— _, ————— _ ————

TIMEANALYZED

011002500429

—————————

_,

—————————

i

Comments:

page 1 ofFORM IV VOA 1/87 Rev

120

4BSEMI VOLATILE METHOD BLANK SUMMARY

Lab Name: ETCNJ . '

Lab Code: £V-r Case No.

Lab File ID: >G*B41




Cont ract :

SAS No.: SDG No.:

Lab Sample ID: QC7008:':,

Ext ract ion:(SepFxCont/Sonc) CONT

Time Analyzed: 2140

Level : ( low/med ) LOUl'

Instrument ID: GC/MS G


1 EPA1 SAMPLE NO.

O i l02 1031041051D6IQFI08109 110111112113114!15116117118119 120 1211221231241251 r261 *:-271281291301

LABSAMPLE ID

CA1907CRCA2139CCA1907CSCA1907CCA2140C

LABFILE ID

>G9043>G9Q45>G9077>G9078>G9079

DATE 1ANALYZED :

11/14/89 111/15/89 111/16/89 l11/16/89 111/16/89 1

11t!1!

111•

1I111111111I

111

Comments

page 1 of .1_FORM W SU 1/87 Rev

121

4BSEMIUOLATILE METHOD BLANK SUMMARY

Lab Name: ETCNJ

Lab Code: Case No.

Lab File ID: >G9Q51



Matrix: Caoi1/water) WATER

Cont ract :

SAS No.: SDG No.:

Lab Sample ID: QC70092C

Extract ion: CSepF/Cont/Sonc) CONT

Time Analyzed: 0618

Level:tlow/med) LOU



Comments:

010203040506070809101112131415161718192021222324252627282930

EPASAMPLE NO.

LABSAMPLE ID

CA1889CCA1890CCA1892CCA1908CCA2141CCA2142CCA2143CCA2149CCA2151CCA1891CCA2144CCA2145CCA2146CCA2152C

LABFILE ID

>G9052>G9053>G9054>G9055>G9056>G9Q57>G9Q58>G9059>G9060>G9061>G9Q64>G9065>G9066>G9067

DATEANALYZED

11/15/8911/15/8911/15/8911/15/8911/15/8911/15/8911/15/8911/15/8911/15/8911/15/8911/15/8911/15/8911/15/8911/15/89

page 1 of __iFORM IU SU 1/87

122

46SEMIUOLATILE METHOD BLANK SUMMARY

Lab Name: ETCNJ

Lab Code: Caae No.

Lab File ID: >G9068




Cont rac t:

SAS No.: SDG No.:

Lab Sample ID: QC70Q91C

Extract ion: (SepF/Cont/Sonc) SERF

Time Analyzed: 2140

Leve1:Clow/mod) LOW



Commen ta

010203040506070809101112131415161718192021222324252627282930

EPASAMPLE NO.

-

LABSAMPLE ID

CA2271CRCA2147CCA2148CCA2271CCA2271CS

LABFILE ID

>G907Q>G9071>G9072>G9073>G9087

DATEANALYZED

11/15x8911/16/8911/16/8911/16/8911/17/89

page 1 of jFORM SO 1/87 Rev;

123

4CPESTICIDE METHOD BLANK SUMMARY

Lab Name: ETCNJ

Lab Code: Case No.

Lab Sample ID: QC70Q50G

M a t r i x : (soil/water) UlnTER

Date E x t r a c t e d : 10/12/99

Date Ana lyzed (1) '• 11/1?-'89

Time Analyzed CD: 1135

Instrument ID (1): HA

GC Column ID (lj: 2250/2401

SDG No . :

Cont rac t :

No . :

Lab F i l e ID:

Leve 1 : C low/med 1 LOU

Ext pact ion : CSepF''Con t <-'Sonc ) SERF

Date Analyzed (2): 11.-23-81'

Time Ana lyzed '.2 ) : 0942

Instrument ID ' 2 ) : KB

GC Column ID (2): 3V3P21QO

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND USD:

0102030405060708091011121314151617181920212223242526

EPASAMPLE NO.

LABSAMPLE ID

CA1889GCA1890GCA1892GCA1908GCA2141GCA2142GCA2143GCA2149GCA2151GCA1891GCA2144GCA2145GCA2146GCA2152G

OATEANALYZED 1

11/15/8911/15/8911/15/8911/15/8911/15/8911/15/8911/15/8911---15/8911/15/8911/15/8911/15/8911/15/8911/15/8911/15/89

DATEANALYZED 2

11^28/89

Comment s:

page 1 ofFORM IU PEST

124


Lab Name: ETCNJ

Lab Code: Case No

Lab Sample ID: QC70030G



Date Analyzed CD: 11/08/89

Time Analyzed (1): 0947

Instrument ID (1): JA

GC Column ID CD: 2250/2401

0252

KB

3SSP2100

THIS METHOD BLANK APPLIES TO THE FOLLOUING SAMPLES, MS AND MSD:

Cont ract:

SAS No.: SDG No.:

Lab File ID: >Jtt49S

Level:Clow/med) LQU

Extract ion:(SepF/Cont/Sonc) SERF

Dete Analyzed (2)

Time Analyzed (2)

Instrument ID (2)

GC Column ID (2)

1 EPA1 SAMPLE NO.

Oil021031041051061071081091101111121131141 -.151161171 *if191191201211221231241 "251261

LABSAMPLE ID

CA1907GCA1907GSCA1907GRCA2139GCA214QG

DATEANALYZED 1

11/09/8911/08/8911/08/8911/08/8911/08/89

DATEANALYZED 2

11/21/89

11/21/89

Comment s:

page 1 ofFORM IU PEST

1251/87 Rev


Lab Name: ETCNJ

Lab Code: Case No

Lab Sample ID: QC70049G

M a t r i x : CsoiI/water) WATER


Date Analyzed CD: 11/16/89

Time Analyzed (1): 1955

Inst rument ID (1): KB

GC Column ID CD: 3SSP-2100

Con t r a c t :

SAS No.: SDG No.:

Lab F i l e ID: iKDO'PQ-

Leve1:Clow/med) LOW

Extract ion:(SepF/Cont/Sonc) SEPF

Date Analyzed C 2 > :

T ime Analyzed C 2):

Instrument ID (2 ) :

GC Column ID (2):


0102030405060708091011121314151617181920212223242526

EPASAMPLE NO.

LABSAMPLE ID

CA2271GSCA2271GRCA2147GCA2148GCA2271G

DATEANALYZED 1

11/16/8911/16/8911/16/8911/16/8911/16/89

DATEANALYZED 2

Common t

page 1 ofFORM IU PEST /87 Rev

• 1AUOLnTILE ORGAN ICS ANALYSIS DATA SHEET

MFl_E. N G

Lab Name: ETCNJ

Lab Code: Case No.:

Hat P ix: (soi1/water) WATER

Sample wt/wol: 5.0 <g/mLJ ML

Leve1: (low/mad) LOW

H Mo is t Lire : not dec .


Con t rac t :

SAS No.: SOG No.:


Lab File ID: >C7407

Date Rece wed: ID/'07/8 9


Dilution Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:tug/L or ug/Kg) UG/L

74-87-3 ------74-83-9 -----75-01-4 —————75-00-3 —————75-09-2 -----67-64-1 ------75-15-0-- ———75-35-4 ------75-34-3 —————540-59-0 — ---67-66-3 ----- -107-06-2 ————78-93-3- —— --71-55-6 ------56-23-5 ——— --1Q8-05-4 -----75-27-4 ------78-87-5 ----- -10061-01-5 ——79-01-6 ------1 94-.4A- 1 - -- -

79-QO-5 —————71-43-2 ------10061-02-6 ——75-25-2 —— ——108-10-1 ————591-78-6 ————127-18-4 ————79-34-5 ------108-88-3 — — -108-90-7 -----100-41-4 -----10Q-42-5 -----1330-20-7 ———

---Ch lorome thane---Bro mo me thane---Uinvl Chlor ide---Ch loroe thane---Methvlene Chloride---Acetone---Carbon Disulfide---1 ,1-Dichloroethene---1 .1-Dichloroethane— -1,2-Dichlorethene (total ) __---Ch lorof orm- — Ir2-Dichloroethane---2-Butanone---1 .1 .1-Tr ich loroethane---Carbon Tetrachloride---Uinyl Acetate---Bro mod ich lorome thane---l;2-Dichloropropane---cis-l,3-Dich loropropene ____---Trichloroethene ,__ _---Dibro mo ch lorome thane---lrl .2-Tnchloroe thane---Benzene ,---trans-l,3-Dich loropropene __---Bromof orm—— 4-Methyl-2-Pentanone---2-Hexanone- — Tet raeh loroethene ,—— 1,1, 2, 2-Tetrach loroethane---To luene---Chlorobenzene---Ethylbenzene---Styrene- — Xylen* ( total )

1010101041055555510551055

5

555510105555555

1IUIUIUIUIJIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

FORM I UQA 1''87

127

1AVQUHU OMMTZCi AlULfSXI MX*

UA SAJ9U MO.

toi Qcnoo

109-99-9 Tetranydrofuran ,

128

IEUQLATI'LE ORGANics ANALYSIS DATA SHEET


ERA SAMPLE NO.

Lab Name:ETCNJ

LaD Code : Case No. :

Mat r ix : '.so i 1 /water JUATEP

Samp lo wt -'vol : 5.0 (g/mL)ML


H M o i s t u r e : not dec._____

Co lumn: (pack/cap )

Number TICs found:

Con tract:

SAS No.: SDG No.:

Lab Samp le ID: QC7QOa2U

Lab File ID: >C7407

Date Received: 10'-'07/39

Date Ana ly zed: 10/16''89

Di l u t i o n Factor: L

CONCENTRATION UNITS:Cug^L or ug/Kg)UG/L

CAS NUMBER

01.02.

COMPOUND NAME


RT

1.631.32

EST. CQNC

9923

Q

aa

FORM I OOA-TIC 1/87 Rev,

129

1AVOLATILE ORGANICS ANALYSIS DATA 3HECT

ERA SAMPLE NQ,

Lab Name: ETC Corp.

Lab Code: Case No.:


Sample u»t/vol : 5.0 Cg/mL) ML

Level: (low/med) LQU



Cont ract

SAS No. : SDG No.:

Lab Sample ID: QC70Q9301

Lab File ID: >D8036XT-

Data Received: 10/WT/89


Dilut ion Factor: 1


74-87-3 ——— ———— Chlorome thane______________11074-83-9———————Bromoma thane_____________11075-01-4————————"Jinyl Chloride_____________11075-00-3————————Chloroe thane_______________11075-Q9-2——————— Me thy lane Chloride_j______1867-64-1 ———————— Acetona___________________1975-15-0————————Carbon Diaulf ida___________1575-35-4———————1,1-0 i chloroe thane________1575-34-3————————1,1-0ichloroethane_________15540-59-0——————1,2-0 ich lore thena (total)__1567-66-3————————Chloroform________________15107-06-2———————1,2-Dichloroe thane_________1578-93-3 ———————— 2-Butanona________________11071-55-6————————1,1,1-Tr ich loroethane______1556-23-5———————Carbon Tet rach lor ide______15108-05-4———————Uinyl Acetate______________I 1075-27-4——------Bromodichlorama thane_______1578-87-5 ——————— 1,2-Dichloropropane_______1510061-01-5—————cis-l,3-Dichloropropene____1579-01-6-'-'————Tr ich la roe thane___________15124-48-1———————Oibromoch lore me thane_______1579-00-5———————1,1,2-Trichloroethane______1571-43-2———-———Banxane_________________1510061-02-eV—-——tran»-l,3-Dichloropropena__1575-25-2--——-—-Bromoform________________15108-10-1——-———4-nathyl-2-Pantanone_______I 10591-78-6——————2-Haxanona_______________110127-18-4———————Tatrachloroethene__________1579-34-5r——————— 1,1,2,2-Tetrachloroethane__15108-88-3*——————Toluana_________________15108-90-7——————Chlorobenzene____________15100-41-4——————Ethylbenzene_____________15100-42-5———————Styrane___________________151330-20-7——————Xylena (total)____________15

IIUtutuIUIIJIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM I UQA 1 30l/87 Rev.

vouffttt

131



ERA SAMPLE NO.

Lab Name:ETC Corp.

Lab Code: Case No.:

M a t r i x : Cso i1 /ua ter ) UIATER

Sample wt/v/ol: 5.0 Cg/mDML

Level: (lou/med) LOU

\ Mo iature: not dec.^___^_

Column: (pack/cap)

Number TICs found:

Cont ract:

SAS No.: SDG No.:


Lab Fi1ft ID: >D8036

Date Received: 10/Vtf/89


Dilution Factor: t

CONCENTRATION UNITS:

CAS NUMBER

-*

COMPOUND NAME RT EST. CONC Q

FORM I UOA-TIC 1/87 Rev

132

VOLATILE ORGANICS ANALYSIS DATA SHEETEPA SAMPLE NO.

Lab Name: ETC Corp.

Lab Code: Case No.:

Matrix: (soiI/water) WATER





Contract

SAS No. ; SDG No.:


Lab File ID: >I8246/•**

Date Received: 10/ie-/89


Dilution Factor: 1


74-87-3——————Chloromethane___________ 1074-83-9———————Bromomethane_____________ 1075-01-4———————Vinyl Chloride___________ 1075-00-3———————Chloroethane_____________ 1075-09-2———————Methylene Chloride________ 767-64-1———————Acetone_________________ 1075-15-0———————Carbon Disulfide__________ 1075-35-4——————1,1-Dichloroethene_______ 575-34-3——————1,1-Dichloroethane_______ 5540-59-0——————1,2-Dichlorethene (total)__ 567-66-3——————Chloroform_____________ 10107-06-2——————1,2-Dichloroethane________ 578-93-3 ——————— 2-Butanone_______________ 1071-55-6———————1,1,1-Tri Chloroethane_____ 556-23-5———————Carbon Tetrachloride______ 5108-05-4—————Vinyl Acetate____;______ 1075-27-4———————Bromodichl or ome thane______ 578-87-5———————1,2-Dichloropropane_______ 510061-01-5————cis-1,3-Dichloropropene____ 579-01-6——————Trichloroethene_________ 5124-48-1—————Dibromochloromethane_____ 579-00-5———————1,1,2-Trichloroethane_____ 571-43-2——————Benzene_______________ 510061-02-6————trans-l,3-Dichloropropene__ 575-25-2———————Bromoform_______________ 5108-10-1——————4-Methyl-2-Pentanone______ 10591-78-6——————2-Hexanone_______________ 10127-18-4——————Tetrachloroethene________ 579-34-5———————1,1,2,2-Tetrachloroethane__ 5108-88-3——————Toluene_________________ 5108-90-7————•—Chlorobenzene____________ 5100-41-4—————Ethylbenzene___________ 5100-42-5—————Styrene_______________ 51330-20-7—————Xylene (total)__________ 5

i————————————————————————————————————i——

UUU

!U

!uuuuuuuuuruuuuruuuuuu'u|u'uiuu|uu!u

133

fOUTXU

109-99-9 Tat rahydrofuran

row z vo» I/it

134

VOLATILE OUCAWICi ANAU$X5 DATA SHIITTINTATIVIW XDWTXmD COMPOUNDS

Contract:Ub Na»a:

Ub Cod«tUb

Ub ma XDiData Kacaivad:Data Analyxad:

Coluan: (poek/eap)

Nuabar TIC* found: _£

Dilution Factor:

CONCtMTIUTION UNITS:or

fORH X VO*-«C

135

1AVOLATILE ORGANXCS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Name: ETC Corp.

Lab Code: Case No.:


Sample vt/vol: 5.0 (3/»L) ML

Lev*1: (1ow/ned) LOW


Column: (pacX/cap) PACK

Contract:

SAS No.: SDG NO,


Dilution Factor:


74-87-3 —————74-83-9 —————75-01-4 —————75-00-3 —————75-09-2 —————67-64-1 —————75-15-0 —————

75-34-3 —————540-59-0 ————67-66-3 —————107-06-2 ————

71-55-6 —————56-23-5 —————108-05-4 ————75-27-4 —————

10061-01-5 ——

79-00-5 —————71-43-2 —————10061-02-6 ——

108-10-1 ————

127-18-4 ————79-34-5 —————

100-41-4 ————100-42-5 ————1330-20-7 ———

i

—— Ch 1 orome thane—— Bromom* thane——Vinyl Chloride—— Chloroe thane—— Methvlene Chloride-—Acetone—— Carbon Disulfide——1 , 1-Dichloroethene——1 . 1-Di chloroe thane—— l , 2-Dichlorethene (total) __——Chloroform—— 1 , 2-Dichloroethane—— 2 - But anon e—— 1 , 1 , 1-Trichloroethane——Carbon Tetrachloride

V 1 1 Y A JtfefW b V I* V

—— Bromodichloromethane—— 1 . 2-Dichloroprooane- — cis-1 , 3-Dichloropropene ___—— Trichloroethene—— Dibromochl orome thane—— 1 , 1 . 2-Trichloroethane—— Dvnzvnv—— trans-1 , 3-Dichloropropene __—— Broaof on—— 4-Methyl-2-Pentanone—— 2-Hexanone— -Te trachl oroethene—— 1 ,1,2, 2-Tetrachloroethane __——Toluene—— Chlorobenzene- — Ethylbenzene—— Stvrene—— Xvlene f total >——— . —— ...... ————————————

101010105105555551055

°555555551010 •;.__.

5' • • £^?jf^^

55-

UUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU

'

oMMaes Aiutnx* am If* SM9U HO,

€•!<•» < (

109-99-9 T«tr»hydrofurmn

137


Contract:

SAS No.:

EPA SAMPLE NO.

Lab Name:ETC Corp. | LeJaaratery •

Lab code: Case No.:

Matrix: (soil/water)WATER

Sample wt/vol: 5.0 (g/»L)ML


% Moisture: not dec.____

Column: (pack/cap) (7*~,Jt-

Number TICs found: O

SDG No.:

/89 -/


Dilution Factor: /


GAS NUMBER COMPOUND NAME RT EST. CONC

FORM I VOA-TIC

VOLATILE ORGAN ICS ANALYSIS DATA SHEETEPA SAMPLE NO.

Lab Name: ETC Corp.

Lab Code: Case No.:

Hatr ix: (5011/water) WATER

Sample ufvol: 5.0 (g/mL) ML

Level : ( low/med) LOUI

S "oisture: not dec.


Cont ract:

5AS No.: SDG No.:

Lab Sample ID: QC7Q09!11.;

Lab F i l e ID: >C7520

Date Received: /3/22/§


Oi lut ion Fac tor: 1


74-87-3--- —— ---Chlorome thane______________I 1074-83-9--- — —— -Bromome thane_______________1 1075-01-4————————Uinyl Chloride_____________I 1075-00-3 ———————— Chlo roe thane_______________HO75-09-2----- —— -Methyl one Chloride_________1567-64-1 ———————— Acetone___________________I 1075-15-0 ———————— Carbon Disulfide___________1575-35-4————————1.1-Dichloroethane ______1575-34-3--- ——— --1,1-0 ichlo roe thane_________15540-59-0———————1,2-Dichlorethene (total )__1567-66-3 — -- ———— Ch loroform_________________15107-06-2-——————1,2-Dichloroe thane_________1578-93-3---- — ---2-Butanone________________I 1071-55-6 —— ——— --1,1,1-Trichloroe thane______1556-23-5 — — -- —— Carbon Tetrachlor ide_______15108-05-4--- — ---Umyl Acetate______________I 1075-27-4---------Bromodichloromethana ____l578-87-5 —— ———— -1,2-Oichloropropane________!510061-01-5- —— --cis-l,3-Dichloropropene____1579-01-6 ———————— Tr ichloroethene____________15124-48-1 ——————— Dibromoch lor-omethane_______1579-00-5————————1,1,2-Trichloroe thane______1571-43-2 ———————— Benzene___________________1510061-02-6-—----tran»-l,3-Dichloropropene___1575-25-2 ———————— Bromoform_________________15108-10-1———————4-nethyl-2-Pentanone_______I 10591-78-6 ——————— 2-Hex«none_______;_________I 10127-19-4———————Tetrachloroethene__________1579-34-5————————1,1,2,2-Tetrachloroethane__15108-88-3 ——————— Toluene___________________15108-90-7- —— - — -Ch lorobenzene______________15100-41-4——- ——— Ethyl benzene______________15100-42-5 ——————— Styrene___________________151330-20-7——————Xylene t total )____________15__________ ____ ____ I

IIIIUtuIUIJtuIUIUIUIUIUIUIUIUIUIUIUIUIUtuIU!UIUIUIUIUIUiUIUIUIUIUIUIUI

FORM I UOft 1/87 Re

139

u WWU MO.

109-99-9 Tetrahydrofuran,

140

ORGAMICS AMAUSXS DATA SHEWKhTATXVIW IDOrrXFItt COHFOUKOS

% Moisture: not

Coluan:

SOO He.:

Ub Saaple XOtUb File XOtDate Received:Date Analysed:Dilution Factor: /

COMCtmUTlOU UMX(uf/t or «•/«§)Nuaber TIC* foundt

1/17 Rev.

141


EPA SAMPLE NO.

Lab Name: ETC Corp.

Laf:. Code: Case No.:

Matrix: (301 I/water) WATER

Sample wt/wol: 5.0 Cg/mL) ML

Level: Clow/mad) LOW

S Moisture: not dec.


Contract:

SAS No.: SDG No . :

Lab Sample ID: QC7009i"J

Lab Fi le ID: >C7531

Date Received:

Date Analyzed: 10 -'2 3/89

Di lut ion Factor : 1

CAS NO. COMPOUNDCONCENTRATION UNITS:CugXL or ug/Kg) UG/L

FURM I 'JOA

•J

74-87-3 —————74-83-9 -----75-01-4 ——————75-00-3 ------7S-Q9-2 ------67-64-1 —————75-15-0 —————75-35-4 ------75-34-3 ------540-59-0 -----6?-66-3 —————107-06-2 -----79-93-3 —— ——71-55-6 ------56-23-5 — — —108-05-4 -----75-27-4 ------78-87-5 — ———10061-01-5 ——79-01-6 —————124 48-1 ————79-00-5 —————71-43-2 —————10061-02-6 ——75-25-2 —————108-10-1 ————591-78-6 ————127-18-4 ————79-34-5 ------108-88-3 ————108-90-7 ————100-41-4 -----100-42-5 ————1330-20-7 — —

1---Chloro me thane * 1---Bromomethane 1---Uinyl Chloride 1---Chloroe thane 1---Methy lena Chloride 1---Acetone, . 1---CarhonDisulfide 1---1 ,1-Oich loroethene 1---1 .1-Dich loroe thane 1— -1,2-Oichlorethene (total ) __ I—— Chloroform 1---1 .2-0 ich lorne thane 1---2-Butanone I---1.1.1-Trich to roe thane 1---Carbon Te t rach lor ide 1---UinylAcetate., 1---Bromod ich lorome thane 1---1,2-Dich loropropane 1---c is-1 , 3-D ich loropropene ____ 1— -Tr ichloroethene . 1- — Dihrnmoeh lorome thane 1— -1 j 1 r2-Tr ieh lor oath an e 1—— Benzene , 1---tran»- 1,3-0 ich loropropene 1---Bremofnrm ,_ 1——— -i-M«thyl-2-Pant«nona 1_--2-Ma*anane , . ._ t---T»t raeh loroethene 1---1 , 1, 2, 2-Tet rach loroe thane __ 1---Toluene^ m< n 1---Ch lorobanzene ... 1---Ethy Ibenzene , _ 1---Styrene 1——— Xylane f total ) 1

1

1010101051055555510551055555555510105555555

1IU 11UIU 1m ;IJ 1IU tIU 1

• iuIU 1IU :IU 1IU :

IU 1IU :IU 1IUtu iIUIU 1IU :IU 1IUIU 1IU :IU lIUIU IIUIU 1IU :IU 1IU :IU 1IU :1 I

"TO"

VOlJkTIU CMAXICS AmySXS OAT&TWTATXVIW lOWTl'IW CO«PWKO»

Ub

Vt/VOl!

Uvol: (lov/Md)I Moisturoi not doc.Column: (p«ck/cop)

Numbor TIC« found)

/D/Z^/BJ^^^^^m^m~tp—~

Otto Analyiodi /$/l 3/ffi^^~m*^*Dilution Motor: /

COHCXJmUTIOWor u«/Kf)

143

' IBSEMI VOLATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

he t r i x : (soil /w« t • r ) LJATER

Sample wt/vol: 1000. <g/mL> ML

Level: ( low/med> LOW




Contrect:

SAS No.: SOG No.:


Lab File ID: >G9Q41

Date Received: \o



Di lution Factor: 1


108-95-2 ——— -111-44-4 ——— -95-57-8 ———— -541-73-1 ——— -lOafc-46-7 ——— -100-51-6 ——— -95-50-1 ———— -95-48-7 ———— -108-60-1 ——— -106-44-5 ——— -621-64-7 ——— -67-72-1 ———— -98-95-3 ———— -78-59-1 ———— -8Q-75-5 ———— -105-67-9 ——— -65-85-0 ———— -111-91-1 ——— -120-83-2 ——— •120-82-1 ——— -91-20-3————106-47-9" ——— •

59-50-7 ———— -91-57-6 ———— -77-47-4 ———— -88-06-2 ———— •95-95-4 ———— -o 1 c a ^V1-7H-7------88-74-4 ————— •131-11-3 ——— •208-96-8 ——— -606-20-2 ——— •

1- —— Phenol 1•- — bis<2-Chloroethyl )ether ____ 1• —— 2-Chlarophenol 1•---1,3-Oichlorobenzane 1•---1 .4-Oich lorobenzene 1. —— Benzyl alcohol 1. — -1 .2-Dich lorobanzane 1• — -2-Methvl phenol 1•---bis (2-Ch loro i sop ropy 1 )ether_l•---4-Methylphanol 1----N-Ni t roso-d i-n-propy lamine _ 1•---Hexaehloroethane 1----Nitrobenzene , 1---- laophorone a ,_ 1- —— 2-Nitrophanal 1-- — 2 ,4-Di methyl phenol 1----Banzaic acid ._,,,.... 1-»--bi»(2-Ch 1 o roe thoxy) me thane _ 1——— 2,4-Oichlorophanol 1- —— 1,2 r4-Tr ichlorobenzene 1——— Naphthalene. . 1----4-Ch Inroan i 1 ina_, _. 1—— -Hexach lorobutad iene t——— 4-Ch loro-3-methy 1 phenol 1——— ?.rl»thylnaph thai ana 1—— -Hexach lorocyc lopentadiene __ 1———— 2,4,A-Tr lehlnrophanal , ., .1----2j4j.5-Trieh loronhenol 1——— 2-thlnranaphthalane 1----2-Ni t roan i 1 ina .., _ , 1----Dimathylphthalata 1• ---Acenaphthylene, ,._ . 1----2.6-Dinitrotoluane 1

t

101010101010101010101010101010105010101010101010101010501050101010

1IUIUIUIUiu- *IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

FORM I SU -1 1/Q7 Rev,

144

'1CSEMIUQLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO

Lab Nama: ETCHJ

Lab Code: Case No.:

na t P i x: (soil/wa t•r) WATER

Sample wt/vol: 1000. (g/mL) ML

Level: (lou/med) LOU

X M o i * t u r e : n o t d e c , dec.



Cont ract:

SAS No.: SDG No.:


Lab F i l e ID: >G9041

Date Received: /o///'/f^

Dete Extracted: 10/11/89

Dete Analyzed: 11x14/89

Oi lution Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:tug/L or ug/Kg) UG/L

99-09-2 ———— -83-32-9 ———— -51*28-5 ———— -10(fcy02-7 ——— -132-64*9 ——— -121-14-2 ——— -84-66-2 ———— -7005-72-3 —— -86-73-7 ———— -100-01-6 ——— -534-52-1 ——— -86-30-6 ———— -101-55-3 ——— -118-74-1 ——— -87-86-5 ———— -85-01-8 ———— -120-12-7 ——— -84-74-2 ———— -206-44-0 ——— •129-00-0 ——— •85-68-7— —— -91-94-1— —— •56-55-3 ———— -218-01-9 ——— -117-81-7 ——— -117-84-0 ——— -205-99-2 ——— -207-08-9 ——— -50-32-8 ———— •193-39-5 ——— -53-70-3 ———— -191-24-2 ——— -

1

---3-Nit roan i 1 ine---Acenaphthena---2 .4-Din i t rooheno 1- — 4-Ni t rophenol---Dibanzof uran---2 .4-Din i t roto luane—— Diethulphthalata— -4-Ch loropheny 1-pheny let her _•---Fluorena---4-Ni t roan i 1 ine----4,6-Oini t ro-2-methy Ipheno 1 _---N-Ni t rosodipheny lamina ( 1 ) _• ---4-Bromophenyl-phenylether.. _ _•---Hexachlorobenzene•---Pentachloropheno i•---Phenanthrene- — -Anthracene.---Di-n-butv lot-it ha late-- — Fluaranthena _

• —— Sutulbanzulohtha late

——— Chryeane ,,_——— bim(2-Ethylhaxyl )ph thai ate _- — -Di-n-oct vlohtha late— --Banzo(b) f luo ran thane-- — Benin (k ) f luoranthena----a«r»zn (a )pyrena_ _-_-- IndanaC 1 r 2 .3-cd )pwrane.-.-rjihanz (• ,h ) anthracene- — -Benzn Cg rh T i Jperulene

1150110150150110110110110110150ISO1 101101101501101101101101101101201101101101331101101101101101101

1IUIUIU

IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIU1IUIUIUIU IIU lIU 11 1

(11 - Cannot be separated from Diphanylantine

FORM I SU -2 1/87 Rev

145

IFSetlIUOLATILE ORGAN ICS ANALYSIS DATA SHEET


EPA SAMPLE NO.

Lab NameiETCNJ

Lab Code: Caae No.:

Matrix: CsoiI/water>UATER

Sample wt/vol: 1000. Cg/mDML

Lavel: (low/mod) LOU

H Moiature: not dec._____ dec.___


GPC Cleanup: CY/N) N oHi

. INumber TICs found: _

Contract t

SAS No.: SDG No.:


Lab File ID: >G9041

Data Received: /9/ff/f^



Ditut ion Factor: /


CAS NUMBER

01. 141--78-602. >03.04. 2233-00-3

COMPOUND NAME

Acetic acid, ethyl esterACETONE DIMERUNKNOWN1-Propene, 3 ,3 ,3-t r ich loro-

.t

RT

5.156.547.949.14

EST. CONC

2702302613

Q

Ji>JJ

FORM I SU-TIC 1/87

146

SEMIUOLATILEId

ORGAN ICS ANALYSIS DATA SHEETt, r H 3 H H r- i_ c. IN u .

Lab Name: ETCNJ . .

Lab Code:. Case No.:


Samp te wt/vol : 1000. (g/mL> ML

Level: (low/med) LOLJ

H flo i s ture : not dec. dec.

Cont rac t:

SAS No.: SOG No.:


Lab P i l e 10: >G9Q68

Date Received: lQ/te/39


;t ion: (SepF/Cont/Sonc ) SERF Date Ana ly zed

leanup: CY/N) N pH: D i l u t i o n Fact

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg ) UG/L

1Q8-95-2--1 1 i_44_4-_95-57-8 ——541-73-1 —106-46-7--100-51-6--95-50-1- -95-48-7 ——108-60-1--1Q6-44-5--621-64-7--67-72-1---98-95-3 ---78-59-1 ——88-75-5 ——105-67-9--65-85-0 ——111-91-1--190-93 2 - -120-82-1--91-20-3 ———106-47-8 —87-68-3 ——59-50 7---91-57-6 ——77-47-4---88-06-2 ——95-95-4---91-58-7 ——88-74-4 ——131-11-3--208-96-8--

————— Phenol. — _ — bia(2-Chloroethul lather------2-Chloropnenol------ 1 .3-Oich lorobenzene------ 1 . 4- Dich lorobenzene------Benzyl a Icoho 1._____! .2-Dich lorobenzene------2-Methy Ipheno 1------bis(2-Ch loro isopropyl )ether_

------N-Ni t roao-d i-n-propy lamine _------Hexach loroethane.-----Nitrobenzene------ laophorone ,_, ,------2-Nitraphenol------2 ,4-Dimathylphanol_ _ _ _ _ _ Be nzoic acid______bis(2-Ch loroethoxy) me thane _------2 .4-Dich lorooheno 1------1.2 .4-TrichlorobenTane------Naphtha lana_ _ _ _ _ _ 4- Chloroani 1 ina---T--- Hexach lorobutadiene------4-Chloro-3-meth«jlphanol— ----2-Mathy 1 naphtha lana-- — --Hexach lorocyc 1 open tad lene- ————— '2J4T6-Trichlorophannl------2J.4|5-Triehlorophanol------2-Ch Inronaph thai ana______2-Nitroaniline_ .------Dima thy Iphtha late . , .,.„,.....------ Ac en a ph thy lene------9/A-Dini troto luene

101010101010101010101010101010105010101010101010101010501050101010

FORM I SU -1

: 11/15/89

or: l

Q

1IUIUIUIU ''IUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

1/87 Re^

147

• 1CSEMIYOLATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

M a t r i x : (soil/water) WATER

Sample wt/vol: 1000. (g/mL) ML

Leve1: (low/med) LOU

\ Moisture: not dec. dec.



Cont rac t :

SAS No.: SDG No.:

Lab Sample ID: QC7QQ91C

Lab File ID: >G9Q68/J

Date Received: 10/f?/39





Cl) - Cannot be separated from Diphenylamine

FORM I SV -2

Q

99-09-2----83-32-9 ———51-28-5 ———100-02-7 ——132-64-9 ——121-14-2 ——84-66-2 ———7005-72-3--86-73-7 ———100-01-6 ——534-52-1 ——86-30-6 ———101-55-3 ——118-74-1 ——87-86-5 ———85-01-8 ———120-12-7 ——84-74-2 ———2Q6-44-0 ——129-00-0 ——85-68-7 ———91-94-1 ———56-55-3 ———218-01-9 ——117-81-7—-117-84-0 ——205-99-2---207-08-9 ——50-32-8 —— -193-39-5---53-70-3 —— -191-24-2 ——

-----3-Nitroani 1 ine----- Ac enaph thane-----2,4-Dinit ropheno 1-----4-Nitropheno 1-----Dibenzofuran-----2 P4-Dinitrotoluene-----Diethulphthalate_____4_Ch lorophenyl-phenyle ther _-----Fluorene_____4-Nitroani 1 ine_____4 >6-Din itro-2-methylpheno 1 _-----N-Nitrosodiphenylamine ( 1 ) '-----4-Bromopheny 1-pheny let her __-----Hexach lorobenzene-----Pentachlorophenol-----Phenan throne-----Anthracene_____Di_n-butulphthalata_____Fluoranthene-----Pyrene-.--.-HutvlbBnz-ulohthalate------3.3'-Dich lorobenz id ine.--__ Senzo (a )anthracene-----Chr yaane——— -bis(2-Ethylhexyl )phthalate _-----Oi-n-oetulphthalate_____BenzQ(b)fluoranthene_____Benzo Ck)fluoranthene_____Benzo(a)pyrena-----IndenoCl .2 .3-cd)pwrene____-Dib*niCa rh)anthracane_____Benzn(g ,h , i )perylane

5010505010101010105050101010501010101010102010101010101010101010

1IIIiuIUIUIUIUtuIUtuIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

1/87 Rev.

148

IFSEMIUOLATILE ORGANICS ANALYSIS DATA SHEET


EPA SAMPLE NO.

Lab Name:ETCNJ

Lab Code: Case No.:

Matr ix: (soi1/water JIJATER

Sample wt/vol: 1000. (g/mL)ML


\ Moisture; not dec. _____ dec . ___


GPC Cleanup: (Y/N) N PH:___

Number TICs found; I

Cont ract:

SAS No.: SDG No.:


Lab File ID: >G9068

Date Received: 1Q/V2/89

Date Ext racted: 10/13/89


D i l u t i o n Factor: I

_£, rf


CAS NUMBER

01.

COMPOUND NAME

ACETONE DIMER

FORM I SU-TIC

RT

6.49

EST. CQNC

84

i/a;

* Q

J

7 Re^-.

149

IBSEMI VOLATILE ORGAN ICS ANALYSIS DATA SHEET EPA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:


Sample wt/vol: 1000. (g/mD ML


S Moist ure: not dec. dec.



Cont ract:

SAS No.: SOG No.:


Lab File ID: >G9Q51

Date Rece ived: (0//4/8J



D ilu tion Factor: 1


108-95-2 ——————— Phenol____________________111-44-4———————bisC2-Chloroethyl )ether____95-57-8 ———————— 2-Chlorophenol_____________541-73-1------—1,3-Dichlorobenzene________106-46-7—— ———— 1,4-Dichlorobenzene________100-51-6 — - —— --Benzyl alcohol_____________95-50-1————-—-1,2-Dichlorobenzene________95-48-7- ———— — -2-Methyl phenol_____________108-60-1——————bi»(2-Chloroi»opropyl)ether_106-44-5———-—-4-Methylphenol_____________621-64-7--------N-Nitroso-di-n-propylamine_67-72-l---------Hexachloroe thane___________98-95-3 —————— --Nitrobenzene_______________78-59-1 ———— -—— Isophorone_________________88-75-5--———-—2-Nitrophenol______________105-67-9--- ———— 2,4-Dimethyl phenol_________65-85-0---------Benzo ic ac id_______________111-91-1 ——————— b is (2-Chloroethoxy)me thane_120-83-2 —————— -2,4-Dichlorophenol_________120-82-1 ——— ——— 1,2,4-Trich lorobenzene_____91-20-3-———————Naphthalene________________106-47-8 ——————— 4-Chloroani 1 ine____________87-68-3————————H«xachlorobutad lene________59-50-7————————4-Chloro-3-methylpheno 1____91-57-6————————2-Methylnaphtha lene________77-47-4---------Hexachlorocyclopentadlene__88-06-2- —— ———— 2,4,6-Trich loropheno 1______95-95-4----——--2,4,5-Trichlorophenol______91-58-7----————2-Chloronaphthalene________88-74-4-- —— —— -2-Nitroani 1 me_____________131-11-3----———Dimethylphthalate__________208-96-8 —— ———— Acenaph thy lene_____________606-20-2 ———— ---2,6-Dinitroto luene_________

101010101010101010101010101010105010101010101010101010501050101010

Q

IUIUIUtuIUIUtuIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM I Sv -1 Rev.


ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No.:

Con t ract :

SAS No.:

Matrix: (soil /water) WATER

Sample uit/vol: 1000. Cg/mL) ML

Level: llow/m«d) LOW

SDG No.:



Date Received:


Extraction: ( SepF/Cont /Sonc ) CONT




Dilution Factor: 1


99-09-2 ———————— 3-Nitroeni 1 ine_____________83-32-9 —————— --Acenaphthene_______________51-28-5-----——-2,4-Dinitrophenol__________100-02-7——————-4-Nitrophenol______________132-64-9—-——--Oibenzofuran_______________121-14-2- —————— 2,4-Dinitroto luene_________84-66-2 ———————— Diethylphthalate___________7005-72-3—-----4-Chlorophenyl-phenylether_86-73-7---------Fluorene ______________100-01-6- — ———— 4-Ni troani 1 me_____________534-52-1---- —— -4,6-Din itro-2-methy 1 phono 1_86-30-6---------N-Nitrosodi phonylamine <1)_101-55-3--------4-Bromophony1-phenyle ther___118-74-l--------Hexachlorobenzene__________87-86-5---------Pentachloropheno 1 _________95-01-8---————-Phenanthrone_______________120-12-7———————Anthracene________________84-74-2----————Di-n-butylphthalate________2 06-44-0-- ————— Fluoranthene_______________129-00-0-- ——— — Pyrene____________________85-68-7—— ———— -Butylbenzylphthalate______91-94-1 ———————— 3,3'-Dichlorobenz id me_____56-55-3----—---BenzoCa)anthracene_________218-01-9 ——————— Chrysene__________________117-81-7———————bisC2-Ethylhexyl Jphthalate_117-84-0 ——————— Di-n-octylphthalate________205-99-2 ——— ———BenzoCb)f luoranthene_______207-08-9————-BenzoCkJfluoranthene_______50-32-8---------Benzo(a)pyrena_____________193-39-5———————Indeno(l,2,3-cd)pyrene_____53-70-3---------Dibenz(a,h Janthracene______191-24-2---- ——— Benzo(g,h,i iperylone_______

(1) - Cannot be separated from Diphenylamme

FORM I SU -2

5010505010101010105050101010501010101010102010101010101010101010

Q

IIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIU

1/97 Rev

151

IFSEMIYOLATI'LE ORGAN ICS ANALYSIS DATA SHEET


EPA SAMPLE NO.

Lab Name:ETCNJ

Lab Code: Case No.:

Matrix: (soiI/water)WATER

Sample wt/vol: 1000. (g/mL)ML

Level: Uow/med) LOU

% Moisture: not dec. _____ dec .___



Number TICa found: *r

Con t rac t:

SAS No.: SDG No.:


Lab File ID: >G9051

Date Received:



Dilution Factor: __ /

CONCENTRATION UNITS:<ug/L or ug/Kg)UG/L

CAS NUMBER01. 141-78-602.03.04.

COMPOUND NAME

Acetic acid, ethyl esterACETONE DIMERUNKNOWNUNKNOWN

RT

5.106.448.907.84

EST. CONC

3901102Q14

Q

JJJJ

FORM I SU-TIC r 2i/a:


ERA SAMPLE NO

Lab Name: ETCNJ

Lab Code: Case No.:

Mat r ix: (soi1/water) WATER

Sample wt/^ol: 10QO. Cg/mLJ ML

Leve1: (low/med) LOW

S M o i s t u r e : not dec. dec.


GPC Cleanup: (.Y/N) N pH:

Con tract:

SAS No.: SDG No.:

Lab Sample ID: QC7QQ?OG

Lab F i l e ID: >HA546

Date Received: \Q (19 IW

Date Ext r acted : 10'12-'89

Date Analysed: 11/15/39


CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L .or ug/Kg,< UG/L

319-64-6 ——————— alpha-BHC_________3-19-65-7- —————— beta-BHC_________319-86-8 ——————— delta-BHC_________58-89-9---—----gamma-BHC(Lindane).76-44-8-———---Heptachlor________309-00-2 —— ————Aldr in___________1024-57-3—————Heptachlor epoxide.959-98-8--------EndosuIfan I______60-57-1 ——— --- — Dieldr in_________72-55-9 ——— ————4,4'-DDE__________72-20-8---------Endrin____________33213-65-9--———Endosulfan II____72-54-8 ———— ———4, 4'-ODD__________1031-07-8--—---Endosulfan su Ifate50-29-3 ———————— 4,4'-DDT__________72-43-5---------Methoxychlor_____53494-70-5-—---Endrin kctone_____5103-71-9 —————— alpha-Chlordane___5103-74-2-------gamma-Chlordane___8001-35-2——-—-Toxaphene________12674-11-2 ————— Aroc lor-1016_____11104-28-2 ————— Aroc lor-1221______11141-16-5 ————— Aroc lor-1232_____53469-21-9 ————— Aroc lor-1242_____12672-29-6 ————— Aroclor-124Q______11097-69-1 ————— Aroc lor-1254_______11096-82-5 ————— Aroc lor-1260______

. 050

. 050

.050

.050

.050

.050

.050

. 050

. 100

. 100

. 100

. 100

. 100

.100

. 100

.500

. 100

. 050

. 0502.500.500.500.500.50011

Q

IIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM I PEST 1/87

15


SAMPLE NO

Lab Nama: ETCNJ

Lab Code: Case No,:


Sample wt/vol: 1000. (g./mL) ML

Level : C low/med) LQCJ

H Molature: not dec. dec.

Extract ion: (SepF/Cont/Sonc) SEPF


Contract :

SnS No.: SDG No.:

Lab Sample ID: QC7QQ30G

Lab File ID: >JA495tt,i» /

Date Received: o»/J 7 f(a fit

Date Extracted: »



CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/KgJ UG/L

319-64-6———————alpha-BHC________319-65-7———————beta-BHC_________319-86-8 —————— delta-BHC_______58-89-9 —————— — gamma-BHCCLindane),76-44-8 ———————— Heptaeh lor_______309-00-2 ——————— Aldrin___________1024-57-3—————-Heptaehlor epoxide,959-98-8———————Endosulfan I_____60-57-1————————Oieldrin_________72-55-9 ———————— 4,4'-DDE__________72-20-8————————Endr in___________33213-65-9—————Endosulfan II____72-54-8 ———————— 4,4'-ODD_________1031-07-8 —————— Endosulfan sulfate.50-29-3————————4,4'-DOT_________72-43-5--- ————— Methoxych lor_____53494-76V5———•—Endr in k«tone____5103-71-9——————alpha-Chlordane___5103-74-2---———gemma-Chlordane___8001-39—ftp-—>---Toxaph«n«_______12674-11J&C-———Aroclor-1016_____11104-28^2————Aroclor-1221_____11141-16-5—————Aroc lor-1232_____53469-21-9—————Aroc lor-1242_____12672-29-6—————Aroc lor-1248_____11097-69-1—————Aroc lor-1254_____11096-82-5—————Aroc lor-1260_____

.050

.050

.050

.050

.050

.050

.050

.050

.100

.100

.100

. 100

.100

.100

.100

.500

.100

.050

.0502.500.500.500.500.50011

IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUiuIUIUIUIU

FORM I PEST 1/87 Rev

54


ERA SAMPLE NO


Lab.Code: Case No.: SAS No.: SDG No.:

M a t P ix: (soi1/water ) WATER Lab Sample ID: QC70049G

Sample wt/vol: 1000. (g/mL) ML Lab F i l e ID: >KBQ99

Level: (low/med) LOW Date Received: 10-"'ia-''ii9

S M o i s t u r e : not dec dec

E x t r a c t ion: (SepF/Cont /Sonc ) SEPF

GPC Cleanup: (Y/N) N pHi





319-64-6 — ——319-65-7 -----319-86-8 —— —59-89-9 ------76-44-8 ------309-00-2 -----1024-57-3 ———959-98-8 -----60-57-1 —— ——72-55-9 ------72-20-8 - — — -33213-65-9 ---72-54-8 — ----1031-07-9 ———50-29-3-" ————72-43-5 ------53494-70-5 ——5103-71-9 ———5103-74-2 ———8001-35-2 ———12674-11-2 ——11104-28-2 ——11141-16-5 ——53469-21-9 ---12672-29-6 ——11097-69-1 ——11096-82-5 ——

—— aloha-BHC—— beta-BHC—— delta-BHC---qamma-BHCCL indane )---Heptach lor---A Idr in---Heptachlor epoxide---Endosu 1 fan I---Die Idr in—— 4.4'-DDE---Endr in---Endosulfan I I—— 4r4'-DDD---Endoaulfan sulfate—— 4.4'-DDT---ttethoxychlor---Endrin ketone,---alpha-Ch lordane--- gamma -Ch lordane---Toxaphene—— Aroclor-1016—— Aroclor-1221— -AroclQr-1232---Arnelar-1242——— Arnclor-1248---Aroclor-1254— -Aroc lor-1260

.050

.050

.050

.050

.050

.050

.050

.050

.100

. 100

. 100

. 100

. 100

.100

.100

.500

.100

.500

.5002.500.500.500.500.50011

1IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1 I

FORM I PEST 1/87 Rev•" co5

8AUOLATILE INTERNAL STANDARD AREA SUMMARY



Lab F i l e ID (Standard): >C74Q8 Data Analyzed: 10''16/89

Instrument ID: GC/MS C T ime An* lyzed: 1354

Mat r ix : Cao i 1 /wat er ) WATER Le^e 1 : ( 1 ow/med ) LQLJ Co I umn : C pack/cap )

01020304050607080910111213141516171819202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.

QC70082UCA1889UCA1890UCA1892UCA1907UCA1908UCA191QUCA20490

IS1CBCM)AREA *

42189

8 A3 78

21094

3659942713399813889031475379213446035775

RT

13.28

13.3013.3213.2813.2813.2913.2913.2813.28

IS2(DFB)AREA #

203322

406644

101661

171925201530195453185362148989185780168447173576

RT

23.72

23.7723.7523.7123.7123.7223.7623.7523 .76

IS31.CB2)AREA ft

155840

311680

77920

130134154129149391142316115252144222131897136509

RT

23.91

28.9228.9228.9228.9028,9128.9528.9428.94

I SI CBCM) - Bromochloromethane152 (DFB) - 1,4-Difluorobenzene153 (CBZ) - Chlorobenzene-d5

UPPER LIMIT - * 10OSof internal standard areaLOWER LIMIT - - 5OSof internal standard area

* Column used to flag internal standard area values with an asterisk.

page * of J_

FORM UII 1 UQA 1/67 Rev

'• •" £I 00

8AVOLATILE INTERNAL STANDARD AREA SUMMARY



Lab File ID (Standard): >C750l Data Analysed: 10/20/89Instrument ID: GC/MS C

Matrix:(soil/water) WATER Level:(low/med) LOW

01020304050607080910111213141516171819202122

——————————

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.

QC70088VCA2146VCA2146V

I*-*

———————————

——————————————————————

———————————.. , —— , —

ISl(BCM)AREA |

39534

79068

19767

392083838337830

————————————————————— .... —— .._

RT

13.28

13.3113.3113.32

———————————————

IS2(DFB)AREA |

177391

354782

88695

178754188257178835

————————

————————————————

XiJH• T**J

23 .75

23.7523.7823.79

——————————

— , ———

• w,' i. -*1 -•-••— '*• — •

144314

288628

72157

146630150869145376

————————————————

\28.90

1

28.9328.9728.98

—————

—————————— i

151 (BCM) - BrOBOChloromethane152 (DFB) - 1,4-Difluorobenzene153 (CBZ) - Chlorobenzene-d5

UPPERof inLOWERof 1

t Column used to flag internal standard area value*page / of J_

PORN VIII VOA

asterisk,

157 1/87 R*v,

\



Lab Code: Case No.: SAS No,: SOG No.:

Lab File ID (Standard): >C7519 Data Analyzed: 10/22/89

Instrument IDs GC/MS C Time Analyzed: 1655

Matrix:(soi I/water) CJATER Leve1:<low/med> LOW Co lumn : (pack/cap ) fflCr~

\\\ 12 HOUR STD

1 UPPER LIMIT

I LOWER LIMIT

1 EPA SAMPLE1 NO.

01IQC7009QIJ02ICA2282U03ICA2282US041CA22B2UR05ICA2266IJ061071081091101111121131141151161171181191201211221

ISKBCM)AREA *

46491

92982

23246

4202436664399283773424557

RT

13.28

13.2713.3613.3113.2813.27

IS2CDFB)AREA *

205876

411752

102938

190197172548183079180366106883

RT

23.76

23.7423.7923.7923.7523.74

1S3CCB2)AREA *

157804

315608

78902

15003113835014674414501589817

RT

28.91

28.9328.9928.9728.9428.93

151 CBCh) - Bromochloromethana152 CDFB) - 1,4-Difluorobenzene153 (CBZ) • Chlorobenzen«-d5

UPPER LIMIT - * 1005Sof internal standard areaLOWER LIMIT - - 50*of internal standard area

# Column usad to flag internal standard area values with an asterisk,

page __[_ of _L

FORM v I I I VOA158

1/87 Rev

FGRF1 vi I 1 1/67 Rev.


Lab Name: ETC Corp. Cont rac t:


Lab File ID (Standard): >C7530 Data Analyzed: 10/23/89

Instrument ID: GC/MS C Time Analyzed: 1007

Mat r ix: Csoi 1/uiater ) UATER Leve1:<low/med) LOCJ Column: (oack/cap) 0

111 12 HOUR STD

1 UPPER LIMIT

1 LOWER LIMIT

1 EPA SAMPLE1 NO.

Q1ICA2266U

031041051061071081091101111121131141151161171181191201211221

IS1CBCM)AREA *

37984

75968

18992

36361

RT

13.28

13.28

IS2CDFB)AREA *

165320

330640

82660

177259

RT

23.76

23.752j ,rs~

IS3CCB2)AREA *

139575

279150

69788

140685

RT

28.95

28.93££.??

151 CBCM) - Sromochloromathana152 CDFB) - 1,4-Difluorobenzene153 CCBZ) - Chlorobenzene-d5

UPPER LIMIT - * 100*of internal standard areaLOWER LIMIT - - 5OXof internal standard area

# Column used to flag internal standard area values with an asterisk

page I_ of 159


Lab Nama: ETC Corp. Contract:

Lab Coda: Case No.: SAS No.: SDG No.:

Lab File ID (Standard): >D8035 Data Analyzed: 10/17/89

Instrument ID: GC/MS D Tine Analyzed: 1353

Matrix: (soil/water) WATER Level:(low/aed) LOW Column: (pack/cap) __

01020304050607080910111213141516171819202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.

QC70083VCA2141VCA2142VCA2143VCA2149VCA2151VCA1891VCA2145VCA2152VCA2153V

--

-

1 , ————————— -

ISl(BCM)AREA /

39166

78332

19583

41410421103719237641382233366537042414403397638085

•

—————————

RT

12.59

12.5812.5812.5812.6212.6212.6112.6412.6112.6912.68

IS2(DFB)AREA *

142356

284712

71178

148994152698133875133042140077120299131855137967120773123053

————————

RT

23.24

23.2323.1923.2223.2323.2723.2223.2523.2623.3023.29

_ ————

IS3(CBZ)AREA *

114710

229420

57355

1145561212331074091083611119649801010726110690097900100167

————————

iRT

28.21

28.4028.1528.2328.3128.3128.2628.2928.3028.3128.33

————— 1————— 1—————

————— 1

151 (BCM) - BroBOChloroaethane152 (DFB) -,1,4-Difluorobenzene153 (CBZ) - Chlorobenzene-d5

UPPER LIMIT - + 100%of internal standard area.LOWER LIMIT - - 50%of internal standard area.

i Column used to flag internal standard area values with an asterisk,

page __{_ of f

FORM VIII VGA 1/87 Rev,

160




Lab File ID (Standard): >I8245 Data Analyzed: 10/18/89

Instrument ID: GC/MS I Time Analyzed: 2242

Matrix:(soil/water) WATER Level:(low/med) LOW Column:(pack/cap) $j<4£.

01020304050607080910111213141516171819202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.

QC70085VQC70085VCA2150VCA2147VCA2144V

___________

———————————

——————————————————————

———————————

ISl (BCM)AREA |

33721

67442

16861

3248129675313123113030945

.

RT

10.84

10.8410.8910.8610.9310.89

—————

—————

———————————————

—————

——————————

_____

IS2(DFB)AREA 1

217291

434582

108645

211363203617205895195838204243

RT

21.47

, ————

21.5021.5121.5121.5521.51

———————————————

—————

—————

—————

——————————

——————————

IS3(CBZ)AREA I

201421

402842

100711

186150176154181340172652180528

—————————

RT

26.30

™«-

'

26.3626.4026.3726.4026.37——————————

-

—————

-

_____

151 (BCM) * Bromochloromethane152 (DFB) - 1,4-Difluorobenzene153 (CBZ) » chlorobenzene-dS

UPPER LIMIT - + 100%of internal standard areaLOWER LIMIT - - 50%of internal standard area

I Column used to flag internal standard area values with an asterisk.

page _f_ of _{_

FORM VIII VGA 1 5-|l/87 Rev

•88I VOLATILE INTERNAL STANDARD AREA SUnriARY

Lab Name: ETCNO . _ Contract:


Lab File ID (Standard): >G9036 Data Analyzed: 1

In-itrument ID: GC/MS G Time Analyzed: 1703

I11 12 HOUR STD

1 UPPER LIMIT

1 LOWER LIMIT

1 EPA SAMPLE1 NO.

01'QC70087C021CA1907CR03ICA2139CQ4I05! ^061071"091D9!1QI11112113 !14115 I16117118 t1912QI21!22 1

I SI (DCS)AREA *

282541

565082

141270

255355288674254550

-

RT

10.65

10.7010.6410.62

IS2CNPT)AREA *

535163

1070326

267581

518146514242532142

RT

14. 44

14.4914.4214.40

I S3 ( ANT JttREA *

189412

373324

94706

175698172977187300

• RT

19.«>'

19.9319.8*19.87

I SI (DCB) - '1,4-DichIorobenzene-d4152 (NPT) • NaphthaIana-d8153 (ANT) - Acenaphthene-dlO

UPPER LIMIT - * 100Sof internal standard areLOWER LIMIT - - 50Sof internal standard are.

Column used to flag internal standard area values with an asterisk

of _i_

FORM Y I I I SU -1 1/87 R

162

SE~IUOLATII_E INTERNAL STANDARD AREA SUMMARY


Lab Code: */; Case No.: SAS No.: SDG No.:

Lab Fila ID (St-*pd«rd): >G9036 Data Analyzed: 1

Instrument ID: GOXMS G Time Ana 1yzed: 1703

I11 12 HOUR STD

1 UPPER LIMIT1 ............1 LOWER LIMIT

1 EPA SAMPLEI NO.

01 IQC70087C02ICA1907CR03 SCA2139C04105!061 A07!08109!10111!12113!14115!16117!18 119 I20121122!

IS<UPHN)AREA #

187149

374298

93575

160667158911167522

RT

24.30

24.3724.2824.30

I 35 (CRY)AREA *

99167

198334

49584

75477 -7767582871

RT

32.32

32.3732.2932.30

1 56 l PRY j.4REA *

32054

164U!3

41027

505745374364060

1RT '.

36. .K :

:

I

36.38136. 3C !36.311

11

• * . i1:1i1:I

I

1

1

I

154 (PHN) *<Ph»n«nthrene-dlO155 (CRY) --'Naphtha Iene-d8156 (PRY) - Peryl8ne-dl2

UPPER LIHIT - * 100Sof internal standard are?LOWER LIMIT - - 50Sof internal standard are-j

4 Column uaed to flag internal standard area values with an asterisk,

page > of >•

FORM y i l l SU -2 1/87 Rev

163

\

SBSEMIUQLATILE INTERNAL STANDARD AREA SUMMARY


Lab Coda: Case No.: SAS No.: SDG No.:

Lab File 10 (Standard): >G9Q50 Data Analyzed: 11/15/89

Instrument ID: GC/MS G Time Analyzed: 0522

111 12 HOUR STD

I UPPER LIMIT

1 LOLJER LIMIT

1 EPA SAMPLE1 NO.

01IQC70092C02ICA1989C03ICA189QC041CA1892CQ5ICA1908C06ICA2141C07ICA2142C08ICA2143C09ICA2149C10ICA2151C11ICA1891C12113114115116 1171181191201211221

I SIC DCS)AREA *

256551

513102

128276

240559230417246079239441242717235102249428244556237764240162240419

RT

10.65

10.6210.6?10.6910.7710.6410.7310.6510.6710.6610.7110.63

IS2CNPT)AREA *

471741

943482

235870

471802462180498070495825490791502344497082475863487364473507502004

RT

14.44

14.4014.4114.6914.5714.4014.5314.4114.4314.4514.4914.41

I S3 CANT)AREA *

141059

282118

70530

168640170195179642180192163346181473184494169610173464176429175644

RT

19.87

19,8719.9720.1320.0219.8719.9719.8719.9019.9119.9319.88

151 CDCB) • l,4-Dichlorobanzene-d4152 CNPT) - Naphthalene-de153 CANT) - Acenaphthene-dlO

UPPER LIMIT - * 100Hof internal standard areaLOUER LIMIT - - 50Hof internal standard area

t Column used to flag internal standard area values with an asterisk

page I of ^

FORM v I I I SU -1 1/87 Rev

164

' 8CSEMI VOLATILE INTERNAL STANDARD AREA SUMMARY

Lab Name: ETCNJ . • Contract:

Lab Code: Case No.: SAS No.: SOG No.:

Lab File ID (Standard): >G9050 Data Analyzed: 11/15/89


11!-------«----1 12 HOUR STD

1 UPPER LIMIT

1 LOWER LI M I T

1 EPA SAMPLE1 NO.

01IQC70092C021CA1989C03ICA1890C04ICA1892C05ICA1908C06ICA2141C07ICA2142C081CA2143C09ICA2149C101CA2151C11ICA1891C12113114115116 117118119 1201211221

1S4CPHN)AREA *

114814

229628

57407

127020138009149915145382120831144621169279143921137686147269144641

RT

24.28

24.3024.2824.5624.4524.2824.4124.3024.3624.3224.3724.31

IS5<CRY)AREA *

44817

89634

22409

3414556608546096138643046456237912354998555766070454223

RT

32.31

32.2832.2932.5732.4632.3032.4132.3132.3432.3332.3732.32

IS6CPRY)AREA *

30368

60736

15184

1895839187298544149423102279215984132865351193827435508

RT

36.32

36.3136.2936.5836.4836.3136.4236.3236.3536.3436.3836.32

154 (PHN) - Ph«nanthrene-dlO155 (CRY) - Naphthalena-dS156 CPRY) - Perylene-dl2

UPPER LIMIT - + 100Sof internal standard areaLOWER LIMIT - - 50*of internal standard area

Column used to flag internal standard area values with an asterisk

P«g«

FORM 01 I I SU -2 1/87 Rev,

165

9BSEMIUQLATILE INTERNAL STANDARD AREA SUMMARY



Lab File ID (Standard): >G9Q63 Data Analyzed: I


01020304050607080910111213141516171819202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.

QC70091CCA2271CRCA2147CCA2148CCA2271C

ISKDCB)AREA t

..........276549

553098

138274

250442275372230515108083*129422*

•

RT

10.65

10.6910.6610.6710.7110.66

IS2(NPT)AREA *

492671

985342

246335

524559529334519116543511496678

RT

14.44

14.4714.4414.4114.4914.44

I S3 (ANT)AREA *

1 5 42 74

308549

77137

18671319281815149910568359580*

RT

19. ay

19.9219.8919.8819.9419.90

151 (DCS) - 1,4-DichIorobenzene-d4152 CNPT) - Naphthalene-dB153 (ANT) - Acenaphthene-dlO

UPPER LIMIT - * 10OHof internal standard areaLOWER LIMIT - - 5OXof internal standard area

If Column used to flag internal standard area va lues with an asterisk

page | of 3,

FORM U I I I SU -1 1/87

166

• acSEMIUOLATILE INTERNAL STANDARD AREA SUMMARY

Lab Name: ETCNJ .. Contract:


Lab File ID (Standard): >G9Q63 Data Analyzed: 11/15/39


II

I 12 HOUR STD

1 UPPER LIMIT|. ...........1 LOWER LIMIT1 ------------1 EPA SAMPLE1 NO.

01IQC70091C02ICA2271CR031CA2147C04ICA2148C05ICA2271C06 107108 109110111112113114115116117118119120121t221

I 54 (PHN)AREA *

133400

266800

66700

167193177060164366153598115409

»

RT

24.33

24.3524.3224.3224.3624.33

I 35 (CRY)AREA *

53074

106148

26537

8068680693763824323720846*

RT

32.34

32.3532.3232.3132.3632.31

IS6(PRY)AREA *

35CI46

70092

17523

62052619351854714251"8751*

RT

36.32

36.3636.3336.3236.3636.32

154 (PHN) • Phenanthrene-dlO155 (CRY) - Naphthalana-d8156 (PRY) - Perylene-dl2

UPPER LIMIT - * 100*of internal standard areaLOWER LIMIT - - 50*of internal standard area


page > of y

FORM UII I SU -2 1/87 Rev,

167

' 8BSEM1UOLATILE INTERNAL. STANDARD AREA SUMMARY

Lab Name; ETCNJ . • Contract:

Lab Code: Case No.: SAS No.: SOG No.:



111 12 HOUR STD

1 UPPER LIMIT

1 LOUER LIMIT

1 ERA SAMPLE1 NO.

01ICA2144C02ICA2145C03ICA2146C04ICA2152C05106107108109 1101111121131141151161171181191201211221

I SI (DCS)AREA *

276549

553098

138274

191857243058239961245749

RT

10.65

10.7010.6610.6510.64

IS2(NPT)AREA *

492671

985342

246335

429069510921492184530356

RT

14.44

14.4614.4414.4314.42

I S3 (ANT)AREA *

154274

309548

77137

132832169355164409187309

RT

19.89

19.8819.9119.8819.89

151 (DCB) - 1,4-Dichlorobanzene-d4152 (NPT) - Naphthalane-d8153 (ANT) • Acanaphthene-dlO

UPPER LIMIT - + 100%of internal standard areaLOUER LIMIT - - 5OSof internal standard area,

t Column used to flag internal standard area value* with an asterisk

page _J_ of "^

FORM UIII SU -1 1x87 Rev

68

8CSEMIVOLATILE INTERNAL STANDARD AREA SUMMARY

Lab Name: ETCNJ . ' Contract:




111 12 HOUR STD|-»«. ........1 UPPER LIMITI............1 LOUER LIMIT

1 EPA SAMPLE1 NO.

01ICA2144C02ICA2145C03ICA2146C041CA2152C05106107108109 110111112113114115116 117118119 1201211221

I S4 ( PHN )AREA *

133400

266800

66700

129544121470128347150911

RT

24.33

24.3024.3224.3124.32

IS5(CRY)AREA *

53074

106148

26537

54664461004801365366

RT

32.34

32.3132.3332.3232.32

IS6CPRY)AREA *

35046

70092

17523

31172292592983247111

RT

36.32

36.3236.3336.3236.33

154 (PHN)155 CCRY)156 (PRY)

Pn»nanthr«ne-dlONaphtha Iene-d8Perylene-dl2

UPPER LIMIT - * 10OHof internal standard areaLOUER LIMIT - - 5QSof internal standard area

$ Column used to flag internal standard area values with an asterisk.

page * of *

1/87 Rev

169FORM V I I I SU -2

. SBSEMIIJOLATILE INTERNAL STANDARD AREA SUMMARY

Lab Name: ETCNJ .. Contract:




0102030405060708091011121?141516171819202122

12 HOUR STD

UPPER LIMIT

LOUER LIMIT

EPA SAMPLENO.

CA2271CSCA2148C

IS1CDCB)AREA *

338478

676956

169239

286120179032

-

RT

10.61

10.5910.58

IS2(NPT)AREA #

730615

1461230

365307

588970548187

RT

14.39

14.3714.36

I S3 (ANT)AREA *

215733

431466

107866

19232796014*

RT

19.83

19.8019.79

151 (DCB) - l,4-Dichlorobenzene-d4152 (NPT) • Naphthal«ne-d8153 (ANT) - Acenaphthene-dlO

UPPER LIMIT « * 100*of internal standard areaLOWER LIMIT - - 50*of internal standard area


page I_ of V

FORM "JI I 1 SU -1 1/87

170

• 8CSEMIUOLATILE INTERNAL STANDARD AREA SUMMARY

Lab Name: ETCNJ . . Contract:


Lab File ID (Standard): >G9Q76 Data Analyzed: 11/16/39


01020304050607080910111213141516171819202122

12 HOUR STD

UPPER LIMIT

LOUER LIMIT

EPA SAMPLENO.

CA2271CSCA2148C

1S4CPHN)AREA *

165383

330766

82692

177951162424

•

JRT

24.25

24.2324.21

IS5(CRY)AREA *

68593

137186

34296

6628423270»

RT

32.26

32.2432.21

IS6CPRY)AREA *

47777

95554

23889

621522610-

RT

36.24

36.2336,23

154 (PHN) - Phenanthrena-dlO155 (CRY) - Naphthalene-dS156 (PRY) - Perylene-dl2

UPPER LIMIT - * 100*of internal standard areaLOUER LIMIT - - 5 OSof internal standard area

# Column used to flag internal standard area va lues with an asterisk

page _£_ of

FORM Y I I I SY -2 1/87 Rev,

171

L«b Mama; ETCNJ

Lab Code:

Lab Tile 10 CS

;-[UQLATILE INTERNAL STANDARD AREA

Cont pact:

'C«»e No.: SAS No.: SDG No.:

>G9076 Data Analyzed: 11/16-->:J

Instrument ID: CtVftS G Time Analyzed:

III 12 HOUR STD

1 UPPER LIMIT

1 LOWER LIMIT

1 EPA SAMPLE1 NO.

01 ICA1907CS02ICA1907C03 :CA214QC04105!06 1 f.07:08109:10111112113 :14115:16117'181191201211221 __ ~»W

IS1CDC8)AREA *

338478

676956

169239

288384259179252117

L

RT

10.61

10.6110.5810.57

IS2CNPT)AREA *

730615

1461230

365307

631399609744589730

RT

14.39

14.3814.3714.36

I S3 t ANT)AREA *

215733

431-166

107366

242119278999244976

1RT :

19.8 '

1

19.83119.82:19.811

!I

• * !1

1

1

1

1

1

I'

1

151 (DCS) JpJjE-O i chip robe152 CNPT) *jft|)ith«Un«-d8IS7 (ANT) - MMnaphth«ne-dlO

UPPER LIMIT - * 10USof internal standard are. .LOWER LIMIT - - 50Sof internal standard are-..

t Column used to flag internal standard area values wi t h an asterisk,

page J_ of _3"

FORM UII I SU -1 1/87 R«

172

Lab Name: ETCNO

Lab Coda:

Lab Fi10 ID CS

_E INTERNAL STANDARD AREA SUMMARY

Cont ract:

Case No.: SAS No.: SDG No. :

rf): >G9076 Data Analyzed: ll/16--'>''

Instrument ID: SC ttS G Time Analyzed: 1426

111 ............1 12 HOUR STD

1 UPPER LIMIT

1 LOWER LIMIT

1 EPA SAMPLE1 NO.

01 :CA19Q7CS02ICA19Q7C03 ICA2140C04105:06 1 *07:08 109 i10111!12 t13!14115:16 117!19119!201211221 _ ._ W

IS4CPHNJAREA *

165383

330766

82692

187290220338181325

I

RT

24.25

24.2424.2524.23

1 55 I CRY)AREA t

68593

137186

34296

748448138177968

RT

32.26

32.2332.2432.21

IS6CPRY)^REA *

47777

9"?5<?4

23339

494825472056880

RT

36.2-

36.2436.2536.22

-• i

ISA CPHN)IS? (CRY)ISA (PRY)

thre.n«-dlOhal»n»-dfltan*-d12

UPPER LIMIT - * 100%of internal standard are*,LOWER LIMIT - - 50*of internal standard are«

Column used to flag internal standard area values with an asterisk.

FORM VJI I I SU -2 1/87 Re.

173

ETC

TABULATED RESULTS

NON CLP PARAMETERS

174

4

— ^^^p" L ' ** ————————————— ——— ——— —— ——— ————————————————————TABLE 1: QUANTITATIVE RESULTS and QUALITY ASSURANCE DATA

Conventional Analysis Data (QR1O)

Chain of Custody Data Required for ETC Data Management Summary Report*

CAI889 WASTE MANAGEMENT, INC. 405 WBL 89 1 006 1447 1ETC >«Mpl< No, CwHKny Ficility SwipJt Point 0*t« Time Hour*

NPOESNumber

Chloride mg/lFluoride mg/1Nitrate as N mg/lPhenolic*. Total mg/lCyanide. Total mg/lTotal Organic Carbon mg/lTotal Organic Carbon mg/lSpecific Conductance urn/ cmSpecific Conductance urn/ cmpH stdpH stdNitrite as N mg/l

Cn

Results

SampleConctn,

30 11

12.7<.050.00126.26.3

770770

7.097 .11

H>L

1.0.1.1

.050.01001.01 .0

10.010.0

.1

DEC 16. 1989

•

ETCOCT 31. 1989

TABLE 1: MISCELLANEOUS DATA (QR64)

Chain of Custody Data Required for ETC Data Management Summary Reports

CA1889 WASTE MANAGEMENT, INC. 405 WBL 891006 1447 1E 1 apsed

ETC Sample rte . Company Facll i ly Sampl* Pojnl Dale Time Hours

Compound

Ammonia as NSulfate as S04Bicarbonate as CaC03Carbonate as CaC03Nitrogen. Total Kjeldahl (TSolids, total dissolved (RO

O\

Resu l t s

SampleConcen .

mg/1

( . 0 440.4

3760

.25467

MDLmg/1

.045.0

10,0

.2010

-

^

pHpHpHPH

C 1 b ————————————————————————————————————————————————————————————————————

TABLE 1: QUANTITATIVE RESULTS and QUALITY ASSURANCE DATA

Field Parameters (QR16)


CA1889 WASTE MANAGEMENT, INC. 405 891006 0

ETC S#nple No. Conpiny Facility Simple Point 0*te Tim* Hours

Parameter

Field ' stdField stdField stdField std

Specif ic Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. C

R e s u l t s

SampleMeasure

7.217 .227 .227.24

784779779779

11.8

MDU

--------

OCT 16. 1989

•

—— __ ^B^K r C 1 L ——————————————————————————————————————————————————————————————————————————————————


Conventional Analysis Data (QR10)


CAI890 WASTE MANAGEMENT, INC. 405 USU 891006 1603 1El*pt*«

ETC S*npl< No. Conpiny Facility S«npl« Point Bite Time Hours

NPDESNumbtr

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenolics, Total mg/1Cyanide, Total mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specific Conductance urn/cmSpecific Conductance urn/ cmpH stdpH stdNitrite as N mg/1

OO

Results

SampleConcen,

14 81

2 .0< .050

.000843 63.7

670670

7 237.25

HDL

1 .0.1.1

.050.0100

1 01 .0

10. 010.0

.1

DEC 16. 1989

———— ^^fe^ t 1 L ————^ =-~



CA1890 WASTE MANAGEMENT. INC. 405 WSW 891006 1603 IElapsed

ETC Sample Mo. Company Facil i ty Sample Point Dale Time Hours

Compound

Ammonia as NSul fa te as S04Bicarbonate as CaC03Carbonate as CaC03Nitrogen. Total Kjeldahl (TSolids, total dissolved (RO

vo

Result s

SampleConcen.

mg/1

< .0427 .3

3130< . 2 0

377

MOLmg/1

.045 .0

10.0

.2010

OCT 31 , 1989

^^te^- C 1 L^^^s^^=




CA1890 WASTE MANAGEMENT. INC. 405 891006 0Elapsed

ETC Sample No. Company Facil i ty Sample Poinl Dale Time Hours

Parameter

pH Field stdpH Field stdpH Field stdpH Field stdSpeci f ic Conductance Field urn/cmSpecif ic Conductance Field urn/cmSpeci f ic Conductance Field urn/cmSpec if ic Conductance Field urn/cmTemperature Deg C

COCD

R e s u l t s

SampleMeasure

7 . 2 07 227.257.27

683688690695

14 0

MDL

OCT 16, 1989

———— ^B^ C | C ———————————————————————————————————— - ——————————————— ———— ———— - ———————————————————————————————^^^^




CA1891 WASTE MANAGEMENT. INC. 405 WIH 891010 1730 1El*p»ed

ETC 8«npl« No, Cawjny FicJlity S«npl« Point D*t« Tim* Hours

NPOESNumber

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenol ic s . Total mg/1Cyanide. Total mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specific Conductance urn/ cmSpecific Conductance urn/cmpH stdpH stdNitrite as N mg/1

CU

Result*

SaMpleConcen ,

7 0< 1< 1

< 050.00152 62 8

384 0386 0

7.557 56< . l

W>L

1 .0.1

1.05001001.01 0

t o o10.0

.1

DEC 16. 1989

—— " If -.-- 1 1 I — •



CAI891 WASTE MANAGEMENT. INC. 405 WIH 891010 1730 1t 1 apt * 3

ETC Sample H<, . Company f a c i l i t y Sample Point Da le Tim* n.-mrs

Compound

Ammonia as NSulfate as S04Bicarbonate as CaC03Carbonate as CaC03Nitrogen, Total Kjeldahl (TSolids, tota l d isso lved (RO

ODNJ

R e s u l t s

SampleConcen

mg/1

< .0423 4

1890

20249

MDLmg/1

045 0

10 0

2010

NOV 3, 1989

-

—— "^^^^ 1 1 u ———————————————————————— • —— • ———————— • ————————————^^^^^gjF



Chain of Custody Data Required 'or ETC Data Management Summary Reports

CAI891 WASTE MANAGEMENT. INC. 405 WIH 891010 1730 IE lapsed

ETC Sample No, Complfiy Facility Sample Point 0*1* Time Haufj

Parameter

pH 'Field stdpH Field stdpH iField stdpH IField stdSpeci f ic Conductance Field urn/cmSpecif ic Conductance Field urn/cmSpecif ic Conductance Field urn/ cmSpecific Conductance Field urn/cmTemperature Deg . C

CoCM

Result s

SampleMeasure

7.367.357.397.40

410419416415

1 2 0

MDL

OCT 17. 1969

—— ^__^ c , L —————————————————————— . —— —— ,. ———— . ————————————————•sir




CA1892 WASTE MANAGEMENT. INC. 405 WU 891006 0836 1

ETC Sample No, Company Facility S«npl« Point D*ie Time Hours

NPDESNumber

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenolics. Total mg/1Cyanide . Total mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specific Conductance urn/cmSpecific Conductance urn/cmpH stdpH stdNitrite as N mg/1

Oo

Result s

SampleConcen .

25.9.1.3

< .050.00124.95.0

690690

7.297.34

MDL

1 .0.1

1.050

.01001 .01 0

1 0 010 0

.1

DEC 16. 1989

—— fi c ' L ——



CA1892 WASTE MANAGEMENT. INC. 405 WLA 891006 0836 1

ETC Sample Mt> . Company Facility Sample Poini Date Time Hours

Compound

Ammonia as NSulfate as S04Bicarbonate as CaC03Carbonate as CaC03Nitrogen Total Kjeldahl (TSol ids, total dissolved (RO

OJcn

Resu l t s

SampleCone en

mg/1

< 0437.6

3280

20384

MDLmg/1

045 0

1 0 0

2010

OCT 31 , 1989

^ C 1 L




CA1892 WASTE MANAGEMENT. INC. 405 891006 0E la pied

ETC Sample fto. Company Faci l i ty Sample Poini Da te lime Hours

Parameter

pH Field stdpH Field stdpH Field stdPH Field stdSpecific Conductance Field urn/cmSpec i f i c Conductance Field urn/cmSpeci f ic Conductance Field urn/cmSpec i f ic Conductance Field urn/ cmTemperature Deg C

OJON

Resu l t s

SampleMeasure

7 357.357.387 40

6586586526S3

1 0 5

MDL

-

OCT 16, 1989

<^ F L IL . . . . . .



Chain o* Custody Data Required for ETC Data Management Summary Reports

CAI907 WASTE MANAGEMENT, INC. 40S XDUP 891006 1447 1

ETC Sample No, Company Facility Sample POIOI Date lime Hours

NPDESNumber

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenol ics , Total mg/1Cyanide, Total mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specific Conductance urn/cmSpecific Conductance urn/cmpH stdpH stdNitrite as N mg/1

Results

SampleConcert.

30 3I

< |<.050.00175.05 .2

780800

7 217 23< 1

WL

1 .0.1. 1

.05001001 .01 0

10.010 0--

.1

DEC 16, 1989

-

—— ^^K c ' L ——TABLE 1: MISCELLANEOUS DATA (QR64)


CA1907 WASTE MANAGEMENT. INC, 405 XDUP 891006 1447 1E lapiea

ETC Sample No. Company faci l i ty Sample Poini Dale Time Hours

Compound

Ammonia as NS u l f a t e as S04Bicarbonate as CaC03Carbonate as CaC03Nitrogen, Tota l Kjeldahl (TSolids, t o ta l d issolved (RO

ODCO

Resu l t s

SampleConcert .

mg/1

< 0440 3

3560

28473

MDLmg/1

045 0

1 0 0

.2010

OCT 31 , 1989

^ C 1 L " , , . , . , . . . , „ .




CA1907 WASTE MANAGEMENT. INC. 405 891006 0E lapsed

ETC Sample No. Company Facility Sample Poinl Dale Time Hour^

Parameter

pH Field stdpH Field stdpH Field stdpH Field stdSpeci f ic Conductance Field urn/cmSpecif ic Conductance Field urn/cmSpecif ic Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. C

— iCO

R e s u l t s

SampleMeasure

7.217.227.227.24

784779779779

11 .8

MDL

-

OCT 16. 1989



Chain of Custody Data Requtred for ETC Data Management Summary Reports

CA1908 WASTE MANAGEMENT. INC 405 X03FB 891006 1400 0£ 1 jpicd

ETC S.*mpl« No. Company Fac i l i t y Sample Poinl Dale Time Mour»

NPDESNumber

Chloride mg/1Fluoride mg/1Ni t rate as N mg/1Phenol ics. Tota l mg/1Cyanide, total mg/1Total Organic Carbon fng/lTota l Organic Carbon mg/lSpec if ic Conductance urn/ cmSpec i f ic Conductance um/cmpH - stdpH stdNitr i te as N mg/1

VOO

Resul t G

SampleConcert .

>0>0

< 1< 050

.00015<1 0<1 010 610 88 528 54< 1

HDL

1 01

. 1050

.01001 01 0

1 0 010.0

. 1

NOV 10, 1989

———— •P!rE" t 1 L. ————^* ' ' =;~



CA1908 WASTE MANAGEMENT. INC. 405 X03FB 891006 1400 0E 1 »pied

ETC Sample No. Company Faci l i ty 3*nple Point Dd<* Time Hours

Compound

Ammonia as NSul fate as S04Bicarbonate as CaC03Carbonate as CaC03Nitrogen, Total Kjeldahl (T

Resu l t s

SampleConcen .

mg/1

< 04<5 .0

<10 00< 20

MDLmg/1

.045 0

10 0-

.20

NOV 21 , 1969

——————————————— __________————— pr - C , ^ ——————————————————————————————————————————————————————————————————————————————————————————————————————————————————————————————————————————————— _ _ _ _ _ . M ———————————————————————————————————————————————————————————————————————————————————————————————————————————————————————————




CA2144 WASTE MANAGEMENT. INC. 405 W1GWP5A 891010 0830 1Elapsed

ETC Sample No. Company Facility Simple Point Date Urn* Hours

NPOESNumber

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenol ics .To ta l mg/1Cyanide, Total mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specific Conductance urn/cmSpecif lc Conductance urn/ cmpH stdpH stdNitrite as N mg/1

, — \

ro

Recult •

SampleConcen .

67 7.3.2

.140.0016

200.3203 7

1320 01320 0

6 .796.79

MDL

1 .01

. 1.050

.01001 .01 .0

10.010.0

1

NOV 27. 1989

—— B^^ e i c ——



CA2U4 WASTE MANAGEMENT. INC. 405 W1GWP5A 891010 0830 1[ lapied

E1C Sample No. Company Faci l i ty Sample Point P a t e lime n>i i rs

Compound

Ammonia as NS u l f a t e as S04Bicarbonate as CaC03Carbonate as CaC03Nitrogen. Total Kjeldahl (TSol ids, tota l d issolved (RO

soOsl

Resul ts

SampleConcer t ,

mg/1

19<5 0

79201 02

1030

MDLmg/1

045 0

10.0

2010

NOV 3, 1989

•

PHpHpHpH

By c i *» ™ ————— """ ——— — . . . . . . . . . — — -- --.- —— - ————— .


Field Parameters (OR 16)

Chain gf Custody Data Required for ETC Data Management Summary Reports

CA2144 WASTE MANAGEMENT, INC. 405 W1GWP5A 891010 0830 1ETC Sample Mo. Camoiny Facility 8*nple Polnl ttite Time Hour*

Parameter

Field stdField stdField stdField! std

Specific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. C

VO-P*

Retultt

SampleMeasure

6.796.987.007 01

1408141114061404

1 0 . 7

MDL

--------

OCT 17, 1989

.

—— ^^^^p. c J L ——————————————— ,„ ———————————————————————————————— _ ——————




CA2145 WASTE MANAGEMENT. INC. 405 W1GWP8A 891010 4.0 0Elspsta

ETC Simple No. Company Fjcilily Sanple Point Date Time Houis

NPDESNumber

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenol ics , Total mg/1Cyanide , Total mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specific Conductance urn/cmSpecific Conductance urn/cmpH stdpH stdNitrite as N mg/1

cn

Resu l t s

SampleConcen .

7 7< .1

9< .050.00231 1 . 111 3

1 1 7 3 . 01 1 7 3 . 0

7 067 07

MDL

1 .011

.050.0100

1 01 0

10 .010 .0

1

NOV 27, 1989

——— ^P^F^ C 1 I ———



CA2I45 WASTE MANAGEMENT. INC. 405 W1GWP8A 891010 4 0 0E J»pied

ETC Samole Mo. Company Facil i ty Sample Poinl Dale Time Hours

Compound

Ammonia as NSu l f a te as S04Bicarbonate as CaC03Carbonate as CaC03Nitrogen, Total Kjeldahl (TSol ids, total dissolved (RO

O\

Resu l t s

SampleConcert .

mg/1

.076.95

6590

. 7 1621

MDLmg/1

045 0

10.0

.2010

NOV 3. 1989

-

VI

pH Fi<pH FipH FipH Fi

B (^ ———————————— . ————————————— . ————————————————————————————————— H ————— __r




CA2145 WASTE MANAGEMENT, INC. 405 W1GWP8A 8 9 1 0 1 0 4 0 0

ETC S**pJe No, Company Facility Sample Point Oile 11** Hou'i

Parameter

sld stdsld stdaid std• Id std

Specific Conductance Field urn/cmSpecific Conductance Field urn/ cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. C

Resu l t s

SampleMeasure

6.506.496.516.50

1026102610301027

10 9

MDL

--------

OCT 17, 1989

.

—— ^pp - . c | ————————————————————————— — -'— ————————— - ——————




CA2146 WASTE MANAGEMENT, INC. 405 WIGWPIOA 8910IO 1405 IElapsea

ETC Sample Ho, Company Facility Sample Point Date Time Hours

NPDESNumber

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenol ics . T o t a l mg/1Cyanide , Total mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specif ic Conductance urn/cmSpecif ic Conductance urn/ cmpH stdpH stdNitrite as N mg/1

OO

Result t

SampleConceit .

27 .3.2

< .1<.050.00191 7 . 717.9

1075 01076 0

6.626 63< I

MDL

1 011

.050.0100

1 .01 0

1 0 01 0 0

1

NOV 27. 1989

——— ^^^_ C 1 L ————



CA2146 WASTE MANAGEMENT, INC. 405 WIGWPIOA 891010 1405 1E 1 ipseJ

ETC Sample No, Company Fac i l i t y Sample Point D a t e Time Hours

Compound

Ammonia as NSulfate as S04Bicarbonate as CaC03Carbonate as CaC03Nit rogen. Total Kjeldahl (TSol ids, total dissolved (RO

VO

Resu l t s

SampleConcen .

mg/1

< 046 26

6450

95841

MDLmg/1

045.0

10 0-

2010

NOV 3. 1989

^Bj6r C 1 U ————————————— —— ——————————————————————————————————————————————— — ———————— - ——



Chain of Custody Data Requked tor ETC Data Management Summary Reports

CA2146 WASTE MANAGEMENT. INC. 405 W1GWPIOA 891010 1405 1El»p»«a

ETC Simple No, Company Facility S*np]e Point Date Tine Hour}

Parameter

pH Field stdpH Field stdpH Field stdpH Field stdSpecif ic Conductance Field urn/cmSpecific Conductance Field urn/cmSpecif ic Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. C

roOCD

Resu l t s

SampleMeasure

6.656 686.696.69

1165116511581158

11 .0

MDL

-

OCT 17. 1989

—— ^ •S" c ' c ——————————— ———— ——— —— — —— —————————————TABLE 1: QUANTITATIVE RESULTS and QUALITY ASSURANCE DATA



CA2147 WASTE MANAGEMENT, INC. 405 W1GWP9A 89IOI1 0933 7E j*pt*d

ETC !*"H>1* No, CMWiny Fjcility 3*npl« Point D*te Time Hours

NPOESNumber

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenolics, Total mg/1Cyanide, total mfl/1Total Organic Carbon mg/1Total Organic Carbon mg/1Specific Conductance urn/ cmSpecific Conductance um/cmpH stdpH stdNitrite as N mg/1

roO

RClUltl

SampleConcen.

28 32

< . 1< 05000326 36 4

775.0776 0

6 916 91< . l

WL

1.01

.1.050

01001 01 0

10.010 0

.1

DEC 16. 1989

•

——— ^MgF = C 1 1* ————



CA2147 WASTE MANAGEMENT. INC. 405 W1GWP9A 891011 0933 7E lapsed

ETC Sample No, Company Faci l i ty Ssmpl* Point Da le Time ^••,\,v,

Compound

Ammon i a a 3 NS u l f a t e as S04Bicarbonate as CaCQ3Carbonate as CaC03Nitrogen. Total Kjeldahl (TSolids, to ta l dissolved (RO

roO

Resu l t s

SampleConcert .

mg/1

< .0432.4

3910

.78538

MDLmg/1

045 0

10 0

2010

NOV 3, 1989

———— __fer CIL ——————————————————— ——— —— " —— " — ' - " — ——————————————— •


Field Parameters <QR16)


CA2M7 WASTE MANAGEMENT. INC. 405 W1GWP9A 8910I1 0933 7E lapsed

EIC Sample No. Company Facility Sample Point Oatft Time HOUM

Parameter

pH Field stdpH Field stdpH Field stdpH Field stdSpec i f ic Conductance Field urn/cmSpecif ic Conductance Field urn/cmSpec i f ic Conductance Field urn/cmSpecif ic Conductance Field urn/cmTemperature Deg C

C>

Result s

SampleMeasure

6.846 846.866 85

833833834838

10 9

MDL

-

OCT 16. 1989

-

—— ^_gg^ c , ^ ———————————————— ,. ——— .,.,..,, ——— —— . „ ——— ,.., ——————————————




CA2148 WASTE MANAGEMENT. INC. 405 W1GUB18RR 891011 1440 1

ETC Sample Mo. Company Faci l i ty Sample Poinl Dat* lime Hours

NPDESNumbtr

Chloride mg/1Fluoride mg/1Nitrate as N mg/1Phenolics . T o t a l mg/1Total Organic Carbon mg/1Total Organic Carbon mg/1Spec if ic Conductance urn/ cmSpecif ic Conductance urn/cmpH stdpH stdNitrite as N mg/1

C>

R e s u l t s

SampleConcert .

44 23

< . \< 05075 778.7

929 0929 0

6 686 68< 1

MDL

1 01

. 1.0501 01 0

1 0 01 0 0

1

NOV 27. 1989

-

————— ^^^7 C 1 1 —————



CA2148 WASTE MANAGEMENT, INC. 405 W1GWB18RR 891011 1440 1E 1 Jpiea

ETC Sample Mo. Company Faci l i ty Sample Point D a t e Time Hours

Compound

Ammonia as NSulfate as S04Bicarbonate as CaC03Carbonate as CaC03Nitrogen. Total Kjeldahl (TSolids, total dissolved (RO

ro

en

R e s u l t s

SampleConcert .

mg/1.35

<5.0493

01 50

631

MDLmg/1

045.0

1 0 0

2010

NQV 3. 1989

^ CIL ————————————————————————————————————— ,..«.—" ———————————————————— __ —— - —————




CA2148 WASTE MANAGEMENT. INC. 405 W1GWB18RR 8910M 1440 1El aps«d

ETC S*nple No. Company Facil ity Sample Poini D a t e Time Hours

Parameter

pH Field stdpH Field stdpH Field stdpH Field stdSpeci f ic Conductance Field urn/cmSpec i f ic Conductance Field urn/cmSpeci f ic Conductance Field urn/cmSpec i f ic Conductance Field urn/ cmTemperature Deg. C

OON

Resu l t s

SampleMeasure

7 647.727 . 7 47 . 7 5

1063105310481048

1 0 . 2

MDL

OCT 16. 1989

————— ^K= tlU ———————————————————————— ' ———— • ———— "" —— " -'" ———— " ———— " ————— ""• ———————————————————




CA2152 WASTE MANAGEMENT. INC. 405 X03FB 891010 1227 0

tIC S.w»ple No. Cimiyany Faci l i ly Sample Pvint 0,ne Time M..U

NPDESNumber

Chloride mg/lFluonde mg/lNi t ra te as N mg/lPhenol ics. Total mg/lCyanide . Total mg/lTotal Organic Carbon mg/lTota l Organic Carbon mg/lSpec if ic Conductance um/cmSpecific Conductance um/cmpH ' stdpH stdNi t r i te as N mg/l

roCJ

R e s u l t s

SampleConcen

<1 0< t< 1

< 0500018

<1 0<l 0

7 87 88 028 11< . 1

MDL

1 0. 1

1.05001001 01 0

10 010 0

1

=

NOV 10, 1989

—— ^BF c i u ——TABLE 1: MISCELLANEOUS DATA (QR64)


CA2152 WASTE MANAGEMENT. INC. 405 X03FB 891010 1227 0t U|>

EtC Sdrnple No. Company Fac i l i t y Sample Poml Date lime H'UJ

Compound

Ammonia as NS u l f a t e as 504Bicarbonate as CaC03Carbonate as CaC03Nitrogen. Total Kieldahl (TSolids, total d issolved (RO

C.)oo

Resu l t s

SampleConcen .

mg/1

< 046 11

<10 00

.2421

MDLmg/1

045 .0

1 0 0

2010

'"..

NOV 3. 1989

^ 1C 1 — —————————————— —— ——————— - ————— - ————————————————— — - ————————————— - —————————




CA2152 WASTE MANAGEMENT. INC. 405 X03FB 89I010 1227 0Elipjea

ETC Simple No, Company F»cility Smple Point 0*1* Time Hours

Parameter

pH FieldpH FieldpH FieldpH FieldSpec i f ic (Specific (Specif ic (Specific (Tempera tu

K?

stds tdstdstd

Conductance Field urn/cmConductance Field urn/cmConductance Field um/cmConductance Field um/cmre Oeg. (

Result c

SampleMeasure

6 846.846.866.85

833833834838

10.9

MDL

-

OCT '7. 1989

TECHNICAL MEMORANDUM NO. 3 FOR REMEDIAL … · facility Sample Point Date Time Hours Swep T Davis...

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