Site Visit Report · 2021. 1. 18. · Site Visit Report The site visit process is a sample on a...
Transcript of Site Visit Report · 2021. 1. 18. · Site Visit Report The site visit process is a sample on a...
Site Visit Report
The site visit process is a sample on a particular day of an installation's compliance with some of its licence conditions. Where non-compliance against a particular condition has not been reported, this should not be construed to mean that there is full compliance with that condition of the licence.
Instructions and actions arising from the visit shall be addressed, or where applicable noted, by the licensee in order to ensure compliance, to improve the environmental performance of the installation and to provide clarification on certain issues.
The licensee shall take the actions specified to close out the non-compliances and observations raised in this Site Visit Report.
Licensee
Name of Installation Arrow Group
Licensee Arrow Group Limited
Licence Register No. P0812-01
CRO Number 132776
Site Address The Maudlins Industrial Estate, Naas, Kildare
Site Visit Reference No. SV18614
Report Detail
Issue Date 18/11/2020
Prepared By David Matthews
Site Visit Detail
Date Of Inspection 05/10/2020
Time In 09:30 Time Out 17:00
EPA Inspector(s) David Matthews
Additional Visitors Socotec
Licensee Personnel and Role See report.
Site Visit Report - SV18614 - Arrow Group Limited Page 1 of 134
1. Site Specific Issues
Answer Condition Number
Non Compliance
Observation
1.1 Odour results Checked 11.11 No Yes
Comment / Corrective Action
Sampling for odour (ouE/m³) at the various emission points occurred on the 5th and 19th October. It was noted that on different dates, different concentrations of odour results were reported at the same emission point, e.g. at Aerox 2, the odour results were 771 ouE/m³ and 1077 ouE/m³ on the 5th October, but 115 ouE/m³ on the 19th October.
Corrective Action Required
Please review the report, and provide the Agency with production records for what was being produced at the various emission points at the times and dates of sampling. The licensee shall submit the production records to the Agency as a new licensee return on EDEN by 30/11/20.
Site Areas Inspected
See report.
Documents Inspected
N/A
Summary
This is a technical report containing the results of monitoring of emissions to air. Sampling initially took place on the 5th October, but some sampling had to be repeated on 19th October 2020, because the courier used to ship the samples to the UK lost some of the samples.
Site Visit Report - SV18614 - Arrow Group Limited Page 2 of 134
STACK EMISSIONS MONITORING REPORT
Page 1 of 127
© 2019 SOCOTEC UK Ltd Opinions and interpretations expressed herein are outside the scope of UKAS accreditation. MCERTS accredited results will only be claimed where both the sampling and analytical stages are UKAS accredited. This test report shall not be reproduced, except in full, without written approval of SOCOTEC UK Ltd.
Carried Out By: SOCOTEC 2-4 Langlands Place Kelvin South Business Park East Kilbride G75 0YF
Carried Out For: Office of Environmental Enforcement Environmental Protection Agency McCumiskey House Richview Dublin 14
Monitoring Dates: 5th & 19th October 2020 Report No: P0812-01-CAR20-01 / Version 1 Permit Reference: P0812-01 Report Date: 13/11/2020 Emission Points Monitored:
AE06 - WWtP AE08 – Aerox 3 AE10 – Aerox 1 AE11 – Aerox 2 AE12 – Pasta Concepts Carbon Filter AE13 – Simply Soups Concepts Carbon Filter
Date
Site Operator: Arrow Group Limited The Maudlins Industrial Estate Naas Co Kildare
Site Visit Report - SV18614 - Arrow Group Limited Page 3 of 134
STACK EMISSIONS MONITORING REPORT
Page 2 of 127
SECTION A Emission Point - AE06 - WWtP
Date
Site Operator: Arrow Group Limited The Maudlins Industrial Estate Naas Co Kildare
Site Visit Report - SV18614 - Arrow Group Limited Page 4 of 134
SOCOTEC Job Number:Report Date:Version: 1Report By: Daniel ScullyMCERTS Number: MM 19 1563MCERTS Level: MCERTS Level 1 - Technician Technical Endorsements:
Report Approved By: David HayMCERTS Number: MM 04 552Business Title: MCERTS Level 2 - Buisness ManagerTechnical Endorsements: 1, 2, 3 & 4
Signature:
2-4 Langlands PlaceKelvin South Business Park
East KilbrideG75 0YF
Tel: 01355 246 730Fax: 01355 249 669
Permit Reference:IE Licence: P0812-01
David HayBusiness Manager - North
Tel: 01355 246 730Email: [email protected]
Your contact at SOCOTEC LTD
Operator & Address:
The Maudlins Industrial Estate Naas
Arrow Group Limited
Co Kildare
Release Point: AEP 6 Waste Water Treatment Plant
Sampling Date(s):05/10/2020 & 19/10/2020
28-Oct-20P0812-01CAR20-01
STACK EMISSIONS MONITORING
SOCOTEC UK Reporting Template v6 Page 3 of 127
Site Visit Report - SV18614 - Arrow Group Limited Page 5 of 134
SOCOTEC UK LTD
www.socotec.co.uk
EXECUTIVE SUMMARY
Stack Emissions Monitoring Objectives
- Plant
- Operator
- Stack Emissions Monitoring Test House
Emissions Summary
Monitoring Times
Process Details
Monitoring Methods
Analytical Methods
- Sampling Methods with Subsequent Analysis
- On-Site Testing
Sampling Location
- Sampling Plane Validation Criteria
- Duct Characteristics
- Sampling Lines & Sample Points
- Sampling Platform
- Sampling Location / Platform Improvement Recommendations
Sampling and Analytical Method Deviations
APPENDICES
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
APPENDIX 3 - Measurement Uncertainty Budget Calculations
CONTENTS
Page 4 of 127
Arrow Group LimitedNaasAEP 6 Waste Water Treatment Plant
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 6 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Plant
AEP 6 Waste Water Treatment Plant
Operator
Arrow Group Limited
The Maudlins Industrial Estate
Naas
Co Kildare
IE Licence: P0812-01
Stack Emissions Monitoring Test House
SOCOTEC - East Kilbride Laboratory2-4 Langlands PlaceKelvin South Business ParkEast KilbrideG75 0YFUKAS and MCERTS Accreditation Number: 1015
Opinions and interpretations expressed herein are outside the scope of UKAS accreditation.MCERTS accredited results will only be claimed where both the sampling and analytical stages are UKAS accredited.This test report shall not be reproduced, except in full, without written approval of SOCOTEC LTD.
MONITORING OBJECTIVES
SOCOTEC LTD were commissioned by The Environmental Protection Agency to carry out stack emissions monitoring to determine the release ofprescribed pollutants from the following Plant under normal operating conditions.
Arrow Group Limited operates a waste water treatment process at Naas which is subject to IE Licence P0812-01, under the EPA Act 1992.
EXECUTIVE SUMMARY
The results of these tests shall be used to demonstrate compliance with a set of emission limit values for prescribed pollutants as specified in thePlant's IE Licence, P0812-01.
Page 5 of 127
Arrow Group LimitedNaasAEP 6 Waste Water Treatment Plant
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 7 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Parameter Units Result Calculated Uncertainty
+/-Odour ouE/m³ 405.33 - -Odour Emission Rate ouE/s 1449.56 - -Stack Gas Temperature oC 20 - -Stack Gas Velocity m/s 13.8 0.32 -Gas Volumetric Flow Rate (Actual) m³/hr 13591 689 -Gas Volumetric Flow Rate (STP, Wet) m³/hr 12874 653 -Gas Volumetric Flow Rate (STP, Dry) m³/hr 10299 522 -Gas Volumetric Flow Rate at Reference Conditions m³/hr 12874 653 -
P
MCERTS accredited
result
ND = None Detected,Results at or below the limit of detection are highlighted by bold italic text.The above volumetric flow rate is calculated using data from the preliminary survey. Mass emissions for non isokinetic tests are calculated using these values. For all isokinetic testing the mass emission is calculated using test specific flow data and not the above values.
EXECUTIVE SUMMARY
EMISSIONS SUMMARY
Reference conditions are 273K, 101.3kPa without correction for water vapour
P
Emission Limit Value (ELV)
Page 6 of 127
Arrow Group LimitedNaasAEP 6 Waste Water Treatment Plant
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 8 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Odour Run 1Odour Run 2Odour Run 3
19 October 202012:00 - 12:04
Preliminary Stack Traverse
12:08 - 12:1312:15 - 12:24
19 October 2020 11:51 - 11:59 -
4 minutes5 minutes9 minutes19 October 2020
Sampling TimesSampling Date(s)Parameter
EXECUTIVE SUMMARY
Sampling DurationMONITORING TIMES
19 October 2020
Page 7 of 127
Arrow Group LimitedNaasAEP 6 Waste Water Treatment Plant
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 9 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Description of process Waste Water Treatment
Continuous or batch Continuous
Product Details N/A
Part of batch to be monitored (if applicable) During treatment
Normal load, throughput or continuous rating 100% Loading
Fuel used during monitoring N/A
Abatement Carbon Filter x 2
Plume Appearance None Visible
PROCESS DETAILS
Parameter
EXECUTIVE SUMMARY
Process Details
Page 8 of 127
Arrow Group LimitedNaasAEP 6 Waste Water Treatment Plant
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 10 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Species SOCOTEC UKAS Lab MCERTS Limit of Calculated CalculatedTechnical Number Accredited Detection MU MUProcedure Method (LOD) +/- % Result +/- % ELV
Odour AE 142 1015 Yes - - N/A - No ELV
Velocity AE 154 1015 Yes 5 Pa 2.3% N/A - No ELV
Volumetric Flow Rate
AE 154 1015 Yes - 5.1% N/A - No ELV
EN 13725
EXECUTIVE SUMMARY
Monitoring Methods
MethodStandard Reference Method /
Alternative Method
The selection of standard reference / alternative methods employed by SOCOTEC is determined, wherever possible by the hierarchy of methodselection outlined in Environmental Protection Agency Technical Guidance Note (Monitoring) AG2.
SRM - EN ISO 16911-1
SRM - EN ISO 16911-1
MONITORING METHODS
Page 9 of 127
Arrow Group LimitedNaasAEP 6 Waste Water Treatment Plant
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 11 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Odour olfactometry 2430 Yes Odournet SOCO20X 201006 8 Weeks
Species Analytical UKAS Lab MCERTS Laboratory Data ArchiveProcedure Number Accredited Archive Period
Analysis Location- - - - - - -
EXECUTIVE SUMMARY
Analytical Technique
olfactometry
Analytical Methods
The following tables list the analytical methods employed together with the custody details. Unless otherwise stated the samples are archived at the analysis lab location.
Analysis LabArchivePeriod
Analytical Procedure
Analytical TechniqueUKAS Lab Number
Species
ON-SITE TESTING
-
UKAS Accredited Lab Analysis
Analysis Report number
SAMPLING METHODS WITH SUBSEQUENT ANALYSIS
Page 10 of 127
Arrow Group LimitedNaasAEP 6 Waste Water Treatment Plant
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 12 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Sampling Plane Validation Criteria Value Units Requirement Compliant Method
Lowest Differential Pressure 104 Pa >= 5 Pa Yes EN 15259
Lowest Gas Velocity 12.2 m/s - - -
Highest Gas Velocity 14.9 m/s - - -
Ratio of Gas Velocities 1.2 : 1 < 3 : 1 Yes EN 15259
Mean Velocity 13.8 m/s - - -
Maximum angle of flow with regard to duct axis <15 o < 15o Yes EN 15259
No local negative flow Yes - - Yes EN 15259
Value Units Isokinetic
Shape Circular -
Depth 0.59 m Sample port size 2" BSP -
Width - m Number of lines used 1 -
Area 0.27 m2 Number of points / line 4 -
Port Depth 40 mm Duct orientation Vertical -
Filtration N/A -
General Platform Information
Permanent / Temporary Platform / Ground level / Floor Level / Roof
Inside / Outside
AG1 Platform requirements
Is there a sufficient working area so work can be performed in a compliant manner
Platform has 2 levels of handrails (approximately 0.5 m & 1.0 m high)
Platform has vertical base boards (approximately 0.25 m high)
Platform has removable chains / self closing gates at the top of ladders
Handrail / obstructions do not hamper insertion of sampling equipment
Depth of Platform = >Stack depth / diameter + wall and port thickness + 1.5m
Sampling Platform Improvement Recommendations (if applicable)
SAMPLING PLATFORM
Non-Iso & Gases
Yes
Yes
Yes
The sampling location meets all the requirements as specified in The EPA's Guidance Note AG1.
SAMPLING LOCATION
N/A
DUCT CHARACTERISTICS
EXECUTIVE SUMMARY
Permananet
Yes
Yes
Inside
SAMPLING LINES & POINTS
Page 11 of 127
Arrow Group LimitedNaasAEP 6 Waste Water Treatment Plant
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 13 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Sample Lines
Sampling & Analytical Method Deviations
Only 1 sample line is available for carrying out preliminary velocity and temperature traverse as opposed to the 2 sample lines stated inEN 15259 and EPA's AG1 Guidance.
EXECUTIVE SUMMARY
Page 12 of 127
Arrow Group LimitedNaasAEP 6 Waste Water Treatment Plant
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 14 of 134
SOCOTEC UK LTD
www.socotec.co.uk
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
APPENDIX 3 - Measurement Uncertainty Budget Calculations
APPENDICES
CONTENTS
Page 13 of 127
Arrow Group LimitedNaasAEP 6 Waste Water Treatment Plant
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 15 of 134
SOCOTEC UK LTD
www.socotec.co.uk
SOCOTEC UKAS Lab MCERTSTechnical Number AccreditedProcedure Method
AE 142 1015 Yes 3AE 154 1015 Yes 1Velocity
Species
Odour
SRM - EN ISO 16911-1
Standard Reference Method / Alternative Method
MethodNumber of Samples
EN 13725
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
MONITORING SCHEDULE
Page 14 of 127
Arrow Group LimitedNaasAEP 6 Waste Water Treatment Plant
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 16 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Equipment I.D. Equipment I.D. Equipment I.D.
- - LEK 15.21
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
NOTE: If the equipment I.D is represented by a dash (-), then this piece of equipment has not been used for this test.
Cylinder I.D Number
Supplier ppm %Analytical
Tolerance +/- %
- - - - -
Level Expiry TE1 TE2 TE3 TE4 H&S
Enda Flood MM 12 1170MCERTS Level 2
Apr-23 Mar-24 Mar-24 Jun-23 Nov-23 Apr-23
Aidan Whiteny MM 20 1603MCERTS Trainee
Sep-25 - - - - Sep-25
20m Heated Line (1)
Gas (traceable to ISO 17025)
Barometer
Equipment
Ecophysics NOx Analyser
Heater Controller
Last Impinger Arm
S-Pitot
FT-IR Gasmet
-
Probe JCT Heated Head Filter
Digital Micromanometer
Bernath 3006 FID Protractor
Personnel
CALIBRATION GASES
FTIR Heater Box for Heated Line
1m Heated Line (3)
MONITORING TEAM
10m Heated Line (2)
15m Heated Line (1)
Heated Line Controller (2)
MCERTS Number
TE / H&S Qualifications and Expiry DateMCERTS
Box Thermocouples Tape Measure
Dioxins Cond. Thermocouple 10m Heated Line (1)
Probe Thermocouple
Stackmaster
Meter Out Thermocouple
Control Box Timer
Stack Thermocouple
1m Heated Line (1)
L-Pitot
Oven Box
Control Box DGM
Instrumental Analyser/s
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
CALIBRATEABLE EQUIPMENT CHECKLISTMiscellaneousExtractive Sampling
Equipment
Meter In Thermocouple Stopwatch
Probe
FT-IR Oven Box
Equipment
Horiba PG-250 Analyser
Callipers
20m Heated Line (2)
Anemometer
Chiller (JCT/MAK 10)
MFC Display module
Site Balance
5m Heated Line (1)
Small DGM
Heated Line Controller (1)
Site temperature Logger
Inclinometer (Swirl Device)
STACK EMISSIONS MONITORING TEAM
Laboratory Balance
1m Heated Line (2)
Mass Flow Controller
Thermo FID
Digital Temperature Meter
Servomex
Probe Thermocouple
Signal 3030 FID
Page 15 of 127
Arrow Group LimitedNaasAEP 6 Waste Water Treatment Plant
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 17 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Duration ELV EmissionMinutes ouE/m³ Rate ouE/s
4 - 1015.64
5 - 1941.88
Run 3 9 - 1391.15
Reference conditions are 273K, 101.3kPa without correction for water vapour
Sampling Times
389.00
12:00 - 12:0419 October 2020
Run 1
12:08 - 12:1319 October 2020
284.00
Test
543.00
ouE/m³Concentration
Run 2
12:15 - 12:2419 October 2020
ODOUR SUMMARY
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
Page 16 of 127
Arrow Group LimitedNaasAEP 6 Waste Water Treatment Plant
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 18 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Stack Diameter / Depth, D 0.59 m
Stack Width, W - m
Stack Area, A 0.27 m2
Average stack gas temperature 20 oC
Stack static pressure 0.19 kPa
Barometric Pressure 102.8 kPa
Component Molar Density Conc Dry Volume Dry Conc Conc Wet Volume Wet ConcMass kg/m3 Dry Fraction kg/m3 Wet Fraction kg/m3
M p % Vol r pi % Vol r pi
CO2 44 1.963059 0.028571 0.000286 0.000561 0.022857 0.000229 0.000449
O2 32 1.427679 21.000000 0.210000 0.299813 16.800000 0.168000 0.239850
N2 28 1.249219 78.971429 0.789714 0.986526 63.177143 0.631771 0.789221
H2O 18 0.803070 - - - 20.000000 0.200000 0.160614
Where: p = M / 22.41 pi = r x p
Determinand
Dry Density (STP), P STD
Wet Density (STP), P STW
Dry Density (Actual), P Actual
Average Wet Density (Actual), P ActualW
Where:
P STD = sum of component concentrations, kg/m3 (not including water vapour) P Actual = P STD x (Ts / Ps) x (Pa / Ta)
P STW = (P STD + pi of H2O) / (1 + (pi of H2O / 0.8036)) P ActualW = P STW x (Ts / Ps) x (Pa / Ta)
1.2191
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
1.1901
kg/m31.2869
kg/m3
Stack Characteristics
Result
kg/m3
Stack Gas Composition & Molecular Weights
PRELIMINARY STACK SURVEY
1.127
kg/m3
Units
Calculation of Stack Gas Densities
Page 17 of 127
Arrow Group LimitedNaasAEP 6 Waste Water Treatment Plant
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 19 of 134
SOCOTEC UK LTD
www.socotec.co.uk
TRAVERSE 1
Traverse Distance DP pt DP pt Temp Velocity O2 Angle
Point into Pa mmH2O oC m/s % of Swirl
duct (m)(average of 3
readings)(average of 3
readings)m³/s Vol o
1 0.05 103.9 10.6 20 12.2 3.3 - <152 0.15 131.3 13.4 20 13.8 3.8 - <153 0.44 143.1 14.6 20 14.4 3.9 - <154 0.54 152.9 15.6 20 14.9 4.1 - <15- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -
Mean - 132.8 13.6 20 13.8 3.8 - -
Traverse Distance DP pt DP pt Temp Velocity O2 Angle
Point into Pa mmH2O oC m/s % of Swirl
duct (m)(average of 3
readings)(average of 3
readings)m³/s Vol o
- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -
Mean - - - - - - - -
Start Value End Value Difference Start Value End Value DifferencemmH2O mmH2O % mmH2O mmH2O %
Run 1 122 120 1.6 Pass 134 133 0.7 Pass
RunFinal Reading
(Pa)
Reading After Purge(Pa)
Difference(%)
Outcome(Permitted
+/- 5%)
Run 1 190 194 2.1 Pass
PRELIMINARY STACK SURVEY QUALITY ASSURANCE CHECKLIST
PRELIMINARY STACK SURVEY
Sampling Line A
Outcome
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
Date of Survey
Velocity Measurement Device: L-Type Pitot
To complete a compliant pitot leak check a pressure of over 80 mmH₂O (or 800 Pa) is applied and the pressure drop monitored over 5 mins. A drop of less than 5% must be observed.
Time of Survey
L-Type Pitot Blockage Test
Pre Traverse Leak RateOutcomeRun
PITOT LEAK CHECK
Sampling Line B
11:51 - 11:5919 October 2020
Volumetric Flow Rate
(actual)
Volumetric Flow Rate
(actual)
Post Traverse Leak Rate
Page 18 of 127
Arrow Group LimitedNaasAEP 6 Waste Water Treatment Plant
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 20 of 134
SOCOTEC UK LTD
www.socotec.co.uk
EA Technical Guidance Note (Monitoring) M1 Units Requirement Compliant
Lowest Differential Pressure Pa >= 5 Pa Yes
Lowest Gas Velocity m/s - -
Highest Gas Velocity m/s - -
Ratio of Gas Velocities - < 3 : 1 Yes
Maximum angle of flow with regard to duct axis o < 15o Yes
No local negative flow - - Yes
Velocity at Traverse Point, V = Kpt x (1-e) * Ö(2 * DP pt / P ActualW)
Where:Kpt = Pitot tube calibration coefficient(1-e) = Compressibility correction factor, assumed at a constant 0.998
Average Stack Gas Velocity, Va 13.8 m/s
Duct gas flow conditions Actual Reference UnitsTemperature 20 0 oC
Total Pressure 102.99 101.3 kPaOxygen 21.0 21 %Moisture 20.00 20.00 %Pitot tube calibration coefficient, Kpt 0.90
Gas Volumetric Flowrate Units
Average Stack Gas Velocity (Va) m/s
Stack Area (A) m2
Gas Volumetric Flowrate (Actual), QActual m3/hr
Gas Volumetric Flowrate (STP, Wet), QSTP m3/hr
Gas Volumetric Flowrate (STP, Dry), QSTP,Dry m3/hr
Gas Volumetric Flowrate (REF), QRef m3/hr
Where:QActual = Va x A x 3600QSTP = Q (Actual) x (Ts / Ta) x (Pa / Ps) x 3600QSTP,Dry = Q (STP) / (100 - (100 / Ma)) x 3600
QRef = Q (STP) x ((100 - Ma) / (100 - Ms)) x ((21 - O2a) / (21 - O2s))
Nomenclature:Ts = Absolute Temperature, Standard Conditions, 273 KPs = Absolute Pressure, Standard Conditions, 101.3 kPaTa = Absolute Temperature, Actual Conditions, KPa = Absolute Pressure, Actual Conditions, kPaMa = Water vapour, Actual Conditions, % VolMs = Water vapour, Reference Conditions, % VolO2a = Oxygen, Actual Conditions, % VolO2s = Oxygen, Reference Conditions, % Vol
104
Result
0.27
13591
Result
14.9
Calculation of Stack Gas Velocity, V
Calculation of Stack Gas Volumetric Flowrate, Q
10299
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
Sampling Plane Validation Criteria
<15
12874
12874
13.81
12.2
1.2
PRELIMINARY STACK SURVEY (CONTINUED)
Yes
Page 19 of 127
Arrow Group LimitedNaasAEP 6 Waste Water Treatment Plant
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 21 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Value UnitsStack Depth 0.59 m Sampling Distance Distance into UnitsStack Width - m Point (% of Depth) StackArea 0.27 m2 - - - -
Sampling Distance Distance into SwirlPoint (% of Depth) Stack (m) o
1 8.5 0.05 < 152 25.0 0.15 < 153 75.0 0.44 < 154 91.5 0.54 < 15
- - - -
- - - -
- - - -
- - - -- - - -- - - -
- - - -- - - -
- - - -
- - - -- - - -- - - -
Isokinetic sampling point - - - -Isokinetic sampling points not used - - - -Non Isokinetic/Gases sampling point - - - -
- - - -
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
SAMPLING LOCATION
Non-Isokinetic/Gases Sampling
STACK DIAGRAM
Isokinetic Sampling
Sampling Line A
1
2
3
4
Page 20 of 127
Arrow Group LimitedNaasAEP 6 Waste Water Treatment Plant
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 22 of 134
SOCOTEC UK LTD
www.socotec.co.uk
13.8 m/s13591 m³/hr
Performance Characteristics & Source of Value Units Values Requirement CompliantUncertainty of Local Gas Velocity Determination
Uncertainty of pitot tube coefficient - 0.010
Uncertainty of mean local dynamic pressures - 1.12
Factor loading, function of the number of measurements. 3 readings 0.591 minimum 3 Yes
Range of measurment device pa 1000
Resolution pa 1.00
Calibration uncertainty pa 21.09<1% of Value or 20
Pa whichever is greater
Yes
Drift % range 0.10
Linearity % range 0.06 <2% of value Yes
Uncertainty of gas density determination
Uncertainty of molar mass determination kg/mol 0.00003
Uncertainty of temperature measurement K 1.49 <1% of value Yes
Uncertainty of absolute pressure in the duct pa 525
Uncertainty associated with the estimate of density - 0.007
Uncertainty associated with the measurement of local velocity - 0.0001Uncertainty associated with the measurement of mean velocity - 0.0001
m/s0.160.32
%1.22.3
m³/hr352689
%2.65.1
Expanded Measurement Uncertainty of Volumetric Flow Rate at a 95% Confidence IntervalExpressed as a % of the Measured Volumetric Flow RateExpanded uncertainty at a 95% Confidence Interval
Measured Velocity at Actual Conditions Measured Volumetric Flow rate at Actual Conditions
Measurement Uncertainty - Velocity
Combined uncertaintyExpanded uncertainty at a 95% Confidence Interval
Note - The expanded uncertainty uses a coverage factor of k = 2.
Expanded Measurement Uncertainty of Velocity at a 95% Confidence Interval
Expressed as a % of the Measured VelocityExpanded uncertainty at a 95% Confidence Interval
Measurement Uncertainty Volumetric Flow Rate
Expanded uncertainty at a 95% Confidence Interval
APPENDIX 3 - Measurement Uncertainty Budget Calculations
MEASUREMENT UNCERTAINTY BUDGET - VELOCITY & VOLUMETRIC FLOW RATE
Combined uncertainty
Note - The expanded uncertainty uses a coverage factor of k = 2.
Reference – SOCOTEC Technical Procedure AE150 Estimation of Uncertainty of Measurement
Page 21 of 127
Arrow Group LimitedNaasAEP 6 Waste Water Treatment Plant
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 23 of 134
SOCOTEC UK LTD
www.socotec.co.uk
END OF REPORT
Thank you for choosing SOCOTEC for your environmental monitoring needs. We hope our services have met your requirements and that you are fully satisfied with your experience of working with us, we really do value your custom and would welcome your feedback. We would appreciate it if you could take a
moment to complete a short online questionnaire so that we can improve our operations and address any areas that have not met with your expectations, by clicking on the following
https://www.surveymonkey.co.uk/r/CAE_customer_feedback_weblink
Page 22 of 127
Arrow Group LimitedNaasAEP 6 Waste Water Treatment Plant
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 24 of 134
STACK EMISSIONS MONITORING REPORT
Page 23 of 127
SECTION B Emission Point - AE08 – Aerox 3
Date
Site Operator: Arrow Group Limited The Maudlins Industrial Estate Naas Co Kildare
Site Visit Report - SV18614 - Arrow Group Limited Page 25 of 134
SOCOTEC Job Number:Report Date:
Version: 1Report By: Daniel ScullyMCERTS Number: MM 19 1563MCERTS Level: MCERTS Level 1 - TechnicianTechnical Endorsements:
Report Approved By: David HayMCERTS Number: MM 04 552Business Title: MCERTS Level 2 - Buisness ManagerTechnical Endorsements: 1, 2, 3 & 4
Signature:
2-4 Langlands PlaceKelvin South Business Park
East KilbrideG75 0YF
Tel: 01355 246 730Fax: 01355 249 669
Permit Reference:IE Licence: P0812-01
David HayBusiness Manager - North
Tel: 01355 246 730Email: [email protected]
Your contact at SOCOTEC LTD
Operator & Address:
The Maudlins Industrial Estate Naas
Arrow Group Limited
Co Kildare
Release Point: AEP 8 - Aerox 3
Sampling Date(s):19 October 2020
28-Oct-20P0812-01CAR20-01
STACK EMISSIONS MONITORING REPORT
SOCOTEC UK Reporting Template v6 Page 24 of 127
Site Visit Report - SV18614 - Arrow Group Limited Page 26 of 134
SOCOTEC UK LTD
www.socotec.co.uk
EXECUTIVE SUMMARY
Stack Emissions Monitoring Objectives
- Plant
- Operator
- Stack Emissions Monitoring Test House
Emissions Summary
Monitoring Times
Process Details
Monitoring Methods
Analytical Methods
- Sampling Methods with Subsequent Analysis
- On-Site Testing
Sampling Location
- Sampling Plane Validation Criteria
- Duct Characteristics
- Sampling Lines & Sample Points
- Sampling Platform
- Sampling Location / Platform Improvement Recommendations
Sampling and Analytical Method Deviations
APPENDICES
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
APPENDIX 3 - Measurement Uncertainty Budget Calculations
CONTENTS
Page 25 of 127
Arrow Group LimitedNaasAEP 8 - Aerox 3
P0812-01CAR20-01 / Version 119/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 27 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Plant
AEP 8 - Aerox 3
Operator
Arrow Group Limited
The Maudlins Industrial Estate
Naas
Co Kildare
IE Licence: P0812-01
Stack Emissions Monitoring Test House
SOCOTEC - East Kilbride Laboratory2-4 Langlands PlaceKelvin South Business ParkEast KilbrideG75 0YFUKAS and MCERTS Accreditation Number: 1015
Opinions and interpretations expressed herein are outside the scope of UKAS accreditation.MCERTS accredited results will only be claimed where both the sampling and analytical stages are UKAS accredited.This test report shall not be reproduced, except in full, without written approval of SOCOTEC LTD.
MONITORING OBJECTIVES
SOCOTEC LTD were commissioned by The Environmental Protection Agency to carry out stack emissions monitoring to determine the release ofprescribed pollutants from the following Plant under normal operating conditions.
Arrow Group Limited operates a production of food products from animal raw materials process at Naas which is subject to IE Licence P0812-01, underthe EPA Act 1992.
EXECUTIVE SUMMARY
The results of these tests shall be used to demonstrate compliance with a set of emission limit values for prescribed pollutants as specified in the Plant'sIE Licence, P0812-01.
Page 26 of 127
Arrow Group LimitedNaasAEP 8 - Aerox 3
P0812-01CAR20-01 / Version 119/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 28 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Parameter Units Result Calculated Uncertainty
+/-Odour ouE/m³ 238.00 - -Odour Emission Rate ouE/s 1036.08 - -Stack Gas Temperature oC 19 - -Stack Gas Velocity m/s 5.9 0.15 -Gas Volumetric Flow Rate (Actual) m³/hr 16624 861 -Gas Volumetric Flow Rate (STP, Wet) m³/hr 15672 812 -Gas Volumetric Flow Rate (STP, Dry) m³/hr 12537 649 -Gas Volumetric Flow Rate at Reference Conditions m³/hr 15672 812 -
P
MCERTS accredited
result
ND = None Detected,Results at or below the limit of detection are highlighted by bold italic text.The above volumetric flow rate is calculated using data from the preliminary survey. Mass emissions for non isokinetic tests are calculated using these values. For all isokinetic testing the mass emission is calculated using test specific flow data and not the above values.
EXECUTIVE SUMMARY
EMISSIONS SUMMARY
Reference conditions are 273K, 101.3kPa without correction for water vapour
P
Emission Limit Value (ELV)
Page 27 of 127
Arrow Group LimitedNaasAEP 8 - Aerox 3
P0812-01CAR20-01 / Version 119/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 29 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Odour Run 1 12:51 - 12:45Preliminary Stack Traverse 19 October 2020 12:48-12:53 -
8 minutes
Sampling TimesSampling Date(s)Parameter
EXECUTIVE SUMMARY
Sampling DurationMONITORING TIMES
19 October 2020
Page 28 of 127
Arrow Group LimitedNaasAEP 8 - Aerox 3
P0812-01CAR20-01 / Version 119/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 30 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Description of process Production of food products from animal raw materials
Continuous or batch Continuous
Product Details Food Production - cooking Line
Part of batch to be monitored (if applicable) N/A
Normal load, throughput or continuous rating Continous
Fuel used during monitoring N/A
Abatement Aerox system
Plume Appearance Visible
PROCESS DETAILS
Parameter
EXECUTIVE SUMMARY
Process Details
Page 29 of 127
Arrow Group LimitedNaasAEP 8 - Aerox 3
P0812-01CAR20-01 / Version 119/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 31 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Species SOCOTEC UKAS Lab MCERTS Limit of Calculated CalculatedTechnical Number Accredited Detection MU MUProcedure Method (LOD) +/- % Result +/- % ELV
Odour AE 142 1015 Yes - - N/A - No ELV
Velocity AE 154 1015 Yes 5 Pa 2.5% N/A - No ELV
Volumetric Flow Rate
AE 154 1015 Yes - 5.2% N/A - No ELV
EN 13725
EXECUTIVE SUMMARY
Monitoring Methods
Method
The selection of standard reference / alternative methods employed by SOCOTEC is determined, wherever possible by the hierarchy of method selectionoutlined in Environmental Protection Agency Technical Guidance Note (Monitoring) AG2.
Standard Reference Method / Alternative Method
SRM - EN ISO 16911-1
SRM - EN ISO 16911-1
MONITORING METHODS
Page 30 of 127
Arrow Group LimitedNaasAEP 8 - Aerox 3
P0812-01CAR20-01 / Version 119/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 32 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Odour olfactometry 2430 Yes Odournet SOCO20X 201020 8 Weeks
Species Analytical UKAS Lab MCERTS Laboratory Data Archive
Procedure Number Accredited Archive PeriodAnalysis Location
- - - - - - -
EXECUTIVE SUMMARY
Analytical Technique
olfactometry
Analytical Methods
The following tables list the analytical methods employed together with the custody details. Unless otherwise stated the samples are archived at the analysis lab location.
Analysis LabArchivePeriod
Analytical Procedure
Analytical TechniqueUKAS Lab Number
Species
ON-SITE TESTING
-
UKAS Accredited Lab Analysis
Analysis Report number
SAMPLING METHODS WITH SUBSEQUENT ANALYSIS
Page 31 of 127
Arrow Group LimitedNaasAEP 8 - Aerox 3
P0812-01CAR20-01 / Version 119/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 33 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Sampling Plane Validation Criteria Value Units Requirement Compliant Method
Lowest Differential Pressure 21 Pa >= 5 Pa Yes EN 15259
Lowest Gas Velocity 5.7 m/s - - -
Highest Gas Velocity 6.0 m/s - - -
Ratio of Gas Velocities 1.1 : 1 < 3 : 1 Yes EN 15259
Mean Velocity 5.9 m/s - - -
Maximum angle of flow with regard to duct axis <15 o < 15o Yes EN 15259
No local negative flow Yes - - Yes EN 15259
Value Units Isokinetic
Shape Circular -
Depth 1.00 m Sample port size 1" bsp -
Width - m Number of lines used 1 -
Area 0.79 m2 Number of points / line 1 -
Port Depth 40 mm Duct orientation horizontal/vertical -
Filtration N/A -
General Platform Information
Permanent / Temporary Platform / Ground level / Floor Level / Roof
Inside / Outside
AG1 Platform requirements
Is there a sufficient working area so work can be performed in a compliant manner
Platform has 2 levels of handrails (approximately 0.5 m & 1.0 m high)
Platform has vertical base boards (approximately 0.25 m high)
Platform has removable chains / self closing gates at the top of ladders
Handrail / obstructions do not hamper insertion of sampling equipment
Depth of Platform = >Stack depth / diameter + wall and port thickness + 1.5m
Sampling Platform Improvement Recommendations (if applicable)
SAMPLING PLATFORM
Non-Iso & Gases
N/A
N/A
N/A
The sampling location meets all the requirements as specified in The EPA's Guidance Note AG1.
SAMPLING LOCATION
N/A
DUCT CHARACTERISTICS
EXECUTIVE SUMMARY
Roof Level
Yes
N/A
Outside
SAMPLING LINES & POINTS
Page 32 of 127
Arrow Group LimitedNaasAEP 8 - Aerox 3
P0812-01CAR20-01 / Version 119/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 34 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Sample Lines
Sampling & Analytical Method Deviations
Only 1 sample line is available for carrying out preliminary velocity and temperature traverse as opposed to the 2 sample lines stated in EN15259 and EPA's AG1 Guidance. In addition the sampling point is less than the recommended 5 hydraulic diameters from the exit of theduct and from a bend.
EXECUTIVE SUMMARY
Page 33 of 127
Arrow Group LimitedNaasAEP 8 - Aerox 3
P0812-01CAR20-01 / Version 119/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 35 of 134
SOCOTEC UK LTD
www.socotec.co.uk
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
APPENDIX 3 - Measurement Uncertainty Budget Calculations
APPENDICES
CONTENTS
Page 34 of 127
Arrow Group LimitedNaasAEP 8 - Aerox 3
P0812-01CAR20-01 / Version 119/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 36 of 134
SOCOTEC UK LTD
www.socotec.co.uk
SOCOTEC UKAS Lab MCERTSTechnical Number AccreditedProcedure Method
AE 142 1015 Yes 1AE 154 1015 Yes 1Velocity
Species
Odour
SRM - EN ISO 16911-1
Standard Reference Method / Alternative Method
MethodNumber of Samples
EN 13725
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
MONITORING SCHEDULE
Page 35 of 127
Arrow Group LimitedNaasAEP 8 - Aerox 3
P0812-01CAR20-01 / Version 119/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 37 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Equipment I.D. Equipment I.D. Equipment I.D.
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
NOTE: If the equipment I.D is represented by a dash (-), then this piece of equipment has not been used for this test.
Cylinder I.D Number
Supplier ppm %Analytical
Tolerance +/- %
- - - - -
Level Expiry TE1 TE2 TE3 TE4 H&S
Enda Flood MM 12 1170MCERTS Level
2Apr-23 Mar-24 Mar-24 Jun-23 Nov-23 Apr-23
Aidan Whiteny MM 20 1603MCERTS Trainee
Sep-25 - - - - Sep-25
20m Heated Line (1)
Gas (traceable to ISO 17025)
Barometer
Equipment
Ecophysics NOx Analyser
Heater Controller
Last Impinger Arm
S-Pitot
FT-IR Gasmet
MONITORING TEAM
-
Probe JCT Heated Head Filter
Digital Micromanometer
Bernath 3006 FID Protractor
Personnel
CALIBRATION GASES
FTIR Heater Box for Heated Line
1m Heated Line (3)
10m Heated Line (2)
15m Heated Line (1)
Heated Line Controller (2)
MCERTS Number
TE / H&S Qualifications and Expiry DateMCERTS
Box Thermocouples Tape Measure
Dioxins Cond. Thermocouple 10m Heated Line (1)
Probe Thermocouple
Stackmaster
Meter Out Thermocouple
Control Box Timer
Stack Thermocouple
1m Heated Line (1)
L-Pitot
Oven Box
Control Box DGM
Instrumental Analyser/s
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
CALIBRATEABLE EQUIPMENT CHECKLISTMiscellaneousExtractive Sampling
Equipment
Meter In Thermocouple Stopwatch
Probe
FT-IR Oven Box
Equipment
Horiba PG-250 Analyser
Callipers
20m Heated Line (2)
Anemometer
Chiller (JCT/MAK 10)
MFC Display module
Site Balance
5m Heated Line (1)
Small DGM
Heated Line Controller (1)
Site temperature Logger
Inclinometer (Swirl Device)
STACK EMISSIONS MONITORING TEAM
Laboratory Balance
1m Heated Line (2)
Mass Flow Controller
Thermo FID
Digital Temperature Meter
Servomex
Probe Thermocouple
Signal 3030 FID
Page 36 of 127
Arrow Group LimitedNaasAEP 8 - Aerox 3
P0812-01CAR20-01 / Version 119/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 38 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Duration ELV EmissionMinutes ouE/m³ Rate ouE/s
8 - 1036.08
Reference conditions are 273K, 101.3kPa without correction for water vapour
Sampling Times
12:51 - 12:4519 October 2020
Run 1 238.00
TestouE/m³
Concentration
ODOUR SUMMARY
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
Page 37 of 127
Arrow Group LimitedNaasAEP 8 - Aerox 3
P0812-01CAR20-01 / Version 119/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 39 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Stack Diameter / Depth, D 1.00 m
Stack Width, W - m
Stack Area, A 0.79 m2
Average stack gas temperature 19 oC
Stack static pressure 0.044 kPa
Barometric Pressure 102.1 kPa
Component Molar Density Conc Dry Volume Dry Conc Conc Wet Volume Wet ConcMass kg/m3 Dry Fraction kg/m3 Wet Fraction kg/m3
M p % Vol r pi % Vol r pi
CO2 44 1.963059 0.028571 0.000286 0.000561 0.022857 0.000229 0.000449
O2 32 1.427679 21.000000 0.210000 0.299813 16.800000 0.168000 0.239850
N2 28 1.249219 78.971429 0.789714 0.986526 63.177143 0.631771 0.789221
H2O 18 0.803070 - - - 20.000000 0.200000 0.160614
Where: p = M / 22.41 pi = r x p
Determinand
Dry Density (STP), P STD
Wet Density (STP), P STW
Dry Density (Actual), P Actual
Average Wet Density (Actual), P ActualW
Where:
P STD = sum of component concentrations, kg/m3 (not including water vapour) P Actual = P STD x (Ts / Ps) x (Pa / Ta)
P STW = (P STD + pi of H2O) / (1 + (pi of H2O / 0.8036)) P ActualW = P STW x (Ts / Ps) x (Pa / Ta)
1.2132
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
1.1901
kg/m31.2869
kg/m3
Stack Characteristics
Calculation of Stack Gas DensitiesResult
kg/m3
Stack Gas Composition & Molecular Weights
PRELIMINARY STACK SURVEY
1.122
kg/m3
Units
Page 38 of 127
Arrow Group LimitedNaasAEP 8 - Aerox 3
P0812-01CAR20-01 / Version 119/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 40 of 134
SOCOTEC UK LTD
www.socotec.co.uk
TRAVERSE 1
Traverse Distance DP pt DP pt Temp Velocity O2 Angle
Point into Pa mmH2O oC m/s % of Swirl
duct (m)(average of 3
readings)(average of 3
readings)m³/s Vol o
1 0.07 22.5 2.3 19 5.7 4.5 - <152 0.25 23.8 2.4 19 5.9 4.6 - <153 0.75 23.8 2.4 19 5.9 4.6 - <154 0.93 25.2 2.6 19 6.0 4.7 - <15- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -
Mean - 23.8 2.4 19 5.9 4.6 - -
Traverse Distance DP pt DP pt Temp Velocity O2 Angle
Point into Pa mmH2O oC m/s % of Swirl
duct (m)(average of 3
readings)(average of 3
readings)m³/s Vol o
- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -
Mean - - - - - - - -
Start Value End Value Difference Start Value End Value DifferencemmH2O mmH2O % mmH2O mmH2O %
Run 1 122 120 1.6 Pass 134 133 0.7 Pass
RunFinal Reading
(Pa)
Reading After Purge(Pa)
Difference(%)
Outcome(Permitted
+/- 5%)
Run 1 44 43 -2.3 Pass
PRELIMINARY STACK SURVEY QUALITY ASSURANCE CHECKLIST
PRELIMINARY STACK SURVEY
Sampling Line A
Outcome
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
Date of Survey
Velocity Measurement Device:
Volumetric Flow Rate
(actual)
L-Type PitotTime of Survey
L-Type Pitot Blockage Test
Pre Traverse Leak RateOutcomeRun
PITOT LEAK CHECK
To complete a compliant pitot leak check a pressure of over 80 mmH₂O (or 800 Pa) is applied and the pressure drop monitored over 5 mins. A drop of less than 5% must be observed.
Sampling Line B
12:48-12:5319 October 2020
Volumetric Flow Rate
(actual)
Post Traverse Leak Rate
Page 39 of 127
Arrow Group LimitedNaasAEP 8 - Aerox 3
P0812-01CAR20-01 / Version 119/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 41 of 134
SOCOTEC UK LTD
www.socotec.co.uk
EA Technical Guidance Note (Monitoring) M1 Units Requirement Compliant
Lowest Differential Pressure Pa >= 5 Pa Yes
Lowest Gas Velocity m/s - -
Highest Gas Velocity m/s - -
Ratio of Gas Velocities - < 3 : 1 Yes
Maximum angle of flow with regard to duct axis o < 15o Yes
No local negative flow - - Yes
Velocity at Traverse Point, V = Kpt x (1-e) * Ö(2 * DP pt / P ActualW)
Where:Kpt = Pitot tube calibration coefficient(1-e) = Compressibility correction factor, assumed at a constant 0.998
Average Stack Gas Velocity, Va 5.9 m/s
Duct gas flow conditions Actual Reference UnitsTemperature 19 0 oC
Total Pressure 102.144 101.3 kPaOxygen 21.0 21 %Moisture 20.00 20.00 %Pitot tube calibration coefficient, Kpt 0.90
Gas Volumetric Flowrate Units
Average Stack Gas Velocity (Va) m/s
Stack Area (A) m2
Gas Volumetric Flowrate (Actual), QActual m3/hr
Gas Volumetric Flowrate (STP, Wet), QSTP m3/hr
Gas Volumetric Flowrate (STP, Dry), QSTP,Dry m3/hr
Gas Volumetric Flowrate (REF), QRef m3/hr
Where:QActual = Va x A x 3600QSTP = Q (Actual) x (Ts / Ta) x (Pa / Ps) x 3600QSTP,Dry = Q (STP) / (100 - (100 / Ma)) x 3600
QRef = Q (STP) x ((100 - Ma) / (100 - Ms)) x ((21 - O2a) / (21 - O2s))
Nomenclature:Ts = Absolute Temperature, Standard Conditions, 273 KPs = Absolute Pressure, Standard Conditions, 101.3 kPaTa = Absolute Temperature, Actual Conditions, KPa = Absolute Pressure, Actual Conditions, kPaMa = Water vapour, Actual Conditions, % VolMs = Water vapour, Reference Conditions, % VolO2a = Oxygen, Actual Conditions, % VolO2s = Oxygen, Reference Conditions, % Vol
23
Result
0.79
16624
Result
6.0
Calculation of Stack Gas Velocity, V
Calculation of Stack Gas Volumetric Flowrate, Q
12537
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
Sampling Plane Validation Criteria
<15
15672
15672
5.88
5.7
1.1
PRELIMINARY STACK SURVEY (CONTINUED)
Yes
Page 40 of 127
Arrow Group LimitedNaasAEP 8 - Aerox 3
P0812-01CAR20-01 / Version 119/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 42 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Value UnitsStack Depth 1.00 m Sampling Distance Distance into Units
Stack Width - m Point (% of Depth) StackArea 0.79 m2 - - - -
Sampling Distance Distance into SwirlPoint (% of Depth) Stack (m) o
1 6.7 0.07 < 152 25.0 0.25 < 153 75.0 0.75 < 154 93.3 0.93 < 15
- - - -
- - - -
- - - -
- - - -- - - -- - - -
- - - -
- - - -
- - - -
- - - -
- - - -- - - -
Isokinetic sampling point - - - -Isokinetic sampling points not used - - - -Non Isokinetic/Gases sampling point - - - -
- - - -
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
SAMPLING LOCATION
Non-Isokinetic/Gases Sampling
STACK DIAGRAM
Isokinetic Sampling
Sampling Line A
1
2
3
4
Page 41 of 127
Arrow Group LimitedNaasAEP 8 - Aerox 3
P0812-01CAR20-01 / Version 119/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 43 of 134
SOCOTEC UK LTD
www.socotec.co.uk
5.9 m/s
16624 m³/hr
Performance Characteristics & Source of Value Units Values Requirement CompliantUncertainty of Local Gas Velocity Determination
Uncertainty of pitot tube coefficient - 0.010
Uncertainty of mean local dynamic pressures - 0.42
Factor loading, function of the number of measurements. 3 readings 0.591 minimum 3 Yes
Range of measurment device pa 1000
Resolution pa 1.00
Calibration uncertainty pa 5.40<1% of Value or 20
Pa whichever is greater
Yes
Drift % range 0.10
Linearity % range 0.06 <2% of value Yes
Uncertainty of gas density determination
Uncertainty of molar mass determination kg/mol 0.00003
Uncertainty of temperature measurement K 1.49 <1% of value Yes
Uncertainty of absolute pressure in the duct pa 521
Uncertainty associated with the estimate of density - 0.007
Uncertainty associated with the measurement of local velocity - 0.0001
Uncertainty associated with the measurement of mean velocity - 0.0002
m/s0.08
0.15
%1.3
2.5
m³/hr439861
%2.65.2
Expanded Measurement Uncertainty of Volumetric Flow Rate at a 95% Confidence IntervalExpressed as a % of the Measured Volumetric Flow RateExpanded uncertainty at a 95% Confidence Interval
Measured Velocity at Actual Conditions
Measured Volumetric Flow rate at Actual Conditions
Measurement Uncertainty - Velocity
Combined uncertainty
Expanded uncertainty at a 95% Confidence Interval
Note - The expanded uncertainty uses a coverage factor of k = 2.
Expanded Measurement Uncertainty of Velocity at a 95% Confidence Interval
Expressed as a % of the Measured Velocity
Expanded uncertainty at a 95% Confidence Interval
Measurement Uncertainty Volumetric Flow Rate
Expanded uncertainty at a 95% Confidence Interval
APPENDIX 3 - Measurement Uncertainty Budget Calculations
MEASUREMENT UNCERTAINTY BUDGET - VELOCITY & VOLUMETRIC FLOW RATE
Combined uncertainty
Note - The expanded uncertainty uses a coverage factor of k = 2.
Reference – SOCOTEC Technical Procedure AE150 Estimation of Uncertainty of Measurement
Page 42 of 127
Arrow Group LimitedNaasAEP 8 - Aerox 3
P0812-01CAR20-01 / Version 119/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 44 of 134
SOCOTEC UK LTD
www.socotec.co.uk
END OF REPORT
Thank you for choosing SOCOTEC for your environmental monitoring needs. We hope our services have met your requirements and that you are fully satisfied with your experience of working with us, we really do value your custom and would welcome your feedback. We would appreciate it if you could take a moment to
complete a short online questionnaire so that we can improve our operations and address any areas that have not met with your expectations, by clicking on the following
https://www.surveymonkey.co.uk/r/CAE_customer_feedback_weblink
Page 43 of 127
Arrow Group LimitedNaasAEP 8 - Aerox 3
P0812-01CAR20-01 / Version 119/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 45 of 134
STACK EMISSIONS MONITORING REPORT
Page 44 of 127
SECTION C Emission Point - AE10 – Aerox 1
Date
Site Operator: Arrow Group Limited The Maudlins Industrial Estate Naas Co Kildare
Site Visit Report - SV18614 - Arrow Group Limited Page 46 of 134
SOCOTEC Job Number:Report Date:Version: 1Report By: Daniel ScullyMCERTS Number: MM 19 1563MCERTS Level: MCERTS Level 1 - TechnicianTechnical Endorsements:
Report Approved By: David HayMCERTS Number: MM 04 552Business Title: MCERTS Level 2 - Buisness ManagerTechnical Endorsements: 1, 2, 3 & 4
Signature:
2-4 Langlands PlaceKelvin South Business Park
East KilbrideG75 0YF
Tel: 01355 246 730Fax: 01355 249 669
Permit Reference:IE Licence: P0812-01
David HayBusiness Manager - North
Tel: 01355 246 730Email: [email protected]
Your contact at SOCOTEC LTD
Operator & Address:
The Maudlins Industrial Estate Naas
Arrow Group Limited
Co Kildare
Release Point: AEP 10 - Aerox1
Sampling Date(s):05 October 2020
28-Oct-20P0812-01CAR20-01
STACK EMISSIONS MONITORING
SOCOTEC UK Reporting Template v6 Page 1 of 127
Site Visit Report - SV18614 - Arrow Group Limited Page 47 of 134
SOCOTEC UK LTD
www.socotec.co.uk
EXECUTIVE SUMMARY
Stack Emissions Monitoring Objectives
- Plant
- Operator
- Stack Emissions Monitoring Test House
Emissions Summary
Monitoring Times
Process Details
Monitoring Methods
Analytical Methods
- Sampling Methods with Subsequent Analysis
- On-Site Testing
Sampling Location
- Sampling Plane Validation Criteria
- Duct Characteristics
- Sampling Lines & Sample Points
- Sampling Platform
- Sampling Location / Platform Improvement Recommendations
Sampling and Analytical Method Deviations
APPENDICES
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
APPENDIX 3 - Measurement Uncertainty Budget Calculations
CONTENTS
Page 2 of 127
Arrow Group LimitedNaasAEP 10 - Aerox1
P0812-01CAR20-01 / Version 105/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 48 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Plant
AEP 10 - Aerox1
Operator
Arrow Group Limited
The Maudlins Industrial Estate
Naas
Co Kildare
IE Licence: P0812-01
Stack Emissions Monitoring Test House
SOCOTEC - East Kilbride Laboratory2-4 Langlands PlaceKelvin South Business ParkEast KilbrideG75 0YFUKAS and MCERTS Accreditation Number: 1015
Opinions and interpretations expressed herein are outside the scope of UKAS accreditation.MCERTS accredited results will only be claimed where both the sampling and analytical stages are UKAS accredited.This test report shall not be reproduced, except in full, without written approval of SOCOTEC LTD.
MONITORING OBJECTIVES
SOCOTEC LTD were commissioned by The Environmental Protection Agency to carry out stack emissions monitoring to determine the release ofprescribed pollutants from the following Plant under normal operating conditions.
Arrow Group Limited operates a production of food products from animal raw materials process at Naas which is subject to IE Licence P0812-01, underthe EPA Act 1992.
EXECUTIVE SUMMARY
The results of these tests shall be used to demonstrate compliance with a set of emission limit values for prescribed pollutants as specified in thePlant's IE Licence, P0812-01.
Page 3 of 127
Arrow Group LimitedNaasAEP 10 - Aerox1
P0812-01CAR20-01 / Version 105/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 49 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Parameter Units Result Calculated Uncertainty
+/-Odour ouE/m³ 966.00 - -Odour Emission Rate ouE/s 5530.58 - -Stack Gas Temperature oC 62 - -Stack Gas Velocity m/s 7.4 0.17 -Gas Volumetric Flow Rate (Actual) m³/hr 25289 1286 -Gas Volumetric Flow Rate (STP, Wet) m³/hr 20611 1048 -Gas Volumetric Flow Rate (STP, Dry) m³/hr 16489 839 -Gas Volumetric Flow Rate at Reference Conditions m³/hr 20611 1048 -
P
MCERTS accredited
result
ND = None Detected,Results at or below the limit of detection are highlighted by bold italic text.The above volumetric flow rate is calculated using data from the preliminary survey. Mass emissions for non isokinetic tests are calculated using these values. For all isokinetic testing the mass emission is calculated using test specific flow data and not the above values.
EXECUTIVE SUMMARY
EMISSIONS SUMMARY
Reference conditions are 273K, 101.3kPa without correction for water vapour
P
Emission Limit Value (ELV)
Page 4 of 127
Arrow Group LimitedNaasAEP 10 - Aerox1
P0812-01CAR20-01 / Version 105/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 50 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Odour Run 1Odour Run 2Odour Run 3
05 October 202010:16 - 10:28
Preliminary Stack Traverse
10:29 - 10:3210:34 - 10:38
05 October 2020 10:14-10:22 -
12 minutes3 minutes4 minutes05 October 2020
Sampling TimesSampling Date(s)Parameter
EXECUTIVE SUMMARY
Sampling DurationMONITORING TIMES
05 October 2020
Page 5 of 127
Arrow Group LimitedNaasAEP 10 - Aerox1
P0812-01CAR20-01 / Version 105/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 51 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Description of process Production of food products from animal raw materials
Continuous or batch Continuous
Product Details Food Production - cooking Line
Part of batch to be monitored (if applicable) N/A
Normal load, throughput or continuous rating Continous
Fuel used during monitoring N/A
Abatement Aerox system
Plume Appearance Visible
PROCESS DETAILS
Parameter
EXECUTIVE SUMMARY
Process Details
Page 6 of 127
Arrow Group LimitedNaasAEP 10 - Aerox1
P0812-01CAR20-01 / Version 105/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 52 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Species SOCOTEC UKAS Lab MCERTS Limit of Calculated CalculatedTechnical Number Accredited Detection MU MUProcedure Method (LOD) +/- % Result +/- % ELV
Odour AE 142 1015 Yes - - N/A - No ELV
Velocity AE 154 1015 Yes 5 Pa 2.3% N/A - No ELV
Volumetric Flow Rate
AE 154 1015 Yes - 5.1% N/A - No ELV
EN 13725
EXECUTIVE SUMMARY
Monitoring Methods
Method
The selection of standard reference / alternative methods employed by SOCOTEC is determined, wherever possible by the hierarchy of methodselection outlined in Environmental Protection Agency Technical Guidance Note (Monitoring) AG2.
Standard Reference Method / Alternative Method
SRM - EN ISO 16911-1
SRM - EN ISO 16911-1
MONITORING METHODS
Page 7 of 127
Arrow Group LimitedNaasAEP 10 - Aerox1
P0812-01CAR20-01 / Version 105/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 53 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Odour olfactometry 2430 Yes Odournet SOCO20X 201006 8 Weeks
- - - - - - -
Species Analytical UKAS Lab MCERTS Laboratory Data ArchiveProcedure Number Accredited Archive Period
Analysis Location- - - - - - -
EXECUTIVE SUMMARY
Analytical Technique
-
olfactometry
Analytical Methods
The following tables list the analytical methods employed together with the custody details. Unless otherwise stated the samples are archived at the analysis lab location.
Analysis LabArchivePeriod
Analytical Procedure
Analytical TechniqueUKAS Lab Number
Species
ON-SITE TESTING
-
UKAS Accredited Lab Analysis
Analysis Report number
SAMPLING METHODS WITH SUBSEQUENT ANALYSIS
Page 8 of 127
Arrow Group LimitedNaasAEP 10 - Aerox1
P0812-01CAR20-01 / Version 105/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 54 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Sampling Plane Validation Criteria Value Units Requirement Compliant Method
Lowest Differential Pressure 28 Pa >= 5 Pa Yes EN 15259
Lowest Gas Velocity 7.2 m/s - - -
Highest Gas Velocity 7.5 m/s - - -
Ratio of Gas Velocities 1.1 : 1 < 3 : 1 Yes EN 15259
Mean Velocity 7.4 m/s - - -
Maximum angle of flow with regard to duct axis <15 o < 15o Yes EN 15259
No local negative flow Yes - - Yes EN 15259
Value Units Isokinetic
Shape Circular -
Depth 1.10 m Sample port size 1" bsp -
Width - m Number of lines used 1 -
Area 0.95 m2 Number of points / line 1 -
Port Depth 40 mm Duct orientation horizontal/vertical -
Filtration N/A -
General Platform Information
Permanent / Temporary Platform / Ground level / Floor Level / Roof
Inside / Outside
AG1 Platform requirements
Is there a sufficient working area so work can be performed in a compliant manner
Platform has 2 levels of handrails (approximately 0.5 m & 1.0 m high)
Platform has vertical base boards (approximately 0.25 m high)
Platform has removable chains / self closing gates at the top of ladders
Handrail / obstructions do not hamper insertion of sampling equipment
Depth of Platform = >Stack depth / diameter + wall and port thickness + 1.5m
Sampling Platform Improvement Recommendations (if applicable)
SAMPLING PLATFORM
Non-Iso & Gases
N/A
N/A
N/A
The sampling location meets all the requirements as specified in The EPA's Guidance Note AG1.
SAMPLING LOCATION
N/A
DUCT CHARACTERISTICS
EXECUTIVE SUMMARY
Roof Level
Yes
N/A
Outside
SAMPLING LINES & POINTS
Page 9 of 127
Arrow Group LimitedNaasAEP 10 - Aerox1
P0812-01CAR20-01 / Version 105/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 55 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Sample Lines
Sampling & Analytical Method Deviations
Only 1 sample line is available for carrying out preliminary velocity and temperature traverse as opposed to the 2 sample lines stated inEN 15259 and EPA's AG1 Guidance. In addition the sampling point is less than the recommended 5 hydraulic diameters from the exit ofthe duct and from a bend.
EXECUTIVE SUMMARY
Page 10 of 127
Arrow Group LimitedNaasAEP 10 - Aerox1
P0812-01CAR20-01 / Version 105/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 56 of 134
SOCOTEC UK LTD
www.socotec.co.uk
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
APPENDIX 3 - Measurement Uncertainty Budget Calculations
APPENDICES
CONTENTS
Page 11 of 127
Arrow Group LimitedNaasAEP 10 - Aerox1
P0812-01CAR20-01 / Version 105/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 57 of 134
SOCOTEC UK LTD
www.socotec.co.uk
SOCOTEC UKAS Lab MCERTSTechnical Number AccreditedProcedure Method
AE 142 1015 Yes 3AE 154 1015 Yes 1Velocity
Species
Odour
SRM - EN ISO 16911-1
Standard Reference Method / Alternative Method
MethodNumber of Samples
EN 13725
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
MONITORING SCHEDULE
Page 12 of 127
Arrow Group LimitedNaasAEP 10 - Aerox1
P0812-01CAR20-01 / Version 105/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 58 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Equipment I.D. Equipment I.D. Equipment I.D.
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
NOTE: If the equipment I.D is represented by a dash (-), then this piece of equipment has not been used for this test.
Cylinder I.D Number
Supplier ppm %Analytical
Tolerance +/- %
- - - - -
Level Expiry TE1 TE2 TE3 TE4 H&S
Enda Flood MM 12 1170MCERTS Level 2
Apr-23 Mar-24 Mar-24 Jun-23 Nov-23 Apr-23
Aidan Whiteny MM 20 1603MCERTS Trainee
Sep-25 - - - - Sep-25
20m Heated Line (1)
Gas (traceable to ISO 17025)
Barometer
Equipment
Ecophysics NOx Analyser
Heater Controller
Last Impinger Arm
S-Pitot
FT-IR Gasmet
MONITORING TEAM
-
Probe JCT Heated Head Filter
Digital Micromanometer
Bernath 3006 FID Protractor
Personnel
CALIBRATION GASES
FTIR Heater Box for Heated Line
1m Heated Line (3)
10m Heated Line (2)
15m Heated Line (1)
Heated Line Controller (2)
MCERTS Number
TE / H&S Qualifications and Expiry DateMCERTS
Box Thermocouples Tape Measure
Dioxins Cond. Thermocouple 10m Heated Line (1)
Probe Thermocouple
Stackmaster
Meter Out Thermocouple
Control Box Timer
Stack Thermocouple
1m Heated Line (1)
L-Pitot
Oven Box
Control Box DGM
Instrumental Analyser/s
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
CALIBRATEABLE EQUIPMENT CHECKLISTMiscellaneousExtractive Sampling
Equipment
Meter In Thermocouple Stopwatch
Probe
FT-IR Oven Box
Equipment
Horiba PG-250 Analyser
Callipers
20m Heated Line (2)
Anemometer
Chiller (JCT/MAK 10)
MFC Display module
Site Balance
5m Heated Line (1)
Small DGM
Heated Line Controller (1)
Site temperature Logger
Inclinometer (Swirl Device)
STACK EMISSIONS MONITORING TEAM
Laboratory Balance
1m Heated Line (2)
Mass Flow Controller
Thermo FID
Digital Temperature Meter
Servomex
Probe Thermocouple
Signal 3030 FID
Page 13 of 127
Arrow Group LimitedNaasAEP 10 - Aerox1
P0812-01CAR20-01 / Version 105/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 59 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Duration ELV EmissionMinutes ouE/m³ Rate ouE/s
12 - 5627.91
3 - 6847.39
Run 3 4 - 4116.45
Reference conditions are 273K, 101.3kPa without correction for water vapour
Leak Test Results
m³ l/min l/min l/min l/min
Run 1 10.0 0.8 0.00 0.00 0.02 Yes
Run 2 10.0 3.3 0.00 0.00 0.07 Yes
Run 3 10.0 2.5 0.00 0.00 0.05 Yes
Leak Tests Acceptable?
Sampling Times
719.00
10:16 - 10:2805 October 2020
Run 1
Acceptable leak rate
Test
10:29 - 10:3205 October 2020
ouE/m³
Run 2
983.00
1196.00
Mean Sampling Rate
Concentration
Post sampling leak rate
10:34 - 10:3805 October 2020
ODOUR QUALITY ASSURANCE CHECKLIST
Total Sample Volume @ ref
Conditions
Pre sampling leak rate
ODOUR SUMMARY
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
Page 14 of 127
Arrow Group LimitedNaasAEP 10 - Aerox1
P0812-01CAR20-01 / Version 105/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 60 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Stack Diameter / Depth, D 1.10 m
Stack Width, W - m
Stack Area, A 0.95 m2
Average stack gas temperature 62 oC
Stack static pressure 0.01 kPa
Barometric Pressure 101.3 kPa
Component Molar Density Conc Dry Volume Dry Conc Conc Wet Volume Wet ConcMass kg/m3 Dry Fraction kg/m3 Wet Fraction kg/m3
M p % Vol r pi % Vol r pi
CO2 44 1.963059 0.028571 0.000286 0.000561 0.022857 0.000229 0.000449
O2 32 1.427679 21.000000 0.210000 0.299813 16.800000 0.168000 0.239850
N2 28 1.249219 78.971429 0.789714 0.986526 63.177143 0.631771 0.789221
H2O 18 0.803070 - - - 20.000000 0.200000 0.160614
Where: p = M / 22.41 pi = r x p
Determinand
Dry Density (STP), P STD
Wet Density (STP), P STW
Dry Density (Actual), P Actual
Average Wet Density (Actual), P ActualW
Where:
P STD = sum of component concentrations, kg/m3 (not including water vapour) P Actual = P STD x (Ts / Ps) x (Pa / Ta)
P STW = (P STD + pi of H2O) / (1 + (pi of H2O / 0.8036)) P ActualW = P STW x (Ts / Ps) x (Pa / Ta)
1.0488
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
1.1901
kg/m31.2869
kg/m3
Stack Characteristics
Calculation of Stack Gas DensitiesResult
kg/m3
Stack Gas Composition & Molecular Weights
PRELIMINARY STACK SURVEY
0.970
kg/m3
Units
Page 15 of 127
Arrow Group LimitedNaasAEP 10 - Aerox1
P0812-01CAR20-01 / Version 105/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 61 of 134
SOCOTEC UK LTD
www.socotec.co.uk
TRAVERSE 1
Traverse Distance DP pt DP pt Temp Velocity O2 Angle
Point into Pa mmH2O oC m/s % of Swirl
duct (m)(average of 3
readings)(average of 3
readings)m³/s Vol o
1 0.07 30.7 3.1 62 7.2 6.8 - <152 0.28 32.7 3.3 62 7.4 7.0 - <153 0.83 33.0 3.4 62 7.4 7.1 - <154 1.03 34.0 3.5 62 7.5 7.2 - <15- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -
Mean - 32.6 3.3 62 7.4 7.0 - -
Traverse Distance DP pt DP pt Temp Velocity O2 Angle
Point into Pa mmH2O oC m/s % of Swirl
duct (m)(average of 3
readings)(average of 3
readings)m³/s Vol o
- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -
Mean - - - - - - - -
Start Value End Value Difference Start Value End Value DifferencemmH2O mmH2O % mmH2O mmH2O %
Run 1 122 120 1.6 Pass 134 133 0.7 Pass
RunFinal Reading
(Pa)
Reading After Purge(Pa)
Difference(%)
Outcome(Permitted
+/- 5%)
Run 1 10 10 0.0 Pass
PRELIMINARY STACK SURVEY QUALITY ASSURANCE CHECKLIST
PRELIMINARY STACK SURVEY
Sampling Line A
Outcome
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
Date of Survey
Velocity Measurement Device:
Volumetric Flow Rate
(actual)
L-Type PitotTime of Survey
L-Type Pitot Blockage Test
Pre Traverse Leak RateOutcomeRun
PITOT LEAK CHECK
To complete a compliant pitot leak check a pressure of over 80 mmH₂O (or 800 Pa) is applied and the pressure drop monitored over 5 mins. A drop of less than 5% must be observed.
Sampling Line B
10:14-10:2205 October 2020
Volumetric Flow Rate
(actual)
Post Traverse Leak Rate
Page 16 of 127
Arrow Group LimitedNaasAEP 10 - Aerox1
P0812-01CAR20-01 / Version 105/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 62 of 134
SOCOTEC UK LTD
www.socotec.co.uk
EA Technical Guidance Note (Monitoring) M1 Units Requirement Compliant
Lowest Differential Pressure Pa >= 5 Pa Yes
Lowest Gas Velocity m/s - -
Highest Gas Velocity m/s - -
Ratio of Gas Velocities - < 3 : 1 Yes
Maximum angle of flow with regard to duct axis o < 15o Yes
No local negative flow - - Yes
Velocity at Traverse Point, V = Kpt x (1-e) * Ö(2 * DP pt / P ActualW)
Where:Kpt = Pitot tube calibration coefficient(1-e) = Compressibility correction factor, assumed at a constant 0.998
Average Stack Gas Velocity, Va 7.4 m/s
Duct gas flow conditions Actual Reference UnitsTemperature 62 0 oC
Total Pressure 101.31 101.3 kPaOxygen 21.0 21 %Moisture 20.00 20.00 %Pitot tube calibration coefficient, Kpt 0.90
Gas Volumetric Flowrate Units
Average Stack Gas Velocity (Va) m/s
Stack Area (A) m2
Gas Volumetric Flowrate (Actual), QActual m3/hr
Gas Volumetric Flowrate (STP, Wet), QSTP m3/hr
Gas Volumetric Flowrate (STP, Dry), QSTP,Dry m3/hr
Gas Volumetric Flowrate (REF), QRef m3/hr
Where:QActual = Va x A x 3600QSTP = Q (Actual) x (Ts / Ta) x (Pa / Ps) x 3600QSTP,Dry = Q (STP) / (100 - (100 / Ma)) x 3600
QRef = Q (STP) x ((100 - Ma) / (100 - Ms)) x ((21 - O2a) / (21 - O2s))
Nomenclature:Ts = Absolute Temperature, Standard Conditions, 273 KPs = Absolute Pressure, Standard Conditions, 101.3 kPaTa = Absolute Temperature, Actual Conditions, KPa = Absolute Pressure, Actual Conditions, kPaMa = Water vapour, Actual Conditions, % VolMs = Water vapour, Reference Conditions, % VolO2a = Oxygen, Actual Conditions, % VolO2s = Oxygen, Reference Conditions, % Vol
31
Result
0.95
25289
Result
7.5
Calculation of Stack Gas Velocity, V
Calculation of Stack Gas Volumetric Flowrate, Q
16489
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
Sampling Plane Validation Criteria
<15
20611
20611
7.39
7.2
1.1
PRELIMINARY STACK SURVEY (CONTINUED)
Yes
Page 17 of 127
Arrow Group LimitedNaasAEP 10 - Aerox1
P0812-01CAR20-01 / Version 105/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 63 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Value UnitsStack Depth 1.10 m Sampling Distance Distance into UnitsStack Width - m Point (% of Depth) StackArea 0.95 m2 - - - -
Sampling Distance Distance into SwirlPoint (% of Depth) Stack (m) o
1 6.7 0.07 < 152 25.0 0.28 < 153 75.0 0.83 < 154 93.3 1.03 < 15
- - - -
- - - -
- - - -
- - - -- - - -- - - -
- - - -- - - -
- - - -
- - - -- - - -- - - -
Isokinetic sampling point - - - -Isokinetic sampling points not used - - - -Non Isokinetic/Gases sampling point - - - -
- - - -
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
SAMPLING LOCATION
Non-Isokinetic/Gases Sampling
STACK DIAGRAM
Isokinetic Sampling
Sampling Line A
1
2
3
4
Page 18 of 127
Arrow Group LimitedNaasAEP 10 - Aerox1
P0812-01CAR20-01 / Version 105/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 64 of 134
SOCOTEC UK LTD
www.socotec.co.uk
7.4 m/s25289 m³/hr
Performance Characteristics & Source of Value Units Values Requirement CompliantUncertainty of Local Gas Velocity Determination
Uncertainty of pitot tube coefficient - 0.010
Uncertainty of mean local dynamic pressures - 0.46
Factor loading, function of the number of measurements. 3 readings 0.591 minimum 3 Yes
Range of measurment device pa 1000
Resolution pa 1.00
Calibration uncertainty pa 6.65<1% of Value or 20
Pa whichever is greater
Yes
Drift % range 0.10
Linearity % range 0.06 <2% of value Yes
Uncertainty of gas density determination
Uncertainty of molar mass determination kg/mol 0.00003
Uncertainty of temperature measurement K 1.71 <1% of value Yes
Uncertainty of absolute pressure in the duct pa 517
Uncertainty associated with the estimate of density - 0.008
Uncertainty associated with the measurement of local velocity - 0.0001Uncertainty associated with the measurement of mean velocity - 0.0001
m/s0.090.17
%1.22.3
m³/hr656
1286
%2.65.1
Expanded Measurement Uncertainty of Volumetric Flow Rate at a 95% Confidence IntervalExpressed as a % of the Measured Volumetric Flow RateExpanded uncertainty at a 95% Confidence Interval
Measured Velocity at Actual Conditions Measured Volumetric Flow rate at Actual Conditions
Measurement Uncertainty - Velocity
Combined uncertaintyExpanded uncertainty at a 95% Confidence Interval
Note - The expanded uncertainty uses a coverage factor of k = 2.
Expanded Measurement Uncertainty of Velocity at a 95% Confidence Interval
Expressed as a % of the Measured VelocityExpanded uncertainty at a 95% Confidence Interval
Measurement Uncertainty Volumetric Flow Rate
Expanded uncertainty at a 95% Confidence Interval
APPENDIX 3 - Measurement Uncertainty Budget Calculations
MEASUREMENT UNCERTAINTY BUDGET - VELOCITY & VOLUMETRIC FLOW RATE
Combined uncertainty
Note - The expanded uncertainty uses a coverage factor of k = 2.
Reference – SOCOTEC Technical Procedure AE150 Estimation of Uncertainty of Measurement
Page 19 of 127
Arrow Group LimitedNaasAEP 10 - Aerox1
P0812-01CAR20-01 / Version 105/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 65 of 134
SOCOTEC UK LTD
www.socotec.co.uk
END OF REPORT
Thank you for choosing SOCOTEC for your environmental monitoring needs. We hope our services have met your requirements and that you are fully satisfied with your experience of working with us, we really do value your custom and would welcome your feedback. We would appreciate it if you could take a
moment to complete a short online questionnaire so that we can improve our operations and address any areas that have not met with your expectations, by clicking on the following
https://www.surveymonkey.co.uk/r/CAE_customer_feedback_weblink
Page 20 of 127
Arrow Group LimitedNaasAEP 10 - Aerox1
P0812-01CAR20-01 / Version 105/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 66 of 134
STACK EMISSIONS MONITORING REPORT
Page 65 of 127
SECTION D Emission Point - AE11 – Aerox 2
Date
Site Operator: Arrow Group Limited The Maudlins Industrial Estate Naas Co Kildare
Site Visit Report - SV18614 - Arrow Group Limited Page 67 of 134
SOCOTEC Job Number:Report Date:Version: 1Report By: Daniel ScullyMCERTS Number: MM 19 1563MCERTS Level: MCERTS Level 1 - Technician Technical Endorsements:
Report Approved By: David HayMCERTS Number: MM 04 552Business Title: MCERTS Level 2 - Buisness ManagerTechnical Endorsements: 1, 2, 3 & 4
Signature:
P0812-01CAR20-01
Sampling Date(s):05/10/2020 & 19/10/20
28-Oct-20
Naas
Arrow Group Limited
Co Kildare
Release Point: AEP 11 - Aerox 2
Your contact at SOCOTEC LTD
Operator & Address:
The Maudlins Industrial Estate
2-4 Langlands PlaceKelvin South Business Park
East KilbrideG75 0YF
Tel: 01355 246 730Fax: 01355 249 669
Permit Reference:IE Licence: P0812-01
David HayBusiness Manager - North
Tel: 01355 246 730Email: [email protected]
STACK EMISSIONS MONITORING
SOCOTEC UK Reporting Template v6 Page 66 of 127
Site Visit Report - SV18614 - Arrow Group Limited Page 68 of 134
SOCOTEC UK LTD
www.socotec.co.uk
EXECUTIVE SUMMARY
Stack Emissions Monitoring Objectives
- Plant
- Operator
- Stack Emissions Monitoring Test House
Emissions Summary
Monitoring Times
Process Details
Monitoring Methods
Analytical Methods
- Sampling Methods with Subsequent Analysis
- On-Site Testing
Sampling Location
- Sampling Plane Validation Criteria
- Duct Characteristics
- Sampling Lines & Sample Points
- Sampling Platform
- Sampling Location / Platform Improvement Recommendations
Sampling and Analytical Method Deviations
APPENDICES
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
APPENDIX 3 - Measurement Uncertainty Budget Calculations
CONTENTS
Page 67 of 127
Arrow Group LimitedNaasAEP 11 - Aerox 2
P0812-01CAR20-01 / Version 105/10/2020 19/10/20IE Licence: P0812-01
Site Visit Report - SV18614 - Arrow Group Limited Page 69 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Plant
AEP 11 - Aerox 2
Operator
Arrow Group Limited
The Maudlins Industrial Estate
Naas
Co Kildare
IE Licence: P0812-01
Stack Emissions Monitoring Test House
SOCOTEC - East Kilbride Laboratory2-4 Langlands PlaceKelvin South Business ParkEast KilbrideG75 0YFUKAS and MCERTS Accreditation Number: 1015
Opinions and interpretations expressed herein are outside the scope of UKAS accreditation.MCERTS accredited results will only be claimed where both the sampling and analytical stages are UKAS accredited.This test report shall not be reproduced, except in full, without written approval of SOCOTEC LTD.
MONITORING OBJECTIVES
SOCOTEC LTD were commissioned by The Environmental Protection Agency to carry out stack emissions monitoring to determine the release ofprescribed pollutants from the following Plant under normal operating conditions.
Arrow Group Limited operates a production of food products from animal raw materials process at Naas which is subject to IE Licence P0812-01, underthe EPA Act 1992.
EXECUTIVE SUMMARY
The results of these tests shall be used to demonstrate compliance with a set of emission limit values for prescribed pollutants as specified in thePlant's IE Licence, P0812-01.
Page 68 of 127
Arrow Group LimitedNaasAEP 11 - Aerox 2
P0812-01CAR20-01 / Version 105/10/2020 19/10/20IE Licence: P0812-01
Site Visit Report - SV18614 - Arrow Group Limited Page 70 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Parameter Units Result Calculated Uncertainty
+/-Odour ouE/m³ 654.33 - -Odour Emission Rate ouE/s 5877.58 - -Stack Gas Temperature oC 33 - -Stack Gas Velocity m/s 11.6 0.27 -Gas Volumetric Flow Rate (Actual) m³/hr 36238 1840 -Gas Volumetric Flow Rate (STP, Wet) m³/hr 32337 1642 -Gas Volumetric Flow Rate (STP, Dry) m³/hr 25870 1314 -Gas Volumetric Flow Rate at Reference Conditions m³/hr 32337 1642 -
Emission Limit Value (ELV)
P
Reference conditions are 273K, 101.3kPa without correction for water vapour
EXECUTIVE SUMMARY
EMISSIONS SUMMARY
ND = None Detected,Results at or below the limit of detection are highlighted by bold italic text.The above volumetric flow rate is calculated using data from the preliminary survey. Mass emissions for non isokinetic tests are calculated using these values. For all isokinetic testing the mass emission is calculated using test specific flow data and not the above values.
MCERTS accredited
result
P
Page 69 of 127
Arrow Group LimitedNaasAEP 11 - Aerox 2
P0812-01CAR20-01 / Version 105/10/2020 19/10/20IE Licence: P0812-01
Site Visit Report - SV18614 - Arrow Group Limited Page 71 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Odour Run 1Odour Run 2Odour Run 3
05 October 2020
MONITORING TIMESSampling TimesSampling Date(s)Parameter
EXECUTIVE SUMMARY
Sampling Duration
19 October 2020
13 minutes8 minutes9 minutes
10:59-11:04 -05 October 202010:45 - 10:5411:21 - 11:2911:07 - 11:20
Preliminary Stack Traverse
05 October 2020
Page 70 of 127
Arrow Group LimitedNaasAEP 11 - Aerox 2
P0812-01CAR20-01 / Version 105/10/2020 19/10/20IE Licence: P0812-01
Site Visit Report - SV18614 - Arrow Group Limited Page 72 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Description of process Production of food products from animal raw materials
Continuous or batch Continuous
Product Details Food Production - cooking Line
Part of batch to be monitored (if applicable) N/A
Normal load, throughput or continuous rating Continous
Fuel used during monitoring N/A
Abatement Aerox system
Plume Appearance Visible
Process Details
EXECUTIVE SUMMARY
PROCESS DETAILS
Parameter
Page 71 of 127
Arrow Group LimitedNaasAEP 11 - Aerox 2
P0812-01CAR20-01 / Version 105/10/2020 19/10/20IE Licence: P0812-01
Site Visit Report - SV18614 - Arrow Group Limited Page 73 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Species SOCOTEC UKAS Lab MCERTS Limit of Calculated CalculatedTechnical Number Accredited Detection MU MUProcedure Method (LOD) +/- % Result +/- % ELV
Odour AE 142 1015 Yes - - N/A - No ELV
Velocity AE 154 1015 Yes 5 Pa 2.3% N/A - No ELV
Volumetric Flow Rate
AE 154 1015 Yes - 5.1% N/A - No ELV
MONITORING METHODS
SRM - EN ISO 16911-1
SRM - EN ISO 16911-1
Standard Reference Method / Alternative Method
The selection of standard reference / alternative methods employed by SOCOTEC is determined, wherever possible by the hierarchy of methodselection outlined in Environmental Protection Agency Technical Guidance Note (Monitoring) AG2.
Method
Monitoring Methods
EXECUTIVE SUMMARY
EN 13725
Page 72 of 127
Arrow Group LimitedNaasAEP 11 - Aerox 2
P0812-01CAR20-01 / Version 105/10/2020 19/10/20IE Licence: P0812-01
Site Visit Report - SV18614 - Arrow Group Limited Page 74 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Odour olfactometry 2430 Yes Odournet SOCO20X 201006 8 Weeks
- - - - - - -
Species Analytical UKAS Lab MCERTS Laboratory Data ArchiveProcedure Number Accredited Archive Period
Analysis Location- - - - - - --
UKAS Accredited Lab Analysis
Analysis Report number
SAMPLING METHODS WITH SUBSEQUENT ANALYSIS
ON-SITE TESTING
Analytical Procedure
Analytical TechniqueUKAS Lab Number
Species
The following tables list the analytical methods employed together with the custody details. Unless otherwise stated the samples are archived at the analysis lab location.
Analysis LabArchivePeriod
olfactometry
Analytical Methods
-
Analytical Technique
EXECUTIVE SUMMARY
Page 73 of 127
Arrow Group LimitedNaasAEP 11 - Aerox 2
P0812-01CAR20-01 / Version 105/10/2020 19/10/20IE Licence: P0812-01
Site Visit Report - SV18614 - Arrow Group Limited Page 75 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Sampling Plane Validation Criteria Value Units Requirement Compliant Method
Lowest Differential Pressure 74 Pa >= 5 Pa Yes EN 15259
Lowest Gas Velocity 10.9 m/s - - -
Highest Gas Velocity 12.2 m/s - - -
Ratio of Gas Velocities 1.1 : 1 < 3 : 1 Yes EN 15259
Mean Velocity 11.6 m/s - - -
Maximum angle of flow with regard to duct axis <15 o < 15o Yes EN 15259
No local negative flow Yes - - Yes EN 15259
Value Units Isokinetic
Shape Circular -
Depth 1.05 m Sample port size 1" bsp -
Width - m Number of lines used 1 -
Area 0.87 m2 Number of points / line 1 -
Port Depth 40 mm Duct orientation horizontal/vertical -
Filtration N/A -
General Platform Information
Permanent / Temporary Platform / Ground level / Floor Level / Roof
Inside / Outside
AG1 Platform requirements
Is there a sufficient working area so work can be performed in a compliant manner
Platform has 2 levels of handrails (approximately 0.5 m & 1.0 m high)
Platform has vertical base boards (approximately 0.25 m high)
Platform has removable chains / self closing gates at the top of ladders
Handrail / obstructions do not hamper insertion of sampling equipment
Depth of Platform = >Stack depth / diameter + wall and port thickness + 1.5m
Sampling Platform Improvement Recommendations (if applicable)
N/A
Outside
SAMPLING LINES & POINTSDUCT CHARACTERISTICS
EXECUTIVE SUMMARY
Roof Level
Yes
N/A
The sampling location meets all the requirements as specified in The EPA's Guidance Note AG1.
SAMPLING LOCATION
N/A
N/A
N/A
SAMPLING PLATFORM
Non-Iso & Gases
Page 74 of 127
Arrow Group LimitedNaasAEP 11 - Aerox 2
P0812-01CAR20-01 / Version 105/10/2020 19/10/20IE Licence: P0812-01
Site Visit Report - SV18614 - Arrow Group Limited Page 76 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Sample Lines
EXECUTIVE SUMMARY
Only 1 sample line is available for carrying out preliminary velocity and temperature traverse as opposed to the 2 sample lines stated inEN 15259 and EPA's AG1 Guidance. In addition the sampling point is less than the recommended 5 hydraulic diameters from the exit ofthe duct and from a bend.
Sampling & Analytical Method Deviations
Page 75 of 127
Arrow Group LimitedNaasAEP 11 - Aerox 2
P0812-01CAR20-01 / Version 105/10/2020 19/10/20IE Licence: P0812-01
Site Visit Report - SV18614 - Arrow Group Limited Page 77 of 134
SOCOTEC UK LTD
www.socotec.co.uk
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
APPENDIX 3 - Measurement Uncertainty Budget Calculations
CONTENTS
APPENDICES
Page 76 of 127
Arrow Group LimitedNaasAEP 11 - Aerox 2
P0812-01CAR20-01 / Version 105/10/2020 19/10/20IE Licence: P0812-01
Site Visit Report - SV18614 - Arrow Group Limited Page 78 of 134
SOCOTEC UK LTD
www.socotec.co.uk
SOCOTEC UKAS Lab MCERTSTechnical Number AccreditedProcedure Method
AE 142 1015 Yes 3AE 154 1015 Yes 1
MONITORING SCHEDULE
Number of Samples
EN 13725
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
Standard Reference Method / Alternative Method
Method
SRM - EN ISO 16911-1Velocity
Species
Odour
Page 77 of 127
Arrow Group LimitedNaasAEP 11 - Aerox 2
P0812-01CAR20-01 / Version 105/10/2020 19/10/20IE Licence: P0812-01
Site Visit Report - SV18614 - Arrow Group Limited Page 79 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Equipment I.D. Equipment I.D. Equipment I.D.
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
NOTE: If the equipment I.D is represented by a dash (-), then this piece of equipment has not been used for this test.
Cylinder I.D Number
Supplier ppm %Analytical
Tolerance +/- %
- - - - -
Level Expiry TE1 TE2 TE3 TE4 H&S
Enda Flood MM 12 1170MCERTS Level 2
Apr-23 Mar-24 Mar-24 Jun-23 Nov-23 Apr-23
Aidan Whiteny MM 20 1603MCERTS Trainee
Sep-25 - - - - Sep-25
STACK EMISSIONS MONITORING TEAM
Laboratory Balance
1m Heated Line (2)
Mass Flow Controller
Thermo FID
Digital Temperature Meter
Servomex
Probe Thermocouple
Signal 3030 FID
Site Balance
5m Heated Line (1)
Small DGM
Heated Line Controller (1)
Site temperature Logger
Inclinometer (Swirl Device)
Chiller (JCT/MAK 10)
MFC Display module
Extractive Sampling
Equipment
Meter In Thermocouple Stopwatch
Probe
FT-IR Oven Box
Equipment
Horiba PG-250 Analyser
Callipers
20m Heated Line (2)
Anemometer
Dioxins Cond. Thermocouple 10m Heated Line (1)
Probe Thermocouple
Stackmaster
Meter Out Thermocouple
Control Box Timer
Stack Thermocouple
1m Heated Line (1)
L-Pitot
Oven Box
Control Box DGM
Instrumental Analyser/s
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
CALIBRATEABLE EQUIPMENT CHECKLISTMiscellaneous
Heated Line Controller (2)
MCERTS Number
TE / H&S Qualifications and Expiry DateMCERTS
Box Thermocouples Tape Measure
Probe JCT Heated Head Filter
Digital Micromanometer
Bernath 3006 FID Protractor
Personnel
CALIBRATION GASES
FTIR Heater Box for Heated Line
1m Heated Line (3)
10m Heated Line (2)
15m Heated Line (1)
MONITORING TEAM
-
S-Pitot
FT-IR Gasmet
Barometer
Equipment
Ecophysics NOx Analyser
Heater Controller
Last Impinger Arm
Gas (traceable to ISO 17025)
20m Heated Line (1)
Page 78 of 127
Arrow Group LimitedNaasAEP 11 - Aerox 2
P0812-01CAR20-01 / Version 105/10/2020 19/10/20IE Licence: P0812-01
Site Visit Report - SV18614 - Arrow Group Limited Page 80 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Duration ELV EmissionMinutes ouE/m³ Rate ouE/s
13 - 6925.55
8 - 9674.21
Run 3 9 - 1032.99
Reference conditions are 273K, 101.3kPa without correction for water vapour
Leak Test Results
m³ l/min l/min l/min l/min
Run 1 10.0 0.8 0.00 0.00 0.02 Yes
Run 2 10.0 1.3 0.00 0.00 0.03 Yes
Run 3 10.0 1.1 0.00 0.00 0.02 Yes
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
ODOUR SUMMARY
ODOUR QUALITY ASSURANCE CHECKLIST
Total Sample Volume @ ref
Conditions
Pre sampling leak rate
10:45 - 10:5419 October 2020
Post sampling leak rate
Concentration
1077.00
Mean Sampling Rate
ouE/m³
Run 2
771.00
Acceptable leak rate
Test
11:21 - 11:2905 October 2020
11:07 - 11:2005 October 2020
Run 1
Leak Tests Acceptable?
Sampling Times
115.00
Page 79 of 127
Arrow Group LimitedNaasAEP 11 - Aerox 2
P0812-01CAR20-01 / Version 105/10/2020 19/10/20IE Licence: P0812-01
Site Visit Report - SV18614 - Arrow Group Limited Page 81 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Stack Diameter / Depth, D 1.05 m
Stack Width, W - m
Stack Area, A 0.87 m2
Average stack gas temperature 33 oC
Stack static pressure 0.022 kPa
Barometric Pressure 101.3 kPa
Component Molar Density Conc Dry Volume Dry Conc Conc Wet Volume Wet ConcMass kg/m3 Dry Fraction kg/m3 Wet Fraction kg/m3
M p % Vol r pi % Vol r pi
CO2 44 1.963059 0.028571 0.000286 0.000561 0.022857 0.000229 0.000449
O2 32 1.427679 21.000000 0.210000 0.299813 16.800000 0.168000 0.239850
N2 28 1.249219 78.971429 0.789714 0.986526 63.177143 0.631771 0.789221
H2O 18 0.803070 - - - 20.000000 0.200000 0.160614
Where: p = M / 22.41 pi = r x p
Determinand
Dry Density (STP), P STD
Wet Density (STP), P STW
Dry Density (Actual), P Actual
Average Wet Density (Actual), P ActualW
Where:
P STD = sum of component concentrations, kg/m3 (not including water vapour) P Actual = P STD x (Ts / Ps) x (Pa / Ta)
P STW = (P STD + pi of H2O) / (1 + (pi of H2O / 0.8036)) P ActualW = P STW x (Ts / Ps) x (Pa / Ta)
PRELIMINARY STACK SURVEY
1.062
kg/m3
Units
Stack Gas Composition & Molecular Weights
Result
kg/m3
Calculation of Stack Gas Densities
Stack Characteristics
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
1.1901
kg/m31.2869
kg/m3
1.1484
Page 80 of 127
Arrow Group LimitedNaasAEP 11 - Aerox 2
P0812-01CAR20-01 / Version 105/10/2020 19/10/20IE Licence: P0812-01
Site Visit Report - SV18614 - Arrow Group Limited Page 82 of 134
SOCOTEC UK LTD
www.socotec.co.uk
TRAVERSE 1
Traverse Distance DP pt DP pt Temp Velocity O2 Angle
Point into Pa mmH2O oC m/s % of Swirl
duct (m)(average of 3
readings)(average of 3
readings)m³/s Vol o
1 0.07 77.4 7.9 33 10.9 9.4 - <152 0.26 86.9 8.9 33 11.5 10.0 - <153 0.79 92.1 9.4 33 11.9 10.3 - <154 0.98 97.0 9.9 33 12.2 10.6 - <15- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -
Mean - 88.4 9.0 33 11.6 10.1 - -
Traverse Distance DP pt DP pt Temp Velocity O2 Angle
Point into Pa mmH2O oC m/s % of Swirl
duct (m)(average of 3
readings)(average of 3
readings)m³/s Vol o
- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -
Mean - - - - - - - -
Start Value End Value Difference Start Value End Value DifferencemmH2O mmH2O % mmH2O mmH2O %
Run 1 122 120 1.6 Pass 134 133 0.7 Pass
RunFinal Reading
(Pa)
Reading After Purge(Pa)
Difference(%)
Outcome(Permitted
+/- 5%)
Run 1 9.8 9.6 -2.1 Pass
Post Traverse Leak Rate
Sampling Line B
10:59-11:0405 October 2020
Volumetric Flow Rate
(actual)
To complete a compliant pitot leak check a pressure of over 80 mmH₂O (or 800 Pa) is applied and the pressure drop monitored over 5 mins. A drop of less than 5% must be observed.
Time of Survey
L-Type Pitot Blockage Test
Pre Traverse Leak RateOutcomeRun
PITOT LEAK CHECK
Volumetric Flow Rate
(actual)
L-Type Pitot
Sampling Line A
Outcome
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
Date of Survey
Velocity Measurement Device:
PRELIMINARY STACK SURVEY
PRELIMINARY STACK SURVEY QUALITY ASSURANCE CHECKLIST
Page 81 of 127
Arrow Group LimitedNaasAEP 11 - Aerox 2
P0812-01CAR20-01 / Version 105/10/2020 19/10/20IE Licence: P0812-01
Site Visit Report - SV18614 - Arrow Group Limited Page 83 of 134
SOCOTEC UK LTD
www.socotec.co.uk
EA Technical Guidance Note (Monitoring) M1 Units Requirement Compliant
Lowest Differential Pressure Pa >= 5 Pa Yes
Lowest Gas Velocity m/s - -
Highest Gas Velocity m/s - -
Ratio of Gas Velocities - < 3 : 1 Yes
Maximum angle of flow with regard to duct axis o < 15o Yes
No local negative flow - - Yes
Velocity at Traverse Point, V = Kpt x (1-e) * Ö(2 * DP pt / P ActualW)
Where:Kpt = Pitot tube calibration coefficient(1-e) = Compressibility correction factor, assumed at a constant 0.998
Average Stack Gas Velocity, Va 11.6 m/s
Duct gas flow conditions Actual Reference UnitsTemperature 33 0 oC
Total Pressure 101.322 101.3 kPaOxygen 21.0 21 %Moisture 20.00 20.00 %Pitot tube calibration coefficient, Kpt 0.90
Gas Volumetric Flowrate Units
Average Stack Gas Velocity (Va) m/s
Stack Area (A) m2
Gas Volumetric Flowrate (Actual), QActual m3/hr
Gas Volumetric Flowrate (STP, Wet), QSTP m3/hr
Gas Volumetric Flowrate (STP, Dry), QSTP,Dry m3/hr
Gas Volumetric Flowrate (REF), QRef m3/hr
Where:QActual = Va x A x 3600QSTP = Q (Actual) x (Ts / Ta) x (Pa / Ps) x 3600QSTP,Dry = Q (STP) / (100 - (100 / Ma)) x 3600
QRef = Q (STP) x ((100 - Ma) / (100 - Ms)) x ((21 - O2a) / (21 - O2s))
Nomenclature:Ts = Absolute Temperature, Standard Conditions, 273 KPs = Absolute Pressure, Standard Conditions, 101.3 kPaTa = Absolute Temperature, Actual Conditions, KPa = Absolute Pressure, Actual Conditions, kPaMa = Water vapour, Actual Conditions, % VolMs = Water vapour, Reference Conditions, % VolO2a = Oxygen, Actual Conditions, % VolO2s = Oxygen, Reference Conditions, % Vol
11.62
10.9
1.1
PRELIMINARY STACK SURVEY (CONTINUED)
Yes
Calculation of Stack Gas Velocity, V
Calculation of Stack Gas Volumetric Flowrate, Q
25870
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
Sampling Plane Validation Criteria
<15
32337
32337
Result
12.2
36238
77
Result
0.87
Page 82 of 127
Arrow Group LimitedNaasAEP 11 - Aerox 2
P0812-01CAR20-01 / Version 105/10/2020 19/10/20IE Licence: P0812-01
Site Visit Report - SV18614 - Arrow Group Limited Page 84 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Value UnitsStack Depth 1.05 m Sampling Distance Distance into UnitsStack Width - m Point (% of Depth) StackArea 0.87 m2 - - - -
Sampling Distance Distance into SwirlPoint (% of Depth) Stack (m) o
1 6.7 0.07 < 152 25.0 0.26 < 153 75.0 0.79 < 154 93.3 0.98 < 15
- - - -
- - - -
- - - -
- - - -- - - -- - - -
- - - -- - - -
- - - -
- - - -- - - -- - - -
Isokinetic sampling point - - - -Isokinetic sampling points not used - - - -Non Isokinetic/Gases sampling point - - - -
- - - -
Isokinetic Sampling
STACK DIAGRAM
Non-Isokinetic/Gases Sampling
SAMPLING LOCATION
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
Sampling Line A
1
2
3
4
Page 83 of 127
Arrow Group LimitedNaasAEP 11 - Aerox 2
P0812-01CAR20-01 / Version 105/10/2020 19/10/20IE Licence: P0812-01
Site Visit Report - SV18614 - Arrow Group Limited Page 85 of 134
SOCOTEC UK LTD
www.socotec.co.uk
11.6 m/s36238 m³/hr
Performance Characteristics & Source of Value Units Values Requirement CompliantUncertainty of Local Gas Velocity Determination
Uncertainty of pitot tube coefficient - 0.010
Uncertainty of mean local dynamic pressures - 0.81
Factor loading, function of the number of measurements. 3 readings 0.591 minimum 3 Yes
Range of measurment device pa 1000
Resolution pa 1.00
Calibration uncertainty pa 14.69<1% of Value or 20
Pa whichever is greater
Yes
Drift % range 0.10
Linearity % range 0.06 <2% of value Yes
Uncertainty of gas density determination
Uncertainty of molar mass determination kg/mol 0.00003
Uncertainty of temperature measurement K 1.56 <1% of value Yes
Uncertainty of absolute pressure in the duct pa 517
Uncertainty associated with the estimate of density - 0.008
Uncertainty associated with the measurement of local velocity - 0.0001Uncertainty associated with the measurement of mean velocity - 0.0001
m/s0.140.27
%1.22.3
m³/hr939
1840
%2.65.1
Reference – SOCOTEC Technical Procedure AE150 Estimation of Uncertainty of Measurement
Combined uncertainty
Note - The expanded uncertainty uses a coverage factor of k = 2.
APPENDIX 3 - Measurement Uncertainty Budget Calculations
MEASUREMENT UNCERTAINTY BUDGET - VELOCITY & VOLUMETRIC FLOW RATE
Measured Velocity at Actual Conditions Measured Volumetric Flow rate at Actual Conditions
Measurement Uncertainty - Velocity
Combined uncertaintyExpanded uncertainty at a 95% Confidence Interval
Note - The expanded uncertainty uses a coverage factor of k = 2.
Expanded Measurement Uncertainty of Velocity at a 95% Confidence Interval
Expressed as a % of the Measured VelocityExpanded uncertainty at a 95% Confidence Interval
Measurement Uncertainty Volumetric Flow Rate
Expanded uncertainty at a 95% Confidence Interval
Expanded Measurement Uncertainty of Volumetric Flow Rate at a 95% Confidence IntervalExpressed as a % of the Measured Volumetric Flow RateExpanded uncertainty at a 95% Confidence Interval
Page 84 of 127
Arrow Group LimitedNaasAEP 11 - Aerox 2
P0812-01CAR20-01 / Version 105/10/2020 19/10/20IE Licence: P0812-01
Site Visit Report - SV18614 - Arrow Group Limited Page 86 of 134
SOCOTEC UK LTD
www.socotec.co.uk
https://www.surveymonkey.co.uk/r/CAE_customer_feedback_weblink
END OF REPORT
Thank you for choosing SOCOTEC for your environmental monitoring needs. We hope our services have met your requirements and that you are fully satisfied with your experience of working with us, we really do value your custom and would welcome your feedback. We would appreciate it if you could take a
moment to complete a short online questionnaire so that we can improve our operations and address any areas that have not met with your expectations, by clicking on the following
Page 85 of 127
Arrow Group LimitedNaasAEP 11 - Aerox 2
P0812-01CAR20-01 / Version 105/10/2020 19/10/20IE Licence: P0812-01
Site Visit Report - SV18614 - Arrow Group Limited Page 87 of 134
STACK EMISSIONS MONITORING REPORT
Page 86 of 127
SECTION E Emission Point - AE12 – Pasta Concepts Carbon Filter Date
Site Operator: Arrow Group Limited The Maudlins Industrial Estate Naas Co Kildare
Site Visit Report - SV18614 - Arrow Group Limited Page 88 of 134
SOCOTEC Job Number:Report Date:Version: 1Report By: Daniel ScullyMCERTS Number: MM 19 1563MCERTS Level: MCERTS Level 1 - TechnicianTechnical Endorsements:
Report Approved By: David HayMCERTS Number: MM 04 552Business Title: MCERTS Level 2 - Buisness ManagerTechnical Endorsements: 1, 2, 3 & 4
Signature:
2-4 Langlands PlaceKelvin South Business Park
East KilbrideG75 0YF
Tel: 01355 246 730Fax: 01355 249 669
Permit Reference:IE Licence: P0812-01
David HayBusiness Manager - North
Tel: 01355 246 730Email: [email protected]
Your contact at SOCOTEC LTD
Operator & Address:
The Maudlins Industrial Estate Naas
Arrow Group Limited
Co Kildare
Release Point: AEP 12 - Pasta Concepts Carbon Filter
Sampling Date(s):05/10/2020 & 19/10/2020
28-Oct-20P0812-01CAR20-01
STACK EMISSIONS MONITORING
SOCOTEC UK Reporting Template v6 Page 87 of 127
Site Visit Report - SV18614 - Arrow Group Limited Page 89 of 134
SOCOTEC UK LTD
www.socotec.co.uk
EXECUTIVE SUMMARY
Stack Emissions Monitoring Objectives
- Plant
- Operator
- Stack Emissions Monitoring Test House
Emissions Summary
Monitoring Times
Process Details
Monitoring Methods
Analytical Methods
- Sampling Methods with Subsequent Analysis
- On-Site Testing
Sampling Location
- Sampling Plane Validation Criteria
- Duct Characteristics
- Sampling Lines & Sample Points
- Sampling Platform
- Sampling Location / Platform Improvement Recommendations
Sampling and Analytical Method Deviations
APPENDICES
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
APPENDIX 3 - Measurement Uncertainty Budget Calculations
CONTENTS
Page 88 of 127
Arrow Group LimitedNaasAEP 12 - Pasta Concepts Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 90 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Plant
AEP 12 - Pasta Concepts Carbon Filter
Operator
Arrow Group Limited
The Maudlins Industrial Estate
Naas
Co Kildare
IE Licence: P0812-01
Stack Emissions Monitoring Test House
SOCOTEC - East Kilbride Laboratory2-4 Langlands PlaceKelvin South Business ParkEast KilbrideG75 0YFUKAS and MCERTS Accreditation Number: 1015
Opinions and interpretations expressed herein are outside the scope of UKAS accreditation.MCERTS accredited results will only be claimed where both the sampling and analytical stages are UKAS accredited.This test report shall not be reproduced, except in full, without written approval of SOCOTEC LTD.
MONITORING OBJECTIVES
SOCOTEC LTD were commissioned by The Environmental Protection Agency to carry out stack emissions monitoring to determine the release ofprescribed pollutants from the following Plant under normal operating conditions.
Arrow Group Limited operates a production of food products from animal raw materials process at Naas which is subject to IE Licence P0812-01, underthe EPA Act 1992.
EXECUTIVE SUMMARY
The results of these tests shall be used to demonstrate compliance with a set of emission limit values for prescribed pollutants as specified in thePlant's IE Licence, P0812-01.
Page 89 of 127
Arrow Group LimitedNaasAEP 12 - Pasta Concepts Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 91 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Parameter Units Result Calculated Uncertainty
+/-Odour ouE/m³ 66.33 - -Odour Emission Rate ouE/s 412.82 - -Stack Gas Temperature oC 15 - -Stack Gas Velocity m/s 6.8 0.16 -Gas Volumetric Flow Rate (Actual) m³/hr 23436 1196 -Gas Volumetric Flow Rate (STP, Wet) m³/hr 22404 1144 -Gas Volumetric Flow Rate (STP, Dry) m³/hr 17923 915 -Gas Volumetric Flow Rate at Reference Conditions m³/hr 22404 1144 -
P
MCERTS accredited
result
ND = None Detected,Results at or below the limit of detection are highlighted by bold italic text.The above volumetric flow rate is calculated using data from the preliminary survey. Mass emissions for non isokinetic tests are calculated using these values. For all isokinetic testing the mass emission is calculated using test specific flow data and not the above values.
EXECUTIVE SUMMARY
EMISSIONS SUMMARY
Reference conditions are 273K, 101.3kPa without correction for water vapour
P
Emission Limit Value (ELV)
Page 90 of 127
Arrow Group LimitedNaasAEP 12 - Pasta Concepts Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 92 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Odour Run 1Odour Run 2Odour Run 3
05 October 202011:55 - 12:00
Preliminary Stack Traverse
12:01 - 12:0710:36 - 10:45
05 October 2020 11:46-11:52 -
5 minutes6 minutes9 minutes19 October 2020
Sampling TimesSampling Date(s)Parameter
EXECUTIVE SUMMARY
Sampling DurationMONITORING TIMES
05 October 2020
Page 91 of 127
Arrow Group LimitedNaasAEP 12 - Pasta Concepts Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 93 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Description of process Production of Food Products from Animal Raw Materials
Continuous or batch Continuous
Product Details Carbon Filter Odour Unit
Part of batch to be monitored (if applicable) During Carbon Filter Odour Unit Operation
Normal load, throughput or continuous rating Fan Exhust 43.1Hz
Fuel used during monitoring N/A
Abatement Carbon Filter
Plume Appearance None Visible
PROCESS DETAILS
Parameter
EXECUTIVE SUMMARY
Process Details
Page 92 of 127
Arrow Group LimitedNaasAEP 12 - Pasta Concepts Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 94 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Species SOCOTEC UKAS Lab MCERTS Limit of Calculated CalculatedTechnical Number Accredited Detection MU MUProcedure Method (LOD) +/- % Result +/- % ELV
Odour AE 142 1015 Yes - - N/A - No ELV
Velocity AE 154 1015 Yes 5 Pa 2.4% N/A - No ELV
Volumetric Flow Rate
AE 154 1015 Yes - 5.1% N/A - No ELV
EN 13725
EXECUTIVE SUMMARY
Monitoring Methods
Method
The selection of standard reference / alternative methods employed by SOCOTEC is determined, wherever possible by the hierarchy of methodselection outlined in Environmental Protection Agency Technical Guidance Note (Monitoring) AG2.
Standard Reference Method / Alternative Method
SRM - EN ISO 16911-1
SRM - EN ISO 16911-1
MONITORING METHODS
Page 93 of 127
Arrow Group LimitedNaasAEP 12 - Pasta Concepts Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 95 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Odour olfactometry 2430 Yes Odournet SOCO20X 201020 8 Weeks
Species Analytical UKAS Lab MCERTS Laboratory Data ArchiveProcedure Number Accredited Archive Period
Analysis Location- - - - - - -
EXECUTIVE SUMMARY
Analytical Technique
olfactometry
Analytical Methods
The following tables list the analytical methods employed together with the custody details. Unless otherwise stated the samples are archived at the analysis lab location.
Analysis LabArchivePeriod
Analytical Procedure
Analytical TechniqueUKAS Lab Number
Species
ON-SITE TESTING
-
UKAS Accredited Lab Analysis
Analysis Report number
SAMPLING METHODS WITH SUBSEQUENT ANALYSIS
Page 94 of 127
Arrow Group LimitedNaasAEP 12 - Pasta Concepts Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 96 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Sampling Plane Validation Criteria Value Units Requirement Compliant Method
Lowest Differential Pressure 25 Pa >= 5 Pa Yes EN 15259
Lowest Gas Velocity 6.2 m/s - - -
Highest Gas Velocity 8.0 m/s - - -
Ratio of Gas Velocities 1.3 : 1 < 3 : 1 Yes EN 15259
Mean Velocity 6.8 m/s - - -
Maximum angle of flow with regard to duct axis <15 o < 15o Yes EN 15259
No local negative flow Yes - - Yes EN 15259
Value Units Isokinetic
Shape Circular -
Depth 1.10 m Sample port size - 1" BSP
Width - m Number of lines used - 1
Area 0.95 m2 Number of points / line - 1
Port Depth 40 mm Duct orientation - Vertical
Filtration - N/A
General Platform Information
Permanent / Temporary Platform / Ground level / Floor Level / Roof
Inside / Outside
AG1 Platform requirements
Is there a sufficient working area so work can be performed in a compliant manner
Platform has 2 levels of handrails (approximately 0.5 m & 1.0 m high)
Platform has vertical base boards (approximately 0.25 m high)
Platform has removable chains / self closing gates at the top of ladders
Handrail / obstructions do not hamper insertion of sampling equipment
Depth of Platform = >Stack depth / diameter + wall and port thickness + 1.5m
Sampling Platform Improvement Recommendations (if applicable)
SAMPLING PLATFORM
Non-Iso & Gases
Yes
Yes
Yes
The sampling location meets all the requirements as specified in The EPA's Guidance Note AG1.
SAMPLING LOCATION
N/A
DUCT CHARACTERISTICS
EXECUTIVE SUMMARY
Permananet
Yes
Yes
Outside
SAMPLING LINES & POINTS
Page 95 of 127
Arrow Group LimitedNaasAEP 12 - Pasta Concepts Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 97 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Sample Lines
Undetected Result
Sampling & Analytical Method Deviations
Only 1 sample line is available for carrying out preliminary velocity and temperature traverse as opposed to the 2 sample lines stated inEN 15259 and EPA's AG1 Guidance.
EXECUTIVE SUMMARY
Note, as reported by the lab, Sample 3 "was not sufficiently odorous for enough panel members to generate the necessary number ofITE results required for a valid analysis result in accordance to EN13725". As a result, this sample has been reported as a '0' result inthis report
Page 96 of 127
Arrow Group LimitedNaasAEP 12 - Pasta Concepts Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 98 of 134
SOCOTEC UK LTD
www.socotec.co.uk
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
APPENDIX 3 - Measurement Uncertainty Budget Calculations
APPENDICES
CONTENTS
Page 97 of 127
Arrow Group LimitedNaasAEP 12 - Pasta Concepts Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 99 of 134
SOCOTEC UK LTD
www.socotec.co.uk
SOCOTEC UKAS Lab MCERTSTechnical Number AccreditedProcedure Method
AE 142 1015 Yes 3AE 154 1015 Yes 1Velocity
Species
Odour
SRM - EN ISO 16911-1
Standard Reference Method / Alternative Method
MethodNumber of Samples
EN 13725
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
MONITORING SCHEDULE
Page 98 of 127
Arrow Group LimitedNaasAEP 12 - Pasta Concepts Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 100 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Equipment I.D. Equipment I.D. Equipment I.D.
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
NOTE: If the equipment I.D is represented by a dash (-), then this piece of equipment has not been used for this test.
Cylinder I.D Number
Supplier ppm %Analytical
Tolerance +/- %
- - - - -
Level Expiry TE1 TE2 TE3 TE4 H&S
Enda Flood MM 12 1170MCERTS Level 2
Apr-23 Mar-24 Mar-24 Jun-23 Nov-23 Apr-23
Aidan Whiteny MM 20 1603MCERTS Trainee
Sep-25 - - - - Sep-25
20m Heated Line (1)
Gas (traceable to ISO 17025)
Barometer
Equipment
Ecophysics NOx Analyser
Heater Controller
Last Impinger Arm
S-Pitot
FT-IR Gasmet
MONITORING TEAM
-
Probe JCT Heated Head Filter
Digital Micromanometer
Bernath 3006 FID Protractor
Personnel
CALIBRATION GASES
FTIR Heater Box for Heated Line
1m Heated Line (3)
10m Heated Line (2)
15m Heated Line (1)
Heated Line Controller (2)
MCERTS Number
TE / H&S Qualifications and Expiry DateMCERTS
Box Thermocouples Tape Measure
Dioxins Cond. Thermocouple 10m Heated Line (1)
Probe Thermocouple
Stackmaster
Meter Out Thermocouple
Control Box Timer
Stack Thermocouple
1m Heated Line (1)
L-Pitot
Oven Box
Control Box DGM
Instrumental Analyser/s
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
CALIBRATEABLE EQUIPMENT CHECKLISTMiscellaneousExtractive Sampling
Equipment
Meter In Thermocouple Stopwatch
Probe
FT-IR Oven Box
Equipment
Horiba PG-250 Analyser
Callipers
20m Heated Line (2)
Anemometer
Chiller (JCT/MAK 10)
MFC Display module
Site Balance
5m Heated Line (1)
Small DGM
Heated Line Controller (1)
Site temperature Logger
Inclinometer (Swirl Device)
STACK EMISSIONS MONITORING TEAM
Laboratory Balance
1m Heated Line (2)
Mass Flow Controller
Thermo FID
Digital Temperature Meter
Servomex
Probe Thermocouple
Signal 3030 FID
Page 99 of 127
Arrow Group LimitedNaasAEP 12 - Pasta Concepts Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 101 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Duration ELV EmissionMinutes ouE/m³ Rate ouE/s
5 - 715.69
6 - 522.77
Run 3 9 - 0.00
Reference conditions are 273K, 101.3kPa without correction for water vapour
Sampling Times
0.00
11:55 - 12:0005 October 2020
Run 1
12:01 - 12:0705 October 2020
Run 2
115.00
Test
84.00
ouE/m³Concentration
10:36 - 10:4519 October 2020
ODOUR SUMMARY
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
Page 100 of 127
Arrow Group LimitedNaasAEP 12 - Pasta Concepts Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 102 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Stack Diameter / Depth, D 1.10 m
Stack Width, W - m
Stack Area, A 0.95 m2
Average stack gas temperature 15 oC
Stack static pressure 0.062 kPa
Barometric Pressure 102.1 kPa
Component Molar Density Conc Dry Volume Dry Conc Conc Wet Volume Wet ConcMass kg/m3 Dry Fraction kg/m3 Wet Fraction kg/m3
M p % Vol r pi % Vol r pi
CO2 44 1.963059 0.028571 0.000286 0.000561 0.022857 0.000229 0.000449
O2 32 1.427679 21.000000 0.210000 0.299813 16.800000 0.168000 0.239850
N2 28 1.249219 78.971429 0.789714 0.986526 63.177143 0.631771 0.789221
H2O 18 0.803070 - - - 20.000000 0.200000 0.160614
Where: p = M / 22.41 pi = r x p
Determinand
Dry Density (STP), P STD
Wet Density (STP), P STW
Dry Density (Actual), P Actual
Average Wet Density (Actual), P ActualW
Where:
P STD = sum of component concentrations, kg/m3 (not including water vapour) P Actual = P STD x (Ts / Ps) x (Pa / Ta)
P STW = (P STD + pi of H2O) / (1 + (pi of H2O / 0.8036)) P ActualW = P STW x (Ts / Ps) x (Pa / Ta)
1.2303
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
1.1901
kg/m31.2869
kg/m3
Stack Characteristics
Calculation of Stack Gas DensitiesResult
kg/m3
Stack Gas Composition & Molecular Weights
PRELIMINARY STACK SURVEY
1.138
kg/m3
Units
Page 101 of 127
Arrow Group LimitedNaasAEP 12 - Pasta Concepts Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 103 of 134
SOCOTEC UK LTD
www.socotec.co.uk
TRAVERSE 1
Traverse Distance DP pt DP pt Temp Velocity O2 Angle
Point into Pa mmH2O oC m/s % of Swirl
duct (m)(average of 3
readings)(average of 3
readings)m³/s Vol o
1 0.07 30.1 3.1 19 6.6 6.2 - <152 0.28 26.8 2.7 19 6.2 5.9 - <153 0.83 45.1 4.6 2 8.0 7.6 - <154 1.03 30.7 3.1 20 6.6 6.3 - <15- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -
Mean - 33.2 3.4 15 6.8 6.5 - -
Traverse Distance DP pt DP pt Temp Velocity O2 Angle
Point into Pa mmH2O oC m/s % of Swirl
duct (m)(average of 3
readings)(average of 3
readings)m³/s Vol o
- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -
Mean - - - - - - - -
Start Value End Value Difference Start Value End Value DifferencemmH2O mmH2O % mmH2O mmH2O %
Run 1 122 120 1.6 Pass 134 133 0.7 Pass
RunFinal Reading
(Pa)
Reading After Purge(Pa)
Difference(%)
Outcome(Permitted
+/- 5%)
Run 1 64 62 -3.2 Pass
PRELIMINARY STACK SURVEY QUALITY ASSURANCE CHECKLIST
PRELIMINARY STACK SURVEY
Sampling Line A
Outcome
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
Date of Survey
Velocity Measurement Device:
Volumetric Flow Rate
(actual)
L-Type PitotTime of Survey
L-Type Pitot Blockage Test
Pre Traverse Leak RateOutcomeRun
PITOT LEAK CHECK
To complete a compliant pitot leak check a pressure of over 80 mmH₂O (or 800 Pa) is applied and the pressure drop monitored over 5 mins. A drop of less than 5% must be observed.
Sampling Line B
11:46-11:5205 October 2020
Volumetric Flow Rate
(actual)
Post Traverse Leak Rate
Page 102 of 127
Arrow Group LimitedNaasAEP 12 - Pasta Concepts Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 104 of 134
SOCOTEC UK LTD
www.socotec.co.uk
EA Technical Guidance Note (Monitoring) M1 Units Requirement Compliant
Lowest Differential Pressure Pa >= 5 Pa Yes
Lowest Gas Velocity m/s - -
Highest Gas Velocity m/s - -
Ratio of Gas Velocities - < 3 : 1 Yes
Maximum angle of flow with regard to duct axis o < 15o Yes
No local negative flow - - Yes
Velocity at Traverse Point, V = Kpt x (1-e) * Ö(2 * DP pt / P ActualW)
Where:Kpt = Pitot tube calibration coefficient(1-e) = Compressibility correction factor, assumed at a constant 0.998
Average Stack Gas Velocity, Va 6.8 m/s
Duct gas flow conditions Actual Reference UnitsTemperature 15 0 oC
Total Pressure 102.162 101.3 kPaOxygen 21.0 21 %Moisture 20.00 20.00 %Pitot tube calibration coefficient, Kpt 0.90
Gas Volumetric Flowrate Units
Average Stack Gas Velocity (Va) m/s
Stack Area (A) m2
Gas Volumetric Flowrate (Actual), QActual m3/hr
Gas Volumetric Flowrate (STP, Wet), QSTP m3/hr
Gas Volumetric Flowrate (STP, Dry), QSTP,Dry m3/hr
Gas Volumetric Flowrate (REF), QRef m3/hr
Where:QActual = Va x A x 3600QSTP = Q (Actual) x (Ts / Ta) x (Pa / Ps) x 3600QSTP,Dry = Q (STP) / (100 - (100 / Ma)) x 3600
QRef = Q (STP) x ((100 - Ma) / (100 - Ms)) x ((21 - O2a) / (21 - O2s))
Nomenclature:Ts = Absolute Temperature, Standard Conditions, 273 KPs = Absolute Pressure, Standard Conditions, 101.3 kPaTa = Absolute Temperature, Actual Conditions, KPa = Absolute Pressure, Actual Conditions, kPaMa = Water vapour, Actual Conditions, % VolMs = Water vapour, Reference Conditions, % VolO2a = Oxygen, Actual Conditions, % VolO2s = Oxygen, Reference Conditions, % Vol
27
Result
0.95
23436
Result
8.0
Calculation of Stack Gas Velocity, V
Calculation of Stack Gas Volumetric Flowrate, Q
17923
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
Sampling Plane Validation Criteria
<15
22404
22404
6.85
6.2
1.3
PRELIMINARY STACK SURVEY (CONTINUED)
Yes
Page 103 of 127
Arrow Group LimitedNaasAEP 12 - Pasta Concepts Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 105 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Value UnitsStack Depth 1.10 m Sampling Distance Distance into UnitsStack Width - m Point (% of Depth) StackArea 0.95 m2 A 50 0.55 m
Sampling Distance Distance into SwirlPoint (% of Depth) Stack (m) o
- - - -- - - -- - - -- - - -
- - - -
- - - -
- - - -
- - - -- - - -- - - -
- - - -- - - -
- - - -
- - - -- - - -- - - -
Isokinetic sampling point - - - -Isokinetic sampling points not used - - - -Non Isokinetic/Gases sampling point - - - -
- - - -
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
SAMPLING LOCATION
Non-Isokinetic/Gases Sampling
STACK DIAGRAM
Isokinetic Sampling
Sampling Line A
A
Page 104 of 127
Arrow Group LimitedNaasAEP 12 - Pasta Concepts Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 106 of 134
SOCOTEC UK LTD
www.socotec.co.uk
6.8 m/s23436 m³/hr
Performance Characteristics & Source of Value Units Values Requirement CompliantUncertainty of Local Gas Velocity Determination
Uncertainty of pitot tube coefficient - 0.010
Uncertainty of mean local dynamic pressures - 0.47
Factor loading, function of the number of measurements. 3 readings 0.591 minimum 3 Yes
Range of measurment device pa 1000
Resolution pa 1.00
Calibration uncertainty pa 6.74<1% of Value or 20
Pa whichever is greater
Yes
Drift % range 0.10
Linearity % range 0.06 <2% of value Yes
Uncertainty of gas density determination
Uncertainty of molar mass determination kg/mol 0.00003
Uncertainty of temperature measurement K 1.47 <1% of value Yes
Uncertainty of absolute pressure in the duct pa 521
Uncertainty associated with the estimate of density - 0.007
Uncertainty associated with the measurement of local velocity - 0.0001Uncertainty associated with the measurement of mean velocity - 0.0001
m/s0.080.16
%1.22.4
m³/hr610
1196
%2.65.1
Expanded Measurement Uncertainty of Volumetric Flow Rate at a 95% Confidence IntervalExpressed as a % of the Measured Volumetric Flow RateExpanded uncertainty at a 95% Confidence Interval
Measured Velocity at Actual Conditions Measured Volumetric Flow rate at Actual Conditions
Measurement Uncertainty - Velocity
Combined uncertaintyExpanded uncertainty at a 95% Confidence Interval
Note - The expanded uncertainty uses a coverage factor of k = 2.
Expanded Measurement Uncertainty of Velocity at a 95% Confidence Interval
Expressed as a % of the Measured VelocityExpanded uncertainty at a 95% Confidence Interval
Measurement Uncertainty Volumetric Flow Rate
Expanded uncertainty at a 95% Confidence Interval
APPENDIX 3 - Measurement Uncertainty Budget Calculations
MEASUREMENT UNCERTAINTY BUDGET - VELOCITY & VOLUMETRIC FLOW RATE
Combined uncertainty
Note - The expanded uncertainty uses a coverage factor of k = 2.
Reference – SOCOTEC Technical Procedure AE150 Estimation of Uncertainty of Measurement
Page 105 of 127
Arrow Group LimitedNaasAEP 12 - Pasta Concepts Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 107 of 134
SOCOTEC UK LTD
www.socotec.co.uk
END OF REPORT
Thank you for choosing SOCOTEC for your environmental monitoring needs. We hope our services have met your requirements and that you are fully satisfied with your experience of working with us, we really do value your custom and would welcome your feedback. We would appreciate it if you could take a
moment to complete a short online questionnaire so that we can improve our operations and address any areas that have not met with your expectations, by clicking on the following
https://www.surveymonkey.co.uk/r/CAE_customer_feedback_weblink
Page 106 of 127
Arrow Group LimitedNaasAEP 12 - Pasta Concepts Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 108 of 134
STACK EMISSIONS MONITORING REPORT
Page 108 of 127
SECTION F Emission Point - AE13 – Simply Soups Concepts Carbon Filter
Date
Site Operator: Arrow Group Limited The Maudlins Industrial Estate Naas Co Kildare
Site Visit Report - SV18614 - Arrow Group Limited Page 109 of 134
SOCOTEC Job Number:Report Date:Version: 1Report By: Daniel ScullyMCERTS Number: MM 19 1563MCERTS Level: MCERTS Level 1 TechnicianTechnical Endorsements:
Report Approved By: David HayMCERTS Number: MM 04 552Business Title: MCERTS Level 2 - Buisness ManagerTechnical Endorsements: 1, 2, 3 & 4
Signature:
2-4 Langlands PlaceKelvin South Business Park
East KilbrideG75 0YF
Tel: 01355 246 730Fax: 01355 249 669
Permit Reference:IE Licence: P0812-01
David HayBusiness Manager - North
Tel: 01355 246 730Email: [email protected]
Your contact at SOCOTEC LTD
Operator & Address:
The Maudlins Industrial Estate Naas
Arrow Group Limited
Co Kildare
Release Point: AEP 13 - Simply Soups Carbon Filter
Sampling Date(s):05/10/2020 & 19/10/2020
28-Oct-20P0812-01CAR20-01
STACK EMISSIONS MONITORING
SOCOTEC UK Reporting Template v6 Page 108 of 127
Site Visit Report - SV18614 - Arrow Group Limited Page 110 of 134
SOCOTEC UK LTD
www.socotec.co.uk
EXECUTIVE SUMMARY
Stack Emissions Monitoring Objectives
- Plant
- Operator
- Stack Emissions Monitoring Test House
Emissions Summary
Monitoring Times
Process Details
Monitoring Methods
Analytical Methods
- Sampling Methods with Subsequent Analysis
- On-Site Testing
Sampling Location
- Sampling Plane Validation Criteria
- Duct Characteristics
- Sampling Lines & Sample Points
- Sampling Platform
- Sampling Location / Platform Improvement Recommendations
Sampling and Analytical Method Deviations
APPENDICES
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
APPENDIX 3 - Measurement Uncertainty Budget Calculations
CONTENTS
Page 109 of 127
Arrow Group LimitedNaasAEP 13 - Simply Soups Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 111 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Plant
AEP 13 - Simply Soups Carbon Filter
Operator
Arrow Group Limited
The Maudlins Industrial Estate
Naas
Co Kildare
IE Licence: P0812-01
Stack Emissions Monitoring Test House
SOCOTEC - East Kilbride Laboratory2-4 Langlands PlaceKelvin South Business ParkEast KilbrideG75 0YFUKAS and MCERTS Accreditation Number: 1015
Opinions and interpretations expressed herein are outside the scope of UKAS accreditation.MCERTS accredited results will only be claimed where both the sampling and analytical stages are UKAS accredited.This test report shall not be reproduced, except in full, without written approval of SOCOTEC LTD.
MONITORING OBJECTIVES
SOCOTEC LTD were commissioned by The Environmental Protection Agency to carry out stack emissions monitoring to determine the release ofprescribed pollutants from the following Plant under normal operating conditions.
Arrow Group Limited operates a production of food products from animal raw materials process at Naas which is subject to IE Licence P0812-01, underthe EPA Act 1992.
EXECUTIVE SUMMARY
The results of these tests shall be used to demonstrate compliance with a set of emission limit values for prescribed pollutants as specified in thePlant's IE Licence, P0812-01.
Page 110 of 127
Arrow Group LimitedNaasAEP 13 - Simply Soups Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 112 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Parameter Units Result Calculated Uncertainty
+/-Odour ouE/m³ 188.00 - -Odour Emission Rate ouE/s 221.69 - -Stack Gas Temperature oC 17 - -Stack Gas Velocity m/s 6.3 0.15 -Gas Volumetric Flow Rate (Actual) m³/hr 4472 228 -Gas Volumetric Flow Rate (STP, Wet) m³/hr 4245 217 -Gas Volumetric Flow Rate (STP, Dry) m³/hr 3396 173 -Gas Volumetric Flow Rate at Reference Conditions m³/hr 4245 217 -
P
MCERTS accredited
result
ND = None Detected,Results at or below the limit of detection are highlighted by bold italic text.The above volumetric flow rate is calculated using data from the preliminary survey. Mass emissions for non isokinetic tests are calculated using these values. For all isokinetic testing the mass emission is calculated using test specific flow data and not the above values.
EXECUTIVE SUMMARY
EMISSIONS SUMMARY
Reference conditions are 273K, 101.3kPa without correction for water vapour
P
Emission Limit Value (ELV)
Page 111 of 127
Arrow Group LimitedNaasAEP 13 - Simply Soups Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 113 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Odour Run 1Odour Run 2Odour Run 3
05 October 202012:41 - 12:45
Preliminary Stack Traverse
12:44 - 12:4910:36 - 10:45
05 October 2020 12:57-13:04 -
4 minutes5 minutes9 minutes19 October 2020
Sampling TimesSampling Date(s)Parameter
EXECUTIVE SUMMARY
Sampling DurationMONITORING TIMES
05 October 2020
Page 112 of 127
Arrow Group LimitedNaasAEP 13 - Simply Soups Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 114 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Description of process Production of Food Products from Animal Raw Materials
Continuous or batch Continuous
Product Details Carbon Filter Odour Unit
Part of batch to be monitored (if applicable) During Carbon Filter Odour Unit Operation
Normal load, throughput or continuous rating Fan Exhust 40.7Hz
Fuel used during monitoring N/A
Abatement Carbon Filter
Plume Appearance None Visible
PROCESS DETAILS
Parameter
EXECUTIVE SUMMARY
Process Details
Page 113 of 127
Arrow Group LimitedNaasAEP 13 - Simply Soups Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 115 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Species SOCOTEC UKAS Lab MCERTS Limit of Calculated CalculatedTechnical Number Accredited Detection MU MUProcedure Method (LOD) +/- % Result +/- % ELV
Odour AE 142 1015 Yes - - N/A - No ELV
Velocity AE 154 1015 Yes 5 Pa 2.4% N/A - No ELV
Volumetric Flow Rate
AE 154 1015 Yes - 5.1% N/A - No ELV
EN 13725
EXECUTIVE SUMMARY
Monitoring Methods
Method
The selection of standard reference / alternative methods employed by SOCOTEC is determined, wherever possible by the hierarchy of methodselection outlined in Environmental Protection Agency Technical Guidance Note (Monitoring) AG2.
Standard Reference Method / Alternative Method
SRM - EN ISO 16911-1
SRM - EN ISO 16911-1
MONITORING METHODS
Page 114 of 127
Arrow Group LimitedNaasAEP 13 - Simply Soups Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 116 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Odour olfactometry 2430 Yes Odournet SOCO20X 201020 8 Weeks
Species Analytical UKAS Lab MCERTS Laboratory Data ArchiveProcedure Number Accredited Archive Period
Analysis Location- - - - - - -
EXECUTIVE SUMMARY
Analytical Technique
olfactometry
Analytical Methods
The following tables list the analytical methods employed together with the custody details. Unless otherwise stated the samples are archived at the analysis lab location.
Analysis LabArchivePeriod
Analytical Procedure
Analytical TechniqueUKAS Lab Number
Species
ON-SITE TESTING
-
UKAS Accredited Lab Analysis
Analysis Report number
SAMPLING METHODS WITH SUBSEQUENT ANALYSIS
Page 115 of 127
Arrow Group LimitedNaasAEP 13 - Simply Soups Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 117 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Sampling Plane Validation Criteria Value Units Requirement Compliant Method
Lowest Differential Pressure 21 Pa >= 5 Pa Yes EN 15259
Lowest Gas Velocity 5.7 m/s - - -
Highest Gas Velocity 6.9 m/s - - -
Ratio of Gas Velocities 1.2 : 1 < 3 : 1 Yes EN 15259
Mean Velocity 6.3 m/s - - -
Maximum angle of flow with regard to duct axis <15 o < 15o Yes EN 15259
No local negative flow Yes - - Yes EN 15259
Value Units Isokinetic
Shape Circular -
Depth 0.50 m Sample port size - 1" BSP
Width - m Number of lines used - 1
Area 0.20 m2 Number of points / line - 1
Port Depth 40 mm Duct orientation - Vertical
Filtration - N/A
General Platform Information
Permanent / Temporary Platform / Ground level / Floor Level / Roof
Inside / Outside
AG1 Platform requirements
Is there a sufficient working area so work can be performed in a compliant manner
Platform has 2 levels of handrails (approximately 0.5 m & 1.0 m high)
Platform has vertical base boards (approximately 0.25 m high)
Platform has removable chains / self closing gates at the top of ladders
Handrail / obstructions do not hamper insertion of sampling equipment
Depth of Platform = >Stack depth / diameter + wall and port thickness + 1.5m
Sampling Platform Improvement Recommendations (if applicable)
SAMPLING PLATFORM
Non-Iso & Gases
Yes
Yes
Yes
The sampling location meets all the requirements as specified in The EPA's Guidance Note AG1.
SAMPLING LOCATION
N/A
DUCT CHARACTERISTICS
EXECUTIVE SUMMARY
Permananet
Yes
Yes
Outside
SAMPLING LINES & POINTS
Page 116 of 127
Arrow Group LimitedNaasAEP 13 - Simply Soups Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 118 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Sample Lines
Undetected Result
Sampling & Analytical Method Deviations
Only 1 sample line is available for carrying out preliminary velocity and temperature traverse as opposed to the 2 sample lines stated inEN 15259 and EPA's AG1 Guidance.
EXECUTIVE SUMMARY
Note, as reported by the lab, Sample 3 "was not sufficiently odorous for enough panel members to generate the necessary number ofITE results required for a valid analysis result in accordance to EN13725". As a result, this sample has been reported as a '0' result inthis report
Page 117 of 127
Arrow Group LimitedNaasAEP 13 - Simply Soups Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 119 of 134
SOCOTEC UK LTD
www.socotec.co.uk
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
APPENDIX 3 - Measurement Uncertainty Budget Calculations
APPENDICES
CONTENTS
Page 118 of 127
Arrow Group LimitedNaasAEP 13 - Simply Soups Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 120 of 134
SOCOTEC UK LTD
www.socotec.co.uk
SOCOTEC UKAS Lab MCERTSTechnical Number AccreditedProcedure Method
AE 142 1015 Yes 3AE 154 1015 Yes 1Velocity
Species
Odour
SRM - EN ISO 16911-1
Standard Reference Method / Alternative Method
MethodNumber of Samples
EN 13725
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
MONITORING SCHEDULE
Page 119 of 127
Arrow Group LimitedNaasAEP 13 - Simply Soups Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 121 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Equipment I.D. Equipment I.D. Equipment I.D.
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
- - -
NOTE: If the equipment I.D is represented by a dash (-), then this piece of equipment has not been used for this test.
Cylinder I.D Number
Supplier ppm %Analytical
Tolerance +/- %
- - - - -
Level Expiry TE1 TE2 TE3 TE4 H&S
Enda Flood MM 12 1170MCERTS Level 2
Apr-23 Mar-24 Mar-24 Jun-23 Nov-23 Apr-23
Aidan Whiteny MM 20 1603MCERTS Trainee
Sep-25 - - - - Sep-25
20m Heated Line (1)
Gas (traceable to ISO 17025)
Barometer
Equipment
Ecophysics NOx Analyser
Heater Controller
Last Impinger Arm
S-Pitot
FT-IR Gasmet
MONITORING TEAM
-
Probe JCT Heated Head Filter
Digital Micromanometer
Bernath 3006 FID Protractor
Personnel
CALIBRATION GASES
FTIR Heater Box for Heated Line
1m Heated Line (3)
10m Heated Line (2)
15m Heated Line (1)
Heated Line Controller (2)
MCERTS Number
TE / H&S Qualifications and Expiry DateMCERTS
Box Thermocouples Tape Measure
Dioxins Cond. Thermocouple 10m Heated Line (1)
Probe Thermocouple
Stackmaster
Meter Out Thermocouple
Control Box Timer
Stack Thermocouple
1m Heated Line (1)
L-Pitot
Oven Box
Control Box DGM
Instrumental Analyser/s
APPENDIX 1 - Monitoring Schedule, Calibration Checklist & Monitoring Team
CALIBRATEABLE EQUIPMENT CHECKLISTMiscellaneousExtractive Sampling
Equipment
Meter In Thermocouple Stopwatch
Probe
FT-IR Oven Box
Equipment
Horiba PG-250 Analyser
Callipers
20m Heated Line (2)
Anemometer
Chiller (JCT/MAK 10)
MFC Display module
Site Balance
5m Heated Line (1)
Small DGM
Heated Line Controller (1)
Site temperature Logger
Inclinometer (Swirl Device)
STACK EMISSIONS MONITORING TEAM
Laboratory Balance
1m Heated Line (2)
Mass Flow Controller
Thermo FID
Digital Temperature Meter
Servomex
Probe Thermocouple
Signal 3030 FID
Page 120 of 127
Arrow Group LimitedNaasAEP 13 - Simply Soups Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 122 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Duration ELV EmissionMinutes ouE/m³ Rate ouE/s
4 - 370.27
5 - 294.80
Run 3 9 - 0.00
Reference conditions are 273K, 101.3kPa without correction for water vapour
Sampling Times
0.00
12:41 - 12:4505 October 2020
Run 1
12:44 - 12:4905 October 2020
Run 2
314.00
Test
250.00
ouE/m³Concentration
10:36 - 10:4519 October 2020
ODOUR SUMMARY
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
Page 121 of 127
Arrow Group LimitedNaasAEP 13 - Simply Soups Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 123 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Stack Diameter / Depth, D 0.50 m
Stack Width, W - m
Stack Area, A 0.20 m2
Average stack gas temperature 17 oC
Stack static pressure 0.058 kPa
Barometric Pressure 102.1 kPa
Component Molar Density Conc Dry Volume Dry Conc Conc Wet Volume Wet ConcMass kg/m3 Dry Fraction kg/m3 Wet Fraction kg/m3
M p % Vol r pi % Vol r pi
CO2 44 1.963059 0.028571 0.000286 0.000561 0.022857 0.000229 0.000449
O2 32 1.427679 21.000000 0.210000 0.299813 16.800000 0.168000 0.239850
N2 28 1.249219 78.971429 0.789714 0.986526 63.177143 0.631771 0.789221
H2O 18 0.803070 - - - 20.000000 0.200000 0.160614
Where: p = M / 22.41 pi = r x p
Determinand
Dry Density (STP), P STD
Wet Density (STP), P STW
Dry Density (Actual), P Actual
Average Wet Density (Actual), P ActualW
Where:
P STD = sum of component concentrations, kg/m3 (not including water vapour) P Actual = P STD x (Ts / Ps) x (Pa / Ta)
P STW = (P STD + pi of H2O) / (1 + (pi of H2O / 0.8036)) P ActualW = P STW x (Ts / Ps) x (Pa / Ta)
1.2217
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
1.1901
kg/m31.2869
kg/m3
Stack Characteristics
Calculation of Stack Gas DensitiesResult
kg/m3
Stack Gas Composition & Molecular Weights
PRELIMINARY STACK SURVEY
1.130
kg/m3
Units
Page 122 of 127
Arrow Group LimitedNaasAEP 13 - Simply Soups Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 124 of 134
SOCOTEC UK LTD
www.socotec.co.uk
TRAVERSE 1
Traverse Distance DP pt DP pt Temp Velocity O2 Angle
Point into Pa mmH2O oC m/s % of Swirl
duct (m)(average of 3
readings)(average of 3
readings)m³/s Vol o
1 0.05 22.9 2.3 17 5.7 1.1 - <152 0.13 30.7 3.1 17 6.6 1.3 - <153 0.38 32.7 3.3 17 6.9 1.3 - <154 0.45 25.5 2.6 17 6.1 1.2 - <15- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -
Mean - 27.9 2.9 17 6.3 1.2 - -
Traverse Distance DP pt DP pt Temp Velocity O2 Angle
Point into Pa mmH2O oC m/s % of Swirl
duct (m)(average of 3
readings)(average of 3
readings)m³/s Vol o
- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -- - - - - - - - -
Mean - - - - - - - -
Start Value End Value Difference Start Value End Value DifferencemmH2O mmH2O % mmH2O mmH2O %
Run 1 122 120 1.6 Pass 134 133 0.7 Pass
RunFinal Reading
(Pa)
Reading After Purge(Pa)
Difference(%)
Outcome(Permitted
+/- 5%)
Run 1 58 57 -1.8 Pass
PRELIMINARY STACK SURVEY QUALITY ASSURANCE CHECKLIST
PRELIMINARY STACK SURVEY
Sampling Line A
Outcome
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
Date of Survey
Velocity Measurement Device:
Volumetric Flow Rate
(actual)
L-Type PitotTime of Survey
L-Type Pitot Blockage Test
Pre Traverse Leak RateOutcomeRun
PITOT LEAK CHECK
To complete a compliant pitot leak check a pressure of over 80 mmH₂O (or 800 Pa) is applied and the pressure drop monitored over 5 mins. A drop of less than 5% must be observed.
Sampling Line B
12:57-13:0405 October 2020
Volumetric Flow Rate
(actual)
Post Traverse Leak Rate
Page 123 of 127
Arrow Group LimitedNaasAEP 13 - Simply Soups Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 125 of 134
SOCOTEC UK LTD
www.socotec.co.uk
EA Technical Guidance Note (Monitoring) M1 Units Requirement Compliant
Lowest Differential Pressure Pa >= 5 Pa Yes
Lowest Gas Velocity m/s - -
Highest Gas Velocity m/s - -
Ratio of Gas Velocities - < 3 : 1 Yes
Maximum angle of flow with regard to duct axis o < 15o Yes
No local negative flow - - Yes
Velocity at Traverse Point, V = Kpt x (1-e) * Ö(2 * DP pt / P ActualW)
Where:Kpt = Pitot tube calibration coefficient(1-e) = Compressibility correction factor, assumed at a constant 0.998
Average Stack Gas Velocity, Va 6.3 m/s
Duct gas flow conditions Actual Reference UnitsTemperature 17 0 oC
Total Pressure 102.158 101.3 kPaOxygen 21.0 21 %Moisture 20.00 20.00 %Pitot tube calibration coefficient, Kpt 0.90
Gas Volumetric Flowrate Units
Average Stack Gas Velocity (Va) m/s
Stack Area (A) m2
Gas Volumetric Flowrate (Actual), QActual m3/hr
Gas Volumetric Flowrate (STP, Wet), QSTP m3/hr
Gas Volumetric Flowrate (STP, Dry), QSTP,Dry m3/hr
Gas Volumetric Flowrate (REF), QRef m3/hr
Where:QActual = Va x A x 3600QSTP = Q (Actual) x (Ts / Ta) x (Pa / Ps) x 3600QSTP,Dry = Q (STP) / (100 - (100 / Ma)) x 3600
QRef = Q (STP) x ((100 - Ma) / (100 - Ms)) x ((21 - O2a) / (21 - O2s))
Nomenclature:Ts = Absolute Temperature, Standard Conditions, 273 KPs = Absolute Pressure, Standard Conditions, 101.3 kPaTa = Absolute Temperature, Actual Conditions, KPa = Absolute Pressure, Actual Conditions, kPaMa = Water vapour, Actual Conditions, % VolMs = Water vapour, Reference Conditions, % VolO2a = Oxygen, Actual Conditions, % VolO2s = Oxygen, Reference Conditions, % Vol
23
Result
0.20
4472
Result
6.9
Calculation of Stack Gas Velocity, V
Calculation of Stack Gas Volumetric Flowrate, Q
3396
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
Sampling Plane Validation Criteria
<15
4245
4245
6.33
5.7
1.2
PRELIMINARY STACK SURVEY (CONTINUED)
Yes
Page 124 of 127
Arrow Group LimitedNaasAEP 13 - Simply Soups Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 126 of 134
SOCOTEC UK LTD
www.socotec.co.uk
Value UnitsStack Depth 0.50 m Sampling Distance Distance into UnitsStack Width - m Point (% of Depth) StackArea 0.20 m2 A 50 0.25 m
Sampling Distance Distance into SwirlPoint (% of Depth) Stack (m) o
- - - -- - - -- - - -- - - -
- - - -
- - - -
- - - -
- - - -- - - -- - - -
- - - -- - - -
- - - -
- - - -- - - -- - - -
Isokinetic sampling point - - - -Isokinetic sampling points not used - - - -Non Isokinetic/Gases sampling point - - - -
- - - -
APPENDIX 2 - Summaries, Calculations, Raw Data and Charts
SAMPLING LOCATION
Non-Isokinetic/Gases Sampling
STACK DIAGRAM
Isokinetic Sampling
Sampling Line A
A
Page 125 of 127
Arrow Group LimitedNaasAEP 13 - Simply Soups Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 127 of 134
SOCOTEC UK LTD
www.socotec.co.uk
6.3 m/s4472 m³/hr
Performance Characteristics & Source of Value Units Values Requirement CompliantUncertainty of Local Gas Velocity Determination
Uncertainty of pitot tube coefficient - 0.010
Uncertainty of mean local dynamic pressures - 0.44
Factor loading, function of the number of measurements. 3 readings 0.591 minimum 3 Yes
Range of measurment device pa 1000
Resolution pa 1.00
Calibration uncertainty pa 5.98<1% of Value or 20
Pa whichever is greater
Yes
Drift % range 0.10
Linearity % range 0.06 <2% of value Yes
Uncertainty of gas density determination
Uncertainty of molar mass determination kg/mol 0.00003
Uncertainty of temperature measurement K 1.48 <1% of value Yes
Uncertainty of absolute pressure in the duct pa 521
Uncertainty associated with the estimate of density - 0.007
Uncertainty associated with the measurement of local velocity - 0.0001Uncertainty associated with the measurement of mean velocity - 0.0001
m/s0.080.15
%1.22.4
m³/hr117228
%2.65.1
Expanded Measurement Uncertainty of Volumetric Flow Rate at a 95% Confidence IntervalExpressed as a % of the Measured Volumetric Flow RateExpanded uncertainty at a 95% Confidence Interval
Measured Velocity at Actual Conditions Measured Volumetric Flow rate at Actual Conditions
Measurement Uncertainty - Velocity
Combined uncertaintyExpanded uncertainty at a 95% Confidence Interval
Note - The expanded uncertainty uses a coverage factor of k = 2.
Expanded Measurement Uncertainty of Velocity at a 95% Confidence Interval
Expressed as a % of the Measured VelocityExpanded uncertainty at a 95% Confidence Interval
Measurement Uncertainty Volumetric Flow Rate
Expanded uncertainty at a 95% Confidence Interval
APPENDIX 3 - Measurement Uncertainty Budget Calculations
MEASUREMENT UNCERTAINTY BUDGET - VELOCITY & VOLUMETRIC FLOW RATE
Combined uncertainty
Note - The expanded uncertainty uses a coverage factor of k = 2.
Reference – SOCOTEC Technical Procedure AE150 Estimation of Uncertainty of Measurement
Page 126 of 127
Arrow Group LimitedNaasAEP 13 - Simply Soups Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 128 of 134
SOCOTEC UK LTD
www.socotec.co.uk
END OF REPORT
Thank you for choosing SOCOTEC for your environmental monitoring needs. We hope our services have met your requirements and that you are fully satisfied with your experience of working with us, we really do value your custom and would welcome your feedback. We would appreciate it if you could take a
moment to complete a short online questionnaire so that we can improve our operations and address any areas that have not met with your expectations, by clicking on the following
https://www.surveymonkey.co.uk/r/CAE_customer_feedback_weblink
Page 127 of 127
Arrow Group LimitedNaasAEP 13 - Simply Soups Carbon Filter
P0812-01CAR20-01 / Version 105/10/2020 19/10/2020
IE Licence: P0812-01Site Visit Report - SV18614 - Arrow Group Limited Page 129 of 134
CERTIFICATE Certificate number SOCO20X_201006 20-10-07 10:33 HD
This certificate is issued with the understanding that neither the issuing laboratory and its owner company nor the United Kingdom Accreditation Service accept any liability for the use of these results. Reproduction of the complete certificate is permitted. Partial reproduction is only permitted after obtaining written permission of the issuing laboratory.
file 201006_SOCO20X_Cert_Bristol
Page 1 of 2
Olfasense UK Ltd Unit 7● Anglo Office Park ● Bristol● BS15 1NT
Phone 01225 868 869 ● [email protected] ● Companies House Cardiff 2900894
Client Organisation SOCOTEC
Contact Enda Flood
Address Office 10, Killowen House
Southern Link Business Park
Naas
Co. Kildare
Telephone 353 0 87 929 5876
Project Project Code SOCO20X_201006
Lab technician Paige Lee-Edmunds
Investigated item Odour concentration in ouE/m³, determined by sensory measurement of odour concentration of an odour sample supplied in a
sampling bag.
The information included within this certificate relates to Olfasense UK’s UKAS accredited odour concentration measurement
procedures including pre-dilution. Sampling procedures and transit conditions are outside of the control of the laboratory and
are not covered within the scope of Olfasense UK's odour concentration measurement accreditation.
Identification The odour sample bags were labelled individually. The label showed the identification of the bag. This identification is
referenced within the results.
Method The odour concentration measurements were performed according to the European Standard EN13725:2003 ‘Air quality –
Determination of odour concentration by dynamic olfactometry’, and according to those parts as described in the internal
procedure QD01: ‘Procedure for olfactometry based on EN13725:2003’. The odour perception characteristic of the panel within
the presentation series for the samples was analogous to that for the butanol calibration. The forced-choice method of
presentation was used and at least two rounds are presented to determine the panel threshold. Sample bags are manufactured
from PET, Nalophane and are not re-used.
Measuring range The dilution range of the olfactometer is 1:147719 to 1:11.4. The lower limit of detection is 30 ouE/m3. If the concentration of
the odour sample exceeded the higher dilution factors the odour sample may have been pre-diluted. If samples are pre-diluted
in the laboratory this is specified under the column Pre-dilution factor Z in Table 1.
Environment The measurements were performed in an air and odour conditioned room, at a temperature of T 25C and with a fluctuation
of less than ±3°C. The CO2 concentration is 0.15%. The laboratory is stationary and permanent.
Dates and times The measurement dates and times are specified together with the results in Table 1.
Results The measurement results are presented in Table 1 of this certificate.
Uncertainty The confidence limits for a value x for one measurement according to EN13725, with a cover factor k = 2 are: x2.40-1
x x2.23. The most recent interlaboratory comparison result is A = 0.095.
Traceability The measurements have been performed using standards for which the traceability to (inter)national standards has been
demonstrated. The assessors are individually selected to comply with fixed criteria and are monitored in time to keep within the
limits set. The results from the assessors are traceable to primary standards (PSM’s) of n-butanol in nitrogen.
Site Visit Report - SV18614 - Arrow Group Limited Page 130 of 134
CERTIFICATE Certificate number SOCO20X_201006 20-10-07 10:33 HD
This certificate is issued with the understanding that neither the issuing laboratory and its owner company nor the United Kingdom Accreditation Service accept any liability for the use of these results. Reproduction of the complete certificate is permitted. Partial reproduction is only permitted after obtaining written permission of the issuing laboratory.
file 201006_SOCO20X_Cert_Bristol
Page 2 of 2
Olfasense UK Ltd Unit 7● Anglo Office Park ● Bristol● BS15 1NT
Phone 01225 868 869 ● [email protected] ● Companies House Cardiff 2900894
Table 1 Measurement results
Analysis file Sample ID Client
Reference
Analysis
result
Pre-dilution factor Z
Odour concentr-
ation
Date and time of
sampling
Date and time of analysis
Number of valid panel
members
Number of
valid ITE
values
Remarks
[ouE.m-3] [ouE.m-3]
201005AEF 20100604 EF 316 983 - 983 05-10-2020
10:28
06-10-2020
12:19
6 12
201005BEF 20100605 EF 317 1196 - 1196 05-10-2020
10:29
06-10-2020
12:27
6 12
201005CEF 20100606 EF 318 719 - 719 05-10-2020
10:34
06-10-2020
12:37
6 12
201005DEF 20100607 EF3 20 771 - 771 05-10-2020
11:07
06-10-2020
12:45
6 12
201005EEF 20100608 EF 321 1077 - 1077 05-10-2020
11:20
06-10-2020
14:30
6 10
201005FEF 20100609 EF 322 115 - 115 05-10-2020
11:55
06-10-2020
14:38
6 8
201005GEF 20100610 EF 323 84 - 84 05-10-2020
12:00
06-10-2020
14:48
6 8
201005HEF 20100611 EF 325 314 - 314 05-10-2020
12:41
06-10-2020
15:15
6 12
201005IEF 20100612 EF 326 250 - 250 05-10-2020
12:45
06-10-2020
15:21
6 12
* Please note the client reference and date/time of sampling is data provided by the client
Certificate approved by:
Holly Dawson
Bristol, 7 October, 2020,
Site Visit Report - SV18614 - Arrow Group Limited Page 131 of 134
CERTIFICATE Certificate number SOCO20X_201020 20-10-21 09:09 A
This certificate is issued with the understanding that neither the issuing laboratory and its owner company nor the United Kingdom Accreditation Service accept any liability for the use of these results. Reproduction of the complete certificate is permitted. Partial reproduction is only permitted after obtaining written permission of the issuing laboratory.
file 201020_SOCO20X_Cert_Bristol
Page 1 of 2
Olfasense UK Ltd Unit 7● Anglo Office Park ● Bristol● BS15 1NT
Phone 01225 868 869 ● [email protected] ● Companies House Cardiff 2900894
Client Organisation SOCOTEC
Contact Enda Flood
Address Office 10, Killowen House
Southern Link Business Park
Jigginstown, Naas
Co. Kildare
Telephone +353 (0) 87 9295876
Project Project Code SOCO20X_201020
Lab technician Paige Lee-Edmunds
Investigated item Odour concentration in ouE/m³, determined by sensory measurement of odour concentration of an odour sample supplied in a
sampling bag.
The information included within this certificate relates to Olfasense UK’s UKAS accredited odour concentration measurement
procedures including pre-dilution. Sampling procedures and transit conditions are outside of the control of the laboratory and
are not covered within the scope of Olfasense UK's odour concentration measurement accreditation.
Identification The odour sample bags were labelled individually. The label showed the identification of the bag. This identification is
referenced within the results.
Method The odour concentration measurements were performed according to the European Standard EN13725:2003 ‘Air quality –
Determination of odour concentration by dynamic olfactometry’, and according to those parts as described in the internal
procedure QD01: ‘Procedure for olfactometry based on EN13725:2003’. The odour perception characteristic of the panel within
the presentation series for the samples was analogous to that for the butanol calibration. The forced-choice method of
presentation was used and at least two rounds are presented to determine the panel threshold. Sample bags are manufactured
from PET, Nalophane and are not re-used.
Measuring range The dilution range of the olfactometer is 1:147719 to 1:11.4. The lower limit of detection is 30 ouE/m3. If the concentration of
the odour sample exceeded the higher dilution factors the odour sample may have been pre-diluted. If samples are pre-diluted
in the laboratory this is specified under the column Pre-dilution factor Z in Table 1.
Environment The measurements were performed in an air and odour conditioned room, at a temperature of T 25C and with a fluctuation
of less than ±3°C. The CO2 concentration is 0.15%. The laboratory is stationary and permanent.
Dates and times The measurement dates and times are specified together with the results in Table 1.
Results The measurement results are presented in Table 1 of this certificate.
Uncertainty The confidence limits for a value x for one measurement according to EN13725, with a cover factor k = 2 are: x2.40-1
x x2.23. The most recent interlaboratory comparison result is A = 0.095.
Traceability The measurements have been performed using standards for which the traceability to (inter)national standards has been
demonstrated. The assessors are individually selected to comply with fixed criteria and are monitored in time to keep within the
limits set. The results from the assessors are traceable to primary standards (PSM’s) of n-butanol in nitrogen.
Site Visit Report - SV18614 - Arrow Group Limited Page 132 of 134
CERTIFICATE Certificate number SOCO20X_201020 20-10-21 09:09 A
This certificate is issued with the understanding that neither the issuing laboratory and its owner company nor the United Kingdom Accreditation Service accept any liability for the use of these results. Reproduction of the complete certificate is permitted. Partial reproduction is only permitted after obtaining written permission of the issuing laboratory.
file 201020_SOCO20X_Cert_Bristol
Page 2 of 2
Olfasense UK Ltd Unit 7● Anglo Office Park ● Bristol● BS15 1NT
Phone 01225 868 869 ● [email protected] ● Companies House Cardiff 2900894
Table 1 Measurement results
Analysis file Sample ID Client
Reference
Analysis
result
Pre-dilution factor Z
Odour concentr-
ation
Date and time of
sampling
Date and time of analysis
Number of valid panel
members
Number of
valid ITE
values
Remarks
[ouE.m-3] [ouE.m-3]
201019AEF 20102011 EF349 – OCU
AEP 12
-- - -- 19-10-2020
10:36
20-10-2020
12:13
5 - The sample was not
sufficiently odorous for
enough panel
members to generate
the necessary number
of ITE results required
for a valid analysis
result in accordance to
EN13725.
201019BEF 20102012 EF350 – AEP 11 115 - 115 19-10-2020
11:02
20-10-2020
12:17
5 10
201019CEF 20102013 EF351 – OCU
AEP 13
-- - -- 19-10-2020
11:23
20-10-2020
12:23
5 - The volume of sample
was insufficient to
complete a valid
analysis in accordance
to EN 13725. The
estimated odour
concentration based
on 5 ITE values is 51
ouE/m3.
201019DEF 20102014 EF352 - WWTP 284 - 284 19-10-2020
12:00
20-10-2020
12:27
5 10
201019EEF 20102015 EF353-WWTP 543 - 543 19-10-2020
12:08
20-10-2020
12:32
5 10
201019FEF 20102016 EF354 - WWTP 389 - 389 19-10-2020
12:15
20-10-2020
12:39
5 10
201019GEF 20102017 EF355 – AEP 8 238 - 238 19-10-2020
12:51
20-10-2020
12:45
5 10
* Please note the client reference and date/time of sampling is data provided by the client
Certificate approved by:
David Donkin
Bristol, 21 October, 2020
Site Visit Report - SV18614 - Arrow Group Limited Page 133 of 134
FOLLOW-UP ACTIONS
You are required to complete the instructions and actions, as outlined in this report, within the specified timeframe. Where required, you shall respond to actions specified in Compliance Investigations within the required timeframe.The licensee shall maintain documentary evidence, for review by the EPA, that the prescribed corrective actions were completed within the required timeframe.
(i) Compliance Investigations
You are not required to respond directly to items contained in this EPA site visit report; where an issue requires a direct response, the EPA will generate a Compliance Investigation through the EDEN system. You will receive notification when a Compliance Investigation instruction or action is generated.
(ii) Publication of reports and licensee response.
Please note that this Site Visit Report will be made available for public viewing via the EPA’s Licence Enforcement Access Portal within one day of the issue date and will be published on the Licence Details Page of the EPA’s website, www.epa.ie, that relates to your licence 60 calendar days after the issue date.
You may if you choose submit, within 45 calendar days of the issue date of this Site Visit Report, a Licensee Public Response that will be published alongside the Site Visit Report. This Response, should you wish to avail of it, provides you with an opportunity to inform the public about how you are implementing the actions set out in the report, activities underway, timescales and target completion dates. Please be aware that the content of your Licensee Public Response must be factual and should not breach the EPAs stated online publication standards.
If you wish to submit a Licensee Public Response to an EPA Site Visit Report, you should do this by clicking on the ‘Make a Response’ link on the Site Visits page in EDEN. A .pdf document containing your response can be attached and submitted from here.
(iii) Response to Site visit report
Where you do wish to respond directly to a site visit report, you should do this by generating a ‘Licensee Return’ of the type ‘Site Updates/Notifications’ and the sub-type ‘Response to EPA Report’ in EDEN.
Please note that you are required to comply with the conditions of your licence at all times, and where noncompliance occurs you must restore compliance within the shortest possible time. These actions will be verified during subsequent EPA visits.
Please quote the above Inspection Reference Number in any future correspondence in relation to this Report.
Site Visit Report - SV18614 - Arrow Group Limited Page 134 of 134