SITE CHARACTERIZATION - Snohomish County Public …€¦ · SITE CHARACTERIZATION ... the findings...

19019 36th Ave West, Suite E | Lynnwood, WA 98036 | Phone: 425.582.9928 | zippergeo.com

SITE CHARACTERIZATION

PROPOSED PORT GARDNER SUBSTATION1210 West Marine View Drive

Everett, Washington

ZGA Project No. 1779.01November 20, 2017

Prepared for:Snohomish County PUD No. 1

Prepared by:

19019 36th Ave West, Suite E | Lynnwood, WA 98036 | Phone: 425.582.9928 | zippergeo.com

Project No. 1779.01November 20, 2017

Snohomish County PUD No. 1Distribution & Engineering Services DivisionPO Box 1107Everett, Washington 98206-1107

Attention: Mr. Jeff Colon, PESubstation Civil/Structural Engineer

Subject: Site CharacterizationProposed Port Gardner Substation1210 West Marine View DriveEverett, Washington

Dear Mr. Colon:

In accordance with your request and written authorization, Zipper Geo Associates, LLC (ZGA) has completed a Site Characterization report for the proposed Port Gardner Substation. This report presents the findings of the subsurface exploration, laboratory testing, and environmental recommendations for the project. Our work was completed in general accordance with the scope of services described in Professional Services Contract No. CW2228393. Written authorization to proceed was provided by theDistrict on 16 February 2017.

We appreciate the opportunity to be of service to you on this project. If you have any questions concerning this report, or if we may be of further assistance, please contact us.

Sincerely,Zipper Geo Associates LLC

Jon Einarsen, LG, LHG David C. Williams, LG, LEGPrincipal Principal

Evelyn ConradoStaff Geologist

Table of Contents1.0 INTRODUCTION................................................................................................................................. 1

1.1 Site Description............................................................................................................................. 1

1.2 Project Information....................................................................................................................... 11.3 Project Objectives ......................................................................................................................... 2

1.4 Standard of Care ........................................................................................................................... 21.5 Reliance......................................................................................................................................... 2

2.0 METHODOLOGY ................................................................................................................................ 2

2.1 Subsurface Exploration ................................................................................................................. 22.2 Soil Sampling ................................................................................................................................. 3

2.3 Groundwater Sampling ................................................................................................................. 32.4 Analytical Laboratory Testing ....................................................................................................... 3

3.0 LIMITED SITE ASSESSMENT RESULTS ................................................................................................ 43.1 Subsurface Conditions .................................................................................................................. 4

3.2 Analytical Laboratory Results........................................................................................................ 4

3.3 Quality Assurance/Quality Control Results................................................................................... 94.0 FINDINGS AND DISCUSSION............................................................................................................10

5.0 RECOMMENDATIONS......................................................................................................................126.0 REFERENCES....................................................................................................................................13

APPENDICES

Appendix A Figure 1 – Site and Exploration Plan

Appendix B Exploration Logs

Appendix C Analytical Laboratory Certificates

Proposed Port Gardner Substation Project No. 1779.01November 20, 2017

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1.0 INTRODUCTION

1.1 Site DescriptionThe project site is located in a parking lot adjoining 1210 West Marine View Drive in Everett, Washington(the Property). The Property is bordered to the north by several warehouse-style buildings occupied by various companies serving the nearby marina with services including diesel engine maintenance, parts manufacturing, boat sales; to the east by West Marine Drive; to the south by a boat yard; and to the west by a parking lot.

The site is located along the Everett waterfront, east of Port Gardner. The former shoreline was located about 200 feet to the east, and the site and surrounding area were filled over the years to create the current waterfront topography. The site and vicinity have a history of industrial land uses dating back to the 1800s.

The Property consists of a small portion of the North Marina Ameron/Hulbert Site, which is part of the PortofEverett’sWaterfrontPlaceRedevelopment project. The Port has previously completed extensive environmental investigations across the entire North Marina Ameron/Hulbert Site, including on the Property. Based on the results of these studies, the potentially liable parties (Port of Everett, Ameron International, and the Hulbert family) have entered into an Agreed Order with Ecology to clean up the North Marina Ameron/Hulbert Site.

According to a Remedial Investigation/Feasibility Study (RI/FS) prepared by Landau Associates in 2014, contaminants of concern (COC) at the overall North Marina Ameron/Hulbert Site consist of carcinogenic polycyclic aromatic hydrocarbons (cPAH), antimony, arsenic, copper, lead, and total petroleum hydrocarbons (TPH) in soil; and copper, arsenic, TPH, 1-1-dichloroethylene, and bis(2-ethylhexyl)phthalate in groundwater.

1.2 Project Information

The project consists of constructing a new single-bank substation. The proposed configuration of the substation is illustrated on the Site and Exploration Plan, Figure 1. Improvements at the site are expected to include:

• The construction of transmission line dead end towers, a circuit switcher, a neutral reactor, and a 12.5 kV switch.

• A new metal-clad switchgear enclosure and slab and a new slab-supported transformer with a perimeter oil containment slab and associated piping.

• The existing site grade is approximately elevation 14 feet, and the substation yard grade is expected to be approximately 2 feet higher.

• Underground electrical conduits will be installed, as well as below-grade pre-cast concrete vaults;• Stormwater will be collected and routed to existing storm sewers which will direct water off-site.• Access to the substation will be provided by an asphalt-paved driveway at the north.

Construction of the substation will require asphalt removal and subsurface work to construct foundations


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for new equipment and installation of utilities. This work may necessitate the removal and off-site disposal of some of the fill soil that underlies the project site, and disposal of construction dewatering effluent.

1.3 Project ObjectivesThe objectives of this project are to characterize the fill soil beneath the project site for potential off-site disposal, to characterize groundwater for potential dewatering activities, and to characterize both soil and groundwater in regard to potential construction worker exposure during earthwork phases of construction.

1.4 Standard of CareThe analytical results within this report are based on samples collected from the indicated locations at the time of sample collection, and should not be construed as a warranty of the subsurface conditions throughout the site or at other times. No environmental investigation can wholly eliminate uncertainty regarding the potential for recognized environmental conditions in connection with a property. This environmental investigation is intended to reduce, but not eliminate, uncertainty regarding the existence of recognized environmental conditions. Within the limitations of scope, schedule and budget for our work, we warrant that our work has been done in accordance with our proposal and generally accepted environmental assessment practices followed in this area at the time the report was prepared. No other warranty, express or implied, is made.

1.5 RelianceThis report has been prepared for the exclusive use of Snohomish County PUD No. 1 and any authorization for use or reliance by any other party (except a governmental entity having jurisdiction over the site) is prohibited without the express written authorization of Snohomish County PUD No. 1 and ZGA.

2.0 METHODOLOGYThis Site Characterization included completion of the following tasks:

1. Advance six direct-push explorations.2. Soil and groundwater sampling.3. Analytical laboratory testing.4. Report preparation, including interpretation of the analytical results relative to cleanup levels

defined in the Model Toxics Control Act (WAC 173-340).

Each of these investigation activities is summarized below.

2.1 Subsurface ExplorationField activities were conducted on April 5, 2017 by Evelyn Conrado, a staff geologist with ZGA, under the supervision of Jon Einarsen, a licensed geologist with ZGA. The approximate location of the explorations in relation to the pertinent structures and general site boundaries are indicated in Figure 1 (Appendix A).Six direct-push soil explorations (GP-1 to GP-6) were advanced. The direct-push sampling device was supplied and operated by Standard Environmental Probe.

The device utilized a direct-push sampler equipped with disposable PVC sample sleeves. Throughout the drilling operation, soil samples were obtained from four-foot long sample intervals using a lined steel sampler driven into the ground using a percussion hammer. The steel sampling tube was extracted from the hole and the liners were removed and split open. Direct-push explorations GP-1 and GP-2 were


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advanced to depths of approximately 22 feet below the ground surface (bgs). Exploration GP-5 and GP-6 were advanced to depths of approximately 20 feet bgs. Explorations GP-3 was advanced to a depth of 24 feet bgs, and GP-4 was advanced to a depth of 23 feet bgs. An effort was made to sample soil continuously from the ground surface to the total depth of each exploration, but sample recovery varied in each exploration.

A field log of each direct-push exploration was maintained, including the thickness and depth of each soil unit encountered and the approximate depth to the uppermost water table. Soil samples were observed to document soil lithology, color, and moisture content. Soils were logged in general accordance with American Society for Testing and Materials (ASTM) Practice Designation D-2488, Standard Practice for Description of Soils (Visual-Manual Procedure). Exploration logs are included in Appendix B of this report.

2.2 Soil SamplingSoil samples retained for chemical analysis and asbestos-containing materials from the direct-push explorations were collected at depths ranging from approximately 4 feet to 24 feet bgs (Table 1). These consisted of 14 fill soil samples and four native soil samples. All soil samples were extracted by hand from the direct-push sample liner using disposable gloves and placed directly into laboratory supplied glassware. Samples designated for the analysis of gasoline were preserved in accordance with EPA Method 5035B.

Each sample container was labeled with the site name, date, time, exploration number, sample number, and sampling personnel. Sample containers were placed in a chilled cooler immediately after sampling, and subsequently transported to the analytical laboratory by ZGA under chain-of-custody procedures.

Investigation-derived waste (IDW, consisting of soil cuttings, temporary monitoring well development water, and equipment cleaning water) generated during the field activities was placed in Department of Transportation (DOT) approved steel drums, closed and appropriately labeled with project-specific information and accumulation date. It is our understanding that the Port of Everett will dispose of the IDW.

2.3 Groundwater SamplingA temporary piezometer was placed into GP-1 and left undisturbed for approximately six hours in an effort to reduce turbidity. The piezometer was subsequently developed with a peristaltic pump until the discharging groundwater was visually clear. Approximately 20 gallons of well development water was placed in a DOT approved steel drum, closed and appropriately labeled with project-specific information and initial accumulation date. A groundwater sample was collected with a peristaltic pump utilizing low flow techniques. The intake of the polyethylene tubing was set approximately one foot below the top of the water table. Discharge from the pump was directed into sample containers supplied by the laboratory.The sample for dissolved metals was field filtered using a 0.45 micron filter.

2.4 Analytical Laboratory TestingEighteen soil samples were submitted for chemical analysis. Soil samples were analyzed by ALS Laboratories of Everett, a Washington State accredited laboratory, as described below:

• Gasoline range hydrocarbons using Northwest Method NWTPH-GX.• Diesel and extended range hydrocarbons using Northwest Method NWTPH-DX using silica gel to


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remove the presence of naturally occurring organic constituents.• Metals (arsenic, lead, copper, and antimony) using EPA Method 6020.• Polycyclic aromatic hydrocarbons (PAH) using EPA Method 8270 SIM.

One groundwater sample was analyzed by ALS Laboratories of Everett as described below:

• Gasoline range hydrocarbons using Northwest Method NWTPH-GX.• Diesel and extended range hydrocarbons using Northwest Method NWTPH-DX using silica gel.• Volatile organic compounds using EPA Method 8260.• Semi-volatile organic compounds using EPA Method 8270.• Polycyclic aromatic hydrocarbons (PAH) using EPA Method 8270 SIM.• Polychlorinated biphenyls (PCB) using EPA Method 8082.• Total and dissolved RCRA 8 metals (mercury, arsenic, barium, cadmium, chromium, lead,

selenium, and silver) and copper and antimony using EPA Method 200.8.

Eighteen soil samples were additionally analyzed for the presence of identifiable asbestos fibers using polarized light microscopy (PLM) in accordance with the EPA 600/R-93-116 test method by NVL Labs of Seattle, Washington.

The executed chain-of-custody forms and laboratory analytical certificates are provided in Appendix C. All analyses were completed using standard turnaround times. Data packages were checked for completeness immediately upon receipt from the laboratory to ensure that data and QA/QC information requested were present. Data quality was assessed by considering holding times, surrogate recovery, method blanks, matrix spike and matrix spike duplicate recovery, and detection limits.

3.0 LIMITED SITE ASSESSMENT RESULTS

3.1 Subsurface ConditionsDetailed lithologic descriptions are presented on the soil boring logs included in Appendix B and are additionally described in our Geotechnical Investigation (submitted under separate cover). In general, subsurface conditions consisted of a heterogeneous mixture of fill soils to depths ranging from about 16to 20 feet beneath the ground surface. The fill soils generally consist of gray sand, silty sand and sandy siltwith varying amounts gravel mixed with shell fragments and black, fine wood fragments. Native soil consisting of gray or brown sand with a trace to some gravel was encountered beneath the fill in all six explorations.

Groundwater was encountered in each of the direct-push borings at depths of about 3 to 3½ feet at the time of probing.

3.2 Analytical Laboratory ResultsThe analytical results for soil presented in Table 1 are compared to Method A cleanup levels defined in the Model Toxics Control Act (MTCA, WAC 173-340). Analytes with no Method A cleanup levels arecompared to the most stringent Method B cleanup levels. Complete laboratory reports and chains-of-custody are included in Appendix C. Additional discussion and interpretation of analytical results relative


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to applicable cleanup levels are included in Section 4.

Laboratory analytical methods have a lowest detectable concentration of an analyte in a sample that can be reported with confidence. This value is referred to as a practical quantification limit (PQL) and is determined by the sample medium, the method of analysis, the technology available for analysis, interference from high levels of other contaminants, and the laboratory’s confidence in the process.Samples with concentrations of analytes that do not exceed PQLs are referred to as non-detect (ND).

Soil QualityEighteen soil samples were collected and analyzed. These included 14 samples of fill soil and four samples of the underlying native sand. Asbestos was not detected in any of the samples. Total petroleum hydrocarbons were not detected in any of the samples, except as noted below:

• Diesel-range and oil-range TPH were detected at concentrations of 31 mg/kg and 160 mg/kg, respectively, in Sample GP5-1, collected at depth of approximately 4 feet. These concentrations are below the Method A cleanup levels established for diesel and oil (2,000 mg/kg).

Polycyclic aromatic hydrocarbons (PAH) were not detected, except as noted below:

• Naphthalene, 2-Methylnaphthalene, acenaphthene, fluorene, phenanthrene, anthracene, fluoranthene, chrysene, and/or pyrene were reported in very low concentrations in samples in GP5-2, GP6-1, GP6-2, and GP6-3. None of the reported concentrations exceeded the most stringent MTCA Method B cleanup level (groundwater protection).

In particular, it should be noted that carcinogenic PAH (cPAH) were not detected in any of the soil samples, except that chrysene was reported at a concentration of 0.021 mg/kg in one sample. The most stringent cleanup level for chrysene is the Method B cleanup level for groundwater protection under saturated conditions, established at 4.77 mg/kg.

Arsenic and lead were detected in every soil sample, but in concentrations below the MTCA Method A cleanup level. Copper was also detected in every sample, and exceeded the Method B cleanup level for groundwater protection in 7 of 18 samples. The reported concentrations for copper do not exceed the Method B cleanup level for direct contact, established at 3,200 mg/kg. As described below, copper was not detected above the PQL in groundwater. Antimony was not detected above the laboratory PQL in any soil sample.

The PQL for antimony (0.50 mg/kg) in soil exceeds the most stringent MTCA Method B cleanup level for groundwater protection (0.272 mg/kg), but does not exceed the Method B cleanup level for direct contact (32 mg/kg). As described below, antimony was not detected above the PQL in groundwater.

Proposed Port Gardner Substation Project No.1779.01May 10, 2017

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Table 1. Summarized Analytical Results (Soil)

SampleApproximate

Depth(Feet)

Soil Type Asbestos

Total Petroleum Hydrocarbons(mg/kg) PAH

(ug/kg)

Metals(mg/kg)

GRO DRO ORO Antimony Arsenic Copper LeadGP1-1 4

FillND ND<3.0 ND<25 ND<50 ND<20 ND<0.50 2.3 9.6 2.3

GP1-2 16 ND ND<3.0 ND<25 ND<50 ND<20 ND<0.50 3.5 11 4.4

GP1-3 22 Native ND ND<3.0 ND<25 ND<50 ND<20 ND<0.50 2.6 15 1.9

GP2-1 4Fill

ND ND<3.0 ND<25 ND<50 ND<20 ND<0.50 4.4 7.1 1.8

GP2-2 14 ND ND<3.0 ND<25 ND<50 ND<20 ND<0.50 8.4 18 7.5


GP3-1 4Fill

ND ND<3.0 ND<25 ND<50 ND<20 ND<0.50 6.0 8.3 2.6

GP3-2 8 ND ND<3.0 ND<25 ND<50 ND<20 ND<0.50 6.9 9.3 2.0


GP4-1 4Fill

ND ND<3.0 ND<25 ND<50 ND<20 ND<0.50 2.5 9.1 2.1

GP4-2 9 ND ND<3.0 ND<25 ND<50 ND<20 ND<0.50 4.2 21 3.9


GP5-1 4

Fill

ND ND<3.0 31 160 ND<20 ND<0.50 3.8 16 3.8

GP5-2 8 ND ND<3.0 ND<25 ND<50 Note A ND<0.50 3.4 18 4.3

GP5-3 15 ND ND<3.0 ND<25 ND<50 ND<20 ND<0.50 4.4 15 7.2

GP6-1 4.5 ND ND<3.0 ND<25 ND<50 Note B ND<0.50 2.0 8.4 14

GP6-2 8 ND ND<3.0 ND<25 ND<50 Note C ND<0.50 2.8 13 2.3

GP6-3 12 ND ND<3.0 ND<25 ND<50 Note D ND<0.50 6.7 14 3.5

WAC 173-340 MTCA Method A Cleanup Level 30/100* 2,000 2,000 Variable 0.272** 20 14.3** 250

mg/kg: milligrams per kilogram (parts-per-million); ND<: Not detected above laboratory PQL; GRO, gasoline-range organics; DRO, diesel-range organics; ORO, oil-range organics; PAH, polycyclic aromatic hydrocarbons. Please refer to Appendix C for the complete set of analytes and analytical results for PAH. *The higher value applies for gasoline mixtures without benzene and the total of toluene, ethylbenzene, and xylenes are less than 1% of the gasoline mixture. ** MTCA Method B cleanup level for the protection of groundwater.

Proposed Port Gardner Substation Project No.1779.01May 10, 2017

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Table 1, Continued

Note A (GP5-2): Naphthalene was reported at a concentration of 0.022 mg/kg, which is below the MTCA Method A cleanup level (5 mg/kg) and the MTCA Method B cleanup level for the protection of groundwater (0.236 mg/kg). No other PAH were detected.

Note B (GP6-1): PAH were not detected, except as noted below:

Analyte Concentration (mg/kg) Cleanup Level (mg/kg)Acenaphthene 0.026 4.98 (Groundwater Protection)Fluorene 0.028 5.12 (Groundwater Protection)Phenanthrene 0.100 Not EstablishedAnthracene 0.040 114 (Groundwater Protection)Fluoranthene 0.054 31.6 (Groundwater Protection)Pyrene 0.033 32.8 (Groundwater Protection)

Note C (GP6-2): PAH were not detected, except as noted below:

Analyte Concentration (mg/kg) Cleanup Level (mg/kg)Naphthalene 0.037 52-Methylnaphthalene 0.026 5Acenaphthene 0.039 4.98 (Groundwater Protection)Fluorene 0.052 5.12 (Groundwater ProtectionPhenanthrene 0.210 Not EstablishedAnthracene 0.051 114 (Groundwater Protection)Fluoranthene 0.130 31.6 (Groundwater Protection)Pyrene 0.077 32.8 (Groundwater Protection)Chrysene 0.021 4.77 (Groundwater Protection)

Note D (GP6-3): PAH were not detected, except as noted below:

Analyte Concentration (mg/kg) Cleanup Level (mg/kg)Phenanthrene 0.036 Not EstablishedAnthracene 0.023 114 (Groundwater Protection)Fluoranthene 0.026 31.6 (Groundwater Protection)

Proposed Port Gardner Substation Project No.1779.01November 20, 2017

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Table 2. Summarized Analytical Results (Groundwater)

Sample

Total Petroleum Hydrocarbons(ug/L) Semi-

VOC(ug/L)

PAH(ug/L)

VOC(ug/L)

PCB(ug/L)

Total Metals(ug/L)

Dissolved Metals(ug/L)

GRO DRO ORO Hg As Ba Cd Total Cr Pb Se Ag Cu Sb Hg As Ba Cd Total

Cr Pb Se Ag Cu Sb

GP-1 <50 <130 <250 ND Note A ND <0.10 <0.20 8.6 16 <1.0 <2.0 <1.0 <4.0 <1.0 <2.0 <2.5 <0.20 8.0 14 <1.0 <2.0 <1.0 <4.0 <1.0 <2.0 <2.5

WAC 173-340 MTCA Method A Cleanup Level

800/1,000* 500 500 Variable Variable Variable 0.1 2 5 2,000** 5 50 15 50** 80** 640** 6.0** Not Established

ug/L: micrograms per liter (parts-per-billion); <: Not detected above laboratory PQL; Shaded values exceed MTCA Method A cleanup levels. GRO, gasoline-range organics; DRO, diesel-range organics; ORO, oil-range organics; Hg, mercury; As, arsenic; Ba, barium; Cd, cadmium; Cr, chromium; Pb, lead; Se, selenium; Ag, silver; Cu, copper; Sb, antimony. Please refer to Appendix C for the complete set of analytes and analytical results for semi-VOC, VOC and PCBs. *The higher value applies for gasoline mixtures without benzene. ** Method B cleanup level.

Note A: Acenaphthene was reported at a concentration of 0.053 ug/L, which is below the Method B cleanup level established at 960 ug/L. No other PAH were reported above the laboratory PQL.


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Groundwater QualityOne groundwater sample was collected from GP-1 using low flow techniques. Total petroleum hydrocarbons, semi-volatile organic compounds, volatile organic compounds, and PCBs were not detected above the PQL in the sample.

A single PAH (acenaphthene) was reported at a concentration of 0.053 ug/L, which is below the Method B cleanup level established at 960 ug/L. No other PAH were detected above the PQL.

Total and dissolved mercury, cadmium, chromium, lead, selenium, silver, copper, and antimony were not detected above the laboratory PQL. Total and dissolved barium were reported at concentrations of 16 ug/L and 14 ug/L, respectively, which is below the Method B cleanup level for groundwater (2,000 ug/L). Total and dissolved arsenic were reported at concentrations of 8.6 and 8.0 ug/L, which exceeds the Method A cleanup level for groundwater (5 ug/L).

We also reviewed the Water Quality Standards for Surface Waters of the State of Washington (WAC 173-201A, August 1, 2016). The most stringent fresh water and marine water quality standards for arsenic are 190 ug/L and 36 ug/l, both of which exceed the concentration of arsenic measured in our study. A surface water quality standard for barium is not defined in WAC 173-201A.

3.3 Quality Assurance/Quality Control ResultsThe analytical results for the current investigation were checked for completeness immediately upon receipt from the laboratory to ensure that data and QA/QC information requested were present. Data quality was assessed by considering hold times, surrogate recovery, method blanks, matrix spike and matrix spike duplicate (MS/MSD) recovery, and detection limits. QA/QC review was completed using guidance described in USEPA Contract Laboratory Program National Functional Guidelines for Superfund Organic Methods Data Review (Draft Final, USEPA, 2005). Our evaluation assumes that the QA/QC is correct as reported by the laboratory, and merely provides an interpretation of the QA/QC results.

Hold Times. All analyses were completed within specified hold times.

Surrogate Recoveries. All surrogate recoveries were within laboratory limits.

Method Blanks. Analytes were not detected in any of the laboratory method blanks.

MS/MSD Results. MS and MSD recoveries were all within laboratory limits, and Relative Percent Differences (RPDs) between MS and MSD recoveries were all within laboratory limits.

Laboratory Reporting Limits. Reporting limits were below relevant MTCA cleanup levels, except as noted below:

• The PQL for antimony (0.50 mg/kg) in soil exceeds the most stringent MTCA Method B cleanup level for groundwater protection (0.272 mg/kg), but does not exceed the Method B cleanup level for direct contact (32 mg/kg). Antimony was not detected above the PQL in groundwater.

Based upon our interpretation of quality control information provided by the laboratories, it is our opinion that the overall dataset is useable as qualified for the purposes of this Phase II Environmental Site Assessment.


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4.0 FINDINGS AND DISCUSSIONZGA completed a Site Characterization for the Port Gardner Substation for the purpose of characterizing the underlying fill soil and groundwater for off-site disposal and for worker health and safety. Six direct-push explorations were advanced to depths of 20 to 24 feet. In general, subsurface conditions consisted of a heterogeneous mixture of fill soils to depths ranging from about 16 to 20 feet beneath the ground surface. The fill soils generally consist of gray sand, silty sand and sandy silt with varying amounts gravel mixed with shell fragments and black, fine wood fragments. Native soil consisting of gray or brown sand with a trace to some gravel was encountered beneath the fill in all six explorations. Groundwater was encountered in each of the direct-push explorations at depths of about 3 to 3½ feet at the time of probing.

Fourteen fill soil samples and four native soil samples were collected and analyzed for asbestos, TPH, PAH and metals (antimony, arsenic, lead, and copper). Asbestos was not detected in any of the soil samples. Diesel-range and oil-range TPH was detected in only one of 18 soil samples, in concentrations below the Method A cleanup levels. Very low concentrations of certain PAH were reported in 4 of 18 soil samples, but in concentrations below the most stringent Method B cleanup levels. Arsenic and lead were reported in concentrations below the Method A cleanup level in all soil samples. Copper was reported in concentrations exceeding the most stringent Method B cleanup level (groundwater protection) in 7 of 18 soil samples, but the concentration of copper did not exceed the Method B cleanup level for direct contact in any of the soil samples. Antimony was not detected in any of the soil samples.

One groundwater sample was collected and analyzed for TPH, PAH, semi-volatile organic compounds(semi-VOC), volatile organic compounds (VOC), PCBs, the RCRA 8 Metals (mercury, arsenic, barium, cadmium, chromium, lead, selenium, and silver) and copper and antimony. TPH, semi-VOC, VOC, PCBs, mercury, cadmium, chromium, lead, selenium, silver, copper and antimony were not detected above the laboratory PQL. Barium was reported at concentrations below the Method B cleanup level. Arsenic was reported at concentrations slightly above the Method A cleanup level.

A Soil and Groundwater Management Plan (SGMP) has been prepared for the Ameron/Hulbert Site by Landau Associates (2017) as part of the overall cleanup efforts at the Site. The purpose of the Plan is to help guide soil and groundwater management during construction and other intrusive activities at the Site, of which the Property comprises a small part. According to the SGMP:

“The requirements thatapply to intrusiveactivities throughout theSite,excluding thedesignated Soil Management Areas (described below), consist of the following:

• All intrusive activities that have the potential to contact contaminated soil will be performed under a Health and Safety Plan that addresses all applicable state and federal requirements.

• Imported material for use as backfill shall meet Site cleanup levels (CULs), which can be exhibited by a quality report either provided by the source or obtained by the Port.

• Information will be submitted to Ecology from the property owner, or in coordination with the property owner if the work was conducted by a third party, documenting the intrusive activities, presenting all environmental data, summarizing post-intrusive activity environmental conditions, and identifying any changes proposed to the restrictive covenant as a result of the intrusive activities.


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Excavated soil shall be handled according to the following requirements:

• Excavated soil that does not contain previously encountered contaminated materials described in Section 4.0 (of the SMGP), or other visual or olfactory indications of potential contamination, may be replaced in the excavation or reused subject to the limitations in the following bullets.

• Excavated material that exhibits any of the conditions of previously encountered contaminated material described in Section 4.0 (of the SMGP), or exhibits other indications of potential contamination (e.g., discoloration, odor), shall be stockpiled separately from unaffected soil and tested to determine appropriate management requirements.

• No excavated soil is to be reused at locations outside of the Site without adequate testing to confirm that the soil does not exceed any MTCA soil CULs.

• Any soil removed from the Site must also meet all other applicable regulations, including the Solid Waste Handling Standards (WAC 173-350).

• Any soil that is tested and exceeds the Site CULs or other applicable criteria must be properlydisposedofatanoffsitepermitteddisposalfacility.”

The SGMP and the RI/FS prepared by Landau (2014, 2017) identify several Soil Management Areas (SMAs) at the Site,includingsome“isolated”SMs. These include an isolated SMA identified as SMA M-1a, which is located on or immediately proximal to the Property. According to the SGMP (page 5-7):

“The location of SMA M-1a is shown on Figure 7. A maximum detected cPAH Toxic Equivalency Quotient concentration of 1.01 mg/kg exceeded the Site CUL along the northern sidewall of an interim action excavation extending to approximately 2 feet bgs conducted south of the Ameron office building. The extent of contamination was bounded in all directions by previous investigations, as shown on Figure 7 and this exceedance appears to be an isolated occurrence.”

These results are generally consistent with our (ZGA) findings, except that cPAH were not detected orwhere detected (chrysene in one sample) was below the Site CULs.

According to the SGMP (page 5-6):

“Soil within the isolated SMAs needs to be properly characterized and managed and, if determined to be contaminated, properly disposed of at an off-site permitted disposal facility. Because soil CUL exceedances were infrequent and/or the concentrations were relatively low, soil characterization may demonstrate that soil within these SMAs do not require management as contaminated soil. Soil characterization can be limited to visual screening for signs of potential contamination if the soil is planned for reuse within the Site. Analytical testing is required if visual screening indicates potential contamination, or if soil is to be reused or disposed of outside of the Site.”

In our opinion, the sampling and analysis described in Section 3 of this Site Characterization report is sufficient to characterize the Property in accordance with the SGMP.


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In regard to groundwater, the SGMP states that:

“TherestrictivecovenantfortheSiterequiresthatgroundwaternotbeusedforpotablewater purposes and that any groundwater extracted for construction dewatering or other non-potable purposes be managed, treated, and discharged in conformance with this Plan. Groundwater extracted for purposes other than construction dewatering is not addressed in this Plan and would require review and approval by Ecology.

Groundwater sampling and testing in advance of construction dewatering would be required to determine management requirements. If testing demonstrates that groundwater does not exceed any of the Site CULs, extracted groundwater could be infiltrated on site, if appropriate, or it could be discharged to the City of Everett sanitary or stormwater sewer systems, subject to obtaining a temporary discharge permit from the City. Alternatively, the contractor could select other means of disposing of extracted groundwater, subject to local, state, and federal regulations.

If groundwater is determined to contain concentrations exceeding Site groundwater CULs, as presented in Table 1, it cannot be infiltrated on site. The groundwater would need to be discharged to the City of Everett sanitary sewer, subject to obtaining a temporary discharge permit, or managed by other means that comply with local, state, andfederalregulations.”

5.0 RECOMMENDATIONSIn general, construction at the Property should be completed in accordance with the SGMP. In accordance with the SGMP, soil to be exported from the site should be stockpiled and analyzed for Site COC prior to off-site disposition. According to Landau (2014) COC in soil at the overall North Marina Ameron/Hulbert Site consist of carcinogenic polycyclic aromatic hydrocarbons (cPAH), antimony, arsenic, copper, lead, and total petroleum hydrocarbons (TPH).

The only CUL exceeded in our groundwater sample was for arsenic, detected at a total metals concentration of 8.6 ug/L. The arsenic CUL is 5 ug/L. The City of Everett waste water limit for arsenic is 500 ug/L (Everett Municipal Code 14.40.080). The most stringent fresh water and marine water quality standards for arsenic are 190 ug/L and 36 ug/l (WAC 173-201A). Based on these parameters, it is our opinion that construction dewatering effluent can likely be discharged to the City of Everett sanitary seweror stormwater sewer. A permit may be needed, and the groundwater may need to be treated for turbidity and analyzed for Site COC prior to discharge. According to Landau (2014), COC in groundwater at the overall North Marina Ameron/Hulbert Site consist of copper, arsenic, TPH, 1-1-dichloroethylene, and bis(2-ethylhexyl) phthalate in groundwater.

Based on the results for arsenic in groundwater at the Property, and because other COC that exceed human health direct contact cleanup levels have been identified elsewhere on the North Marina Ameron/Hulbert Site, it is our opinion that the earthwork contractor will need to prepare a site Health and Safety Plan (HASP) to satisfy the requirements as set forth in 29 CFR 1910.120 and Chapter 296-843 WAC intended to ensure safe work practices. This HASP should also apply to all subcontractors during excavation and shoring when working on the Property. The earthwork contractor should make available an appropriate number of employees who satisfy the requirements as set forth in the contractor-specific Health and Safety Plan. In particular, a select number of the contractors’workforceshould be responsible


Page | 13

for providing documentation of current 40-hour OSHA training (or annual 8-hour refresher course) in accordance with 29 CFR 1910.120.

6.0 REFERENCESLandau Associates, 2014, Final Remedial Investigation/Feasibility Study, North Marina Ameron/Hulbert Site, Everett, Washington.

Landau Associates, 2017, Soil and Groundwater Management Plan, Ameron/Hulbert Site, Everett, Washington.

APPENDIX A

FIGURES

B-2

B-1

GP-3

GP-4

GP-5

GP-1

GP-2

GP-6

A

'

A

REFERENCE: CONCEPTUAL SITE PLAN PROVIDED BY SNOHOMISH PUD, SEPT. 9, 2016

FIGUREJob No.

Zipper Geo Associates, LLC19023 36th Ave. W.,Suite D

Lynnwood, WA

SHT. of 11

SITE AND EXPLORATION PLAN

1779.01DATE: APRIL 2017

1

PORT GARDNER SUBSTATION1210 Marine View Drive

Everett, Washington

SCALE IN FEET

020 2010

LEGEND

B-1 BORING NUMBER AND

APPROXIMATE LOCATION

GP-1 GEOPROBE NUMBER AND

APPROXIMATE LOCATION

APPENDIX B

EXPLORATION LOGS

GEOPROBE BORING LOGProject Number : 1779.01Boring Number : GP-1

Project Name : Port Gardner Substation Ground Surface Elevation : NALocation : North, middle of parking lot Depth to Water : 3.15 ftDriller / Crew : Standard Environmental Probe Start / Finish Date : 4/05/17

Depth (ft.)

Monitoring Well Completion

Sample ID / Recovery (in.)

Laboratory Samples PID (ppm) Sheen Description

Depth (ft.)

Approximately 3-inches of asphalt.None

ND

GP1-15 5

NoneND

None

10 ND 10

None

0.215 15

GP1-2

ND

20 20Sampler Type Static Water Level Logged by: EICContinuous Core Water Level (ATD) Approved by: JME

Gray, silty fine SAND, some wood fragments, saturated, moderate odor (not hydrocarbon).

At 19 1/2 ft, gray, gravelly fine to medium SAND, medium dense, moist, moderate odor (not hydrocarbon).

Sheet 1 of 2Zipper Geo Associates, LLC

Gray, fine to medium SAND with shell fragments, moist. (Fill)

Gray, fine SAND with trace silt, some wood fragments, grading to gray, silty SAND, and grading to gray, fine SAND, saturated. (Fill)

S1/36

S2/42

S3/42

S4/42

S5/42

Gray, fine SAND with trace silt, some wood fragments, saturated, no odor.

Gray, SILT with fine sand, grading to silty fine SAND, saturated, moderate odor (not hydrocarbon).


Project Name : Port Gardner Substation Ground Surface Elevation : NALocation : North, middle of parking lot Depth to Water : 3.15 ftDriller / Crew : Standard Environmental Probe Start / Finish Date : 4/05/17

Depth (ft.)




Depth (ft.)

20 None

GP1-3 NDBoring terminated at 22 ft due to heaving.

25 25

30 30

35 35



S6/24

Brown, fine to medium SAND with trace gravel at 21 ft, medium dense, moist, no odor. (Native)


Project Name : Port Gardner Substation Ground Surface Elevation : NALocation : East side of parking lot Depth to Water : 3.5 ftDriller / Crew : Standard Enviromental Probe Start / Finish Date : 4/05/17

Depth (ft.)




Depth (ft.)


ND

GP2-1 1-inch lense of gray, silty SAND.

None5 5

ND

None

10 ND 10

None

GP2-2 0.415 15

None

ND

GP2-3 None


Gray, fine SAND with trace silt, saturated, moderate odor (none hydrocarbon). At 19 1/2 ft, 4-inch lense of gravel.

At 19.9 ft, gray, gravelly fine to medium SAND, medium dense, moist, moderate odor (not hydrocarbon).


S1/30

S2/30

S3/42

S4/36

S5/36

Brown, fine to medium SAND with shell fragments, moist, moderate odor (not hydrocarbon). (Fill)

Gray, fine SAND, grading to gray, silty SAND, some wood fragments, saturated, moderate odor (not hydrocarbon). (Fill)

Gray, fine SAND with trace silt, some wood fragments, saturated, moderate odor (not hydrocarbon). (Fill)

Gray, SILT with fine sand, some wood fragments, wet, moderate odor (not hydrocarbon). (Fill)


Project Name : Port Gardner Substation Ground Surface Elevation : NALocation : East side of parking lot Depth to Water : 3.5 ftDriller / Crew : Standard Environmental Probe Start / Finish Date : 4/5/17

Depth (ft.)




Depth (ft.)

20 None

Boring terminated at 22 ft due to heaving.

25 25

30 30

35 35



S6/24

Brown, fine to medium SAND with trace gravel, grading to fine to medium SAND, saturated, no odor. (Native)


Project Name : Port Gardner Substation Ground Surface Elevation : NALocation : SE of parking lot near boat yard fence Depth to Water : 3.0 ftDriller / Crew : Standard Environmental Probe Start / Finish Date : 4/05/17

Depth (ft.)




Depth (ft.)


ND

GP3-1None

5 5

ND

GP3-2

None

10 ND 10

None

ND

15 15

0.5 None

20 4-inch gravel layer with wood fragments. 20Sampler Type Static Water Level Logged by: EICContinuous Core Water Level (ATD) Approved by: JME

Sheet 1 of 2

S5/24

Brown, gravelly SAND with shell fragments, moist, moderate odor (not hydrocarbon). (Fill)

Gray, silty SAND, some with wood fragments, saturated, moderate odor (not hydrocarbon). (FILL)

Zipper Geo Associates, LLC

S1/42

S2/42

S3/42

S4/24

Gray, gravelly SAND with some silt, saturated, moderate odor (not hydrocarbon). (Fill)

Gray, fine SAND with trace silt grading to gray, silty SAND, some shell fragments, moist to wet, moderate odor (not hydrocarbon). (Fill)

At 11 1/2 ft, gray, SILT with fine sand, wet, moderate odor (not hydrocarbon).

Gray, SILT with fine sand grading to gray, silty fine SAND, some wood fragments, saturated to wet, moderate odor (not hydrocarbon). (Fill)


Project Name : Port Gardner Substation Ground Surface Elevation : NALocation : SE of parking lot near boat yard fence Depth to Water : 3.0 ftDriller / Crew : Standard Environmental Probe Start / Finish Date : 4/5/17

Depth (ft.)




Depth (ft.)

20 None

ND

GP3-3Boring terminated at 24 ft due to heaving.

25 25

30 30

35 35



S6/48

Brown, fine to medium SAND with trace gravel, moist, no odor. (Native)


Project Name : Port Gardner Substation Ground Surface Elevation : NALocation : SW of parking lot near boat yard Depth to Water : 3.5 ftDriller / Crew : Standard Environmental Probe Start / Finish Date : 4/05/17

Depth (ft.)




Depth (ft.)


GP4-1 0.9None

5 5

ND

Some wood fragments.

NoneGP4-2

10 ND 10

None

ND

15 15

No recovery.


S5/0

Gray, fine to medium SAND, moist, strong odor (not hydrocarbon). (Fill)

Gray, fine SAND with trace silt, moist, moderate odor (not hydrocarbon). (Fill)

Gray, fine SAND with trace silt grading to gray silty SAND, some wood fragments, saturated, moderate odor (not hydrocarbon). (Fill)

Gray, silty SAND, some wood fragments, saturated, no odor. (Fill)

At 15 ft, gray, SILT with some fine sand, wood fragments, moist, moderate odor (not hydrocarbon). (Fill)

S4/18


S1/42

S2/42

S3/48


Project Name : Port Gardner Substation Ground Surface Elevation : NALocation : SW of parking lot near boat yard fence Depth to Water : 3.50 ftDriller / Crew : Standard Environmental Probe Start / Finish Date : 4/05/17

Depth (ft.)




Depth (ft.)

20 None

ND

GP4-3Boring terminated at 23 ft due to heaving.

25 25

30 30

35 35



S6/36

Brown, fine to medium SAND with some gravel, moist, no odor.


Project Name : Port Gardner Substation Ground Surface Elevation : NALocation : West side of parking lot Depth to Water : 3 ftDriller / Crew : Standard Environmental Probe Start / Finish Date : 4/05/17

Depth (ft.)




Depth (ft.)


GP5-1 0.9None

5 5

ND

GP5-2None

10 ND 10

None

ND

15 GP5-3 15

NDNone

20 Boring terminated at 20 ft due to heaving. 20Sampler Type Static Water Level Logged by: EICContinuous Core Water Level (ATD) Approved by: JME

S3/24

S4/42

S5/42

Gray, medium SAND with shall fragments, some wood fragments, moist, moderate odor (potentially hydrocarbon). (Fill)

Gray, silty fine SAND, some wood fragments, moist. (Fill)

Gray, silty fine SAND, some wood fragments, saturated. (Fill)

Gray, silty fine SAND grading to black, silty fine SAND, some wood fragments, saturated. (Fill)

Gray, medium SAND with some silt, trace gravel and wood fragments, wet, moderate odor (potentially hydrocarbon). (Fill)

Gray, fine to medium SAND with some gravel, saturated.

Brown, gravelly SAND, saturated to moist, no odor. (Native)


Gray, fine to medium SAND, some wood fragments, moist, moderate odor (potentially hydrocarbon). (Fill)

S1/30

S2/42


Project Name : Port Gardner Substation Ground Surface Elevation : NALocation : North of parking lot near gate entrance Depth to Water : 3.5 ftDriller / Crew : Standard Environmental Probe Start / Finish Date : 4/05/17

Depth (ft.)




Depth (ft.)


0.9

None5 GP6-1 5

ND

GP6-2None

10 ND 10

GP6-3No recovery.

15 15

None

ND

20 Boring terminated at 20 ft due to heaving. 20Sampler Type Static Water Level Logged by: EICContinuous Core Water Level (ATD) Approved by: JME

Brown, fine to medium SAND containing pyrite with gravel, saturated, no odor. (Native)


S1/30

S2/48

S3/24

S4/0

S5/36

Gray, fine to medium SAND with gravel, moist, strong odor (not hydrocarbon). (Fill)

At 3 1/2 ft, wood layer with strong odor (not hydrocarbon).

Gray, fine to medium SAND, trace shell and wood fragments, moist, strong to moderate odor (not hydrocarbon). (Fill)

Gray, silty fine SAND, moist, moderate odor (not hydrocarbon). (Fill)

APPENDIX C

ANALYTICAL LABORATORY CERTIFICATES

Nick Ly, Technical Director

Client Project: Port Gardner SubstationLocation: Everett, WA

Dear Mr. Einarsen ,

Enclosed please find test results for the 18 sample(s) submitted to our laboratory for analysis on4/6/2017.

Examination of these samples was conducted for the presence of identifiable asbestos fibers usingpolarized light microscopy (PLM) with dispersion staining in accordance with both EPA 600/M4-82-020,Interim Method for the Determination of Asbestos in Bulk Insulation Samples and EPA 600/R-93/116Method for the Determination of Asbestos in Bulk Building Materials.

For samples containing more than one separable layer of materials, the report will include findings foreach layer (labeled Layer 1 and Layer 2, etc. for each individual layer). The asbestos concentration inthe sample is determined by calibrated visual estimation.

For those samples with asbestos concentrations between 1 and 10 percent based on visual estimation,the EPA recommends a procedure known as point counting (NESHAPS, 40 CFR Part 61). Pointcounting is a statistically more accurate means of quantification for samples with low concentrations ofasbestos.

The detection limit for the calibrated visual estimation is <1%, 400 point counts is 0.25% and 1000 pointcounts is 0.1%

Samples are archived for two weeks following analysis. Samples that are not retrieved by the client arediscarded after two weeks.

Thank you for using our laboratory services. Please do not hesitate to call if there is anything further wecan assist you with.

Sincerely,

Enc.: Sample Results

April 13, 2017

Jon EinarsenZipper Geo Associates, LLC19023 36th Avenue West, Suite DLynnwood, WA 98036

RE: Bulk Asbestos Fiber Analysis; NVL Batch # 1706115.00

page 1 of 9

< Client:Address:

Attention: Mr. Jon EinarsenEverett, WA

Client Project #: Port Gardner Substation

Samples Received: 18

By Polarized Light MicroscopyBulk Asbestos Fibers Analysis

Zipper Geo Associates, LLC19023 36th Avenue West, Suite DLynnwood, WA 98036

Method: EPA/600/R-93/116& EPA/600/M4-82-020

Samples Analyzed: 18Project Location:

Batch #: 1706115.00

Date Received: 4/6/2017

17032045Lab ID: Client Sample #:Location: Everett, WAComments: Qualitative analysis was conducted for the presence of asbestos fibers in this sample.

GP1-1

Layer 1 of 1 Description: Gray sandy materialNon-Fibrous Materials: Other Fibrous Materials:% Asbestos Type: %

Sand, Fine grains Cellulose None Detected ND


GP1-2




GP1-3




GP2-1

Layer 1 of 1 Description: Beige sandy materialNon-Fibrous Materials: Other Fibrous Materials:% Asbestos Type: %

Sand, Fine grains NDNone Detected None Detected ND

Note: If samples are not homogeneous, then subsamples of the components were analyzed separately. All bulk samples are analyzed using both EPA600/R-93/116 and 600/M4-82-020 Methods with the following measurement uncertainties for the reported % Asbestos (1%=0-3%, 5%=1-9%, 10%=5-15%,20%=10-30%, 50%=40-60%). This report relates only to the items tested. If sample was not collected by NVL personnel, then the accuracy of the results islimited by the methodology and acuity of the sample collector. This report shall not be reproduced except in full, without written approval of NVLLaboratories, Inc. It shall not be used to claim product endorsement by NVLAP or any other agency of the US Government

ClientJacob LaugesonAnalyzed by:Nick LyReviewed by:

04/12/2017 Date:04/13/2017Date:

Sampled by:


page 2 of 9

< Client:Address:






Method: EPA/600/R-93/116& EPA/600/M4-82-020


Batch #: 1706115.00



GP2-2


Sand, Fine grains Wood fibers None Detected ND


GP2-3




GP3-1




GP3-2





04/12/2017 Date:04/13/2017Date:

Sampled by:


page 3 of 9

< Client:Address:






Method: EPA/600/R-93/116& EPA/600/M4-82-020


Batch #: 1706115.00



GP3-3


Sand, Mineral grains NDNone Detected None Detected ND


GP4-1




GP4-2




GP4-3





04/12/2017 Date:04/13/2017Date:

Sampled by:


page 4 of 9

< Client:Address:






Method: EPA/600/R-93/116& EPA/600/M4-82-020


Batch #: 1706115.00



GP5-1




GP5-2




GP5-3




GP6-1





04/12/2017 Date:04/13/2017Date:

Sampled by:


page 5 of 9

< Client:Address:






Method: EPA/600/R-93/116& EPA/600/M4-82-020


Batch #: 1706115.00



GP6-2




GP6-3





04/12/2017 Date:04/13/2017Date:

Sampled by:


page 6 of 9

Zipper Geo Associates, LLC 1706115.00

18

Company NVL Batch Number

Total Number of Samples

Everett, WA

5 DaysTAT

4/13/2017Due Date 1:10 PMTime

(425) [email protected]

Project Manager Mr. Jon Einarsen(425) 582-9928Phone

Rush Samples

Rush TATNoAH

Port GardnerSubstation

Project Name/Number: Project Location:

Sample ID Description A/RLab ID

ASBESTOS LABORATORY SERVICES

Subcategory

Item Code

PLM Bulk

MetalsASB-02 EPA 600/R-93-116 Asbestos by PLM <bulk>

19023 36th Avenue West, Suite DLynnwood, WA 98036

Address

GP1-11 A17032045GP1-22 A17032046GP1-33 A17032047GP2-14 A17032048GP2-25 A17032049GP2-36 A17032050GP3-17 A17032051GP3-28 A17032052GP3-39 A17032053GP4-110 A17032054GP4-211 A17032055GP4-312 A17032056GP5-113 A17032057GP5-214 A17032058GP5-315 A17032059GP6-116 A17032060GP6-217 A17032061GP6-318 A17032062

Office Use Only Print Name Company Date TimeSignature

Faxed Emailed

Company Date TimeSignatureClientSampled by

Jacob LaugesonReceived by

ClientRelinquished by

Jacob LaugesonAnalyzed byResults Called by

NVLNVL

4/6/174/12/17

1310

Print Name

Entered By: Jacob Laugeson

Date: 4/6/2017Time: 1:48 PM

SpecialInstructions:

page 7 of 9

Mr. Jon EinarsenZipper Geo Associates19023 - 36th Ave W., Suite DLynnwood, WA 98036

Dear Mr. Einarsen,

On April 6th, 19 samples were received by our laboratory and assigned our laboratory project number EV17040044. The project was identified as your 1779.01. The sample identification and requested analyses are outlined on the attached chain of custody record.

No abnormalities or nonconformances were observed during the analyses of the project samples.

Please do not hesitate to call me if you have any questions or if I can be of further assistance.

Sincerely,

ALS Laboratory Group

Rick BaganLaboratory Director

May 5, 2017

Page 1

ADDRESS PHONE FAX| |8620 Holly Drive, Suite 100, Everett, WA 98208 425-356-2600 425-356-2626ALS Group USA, Corp dba ALS Environmental

CERTIFICATE OF ANALYSIS

CLIENT PROJECT: 1779.01CLIENT SAMPLE ID GP1-1

COLLECTION DATE: 4/5/2017 9:51:00 AM

CLIENT: Zipper Geo Associates19023 - 36th Ave W., Suite DLynnwood, WA 98036

EV17040044ALS SAMPLE#: EV17040044-01

DATE: 5/5/2017

DATA RESULTSWDOE ACCREDITATION: C601

CLIENT CONTACT: Jon Einarsen DATE RECEIVED: 04/06/2017

DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE

DILUTION FACTOR UNITS

LIMITSXXXXX XXX

REPORTING LIMITSRESULTSMETHOD

ANALYSIS DATE

ANALYSIS BY

QUALXXXXX

04/07/2017 SNC13.0 0.72 U1U 04/07/2017MG/KGTPH-Volatile Range NWTPH-GX XXX3.0 XXXXX XXXXXXXX04/12/2017 EBS125 9.9 U1U 04/11/2017MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25 XXXXX XXXXXXXX04/12/2017 EBS150 19 U1U 04/11/2017MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50 XXXXX XXXXXXXX04/18/2017 GAP120 2.7 U1U 04/17/2017UG/KGNaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.3 U1U 04/17/2017UG/KG2-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.7 U1U 04/17/2017UG/KG1-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.4 U1U 04/17/2017UG/KGAcenaphthylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.2 U1U 04/17/2017UG/KGAcenaphthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.2 U1U 04/17/2017UG/KGFluorene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.3 U1U 04/17/2017UG/KGPhenanthrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.6 U1U 04/17/2017UG/KGAnthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.5 U1U 04/17/2017UG/KGFluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.8 U1U 04/17/2017UG/KGPyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.8 U1U 04/17/2017UG/KGBenzo[A]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.8 U1U 04/17/2017UG/KGChrysene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.7 U1U 04/17/2017UG/KGBenzo[B]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.0 U1U 04/17/2017UG/KGBenzo[K]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.0 U1U 04/17/2017UG/KGBenzo[A]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.5 U1U 04/17/2017UG/KGIndeno[1,2,3-Cd]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.2 U1U 04/17/2017UG/KGDibenz[A,H]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.7 U1U 04/17/2017UG/KGBenzo[G,H,I]Perylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.28 U5U 04/17/2017MG/KGAntimony EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL51.0 0.86 5 04/17/20172.3 MG/KGArsenic EPA-6020 XXX1.0 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.28 5 04/17/20179.6 MG/KGCopper EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.28 5 04/17/20172.3 MG/KGLead EPA-6020 XXX0.50 XXXXX XXXXXXXX

MINSURROGATE

SPIKE ADDED

LIMITSXXXXX XXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS DATE

ANALYSIS BY

QUALXXXXX

04/07/2017 SNC1140 0.409 04/07/201773.5 TFT NWTPH-GX XXX60 XXXXX XXXXX XXXXXXXXXXXXX04/12/2017 EBS1134 4.19 04/11/201778.4 C25 NWTPH-DX w/ SGA XXX58 XXXXX XXXXX XXXXXXXXXXXXX04/18/2017 GAP1157 841 04/17/201771.8 Terphenyl-d14 EPA-8270 SIM XXX28.9 XXXXX XXXXX XXXXXXXXXXXXX

U - Analyte analyzed for but not detected at level above reporting limit.

Page 2






EV17040044ALS SAMPLE#: EV17040044-02

DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE


LIMITSXXXXX XXX


ANALYSIS DATE

ANALYSIS BY

QUALXXXXX

04/07/2017 SNC13.0 0.88 U1U 04/07/2017MG/KGTPH-Volatile Range NWTPH-GX XXX3.0 XXXXX XXXXXXXX04/12/2017 EBS125 10 U1U 04/11/2017MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25 XXXXX XXXXXXXX04/12/2017 EBS150 20 U1U 04/11/2017MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50 XXXXX XXXXXXXX04/18/2017 GAP120 3.0 U1U 04/17/2017UG/KGNaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.7 U1U 04/17/2017UG/KG2-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.0 U1U 04/17/2017UG/KG1-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.7 U1U 04/17/2017UG/KGAcenaphthylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.5 U1U 04/17/2017UG/KGAcenaphthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.7 U1U 04/17/2017UG/KGFluorene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.9 U1U 04/17/2017UG/KGPhenanthrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.1 U1U 04/17/2017UG/KGAnthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.9 U1U 04/17/2017UG/KGFluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.3 U1U 04/17/2017UG/KGPyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.1 U1U 04/17/2017UG/KGBenzo[A]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.3 U1U 04/17/2017UG/KGChrysene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.2 U1U 04/17/2017UG/KGBenzo[B]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.5 U1U 04/17/2017UG/KGBenzo[K]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.4 U1U 04/17/2017UG/KGBenzo[A]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.0 U1U 04/17/2017UG/KGIndeno[1,2,3-Cd]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.8 U1U 04/17/2017UG/KGDibenz[A,H]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 5.4 U1U 04/17/2017UG/KGBenzo[G,H,I]Perylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.31 U5U 04/17/2017MG/KGAntimony EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL51.0 0.97 5 04/17/20173.5 MG/KGArsenic EPA-6020 XXX1.0 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.31 5 04/17/201711 MG/KGCopper EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.31 5 04/17/20174.4 MG/KGLead EPA-6020 XXX0.50 XXXXX XXXXXXXX

MINSURROGATE

SPIKE ADDED

LIMITSXXXXX XXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS DATE

ANALYSIS BY

QUALXXXXX



Page 3






EV17040044ALS SAMPLE#: EV17040044-03

DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE


LIMITSXXXXX XXX


ANALYSIS DATE

ANALYSIS BY

QUALXXXXX


MINSURROGATE

SPIKE ADDED

LIMITSXXXXX XXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS DATE

ANALYSIS BY

QUALXXXXX



Page 4






EV17040044ALS SAMPLE#: EV17040044-04

DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE


LIMITSXXXXX XXX


ANALYSIS DATE

ANALYSIS BY

QUALXXXXX


MINSURROGATE

SPIKE ADDED

LIMITSXXXXX XXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS DATE

ANALYSIS BY

QUALXXXXX



Page 5






EV17040044ALS SAMPLE#: EV17040044-05

DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE


LIMITSXXXXX XXX


ANALYSIS DATE

ANALYSIS BY

QUALXXXXX


MINSURROGATE

SPIKE ADDED

LIMITSXXXXX XXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS DATE

ANALYSIS BY

QUALXXXXX

04/07/2017 SNC1140 0.492 04/07/201785.8 TFT NWTPH-GX XXX60 XXXXX XXXXX XXXXXXXXXXXXX04/12/2017 EBS1134 4.57 04/11/2017105 C25 NWTPH-DX w/ SGA XXX58 XXXXX XXXXX XXXXXXXXXXXXX04/18/2017 GAP1157 964 04/17/201768.2 Terphenyl-d14 EPA-8270 SIM XXX28.9 XXXXX XXXXX XXXXXXXXXXXXX


Page 6






EV17040044ALS SAMPLE#: EV17040044-06

DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE


LIMITSXXXXX XXX


ANALYSIS DATE

ANALYSIS BY

QUALXXXXX


MINSURROGATE

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Page 7




COLLECTION DATE: 4/5/2017 12:56:00 PM


EV17040044ALS SAMPLE#: EV17040044-07

DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE


LIMITSXXXXX XXX


ANALYSIS DATE

ANALYSIS BY

QUALXXXXX

04/07/2017 SNC13.0 0.80 U1U 04/07/2017MG/KGTPH-Volatile Range NWTPH-GX XXX3.0 XXXXX XXXXXXXX04/12/2017 EBS125 10 U1U 04/11/2017MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25 XXXXX XXXXXXXX04/12/2017 EBS150 20 U1U 04/11/2017MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50 XXXXX XXXXXXXX04/18/2017 GAP120 2.7 U1U 04/17/2017UG/KGNaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.3 U1U 04/17/2017UG/KG2-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.7 U1U 04/17/2017UG/KG1-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.4 U1U 04/17/2017UG/KGAcenaphthylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.3 U1U 04/17/2017UG/KGAcenaphthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.3 U1U 04/17/2017UG/KGFluorene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.4 U1U 04/17/2017UG/KGPhenanthrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.7 U1U 04/17/2017UG/KGAnthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.6 U1U 04/17/2017UG/KGFluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.8 U1U 04/17/2017UG/KGPyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.8 U1U 04/17/2017UG/KGBenzo[A]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.9 U1U 04/17/2017UG/KGChrysene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.8 U1U 04/17/2017UG/KGBenzo[B]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.1 U1U 04/17/2017UG/KGBenzo[K]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.1 U1U 04/17/2017UG/KGBenzo[A]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.6 U1U 04/17/2017UG/KGIndeno[1,2,3-Cd]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.3 U1U 04/17/2017UG/KGDibenz[A,H]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.8 U1U 04/17/2017UG/KGBenzo[G,H,I]Perylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.29 U5U 04/17/2017MG/KGAntimony EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL51.0 0.89 5 04/17/20176.0 MG/KGArsenic EPA-6020 XXX1.0 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.29 5 04/17/20178.3 MG/KGCopper EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.29 5 04/17/20172.6 MG/KGLead EPA-6020 XXX0.50 XXXXX XXXXXXXX

MINSURROGATE

SPIKE ADDED

LIMITSXXXXX XXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS DATE

ANALYSIS BY

QUALXXXXX



Page 8






EV17040044ALS SAMPLE#: EV17040044-08

DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE


LIMITSXXXXX XXX


ANALYSIS DATE

ANALYSIS BY

QUALXXXXX

04/07/2017 SNC13.0 0.75 U1U 04/07/2017MG/KGTPH-Volatile Range NWTPH-GX XXX3.0 XXXXX XXXXXXXX04/12/2017 EBS125 10 U1U 04/11/2017MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25 XXXXX XXXXXXXX04/12/2017 EBS150 20 U1U 04/11/2017MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50 XXXXX XXXXXXXX04/18/2017 GAP120 2.7 U1U 04/17/2017UG/KGNaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.3 U1U 04/17/2017UG/KG2-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.7 U1U 04/17/2017UG/KG1-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.4 U1U 04/17/2017UG/KGAcenaphthylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.2 U1U 04/17/2017UG/KGAcenaphthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.2 U1U 04/17/2017UG/KGFluorene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.3 U1U 04/17/2017UG/KGPhenanthrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.7 U1U 04/17/2017UG/KGAnthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.5 U1U 04/17/2017UG/KGFluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.8 U1U 04/17/2017UG/KGPyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.8 U1U 04/17/2017UG/KGBenzo[A]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.8 U1U 04/17/2017UG/KGChrysene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.7 U1U 04/17/2017UG/KGBenzo[B]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.0 U1U 04/17/2017UG/KGBenzo[K]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.0 U1U 04/17/2017UG/KGBenzo[A]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.6 U1U 04/17/2017UG/KGIndeno[1,2,3-Cd]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.2 U1U 04/17/2017UG/KGDibenz[A,H]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.7 U1U 04/17/2017UG/KGBenzo[G,H,I]Perylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.29 U5U 04/17/2017MG/KGAntimony EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL51.0 0.89 5 04/17/20176.9 MG/KGArsenic EPA-6020 XXX1.0 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.29 5 04/17/20179.3 MG/KGCopper EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.29 5 04/17/20172.0 MG/KGLead EPA-6020 XXX0.50 XXXXX XXXXXXXX

MINSURROGATE

SPIKE ADDED

LIMITSXXXXX XXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS DATE

ANALYSIS BY

QUALXXXXX



Page 9






EV17040044ALS SAMPLE#: EV17040044-09

DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE


LIMITSXXXXX XXX


ANALYSIS DATE

ANALYSIS BY

QUALXXXXX

04/07/2017 SNC13.0 0.75 U1U 04/07/2017MG/KGTPH-Volatile Range NWTPH-GX XXX3.0 XXXXX XXXXXXXX04/12/2017 EBS125 9.4 U1U 04/11/2017MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25 XXXXX XXXXXXXX04/12/2017 EBS150 18 U1U 04/11/2017MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50 XXXXX XXXXXXXX04/18/2017 GAP120 2.5 U1U 04/17/2017UG/KGNaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.1 U1U 04/17/2017UG/KG2-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.5 U1U 04/17/2017UG/KG1-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.3 U1U 04/17/2017UG/KGAcenaphthylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.1 U1U 04/17/2017UG/KGAcenaphthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.1 U1U 04/17/2017UG/KGFluorene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.1 U1U 04/17/2017UG/KGPhenanthrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.5 U1U 04/17/2017UG/KGAnthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.3 U1U 04/17/2017UG/KGFluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.6 U1U 04/17/2017UG/KGPyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.6 U1U 04/17/2017UG/KGBenzo[A]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.6 U1U 04/17/2017UG/KGChrysene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.5 U1U 04/17/2017UG/KGBenzo[B]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.9 U1U 04/17/2017UG/KGBenzo[K]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.8 U1U 04/17/2017UG/KGBenzo[A]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.4 U1U 04/17/2017UG/KGIndeno[1,2,3-Cd]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.0 U1U 04/17/2017UG/KGDibenz[A,H]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.5 U1U 04/17/2017UG/KGBenzo[G,H,I]Perylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.28 U5U 04/17/2017MG/KGAntimony EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL51.0 0.87 5 04/17/20172.8 MG/KGArsenic EPA-6020 XXX1.0 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.28 5 04/17/201715 MG/KGCopper EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.28 5 04/17/20172.0 MG/KGLead EPA-6020 XXX0.50 XXXXX XXXXXXXX

MINSURROGATE

SPIKE ADDED

LIMITSXXXXX XXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS DATE

ANALYSIS BY

QUALXXXXX



Page 10






EV17040044ALS SAMPLE#: EV17040044-10

DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE


LIMITSXXXXX XXX


ANALYSIS DATE

ANALYSIS BY

QUALXXXXX


MINSURROGATE

SPIKE ADDED

LIMITSXXXXX XXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS DATE

ANALYSIS BY

QUALXXXXX



Page 11






EV17040044ALS SAMPLE#: EV17040044-11

DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE


LIMITSXXXXX XXX


ANALYSIS DATE

ANALYSIS BY

QUALXXXXX


MINSURROGATE

SPIKE ADDED

LIMITSXXXXX XXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS DATE

ANALYSIS BY

QUALXXXXX



Page 12






EV17040044ALS SAMPLE#: EV17040044-12

DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE


LIMITSXXXXX XXX


ANALYSIS DATE

ANALYSIS BY

QUALXXXXX

04/07/2017 SNC13.0 0.72 U1U 04/07/2017MG/KGTPH-Volatile Range NWTPH-GX XXX3.0 XXXXX XXXXXXXX04/12/2017 EBS125 9.5 U1U 04/11/2017MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25 XXXXX XXXXXXXX04/12/2017 EBS150 18 U1U 04/11/2017MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50 XXXXX XXXXXXXX04/18/2017 GAP120 2.7 U1U 04/17/2017UG/KGNaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.2 U1U 04/17/2017UG/KG2-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.7 U1U 04/17/2017UG/KG1-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.4 U1U 04/17/2017UG/KGAcenaphthylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.2 U1U 04/17/2017UG/KGAcenaphthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.2 U1U 04/17/2017UG/KGFluorene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.2 U1U 04/17/2017UG/KGPhenanthrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.6 U1U 04/17/2017UG/KGAnthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.4 U1U 04/17/2017UG/KGFluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.7 U1U 04/17/2017UG/KGPyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.7 U1U 04/17/2017UG/KGBenzo[A]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.7 U1U 04/17/2017UG/KGChrysene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.6 U1U 04/17/2017UG/KGBenzo[B]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.0 U1U 04/17/2017UG/KGBenzo[K]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.0 U1U 04/17/2017UG/KGBenzo[A]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.5 U1U 04/17/2017UG/KGIndeno[1,2,3-Cd]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.2 U1U 04/17/2017UG/KGDibenz[A,H]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.7 U1U 04/17/2017UG/KGBenzo[G,H,I]Perylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.28 U5U 04/17/2017MG/KGAntimony EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL51.0 0.86 5 04/17/20172.1 MG/KGArsenic EPA-6020 XXX1.0 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.28 5 04/17/201714 MG/KGCopper EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.28 5 04/17/20171.9 MG/KGLead EPA-6020 XXX0.50 XXXXX XXXXXXXX

MINSURROGATE

SPIKE ADDED

LIMITSXXXXX XXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS DATE

ANALYSIS BY

QUALXXXXX



Page 13






EV17040044ALS SAMPLE#: EV17040044-13

DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE


LIMITSXXXXX XXX


ANALYSIS DATE

ANALYSIS BY

QUALXXXXX

04/07/2017 SNC13.0 0.85 U1U 04/07/2017MG/KGTPH-Volatile Range NWTPH-GX XXX3.0 XXXXX XXXXXXXX04/12/2017 EBS125 10 1 04/11/201731 MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25 XXXXX XXXXXXXX04/12/2017 EBS150 20 1 04/11/2017160 MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50 XXXXX XXXXXXXX04/18/2017 GAP120 3.0 U1U 04/17/2017UG/KGNaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.6 U1U 04/17/2017UG/KG2-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.0 U1U 04/17/2017UG/KG1-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.6 U1U 04/17/2017UG/KGAcenaphthylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.5 U1U 04/17/2017UG/KGAcenaphthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.6 U1U 04/17/2017UG/KGFluorene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.7 U1U 04/17/2017UG/KGPhenanthrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.0 U1U 04/17/2017UG/KGAnthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.8 U1U 04/17/2017UG/KGFluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.1 U1U 04/17/2017UG/KGPyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.1 U1U 04/17/2017UG/KGBenzo[A]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.2 U1U 04/17/2017UG/KGChrysene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.1 U1U 04/17/2017UG/KGBenzo[B]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.4 U1U 04/17/2017UG/KGBenzo[K]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.3 U1U 04/17/2017UG/KGBenzo[A]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.9 U1U 04/17/2017UG/KGIndeno[1,2,3-Cd]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.6 U1U 04/17/2017UG/KGDibenz[A,H]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 5.2 U1U 04/17/2017UG/KGBenzo[G,H,I]Perylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.30 U5U 04/17/2017MG/KGAntimony EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL51.0 0.94 5 04/17/20173.8 MG/KGArsenic EPA-6020 XXX1.0 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.30 5 04/17/201716 MG/KGCopper EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.30 5 04/17/20173.8 MG/KGLead EPA-6020 XXX0.50 XXXXX XXXXXXXX

MINSURROGATE

SPIKE ADDED

LIMITSXXXXX XXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS DATE

ANALYSIS BY

QUALXXXXX


U - Analyte analyzed for but not detected at level above reporting limit.Chromatogram indicates that it is likely that sample contains light oil/lube oil.

Page 14






EV17040044ALS SAMPLE#: EV17040044-14

DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE


LIMITSXXXXX XXX


ANALYSIS DATE

ANALYSIS BY

QUALXXXXX

04/07/2017 SNC13.0 0.93 U1U 04/07/2017MG/KGTPH-Volatile Range NWTPH-GX XXX3.0 XXXXX XXXXXXXX04/12/2017 EBS125 11 U1U 04/11/2017MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25 XXXXX XXXXXXXX04/12/2017 EBS150 21 U1U 04/11/2017MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50 XXXXX XXXXXXXX04/18/2017 GAP120 3.0 1 04/17/201722 UG/KGNaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.6 U1U 04/17/2017UG/KG2-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.0 U1U 04/17/2017UG/KG1-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.7 U1U 04/17/2017UG/KGAcenaphthylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.5 U1U 04/17/2017UG/KGAcenaphthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.6 U1U 04/17/2017UG/KGFluorene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.8 U1U 04/17/2017UG/KGPhenanthrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.1 U1U 04/17/2017UG/KGAnthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.9 U1U 04/17/2017UG/KGFluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.2 U1U 04/17/2017UG/KGPyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.1 U1U 04/17/2017UG/KGBenzo[A]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.2 U1U 04/17/2017UG/KGChrysene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.1 U1U 04/17/2017UG/KGBenzo[B]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.4 U1U 04/17/2017UG/KGBenzo[K]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.3 U1U 04/17/2017UG/KGBenzo[A]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.0 U1U 04/17/2017UG/KGIndeno[1,2,3-Cd]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.7 U1U 04/17/2017UG/KGDibenz[A,H]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 5.3 U1U 04/17/2017UG/KGBenzo[G,H,I]Perylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.31 U5U 04/17/2017MG/KGAntimony EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL51.0 0.97 5 04/17/20173.4 MG/KGArsenic EPA-6020 XXX1.0 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.31 5 04/17/201718 MG/KGCopper EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.31 5 04/17/20174.3 MG/KGLead EPA-6020 XXX0.50 XXXXX XXXXXXXX

MINSURROGATE

SPIKE ADDED

LIMITSXXXXX XXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS DATE

ANALYSIS BY

QUALXXXXX



Page 15






EV17040044ALS SAMPLE#: EV17040044-15

DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE


LIMITSXXXXX XXX


ANALYSIS DATE

ANALYSIS BY

QUALXXXXX


MINSURROGATE

SPIKE ADDED

LIMITSXXXXX XXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS DATE

ANALYSIS BY

QUALXXXXX



Page 16






EV17040044ALS SAMPLE#: EV17040044-16

DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE


LIMITSXXXXX XXX


ANALYSIS DATE

ANALYSIS BY

QUALXXXXX

04/07/2017 SNC13.0 0.74 U1U 04/07/2017MG/KGTPH-Volatile Range NWTPH-GX XXX3.0 XXXXX XXXXXXXX04/12/2017 EBS125 9.9 U1U 04/11/2017MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25 XXXXX XXXXXXXX04/12/2017 EBS150 19 U1U 04/11/2017MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50 XXXXX XXXXXXXX04/18/2017 GAP120 2.7 U1U 04/17/2017UG/KGNaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.3 U1U 04/17/2017UG/KG2-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.7 U1U 04/17/2017UG/KG1-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.4 U1U 04/17/2017UG/KGAcenaphthylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.2 1 04/17/201726 UG/KGAcenaphthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.2 1 04/17/201728 UG/KGFluorene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.3 1 04/17/2017100 UG/KGPhenanthrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.7 1 04/17/201740 UG/KGAnthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.5 1 04/17/201754 UG/KGFluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.8 1 04/17/201733 UG/KGPyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.8 U1U 04/17/2017UG/KGBenzo[A]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.8 U1U 04/17/2017UG/KGChrysene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.7 U1U 04/17/2017UG/KGBenzo[B]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.1 U1U 04/17/2017UG/KGBenzo[K]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.0 U1U 04/17/2017UG/KGBenzo[A]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.6 U1U 04/17/2017UG/KGIndeno[1,2,3-Cd]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.2 U1U 04/17/2017UG/KGDibenz[A,H]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.8 U1U 04/17/2017UG/KGBenzo[G,H,I]Perylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.29 U5U 04/17/2017MG/KGAntimony EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL51.0 0.89 5 04/17/20172.0 MG/KGArsenic EPA-6020 XXX1.0 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.29 5 04/17/20178.4 MG/KGCopper EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.29 5 04/17/201714 MG/KGLead EPA-6020 XXX0.50 XXXXX XXXXXXXX

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EV17040044ALS SAMPLE#: EV17040044-17

DATE: 5/5/2017



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ANALYSIS BY

QUALXXXXX

04/08/2017 SNC13.0 0.71 U1U 04/07/2017MG/KGTPH-Volatile Range NWTPH-GX XXX3.0 XXXXX XXXXXXXX04/12/2017 EBS125 9.7 U1U 04/11/2017MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25 XXXXX XXXXXXXX04/12/2017 EBS150 19 U1U 04/11/2017MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50 XXXXX XXXXXXXX04/18/2017 GAP120 2.7 1 04/17/201737 UG/KGNaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.3 1 04/17/201726 UG/KG2-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.7 U1U 04/17/2017UG/KG1-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.4 U1U 04/17/2017UG/KGAcenaphthylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.3 1 04/17/201739 UG/KGAcenaphthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.3 1 04/17/201752 UG/KGFluorene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.3 1 04/17/2017210 UG/KGPhenanthrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.7 1 04/17/201751 UG/KGAnthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.5 1 04/17/2017130 UG/KGFluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.8 1 04/17/201777 UG/KGPyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.8 U1U 04/17/2017UG/KGBenzo[A]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.8 1 04/17/201721 UG/KGChrysene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.7 U1U 04/17/2017UG/KGBenzo[B]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.1 U1U 04/17/2017UG/KGBenzo[K]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.0 U1U 04/17/2017UG/KGBenzo[A]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.6 U1U 04/17/2017UG/KGIndeno[1,2,3-Cd]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.3 U1U 04/17/2017UG/KGDibenz[A,H]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.8 U1U 04/17/2017UG/KGBenzo[G,H,I]Perylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.28 U5U 04/17/2017MG/KGAntimony EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL51.0 0.87 5 04/17/20172.8 MG/KGArsenic EPA-6020 XXX1.0 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.28 5 04/17/201713 MG/KGCopper EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.28 5 04/17/20172.3 MG/KGLead EPA-6020 XXX0.50 XXXXX XXXXXXXX

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Page 18






EV17040044ALS SAMPLE#: EV17040044-18

DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

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LIMITSXXXXX XXX


ANALYSIS DATE

ANALYSIS BY

QUALXXXXX

04/08/2017 SNC13.0 0.92 U1U 04/07/2017MG/KGTPH-Volatile Range NWTPH-GX XXX3.0 XXXXX XXXXXXXX04/12/2017 EBS125 11 U1U 04/11/2017MG/KGTPH-Diesel Range NWTPH-DX w/ SGA XXX25 XXXXX XXXXXXXX04/12/2017 EBS150 21 U1U 04/11/2017MG/KGTPH-Oil Range NWTPH-DX w/ SGA XXX50 XXXXX XXXXXXXX04/18/2017 GAP120 2.9 U1U 04/17/2017UG/KGNaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.6 U1U 04/17/2017UG/KG2-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.9 U1U 04/17/2017UG/KG1-Methylnaphthalene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.6 U1U 04/17/2017UG/KGAcenaphthylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 2.4 U1U 04/17/2017UG/KGAcenaphthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.5 U1U 04/17/2017UG/KGFluorene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.7 1 04/17/201736 UG/KGPhenanthrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.0 1 04/17/201723 UG/KGAnthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.8 1 04/17/201726 UG/KGFluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.1 U1U 04/17/2017UG/KGPyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.0 U1U 04/17/2017UG/KGBenzo[A]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.1 U1U 04/17/2017UG/KGChrysene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.0 U1U 04/17/2017UG/KGBenzo[B]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.3 U1U 04/17/2017UG/KGBenzo[K]Fluoranthene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.3 U1U 04/17/2017UG/KGBenzo[A]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 3.9 U1U 04/17/2017UG/KGIndeno[1,2,3-Cd]Pyrene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 4.6 U1U 04/17/2017UG/KGDibenz[A,H]Anthracene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 GAP120 5.2 U1U 04/17/2017UG/KGBenzo[G,H,I]Perylene EPA-8270 SIM XXX20 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.31 U5U 04/17/2017MG/KGAntimony EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL51.0 0.97 5 04/17/20176.7 MG/KGArsenic EPA-6020 XXX1.0 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.31 5 04/17/201714 MG/KGCopper EPA-6020 XXX0.50 XXXXX XXXXXXXX04/18/2017 RAL50.50 0.31 5 04/17/20173.5 MG/KGLead EPA-6020 XXX0.50 XXXXX XXXXXXXX

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Page 19



CLIENT PROJECT: 1779.01CLIENT SAMPLE ID GP-1



EV17040044ALS SAMPLE#: EV17040044-19

DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

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ANALYSIS BY

QUALXXXXX

04/06/2017 SNC150 14 U1U 04/06/2017UG/LTPH-Volatile Range NWTPH-GX XXX50 XXXXX XXXXXXXX04/12/2017 EBS1130 95 U1U 04/12/2017UG/LTPH-Diesel Range NWTPH-DX w/ SGA XXX130 XXXXX XXXXXXXX04/12/2017 EBS1250 87 U1U 04/12/2017UG/LTPH-Oil Range NWTPH-DX w/ SGA XXX250 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.094 U1U 04/06/2017UG/LDichlorodifluoromethane EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.23 U1U 04/06/2017UG/LChloromethane EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC10.20 0.031 U1U 04/06/2017UG/LVinyl Chloride EPA-8260 XXX0.20 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.14 U1U 04/06/2017UG/LBromomethane EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.12 U1U 04/06/2017UG/LChloroethane EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.025 U1U 04/06/2017UG/LCarbon Tetrachloride EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.045 U1U 04/06/2017UG/LTrichlorofluoromethane EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.054 U1U 04/06/2017UG/LCarbon Disulfide EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC125 0.68 U1U 04/06/2017UG/LAcetone EPA-8260 XXX25 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.014 U1U 04/06/2017UG/L1,1-Dichloroethene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC15.0 0.68 U1U 04/06/2017UG/LMethylene Chloride EPA-8260 XXX5.0 XXXXX XXXXXXXX04/06/2017 DLC110 0.057 U1U 04/06/2017UG/LAcrylonitrile EPA-8260 XXX10 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.034 U1U 04/06/2017UG/LMethyl T-Butyl Ether EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.097 U1U 04/06/2017UG/LTrans-1,2-Dichloroethene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.030 U1U 04/06/2017UG/L1,1-Dichloroethane EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC110 1.4 U1U 04/06/2017UG/L2-Butanone EPA-8260 XXX10 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.068 U1U 04/06/2017UG/LCis-1,2-Dichloroethene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.041 U1U 04/06/2017UG/L2,2-Dichloropropane EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.11 U1U 04/06/2017UG/LBromochloromethane EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.14 U1U 04/06/2017UG/LChloroform EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.059 U1U 04/06/2017UG/L1,1,1-Trichloroethane EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.067 U1U 04/06/2017UG/L1,1-Dichloropropene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.014 U1U 04/06/2017UG/L1,2-Dichloroethane EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.028 U1U 04/06/2017UG/LBenzene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.054 U1U 04/06/2017UG/LTrichloroethene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.063 U1U 04/06/2017UG/L1,2-Dichloropropane EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.071 U1U 04/06/2017UG/LDibromomethane EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.059 U1U 04/06/2017UG/LBromodichloromethane EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.058 U1U 04/06/2017UG/LTrans-1,3-Dichloropropene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC110 0.34 U1U 04/06/2017UG/L4-Methyl-2-Pentanone EPA-8260 XXX10 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.015 U1U 04/06/2017UG/LToluene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.048 U1U 04/06/2017UG/LCis-1,3-Dichloropropene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.052 U1U 04/06/2017UG/L1,1,2-Trichloroethane EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC110 0.94 U1U 04/06/2017UG/L2-Hexanone EPA-8260 XXX10 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.066 U1U 04/06/2017UG/L1,3-Dichloropropane EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.023 U1U 04/06/2017UG/LTetrachloroethylene EPA-8260 XXX2.0 XXXXX XXXXXXXX

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DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

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ANALYSIS DATE

ANALYSIS BY

QUALXXXXX

04/06/2017 DLC12.0 0.074 U1U 04/06/2017UG/LDibromochloromethane EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC10.010 0.010 U1U 04/06/2017UG/L1,2-Dibromoethane EPA-8260 XXX0.010 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.024 U1U 04/06/2017UG/LChlorobenzene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.087 U1U 04/06/2017UG/L1,1,1,2-Tetrachloroethane EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.029 U1U 04/06/2017UG/LEthylbenzene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC14.0 0.11 U1U 04/06/2017UG/Lm,p-Xylene EPA-8260 XXX4.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.020 U1U 04/06/2017UG/LStyrene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.069 U1U 04/06/2017UG/Lo-Xylene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.053 U1U 04/06/2017UG/LBromoform EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.038 U1U 04/06/2017UG/LIsopropylbenzene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.029 U1U 04/06/2017UG/L1,1,2,2-Tetrachloroethane EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.023 U1U 04/06/2017UG/L1,2,3-Trichloropropane EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.041 U1U 04/06/2017UG/LBromobenzene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.036 U1U 04/06/2017UG/LN-Propyl Benzene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.032 U1U 04/06/2017UG/L2-Chlorotoluene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.041 U1U 04/06/2017UG/L1,3,5-Trimethylbenzene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.040 U1U 04/06/2017UG/L4-Chlorotoluene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.051 U1U 04/06/2017UG/LT-Butyl Benzene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.054 U1U 04/06/2017UG/L1,2,4-Trimethylbenzene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.019 U1U 04/06/2017UG/LS-Butyl Benzene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.035 U1U 04/06/2017UG/LP-Isopropyltoluene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.041 U1U 04/06/2017UG/L1,3-Dichlorobenzene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.045 U1U 04/06/2017UG/L1,4-Dichlorobenzene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.053 U1U 04/06/2017UG/LN-Butylbenzene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.028 U1U 04/06/2017UG/L1,2-Dichlorobenzene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC110 0.10 U1U 04/06/2017UG/L1,2-Dibromo 3-Chloropropane EPA-8260 XXX10 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.047 U1U 04/06/2017UG/L1,2,4-Trichlorobenzene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.069 U1U 04/06/2017UG/LHexachlorobutadiene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.055 U1U 04/06/2017UG/LNaphthalene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/06/2017 DLC12.0 0.045 U1U 04/06/2017UG/L1,2,3-Trichlorobenzene EPA-8260 XXX2.0 XXXXX XXXXXXXX04/18/2017 GAP10.020 0.0022 U1U 04/10/2017UG/LNaphthalene EPA-8270 SIM XXX0.020 XXXXX XXXXXXXX04/18/2017 GAP10.020 0.0049 U1U 04/10/2017UG/L2-Methylnaphthalene EPA-8270 SIM XXX0.020 XXXXX XXXXXXXX04/18/2017 GAP10.020 0.0028 U1U 04/10/2017UG/L1-Methylnaphthalene EPA-8270 SIM XXX0.020 XXXXX XXXXXXXX04/18/2017 GAP10.020 0.0069 U1U 04/10/2017UG/LAcenaphthylene EPA-8270 SIM XXX0.020 XXXXX XXXXXXXX04/18/2017 GAP10.020 0.010 1 04/10/20170.053 UG/LAcenaphthene EPA-8270 SIM XXX0.020 XXXXX XXXXXXXX04/18/2017 GAP10.020 0.0030 U1U 04/10/2017UG/LFluorene EPA-8270 SIM XXX0.020 XXXXX XXXXXXXX04/18/2017 GAP10.020 0.0059 U1U 04/10/2017UG/LPhenanthrene EPA-8270 SIM XXX0.020 XXXXX XXXXXXXX04/18/2017 GAP10.020 0.0076 U1U 04/10/2017UG/LAnthracene EPA-8270 SIM XXX0.020 XXXXX XXXXXXXX04/18/2017 GAP10.020 0.0017 U1U 04/10/2017UG/LFluoranthene EPA-8270 SIM XXX0.020 XXXXX XXXXXXXX

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DATE: 5/5/2017



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LIMITSXXXXX XXX


ANALYSIS DATE

ANALYSIS BY

QUALXXXXX

04/18/2017 GAP10.020 0.0035 U1U 04/10/2017UG/LPyrene EPA-8270 SIM XXX0.020 XXXXX XXXXXXXX04/18/2017 GAP10.020 0.0028 U1U 04/10/2017UG/LBenzo[A]Anthracene EPA-8270 SIM XXX0.020 XXXXX XXXXXXXX04/18/2017 GAP10.020 0.0058 U1U 04/10/2017UG/LChrysene EPA-8270 SIM XXX0.020 XXXXX XXXXXXXX04/18/2017 GAP10.020 0.0085 U1U 04/10/2017UG/LBenzo[B]Fluoranthene EPA-8270 SIM XXX0.020 XXXXX XXXXXXXX04/18/2017 GAP10.020 0.014 U1U 04/10/2017UG/LBenzo[K]Fluoranthene EPA-8270 SIM XXX0.020 XXXXX XXXXXXXX04/18/2017 GAP10.020 0.0064 U1U 04/10/2017UG/LBenzo[A]Pyrene EPA-8270 SIM XXX0.020 XXXXX XXXXXXXX04/18/2017 GAP10.020 0.0052 U1U 04/10/2017UG/LIndeno[1,2,3-Cd]Pyrene EPA-8270 SIM XXX0.020 XXXXX XXXXXXXX04/18/2017 GAP10.020 0.0099 U1U 04/10/2017UG/LDibenz[A,H]Anthracene EPA-8270 SIM XXX0.020 XXXXX XXXXXXXX04/18/2017 GAP10.020 0.0055 U1U 04/10/2017UG/LBenzo[G,H,I]Perylene EPA-8270 SIM XXX0.020 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.9 U1U 04/07/2017UG/LPyridine EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.4 U1U 04/07/2017UG/LN-Nitrosodimethylamine EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.98 U1U 04/07/2017UG/LPhenol EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.9 U1U 04/07/2017UG/LAniline EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.87 U1U 04/07/2017UG/LBis(2-Chloroethyl)Ether EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.79 U1U 04/07/2017UG/L2-Chlorophenol EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.3 U1U 04/07/2017UG/L1,3-Dichlorobenzene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.96 U1U 04/07/2017UG/L1,4-Dichlorobenzene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.96 U1U 04/07/2017UG/LBenzyl Alcohol EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.3 U1U 04/07/2017UG/L1,2-Dichlorobenzene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.2 U1U 04/07/2017UG/L2-Methylphenol EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.58 U1U 04/07/2017UG/LBis(2-Chloroisopropyl)Ether EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.75 U1U 04/07/2017UG/L3&4-Methylphenol EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.9 U1U 04/07/2017UG/LN-Nitroso-Di-N-Propylamine EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.9 U1U 04/07/2017UG/LHexachloroethane EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.1 U1U 04/07/2017UG/LNitrobenzene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.1 U1U 04/07/2017UG/LIsophorone EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.1 U1U 04/07/2017UG/L2-Nitrophenol EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.81 U1U 04/07/2017UG/L2,4-Dimethylphenol EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP110 2.3 U1U 04/07/2017UG/LBenzoic Acid EPA-8270 XXX10 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.98 U1U 04/07/2017UG/LBis(2-Chloroethoxy)Methane EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.73 U1U 04/07/2017UG/L2,4-Dichlorophenol EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.0 U1U 04/07/2017UG/L1,2,4-Trichlorobenzene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.54 U1U 04/07/2017UG/LNaphthalene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.8 U1U 04/07/2017UG/L4-Chloroaniline EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.70 U1U 04/07/2017UG/L2,6-Dichlorophenol EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.8 U1U 04/07/2017UG/LHexachlorobutadiene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.1 U1U 04/07/2017UG/L4-Chloro-3-Methylphenol EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.96 U1U 04/07/2017UG/L2-Methylnaphthalene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.90 U1U 04/07/2017UG/L1-Methylnaphthalene EPA-8270 XXX2.0 XXXXX XXXXXXXX

Page 22






EV17040044ALS SAMPLE#: EV17040044-19

DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE


LIMITSXXXXX XXX


ANALYSIS DATE

ANALYSIS BY

QUALXXXXX

04/08/2017 GAP12.0 1.9 U1U 04/07/2017UG/LHexachlorocyclopentadiene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.83 U1U 04/07/2017UG/L2,4,6-Trichlorophenol EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.4 U1U 04/07/2017UG/L2,4,5-Trichlorophenol EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.84 U1U 04/07/2017UG/L2-Chloronaphthalene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.71 U1U 04/07/2017UG/L2-Nitroaniline EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.74 U1U 04/07/2017UG/LAcenaphthylene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.64 U1U 04/07/2017UG/LDimethylphthalate EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.7 U1U 04/07/2017UG/L2,6-Dinitrotoluene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.74 U1U 04/07/2017UG/LAcenaphthene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP15.0 1.3 U1U 04/07/2017UG/L3-Nitroaniline EPA-8270 XXX5.0 XXXXX XXXXXXXX04/08/2017 GAP110 2.7 U1U 04/07/2017UG/L2,4-Dinitrophenol EPA-8270 XXX10 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.9 U1U 04/07/2017UG/L4-Nitrophenol EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.47 U1U 04/07/2017UG/LDibenzofuran EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.72 U1U 04/07/2017UG/L2,4-Dinitrotoluene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.98 U1U 04/07/2017UG/L2,3,4,6-Tetrachlorophenol EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.74 U1U 04/07/2017UG/LDiethylphthalate EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.94 U1U 04/07/2017UG/LFluorene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.68 U1U 04/07/2017UG/L4-Chlorophenyl-Phenylether EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.9 U1U 04/07/2017UG/L4-Nitroaniline EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.9 U1U 04/07/2017UG/L4,6-Dinitro-2-Methylphenol EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.86 U1U 04/07/2017UG/LN-Nitrosodiphenylamine EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.5 U1U 04/07/2017UG/LAzobenzene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.73 U1U 04/07/2017UG/L4-Bromophenyl-Phenylether EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.59 U1U 04/07/2017UG/LHexachlorobenzene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP15.0 3.4 U1U 04/07/2017UG/LPentachlorophenol EPA-8270 XXX5.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.89 U1U 04/07/2017UG/LPhenanthrene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.75 U1U 04/07/2017UG/LAnthracene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.5 U1U 04/07/2017UG/LCarbazole EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.77 U1U 04/07/2017UG/LDi-N-Butylphthalate EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.87 U1U 04/07/2017UG/LFluoranthene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.57 U1U 04/07/2017UG/LPyrene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.62 U1U 04/07/2017UG/LButylbenzylphthalate EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.9 U1U 04/07/2017UG/L3,3-Dichlorobenzidine EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.69 U1U 04/07/2017UG/LBenzo[A]Anthracene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.74 U1U 04/07/2017UG/LChrysene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.75 U1U 04/07/2017UG/LBis(2-Ethylhexyl)Phthalate EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.81 U1U 04/07/2017UG/LDi-N-Octylphthalate EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.1 U1U 04/07/2017UG/LBenzo[B]Fluoranthene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 1.2 U1U 04/07/2017UG/LBenzo[K]Fluoranthene EPA-8270 XXX2.0 XXXXX XXXXXXXX

Page 23






EV17040044ALS SAMPLE#: EV17040044-19

DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

RL PQLANALYTE


LIMITSXXXXX XXX


ANALYSIS DATE

ANALYSIS BY

QUALXXXXX

04/08/2017 GAP12.0 0.45 U1U 04/07/2017UG/LBenzo[A]Pyrene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.54 U1U 04/07/2017UG/LIndeno[1,2,3-Cd]Pyrene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.89 U1U 04/07/2017UG/LDibenz[A,H]Anthracene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/08/2017 GAP12.0 0.50 U1U 04/07/2017UG/LBenzo[G,H,I]Perylene EPA-8270 XXX2.0 XXXXX XXXXXXXX04/17/2017 GAP10.10 0.063 U1U 04/07/2017UG/LPCB-1016 EPA-8082 XXX0.10 XXXXX XXXXXXXX04/17/2017 GAP10.10 0.063 U1U 04/07/2017UG/LPCB-1221 EPA-8082 XXX0.10 XXXXX XXXXXXXX04/17/2017 GAP10.10 0.063 U1U 04/07/2017UG/LPCB-1232 EPA-8082 XXX0.10 XXXXX XXXXXXXX04/17/2017 GAP10.10 0.063 U1U 04/07/2017UG/LPCB-1242 EPA-8082 XXX0.10 XXXXX XXXXXXXX04/17/2017 GAP10.10 0.063 U1U 04/07/2017UG/LPCB-1248 EPA-8082 XXX0.10 XXXXX XXXXXXXX04/17/2017 GAP10.10 0.063 U1U 04/07/2017UG/LPCB-1254 EPA-8082 XXX0.10 XXXXX XXXXXXXX04/17/2017 GAP10.10 0.063 U1U 04/07/2017UG/LPCB-1260 EPA-8082 XXX0.10 XXXXX XXXXXXXX04/17/2017 GAP10.10 0.063 U1U 04/07/2017UG/LPCB-1268 EPA-8082 XXX0.10 XXXXX XXXXXXXX04/10/2017 RAL10.20 0.11 U1U 04/10/2017UG/LMercury EPA-245.1 XXX0.20 XXXXX XXXXXXXX04/10/2017 RAL10.20 0.11 U1U 04/10/2017UG/LMercury (Dissolved) EPA-245.1 XXX0.20 XXXXX XXXXXXXX04/13/2017 RAL12.5 0.32 U1U 04/12/2017UG/LAntimony EPA-200.8 XXX2.5 XXXXX XXXXXXXX04/13/2017 RAL11.0 0.45 1 04/12/20178.6 UG/LArsenic EPA-200.8 XXX1.0 XXXXX XXXXXXXX04/13/2017 RAL11.0 0.67 1 04/12/201716 UG/LBarium EPA-200.8 XXX1.0 XXXXX XXXXXXXX04/13/2017 RAL11.0 0.36 U1U 04/12/2017UG/LCadmium EPA-200.8 XXX1.0 XXXXX XXXXXXXX04/13/2017 RAL12.0 0.29 U1U 04/12/2017UG/LChromium EPA-200.8 XXX2.0 XXXXX XXXXXXXX04/13/2017 RAL12.0 0.80 U1U 04/12/2017UG/LCopper EPA-200.8 XXX2.0 XXXXX XXXXXXXX04/13/2017 RAL11.0 0.28 U1U 04/12/2017UG/LLead EPA-200.8 XXX1.0 XXXXX XXXXXXXX04/13/2017 RAL14.0 3.4 U1U 04/12/2017UG/LSelenium EPA-200.8 XXX4.0 XXXXX XXXXXXXX04/13/2017 RAL11.0 0.20 U1U 04/12/2017UG/LSilver EPA-200.8 XXX1.0 XXXXX XXXXXXXX04/13/2017 RAL12.5 0.32 U1U 04/12/2017UG/LAntimony (Dissolved) EPA-200.8 XXX2.5 XXXXX XXXXXXXX04/13/2017 RAL11.0 0.45 1 04/12/20178.0 UG/LArsenic (Dissolved) EPA-200.8 XXX1.0 XXXXX XXXXXXXX04/13/2017 RAL11.0 0.67 1 04/12/201714 UG/LBarium (Dissolved) EPA-200.8 XXX1.0 XXXXX XXXXXXXX04/13/2017 RAL11.0 0.36 U1U 04/12/2017UG/LCadmium (Dissolved) EPA-200.8 XXX1.0 XXXXX XXXXXXXX04/13/2017 RAL12.0 0.29 U1U 04/12/2017UG/LChromium (Dissolved) EPA-200.8 XXX2.0 XXXXX XXXXXXXX04/13/2017 RAL12.0 0.80 U1U 04/12/2017UG/LCopper (Dissolved) EPA-200.8 XXX2.0 XXXXX XXXXXXXX04/13/2017 RAL11.0 0.28 U1U 04/12/2017UG/LLead (Dissolved) EPA-200.8 XXX1.0 XXXXX XXXXXXXX04/13/2017 RAL14.0 3.4 U1U 04/12/2017UG/LSelenium (Dissolved) EPA-200.8 XXX4.0 XXXXX XXXXXXXX04/13/2017 RAL11.0 0.20 U1U 04/12/2017UG/LSilver (Dissolved) EPA-200.8 XXX1.0 XXXXX XXXXXXXX

MINSURROGATE

SPIKE ADDED

LIMITSXXXXX XXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS DATE

ANALYSIS BY

QUALXXXXX

04/06/2017 SNC1140 10.0 04/06/201787.2 TFT NWTPH-GX XXX60 XXXXX XXXXX XXXXXXXXXXXXX04/12/2017 EBS1126 80.0 04/12/2017103 C25 NWTPH-DX w/ SGA XXX60 XXXXX XXXXX XXXXXXXXXXXXX04/06/2017 DLC1130 5.00 04/06/2017101 1,2-Dichloroethane-d4 EPA-8260 XXX71 XXXXX XXXXX XXXXXXXXXXXXX04/06/2017 DLC1120 5.00 04/06/201799.2 Toluene-d8 EPA-8260 XXX80 XXXXX XXXXX XXXXXXXXXXXXX

Page 24






EV17040044ALS SAMPLE#: EV17040044-19

DATE: 5/5/2017



DATA RESULTS

ALS JOB#:

SAMPLE DATA RESULTS

MINSURROGATE

SPIKE ADDED

LIMITSXXXXX XXXMAX

LIMITS

%REC REPORTINMETHOD

ANALYSIS DATE

ANALYSIS BY

QUALXXXXX

04/06/2017 DLC1120 5.00 04/06/2017103 4-Bromofluorobenzene EPA-8260 XXX78 XXXXX XXXXX XXXXXXXXXXXXX04/18/2017 GAP1147 18.6 04/10/201770.0 Terphenyl-d14 EPA-8270 SIM XXX50 XXXXX XXXXX XXXXXXXXXXXXX04/08/2017 GAP1105 37.2 04/07/201735.7 2-Fluorophenol EPA-8270 XXX29 XXXXX XXXXX XXXXXXXXXXXXX04/08/2017 GAP188 37.2 04/07/201719.8 Phenol-d5 EPA-8270 XXX5 XXXXX XXXXX XXXXXXXXXXXXX04/08/2017 GAP1125 18.6 04/07/201764.1 Nitrobenzene-d5 EPA-8270 XXX53 XXXXX XXXXX XXXXXXXXXXXXX04/08/2017 GAP1127 18.6 04/07/201757.5 2-Fluorobiphenyl EPA-8270 XXX46 XXXXX XXXXX XXXXXXXXXXXXX04/08/2017 GAP1143 37.2 04/07/201770.6 2,4,6-Tribromophenol EPA-8270 XXX45 XXXXX XXXXX XXXXXXXXXXXXX04/08/2017 GAP1132 18.6 04/07/201768.3 Terphenyl-d14 EPA-8270 XXX58 XXXXX XXXXX XXXXXXXXXXXXX04/17/2017 GAP1120 0.0381 04/07/201746.6 TCMX EPA-8082 XXX5 XXXXX XXXXX XXXXXXXXXXXXX04/17/2017 GAP1131 0.0381 04/07/2017100 DCB EPA-8082 XXX10 XXXXX XXXXX XXXXXXXXXXXXX


Page 25



LABORATORY BLANK RESULTS

CLIENT PROJECT: 1779.01


ALS SDG#: EV17040044DATE: 5/5/2017

WDOE ACCREDITATION: C601CLIENT CONTACT: Jon Einarsen

MBG-040717S - Batch 115106 - Soil by NWTPH-GX

METHOD

ANALYSIS

DATE

ANALYSIS

BYANALYTE

DET

ORG

RSLT TYPEXXX

RL PQLQUAL UNITS

LIMITS

XXXXX XXXXXXXXX LIMITS

REPORTING

RESULTS QUALXXXX

TPH-Volatile Range 04/07/2017 SNC TRGN YXXX3.0 1.5MG/KG 3.0UU XXXXX XXXXXXXXXNWTPH-GX


MBG-040617W2 - Batch 115065 - Water by NWTPH-GX

METHOD

ANALYSIS

DATE

ANALYSIS

BYANALYTE

DET

ORG

RSLT TYPEXXX

RL PQLQUAL UNITS

LIMITS


REPORTING

RESULTS QUALXXXX

TPH-Volatile Range 04/06/2017 SNC TRGN YXXX50 29UG/L 50UU XXXXX XXXXXXXXXNWTPH-GX


MB-041117S - Batch 115303 - Soil by NWTPH-DX

METHOD

ANALYSIS

DATE

ANALYSIS

BYANALYTE

DET

ORG

RSLT TYPEXXX

RL PQLQUAL UNITS

LIMITS


REPORTING

RESULTS QUALXXXX

TPH-Diesel Range 04/11/2017 EBS TRGN YXXX25 12MG/KG 25UU XXXXX XXXXXXXXXNWTPH-DX

TPH-Oil Range 04/11/2017 EBS TRGN YXXX50 23MG/KG 50UU XXXXX XXXXXXXXXNWTPH-DX


MB-040617W - Batch 115092 - Water by NWTPH-DX

METHOD

ANALYSIS

DATE

ANALYSIS

BYANALYTE

DET

ORG

RSLT TYPEXXX

RL PQLQUAL UNITS

LIMITS


REPORTING

RESULTS QUALXXXX

TPH-Diesel Range 04/06/2017 EBS TRGN YXXX130 120UG/L 130UU XXXXX XXXXXXXXXNWTPH-DX

TPH-Oil Range 04/06/2017 EBS TRGN YXXX250 110UG/L 250UU XXXXX XXXXXXXXXNWTPH-DX


MB-040317W - Batch 115052 - Water by EPA-8260

METHOD

ANALYSIS

DATE

ANALYSIS

BYANALYTE

DET

ORG

RSLT TYPEXXX

RL PQLQUAL UNITS

LIMITS


REPORTING

RESULTS QUALXXXX

Dichlorodifluoromethane 04/03/2017 DLC TRGN YXXX2.0 0.094UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Chloromethane 04/03/2017 DLC TRGN YXXX2.0 0.23UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Vinyl Chloride 04/03/2017 DLC TRGN YXXX0.20 0.031UG/L 0.20UU XXXXX XXXXXXXXXEPA-8260

Bromomethane 04/03/2017 DLC TRGN YXXX2.0 0.14UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Chloroethane 04/03/2017 DLC TRGN YXXX2.0 0.12UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Carbon Tetrachloride 04/03/2017 DLC TRGN YXXX2.0 0.025UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Trichlorofluoromethane 04/03/2017 DLC TRGN YXXX2.0 0.045UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Carbon Disulfide 04/03/2017 DLC TRGN YXXX2.0 0.054UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Acetone 04/03/2017 DLC TRGN YXXX25 0.68UG/L 25UU XXXXX XXXXXXXXXEPA-8260

1,1-Dichloroethene 04/03/2017 DLC TRGN YXXX2.0 0.014UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Methylene Chloride 04/03/2017 DLC TRGN YXXX5.0 0.68UG/L 5.0UU XXXXX XXXXXXXXXEPA-8260

Acrylonitrile 04/03/2017 DLC TRGN YXXX10 0.057UG/L 10UU XXXXX XXXXXXXXXEPA-8260

Page 26






ALS SDG#: EV17040044DATE: 5/5/2017


MB-040317W - Batch 115052 - Water by EPA-8260Methyl T-Butyl Ether 04/03/2017 DLC TRGN YXXX2.0 0.034UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Trans-1,2-Dichloroethene 04/03/2017 DLC TRGN YXXX2.0 0.097UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

1,1-Dichloroethane 04/03/2017 DLC TRGN YXXX2.0 0.030UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

2-Butanone 04/03/2017 DLC TRGN YXXX10 1.4UG/L 10UU XXXXX XXXXXXXXXEPA-8260

Cis-1,2-Dichloroethene 04/03/2017 DLC TRGN YXXX2.0 0.068UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

2,2-Dichloropropane 04/03/2017 DLC TRGN YXXX2.0 0.041UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Bromochloromethane 04/03/2017 DLC TRGN YXXX2.0 0.11UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Chloroform 04/03/2017 DLC TRGN YXXX2.0 0.14UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

1,1,1-Trichloroethane 04/03/2017 DLC TRGN YXXX2.0 0.059UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

1,1-Dichloropropene 04/03/2017 DLC TRGN YXXX2.0 0.067UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

1,2-Dichloroethane 04/03/2017 DLC TRGN YXXX2.0 0.014UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Benzene 04/03/2017 DLC TRGN YXXX2.0 0.028UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Trichloroethene 04/03/2017 DLC TRGN YXXX2.0 0.054UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260


Dibromomethane 04/03/2017 DLC TRGN YXXX2.0 0.071UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Bromodichloromethane 04/03/2017 DLC TRGN YXXX2.0 0.059UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Trans-1,3-Dichloropropene 04/03/2017 DLC TRGN YXXX2.0 0.058UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

4-Methyl-2-Pentanone 04/03/2017 DLC TRGN YXXX10 0.34UG/L 10UU XXXXX XXXXXXXXXEPA-8260

Toluene 04/03/2017 DLC TRGN YXXX2.0 0.015UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Cis-1,3-Dichloropropene 04/03/2017 DLC TRGN YXXX2.0 0.048UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

1,1,2-Trichloroethane 04/03/2017 DLC TRGN YXXX2.0 0.052UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

2-Hexanone 04/03/2017 DLC TRGN YXXX10 0.94UG/L 10UU XXXXX XXXXXXXXXEPA-8260


Tetrachloroethylene 04/03/2017 DLC TRGN YXXX2.0 0.023UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Dibromochloromethane 04/03/2017 DLC TRGN YXXX2.0 0.074UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

1,2-Dibromoethane 04/03/2017 DLC TRGN YXXX0.010 0.01UG/L 0.010UU XXXXX XXXXXXXXXEPA-8260

Chlorobenzene 04/03/2017 DLC TRGN YXXX2.0 0.024UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

1,1,1,2-Tetrachloroethane 04/03/2017 DLC TRGN YXXX2.0 0.087UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Ethylbenzene 04/03/2017 DLC TRGN YXXX2.0 0.029UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

m,p-Xylene 04/03/2017 DLC TRGN YXXX4.0 0.11UG/L 4.0UU XXXXX XXXXXXXXXEPA-8260

Styrene 04/03/2017 DLC TRGN YXXX2.0 0.020UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

o-Xylene 04/03/2017 DLC TRGN YXXX2.0 0.069UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Bromoform 04/03/2017 DLC TRGN YXXX2.0 0.053UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Isopropylbenzene 04/03/2017 DLC TRGN YXXX2.0 0.038UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

1,1,2,2-Tetrachloroethane 04/03/2017 DLC TRGN YXXX2.0 0.029UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

1,2,3-Trichloropropane 04/03/2017 DLC TRGN YXXX2.0 0.023UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Bromobenzene 04/03/2017 DLC TRGN YXXX2.0 0.041UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

N-Propyl Benzene 04/03/2017 DLC TRGN YXXX2.0 0.036UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

2-Chlorotoluene 04/03/2017 DLC TRGN YXXX2.0 0.032UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

1,3,5-Trimethylbenzene 04/03/2017 DLC TRGN YXXX2.0 0.041UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

4-Chlorotoluene 04/03/2017 DLC TRGN YXXX2.0 0.040UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Page 27






ALS SDG#: EV17040044DATE: 5/5/2017


MB-040317W - Batch 115052 - Water by EPA-8260T-Butyl Benzene 04/03/2017 DLC TRGN YXXX2.0 0.051UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

1,2,4-Trimethylbenzene 04/03/2017 DLC TRGN YXXX2.0 0.054UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

S-Butyl Benzene 04/03/2017 DLC TRGN YXXX2.0 0.019UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

P-Isopropyltoluene 04/03/2017 DLC TRGN YXXX2.0 0.035UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

1,3-Dichlorobenzene 04/03/2017 DLC TRGN YXXX2.0 0.041UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260


N-Butylbenzene 04/03/2017 DLC TRGN YXXX2.0 0.053UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260


1,2-Dibromo 3-Chloropropane 04/03/2017 DLC TRGN YXXX10 0.10UG/L 10UU XXXXX XXXXXXXXXEPA-8260

1,2,4-Trichlorobenzene 04/03/2017 DLC TRGN YXXX2.0 0.047UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Hexachlorobutadiene 04/03/2017 DLC TRGN YXXX2.0 0.069UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

Naphthalene 04/03/2017 DLC TRGN YXXX2.0 0.055UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260

1,2,3-Trichlorobenzene 04/03/2017 DLC TRGN YXXX2.0 0.045UG/L 2.0UU XXXXX XXXXXXXXXEPA-8260


MB-041717S - Batch 115467 - Soil by EPA-8270 SIM

METHOD

ANALYSIS

DATE

ANALYSIS

BYANALYTE

DET

ORG

RSLT TYPEXXX

RL PQLQUAL UNITS

LIMITS


REPORTING

RESULTS QUALXXXX

Naphthalene 04/18/2017 GAP TRGN YXXX20 3.2UG/KG 20UU XXXXX XXXXXXXXXEPA-8270 SIM

2-Methylnaphthalene 04/18/2017 GAP TRGN YXXX20 3.9UG/KG 20UU XXXXX XXXXXXXXXEPA-8270 SIM

1-Methylnaphthalene 04/18/2017 GAP TRGN YXXX20 3.2UG/KG 20UU XXXXX XXXXXXXXXEPA-8270 SIM

Acenaphthylene 04/18/2017 GAP TRGN YXXX20 2.8UG/KG 20UU XXXXX XXXXXXXXXEPA-8270 SIM

Acenaphthene 04/18/2017 GAP TRGN YXXX20 2.6UG/KG 20UU XXXXX XXXXXXXXXEPA-8270 SIM

Fluorene 04/18/2017 GAP TRGN YXXX20 3.8UG/KG 20UU XXXXX XXXXXXXXXEPA-8270 SIM

Phenanthrene 04/18/2017 GAP TRGN YXXX20 5.1UG/KG 20UU XXXXX XXXXXXXXXEPA-8270 SIM

Anthracene 04/18/2017 GAP TRGN YXXX20 4.3UG/KG 20UU XXXXX XXXXXXXXXEPA-8270 SIM

Fluoranthene 04/18/2017 GAP TRGN YXXX20 4.1UG/KG 20UU XXXXX XXXXXXXXXEPA-8270 SIM

Pyrene 04/18/2017 GAP TRGN YXXX20 4.5UG/KG 20UU XXXXX XXXXXXXXXEPA-8270 SIM

Benzo[A]Anthracene 04/18/2017 GAP TRGN YXXX20 3.3UG/KG 20UU XXXXX XXXXXXXXXEPA-8270 SIM

Chrysene 04/18/2017 GAP TRGN YXXX20 4.5UG/KG 20UU XXXXX XXXXXXXXXEPA-8270 SIM

Benzo[B]Fluoranthene 04/18/2017 GAP TRGN YXXX20 4.4UG/KG 20UU XXXXX XXXXXXXXXEPA-8270 SIM

Benzo[K]Fluoranthene 04/18/2017 GAP TRGN YXXX20 3.6UG/KG 20UU XXXXX XXXXXXXXXEPA-8270 SIM

Benzo[A]Pyrene 04/18/2017 GAP TRGN YXXX20 3.5UG/KG 20UU XXXXX XXXXXXXXXEPA-8270 SIM

Indeno[1,2,3-Cd]Pyrene 04/18/2017 GAP TRGN YXXX20 4.2UG/KG 20UU XXXXX XXXXXXXXXEPA-8270 SIM

Dibenz[A,H]Anthracene 04/18/2017 GAP TRGN YXXX20 5.0UG/KG 20UU XXXXX XXXXXXXXXEPA-8270 SIM

Benzo[G,H,I]Perylene 04/18/2017 GAP TRGN YXXX20 5.6UG/KG 20UU XXXXX XXXXXXXXXEPA-8270 SIM


Page 28






ALS SDG#: EV17040044DATE: 5/5/2017


MB-041017W - Batch 115259 - Water by EPA-8270 SIM

METHOD

ANALYSIS

DATE

ANALYSIS

BYANALYTE

DET

ORG

RSLT TYPEXXX

RL PQLQUAL UNITS

LIMITS


REPORTING

RESULTS QUALXXXX

Naphthalene 04/10/2017 PAB TRGN YXXX0.020 0.0024UG/L 0.020UU XXXXX XXXXXXXXXEPA-8270 SIM

2-Methylnaphthalene 04/10/2017 PAB TRGN YXXX0.020 0.0052UG/L 0.020UU XXXXX XXXXXXXXXEPA-8270 SIM

1-Methylnaphthalene 04/10/2017 PAB TRGN YXXX0.020 0.0030UG/L 0.020UU XXXXX XXXXXXXXXEPA-8270 SIM

Acenaphthylene 04/10/2017 PAB TRGN YXXX0.020 0.0074UG/L 0.020UU XXXXX XXXXXXXXXEPA-8270 SIM

Acenaphthene 04/10/2017 PAB TRGN YXXX0.020 0.011UG/L 0.020UU XXXXX XXXXXXXXXEPA-8270 SIM

Fluorene 04/10/2017 PAB TRGN YXXX0.020 0.0033UG/L 0.020UU XXXXX XXXXXXXXXEPA-8270 SIM

Phenanthrene 04/10/2017 PAB TRGN YXXX0.020 0.0063UG/L 0.020UU XXXXX XXXXXXXXXEPA-8270 SIM

Anthracene 04/10/2017 PAB TRGN YXXX0.020 0.0082UG/L 0.020UU XXXXX XXXXXXXXXEPA-8270 SIM

Fluoranthene 04/10/2017 PAB TRGN YXXX0.020 0.0018UG/L 0.020UU XXXXX XXXXXXXXXEPA-8270 SIM

Pyrene 04/10/2017 PAB TRGN YXXX0.020 0.0038UG/L 0.020UU XXXXX XXXXXXXXXEPA-8270 SIM

Benzo[A]Anthracene 04/10/2017 PAB TRGN YXXX0.020 0.0031UG/L 0.020UU XXXXX XXXXXXXXXEPA-8270 SIM

Chrysene 04/10/2017 PAB TRGN YXXX0.020 0.0062UG/L 0.020UU XXXXX XXXXXXXXXEPA-8270 SIM

Benzo[B]Fluoranthene 04/10/2017 PAB TRGN YXXX0.020 0.0091UG/L 0.020UU XXXXX XXXXXXXXXEPA-8270 SIM

Benzo[K]Fluoranthene 04/10/2017 PAB TRGN YXXX0.020 0.015UG/L 0.020UU XXXXX XXXXXXXXXEPA-8270 SIM

Benzo[A]Pyrene 04/10/2017 PAB TRGN YXXX0.020 0.0069UG/L 0.020UU XXXXX XXXXXXXXXEPA-8270 SIM

Indeno[1,2,3-Cd]Pyrene 04/10/2017 PAB TRGN YXXX0.020 0.0055UG/L 0.020UU XXXXX XXXXXXXXXEPA-8270 SIM

Dibenz[A,H]Anthracene 04/10/2017 PAB TRGN YXXX0.020 0.011UG/L 0.020UU XXXXX XXXXXXXXXEPA-8270 SIM

Benzo[G,H,I]Perylene 04/10/2017 PAB TRGN YXXX0.020 0.0060UG/L 0.020UU XXXXX XXXXXXXXXEPA-8270 SIM


MB-040717W - Batch 115471 - Water by EPA-8270

METHOD

ANALYSIS

DATE

ANALYSIS

BYANALYTE

DET

ORG

RSLT TYPEXXX

RL PQLQUAL UNITS

LIMITS


REPORTING

RESULTS QUALXXXX

Pyridine 04/08/2017 GAP TRGN YXXX2.0 2.0UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

N-Nitrosodimethylamine 04/08/2017 GAP TRGN YXXX2.0 1.5UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Phenol 04/08/2017 GAP TRGN YXXX2.0 1.0UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Aniline 04/08/2017 GAP TRGN YXXX2.0 2.0UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Bis(2-Chloroethyl)Ether 04/08/2017 GAP TRGN YXXX2.0 0.94UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

2-Chlorophenol 04/08/2017 GAP TRGN YXXX2.0 0.85UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

1,3-Dichlorobenzene 04/08/2017 GAP TRGN YXXX2.0 1.4UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270


Benzyl Alcohol 04/08/2017 GAP TRGN YXXX2.0 1.0UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270


2-Methylphenol 04/08/2017 GAP TRGN YXXX2.0 1.3UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Bis(2-Chloroisopropyl)Ether 04/08/2017 GAP TRGN YXXX2.0 0.62UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

3&4-Methylphenol 04/08/2017 GAP TRGN YXXX2.0 0.81UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

N-Nitroso-Di-N-Propylamine 04/08/2017 GAP TRGN YXXX2.0 2.0UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Hexachloroethane 04/08/2017 GAP TRGN YXXX2.0 2.0UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Nitrobenzene 04/08/2017 GAP TRGN YXXX2.0 1.2UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Page 29






ALS SDG#: EV17040044DATE: 5/5/2017


MB-040717W - Batch 115471 - Water by EPA-8270Isophorone 04/08/2017 GAP TRGN YXXX2.0 1.2UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

2-Nitrophenol 04/08/2017 GAP TRGN YXXX2.0 1.1UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

2,4-Dimethylphenol 04/08/2017 GAP TRGN YXXX2.0 0.87UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Benzoic Acid 04/08/2017 GAP TRGN YXXX10 2.4UG/L 10UU XXXXX XXXXXXXXXEPA-8270

Bis(2-Chloroethoxy)Methane 04/08/2017 GAP TRGN YXXX2.0 1.0UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

2,4-Dichlorophenol 04/08/2017 GAP TRGN YXXX2.0 0.79UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

1,2,4-Trichlorobenzene 04/08/2017 GAP TRGN YXXX2.0 1.1UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Naphthalene 04/08/2017 GAP TRGN YXXX2.0 0.58UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

4-Chloroaniline 04/08/2017 GAP TRGN YXXX2.0 1.9UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

2,6-Dichlorophenol 04/08/2017 GAP TRGN YXXX2.0 0.75UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Hexachlorobutadiene 04/08/2017 GAP TRGN YXXX2.0 2.0UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

4-Chloro-3-Methylphenol 04/08/2017 GAP TRGN YXXX2.0 1.2UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

2-Methylnaphthalene 04/08/2017 GAP TRGN YXXX2.0 1.0UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

1-Methylnaphthalene 04/08/2017 GAP TRGN YXXX2.0 0.97UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Hexachlorocyclopentadiene 04/08/2017 GAP TRGN YXXX2.0 2.0UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

2,4,6-Trichlorophenol 04/08/2017 GAP TRGN YXXX2.0 0.90UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

2,4,5-Trichlorophenol 04/08/2017 GAP TRGN YXXX2.0 1.5UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

2-Chloronaphthalene 04/08/2017 GAP TRGN YXXX2.0 0.90UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

2-Nitroaniline 04/08/2017 GAP TRGN YXXX2.0 0.76UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Acenaphthylene 04/08/2017 GAP TRGN YXXX2.0 0.80UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Dimethylphthalate 04/08/2017 GAP TRGN YXXX2.0 0.69UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

2,6-Dinitrotoluene 04/08/2017 GAP TRGN YXXX2.0 1.8UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Acenaphthene 04/08/2017 GAP TRGN YXXX2.0 0.79UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270


2,4-Dinitrophenol 04/08/2017 GAP TRGN YXXX10 2.9UG/L 10UU XXXXX XXXXXXXXXEPA-8270

4-Nitrophenol 04/08/2017 GAP TRGN YXXX2.0 2.0UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Dibenzofuran 04/08/2017 GAP TRGN YXXX2.0 0.51UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

2,4-Dinitrotoluene 04/08/2017 GAP TRGN YXXX2.0 0.78UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

2,3,4,6-Tetrachlorophenol 04/08/2017 GAP TRGN YXXX2.0 1.1UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Diethylphthalate 04/08/2017 GAP TRGN YXXX2.0 0.80UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Fluorene 04/08/2017 GAP TRGN YXXX2.0 1.0UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

4-Chlorophenyl-Phenylether 04/08/2017 GAP TRGN YXXX2.0 0.74UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270


4,6-Dinitro-2-Methylphenol 04/08/2017 GAP TRGN YXXX2.0 2.0UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

N-Nitrosodiphenylamine 04/08/2017 GAP TRGN YXXX2.0 0.92UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Azobenzene 04/08/2017 GAP TRGN YXXX2.0 1.6UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

4-Bromophenyl-Phenylether 04/08/2017 GAP TRGN YXXX2.0 0.79UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Hexachlorobenzene 04/08/2017 GAP TRGN YXXX2.0 0.63UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Pentachlorophenol 04/08/2017 GAP TRGN YXXX5.0 3.7UG/L 5.0UU XXXXX XXXXXXXXXEPA-8270

Phenanthrene 04/08/2017 GAP TRGN YXXX2.0 0.96UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Anthracene 04/08/2017 GAP TRGN YXXX2.0 0.80UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Page 30






ALS SDG#: EV17040044DATE: 5/5/2017


MB-040717W - Batch 115471 - Water by EPA-8270Carbazole 04/08/2017 GAP TRGN YXXX2.0 1.7UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Di-N-Butylphthalate 04/08/2017 GAP TRGN YXXX2.0 0.83UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Fluoranthene 04/08/2017 GAP TRGN YXXX2.0 0.93UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Pyrene 04/08/2017 GAP TRGN YXXX2.0 0.61UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Butylbenzylphthalate 04/08/2017 GAP TRGN YXXX2.0 0.67UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

3,3-Dichlorobenzidine 04/08/2017 GAP TRGN YXXX2.0 2.0UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Benzo[A]Anthracene 04/08/2017 GAP TRGN YXXX2.0 0.74UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Chrysene 04/08/2017 GAP TRGN YXXX2.0 0.80UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Bis(2-Ethylhexyl)Phthalate 04/08/2017 GAP TRGN YXXX2.0 0.81UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Di-N-Octylphthalate 04/08/2017 GAP TRGN YXXX2.0 0.87UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Benzo[B]Fluoranthene 04/08/2017 GAP TRGN YXXX2.0 1.1UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Benzo[K]Fluoranthene 04/08/2017 GAP TRGN YXXX2.0 1.3UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Benzo[A]Pyrene 04/08/2017 GAP TRGN YXXX2.0 0.48UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Indeno[1,2,3-Cd]Pyrene 04/08/2017 GAP TRGN YXXX2.0 0.58UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Dibenz[A,H]Anthracene 04/08/2017 GAP TRGN YXXX2.0 0.95UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270

Benzo[G,H,I]Perylene 04/08/2017 GAP TRGN YXXX2.0 0.54UG/L 2.0UU XXXXX XXXXXXXXXEPA-8270


MBLK-293315 - Batch R293315 - Water by EPA-245.1

METHOD

ANALYSIS

DATE

ANALYSIS

BYANALYTE

DET

ORG

RSLT TYPEXXX

RL PQLQUAL UNITS

LIMITS


REPORTING

RESULTS QUALXXXX

Mercury 04/10/2017 RAL TRGN NXXX0.20 0.11UG/L 0.20UU XXXXX XXXXXXXXXEPA-245.1


MBLK-R293007 - Batch R293007 - Water by EPA-245.1

METHOD

ANALYSIS

DATE

ANALYSIS

BYANALYTE

DET

ORG

RSLT TYPEXXX

RL PQLQUAL UNITS

LIMITS


REPORTING

RESULTS QUALXXXX

Mercury (Dissolved) 04/10/2017 RAL TRGN NXXX0.20 0.11UG/L 0.20UU XXXXX XXXXXXXXXEPA-245.1


MB-041717S - Batch 115403 - Soil by EPA-6020

METHOD

ANALYSIS

DATE

ANALYSIS

BYANALYTE

DET

ORG

RSLT TYPEXXX

RL PQLQUAL UNITS

LIMITS


REPORTING

RESULTS QUALXXXX

Antimony 04/18/2017 RAL TRGN NXXX0.10 0.047MG/KG 0.10UU XXXXX XXXXXXXXXEPA-6020

Arsenic 04/18/2017 RAL TRGN NXXX0.20 0.15MG/KG 0.20UU XXXXX XXXXXXXXXEPA-6020

Copper 04/18/2017 RAL TRGN NXXX0.10 0.047MG/KG 0.10UU XXXXX XXXXXXXXXEPA-6020

Lead 04/18/2017 RAL TRGN NXXX0.10 0.047MG/KG 0.10UU XXXXX XXXXXXXXXEPA-6020


Page 31






ALS SDG#: EV17040044DATE: 5/5/2017


MB-041217W - Batch 115320 - Water by EPA-200.8

METHOD

ANALYSIS

DATE

ANALYSIS

BYANALYTE

DET

ORG

RSLT TYPEXXX

RL PQLQUAL UNITS

LIMITS


REPORTING

RESULTS QUALXXXX

Antimony 04/13/2017 RAL TRGN NXXX2.5 0.32UG/L 2.5UU XXXXX XXXXXXXXXEPA-200.8

Arsenic 04/13/2017 RAL TRGN NXXX1.0 0.45UG/L 1.0UU XXXXX XXXXXXXXXEPA-200.8

Barium 04/13/2017 RAL TRGN NXXX1.0 0.67UG/L 1.0UU XXXXX XXXXXXXXXEPA-200.8

Cadmium 04/13/2017 RAL TRGN NXXX1.0 0.36UG/L 1.0UU XXXXX XXXXXXXXXEPA-200.8

Chromium 04/13/2017 RAL TRGN NXXX2.0 0.29UG/L 2.0UU XXXXX XXXXXXXXXEPA-200.8

Copper 04/13/2017 RAL TRGN NXXX2.0 0.80UG/L 2.0UU XXXXX XXXXXXXXXEPA-200.8

Lead 04/13/2017 RAL TRGN NXXX1.0 0.28UG/L 1.0UU XXXXX XXXXXXXXXEPA-200.8

Selenium 04/13/2017 RAL TRGN NXXX4.0 3.4UG/L 4.0UU XXXXX XXXXXXXXXEPA-200.8

Silver 04/13/2017 RAL TRGN NXXX1.0 0.20UG/L 1.0UU XXXXX XXXXXXXXXEPA-200.8


MB-041217W - Batch 115312 - Water by EPA-200.8

METHOD

ANALYSIS

DATE

ANALYSIS

BYANALYTE

DET

ORG

RSLT TYPEXXX

RL PQLQUAL UNITS

LIMITS


REPORTING

RESULTS QUALXXXX

Antimony (Dissolved) 04/13/2017 RAL TRGN NXXX2.5 0.32UG/L 2.5UU XXXXX XXXXXXXXXEPA-200.8

Arsenic (Dissolved) 04/13/2017 RAL TRGN NXXX1.0 0.45UG/L 1.0UU XXXXX XXXXXXXXXEPA-200.8

Barium (Dissolved) 04/13/2017 RAL TRGN NXXX1.0 0.67UG/L 1.0UU XXXXX XXXXXXXXXEPA-200.8

Cadmium (Dissolved) 04/13/2017 RAL TRGN NXXX1.0 0.36UG/L 1.0UU XXXXX XXXXXXXXXEPA-200.8

Chromium (Dissolved) 04/13/2017 RAL TRGN NXXX2.0 0.29UG/L 2.0UU XXXXX XXXXXXXXXEPA-200.8

Copper (Dissolved) 04/13/2017 RAL TRGN NXXX2.0 0.80UG/L 2.0UU XXXXX XXXXXXXXXEPA-200.8

Lead (Dissolved) 04/13/2017 RAL TRGN NXXX1.0 0.28UG/L 1.0UU XXXXX XXXXXXXXXEPA-200.8

Selenium (Dissolved) 04/13/2017 RAL TRGN NXXX4.0 3.4UG/L 4.0UU XXXXX XXXXXXXXXEPA-200.8

Silver (Dissolved) 04/13/2017 RAL TRGN NXXX1.0 0.20UG/L 1.0UU XXXXX XXXXXXXXXEPA-200.8


Page 32



LABORATORY CONTROL SAMPLE RESULTS



ALS SDG#: EV17040044DATE: 5/5/2017


XXXLABORATORY CONTROL SAMPLE RESULTS

115106 - Soil by NWTPH-GXALS Test Batch ID:

METHOD

ANALYSIS

DATERPD

ANALYSIS BY

MIN MAX RPDSPIKED COMPOUND QUAL

SPIKE

ADDED%REC

LIMITSD

ET

OR

GRSLT

TYPE

RPRTXXX

RESULTREPORTING MIN MAX

LIMITS

TPH-Volatile Range - BS 0.493.0 04/07/2017 SNC1 66.5 122.725.0 SC YesY Y92.4 XXXNWTPH-GX 23.1REPORTING REPORTING66.5 122.7

TPH-Volatile Range - BSD 0.49 1.53.0 04/07/2017 SNC1 66.5 122.725.0 SC YesY Y092.8 9.14 XXXNWTPH-GX 23.2REPORTING REPORTING66.5 122.7

115065 - Water by NWTPH-GXALS Test Batch ID:

METHOD

ANALYSIS

DATERPD

ANALYSIS BY


SPIKE

ADDED%REC

LIMITSD

ET

OR

GRSLT

TYPE

RPRTXXX


LIMITS

TPH-Volatile Range - BS 9.850 04/06/2017 SNC1 66.5 122.7500 SC YesY Y91.6 XXXNWTPH-GX 458REPORTING REPORTING66.5 122.7

TPH-Volatile Range - BSD 9.8 2950 04/06/2017 SNC1 66.5 122.7500 SC YesY Y293.5 9.14 XXXNWTPH-GX 467REPORTING REPORTING66.5 122.7

115303 - Soil by NWTPH-DXALS Test Batch ID:

METHOD

ANALYSIS

DATERPD

ANALYSIS BY


SPIKE

ADDED%REC

LIMITSD

ET

OR

GRSLT

TYPE

RPRTXXX


LIMITS

TPH-Diesel Range - BS 3.925 04/12/2017 EBS1 75.5 122.1125 SC YesY Y105 XXXNWTPH-DX 132REPORTING REPORTING75.5 122.1

TPH-Diesel Range - BSD 3.9 1225 04/12/2017 EBS1 75.5 122.1125 SC YesY Y3102 12 XXXNWTPH-DX 127REPORTING REPORTING75.5 122.1

115092 - Water by NWTPH-DXALS Test Batch ID:

METHOD

ANALYSIS

DATERPD

ANALYSIS BY


SPIKE

ADDED%REC

LIMITSD

ET

OR

GRSLT

TYPE

RPRTXXX


LIMITS

TPH-Diesel Range - BS 40130 04/06/2017 EBS1 67 125.21250 SC YesY Y82.2 XXXNWTPH-DX 1030REPORTING REPORTING67 125.2

TPH-Diesel Range - BSD 40 120130 04/06/2017 EBS1 67 125.21250 SC YesY Y384.9 10.8 XXXNWTPH-DX 1060REPORTING REPORTING67 125.2

115052 - Water by EPA-8260ALS Test Batch ID:

METHOD

ANALYSIS

DATERPD

ANALYSIS BY


SPIKE

ADDED%REC

LIMITSD

ET

OR

GRSLT

TYPE

RPRTXXX


LIMITS

1,1-Dichloroethene - BS 0.00462.0 04/03/2017 DLC1 72.5 13610.0 SC YesY Y102 XXXEPA-8260 10.2REPORTING REPORTING72.5 136

1,1-Dichloroethene - BSD 0.0046 0.0142.0 04/03/2017 DLC1 72.5 13610.0 SC YesY Y398.6 20.5 XXXEPA-8260 9.86REPORTING REPORTING72.5 136

Benzene - BS 0.00942.0 04/03/2017 DLC1 74.7 14310.0 SC YesY Y96.8 XXXEPA-8260 9.68REPORTING REPORTING74.7 143

Benzene - BSD 0.0094 0.0282.0 04/03/2017 DLC1 74.7 14310.0 SC YesY Y394.1 20.5 XXXEPA-8260 9.41REPORTING REPORTING74.7 143

Trichloroethene - BS 0.0182.0 04/03/2017 DLC1 74.4 14110.0 SC YesY Y92.3 XXXEPA-8260 9.23REPORTING REPORTING74.4 141

Trichloroethene - BSD 0.018 0.0542.0 04/03/2017 DLC1 74.4 14110.0 SC YesY Y191.2 20.5 XXXEPA-8260 9.12REPORTING REPORTING74.4 141

Toluene - BS 0.00512.0 04/03/2017 DLC1 71.7 13910.0 SC YesY Y96.9 XXXEPA-8260 9.69REPORTING REPORTING71.7 139

Toluene - BSD 0.0051 0.0152.0 04/03/2017 DLC1 71.7 13910.0 SC YesY Y394.1 20.5 XXXEPA-8260 9.41REPORTING REPORTING71.7 139

Chlorobenzene - BS 0.00802.0 04/03/2017 DLC1 73 13110.0 SC YesY Y98.8 XXXEPA-8260 9.88REPORTING REPORTING73 131

Chlorobenzene - BSD 0.0080 0.0242.0 04/03/2017 DLC1 73 13110.0 SC YesY Y396.1 20.5 XXXEPA-8260 9.61REPORTING REPORTING73 131

115467 - Soil by EPA-8270 SIMALS Test Batch ID:

METHOD

ANALYSIS

DATERPD

ANALYSIS BY


SPIKE

ADDED%REC

LIMITSD

ET

OR

GRSLT

TYPE

RPRTXXX


LIMITS

Naphthalene - BS 1.120 04/18/2017 GAP1 49.2 140500 SC YesY Y123 XXXEPA-8270 SIM 616REPORTING REPORTING49.2 140

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METHOD

ANALYSIS

DATERPD

ANALYSIS BY


SPIKE

ADDED%REC

LIMITSD

ET

OR

GRSLT

TYPE

RPRTXXX


LIMITS

Naphthalene - BSD 1.1 3.220 04/18/2017 GAP1 49.2 140500 SC YesY Y12109 17.3 XXXEPA-8270 SIM 545REPORTING REPORTING49.2 140

Acenaphthene - BS 0.8820 04/18/2017 GAP1 55 147500 SC YesY Y90.3 XXXEPA-8270 SIM 451REPORTING REPORTING55 147

Acenaphthene - BSD 0.88 2.620 04/18/2017 GAP1 55 147500 SC YesY Y19109 19 XXXEPA-8270 SIM 545REPORTING REPORTING55 147

Pyrene - BS 1.520 04/18/2017 GAP1 47.9 176500 SC YesY Y95.5 XXXEPA-8270 SIM 477REPORTING REPORTING47.9 176

Pyrene - BSD 1.5 4.520 04/18/2017 GAP1 47.9 176500 SC YesY Y18115 21.3 XXXEPA-8270 SIM 575REPORTING REPORTING47.9 176

Benzo[G,H,I]Perylene - BS 1.920 04/18/2017 GAP1 40.4 143500 SC YesY Y105 XXXEPA-8270 SIM 526REPORTING REPORTING40.4 143

Benzo[G,H,I]Perylene - BSD 1.9 5.620 04/18/2017 GAP1 40.4 143500 SC YesY Y20129 22.8 XXXEPA-8270 SIM 644REPORTING REPORTING40.4 143

115259 - Water by EPA-8270 SIMALS Test Batch ID:

METHOD

ANALYSIS

DATERPD

ANALYSIS BY


SPIKE

ADDED%REC

LIMITSD

ET

OR

GRSLT

TYPE

RPRTXXX


LIMITS

Naphthalene - BS 0.000780.020 04/11/2017 PAB1 36 1185.00 SC YesY Y62.4 XXXEPA-8270 SIM 3.12REPORTING REPORTING36 118

Naphthalene - BSD 0.00078 0.00240.020 04/12/2017 PAB1 36 1185.00 SC YesY Y867.5 27 XXXEPA-8270 SIM 3.38REPORTING REPORTING36 118

Acenaphthene - BS 0.00360.020 04/11/2017 PAB1 37 1255.00 SC YesY Y72.2 XXXEPA-8270 SIM 3.61REPORTING REPORTING37 125

Acenaphthene - BSD 0.0036 0.0110.020 04/12/2017 PAB1 37 1255.00 SC YesY Y878.5 29 XXXEPA-8270 SIM 3.93REPORTING REPORTING37 125

Pyrene - BS 0.00130.020 04/11/2017 PAB1 59 1565.00 SC YesY Y97.5 XXXEPA-8270 SIM 4.88REPORTING REPORTING59 156

Pyrene - BSD 0.0013 0.00380.020 04/12/2017 PAB1 59 1565.00 SC YesY Y18117 22 XXXEPA-8270 SIM 5.84REPORTING REPORTING59 156

Benzo[G,H,I]Perylene - BS 0.00200.020 04/11/2017 PAB1 43 1405.00 SC YesY Y109 XXXEPA-8270 SIM 5.47REPORTING REPORTING43 140

Benzo[G,H,I]Perylene - BSD 0.0020 0.00600.020 04/12/2017 PAB1 43 1405.00 SC YesY Y3113 21 XXXEPA-8270 SIM 5.66REPORTING REPORTING43 140

115471 - Water by EPA-8270ALS Test Batch ID:

METHOD

ANALYSIS

DATERPD

ANALYSIS BY


SPIKE

ADDED%REC

LIMITSD

ET

OR

GRSLT

TYPE

RPRTXXX


LIMITS

Phenol - BS 0.352.0 04/08/2017 GAP1 5 8450.0 SC YesY Y31.4 XXXEPA-8270 15.7REPORTING REPORTING5 84

Phenol - BSD 0.35 1.02.0 04/08/2017 GAP1 5 8450.0 SC YesY Y1527.0 22 XXXEPA-8270 13.5REPORTING REPORTING5 84

2-Chlorophenol - BS 0.282.0 04/08/2017 GAP1 45 11150.0 SC YesY Y82.4 XXXEPA-8270 41.2REPORTING REPORTING45 111

2-Chlorophenol - BSD 0.28 0.852.0 04/08/2017 GAP1 45 11150.0 SC YesY Y1372.0 17 XXXEPA-8270 36.0REPORTING REPORTING45 111

1,4-Dichlorobenzene - BS 0.342.0 04/08/2017 GAP1 27.1 11425.0 SC YesY Y55.6 XXXEPA-8270 13.9REPORTING REPORTING27.1 114

1,4-Dichlorobenzene - BSD 0.34 1.02.0 04/08/2017 GAP1 27.1 11425.0 SC YesY Y2145.1 21 XXXEPA-8270 11.3REPORTING REPORTING27.1 114

N-Nitroso-Di-N-Propylamine - BS 0.702.0 04/08/2017 GAP1 42.2 11925.0 SC YesY Y100 XXXEPA-8270 25.1REPORTING REPORTING42.2 119

N-Nitroso-Di-N-Propylamine - BSD 0.70 2.02.0 04/08/2017 GAP1 42.2 11925.0 SC YesY Y1586.1 14 XXXEPA-8270 21.5REPORTING REPORTING42.2 119

1,2,4-Trichlorobenzene - BS 0.372.0 04/08/2017 GAP1 29.4 12025.0 SC YesY Y59.3 XXXEPA-8270 14.8REPORTING REPORTING29.4 120

1,2,4-Trichlorobenzene - BSD 0.37 1.12.0 04/08/2017 GAP1 29.4 12025.0 SC YesY Y2148.3 23 XXXEPA-8270 12.1REPORTING REPORTING29.4 120

4-Chloro-3-Methylphenol - BS 0.402.0 04/08/2017 GAP1 44 11350.0 SC YesY Y80.7 XXXEPA-8270 40.3REPORTING REPORTING44 113

4-Chloro-3-Methylphenol - BSD 0.40 1.22.0 04/08/2017 GAP1 44 11350.0 SC YesY Y1172.2 18 XXXEPA-8270 36.1REPORTING REPORTING44 113

Acenaphthene - BS 0.262.0 04/08/2017 GAP1 41 10725.0 SC YesY Y103 XXXEPA-8270 25.8REPORTING REPORTING41 107

Acenaphthene - BSD 0.26 0.792.0 04/08/2017 GAP1 41 10725.0 SC YesY Y1390.3 13 XXXEPA-8270 22.6REPORTING REPORTING41 107

4-Nitrophenol - BS 1.52.0 04/08/2017 GAP1 5 6350.0 SC YesY Y21.8 XXXEPA-8270 10.9REPORTING REPORTING5 63

4-Nitrophenol - BSD 1.5 2.02.0 04/08/2017 GAP1 5 6350.0 SC YesY Y1219.3 25 XXXEPA-8270 9.67REPORTING REPORTING5 63

2,4-Dinitrotoluene - BS 0.262.0 04/08/2017 GAP1 53.1 13625.0 SC YesY Y105 XXXEPA-8270 26.2REPORTING REPORTING53.1 136

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METHOD

ANALYSIS

DATERPD

ANALYSIS BY


SPIKE

ADDED%REC

LIMITSD

ET

OR

GRSLT

TYPE

RPRTXXX


LIMITS

2,4-Dinitrotoluene - BSD 0.26 0.782.0 04/08/2017 GAP1 53.1 13625.0 SC YesY Y1193.3 18 XXXEPA-8270 23.3REPORTING REPORTING53.1 136

Pentachlorophenol - BS 1.25.0 04/08/2017 GAP1 33 12450.0 SC YesY Y71.2 XXXEPA-8270 35.6REPORTING REPORTING33 124

Pentachlorophenol - BSD 1.2 3.75.0 04/08/2017 GAP1 33 12450.0 SC YesY Y1660.4 30 XXXEPA-8270 30.2REPORTING REPORTING33 124

Pyrene - BS 0.202.0 04/08/2017 GAP1 18 13625.0 SC YesY Y114 XXXEPA-8270 28.6REPORTING REPORTING18 136

Pyrene - BSD 0.20 0.612.0 04/08/2017 GAP1 18 13625.0 SC YesY Y1796.3 18 XXXEPA-8270 24.1REPORTING REPORTING18 136

R293315 - Water by EPA-245.1ALS Test Batch ID:

METHOD

ANALYSIS

DATERPD

ANALYSIS BY


SPIKE

ADDED%REC

LIMITSD

ET

OR

GRSLT

TYPE

RPRTXXX


LIMITS

Mercury - BS 0.0360.20 04/10/2017 RAL1 80.6 118100 SC YesY N92.0 XXXEPA-245.1 92.0REPORTING REPORTING80.6 118

Mercury - BSD 0.036 0.110.20 04/10/2017 RAL1 80.6 118100 SC YesY N8100 7.94 XXXEPA-245.1 100REPORTING REPORTING80.6 118

R293007 - Water by EPA-245.1ALS Test Batch ID:

METHOD

ANALYSIS

DATERPD

ANALYSIS BY


SPIKE

ADDED%REC

LIMITSD

ET

OR

GRSLT

TYPE

RPRTXXX


LIMITS

Mercury (Dissolved) - BS 0.0360.20 04/10/2017 RAL1 80.6 118100 SC YesY N92.0 XXXEPA-245.1 92.0REPORTING REPORTING80.6 118

Mercury (Dissolved) - BSD 0.036 0.110.20 04/10/2017 RAL1 80.6 118100 SC YesY N8100 7.94 XXXEPA-245.1 100REPORTING REPORTING80.6 118

115403 - Soil by EPA-6020ALS Test Batch ID:

METHOD

ANALYSIS

DATERPD

ANALYSIS BY


SPIKE

ADDED%REC

LIMITSD

ET

OR

GRSLT

TYPE

RPRTXXX


LIMITS

Antimony - BS 0.0160.10 04/18/2017 RAL1 80 1205.00 SC YesY N95.0 XXXEPA-6020 4.75REPORTING REPORTING80 120

Antimony - BSD 0.016 0.0470.10 04/18/2017 RAL1 80 1205.00 SC YesY N397.7 9.83 XXXEPA-6020 4.89REPORTING REPORTING80 120

Arsenic - BS 0.0490.20 04/18/2017 RAL1 80 1205.00 SC YesY N96.6 XXXEPA-6020 4.83REPORTING REPORTING80 120

Arsenic - BSD 0.049 0.150.20 04/18/2017 RAL1 80 1205.00 SC YesY N298.4 8.91 XXXEPA-6020 4.92REPORTING REPORTING80 120

Copper - BS 0.0160.10 04/18/2017 RAL1 80 1205.00 SC YesY N99.6 XXXEPA-6020 4.98REPORTING REPORTING80 120

Copper - BSD 0.016 0.0470.10 04/18/2017 RAL1 80 1205.00 SC YesY N2102 8.69 XXXEPA-6020 5.09REPORTING REPORTING80 120

Lead - BS 0.0160.10 04/18/2017 RAL1 80 1205.00 SC YesY N98.5 XXXEPA-6020 4.92REPORTING REPORTING80 120

Lead - BSD 0.016 0.0470.10 04/18/2017 RAL1 80 1205.00 SC YesY N2100 9.36 XXXEPA-6020 5.02REPORTING REPORTING80 120

115320 - Water by EPA-200.8ALS Test Batch ID:

METHOD

ANALYSIS

DATERPD

ANALYSIS BY


SPIKE

ADDED%REC

LIMITSD

ET

OR

GRSLT

TYPE

RPRTXXX


LIMITS

Antimony - BS 0.112.5 04/13/2017 RAL1 88.9 114100 SC YesY N103 XXXEPA-200.8 103REPORTING REPORTING88.9 114

Antimony - BSD 0.11 0.322.5 04/13/2017 RAL1 88.9 114100 SC YesY N3106 10 XXXEPA-200.8 106REPORTING REPORTING88.9 114

Arsenic - BS 0.151.0 04/13/2017 RAL1 89.1 110100 SC YesY N100 XXXEPA-200.8 100REPORTING REPORTING89.1 110

Arsenic - BSD 0.15 0.451.0 04/13/2017 RAL1 89.1 110100 SC YesY N3103 10 XXXEPA-200.8 103REPORTING REPORTING89.1 110

Barium - BS 0.221.0 04/13/2017 RAL1 88.5 108100 SC YesY N102 XXXEPA-200.8 102REPORTING REPORTING88.5 108

Barium - BSD 0.22 0.671.0 04/13/2017 RAL1 88.5 108100 SC YesY N3104 10 XXXEPA-200.8 104REPORTING REPORTING88.5 108

Cadmium - BS 0.121.0 04/13/2017 RAL1 89.4 109100 SC YesY N101 XXXEPA-200.8 101REPORTING REPORTING89.4 109

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METHOD

ANALYSIS

DATERPD

ANALYSIS BY


SPIKE

ADDED%REC

LIMITSD

ET

OR

GRSLT

TYPE

RPRTXXX


LIMITS

Cadmium - BSD 0.12 0.361.0 04/13/2017 RAL1 89.4 109100 SC YesY N3105 10 XXXEPA-200.8 105REPORTING REPORTING89.4 109

Chromium - BS 0.102.0 04/13/2017 RAL1 88.3 110.2100 SC YesY N99.7 XXXEPA-200.8 99.7REPORTING REPORTING88.3 110.2

Chromium - BSD 0.10 0.292.0 04/13/2017 RAL1 88.3 110.2100 SC YesY N3103 10 XXXEPA-200.8 103REPORTING REPORTING88.3 110.2

Copper - BS 0.272.0 04/13/2017 RAL1 85.4 109100 SC YesY N102 XXXEPA-200.8 102REPORTING REPORTING85.4 109

Copper - BSD 0.27 0.802.0 04/13/2017 RAL1 85.4 109100 SC YesY N2104 10 XXXEPA-200.8 104REPORTING REPORTING85.4 109

Lead - BS 0.0901.0 04/13/2017 RAL1 87.5 107100 SC YesY N99.1 XXXEPA-200.8 99.1REPORTING REPORTING87.5 107

Lead - BSD 0.090 0.281.0 04/13/2017 RAL1 87.5 107100 SC YesY N4103 10 XXXEPA-200.8 103REPORTING REPORTING87.5 107

Selenium - BS 1.14.0 04/13/2017 RAL1 90.2 113100 SC YesY N101 XXXEPA-200.8 101REPORTING REPORTING90.2 113

Selenium - BSD 1.1 3.44.0 04/13/2017 RAL1 90.2 113100 SC YesY N4104 10 XXXEPA-200.8 104REPORTING REPORTING90.2 113

Silver - BS 0.0701.0 04/13/2017 RAL1 80 120100 SC YesY N99.6 XXXEPA-200.8 99.6REPORTING REPORTING80 120

Silver - BSD 0.070 0.201.0 04/13/2017 RAL1 80 120100 SC YesY N3103 10 XXXEPA-200.8 103REPORTING REPORTING80 120

115312 - Water by EPA-200.8ALS Test Batch ID:

METHOD

ANALYSIS

DATERPD

ANALYSIS BY


SPIKE

ADDED%REC

LIMITSD

ET

OR

GRSLT

TYPE

RPRTXXX


LIMITS

Antimony (Dissolved) - BS 0.112.5 04/13/2017 RAL1 88.9 114100 SC YesY N103 XXXEPA-200.8 103REPORTING REPORTING88.9 114

Antimony (Dissolved) - BSD 0.11 0.322.5 04/13/2017 RAL1 88.9 114100 SC YesY N3106 2.29 XXXEPA-200.8 106REPORTING REPORTING88.9 114

Arsenic (Dissolved) - BS 0.151.0 04/13/2017 RAL1 89.1 110100 SC YesY N100 XXXEPA-200.8 100REPORTING REPORTING89.1 110

Arsenic (Dissolved) - BSD 0.15 0.451.0 04/13/2017 RAL1 89.1 110100 SC YesY N3103 3.36 XXXEPA-200.8 103REPORTING REPORTING89.1 110

Barium (Dissolved) - BS 0.221.0 04/13/2017 RAL1 88.5 108100 SC YesY N102 XXXEPA-200.8 102REPORTING REPORTING88.5 108

Barium (Dissolved) - BSD 0.22 0.671.0 04/13/2017 RAL1 88.5 108100 SC YesY N3104 3.32 XXXEPA-200.8 104REPORTING REPORTING88.5 108

Cadmium (Dissolved) - BS 0.121.0 04/13/2017 RAL1 89.4 109100 SC YesY N101 XXXEPA-200.8 101REPORTING REPORTING89.4 109

Cadmium (Dissolved) - BSD 0.12 0.361.0 04/13/2017 RAL1 89.4 109100 SC YesY N3105 2.7 XXXEPA-200.8 105REPORTING REPORTING89.4 109

Chromium (Dissolved) - BS 0.102.0 04/13/2017 RAL1 86.2 107100 SC YesY N99.7 XXXEPA-200.8 99.7REPORTING REPORTING86.2 107

Chromium (Dissolved) - BSD 0.10 0.292.0 04/13/2017 RAL1 86.2 107100 SC YesY N3103 2.97 XXXEPA-200.8 103REPORTING REPORTING86.2 107

Copper (Dissolved) - BS 0.272.0 04/13/2017 RAL1 85.4 109100 SC YesY N102 XXXEPA-200.8 102REPORTING REPORTING85.4 109

Copper (Dissolved) - BSD 0.27 0.802.0 04/13/2017 RAL1 85.4 109100 SC YesY N2104 2.84 XXXEPA-200.8 104REPORTING REPORTING85.4 109

Lead (Dissolved) - BS 0.0901.0 04/13/2017 RAL1 87.5 107100 SC YesY N99.1 XXXEPA-200.8 99.1REPORTING REPORTING87.5 107

Lead (Dissolved) - BSD 0.090 0.281.0 04/13/2017 RAL1 87.5 107100 SC YesY N4103 2.43 XXXEPA-200.8 103REPORTING REPORTING87.5 107

Selenium (Dissolved) - BS 1.14.0 04/13/2017 RAL1 90.2 113100 SC YesY N101 XXXEPA-200.8 101REPORTING REPORTING90.2 113

Selenium (Dissolved) - BSD 1.1 3.44.0 04/13/2017 RAL1 90.2 113100 SC YesY N4104 4.68 XXXEPA-200.8 104REPORTING REPORTING90.2 113

Silver (Dissolved) - BS 0.0701.0 04/13/2017 RAL1 80 120100 SC YesY N99.6 XXXEPA-200.8 99.6REPORTING REPORTING80 120

Silver (Dissolved) - BSD 0.070 0.201.0 04/13/2017 RAL1 80 120100 SC YesY N3103 2.74 XXXEPA-200.8 103REPORTING REPORTING80 120

APPROVED BY:

Laboratory Director

APPROVED BY

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