Sample Name: Sirius Black Tested for: Western Oregon … Testing/REC... · 2020. 12. 11. · Sample...

Analytical ResultsSC Laboratories Oregon LLC ORELAP# 4133/OLCC# 1004748743D

15865 SW 74th Ave Suite 110, Tigard, OR

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Sirius Black

Western Oregon Botanicals

Laboratory ID: 19F0121-02

Matrix: Useable Marijuana

Sample Metrc ID: 1A40103000098BF000001733

Sample Name:

Tested for:

Compliance - Usable

Batch Size: 772.3 (g)

Batch RFID: 1A40103000098BF000001705

Lot # 5/2 SB

Strain: Sirius Black

Date Sampled: 06/26/19 10:12

Date Accepted: 06/26/19

License: 020-10021071D94

Potency Analysis

Analysis Method/SOP: Potency

* - ORELAP certified analyte

1.06

16.50

0.090.530.04

THC 1.06

THCA 16.50

CBG 0.09

CBGA 0.53

CBC 0.04

Total: 18.22

Cannabinoids Profile

Date Extracted: 07/01/19

Date Analyzed: 07/02/19

Cannabinoids mg/g LOQ (%)% weight

Total THC ((THCA*0.877)+d9) 155.315.53 0.03

Total CBD ((CBDA*0.877)+CBD) < LOQ< LOQ 0.03

1.06d9-THC (d9-Tetrahydrocannabinol)* 10.6 0.04

< LOQd8-THC (d8-Tetrahydrocannabinol)* < LOQ 0.04

16.50THCA (d9-Tetrahydrocannabinolic Acid)* 165 0.07

< LOQCBD (Cannabidiol)* < LOQ 0.03

< LOQCBDA (Cannabidiolic Acid)* < LOQ 0.07

< LOQCBN (Cannabinol)* < LOQ 0.03

0.09CBG (Cannabigerol)* 0.9 0.04

0.53CBGA (Cannabigerolic Acid) 5.3 0.04

< LOQCBDV (Cannabidivarin)* < LOQ 0.04

< LOQCBDVA (Cannabidivarinic Acid) < LOQ 0.04

0.04CBC (Cannabichromene)* 0.4 0.04

< LOQTHCV (Tetrahydrocannabivarin) < LOQ 0.04

181.8Total Cannabinoids 18.18 0.03

Water Activity and Moisture

ResultAnalyte LOQ Analyzed MethodUnitsLimit

0.543 0.0300AW Water Activity07/01/2019Water Activity 0.65

9.02 0.10% Moisture07/01/2019Percent Moisture 15

Results above the action level are highlighted in red #.Cannabinoids reported as dry weight (moisture corrected)



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Terpene Analysis





Date Sampled: 06/26/19 10:12

Sample Name:

Tested for:

Sirius Black


Compliance - Usable

Lot # 5/2 SB

Batch RFID: 1A40103000098BF000001705



License: 020-10021071D94

Date Extracted: 07/01/19

Date Analyzed: 07/02/19

Analysis Method/SOP: Potency

Analyte LOQ Analyte Result LOQResult (%)

alpha Pinene 0.042 0.019 Myrcene 0.406 0.019

alpha Phellandrene < LOQ 0.019 3-Carene < LOQ 0.019

alpha Terpinene < LOQ 0.019 Limonene 0.201 0.019

Terpinolene < LOQ 0.019 Linalool 0.095 0.019

Fenchol 0.042 0.019 Borneol < LOQ 0.019

Terpineol 0.041 0.019 Geraniol 0.052 0.019

alpha Humulene 0.040 0.019 beta Caryophyllene 0.124 0.019

Caryophyllene Oxide < LOQ 0.019 alpha Bisabolol 0.074 0.019

Camphene < LOQ 0.019 beta Pinene 0.060 0.019

Ocimene 0.042 0.019 Sabinene < LOQ 0.019

Camphor < LOQ 0.019 Isoborneol < LOQ 0.019

Menthol < LOQ 0.019 alpha Cedrene < LOQ 0.019

Nerolidol 0.024 0.019 R-(+)-Pulegone < LOQ 0.019

Eucalyptol < LOQ 0.019 p-Cymene < LOQ 0.019

(-)-Isopulegol < LOQ 0.019 Geranyl Acetate < LOQ 0.019

Guaiol < LOQ 0.019 Valencene 0.065 0.019

Phytol 0.044 0.019 Citronellol < LOQ 0.019

gamma-Terpinene < LOQ 0.019

Total Terpenes 1.352 %



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Date Accepted: 06/26/19 14:52

Date Sampled: 06/26/19 10:12

Laboratory ID: 19F0121-02 Client/Metrc ID: 1A40103000098BF000001733

Terpene Profile

Tested for:

Sample Name:


Sirius Black

Compliance - Usable

License: 020-10021071D94

0.00 0.05 0.10 0.15 0.20 0.25 0.30 0.35 0.40 0.45

alpha Pinene

Myrcene

alpha Phellandrene

3-Carene

alpha Terpinene

Limonene

Terpinolene

Linalool

Fenchol

Borneol

Terpineol

Geraniol

alpha Humulene

beta Caryophyllene

Caryophyllene Oxide

alpha Bisabolol

Camphene

beta Pinene

Ocimene

Sabinene

Camphor

Isoborneol

Menthol

alpha Cedrene

Nerolidol

R-(+)-Pulegone

Eucalyptol

p-Cymene

(-)-Isopulegol

Geranyl Acetate

Guaiol

Valencene

Phytol

Citronellol

gamma-Terpinene

%

These results relate only to the sample included on this report. The report may not be reproduced except in full, without

the written permission of SC Laboratories. Samples tested in accordance with Oregon Administrative Rules, TNI 2009

Standard and SC Laboratories quality assurance plan unless otherwise noted.

Page 3 of 18 07/02/2019 17:41

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Pesticide Analysis in ppm

Date Sampled: 06/26/19 10:12






Sirius BlackSample Name:

Tested for:

Compliance - Usable


Batch RFID: 1A40103000098BF000001705

Lot # 5/2 SB


License: 020-10021071D94

Date Analyzed:

Date Extracted: 07/01/19 Analysis Method/SOP: Pesticides

07/02/19 Results above the action levels are highlighed in red #.

Analyte LOQResult Action Level Analyte Result Action Level LOQ

0.5< LOQ 0.25Abamectin 0.4< LOQ 0.20Acephate

2< LOQ 0.99Acequinocyl 0.2< LOQ 0.10Acetamiprid

0.4< LOQ 0.20Aldicarb 0.2< LOQ 0.10Azoxystrobin

0.2< LOQ 0.10Bifenazate 0.2< LOQ 0.10Bifenthrin

0.4< LOQ 0.20Boscalid 0.2< LOQ 0.10Carbaryl

0.2< LOQ 0.10Carbofuran 0.2< LOQ 0.10Chlorantraniliprole

1< LOQ 0.49Chlorfenapyr 0.2< LOQ 0.10Chlorpyrifos

0.2< LOQ 0.10Clofentezine 1< LOQ 0.49Cyfluthrin

1< LOQ 0.49Cypermethrin 1< LOQ 0.49Daminozide

1< LOQ 0.49DDVP (Dichlorvos) 0.2< LOQ 0.10Diazinon

0.2< LOQ 0.10Dimethoate 0.2< LOQ 0.10Ethoprophos

0.4< LOQ 0.20Etofenprox 0.2< LOQ 0.10Etoxazole

0.2< LOQ 0.10Fenoxycarb 0.4< LOQ 0.20Fenpyroximate

0.4< LOQ 0.20Fipronil 1< LOQ 0.49Flonicamid

0.4< LOQ 0.20Fludioxonil 1< LOQ 0.49Hexythiazox

0.2< LOQ 0.10Imazalil 0.4< LOQ 0.20Imidacloprid

0.4< LOQ 0.20Kresoxim-methyl 0.2< LOQ 0.10Malathion

0.2< LOQ 0.10Metalaxyl 0.2< LOQ 0.10Methiocarb

0.4< LOQ 0.20Methomyl 0.2< LOQ 0.10Methyl parathion

0.2< LOQ 0.10MGK-264 0.2< LOQ 0.10Myclobutanil

0.5< LOQ 0.25Naled 1< LOQ 0.49Oxamyl

0.4< LOQ 0.20Paclobutrazol 0.2< LOQ 0.10Permethrins (total)

0.2< LOQ 0.10Phosmet 2< LOQ 0.49Piperonyl butoxide

0.2< LOQ 0.10Prallethrin 0.4< LOQ 0.20Propiconazole

0.2< LOQ 0.10Propoxur 1< LOQ 0.49Pyrethrins (total)

0.2< LOQ 0.10Pyridaben 0.2< LOQ 0.10Spinosad

0.2< LOQ 0.10Spiromesifen 0.2< LOQ 0.10Spirotetramat

0.4< LOQ 0.20Spiroxamine 0.4< LOQ 0.20Tebuconazole

0.2< LOQ 0.10Thiacloprid 0.2< LOQ 0.10Thiamethoxam

0.2< LOQ 0.10Trifloxystrobin



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Case Narrative

Receiving: Samples: 19F0121-01 (1732) and 19F0121-02 (1733) composited for Pesticide,

Moisture Content and Water Activity.

Pesticides - Abamectin, Imidachloprid, and Spiroxamine recovered above the upper acceptance

limit in the Blank Spike, Matrix Spike, and Matrix Spike Duplicate. Daminozide recovered above

the upper acceptance limit in the Blank Spike. Analytes were below the reporting limit in all client

samples.

Terpenes - Phytol result was above QC criteria in the Method Blank.

Nerolidol exceeded normally accepted RPD criteria in the Sample Duplicate due to relatively

large variations in very small values.

Quality Control

Potency

Batch: B191141 - Potency/Terpenes

Blank(B191141-BLK1) Extracted - 07/01/19 16:00 Analyzed - 07/01/19 22:26

Analyte Result Units

Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

d9-THC (d9-Tetrahydrocannabinol) < LOQ %

d8-THC (d8-Tetrahydrocannabinol) < LOQ %

THCA (d9-Tetrahydrocannabinolic Acid) < LOQ %

CBD (Cannabidiol) < LOQ %

CBDA (Cannabidiolic Acid) < LOQ %

CBN (Cannabinol) < LOQ %

CBG (Cannabigerol) < LOQ %

CBGA (Cannabigerolic Acid) < LOQ %

CBDV (Cannabidivarin) < LOQ %

CBDVA (Cannabidivarinic Acid) < LOQ %

CBC (Cannabichromene) < LOQ %

THCV (Tetrahydrocannabivarin) < LOQ %

Duplicate(B191141-DUP1) Extracted - 07/01/19 16:00 Analyzed - 07/01/19 22:43


Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

d9-THC (d9-Tetrahydrocannabinol) 0.53 % 0.62 14.4 20

d8-THC (d8-Tetrahydrocannabinol) < LOQ % < LOQ 20

THCA (d9-Tetrahydrocannabinolic Acid) 25.30 % 28.52 12.0 20

CBD (Cannabidiol) < LOQ % < LOQ 20

CBDA (Cannabidiolic Acid) 0.07 % 0.08 12.8 20

CBN (Cannabinol) < LOQ % < LOQ 20




Page 5 of 18 07/02/2019 17:41


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Quality Control

Potency (Continued)

Batch: B191141 - Potency/Terpenes (Continued)



Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

CBG (Cannabigerol) 0.08 % 0.08 8.75 20

CBGA (Cannabigerolic Acid) 1.24 % 1.39 11.2 20

CBDV (Cannabidivarin) < LOQ % < LOQ 20

CBDVA (Cannabidivarinic Acid) < LOQ % < LOQ 20

CBC (Cannabichromene) < LOQ % < LOQ 20

THCV (Tetrahydrocannabivarin) < LOQ % < LOQ 20

LCS(B191141-BS1) Extracted - 07/01/19 16:00 Analyzed - 07/02/19 11:39


Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

d9-THC (d9-Tetrahydrocannabinol) 0.05 % 0.0400 118 80-120

CBD (Cannabidiol) 0.04 % 0.0400 108 80-120

CBDA (Cannabidiolic Acid) 0.04 % 0.0400 97.3 80-120

CBN (Cannabinol) 0.04 % 0.0400 101 80-120




Page 6 of 18 07/02/2019 17:41


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Pesticide Analysis

Batch: B191140 - Pesticide Prep



Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Abamectin < LOQ ppm

Acephate < LOQ ppm

Acequinocyl < LOQ ppm

Acetamiprid < LOQ ppm

Aldicarb < LOQ ppm

Azoxystrobin < LOQ ppm

Bifenazate < LOQ ppm

Bifenthrin < LOQ ppm

Boscalid < LOQ ppm

Carbaryl < LOQ ppm

Carbofuran < LOQ ppm

Chlorantraniliprole < LOQ ppm

Chlorfenapyr < LOQ ppm

Chlorpyrifos < LOQ ppm

Clofentezine < LOQ ppm

Cyfluthrin < LOQ ppm

Cypermethrin < LOQ ppm

Daminozide < LOQ ppm

DDVP (Dichlorvos) < LOQ ppm

Diazinon < LOQ ppm

Dimethoate < LOQ ppm

Ethoprophos < LOQ ppm

Etofenprox < LOQ ppm

Etoxazole < LOQ ppm

Fenoxycarb < LOQ ppm

Fenpyroximate < LOQ ppm

Fipronil < LOQ ppm

Flonicamid < LOQ ppm

Fludioxonil < LOQ ppm

Hexythiazox < LOQ ppm

Imazalil < LOQ ppm

Imidacloprid < LOQ ppm

Kresoxim-methyl < LOQ ppm

Malathion < LOQ ppm

Metalaxyl < LOQ ppm




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Quality Control

Pesticide Analysis (Continued)

Batch: B191140 - Pesticide Prep (Continued)



Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Methiocarb < LOQ ppm

Methomyl < LOQ ppm

Methyl parathion < LOQ ppm

MGK-264 < LOQ ppm

Myclobutanil < LOQ ppm

Naled < LOQ ppm

Oxamyl < LOQ ppm

Paclobutrazol < LOQ ppm

Permethrins (total) < LOQ ppm

Phosmet < LOQ ppm

Piperonyl butoxide < LOQ ppm

Prallethrin < LOQ ppm

Propiconazole < LOQ ppm

Propoxur < LOQ ppm

Pyrethrins (total) < LOQ ppm

Pyridaben < LOQ ppm

Spinosad < LOQ ppm

Spiromesifen < LOQ ppm

Spirotetramat < LOQ ppm

Spiroxamine < LOQ ppm

Tebuconazole < LOQ ppm

Thiacloprid < LOQ ppm

Thiamethoxam < LOQ ppm

Trifloxystrobin < LOQ ppm



Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Abamectin 1.51 ppm 0.980 154 29-150

Acephate 0.99 ppm 1.00 99.5 48-133

Acequinocyl 0.52 ppm 1.00 52.3 48-150

Acetamiprid 0.99 ppm 1.00 99.0 45-150

Aldicarb 1.14 ppm 1.00 114 58-134

Azoxystrobin 1.00 ppm 1.00 99.9 25-150

Bifenazate 0.96 ppm 1.00 95.9 46-141

Bifenthrin 0.99 ppm 1.00 98.6 55-150




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Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Boscalid 0.99 ppm 1.00 99.4 34-141

Carbaryl 1.02 ppm 1.00 102 67-125

Carbofuran 1.14 ppm 1.00 114 71-128

Chlorantraniliprole 0.93 ppm 1.00 93.4 43-138

Chlorfenapyr 1.02 ppm 1.00 102 45-150

Chlorpyrifos 0.97 ppm 1.00 97.4 36-150

Clofentezine 1.01 ppm 1.00 101 59-135

Cyfluthrin 1.45 ppm 1.00 145 33-150

Cypermethrin 1.22 ppm 1.00 122 47-148

Daminozide 1.47 ppm 1.00 147 18-116

DDVP (Dichlorvos) 1.11 ppm 1.00 111 65-150

Diazinon 1.01 ppm 1.00 101 60-130

Dimethoate 1.05 ppm 1.00 105 65-131

Ethoprophos 1.02 ppm 1.00 102 52-150

Etofenprox 0.90 ppm 1.00 89.5 60-139

Etoxazole 0.91 ppm 1.00 91.0 59-122

Fenoxycarb 1.09 ppm 1.00 109 39-146

Fenpyroximate 1.19 ppm 1.00 119 44-147

Fipronil 1.10 ppm 1.00 110 40-143

Flonicamid 0.99 ppm 1.00 99.4 50-142

Fludioxonil 0.93 ppm 1.00 92.7 49-150

Hexythiazox 1.06 ppm 1.00 106 41-142

Imazalil 1.02 ppm 1.00 102 61-127

Imidacloprid 1.91 ppm 1.00 191 36-150

Kresoxim-methyl 0.99 ppm 1.00 99.3 53-131

Malathion 1.01 ppm 1.00 101 55-134

Metalaxyl 1.02 ppm 1.00 102 64-127

Methiocarb 1.08 ppm 1.00 108 53-144

Methomyl 1.03 ppm 1.00 103 47-141

Methyl parathion 1.20 ppm 1.00 120 48-142

MGK-264 0.61 ppm 0.630 97.5 38-150

Myclobutanil 1.00 ppm 1.00 100 45-146

Naled 0.81 ppm 1.00 80.8 28-113

Oxamyl 1.13 ppm 1.00 113 48-133

Paclobutrazol 1.04 ppm 1.00 104 37-150




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Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Permethrins (total) 1.19 ppm 1.00 119 46-150

Phosmet 1.02 ppm 1.00 102 48-137

Piperonyl butoxide 0.97 ppm 1.00 97.5 43-142

Prallethrin 1.05 ppm 1.00 105 48-144

Propiconazole 1.04 ppm 1.00 104 52-136

Propoxur 1.10 ppm 1.00 110 61-131

Pyrethrins (total) 0.82 ppm 0.630 131 24-150

Pyridaben 1.01 ppm 1.00 101 40-150

Spinosad 0.86 ppm 0.820 104 42-148

Spiromesifen 0.99 ppm 1.00 98.9 38-150

Spirotetramat 1.03 ppm 1.00 103 37-132

Spiroxamine 0.99 ppm 0.550 180 49-136

Tebuconazole 1.07 ppm 1.00 107 46-142

Thiacloprid 0.99 ppm 1.00 99.4 48-150

Thiamethoxam 1.32 ppm 1.00 132 46-138

Trifloxystrobin 0.97 ppm 1.00 97.4 44-144

Matrix Spike(B191140-MS1) Extracted - 07/01/19 1:09 Analyzed - 07/01/19 21:55


Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Abamectin 1.94 ppm 0.969 200 15-150< LOQ

Acephate 0.93 ppm 0.989 94.4 45-130< LOQ

Acequinocyl 0.57 ppm 0.989 58.0 31-146< LOQ

Acetamiprid 1.04 ppm 0.989 105 39-150< LOQ

Aldicarb 1.05 ppm 0.989 107 47-143< LOQ

Azoxystrobin 1.04 ppm 0.989 105 21-150< LOQ

Bifenazate 1.08 ppm 0.989 110 31-150< LOQ

Bifenthrin 0.64 ppm 0.989 64.8 23-132< LOQ

Boscalid 1.15 ppm 0.989 116 41-141< LOQ

Carbaryl 1.02 ppm 0.989 103 60-125< LOQ

Carbofuran 1.12 ppm 0.989 113 57-136< LOQ

Chlorantraniliprole 1.22 ppm 0.989 123 32-145< LOQ

Chlorfenapyr 1.33 ppm 0.989 135 29-150< LOQ

Chlorpyrifos 0.89 ppm 0.989 90.4 29-146< LOQ

Clofentezine 0.93 ppm 0.989 93.8 48-128< LOQ

Cyfluthrin 1.22 ppm 0.989 123 16-150< LOQ




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Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Cypermethrin 1.15 ppm 0.989 116 22-150< LOQ

Daminozide 1.47 ppm 0.989 149 34-150< LOQ

DDVP (Dichlorvos) 1.06 ppm 0.989 107 55-133< LOQ

Diazinon 1.02 ppm 0.989 103 54-126< LOQ

Dimethoate 0.97 ppm 0.989 98.3 60-129< LOQ

Ethoprophos 1.03 ppm 0.989 104 40-150< LOQ

Etofenprox 0.81 ppm 0.989 81.8 25-135< LOQ

Etoxazole 0.90 ppm 0.989 91.0 26-149< LOQ

Fenoxycarb 1.15 ppm 0.989 116 37-145< LOQ

Fenpyroximate 1.21 ppm 0.989 122 27-150< LOQ

Fipronil 0.94 ppm 0.989 95.4 27-150< LOQ

Flonicamid 0.95 ppm 0.989 96.0 46-139< LOQ

Fludioxonil 1.00 ppm 0.989 101 31-150< LOQ

Hexythiazox 1.09 ppm 0.989 111 32-150< LOQ

Imazalil 1.06 ppm 0.989 107 44-142< LOQ

Imidacloprid 1.72 ppm 0.989 174 23-150< LOQ

Kresoxim-methyl 0.98 ppm 0.989 98.8 49-130< LOQ

Malathion 1.05 ppm 0.989 106 25-150< LOQ

Metalaxyl 1.05 ppm 0.989 106 49-141< LOQ

Methiocarb 1.06 ppm 0.989 108 44-146< LOQ

Methomyl 0.99 ppm 0.989 100 44-136< LOQ

Methyl parathion 1.06 ppm 0.989 107 15-150< LOQ

MGK-264 0.56 ppm 0.623 89.6 22-150< LOQ

Myclobutanil 1.08 ppm 0.989 109 34-150< LOQ

Naled 0.94 ppm 0.989 94.9 38-142< LOQ

Oxamyl 1.06 ppm 0.989 107 40-132< LOQ

Paclobutrazol 1.08 ppm 0.989 110 29-147< LOQ

Permethrins (total) 0.78 ppm 0.989 79.0 27-104< LOQ

Phosmet 1.11 ppm 0.989 112 35-150< LOQ

Piperonyl butoxide 0.89 ppm 0.989 90.1 34-143< LOQ

Prallethrin 1.05 ppm 0.989 106 33-150< LOQ

Propiconazole 1.15 ppm 0.989 116 46-138< LOQ

Propoxur 1.08 ppm 0.989 110 50-138< LOQ

Pyrethrins (total) 0.79 ppm 0.623 127 21-150< LOQ

Pyridaben 0.51 ppm 0.989 51.4 39-150< LOQ




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Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Spinosad 0.88 ppm 0.811 109 31-150< LOQ

Spiromesifen 0.97 ppm 0.989 98.3 27-141< LOQ

Spirotetramat 1.17 ppm 0.989 118 31-141< LOQ

Spiroxamine 1.04 ppm 0.544 191 57-139< LOQ

Tebuconazole 1.11 ppm 0.989 112 32-140< LOQ

Thiacloprid 1.00 ppm 0.989 101 45-150< LOQ

Thiamethoxam 1.21 ppm 0.989 122 40-141< LOQ

Trifloxystrobin 0.98 ppm 0.989 99.3 30-137< LOQ

Matrix Spike Dup(B191140-MSD1) Extracted - 07/01/19 1:09 Analyzed - 07/01/19


Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Abamectin 1.84 ppm 0.953 193 15-150< LOQ 3.39 40

Acephate 0.92 ppm 0.973 94.4 45-130< LOQ 0.0875 26

Acequinocyl 0.61 ppm 0.973 63.1 31-146< LOQ 8.34 50

Acetamiprid 0.99 ppm 0.973 102 39-150< LOQ 2.75 21

Aldicarb 1.02 ppm 0.973 104 47-143< LOQ 2.06 30

Azoxystrobin 0.99 ppm 0.973 102 21-150< LOQ 2.74 21

Bifenazate 1.05 ppm 0.973 108 31-150< LOQ 1.91 20

Bifenthrin 0.62 ppm 0.973 63.7 23-132< LOQ 1.70 30

Boscalid 1.12 ppm 0.973 115 41-141< LOQ 0.322 20

Carbaryl 0.98 ppm 0.973 101 60-125< LOQ 2.72 20

Carbofuran 1.09 ppm 0.973 112 57-136< LOQ 1.36 24

Chlorantraniliprole 1.19 ppm 0.973 122 32-145< LOQ 0.765 20

Chlorfenapyr 1.42 ppm 0.973 146 29-150< LOQ 8.39 50

Chlorpyrifos 0.89 ppm 0.973 91.4 29-146< LOQ 1.14 24

Clofentezine 0.91 ppm 0.973 93.2 48-128< LOQ 0.731 20

Cyfluthrin 1.32 ppm 0.973 136 16-150< LOQ 10.1 50

Cypermethrin 1.21 ppm 0.973 124 22-150< LOQ 6.70 30

Daminozide 1.43 ppm 0.973 147 34-150< LOQ 0.966 30

DDVP (Dichlorvos) 1.04 ppm 0.973 107 55-133< LOQ 0.140 30

Diazinon 0.98 ppm 0.973 101 54-126< LOQ 1.82 20

Dimethoate 0.98 ppm 0.973 100 60-129< LOQ 2.12 20

Ethoprophos 0.97 ppm 0.973 99.9 40-150< LOQ 3.99 29

Etofenprox 0.80 ppm 0.973 81.7 25-135< LOQ 0.0784 24

Etoxazole 0.87 ppm 0.973 89.2 26-149< LOQ 1.98 30




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Matrix Spike Dup(B191140-MSD1) Extracted - 07/01/19 1:09 Analyzed - 07/01/19


Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Fenoxycarb 1.11 ppm 0.973 114 37-145< LOQ 1.54 23

Fenpyroximate 1.18 ppm 0.973 122 27-150< LOQ 0.446 20

Fipronil 0.90 ppm 0.973 92.6 27-150< LOQ 2.96 28

Flonicamid 0.96 ppm 0.973 98.9 46-139< LOQ 2.96 29

Fludioxonil 0.96 ppm 0.973 98.6 31-150< LOQ 2.83 30

Hexythiazox 1.07 ppm 0.973 110 32-150< LOQ 0.820 28

Imazalil 1.02 ppm 0.973 105 44-142< LOQ 1.91 25

Imidacloprid 1.71 ppm 0.973 176 23-150< LOQ 0.866 30

Kresoxim-methyl 0.94 ppm 0.973 97.1 49-130< LOQ 1.76 20

Malathion 1.03 ppm 0.973 106 25-150< LOQ 0.0625 21

Metalaxyl 0.98 ppm 0.973 101 49-141< LOQ 4.70 20

Methiocarb 1.04 ppm 0.973 107 44-146< LOQ 0.353 20

Methomyl 0.97 ppm 0.973 99.5 44-136< LOQ 0.461 30

Methyl parathion 0.93 ppm 0.973 95.1 15-150< LOQ 12.2 50

MGK-264 0.54 ppm 0.613 87.6 22-150< LOQ 2.19 24

Myclobutanil 1.04 ppm 0.973 107 34-150< LOQ 1.85 23

Naled 0.87 ppm 0.973 89.7 38-142< LOQ 5.61 25

Oxamyl 1.07 ppm 0.973 110 40-132< LOQ 2.65 30

Paclobutrazol 1.08 ppm 0.973 111 29-147< LOQ 1.11 20

Permethrins (total) 0.72 ppm 0.973 73.7 27-104< LOQ 6.84 30

Phosmet 1.11 ppm 0.973 114 35-150< LOQ 1.43 20

Piperonyl butoxide 0.87 ppm 0.973 89.6 34-143< LOQ 0.516 21

Prallethrin 1.02 ppm 0.973 105 33-150< LOQ 0.954 25

Propiconazole 1.09 ppm 0.973 112 46-138< LOQ 3.80 20

Propoxur 1.07 ppm 0.973 110 50-138< LOQ 0.111 28

Pyrethrins (total) 0.79 ppm 0.613 129 21-150< LOQ 1.52 28

Pyridaben 0.49 ppm 0.973 50.9 39-150< LOQ 0.994 23

Spinosad 0.85 ppm 0.798 106 31-150< LOQ 2.58 30

Spiromesifen 0.95 ppm 0.973 97.6 27-141< LOQ 0.661 30

Spirotetramat 1.11 ppm 0.973 114 31-141< LOQ 3.80 25

Spiroxamine 1.01 ppm 0.535 188 57-139< LOQ 1.25 20

Tebuconazole 1.08 ppm 0.973 111 32-140< LOQ 1.49 20

Thiacloprid 0.96 ppm 0.973 98.9 45-150< LOQ 1.77 21

Thiamethoxam 1.21 ppm 0.973 125 40-141< LOQ 2.00 30

Trifloxystrobin 0.96 ppm 0.973 98.9 30-137< LOQ 0.404 29




Page 13 of 18 07/02/2019 17:41


Lab Director



503-272-8830

www.sclabs.com

Quality Control

Terpene Analysis

Batch: B191142 - Potency/Terpenes



Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

alpha Pinene < LOQ %

Myrcene < LOQ %

alpha Phellandrene < LOQ %

3-Carene < LOQ %

alpha Terpinene < LOQ %

Limonene < LOQ %

Terpinolene < LOQ %

Linalool < LOQ %

Fenchol < LOQ %

Borneol < LOQ %

Terpineol < LOQ %

Geraniol < LOQ %

alpha Humulene < LOQ %

beta Caryophyllene < LOQ %

Caryophyllene Oxide < LOQ %

alpha Bisabolol < LOQ %

Camphene < LOQ %

beta Pinene < LOQ %

Ocimene < LOQ %

Sabinene < LOQ %

Camphor < LOQ %

Isoborneol < LOQ %

Menthol < LOQ %

alpha Cedrene < LOQ %

Nerolidol < LOQ %

R-(+)-Pulegone < LOQ %

Eucalyptol < LOQ %

p-Cymene < LOQ %

(-)-Isopulegol < LOQ %

Geranyl Acetate < LOQ %

Guaiol < LOQ %

Valencene < LOQ %

Phytol 0.139 %

Citronellol < LOQ %

gamma-Terpinene < LOQ %




Page 14 of 18 07/02/2019 17:41


Lab Director



503-272-8830

www.sclabs.com

Quality Control

Terpene Analysis (Continued)




Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

alpha Ocimene < LOQ % < LOQ 20

alpha Terpineol 0.052 % 0.059 12.7 20

beta Ocimene 0.054 % 0.059 8.49 20

beta Terpineol < LOQ % < LOQ 20

cis-Nerolidol < LOQ % 0.021 20

Phytol 1 < LOQ % < LOQ 20

Phytol 2 0.036 % 0.042 15.3 20

trans-Nerolidol < LOQ % 0.030 37.6 20

alpha Pinene 0.091 % 0.105 14.8 20

Myrcene 0.192 % 0.219 12.9 20

alpha Phellandrene 0.054 % 0.062 14.8 20

3-Carene 0.042 % 0.047 11.6 20

alpha Terpinene 0.029 % 0.035 19.8 20

Limonene 0.276 % 0.323 15.4 20

Terpinolene 0.877 % 0.999 13.0 20

Linalool 0.225 % 0.255 12.8 20

Fenchol 0.034 % 0.040 14.1 20

Borneol < LOQ % < LOQ 20

Terpineol 0.052 % 0.059 12.7 20

Geraniol < LOQ % < LOQ 20

alpha Humulene 0.099 % 0.110 9.93 20

beta Caryophyllene 0.260 % 0.287 9.79 20

Caryophyllene Oxide < LOQ % < LOQ 20

alpha Bisabolol 0.039 % 0.046 15.6 20

Camphene < LOQ % < LOQ 20

beta Pinene 0.150 % 0.173 14.4 20

Ocimene 0.054 % 0.059 8.49 20

Sabinene < LOQ % < LOQ 20

Camphor < LOQ % < LOQ 20

Isoborneol < LOQ % < LOQ 20

Menthol < LOQ % < LOQ 20

alpha Cedrene < LOQ % < LOQ 20

Nerolidol < LOQ % 0.051 86.1 20

R-(+)-Pulegone < LOQ % < LOQ 20

Eucalyptol < LOQ % < LOQ 20




Page 15 of 18 07/02/2019 17:41


Lab Director



503-272-8830

www.sclabs.com

Quality Control

Terpene Analysis (Continued)




Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

p-Cymene < LOQ % < LOQ 20

(-)-Isopulegol < LOQ % < LOQ 20

Geranyl Acetate < LOQ % < LOQ 20

Guaiol < LOQ % < LOQ 20

Valencene < LOQ % < LOQ 20

Phytol 0.036 % 0.042 15.3 20

Citronellol < LOQ % < LOQ 20

gamma-Terpinene 0.021 % 0.022 5.35 20

Batch: B191143 - Water Activity



Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Water Activity 0.446 AW 0.451 1.16 20

Batch: B191144 - Gravimetric



Spike

Level

Source

Result %REC

%REC

Limits RPD

RPD

Limit

Percent Moisture 7.38 % 7.49 1.39 20




Page 16 of 18 07/02/2019 17:41


Lab Director

Client: Western Oregon Botanicals Client License: 02010021071d94 Date Sampled: 6/26/2019 Thermometer ID: T014

Address Where

Sampled:Requestor: Abdullah Naimi Event ID: 19F0121 Balance ID: SAMP_BAL_02

Sampler Signature

Sampling SOP & Rev.

#:SC-OR-SAMP-003 Sampler: Scott Forster Transporter: Scott Forster Hygrometer ID: Anemometer_02

Lab ORELAP ID: 4133 Weight used (g) Weight Set IDAcceptance

CriteriaInitial Measured Initial P/F Final Measured Final P/F

Lab OLCC ID: 1004748743D 0.5 SAMP_CAL_02 ±2.5% 0.5 0.5

200 ±2.5% 199.9 199.86

Container Type METRC Harvest/Processing Lot ID #: Product Type Client Sample Name Product Date Batch Size (g)

storage tubs 1A40103000098BF000001706 Usable Marijuana Pennywise 5/1/2019 1587.57

METRC Batch IDProduct Temp

(°C)Humidity (%) # of Containers Sampling Media # Zones # of Inc.

1° Sample Size

(g)Sample Name

22 59.8 2 mylar bag 4 7 1.5 Pennywise Primary

Container ID Increment ZoneSampling

Media Wt. (g)Wt. Inc+Media (g)

Increment

Weight (g)Sample METRC ID#

19D0121-01 Pennywise-1 A1 0 1.65 1.65 1732

19D0121-01 Pennywise-1 A4 1.65 3.2 1.55 1732

19D0121-01 Pennywise-2 B1 3.2 4.9 1.7 1732

19D0121-01 Pennywise-2 B1 4.9 5.75 0.85 1732

19D0121-01 Pennywise-2 B2 5.75 7.13 1.38 1732

19D0121-01 Pennywise-2 B3 7.13 9.35 2.22 1732

19D0121-01 Pennywise-2 B4 9.35 10.93 1.58 1732

Totals:Minimum Sample Size = 9.1g (Usable

Marijuana Only)7 Total Sample Mass = 10.93

Batch # Equipment Cont. Types/Sizes Uniform Plant Colors Shape and Size Sampling Plan ID & Rev. Date

Observations and Abnormalities:

.

Container Type METRC Harvest/Processing Lot ID #: Product Type Client Sample Name Product Date Batch Size (g)

storage tubs 1A40103000098BF000001705 Usable Marijuana Sirius Black 5/1/2019 772.3

METRC Batch IDProduct Temp

(°C)Humidity (%) # of Containers Sampling Media # Zones # of Inc.

1° Sample Size

(g)Sample Name

21.7 59.8 1 mylar bag 4 7 1 Sirius Black Primary

Container ID Increment ZoneSampling

Media Wt. (g)Wt. Inc+Media (g)

Increment

Weight (g)Sample METRC ID#

19D0121-02 Sirius Black-1 A1 0 1.93 1.93 1733

19D0121-02 Sirius Black-1 A1 1.93 2.83 0.9 1733

19D0121-02 Sirius Black-1 A2 2.83 3.65 0.82 1733

19D0121-02 Sirius Black-1 A2 3.65 4.38 0.73 1733

19D0121-02 Sirius Black-1 A3 4.38 6.18 1.8 1733

19D0121-02 Sirius Black-1 A3 6.18 7.39 1.21 1733

19D0121-02 Sirius Black-1 A4 7.39 9.63 2.24 1733

Lab Sample ID

Lab Sample ID

P P

18270 SW Benton Rd Sherwood OR

Sampling Report Page 1 of 2

Form Page 1 of 1SC-OR-SAMP-010, Rev. 1.00

Issued by DoQA of 07/05/2018

Totals:Minimum Sample Size = 7g (Usable

Marijuana Only)7 Total Sample Mass = 9.63

Batch # Equipment Cont. Types/Sizes Uniform Plant Colors Shape and Size Sampling Plan ID & Rev. Date

Observations and Abnormalities:

.

Sampling Report Page 2 of 2

Form Page 1 of 1SC-OR-SAMP-010, Rev. 1.00

Issued by DoQA of 07/05/2018

Sample Name: Sirius Black Tested for: Western Oregon … Testing/REC... · 2020. 12. 11. · Sample...

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