RE: ENCLOSED REPORTS FOR SAMPLE NO'S F0536 & F0564 - …Report careoFor y 5 Environmental Protection...
Transcript of RE: ENCLOSED REPORTS FOR SAMPLE NO'S F0536 & F0564 - …Report careoFor y 5 Environmental Protection...
ReportcareoFor y 5 Environmental Protection Agency
First International Building1201 Elm StreetDallas, TX 75270Attention: Charles Gazda
o^ugust3l|IiPl!!M^^
^P 9 198f ?•-
^AD/V/SJON |*
P.O.NO. 68-01-6035 Job No. 21881/jig
"oron of Samoles
Enclosed are the reports for sample numbers: F0536, and F0564-F5071,Case number: 580. Chain of Custody was not received.
0t^ir\
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••ouic aoG''ecia;e a teleofwie call it you "aw any questions regarding this report. Page 1 of 1 sages.
-. —a; "••s '6001 :'Lily retresents the <inoi''gs of work oerforrreo by me.-'"-•. J 'K'. suDer«isro". _" _ :_ ^ ^
Re/'eweo ana ADorovefl
/ / //.A^.^'...—--Robert Swaim, Ph. D.Staff Chemist
D. J . Northington, Ph. D.Technical Director
'•••s reoort ce'la'ns only 10 t^e samples in^esttgateo ana does not necessarily apply lo other apoarently identical or similar matenals. This report is SiJpmineo tor tnc exclusive Jse o* we ci-eni to -Anom it .s aooressea-py reDroouclion of tnis reDon or use of this LaDO'aiory s name tor aavertising or puolicity purposes without written authonution is pronioited
Ecology and Environment, Inc.
Region VI
MEMORANDUM
TO: Charles Gazda,Chief Compliance Section
FROM: David Anderson, FIT ^ a.E&E Region VI
THRU: K. Malone, FITL ^^E&E Region VI
DATE: September 15 , 1981 ^ ^
RE: TDD F-6-8109-20, Review of Sample Data from Vertac lr\
0Attached is a review of and quantification of 8 well water samples collected by 0the state at Vertac. Only one anomaly appeared in the results, that being thepresence of acetone in 6 of the 8 samples. Acetone has not been present inprevious samples and its presence is probably due to improper preparation ofsample containers or contamination by the analytical lab.
Sources
Standards:EPA Water Quality Criteria DocumentsNovember 28, 1980
Toxici t ies:
- ,v. ^; ^
Registery of Toxic Effects1979 Editiony^fc <(. I F
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\\\i{^.\''o ao<w\
*<-/\i/^r(?c<./^:^
O^IO^dlV / Av"»-tJ''t»J
07105934
ORGANICS TRAFFIC REPORTT) Case Number:
s^o
Sample Site Name/Code:/grtfK Jhc
T) Regional Office:•ximpling Personnel:
.J AD^e.(Name)
•?/ ^•7t-nol(Phone)
ximplingDcrte:
• - 'J -^ -^ / ..S^4*
(Begin) (End)
^) Shipping Information
:x,/Name of Shipper:
-—' " --- <~ ;. - -,?^ - .y/Date Shipped:
Airbill Number:
© Sample Type: (Check One)
___ RunOff
- . WeB
Receiving Water
Leachate
Effluent
Other (specify)
(j) Ship To:
We^ C^^^ Tcth se
\^(y05 P^h^aa^y
Ce^.h^ C.l^
Attn:
^) Description of Sample Location:
H/ / ^/
^) Special Handling Instructions:(e.g., safety precautions, hazardous nature)
; y • •' -, ,./^ /,f/ yREGIONAL OFFICE FILE COPY
Kiffigti
SAMF
LAB
DAT!
DATE
STD
CONC
Acid
21A
22A
24A
31A
34A
57A
58A
59A
60A
64A
65A
Base
1B
5B
8B
9B
12B
l8B
20B
25B
26B
27B
28B
35B
36B
37B
39B
40B
D W€5T COAST T€Ch^
*LE ID F0536
ID 21881A13
; EXTRACTED7/31/81
; INJECTED 8/17/81
ID SENS178 PHEN3E
: FACTOR 1000
Compounds
2, 4, 6-trlchlorophenol
p-chloro-m-cresol
2-chlorophenol
2, 4-dichlorophenol
2,4-dimethylphenol
2-nitrophenol
4-nitrophenol
2,4-dinitrophenol
4,6-dinitro-o-cresol
pentachlorophenol
phenol
/Neutral Compounds
acenaphthene
benzidine
1,2,4-trichlorobenzene
hexachlorobenzene
hexachloroethane
bis(2-chloroethyl)ether
2-chloronapthalene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
3,3'-dichlorobenzidine
2,4-dinitrotoluene
2,6-dinitrotoluene
1,2-diphenylhydrazine
(as azobenzene)
f luoran thene
4-chlorophenyl phenyl
IICALS6RVH
i5
ug/1
NO
NO
NO
ND
ND
ND*
NO
NO*
117
ND
ND
ND
ND
ND
ND
ND
N D
ND
ND
N D
ND
ND
NDN D
e t h e r N D
:6 INC.
SAMP:
LAB ]
DATE
DATE
STD I
CONC
Base/
41B
42B
43B
52B
53B
54B
55B
56B
61B
62B
63 B
66 B
67B68B
69B
70B
71B
72B
73 B
74B
75B
76B
77B
78B
79B
80B
81B
82B
83B
84B
129B
p-dio0710£S36^ ^
INDUSTRIAL CATEGORY
LE ID F0536
^ D ?1RS1R?
EXTRACTED 7 / ^ 1 / R l
INJECTED s/T^/81
D RFN73q7 R N ^ T n A I A
FACTOR mno
'Neutral Compounds ui
4-bromophenyl phenyl ether
bis(2-chloroisopropyl) ether
bis (2-chloroethoxy) methane
hexachlorobutadiene
hexachlorocyclopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodi methyl a mine
N-nitrosodiphenylamine
N-nitrosodi-n-propylamine
bis (2-ethylhexyl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
di-n-octyl phthalate
diethyl phthalate
dimethyl phthalate
benzo(a) anthracene
benzo(a)pyrene
3,4-benzofluoranthene
b e n z o ( k ) f luoranthene
chrysene
acenaphthylene
anthracene
benzo(ghl )pery lene
fluorene
phenanthrene
d i b e n z o ( a , h ) a n t h r a c e n e
indeno( 1 ,2 ,3-cd)pyrene
pyrene
2,3,7,8-tetrachlorodibenzo-
xin fi^lO^M^ri
^1N D
ND
ND
ND
N D
ND ^>
N D ^u\
ND
N D <-)
ND 0
ND
ND
ND*
ND*
N D
ND
ND
ND
N D
ND
N D
N D
N D
N n
N D
N D
M D
N D
ND
SAMP
LAB
DATE
STD :
CONC
Volat
2V
3V
4V
6V
7V
10V
11V
13V
uv15V
l6V
>imxxm^m)(»)^x^xx^Mixxxxxxxxxxx19V
23V
29V
30V
32V
33V
38V
44V
45V
46V
47V
48V
49V
50V
51V
85V
86V
87V
88V
^ WCS 1 UJAST T6CHNICAL
LE ID F0536
ID 21881V2
INJECTED 8/5/81
ID BFB35 VOA156 DATE INJECTED 8/6/81f A f~"Tt~\T> -
lies
acrolein
acrylonltrile
benzene
carbon tetrachloride
chlorobenzene
1,2-dichloroethane
1,1,1-trichloroethane
1,1-dichloroethane
1,1,2-trichloroethane
1,1,2,2-tetrachloroethane
chloroethane
2-chloroethylvinyl ether
chloroform
1,1-dichloroethylene
1,2-trans-dichloroethylene
1,2-dichloropropane
1,3-dichloropropylene
ethylbenzene
methylene chloride
methyl chloride
methyl bromide
bromoform
dichlorobromomethane
trie hlorofluorome thane
dichlorodif luoromethane
chlorodibromo methane
tetrachloroethylene
toluene
trichloroethylene
vinyl chloride
S6RVICG
LAB ID TRACE N141
DATE EXTRACTED 7/31/81
ug/1
ND
ND
N O
ND
N D
ND
ND
N D
N D
N D
ND
ND
13
ND
ND
ND
N D
N D
19
ND
ND
ND
N D
ND
ND
N D*
N D
N D
N D
INC INnii^TRlAi i ^i.-^ORY
SAMPLE ID F0536
STD ID TRACE #4140
CONC. FACTOR 50
Pesticides
89P aldrin
90P dieldrin
91P chlordane
92P 4 ,4 ' -DDT
93P 4 , 4 ' - D D E
94P 4 , 4 ' - D D D
95P alpha-endosulfan
96P beta-endosulfan
97P endosulfan sulfate
98P endrin
99P endrin aldehyde
100P heptachlor
101P heptachlor epoxide
102P alpha-BHC
103P beta-BHC
104P gamma-BHC
105P delta-BHC
106P PCB-1242
107P PCB-1254
108P PCB-1221
109P PCB-1232
HOP PCB-1248
HIP PCB-1260
112P PCB-1016
113P toxaphene
••'•• = Less than 10 ug/1
(pesticides less than 5 ug/1)
ND = Not detected
-;,--„- ^ ^o^ confirmed by GCMS
GW
ug/1
ND
. ND
ND
ND
ND
^ ND
^ ND-tf<———
N D
0 ND
0 N D
N D
N D
N D
ND
ND
ND
ND
N D
N D
ND
ND
ND
N D
N D
N D
^4f7
17605 Fabnca Way Suite 0 Cerntos. Cali fornia 90701 2 1 3 / 9 2 1 - 9 8 3 1
WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3
QC Report No: 36Sample Number
F0536
A. SURROGATE SPIKE RESULTS
COMPOUND
Benzene - d6
l-Chloro-2-Bromopropane
Toluene - d8
2-Fluorophenol
Phenol - d5
Nitrobenzene - d5
2-Fluorobiphenyl
Naphthalene-DS
Fraction
VGA
VOA
VGA
ACID
ACID
B/N
B/N
B/N
Cone.(ug/1)
49
46
48
72
92
69
75
74
(Surrogates only)Spike
Added (uq /1)
50
50
50
100
103
1 0 1
1 0 1
101
%Recovery
98
92
96
72
89
68——————66
74 ^
73 IT
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
1 1 .
12.
13.
14.
15.
16.
17 .
18.
19.
20.
CAS # COMPOUND NAME FRACTION
% Maximum Score Attained 0
Mass Matching Routine: FIT(specify)
'
————————(m0^938——
^}tml'2t-styrV/ « J* V tff^J^i ^
•' -7
-r-.T- ~^hrif,i w-iv Suita D Cerritos California 90701 ?11 •n^i ^ " 1 1
ORGANICS TRAFFIC REPORT(l) Case Number:
£so
Sample Site Name/Code:
Vfyt^t, J^C ,
© Sample Type: (Check One)
___ RunOff
-X WeH
Receiving Water
Leachate
Effluent
Ofher (specify)
(j) Shy To:
Wcsl- C^sf 7 ' se\<'f7k06 /^/<^
Ce^^f^^ ^^^^^D7P/
Attn:
'^i^^*\ P^^^e^
(^Regional Office:
Sampling Perscnnel:
t^^ M^.^.fftwY)
(^) Mark Volume Level on Sample Bottle
(Name)
.fD/ -^f-no^ Extractable
(Phone)
Sampling Date:
7-J^-^/
Extractable
(Begin) (End)Extractable
(6) Shipping Information Extractable
J^y J^JT// KTi^-mo .^^nr~\rv=i
^y ^JT/i<Zi KTi -mo i f . n r~\rv=ir'
VOA Unpreserved7
/ Name of Shipper:
-7- 3 o " gyVOA Unpreserved(Duplicate)
Date Shipped:
Airbill Number:
DateSampled
7-2 7- /
(7) Description of Sample Location:
Welf ^ ^
(s) Spedai Handling Instructions:(e.g., safety precautions, hazardous nature)
, /^^..i>i (-'-< •''fi'
REGIONAL OFFICE FILE COPY
W€5T COAST TECHNICAL S6RVICG INC. INDUSTRIAL CATEGORY
SAMP
LAB •
DATE
DATE
STD 1
CONC
Acid
21A
22A
2^A
31A
34A
57A
58A
59A
60A
6^A
65A
Base/
1B
5B
8B
9B
12B
18B
20B
25B
26B
27B
28B
35B
36B
37B
39B
^OB
LE ID F0564
[D 21881A2
EXTRACTED 8/1/81
INJECTED 8/9/81
'.'D SENS176 PHEN353
FACTOR 1000
Compounds u
2, L., 6-trichlorophenol
p-chloro-m-cresol
2-chlorophenol
2,4-dichlorophenol
2,4-dimethylphenol
2-nitrophenol
^-nitrophenol
2,4-dinitrophenol
U,6-dinitro-o-cresol
pentachlorophenol
phenol
'Neutral Compounds
acenaphthene
benzidine
1,2,^-trichlorobenzene
hexachlorobenzene
hexachloroethane
bis(2-chloroethyl)ether
2-chloronapthalene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
3,3'-dichlorobenzidine
2,^-dinitrotoluene
2,6-dinitrotoluene
1,2-diphenylhydrazine
(as azobenzene)
f luoranthene
^-chlorophenyl phenyl ether
g/1*
ND
ND
14
ND
ND
ND
ND
ND
ND*
ND
ND
N D
ND
ND
ND
ND
ND
N D
ND
N D
ND
N D
NnN D
ND
SAMP
LAB
DATE
DATE
STD
CONC
Base,
41B
^2B
A3B
52B
53B54B
55B
56B
61B
62 B
63 B
66B
67B
68B
69 B
70B
71B
72B
73B
7AB
75B
76B
77B
78B
79 B
SOB
81B
82B
83B
8^B
129B
p-dic
LE ID F0564
ID 21881B3
. EXTRACTED 7/31/81
INJECTED 8/13/81
ID BENZ397 BNSTD414
FACTOR 1000
/Neutral Compounds us
4-bromophenyl phenyl ether
bis(2-chloroisopropyl) ether
bis (2-chloroethoxy) methane
hexachlorobutadiene
hexachlorocyclopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodimethylamine
N-nitrosodiphenylamine
N-nitrosodi-n-propylamine
bis (2-ethylhexyl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
di-n-octyl phthalate
diethyl phthalate
dimethyl phthalate
benzo(a) anthracene
benzo(a)pyrene
3,4-benzofluoranthene
benzo(k ) f luoran thene
chrysene
acenaphthylene
anthracene
benzo(gh i )pe ry lene
fluorenephenanthrene
d ibenzo (a ,h ) an th racene
indeno( 1 ,2 ,3-cd)pyrene
pvrene
2,3,7,8-tetrachlorodibenzo- l J ' J
(mo is
1ND
ND
ND
ND
N D 0
N D ^——tf\ND
ND 0
N D O
ND
ND
11
ND*
ND*
ND
ND
ND
ND
N D
N D
N D
N D
N D
N D
N n
N nwnN D.05940
'ND
^-^.-^ WCSl t-uAST TECHNICAL
SAMPLE ID F0564
LAB ID 21881V3
DATE INJECTED 8/5/81
STD ID BFB35 VOA156
CONC. FACTOR ———-
Volatiles
2V acrolein
3V acrylonltrlle
4V benzene
6V carbon tetrachloride
7V chlorobenzene
10V 1,2-dichloroethane
11V 1,1,1-trlchloroethane
13V 1,1-dlchloroethane
14V 1,1,2-trichloroethane
15V 1,1,2,2-tetrachloroethane
l6V chloroethane
)imXXmmm»)^}WXMl»MiXXXXXXXXXXX
19V 2-chloroethylvinyl ether
23V chloroform
29V 1,1-dichloroethylene
30V 1,2-trans-dichloroethylene
32V 1,2-dichloropropane
33V 1,3-dichloropropylene
38V ethylbenzene
44V methylene chloride
45V methyl chloride
46V methyl bromide
47V bromoform
48V dichlorobromomethane
49V tr ichlorofluoromethane
50V dichlorodif luoromethane
51V chlorodibromomethane
S5V te t rachloroethvlene
SoV toluene
S7V tr ichloroethvlene
SSV vinvl chloride
17605 FaDnca Way Sui te D Cern'o
SfctWii-c
LAB ID TRACE N144
ug/1
ND
NO
N D
NO
ND
NO
N D
N D
N D
N D
ND
ND*
ND
ND
ND
ND
N D
20
N D
ND
N D
N D
ND
ND
N D
10
N D
W
N D
INC. INLJU^ 1 Mi/-..- v-^< ^uOKY
SAMPLE ID F0564
DATE EXTRACTED 7/31/81
DATE I N J E C T E D 8/6/81
STD ID TRACE N143
CONC. FACTOR 50
Pesticides
89P aldrin
90P dieldrin
91P chlordane
92P 4 ,4 ' -DDT
93P 4 ,4 ' -DDE
94P 4 , 4 ' - D D D
95P alpha-endosulfan
96P beta-endosulfan
97P endosulfan sulfate
98P endrin
99P endrin aldehyde
100P heptachlor
101P heptachlor epoxide
102P alpha-BI-IC
103P beta-BHC
104P gamma-BHC
105P delta-BHC
106P PCB-1242
107P PCB-1254
108P PCB-1221
109P PCB-1232
HOP PCB-1248
H I P PCB-1260
112P PCB-1016
113P toxaphene
••'•" = Less than 10 ug/1
(pest icides less than 5 ug/1)
ND = Not detected
••'•-* = Not confirmed by GCMS
0!2-1-
s. C a l i f o r n i a 90701 213/921-9831 O^'l
Ug/1
0.1**
2.5**
ND
1.6**
NDr-
ND^
O.I1**
^0ND-,
0.1**
1.0**
N D
ND
0.6**
1.5**
1.8**
0.7**
N D
N D
N D
ND
ND
N D
ND
N D
e^5bo
,05941
WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3
QC Report No :_ 36Sample Number
F0564
A. SURROGATE SPIKE RESULTS•
COMPOUND
Benzene - d6
l-Chloro-2-Bromopropa.ne
Toluene - d8
2-Fluorophenol
Phenol - d5
Nitrobenzene - d5
2-Fluorobiphenyl
Naphthalene-DS
Fraction
VOA
VOA
VOA
ACID
ACID
B/N
B/N
B/N
C o n e . ( u g / 1 )
49
45
47
84
103
52
64
59
(Surrogates only)Spike
Added (ug /1 )
50
50
50
100
103
1 0 1
1 0 1
1 0 1
%Recovery
98
90
94
84
100
51
63
58
B . TENTATIVELY IDENTIFIED COMPOUNDS
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
1 1 .
12.
13.
14.
15.
16.
17 .
18.
iq
20.
CAS ft COMPOUND NAME
ACETONE
.
FRACTION
VOA #85
% Maximum Score Attained
Mass Matching Routine: FIT(specify)
882
•
•
(VW^5C^
- ... - n 'i n.s
c
^
^{\'7
ORGANICS TRAFFIC REPORT(T) Case Number:
^0
Sample Site Name/Code:
'/f/t^^ .T^L
©D Sample Type: (Check One)
Run Off
/^Well
——— Ffeoeiving Water
Leachate
Effluent
Ofher (specify)
(J) Ship To:
^J-A C^J-^ Tc^.J^17^W F^bf'.'c^ ^y
Ce^'/^ ^/'
^070fAttn:
A;') c'<-,
(?) Regional Office:Sampling Personnel:
^^J /kIL^W
(^) Mark Volume Level on Sample Bottle
(Name)
;^/ ?-?/-/7^ /Extractable
(Phone)
ScimplingDate:
2,1^-JU-
Extractable
(Begin) (End)Extractable
(^) Shipping Information
T TT-/'J{., , J^ .f t.' (.
Extractable
VOA Unpreserved
Name of Shipper:VOA Unpreserved(Duplicate)
Date Shipped:
.., •— '-•"* •--- ""»-/ 5 .:> ..-) / 3Airbill Number:
(7) Description of Sample Location:
(J) Special Ifandling Instructions:(e.g., safety precautions, hazardous nature)
REGIONAL OFFICE FILE COPY
Q iozsga07105943
WSfSsSs
SAMP
LAB
DATE
DATE
STD •
CONC
Acid
21A
22A
24A
31A
34A
57A
58A
59A
60A
64A
65A
Base/
1B
5B
8B
9B
12B
18B
20B
25 B
26B
27B
28B
35B
36B
37B
39B
40B
-0 WEST COAST TECHNICAL
LE ID F0565
ID 21881A5EXTRACTED s/ i /gi
INJECTED 8/9/81
ID SENS176 PHEN353
FACTOR 1000
Compounds u
2,4,6-trichlorophenol
p-chloro-m-cresol
2-chlorophenol
2,4-dichlorophenol
2,4-dimethylphenol
2-nitrophenol
4-nitrophenol
2,4-dinitrophenol
4,6-dinitro-o-cresol
pentachlorophenol
phenol
Neutral Compounds
acenaphthene
benzidine
1,2,4-trichlorobenzene
hexachlorobenzene
hexachloroethane
bis(2-chloroethyl)ether
2-chloronapthalene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
3,3'-dichlorobenzidine
2,4-dinitrotoluene
2,6-dinitrotoluene
1,2-diphenylhydrazine
(as azobenzene)
fluoranthene
4-chlorophenvl phenyl ether
5€RV
g/1
ND
NDNONDNDNDND
NDNnNnNn
ND
NO
ND
ND
ND
NDNDNDNDNDND
ND
ND
NnND
ND
IC6 INC.
SAMP
LAB
DATE
DATE
STD ;
CONC
Base/Neutral Compounds u^
41B
42B
43 B
52B
53B
54B
55B
56B
61B
62B
63B
66B
67B
68B
69B
70B
71B
72B
73B
74B
75B
76B
77B
78B
79B
80B
81B
82B
83B
84B
129B
p-dic
INDUSTRIAL CATEGORY
LE ID F0565
ID 21881B6
EXTRACTED 7/31/81
INJECTED 8/13/81
[D BENZ397 BNSTD414
FACTOR 1000
4-bromophenyl phenyl ether
bis(2-chloroisopropyl) ether
bis (2-chloroethoxy) methane
hexachlorobutadiene
hexachlorocyclopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodimethylamine
N-nitrosodiphenylamine
N-nitrosodi-n-propylamine
bis (2-ethylhexyl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
dl-n-octyl phthalate
diethyl phthalate
dimethyl phthalate
benzo(a) anthracene
benzo(a)pyrene
3,4-benzofluoranthene
benzo(k)f luoranthene
chrysene
acenaphthylene
anthracene
benzo(ghi)perylene
fluorene
phenanthrene
d ibenzo(a ,h )an th racene
indeno (1 ,2 ,3-cd) pyrePe^t0^^pvrene '--••€-
2,3,7,8-tetrachlorodibenzo-^ 07105944
^1ND
ND
ND
ND
N^.NilnND-
N[P
ND^
ND
ND10
ND*
ND-*
ND
ND
ND
NDN DN DNDNONDND
NnNn
ND
ND
I^L/il/.v^C
SAMP
LAB
DATE
STD •
CONC
Volat
2V
3V
4V
6V
7V
10V
11V
13V
14V
15V
l6V
)W^xx)&xxxxM^»)«©t»)^xx^eti(8&xxxxxxxxxn19V
23V
29V
30V
32V
33V
38V
44V
45V
46V
47V
48V
49V
50V
51V
85V
86V
87V
88V
^ W6ST COAST TECHNICAL
LE ID F0565
ID 21881V4
INJECTED 8/5/81
ID BFB35 VOA15617 A ^TOD
lies
acrolein
acrylonitrile
benzene
carbon tetrachloride
chlorobenzene
1,2-dichloroethane
1.1,1-trichloroethane
1,1-dichloroethane
1,1,2-trichloroethane
1.1,2,2-tetrachloroethane
chloroethane
2-chloroethylvinyl ether
chloroform
1,1-dichloroethylene
1,2-trans-dichloroethylene
1,2-dichloropropane
1,3-dichloropropylene
ethylbenzene
methylene chloride
methyl chloride
methyl bromide
bromoform
dichlorobromomethane
trichlorofluoromethane
dichlorodifluoromethane
chlorodibromo methane
tetrachloroethvlene
toluene
trichloroethylene
vinyl chloride
.S6RVK
ug/1
ND
NO
ND
N D .
ND
ND
ND
ND
ND
N D
ND
ND
ND
ND
ND
ND
N D
ND
20
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
:e INC.
SAMP
LAB
DATE
DATE
STD •
CONC
Pesti
89P
90P
91P92P
93P
94P
95P
96P
97P98P
99P
100P
101P
102P
103P
104P
105P
106P
107P
108P
109P
HOP
HIP
112P
113P
* = I
(p<=
ND =* * ^
INDUSTRIAL LATGGORY
LE ID F0565
ID TRACE Ml 52
EXTRACTED 7/31/81
INJECTED 8/7/81
ID TRACE Ml 51
. FACTOR 50
cides
aldrin
dieldrin
chlordane
4,4'-DDT
4.4 '-DDE
4.4'-DDD
alpha-endosulfan
beta-endosulfan
endosulfan sulfate
endrin
endrin aldehyde
heptachlor
heptachlor epoxide
alpha-BHC
beta-BHC
gamma-BHC
delta-BHC
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
toxaphene
-ess than 10 ug/I
•sticides less than 5 ug/1)
Not detected
Not confirmed by GCMSO^H^
ug/1
ND
. ND
ND
ND
'yt)———a-'i-ifiW
W
^
'ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
N D
ND
ND
ND
NO
ND
ND
£'554
0710594517605 Fabnca Way, Suite D Cerntos. California 90701 213/921-9831
WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3
QC Report No: 36Sample Number
F0565
A. SURROGATE SPIKE RESULTS
COMPOUND
Benzene - d6
l-Chloro-2-Bromopropane
Toluene - d8
2-Fluorophenol
Phenol - d5Nitrobenzene - d52-FluorobiphenylNaphthalene-DS
Fraction
VOA
VOA
VOA
ACID
ACID
B/N
B/N
B/N
Cone . (uq /1 )
49
44
461
1586665
(Surrogates only)Spike
Added (ug/1)
RD
50
50100103101101101
%Recovery
wfiR
92
11 ^
57 ln
————HT-6564 0
B. TENTATIVELY IDENTIFIED COMPOUNDS
1.2.
3.4.
5.
6.
7.8.9.10.11.12.
13.
14.
15.16.
17.18.
19.
20.
CAS # COMPOUND NAME
ACETONE
FRACTION
VOA #65
% Maximum Score Attained
Mass Matching Routine: FIT(specify)
868
-
u'zJL^ri^5-
07105946
"''"" "^hrir-n w.iv. S i n t n 0 Cprritos. C n l i f o r n i n POTOI ?1'!/03 1-0331
ORGANICS TRAFFIC REPORT(J) Case Number:
^0
Sample Site Name/Code:j/ff^-f-ffL "7^ f
©
-X-
2) Sample Type: (Check One)
Run Off
Wen
Receiving Water
Leachate
Effluent
Other (specify)
@ Shy To:
l/\/es^ Co^5' T^^"*l^(s>05 ^/'^ ^v
Ce^h^ C^h^yo7o/
Attn:
/~i^ df< B^^^d
(^Regional Office:Sampling Peracrmel:
^^ A^fiy>/^
Q[) Mark Volume Level on Sample Botfle
(Name)
L-v 37/-/^/ Extractable
(Phone)
Sampling Date:
.. -•/- </- f/____So^f
Exiractable
(Begin) (End)Extractable
(D Shipping Information
VOA Unpreserved/ Name of Shipper:
?-7J -57
VOA Unpreserved(Duplicate)
Date Shipped:
Airbill Number:
(7) Description of Sample Location:
® Special Hanaling Instructions:(eg., safety precautions, hazardous nature)
REGIONAL OFFICE FILE COPY
WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
SAMP
LAB •
DATE
DATE
STD 1
CONC
Acid
21A
22A
24A
31A
34A
57A
58A
59A60A
64A
65A
Base/
1B
5B
8B
9B
12B
18B
20B
25 B
26B
27B
28B
35B
36B
37B
39B
40B
LE ID F0566
ID 21881A6
EXTRACTED 8/1/81
INJECTED 8/9/81
[D SENS176 PHEN353
FACTOR 1000
Compounds u'
2,4,6-trichlorophenol
p-chloro-m-cresol
2-chlorophenol
2,4-dichlorophenol
2,4-dimethylphenol
2-nitrophenol
4-nitrophenol
2,4-dinitrophenol
4.6-dinitro-o-cresol
pentachlorophenol
phenol
^Neutral Compounds
acenaphthene
benzidine
1,2,4-trichlorobenzene
hexachlorobenzene
hexachloroethane
bis(2-chloroethyl)ether
2-chloronapthalene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
3,3'-dichlorobenzidine
2,4-dinitrotoluene
2,6-dinitrotoluene
1,2-diphenylhydrazine
(as azobenzene)
fluoranthene
4-chlorophenyl phenyl ether
g/1
ND
NDNDNDNDNDND
ND
ND
NDND
ND
ND
ND
ND
ND
NDND
ND
NDNP
ND
ND
ND
NOND
ND
SAMP
LAB
DATE
DATE
STD
CONC
Base/Neutral Compounds u
41B
42B
43B
52B
53B
54B
55B
56B61B
62B
63B
66B
67B
68B
69B
70B
71B
72B
73 B
74B
75B
76B
77B
78B
79B
SOB
81B
82B
83 B
84B
129B
p-dicu /JlUJayo
LE ID F0566
ID 21881B7
EXTRACTED 7/31/81
INJECTED 8/13/81
ID BENZ397 BNSTD414
FACTOR 1000
4-bromophenyl phenyl ether
bis(2-chloroisopropyl) ether
bis (2-chloroethoxy) methane
hexachlorobutadiene
hexachlorocyclopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodimethylamine
N-nitrosodiphenylamine
N-nitrosodi-n-propylamine
bis (2-ethylhexyl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
di-n-octyl phthalate
diethyl phthalate
dimethyl phthalate
benzo(a) anthracene
benzo(a)pyrene
3,4-benzofluoranthene
benzo(k)f luoranthene
chrysene
acenaphthylene
anthracene
benzo(ghi)perylene
fluorene
phenanthrene
dibenzo(a ,h)an thracene
indeno( 1,2,3-cd)pyrene
pyrene OW^J^l
2,3,7,8-tetrachlorodibenzo-
g/1
ND
ND
ND
N00
NtP—tf^-
ND-
ND
NIP
ND
ND
ND
12
ND*
ND*
ND
ND
ND
ND
ND
NDNDNDN1)NDN DNnNn
L'.L^
rNQ
t^^
SAMP
LAB :
DATE
STD 1
CONC
Volat
2V
3V
4V
6V
7V
10V
11V
13V
14V
15V
l6V
)m%XX»XXXXKX«^)ti©t»)^DOX)^OtX^XXX
19V
23V
29V
30V
32V
33V
38V
44V
45V
46V
47V
48V
49V
50V
51V
85V
86V
87V
88V
^ WEST COAST TECHNICAL
LE ID R0566
ID 21881V9
INJECTED 8/5/81
[D BFB35 VOA156
. FACTOR ----—
lies
acrolein
acrylonitrile
benzene
carbon tetrachloride
chlorobenzene
1,2-dichloroethane
1,1,1-trichloroethane
1,1-dichloroethane
1,1,2-trichloroethane
1,1,2,2-tetrachloroethane
chloroethane
2-chloroethylvinyl ether
chloroform
1,1-dichloroethylene
1,2-trans-dichloroethylene
1,2-dichloropropane
1,3-dichloropropylene
ethylbenzene
methylene chloride
methyl chloride
methyl bromide
bromoform
dichlorobromo methane
trichlorofluoromethane
dichlorodifluoromethane
chlorodibromomethane
tetrachloroethylene
toluene
trichloroethylene
vinyl chloride
.S6RVK
ug/1
NO
ND
NO
ND
N D
ND
ND
N D
ND
N D
ND
ND
ND
ND
ND
ND
ND
ND18
ND
ND
ND
ND
ND
ND
ND
N D
NO
ND
ND
:6 INC.
SAMP
LAB
DATE
DATE
STD
CONC
Pesti
89P
90P
91P
92P
93P
94P
95P
96P
97P
98P
99P
100P
101P
102P
103P
104P
105P
106P
107P
108P
109P
HOP
HIP
112P
113P
* = I
( p <
ND =** ^
INDUSTRIAL CATEGORY
LE ID F0566
ID TRACE #4145
EXTRACTED 7/31/81
INJECTED 8/6/81
ID TRACE #4143
. FACTOR 100
cides
aldrin
dieldrin
chlordane
4,4 '-DDT
4,4 '-DDE
4,4 ' -DDD
alpha-endosulfan
beta-endosulfan
endosulfan sulfate
endrin
endrin aldehyde
heptachlor
heptachlor epoxide
alpha-BHC
beta-BHC
gamma-BHC
delta-BHC
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
toxaphene
-ess than 10 ug/1
'sticides less than 5 ug/1)
Not detected
Not confirmed by GCMS
w
ug/1
NO
. ND
ND
WNth
^
NiL
^ND
ND
N D
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
WS5
0710594917605 Fabnca Way. Suite D Cerntos. California 90701 213/921-9831
WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3
QC Report No:_ 36Sample Number
F0566
A. SURROGATE SPIKE RESULTS
COMPOUND
Benzene - d6
l-Chloro-2-Bromopropane
Toluene - d8
2-Fluorophenol
Phenol - d5
Nitrobenzene - d5
2-Fluorobiphenyi
Naph-thalene-DS
Fraction
VGA
VOA
VOA
ACID
ACID
B/N
B/N
B/N
C o n c . ( u g / 1 )
48&0.
48
0
0
49
59
57
(Surrogates on ly)Spike
Added ( u q / 1 )
w
w
50
100
103
101
101
101
%Recovery
qfi
as
96
0
0
48
58
56
B. TENTATIVELY IDENTIFIED COMPOUNDS
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
1 1 .
12 .
13.
14.
15.
16.
17.
18.
19.
20.
CAS # COMPOUND NAME
ACETONE
FRACTION
VOA #86
% Maximum Score Attained
Mass Matching Routine: FIT(specify)
868
•
O^l^rnc.flV/ rf AV» » » 9JAJ\J^
. [W. ^
ORGANICS TRAFFIC REPORT(7) Case Number:
c^
Sample Site Name/Code:
(/^"T^c J^
©
) Sample Type: (Check One)
— RunOff
WeD
Rsoeiving Water
Leachate
Effluent
Ofher (specify)
© Shy To:
^/fsf Co^r 'Tec^^ic^''
1^05 pt^^ ^yCen^o^ Ctl^
fc?^o/Attn:
©Regional Office:
Sampling Personnel:
^/wJ Ak^^fr
(j) Mark Volume Level on Sample Botfle
•(Name)
C / - 371- HDI(Phone)
Extractable
Sampling Date:
?- Uf^ ^f
Ebctractable
rJ>ai^f
(Begin) (End) Extractable
(D Shipping Information
"hy.., \ ) ' J < - f , ^
Extractable
VOA Unpreserved
/ Name of Shipper:VOA Unpreserved(Duplicate)
Date Shipped:
:A^i? 3 5'3'^'3Airbill Number
(7) Description of Sample Location:
Q[) Special Handling Instructions:(e.g., safety precautions, hazardous nature)
REGIONAL OfTICE FILE'COPY
O IOSSSI(yyiogseo ..
WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
SAMP
LAB
DAT!
DATE
STD
CONC
Acid
21A
22A
24A
31A
34A
57A
58A
59A60A
64A
65A
Base
1B
5B
8B
9B
12B
18B
20B
25B
26B
27B
28B
35B
36B
37B
39B
40B
'LE ID F0567
ID 21881
; EXTRACTED 8/1/8
; INJECTED 8/9/8
ID SENS176
; FACTOR 1000
Compounds
2,4,6-trichlorophenol
p-chloro-m-cresol
2-chlorophenol
2,4-dichlorophenol
2,4-dimethylphenol
2-nitrophenol
4-nitrophenol
2,4-dinitrophenol
U,6-dinitro-o-cresol
pentachlorophenol
phenol
/Neutral Compounds
acenaphthene
benzidine
1,2,4-trichlorobenzene
hexachlorobenzene
hexachloroethane
bis(2-chloroethyl)ether
2-chloronapthalene
1,2-dichlorobenzene
1,3-dichlorobenzene
1, -dichlorobenzene
3,3'-dichlorobenzidine
2, A-dinitrotoluene
2,6-dinitrotoluene
1,2-diphenylhydrazine
(as azobenzene)
fluoranthene
4-chlorophenyl phenyl
A7
1
.1
PHEN353
ug/1
'TIS
NO
154
153
ND
ND
ND
NnNn
NnNn
ND
ND*
NDND
NDND
ND
ND
ND
ND
NnNH
NnND
e t h e r N D
•.- r\
SAMP I
LAB I
DATE
DATE
STD ID BENZ398 ;BNSTD415
CONC
Base/Neutral Compounds Uj
41B
42B
43B
52B
53B
54B
55B
56B
61B
62 B
63B
66B
67B
68B
69B
70B
71B
72B
73B
7^B
75B
76B
77B
78B
79B
80B
81B
82B
83B
84B
129B
p-dio:
^ .1 ( - .
-E ID F0567
D 21881B8
EXTRACTED 7/31/81
INJECTED 8/13/81
FACTOR 1000
4-bromophenyl phenyl ether
bis(2-chloroisopropyl) ether
bis (2-chloroethoxy) methane
hexachlorobutadiene
hexachlorocyclopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodimethylamine
N-nitrosodiphenylamine
N-nitrosodi-n-propylamine
bis (2-ethylhexyl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
di-n-octyl phthalate
diethyl phthalate
dimethyl phthalate
benzo(a) anthracene
benzo(a)pyrene
3,4-benzofluoranthene
benzo(k) fluoranthene
chrysene
acenaphthylene
anthracene
benzo(ghi)perylene
fluorene
phenanthrene
dibenzo(a ,h)anthracene
indeno( l ,2 ,3-cd)pyrene
pyrene
2,3,7,8-tetrachlorodibenzo-
<in 07105952-. - r.r'-^- -'-n •0'7i QP^ i
g/1
ND
ND
ND
ND
N D ,——c-<t
NDsONDn
NCT"
ND0
—©-ND
ND
29
NDND
NO
ND
ND
ND
ND
ND
ND
ND
ND
NP
ND
NnNnND c
^
Nn SN D ^
ND'^1
fe^<5toa WEST COAST TECHNICAL
SAMPLE ID F0567
LAB ID 21881V10
DATE INJECTED 8/5/81
STD ID BFB35 VOA156
v^UIN^. rA^HJK
Volatiles
2V acrolein
3V acrylonitrile
4V benzene
6V carbon tetrachloride
7V chlorobenzene
10V 1,2-dichloroethane
11V 1,1,1-trichloroethane
13V 1,1-dichloroethane
14V 1,1,2-trichloroethane
15V 1,1,2,2-tetrachloroethane
l6V chloroethane
)imxxmxxm^»m^x%i(eti4^xxxxxxxxxx19V 2-chloroethylvinyl ether
23V chloroform
29V 1,1-dichloroethylene
30V 1,2-trans-dichloroethylene
32V 1,2-dichloropropane
33V 1,3-dichloropropylene
38V ethylbenzene
44V methylene chloride
45V methyl chloride
46V methyl bromide
47V bromoform
48V dichlorobromomethane
49V trichlorofluoromethane
50V dichlorodifluoromethane
51V chlorodibromomethane
85V tetrachloroethylene
86V toluene
87V trichloroethylene
88V vinyl chloride
SERVICE
LAB ID TRACE N146
DATE EXTRACTED 7/31/81
DATE INJECTED 8/6/81
ug/1
ND
NO
NO
ND
ND
ND
ND
ND
ND
N D
ND
ND
ND
ND
ND
ND
ND
ND
20ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
INC INDUSTRIAL FATPGQRY
SAMPLE ID F0567
STD ID TRACE N143
CONC. FACTOR 100
Pesticides
89P aldrin
90P dieldrin
91P chlordane
92P 4.4'-DDT
93P 4.4'-DDE
94P 4.4'-DDD
95P alpha-endosulfan
96P beta-endosulfan
97P endosulfan sulfate
98P endrin
99P endrin aldehyde
100P heptachlor
101P heptachlor epoxide
102P alpha-BHC
103P beta-BHC
104P gamma-BHC
105P delta-BHC
106P PCB-1242
107P PCB-1254
108P PCB-1221
109P PCB-1232
HOP PCB-1248
HIP PCB-1260
112P PCB-1016
113P toxaphene
* = Less than 10 ug/1
(pesticides less than 5 ug/1)
ND = Not detected
** = Not confirmed by GCMS
-^
ug/1
ND
. ND
ND
ND
NOt
Nfi»
^
WMS)ND
ND
ND
ND
ND
ND
ND
ND
ND
N D
ND
ND
ND
ND
ND
N D
^
17605 Fabrica Way, Suite D Cerritos. California 90701 213/921-9831 07105953
W65T COAST T€CHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3
QC Report No: 36Sample Number
F0567
A. SURROGATE SPIKE RESULTS
COMPOUND
Benzene - d6
l-Chloro-2-Bromopropane
Toluene - d8
2-Fluorophenol
Phenol - d5
Nitrobenzene - d5
2-Fluorobiphenyi
Naphthalene-DS
Fraction
VOA
VOA
VOA
ACID
ACID
B/N
B/N
B/N
Conc.(uq/1)
44
43
46
40
2
60
68
60
(Surroqates only)Spike
Added (uq/1)
50
50
50
100
103
101
101
101
%Recovery
88
86
92
40
2 ^
59 ,n
67 in59 ^~
B . TENTATIVELY IDENTIFIED COMPOUNDS 0
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11 .
12.
13.
14.
15.
16.
17.
18.
19.
20.
CAS # COMPOUND NAME
ACETONE
TETRAHYDROFURAN
DICHLOROPHENOL
CHLOROPHENOL
2,4,5-TRICHLOROPHENOL
DICHLOROPHENOL
UNKNOWN
UNKNOWN
2-ETHYL-1-HEXANOL
TRICHLOROMETHOXYBENZEN
UNKNOWN
UNKNOWN
FRACTION
VOA #86
VOA #130
ACID #146
ACID # 1 9 6
ACID #207
ACID #264
ACID #492
ACID #515
B/N #142
: B/N #296
B/N #324
B/N #330
% Maximum Score Attained
Mass Matching Routine: FIT(specify)
835
993
GENERAL FIT
GENERAL FIT
966
GENERAL FIT
NO GOOD FIT
NOlCOOD FIT
942
GENERAL FIT
NO'SOOD FIT
NO GOOD FIT
OyiO ifia-^^
———————————————r^i-l nr.Qg^-rnr, r.,],r'^-i W-iy ^ in ton forritrT; (''-llif"rnin Qn7D1 71'l n "'I-n'T'I
ORGANICS TRAFFIC REPORT
Sample Site Name/Code:{/y^jn.c. ^ (-
Oc: <. ts^^f ( ( f , f7^
®2) Sample Type: (Check One)
RunQff
WeU
Rsceiving WatBr
Leachate
Effluent--
Other (specify)
© Ship To: ,
W<?^ Co^sf Tec^h'.^/ s>
/^(pOS P^b^c^ ^yCcr^^^J CA//^
9070/Attn:
A i c- i 0^i C- 1 fcM ^ €^
Q Regional Office:Sampling Personnel:
(j) Mark Volume Level on Sample Bottle
/.. /MD^.ft^)/TiT_____ \ \ /(Name)
. / - /-no/ Extractable
(Phone)
Sampling Date:
;^.^-S/ ^f(Begin) (End)
Extractable
(6) Shipping Information Extractable
T 1,^;,. MM^) VOAUnp^en^d/ Name of Shipper:
VOA Unpreserved(Duplicate)
Date Shipped:
Airbill Number:
DaleSampled
(7) Description of Sample Location:
(^) Special Handling Instructions:(e.g., safety precautions, hazardous nature)
REGIONAL OFnCE FILE COPY
W€ST COAST TECHNICAL S6RVIC6 INC. INDUSTRIAL CATEGORY
SAMP
LAB
DATE
DATE
STD •
CONC
Acid
21A
22A
24A
31A
34A
57A
58A
59A
60A
64A
65A
Base/
1B
5B
8B
9B
12B
18B
20B
25B
26B
27B
28B
35B
36B
37B
39B
40B
LE ID F0568
ID 21881A8
EXTRACTED 8/1/81
INJECTED 8/9/81
ID SESN176 PHEN353
FACTOR 1000
Compounds u,
2,4,6-trichlorophenol
p-chloro-m-cresol
2-chlorophenol
2,4-dichlorophenol
2,4-dimethylphenol
2-nitrophenol
4-nitrophenol
2,4-dinitrophenol
4,6-dinitro-o-cresol
pentachlorophenol
phenol
^Neutral Compounds
acenaphthene
benzidine
1,2,4-trichlorobenzene
hexachlorobenzene
hexachloroethane
bis(2-chloroethyl)ether
2-chloronapthalene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
3,3'-dichlorobenzidine
2,4-dinitrotoluene
2,6-dinitrotoluene
1,2-diphenylhydrazine
(as azobenzene)
fluoranthene
4-chlorophenyl phenyl ether
g/1*
NDND26
NDNOND
NnND
NnNn
ND
ND
NDND
ND
NDNDND
NDNDND
NnND
NnNDND
SAMP
LAB
DATE
DATE
STD :
CONC
Base/Neutral Compounds ui
41B
42B
43B
52B
53B
54B
55B
56 B
61B
62B
63B
66B
67B
68B
69B
70B
71B
72B
73B
74B
75B
76B
77B
78B
79B
SOB
81B
82B
83B
84B
129B
p-dio
LE ID F0568
ID 21881B9
EXTRACTED 7/31/81
INJECTED 8/13/81
ID BENZ398 BNSTD415
FACTOR 1DDO
4-bromophenyl phenyl ether
bis(2-chloroisopropyl) ether
bis (2-chloroethoxy) methane
hexachlorobutadiene
hexachlorocyclopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodimethylamine
N-nitrosodiphenylamine
N-nitrosodi-n-propylamine
bis (2-ethylhexyl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
di-n-octyl phthalate
diethyl phthalate
dimethyl phthalate
benzo(a) anthracene
benzo(a)pyrene
3,4-benzofluoranthene
benzo(k)fluoranthene
chrysene
acenaphthylene
anthracene
benzo(ghi)perylene
fluorene
phenanthrene
dibenzo(a ,h)anthracene
indeno( 1,2,3-cd)pyrene
pyrene
2,3,7,8-tetrachlorodibenzo-,0^105956
•xin
1ND
ND
ND
N D -—''s-NDnNB^
NIT
^
ND
ND
ND
18
ND*
N&
ND
ND
ND
ND
ND
ND
NDND
N D
ND
ND
Nn ^Nn VN n 1:N D ,?
s
,'./
ND
SAMP
LAB
DATE
STD
CONC
Volat
2V
3V
4V
6V
7V
10V
11V
13V
14V
15V
l6V
)™xx»xxxax^»)tm^xMW4Xixxxxxxxxx?o(19V23V
29V
30V
32V
33V
38V
44V
45V
46V
47V
48V
49V
50V51V
85V
86V
87V
9 W€ST COAST TECHNICAL
LE ID F0568
ID 21881V15
INJECTED 8/6/81
ID BFB36 VOA157T- A c"mD
lies
acrolein
acrylonitrile
benzene
carbon tetrachloride
chlorobenzene
1,2-dichloroethane
1,1,1-trichloroethane
1,1-dichloroethane
1,1,2-trichloroethane
1,1,2,2-tetrachloroethane
chloroethane
2-chloroethylvinyl ether
chloroform
1,1-dichloroethylene
1,2-trans-dichloroethylene
1,2-dichloropropane
1,3-dichloropropylene
ethylbenzene
methylene chloride
methyl chloride
methyl bromide
bromoform
dichlorobromo methane
trichlorofluoromethane
dichlorodifluoromethane
chlorodibromomethane
tetrachloroethylene
toluene
trichloroethylene
.SGRVK
ug/1
ND
ND
N D
ND
ND
ND
ND
N D
ND
N D
ND
ND
ND
ND
ND
ND
ND
ND13
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
:e INC.SAMP
LAB
DATE
DATE
STD
CONC
Pesti
89P
90P
91P
92P
93P
94P
95P
96P
97P
98P
99P
100P
101P
102P
103P
104P
105P
106P
107P
108P
109P
HOP
HIP
112P
113P
* = 1
(pe
ND =* * ^
INDUSTRIAL CATEGORY
LE ID F0568
ID TRACE N154
EXTRACTED 7/31/81
INJECTED 8/7/81
ID TRACE M151
. FACTOR 100
cides
aldrin
dieldrin
chlordane
4,4 '-DDT
4,4 ' -DDE
4,4 ' -DDD
alpha-endosulfan
beta-endosulfan
endosulfan sulfate
endrin
endrin aldehyde
heptachlor
heptachlor epoxide
alpha-BHC
beta-BHC
gamma-BHC
delta-BHC
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
toxaphene
.-ess than 10 ug/1
•sticides less than 5 ug/l)0
Not detected iv~,-Vf\r,r"^M^b&e^
Not confirmed by GCMS .-' -
ug/1
ND
ND
ND
rNO\^)
%
W
<SD
ND
N D
N D
ND
ND
ND
N D
ND
ND
ND
ND
ND
ND
ND
N D
ND
ND
7105957
88V vinyl chloride
WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3
QC Report No: 36Sample Number
F0568
A. SURROGATE SPIKE RESULTS
COMPOUND
Benzene - d6
l-Chloro-2-Bromopropane
Toluene - d8
2-Fluorophenol
Phenol - d5
Nitrobenzene - d5
2-Fluorobiphenyl
Naphthalene-DS
Fraction
VOA
VOA
VOA
ACID
ACID
B/N
B/N
B/N
Cone.(ug/1)
56
49
55
48
61
69
72
67
(Surrogates only)Spike
Added (uq/1)
50
50
50
100
103
101
101
101
%Recovery
1 1 2
98
1 1 0
48
59
68
71
66
B. TENTATIVELY IDENTIFIED COMPOUNDS
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
1 1 .
12.
13.
14.
15.
16.
17.
18.
19.
20.
CAS # COMPOUND NAME
ACETONE
TETRAHYDROFURAN
FRACTION
VOA #88
VOA #134
% Maximum Score Attained
Mass Matching Routine: FIT(specify)
909
958
•
O'W^i
O'-^inc.oi————————————————————————— IAUDJ,
-rn'-, r ,:.,,,.-, lAi-i.,. i^.i,,^ n Cprri»r'<; Cfllifnrni'n 00701 "1 ^ 'n^i .nni i
ROTECTION AGENCY HWI Sample i&magement Office Sample Number
ORGANICS TRAFFIC REPORTQ Case Number:
S
Sample Site Name/Code:./r^hf , f^(
@ Sample Type: (Check One)
—— RunOff
X Wefl
——— Receiving Water
Leachate
Effluent
OSier (specify)
(J) Shy To: ^\^^ ca^sf TPC^/^/^./ >6 05 pf»b^i c^ ^yerr/-/^ Q/^
9P7^/
(^) Description of Sample Location
(^) Special Handling Instructions:(e.g., safety precautions, hazardous nature)
REGIONAL OFFICE FILE COPY
W€ST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
SAMP
LAB
DATE
DATE
STD •
CONC
Acid
21A
22A
24A
31A
34A
57A
58A
59A
60A
64A
65A
Base/
1B
5B
8B
9B12B
18B
20B
25B
26B
27B
28B
35B
36 B
37B
39B
40 B
LE ID F0569
ID 21881A9
EXTRACTED 8/1/81
INJECTED 8/9/81
[D SENS176 PHEN353
FACTOR 1000
Compounds
2,4,6-trichlorophenol
p-chloro-m-cresol
2-chlorophenol
2,4-dichlorophenol
2,4-dimethylphenol
2-nitrophenol
4-nitrophenol
2,4-dinitrophenol
4,6-dinitro-o-cresol
pentachlorophenol
phenol
^Neutral Compounds
acenaphthene
benzidine
1,2,4-trichlorobenzene
hexachlorobenzene
hexachloroethane
bis(2-chloroethyl)ether
2-chloronapthalene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
3,3'-dichlorobenzidine
2,4-dinitrotoluene
2,6-dinitrotoluene
1,2-diphenylhydrazine
(as azobenzene)
f luoranthene
4-chlorophenyl phenyl
ug/1*
NDND
21
ND
NDND
NnNDNn*
ND
ND
?q
ND
ND
ND
ND30
50
493
ND
ND
ND
NnNO
e t h e r N D
SAMP
LAB
DATE
DATE
STD :
CONC
Base/
41B
42B
43B
52B
53B54B55B56B61B62B
63B
66B
67B
68B
69B
70B
71B
72B
73B
74B
75B
76B
77B
78B
79B
SOB
81B
82B
83B
84B
129B
p-dic
LE ID F0569
ID 21881B10 & 21881
EXTRACTED 7/31/81
INJECTED 8/13/81 8/21/81
ID BENZ398. BNSTD415/BENZ401 BNSTD418
FACTOR 1000 & 100
•''Neutral Compounds u j
4-bromophenyl phenyl ether
bis(2-chloroisopropyl) ether
bis (2-chloroethoxy) methane
hexachlorobutadiene
hexachlorocyclopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodimethylamine
N-nitrosodiphenylamine
N-nitrosodi-n-propylamine
bis (2-ethylhexyl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
di-n-octyl phthalate
. diethyl phthalate
dimethyl phthalate
benzo(a) anthracene
benzo(a)pyrene
3,4-benzofluoranthene
benzo(k)f luoranthene
chrysene
acenaphthylene
anthracene
benzo(ghi)perylene
fluorene
phenanthrene
d ibenzo(a ,h )an th racene
indeno( l ,2 ,3-cd)pyrene
pyrene
2,3,7,8-tetrachlorodibenzof^/x
xin 0710.S<^0
B13
^LND
ND
ND
NB)
?5-^
NA-^—Ng?ND<*
ND*
ND*
ND*
NDND
ND
ND
ND
N D
ND
ND
ND
Nn
NnNnwnN D
^^ShND 1- '
WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
SAMP
LAB
DATE
STD
CONC
Volat
2V
3V
4V
6V
7V
10V
11V
13V
14V
15V
16V
)™xxmxax^»%mwxMi)ti4mxxxxxxxxx19V23V29V
30V
32V
33V
38V
44V
45V
46V
47V
48V
49V
50V
51V85V
86V87V
88V
LE ID F0569
ID 21881V12 & 21881V16
INJECTED 8/5/81 & 8/6/81
ID BFB35 VOA156 & BFB36 VOA157
. FACTOR ——- & 1/10 D i l u t i o n
lies u
acrolein
acrylonitrile
benzene
carbon tetrachloride
chlorobenzene
1,2-dichloroethane
1,1,1-trichloroethane
1,1-dichloroethane
1,1,2-trichloroethane
1,1,2,2-tetrachloroethane
chloroethane
2-chloroethylvinyl ether
chloroform
1,1-dichloroethylene
1,2-trans-dichloroethylene
1,2-dichloropropane
1,3-dichloropropylene
ethylbenzene
methylene chloride
methyl chloride
methyl bromide
bromoform
dichlorobromo methane
trichlorofluoro methane
dichlorodifluoromethane
chlorodibromomethane
tetrachloroethylene
toluene
trichloroethylene
vinyl chloride
LAB ID TRACE N155
DATE EXTRACTED 7/31/81
g/1
ND
ND*
ND
392
ND
ND
N D
ND
N D
ND
ND
ND
ND
ND
ND
N D
ND
20
ND
ND
ND
ND
ND
ND
ND
ND
16
NP
ND
SAMPLE ID F0569
DATE INJECTED 8/7/81
STD ID TRACE #4156
CONC. FACTOR 100
Pesticides
89P aldrin
90P dieldrin
91P chlordane
92P 4,4 ' -DDT
93P 4,4 ' -DDE
94P 4.4'-DDD
95P ' alpha-endosulfan
96P beta-endosulfan
97P endosulfan sulfate
98P endrin
99P endrin aldehyde
100P heptachlor
101P heptachlor epoxide
102P alpha-BHC
103P beta-BHC
104P gamma-BHC
105P delta-BHC
106P PCB-1242
107P PCB-1254
108P PCB-1221
109P PCB-1232
HOP PCB-1248
HIP PCB-1260
112P PCB-1016
113P toxaphene
* = Less than 10 ug/1
(pesticides less than 5 ug/1)
ND = Not detected
-;;* ^ ^Q^ confirmed by GCMS n
ug/1
ND
NO
ND
•W
•NO-en
ND
ffl
•TO
NO
NO
NO
NO
ND
0.1**
n.3**ND
0.2**
ND
N D
NOND
ND
ND
ND
NO
7105961
WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS. DATA SHEET - Page 3
QC Report No: 36Sample Number
F0569
A. SURROGATE SPIKE RESULTS
COMPOUND
Benzene - d6
l-Chloro-2-Bromopropan6
Toluene - d8
2-Fluorophenol
Phenol - d5
Nitrobenzene - d5
2-Fluorobiphenyi
Naphthalene-DS
Fraction
VOA
VOA
VOA
ACID
ACID
B/N
B/N
B/N
Cone.(ug/1)
48
45
47
0
2
72
81
74
(Surrogates only)Spike
Added (ug /1 )
50
50
50
100
103
1 0 1
101
101
%Recovery
96
90
94
0
2 C\J
71 ^—————HT
80
73 0
B . TENTATIVELY IDENTIFIED COMPOUNDS
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
1 1 .
12.
13.
14.
15.
16.
17 .
18.
19.
20.
CAS # COMPOUND NAME
TOLUENE
CHLOROBENZENE
TRICHLOROBENZENE
FRACTION
VN #43
B/N #68
B/N #209
% Maximum Score Attained
Mass Matching Routine: FIT(specify)
999
991
GENERAL FIT
•
{V^W^ /AC(--
- n'71 fu.nr.0
ORGANICS TRAFFIC REPORT(T) Case Number:
^%0
Sample Site Name/Code:[Ar^ X.f
©) Sample Type: (Check One)
Run Off
WeU
Receiving Water
Leachate
Effluent. -•
Other (specify)
@ Ship To:
W^s^ Co^st' fe^h'i^^^j^^oS ^A^ ^yCe^f^s, C«/'^ /
^D^ot
Attn:
(4) Regional Office:Sampling Personnel:
..^A^ /Uc^^^e
(y Mark Volume Level on Sample Bottle
(Name)
:/ 37/- /7C^/Extractable
(Phone)
Sampling Date:
•-; - ^/ J^^ ^
Extractable
(Begin) (End)Extractable
(6) Shipping Information Extractable
J VOA Unpreserved
Name of Shipper:
-~ "^ -. >-' /.' ^ (_/ - .; /
VOA Unpreserved(Duplicate)
Date Shipped:
-, , ..- -i r~ •"' '—> ~"J' * • - ' ' " / J '-.-.? "S
Airbill Number:
DateSampled
(7) Description of Sample Location:
\J[) Special Handling Instructions:(e.g., safety precautions, hazardous ncrture)
0710257
07105963REGIONAL OFFICE FILE COPY
WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
SAMP
LAB i
DATE
DATE
STD I
CONC
Acid
21A
22A
24A
31A
34A
57A58A59A60A
64A
65A
Base/
1B
5B
8B
9B
12B
l8B
20B
25B
26B
27B
28B
35B
36B
37B
39B
40B
i7pnt - p.,1^.^ , 11.',., Q.n .p [-;
LE ID F0570
ID 21881A10
EXTRACTED 8/1/81
INJECTED 8/10/81
:D SENS177 PHEN354
FACTOR 1000
Compounds w
2,4,6-trlchlorophenol
p-chloro-m-cresol
2-chlorophenol
2,4-dichlorophenol
2,4-dimethylphenol
2-nitrophenol
4-nitrophenol
2,4-dinitrophenol
4,6-dinitro-o-cresol
pentachlorophenol
phenol
'Neutral Compounds
acenaphthene
benzidine
1,2,4-trichlorobenzene
hexachlorobenzene
hexachloroethane
bis(2-chloroethyl)ether
2-chloronapthalene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene3,3'-dichlorobenzidine
2,4-dinitrotoluene
2,6-dinitrotoluene
1,2-diphenylhydrazine
(as azobenzene)
f luoranthene
4-chlorophenyl phenyl ether
g/1
NP
NDNO*
NPNnNUWNnNnNn
ND
ND
N D
ND
ND
NDNONONn*
NnNnNn
NnN D
ND
SAMP I
LAB I
DATE
DATE
STD ID BENZ398 ENSTD415
CONC
Base/Neutral Compounds u.i
41B
42B
43B
52B
53B
54B
55B
• 56B
61B
62B
63B
66B
67B
68B69B70B
71B
72B
73B
74B
75B
76B
77B
78B
79B
80 B
81B
82B
83B
84B
129B
p-dio:
r ' ^ , - ,>nc r ' ^ i i ^ r p i a qn7C1 '?^'~',:^?\-W\^
.E ID F0570
D 21881B11
EXTRACTED 7/31/81
INJECTED 8/13/81
FACTOR 1000
4-bromophenyl phenyl ether
bis(2-chloroisopropyl) ether
bis (2-chloroethoxy) methane
hexachlorobutadiene
hexachlorocyclopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodimethylamine
N-nitrosodiphenylamine
N-nitrosodi-n-propylamine
bis (2-ethylhexyl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
di-n-octyl phthalate
diethyl phthalate
dimethyl phthalate
benzo(a) anthracene
benzo(a)pyrene
3,4-benzofluoranthene
benzo (k ) fluoranthene
chrysene
acenaphthylene
anthracene
benzo(ghi)perylene
fluorene
phenanthrene
d ibenzo(a ,h )an th racene
indeno( 1,2,3-cd)pyrene
pyrene
2,3,7,8-tetrachlorodibenzo-O^;
xin
^1
ND
ND
ND
ND•q-
NC^
NQLnNCT-ND0
ND
ND
ND*
ND*
NO*
N D
ND
ND
ND
N D
N D
N D
N D
ND ^
^- ^
^- ^Nn ^N n °N D " •—
105964N D
VSSSS^ WEST COAST TECHNICAL
SAMPLE ID F0570
LAB ID 21881V17
DATE INJECTED 8/6/81
STD ID BFB36 VOA157
CONC. FACTOR -------
Volatiles
2V acrolein
3V acrylonitrile
4V benzene
6V carbon tetrachloride
7V chlorobenzene
10V 1,2-dichloroethane
11V 1,1,1-trichloroethane
13V 1,1-dichloroethane
14V 1,1,2-trichloroethane
15V 1,1,2.2-tetrachloroethane
l6V chloroethane
)^XX»XXXX)iX^)tmWXMl)tM)XXXXXXXXXXX
19V 2-chloroethylvinyl ether
23V chloroform
29V 1,1-dichloroethylene
30V 1,2-trans-dichloroethylene
32V 1,2-dichloropropane
33V 1,3-dichloropropylene
38V ethylbenzene
44V methylene chloride
45V methyl chloride
46V methyl bromide
47V bromoform
48V dichlorobromomethane
49V trichlorofluoromethane
50V dichlorodifluoromethane
51V chlorodibromomethane
85V tetrachloroethylene
86V toluene
87V trichloroethylene
88V vinyl chloride
SERVICE
DATE EXTRACTED 7/31/81
ug/1
ND
NO
ND
ND
ND
ND
ND
N D
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
13
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
INC. INDUSTRIAL CATEGORY
SAMPLE ID F0570
LAB ID TRACE Ml 57
DATE INJECTED 8/7/81
STD ID TRACE N156
CONC. FACTOR 100
Pesticides
89P aldrin
90P dieldrin
91P chlordane
92P 4.4'-DDT
93P 4.4 ' -DDE
94P 4 ,4 ' -DDD
95P alpha-endosulfan
96P beta-endosulfan
97P endosulfan sulfate
98P endrin
99P endrin aldehyde
100P heptachlor
101P heptachlor epoxide
102P alpha-BHC
103P beta-BHC
104P gamma-BHC
105P delta-BHC
106P PCB-1242
107P PCB-1254
108P PCB-1221
109P PCB-1232
HOP PCB-1248
HIP PCB-1260
112P PCB-1016
113P toxaphene
* = Less than 10 ug/1
(pesticides less than 5 ug/1)
ND = Not detected
** = Not confirmed by GCMS ^ * i^y
ug/1
ND
ND
ND
W3
INfi
WD
ip——©-MND
ND
ND
ND
ND
ND
ND
ND
ND
ND
N D
ND
ND
ND
N D
ND
NO
^
07105965
WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3
QC Report No:Sample Number
F0570
A. SURROGATE SPIKE RESULTS
COMPOUND
Benzene - d6
l-Chloro-2-Bromopropane
Toluene - d8
2-Fluorophenol
Phenol - d5
Nitrobenzene - d5
2-Fluorobiphenyl
Naphtha 1ene-D8
Fraction
VOA
VOA
VOA
ACID
ACID
B/N
B/N
B/N
Cone.(ug/1)
56
49
52
2
2
62
75
70
(Surrogates only)Spike
Added (ug/1)
50
50
50
100
103
101
101
101
%Recovery
1 1 2
98
104
2
2 ^
61 u74 .
69 <
B . TENTATIVELY IDENTIFIED COMPOUNOS
1.
2^
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.
17.
18.
19.
20.
CAS % COMPOUND NAME
TETRAHYDROFURAN
UNKNOWN
FRACTION
VOA #131
VOA M21
% Maximum Score Attained
Mass Matching Routine: FIT(specify)
928
NO SOOD FIT
.
-
o^w^
————————————————r>"« ne.'i-n'-, r-^ri.r-1 W.iv SnitP 0 Orritos. Cali-fnrnia 00701 ?11' '92l-Qa31
i 5 St'P i'^d]
Potential Hazardous Waste Site•r<^n-s -^
Charles A. Gazda, ChiefCompliance Section (6SA-SC)
Bruce Elliot, ChiefGeneral Enforcement Branch (6EG)
c^P - 6 ../h—' *
Site NameLocationHazsit NoTDD No.
A. Fiel
T207T207ISSISS
B. §311
1.2.3.
VorktC-'.hr ^^ //<3A/?'/^f - ^ - W-7 -^•
d Report:
0-20-3 recon sampiingCompiiance ReportNon-Notifior Report
potential (completed by 6SA-E
§311 sample collectedAnalytical results attachedProposed §311 action:
attached ( )attached ( )attached ( )attached ( )
) yes ( ) no ( )
yes ( ) no ( )yes ( ) no ( )
r-r-m
00
C.
D.
Were drinking water wellssampled?
Analytical Data: P^/vf-K/
1. FIT data review
no ( )
y
yes ( )
-SQ^O^O by flOPC^I^.
attached (^j
E.
2. Contract lab results:
watersoi l , waste
3. Houston Lab results
Comments:
attached (Xfattached ( )
attached ( )
S£-—A4e-l-e MiLcl ie l I (bW-S :
Ecology and Environment, Inc.
Region VI
MEMORANDUM
TO: Charles Gazda,Chief Compliance Section
FROM: David Anderson, FIT ^.E&E Region VI
THRU: K. Matone, FITL ^Y^^E&E Region VI
' CO
DATE: September 1 5 , 1 9 8 1 '"-LPt
RE: TDD F-6-8109-20, Review of Sample Data from Vertac ^_
Attached is a review of and quantif ication of 8 wel l water samples collected bythe state at Vertac. Only one anomaly appeared in the results, that being thepresence of acetone in 6 of the 8 samples. Acetone has not been present inprevious samples and its presence is probably due to improper preparation ofsample containers or contamination by the analytical lab.
00
Sources
Standards:EPA water Quality Criteria DocumentsNovember 28, 1980
Toxicities:Registery of Toxic Effects1979 Edition
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A ,2^'>'
C^,; r, 1,. .'c' c r' • f<. n
; i ^ 5 ^ec i r • ' /-! / 5^- ine-r
/f- -.?? 7
^( nA'no^^
/^ 3/<?
^n ^ noi
. . . ^-....- . - . - . - - . ^ur\kno^n
/7) 47
(( n \<^r\
C^\CI-L r ^ e ^ y f b^ns^-nt- /3 A'L-
^ n,';/.''1'^'''' ^1 / SL'-T"'"
^.^J-1-/>^^^/ ^l1^
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H ^ S p ^ ' ' ' tr< '^'1'"'-
- • ^ i '13^ /
/ / ' I c ,",lc'^' ^et/ i f^ i / b'r'"-7''^^-/
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27-L^L^b
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m- 5^^b
l; - 2,33^
^- l^f^b
^S- IL-.^^b
) i 7- ^3c^
(, . - I^CC^^
/7 - 3;';-^
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^ -^cc^b
^ " ) - ^3.) j.p/;)
-
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———-
-——
———
——
——-
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,,
.————
————
——-—-
————.
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l^rift^
-ITS—
h/<lA A^-
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t^csr^ eh/ore)
•s—
.0^
chic^- lfK//.3^l Z »'"«•- "3 •^•^~
0
0
^ I I<ck I'-'r-' ^h^^i
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•^7/-,c^^Y.<
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0710S981
US Environmental Protection AgencyHazardous Waste Investigation
Sample Management OfficeP.O. Box 818
Alexandria, Virginia 22313(703)683-0885
SEP 21 1981
S & A DIVISION 1I
MEMORANDUM
DATE: September 14, 1981
SUBJECT: RETURN OF SAMPLE TRACKING DOCUMENTSCM0^in
FROM: Sample ^anagenent Office (-{^J^ ^-A^Uts^ 0\
• inTO: Charles Gazda, Project Officer, USEPA Region VI ,—
Enclosed please find the Regional copies of the sample tracking documents576, 577.
for case/s 580, 554, 556, 557, 575 , . Included are a photocopy of the Laboratory
Traff ic Report, the Regional Laboratory Chronicle, and the Regional Analysis
Chronicle. These documents along wi th your copy of the Sampling Tra f f i c Report
comprise the entire Sample Tracking Package. The IFB Laboratory w i l t forward
the Final Analysis' Data Forms directly to the Regional Project Officer or his
designated representative.
The IFB Laboratories will be audited on a quarterly basis (every three
months) for quality control procedures and technical verification by EMSL-LV
and NEIC. Any information from these audits which relates to the samples wi l l
be forwarded to the Region.
If you have any questions on these documents or procedures, please feel
free to call the Sample Management Off ice.
00
0*710^3? -
07105982
ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)
Laboratory Nome
Case NumberSEP 9^
Sample Description Technician SignatureDate/Ime Extraction Completed
Detedl Below Pertinent Infannafion and /orProblenis Asscaated wifti Esdractkxi
Extractable(Add)
^- ^/ /^ • ..o - '^u^-
i / '/--<-l't7$7"z -
Extractable(Pesticides)
•• / <•-<•-•.-. -' ae<;/ // / ,- y'A^fl^^ -- /'r,7^^
Extractable(Dioxins)
• ~o0
QCExtractable(Base/Neutral)
QC Extractable(Add)
QCExtradable(Pesticides)
QCExtroctable(Dioxins)
Additional Comments:
(measea-
07105983SMO COPY FOR RETURN TO REGION
I AGENCY HWI Sample Management Office
ORGANICS LABORATORY CHRONICLE (ANALYSIS)Sample Number
F 0536
Laboratory Name
Case Number
Sample Description Analyst SignatureDate /Time Analysis Completed
SEP ^wDetail Below Pertinent Information and /or
Problems Associated with Analysis
Extractable(Base/Neutral)
•:' I i^l - L
• r ' ^ [i s I• -.•'.A.^.A [ .
Extractable(Add)
,.-"7/ f^i A
Extractable(Pesticides)
A /••--
Extradable(Dioxins)
VOAUnpreserved 00
VOAUnpreserved(Duplicate)
QCExliactable(Base/Neutral)
QCExfanctable(Add)
QC Extractable(Pesticides)
QCExliadabb(Dioxins)
Additional Comments:
SMO COPY FOR RETURN TO REGION
ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)
Sample Description Tedmidan SignatureDate /Time Exhaction Completed.
I^tailBekwPerfnentlniamntm and/orProblenisAsaodatedwilhEsctiaction
Extractable(Base/Neutral)
/y^J^^- • / 1 ' ^^/f/^____^^r
Extractable(Add)
^^^a^ ^ J^i^i/ ^'f } ~"? A
^ --< ''? I L-C^T? -
^' / T^--'''!^^.^-
Extroctables)
^ ^ a5< -&<?°ia»y
9/^//^___________/^^^^ - ^
Extractable(Dioxins)
0''m
QC Extractable(Base/Neutral)
';/;,, . - »i'7- -
^.-r^-"
00
QCExhuctable(Add)
'(-'•••/'•. '-'- // ,.v^.-^-^^f^
/3/S~-../-
QC Extractable(Pestiddes)
QCExtreictable(Dioxins)
Additional Comments:
SMO COPY FOR RETUBN TO REGION
ORGANICS LABORATORY CHRONICLE (ANALYSIS)Sample Number
W 0564
Laboratory Name
Case Number. S8PSample Description Analyst Signature
Date /Tune Ancdyas CompletedDetcril BekawPertmenti^CTinalionand/cT
Problems Assodated with Ancdyas
Extrnctoble(Base/Neutral)
^//y^,-^ ' /"^r^J^ ^^
Extzactable(Add)
Ebcbactable5)
^ - . ' : / ^ •/-•
<^ L.iExtractable(Dioxins)
LPt
VOA Unpreserved00
VOA Unpreserved(Duplicate)
/ /';; i -<• -^' -/^-' /
-M.QCEidractable(Base/Neutral)
QC Extractable(Add)
QCExfaactable(Pesticides)
QC Extractable(Dioxins)
Additional Comments:
SMO COPY FOR RETURN TO REGION
<mo%B&5"
07105986
iple Management Umce
ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)
Laboratory Name
Case NumberSEP 9W
Sample Description . Technkaan SignatureDate /Time Extraction Completed
Deted Bekw Pertinent infexmalidn and/orRrdslemsAsscckitedwiftiEJctox'tion
Exttactable(Base/Neutral)
^^a^^ .^ ^^-^^(
^//^___________^S~/ WS. -6 //
^/^ „_______„ /S^T//^r,!:^-^C' ^ ^^-{^SX^
^/5l ^_______/^
Exbuctable(Add)
ExtractaUes)
Extractable(Dioxins)
QCExtructable(Base/Neutral)
00
QCExtrcidable(Add)
QCExtroctable(Pesticides)
1 '' /i'''^n :-<(. 6-
QCExtractable(Dioxins)
Additional Comments:
SMO COPY FOR RETURN TO REGION
;t° ST^ )N AGENCY HWI Sample Management Office
ORGANICS LABORATORY CHRONICLE (ANALYSIS)I Sample Number
IF 0565
Laboratory Name
Case Number. SEPSample Description Analyst Signature
Date/Tune Analysis CompletedDetail Below Pertinent Infonncrtion and/or
Problems Associated with Analysis
Extractable(Base/Neutral)
on^V I' { ! ' I^-—.^.i^-^J^,' \, A^
Extractable(Add)
Extractable(Pesticides)
...-/^W-
IJ. ' .A .00
-Oi-Extractable
(Dioxms)LTl
VOA Unpreserved'S5"0
VOA Unpreserved(Duplicate)
^/.-A ./
QCExtKidable(Base/Neutrcd)
QCExtixictable(Add)
QCExtradnble(Pesticides)
QC Extractable(Dioxins)
Additional Comments:
SMO COPY FOR RETURN TO REGION
OBGANICS LABORATORY CHRONICLE (EXTRACTIONS)
SEP
i:' -'' Sample Number
tP 056&
Saraple Description Technician SrcinatureDate /Time Extraction Completed
Deteril Bekw PertiniMitInionriationand/orPioblenas Associated wiftiExtractial
ExtaackdJe(Base/Neutrcd)
ExtracfcAle(Aad)
(•' ^^C^€3L^
/wEschcoctadw(Pesticides)
Z^^--^^ <^ ^sy^^y^^.
y-^y/f/______/^^ ^-^ - ^^Exbuctable(Dioxms)
QCExtradable(Base/Neutrcd)
00
QC Extendable(Add)
QCExtroctable(Pesticides)
QCExtrctdafale(Dioxins)
Additional Comments:
SMO COPY FOR RETURN TO REGION
I AGENCY HWI Sample Management OfficeSample Number
ORGANICS LABORATORY CHRONICLE (ANALYSIS)
Laboratary Name
Case Number.
Scanple Description Analyst SignatureDate /Time Analysis Completed
SEP 91981Detail Below Pertinent Infomialion and/or
Problems Associated with Ancdyas
Extnictoble(Base/Neulral)
Extractable(Add)
•^w^l^ v' f ^Y' ( A
——^^
Extractable(Pesticides) '( y
'r.^ / ^ / ^h
{ ; ( ) ^. .--•v--;. . ^^A.0
Extractable(Dioxins)
VOAUnpreserved- .•f • i 0
0
VOAUnpreserved(Duplicate)
QCExtroctable(Base/Neutral)
QCExtiactable(Add)
QCExtiadable(Pesticides)
QC Extractable(Dioxins)
Additional Comments:
SMO COPY FOR RETURN TO REGION
OBGANICS IABORATOBY 'CHRONICLE (EXTRACTIONS)
Laboratory Nome
Case NumberSEP
Sample Description Technician SignatureDate/TBn&ExtracScn Completed
ttetafl BekwPerfeiHitInfaroiafion and/cyPrcMemsAsacdated« i Exiradion
Extxactable(Base/Neutral)
^ac^^^'^ -s^m^i/
gy^/^/ ____/^/yy , i l /^ y^^s^'
ExtrnctnUe(Add)
ExfaactaUe
-0"
\D
QC Ebctractable(Base/Neutml)
0
0
QCExtroctable(Add)
QCExtractable(Pesticides)
QCExIractable(Dioxins)
Aaditional Comments:
SMO COPY FOR RETURN TO REGION
)N AGENCY HWT Sample Management Office
ORGANICS LABORATORY CHRONICLE (ANALYSIS)'Sample Number
0567
Laboratory Name
Case Number. SEP 91981
Sample Description Analyst SignatureDate/Time Ancdyas Completed
Detail Below Pertinent Infannatton and / orProblems Associated with Ancdyas
Extmctable(Bose/Neutrcri)
r'^, 7, /-"'fcrl. v ( / .
Exfauctoble(Add)
u '..-^ {\ \ } f f^J^-^^ ^A-^f ,/ f\
^^UM
-'L,0 ( ^ExtractaUe(Dioxins) C^
-0"
v0VOA Unpreserved
VOA Unpreserved(Duplicate)
00
QC Extractable(Base/Neutrcd)
QCExIractable(Add)
QC Extractable(Pesdddes)
QC Extractable(Dioxins)
Additional Comments:
SMO COPY FOR RETURN TO REGION
ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)S- Sample Number •
r 05681
Laboratory Nome
Case Number.
Sample D6sciiptjoii. Techrricym Sgncrtiire •Date/Time Exiiaction Completed
DeterilBelowPerfnentlhiontoafcti and/orPirchtemsAssocacttedwifliEsdracticn
y^^^
^ I /flExbackdJe(Base/Neutrai)
//4^^f-^ ^ c^a^^
8/^) /s/dr/^^i^c^ ^ •:y^^^^
-?/3//^________^
Extractable(Add)
Extractable(Koxins)
0' 0
QCExtractable(Base/Neutrai)
00
QCExfanctable(Add)
QCExtractable(Pesticides)
QCExtractable(Dioxins)
Additional Comments:
SMO COPY FOR RETURN TO REGION
"It WO't'
iGENCY HWI Sample Management Office
ORGANICS LABORATORY CHRONICLE (ANALYSIS)|fcSampteNumber
EF 0568
LAorcriory Name
Case Number. SEP ^w
Sample Description Analyst SignatureDate/Time Anatyas Completed
DetedBekwPertinentInfanna&XKand/orPrchlems Associated with Analysis
rsKv^V^v^'V'wQ
(Base/Neutrcd)
ExtractaUe(Add)
Extroctable(Pesticides)
ExtractaUe(Dioxins)
0
\0
VOA Unpreserved. . . " J t f / r i / ' " ,
-' y • /
r- ..;., !,, . Loo
VOA Unpreserved(Duplicate)
QCExtractable(Base/Neutecd)
QCExtractable(Add)
QCExtractable(Pesticides)
QCExtractable(Dioxins)
Additional Comments:
SMO COPY FOR RETURN TO REGION
ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)
Laboratory Nome
Case Number
Sample Description •• ^ „ ^^IfedB'ucKm Signature. Date/Time Exircicticn Completed
Deteni BelcwPeifee firfeiniaficftcind/OrPnAtemsAssocKrtedwtti ExteicticHi
ExIiackdJe(Base/Neutrai)
^-'^/ ^ffK^ftM ftt^
C^rcL^h-^ 'Extractahle(Add)
Exfanctahte(Pesticides)
//^€C^ ^ t^^
^/^hi_____/^/^^a^ ^^^^7
•9-/2f/yi________^£>0
Extractable(Dioxins)
0
vO
QC Extractable(Base/Neutrcri)
00
QC Extractable(Add)
QC Extractable(Pestiddes)
QC Extractable(Dioxins)
Additicaial Comments:
SMO COPY FOR RETURN TO REGION
rENCY HWI Sample Management Office
ORGANICS LABORATORY CHRONICLE (ANALYSIS)|? Sample Number
0569
Laboratory Name
Case Number. 8EP S1"1
Sample Description Analyst SignatureDate/Tune Analyas Completed
Detoril Bekw Pertinent Infonnaficn and /acPrciblemsAsscciated with Ancdysis
Extractable(Base/Neuhxd)
Extractable(Add)
ExtractaUeB)
Ebdractable(Dioxins)
VOA Unpreserved'A"' -
/-^'! » . /
:.-' .- .. < ^
00
VOA Unpreserved(Duplicate)
QCExfaudable(Base/Neutral)
QCExtrcictable(Add)
QCExtractable(Pestiddes)
QCExtractable(Dioxins)
Additional Comments:
SMO COPY FOR RETURN TO REGION '. ..- ^ -,' --£f»;,.._
ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)
Laboratory Name
Case Number
Sample Description,: .: Technician Signature -•Date/TuneExtrciction Conipleted
' .C? ^I • • » ,>W ..-•X • • y
DefcdIBelowPialinatihieeHg ^- PnAtemsAsasdated wilbExtracticn
Exhndable(Base/Neutrcd)
^^^i^^'
^/^/, , _ /3/S^a^--^'^- <5r <^<»^
7/3//^ /^^
Extractable(Add)
Extractable(Pesticides) ^^ - . ,
Extroctable(Dioxins)
0\0
QC Extmctabre.(Base/Neutral)
00
QC Extractable(Add)
QC Extractable(Pesdddes)
QC Extractable(Dioxins)
Additional Comments:
SMO COPY FOR RETURN TO REGION
ON AGENCY FIWI So^de Monaqement Office
ORGANICS LABORATORY CHRONICLE (ANALYSIS)
Case Number, SEP 9
Sample Description r.:v.^y-^ - -Ancdyst Signature- ' . > A -•'.:. Date/rnneAnaIygs Completed
Extnx'tnhle ;(Base/Neutral) eu%"ExtractaUe(Add)
Exfmctables) CD
ExtractaUe(Dioxins)
VOA Unpreserved-/^
r^^JU ( {00
VOA Unpreserved(Duplicate)
QCExtractahle(Base/Neutrcd)
QCExtractable(Add)
QCExtroctable(Pestiddes)
QCExtractable(Dioxins)
Additional Comments:
SMO COPY FOR RETURN TO REGION
ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)
Laboratory Nome
Case Number
fv -----^1- - T* • I I •••• I! ^Loampie uescnption ' Technician SignatureDcrte/TinKEbdiaction Completed
DetodlBebwPerlmentInfonnatfcti and/orProbtemsAsscckitedwthEJdiacttan
^^<^;5r
^///^/______/o?^rExtzuctable(Base/Neutral)
Extractable(Add)
EbctrcictaMe(Pesticides) ^/^(/^ - ^ U^~
ExtractaUe -(Dioxins)
0
<0
QC Extrnctezble(Base/Neutral)
00
QCExtractable(Add)
QCExtructable(Pesticides)
QCExtradable(Dioxins)
Additional Comments:
•--- L, ^%sy»—
SMO COPY FOR RETURN TO REGION
r AGENCY HWI Sample Management Office
ORGANICS LABORATORY CHRONICLE (ANALYSIS)(^ Sample Number
^: 0571
Laboratory Name
Case Number _
Sample Analyst SignatureCterte/InneAncdyas Ccxn]deted
SEP 91981
Deteril Bebw Pertinent Infanixriia'i and/orProblems Associated with Analysis
Extractable(Base/Neutral)
Extractable(Add)
., .T/W^.-^ /• / I /• •
k. .JL- L .Extractable ^(Pesticides) o
Extractable(Dioxins)
VOA Unpreserved00
VOA Unpreserved(Duplicate)
QC Extractable(Base/Neutral)
QCExIractable(Add)
QCExtraclable(Pesticides)
QC Extractable(Dioxins)
Additional Comments:
- ^^-f..
SMO COPY FOR RETURN TO REGION
">? A T!
isszy\ BBOlt."•'( men®
U.S. ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management OfficeP.O. Box 818. Alexandria. Virginia 22313-703 557-2490 • FIE •557-2490
ORGANICS TBAFnC REPORTSample Number
F 053S
©Case Number:
Sample Site Name/Code:
VP.nT^.
©2) Sample Type: (Check One)
— RunOff
Well
Receiving Water
Leachate
Eifluent
© Ship To:
Attn:
Oher (specify)
©Regional Office:
Sampling Personnel:
© Mark Volume Level on Sample Bottle
(Name)0 / Extractable
DateSampled
© Analysis Lab:Rec'dby: ^> ^^Legu^CDrrt^/Tim^Rpf'd -?/3//^^/^7-
Sample Condition on fteceipt(e.g. broken, no ice, Chainoi-lStstody, etc.)
0(Phone)
Sampling Date:Extractable
\^J6 duJSTft^ -^AfcA-.^MQ ..L<M^t*A/O <l^L^mu^i*^<'^^as^ U-dV. -^j;^]-c<u n^u ,A£^ fif ^?y&T'
(Begin) (End)Extractable
© Shipping mformation Extractable
VOA Unpreserved
Name oi Shipper:VOA Unpreserved(Duplicate)
Date Shipped:
Airbill Number
© Description of Sample Location:
®) Special Handling Instructions:(i' g, :AiietY prccrrnfaons, h(-i7.ardous nature)
07106001T "R I'T^PY rnr; "!--n \w Tr^ •-mn
SAMI
LAB
DATE
STD
CONC
Vola-
2V
3V
4V
6V
7V
10V
11V
13V
14V
15V
16V
u^mmwmM&mwm^^n\m19V
23V
29V
30V
32V
33V
38V
44V
45V
46V
47V
48V
49V
50V
51V
85V
86V
87V
88V
R WEST COAST TECHNICAL
'LE ID LAB BLANK
ID 21881V14
; INJECTED 8/6/81
ID BFB36 VOA157
:. FACTOR ————--
tiles
acrolein
acrylonitrile
benzene
carbon tetrachloride
chlorobenzene
1,2-dichloroethane
1,1,1-trlchloroethane
1,1-dichloroethane
1,1,2-trichloroethane
1,1,2,2-tetrachloroethane
chloroethane
2-chloroethylvinyl ether
chloroform
1,1-dichloroethylene
1,2-trans-dichloroethylene
1,2-dichloropropane
1,3-dichloropropylene
ethylbenzene
methylene chloride
methyl chloride
methyl bromide
bromoform
dichlorobromo methane
trichlorofluoromethane
dichlorodifluoromethane
chlorodibromo methane
tetrachloroethylene
toluene
trichloroethylene
vinyl chloride
S6RVK
ug/1
NnND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
14
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
CEINC
SAMI
LAB
DATI
DATI
STD
CON(
Pest-
89P
90P
91P
92P
93P
94P
95P
96P
97P
98P
99P
100P
101P
102P
103P
104P
105P
106P
107P
108P
109P
HOP
HIP
112P
113P
* =
(p
ND =** ^
. INDUSTRIAL CATEGORY
'LE ID NO SAMPLE
ID
:: EXTRACTED
; INJECTED
ID
;. FACTOR
Lcides
aldrin
dieldrin
chlordane
4,4 '-DDT
4,4 ' -DDE
4.4'-DDD
alpha-endosulfan
beta-endosulfan
endosulfan sulfate
endrin
endrin aldehyde
heptachlor
heptachlor epoxide
alpha-BHC
beta-BHC
gamma-BHC
delta-BHC
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
toxaphene
Less than 10 ug/1
esticides less than 5 ug/1)
Not detected
Not confirmed by GCMS(mo tsi
ug/1
NA
NA
NA
MAl
IW
^
NA,
K&
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
A
t—
0710600217605 Fabnca Way, Suite D Cerntos. California 90701 213/921-9831
WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3
QC Report No:Sample Number
LAB BLANK
A. SURROGATE SPIKE RESULTS
COMPOUND
Benzene - d6
l-Chloro-2-Bromopropane
Toluene - d8
2-Fluorophenol
Phenol - d5
Nitrobenzene - d5
2-Fluorobiphenyl
Naphthalene-DS
Fraction
VOA
VOA
VOA
ACID
ACID
B/N
B/N
B/N
C o n e . ( u g / 1 )
54
50
56„
-
(Surrogates only)Spike
Added (ug/1)
50
50
50
-
-
-
%Recovery
108
100
112^
^^~^0
——————^~
(-1
B . TENTATIVELY IDENTIFIED COMPOUNDS 0
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
1 1 .
12.
13.
14.
15.
16.
17.
18.
19.
20.
CAS # COMPOUND NAME FRACTION
% Maximum Score Attained
Mass Matching Routine: FIT(specify)
'
/-1»-<-1 f\ryfSJf———vf-ivrwS.Z
07106003^o^ '--ihrii-n Wiv SmtpD Cerritos. California 90701 SIS.''0"1-"'^ I
W€5T COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
SAMP
LAB
DATE
DATE
STD
CONC
Acid
21A
22A
24A
31A
34A
57A
58A
59A
60A
64A
65A
Base/
1B
5B
8B
9B
12B
18B
20B
25B
26B
27B
28B
35B
36B
37B
39B
LE ID METHOD BLANK
ID 21881A1
EXTRACTED 8/1/81
INJECTED 8/9/81
ID SENS176 PHEN353
FACTOR 1000
Compounds u
2,4,6-trichlorophenol
p-chloro-m-cresol
2-chlorophenol
2,4-dichlorophenol
2,4-dimethylphenol
2-nitrophenol
4-nitrophenol
2,4-dinitrophenol
4,6-dinitro-o-cresol
pentachlorophenol
phenol
/Neutral Compounds
acenaphthene
benzidine
1,2,4-trichlorobenzene
hexachlorobenzene
hexachloroethane
bis(2-chloroethyl)ether
2-chloronapthalene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
3,3'-dichlorobenzidine
2,4-dinitrotoluene
2,6-dinitrotoluene
1,2-diphenylhydrazine
(as azobenzene)
f luoranthene
g/1
ND
ND
ND
ND
ND
ND
N D
ND
N D
NnND
ND
ND
N D
ND
ND
ND
N D
N D
N D
ND
ND
ND
ND
NDND
SAMP]
LAB I
DATE
DATE
STD I
CONC
Base/
41B
42B
43 B
52B
53B
54B
55B
56B
61B
62B
63B
66 B
67B
68 B
69B
70B
71B
72B
73 B
74B
75B
76B
77B
78B
79B
80 B
81B
82B
83B
84B
-E ID METHOD B L A N K
D 21881B1
EXTRACTED 7/31/81
INJECTED 8/13/81
D BENZ397 BNSTD414
FACTOR 1000
Neutral Compounds u
4-bromophenyl phenyl ether
bis(2-chloroisopropyl) ether
bis (2-chloroethoxy) methane
hexachlorobutadiene
hexachlorocyclopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodi methyl a mine
N-nitrosodiphenylamine
N-nitrosodi-n-propylamine
bis (2-ethylhexyl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
di-n-octyl phthalate
diethyl phthalate
dimethyl phthalate
benzo(a ) anthracene
benzo(a)pyrene
3,4-benzofluoranthene
b e n z o ( k ) f luoranthene
chrysene
acenaphthylene
anthracene
benzo(gh i )pe ry lene
fluorene
phenanthrene
d i b e n z o ( a , h ) a n t h r a c e n e
indeno( 1,2,3-cd )pyrene
pyrene ^^ww-^'-^Q-
g/1
N D
ND
ND
W
HD-^e—JtiD<ss<^ND
ND
ND
ND
N D
*
ND
*
N D
ND
ND
NDND
ND
N DN DNON D
N nNnN D
40B 4-chlorophenyl phenyl ether ND 129B 2,3,7,8-tetrachlorodibenzo-rtr-<jiogQ04
p-dioxin______________________ND
WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
SAMP
LAB
DATE
STD
CONC
Volat
2V
3V
4V
6V
7V
10V
11V
13V
14V
15V
16V
)imXX»XX^KX^)^WX)^X<XiXXXXXXXXXXX
19V
23V
29V
30V
32V
33V38V44V
45V
46V
47V
48V
49V
50V
51V85V
86V
87V
88V
LE ID LAB B L A N K
ID 21881V1
I N J E C T E D 8/5/81
ID BFB34 VOA156r- APTTIP
;iles
acrolein
acrylonitrile
benzene
carbon tetrachloride
chlorobenzene
1,2-dichloroethane
1,1,1-trichloroethane
1,1-dichloroethane
1,1,2-t.richloroethane
1,1,2,2-tetrachloroethane
chloroethane
2-chloroethylvinyl ether
chloroform
1,1-dichloroethylene
1,2-trans-dichloroethylene
1,2-dichloropropane
1,3-dichloropropylene
ethylbenzene
methylene chloride
methyl chloride
methyl bromide
bromoform
dichlorobromome thane
trichlorofluoro methane
die hlorodifluorome thane
chlorodibromomethane
tetrachloroethvlene
toluene
trichloroethylene
vinyl chloride
-
ug/1
ND
ND
ND
ND
N D
N D
ND
N D
N D
N D
ND
ND
ND
ND
ND
ND
N D
ND
19
ND
N D
ND
ND
ND 113P
ND
ND*
ND
N D
ND
SAMP
LAB
DATE
DATE
STD
CONC
Pesti
89P
90P
91P
92P
93P
94P
95P
96P
97P
98P
99P
100P
101P
102P
103P
104P
105P
106P
107P
108P
109P
HOP
HIP
112P
* = I
( p e
ND =-,',- •;';• ^
LE ID METHOD BLANK
ID TRACE #4142
EXTRACTED 7/31/81
INJECTED 8/6/81
ID TRACE M140
. FACTOR 100
cides
aldrin
dieldrin
chlordane
4 , 4 ' - D D T
4 , 4 ' - D D E
4 , 4 ' - D D D
alpha-endosulfan
beta-endosulfan
endosulfan sulfate
endrin
endrin aldehyde
heptachlor
heptachlor epoxide
alpha-BHC
beta-BHC
'gamma-BHC
delta-BHC
PCB-1242
PCB-1254
PCB-1221
. PCB-1232
PCB-1248
PCB-1260
PCB-1016
toxaphene
.ess than 10 ug/1
'sticides less than 5 ug/D
Not detected n^-i f\'\) i JL\}i\Not confirmed by GCMS
071
ug/1
ND
ND
ND
^D
^D
^ND
9D0
N D
ND
N D
N D
N D
ND
ND
ND
ND
N D
N D
N D
ND
ND
N D
N D
N D
N D
rt5t4-f
06005
WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3
QC Report No: 36Sample Number
LAB BLANK
A. SURROGATE SPIKE RESULTS
COMPOUND
Benzene - d6
l-Chloro-2-Bromopropane
Toluene - d8
2-Fluorophenol
Phenol - d5
Nitrobenzene - d5
2-Fluorobiphenyl
Naphthalene-DS
Fraction
VOA
VOA
VOA
ACID
ACID
B/N
B/N
B/N
Cone.(ug/1)
43 l
42
45
66
79
46
55
54
(Surrogates only)Spike
Added (uq /1)
50
50
50
100
103
1 0 1
1 0 1
101
%Recovery
86
84
90
66
77
45 ^0
54 "-————^&-
53
B . TENTATIVELY IDENTIFIED COMPOUNDS
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
1 1 .
12.
13.
14.
15 .
16.
17.
18.
19.
20.
CAS # COMPOUND NAME FRACTION
% Maximum Score Attained
Mass Matching Routine: FIT(specify)
OW^sK-^
07106006
IA/-.V ^ [ l i l r iO fprritn<; C^l i f^rni - on-Til nn "•.OPT
•UPlNTITfiTION REPORT F ILE; 21SS1B2
flTfl: 21881B2.TI3/-13/S1 10:47:80UMPLE: F053G - LflB BLftNK
;ONDS. : E^T/Z. 1 /S 1 CF=l!230"ORMUI. 0 : P1^7"?'13'* TN^TPi'rcMT: F ' ' WJSr-lITT?:^ r'.': '"'":•'.;'14 nNF.LYST- nT "47?
i-lOUMT-F;'7';;"! •••: F'EF.l':M'•;T.•/(F•ErF.l•',REl"!:•'; RE';P.F?;CT?
1.if- •'ni-iT' ''" ('"'"iia
1-~-
\0
00
07106007
oyiogeib-
NO NAME.43 NfiFHTTOLENE CS•4'3 UHKriCU;-;50 Uni Cl,;;.;
Tirc23:43
REF RRT r ETH1 3.000 ft BB
flRER ^r-'^L'NT ";TOT''?^^^'tn;7 —r'^ '"^'^n f fi^ /t < - ,^-^1^-'^'-'-^ • ^•C-','JU^i L_li_]/ L, I 1 ,(,'-—
0.437 l"! FE
00
00
'S: 14 1 P.F?? ft [-•-
^^ n - b tL- ^^tAx^c^a
NO R E T C L ) P1TTIO RRT(L) RATIO RNMT l"smT(L) R . F P C R.F'"-:rL) PRTIO1 2B;40 I . eO 1.000 1.05 30.00 30.00 1.1:33 1 . D C Q 1.133
9
1011 10:35 0.97 0.512 P."? 7.64 75.!""? I.C.-'O 0.335 '?,'-a12131415161713ISSO21-)-'^'^i—3324 1S;E2 1.S1 G.S~2 I .e i 1.3S ZO.1''" O.e^S '~1.??Q 3 ,G5':5?b:7^0.,u
:93031 22:32 1 .P3 l.B?B 1.0° 1.54 30.C3 3.E?S I.;;'?'? ^.':53233343536373S39404112
C^
\0
00
i-" „ i'"' ' i"f <"' •''"""''' '1 r^'' /~''' ^~''~' ''"' i i"'
07106009
-<mo%rr
81280.
PATA: 21881B2 R lBIC68/13/81 10-.47:e9SAMPLE; FG536 - LAB BLAESKRANGE: G 1,1909 LABEL: 11
m 2 3
SCA^S 50 TO E 7 ?C/Ai: F672331 H
0, 4.9 Q'JAt-t: A 0. 1 .0 BASE: U 20, 3
401
\^- ./- \^. 315 353 ! i 433 . ,, (-1— c - ,-: nTt-";^ 9 ft-, f-v'i oc^^^•w'' • ~^>- --,. -,,,. ,-> ,_\, \^_i\ »'i' :j ~)-'.^> „ •- ^ _.;-' ••'w U'l.^S'k, -..'s'-- - .—J ';-" :L"l-i'
6C3469-k , ^ , . T,
SCANTTKT7
DUAL HASS SFECTPJJH68/13/81 10:47:63 + 10:17SAS1PLE; FC535 - LAR ELA'^KEt-IH^KED (S !53 2H GT)
DATA: 21831B2 RIS9CALI: FC723C1 ;/!
BASE It/E: f;3/ 1.:-;'EIC: 71.^5./ f 55.
_,_^,_ .."T
!'I „.
0 0 1 6 2 1
DUAL «ASS SFECTEUn68/13/81 ie:47:69 + IS: HSAHPLE; FC53S - LAB BLAKKENHANCED <S 15B 2E1 87)
BATA: 2183152 ^^3 BASH n/5: I-;;?/ -:'C/.LI: FC723ol 1:1 EIC: 7 '^ . / :.;79.
T ~~ -r ""'—-T—T— T-H/E ^ ?C" 159
_i_._L__J__J__L_'_ i- I i I I I i I i_.J__\_..I_i i i_^i, .. i_ . '
0 0 1 6 2 2
DUAL MASS STECTElf:!e8/!3/81 10:-17:63 + 22:33SAnPLE: F':33S - LAS rLAt:KEHHA':CE3 (S 153 W GT)
DA7A; 2i83[B2 ^^33CALI: FC7233! (:!
BASE S'/E: i1..?/ I - . : 'RIC: 121.5. / ' • 8 7 .
^( ; / ^^A '
""T——r"
0 0 1 6 2 5
^ WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3
QC Report No:, 36Sample Number
F0571 Cont.
A. SURROGATE S P I K E RESULTS
COMPOUND
Benzene - d6
l-Chloro-2-Bromopropans
Toluene - d8
2-Fluorophenol
Phenol - d5
Nitrobenzene - d5
2-Fluorobiphenyl
Naphthalene-DS
Fraction
VOA
VOA
VOA
ACID
ACID
B/N
B/N
B/N
C o n e . ( u g / 1 )
(Surrogates on ly)Spike
Added (ug /1 )%
Recovery
e^—————CM-
\0
0
B . TENTATIVELY IDENTIFIED COMPOUNDS
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
1 1 .
12 .
13.
14.
15 .
16.
17.
18.
19.
20.
CAS # COMPOUND NAME
CHLOROPHENOL
TRICHLOROMETHOXY-
BENZENE
UNKNOWN
HYDROCARBON
HYDROCARBON
HYDROCARBON
HYDROCARBON
FRACTION
B/N # 2 1 3
B/N #301
B/N #334
B/N #456
B/N #489
B/N #509
B/N # 5 1 8
% Maximum Score Attained
Mass Matching Routine: FIT(specify)
GENERAL FIT
GENERAL FIT
NO GOOD FIT
GENERAL FIT
GENERAL FIT
GENERAL FIT
GENERAL FIT
'
(mn^ni.i
- » •0^-1 /»r;'i-"''?^l- - —4 Jl.O.'-.b .tJ^
WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3
QC Report No: 36Sample Number
F0571
A. SURROGATE SPIKE RESULTS
COMPOUND
Benzene - d6
l-Chloro-2-Broniopropane
Toluene - d8
2-Fluorophenol
Phenol - d5
Nitrobenzene - d5
2-FluorobiphenyJL
Naphtha 1ene-D8
Fraction
VOA
VOA
VOA
ACID
ACID
B/N
B/N
B/N
Conc.(ug/1)
54
42
54
50
75
105
91
88
(Surrogates only)Spike
Added (ug/1)
50
50
50
100
103
101
101
101
%Recovery
108
84
108
50 IT
73 C\
104 ^
90. ^
87 c
B. TENTATIVELY IDENTIFIED COMPOUNDS
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.
17.
18.
19.
20.
CAS % COMPOUND NAME
ACETONE
2-METHYLPROPANAL
BUTANAL
PENTANE
CYCLOHEXANE
1-BUTANOL
3-METHYLHEXANE
2-METHYLHEXANE
4-CHLOROPHENOL
UNKNOWN
',4,5-TRICHLOROPHENOL
4.5-DICHLORO-2-METHOXY
PHENOL
DICHLOROPHENOL
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
CHLORO-METHYL-BENZENE
2-ETHYL-1-HEXANOL
FRACTION
VOA #88VOA #135
VOA #158
VOA #184
VOA #193
VOA #208
VOA #337
VOA #346
ACID #92
ACID #194
ACID #208
ACID #229
ACID #265
ACID #287
AICD # 3 1 9
ACID #454
B/N #47
B/N #106
B/N #126
% Maximum Score Attained
Mass Matching Routine: FIT(specify)
965
874
983
935
987
973
985
990
792
NO GOOD FIT
696
935
GENERAL FIT
NO GOOD FIT
NO GOOD FIT
NO GOOD FIT
NO GOOD FIT
GENERAL FIT lUbUlt
963 0^3-0^24
r>r r.,l,r.r,-. ».«.'-.. .• c;||jfr.n ramtn<!. C.-llifrirni-l "0701 ?n fa^.gff^f
WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
SAMP
LAB
DATE
STD •
CONC
Volat
2V
3V
4V
6V
7V
10V
11V
13V
14V
15V
l6V
m^nw^u^wwwJW^mwuwunn19V
23V
29V
30V
32V
33V
38V
44V
45V
46V
47V
48V
49V
50V
51V
85V
86V
87V
88V
LE ID F0571
ID 21881V18 & 21i
INJECTED 8/6/81
ID BFB36 VOA157
« rA'^.i 'JK
iles
acrolein
acrylonitrile
benzene
carbon tetrachloride
chlorobenzene
1,2-dichloroethane
1,1,1-trichloroethane
1,1-dichloroethane
1,1,2-trichloroethane
1,1,2,2-tetrachloroethane
chloroethane
2-chloroethylvinyl ether
chloroform
1,1-dichloroethylene
1,2-trans-dichloroethylene
1,2-dichloropropane
1,3-dichloropropylene
ethylbenzene
methylene chloride
methyl chloride
methyl bromide
bromoform
dichlorobromo methane
trichlorofluoro methane
dichlorodifluoromethane
chlorodibromomethane
tetrachloroethylene
toluene
trichloroethylene
vinyl chloride
381V19
ug/1
ND
NO
124
ND
*
ND
ND
N D
ND
ND
ND
ND*
*
ND
ND
ND*
13
ND
ND
ND
ND
ND
ND
ND
ND
270QO*
ND
SAMPI
LAB I
DATE
DATE
STD I
CONC.
Pestic
89P
90P
91P
92P
93P
94P
95P
96P
97P
98P
99P
100P
101P
102P
103P
104P
105P106P
107P
108P
109P
HOP
111P
112P
113P
* = L
(pe
ND =* * ^
VOA ND =
-E ID F0571
D TRACE #4158
EXTRACTED 7/31/81
INJECTED 8/7/81
D TRACE #4156
FACTOR 100
tides
aldrin
dieldrin
chlordane
4,4 ' -DDT
4,4 ' -DDE
4.4 ' -DDD
alpha-endosulfan
beta-endosulfan
endosulfan sulfate
endrin
endrin aldehyde
heptachlor
heptachlor epoxide
alpha-BHC
beta-BHC
gamma-BHC
delta-BHC
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
toxaphene
ess than 10 ug/1
sticides less than 5 ug/1)
Not detected
Not confirmed by GCMS
less than 2 ug/1 fvy&^w
ug/1
ND
ND
^^
N§^
——————Q-
1
N D
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
N D
NO
ND
NOND
ND
N D
(W06oi6
-K25
WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
SAMP
LAB
DATE
DATE
STD :
CONC
Acid
21A
22A
24A
31A
34A
57A
58A
59A
60A
64A
65A
Base/
1B
5B
8B
9B
12B
18B
20B
25B
26B
27B
28B
35B
36B
37B
39B
40B
LE ID F0571
ID 21881A11 & 21881A12
EXTRACTED 8/1/81
INJECTED 8/10/81
ID SENS177 PHEN354
FACTOR 1000 & 20
Compounds
2,4,6-trichlorophenol
p-chloro-m-cresol
2-chlorophenol
2,4-dichlorophenol
2,4-dimethylphenol
2-nitrophenol
4-nitrophenol
2,4-dinitrophenol
4,6-dinitro-o-cresol
pentachlorophenol
phenol
•^Neutral Compounds
acenaphthene
benzidine
1,2,4-trichlorobenzene
hexachlorobenzene
hexachloroethane
bis(2-chloroethyl)ether
2-chloronapthalene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
3,3'-dichlorobenzidine
2,4-dinitrotoluene
2,6-dinitrotoluene
1,2-diphenylhydrazine
(as azobenzene)
fluoranthene
4-chlorophenyl phenyl ether ND
ug/1
2400
ND
4000
14000
ND
ND
ND
NDND
ND
1200
ND
ND
33
ND
ND
ND
ND*
ND*
ND
NDND
NnND
SAMP
LAB
DATE
DATE
STD
CONC
Base/Neutral Compounds u;
41B
42B
43B
52B
53B54B
55B56B
61B
62 B
63B
66 B
67B
68B
69B70B
71B72B
73B
74B
75B
76B
77B
78B79B80B
81B
82B
83B
84B
129B
p-dic
LE ID F0571
ID 21881B12
EXTRACTED 7/31/81
INJECTED 8/21/81
ID BENZ401 BNSTD418
FACTOR 1000
4-bromophenyl phenyl ether
bis(2-chloroisopropyl) ether
bis (2-chloroethoxy) methane
hexachlorobutadiene
hexachlorocyclopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodimethylamine
N-nitrosodiphenylamine
N-nitrosodi-n-propylamine
bis (2-ethylhexyl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
di-n-octyl phthalate
diethyl phthalate
dimethyl phthalate
benzo(a) anthracene
benzo(a)pyrene
3,4-benzofluoranthene
benzo(k)f luoranthene
chrysene
acenaphthylene
anthracene
benzo(ghi)perylene
fluorene
phenanthrene
dibenzo(a ,h)an thracene
indeno( 1,2,3-cd)]3yr,ene,,^ (T/106U-17
pyrene
2,3,7,8-tetrachlorodiben£b'?K^
>xin
g/1
ND
ND
ND
ND
N D r-N D ^
ND'0
NDQ
NDO
ND
ND
17*
*
*
*
ND
ND
ND
ND
N D
ND
ND
N D
ND
N D
NnNnNnND
^t2G~
ND
ORGANICS TRAFFIC REPORT3) Sample Type: (Check One)
—— RunOtf
Well
Receiving Water
Leachate
Effluent
. Ofher (specify)
Attn:
Regional Office:npling Personnel:
(j) Mark Volume Level on Sample Bottle
; i •• /'••••^ ^ /. ! i 'J ,/•/•'•€-
(Name).-• 7 / / Extradable
DateSampled
(D AncdysisLab:Rec'dby: / ^ ^v^^sm.Date/Time Rec'd ^//^ //^ah
Sample Condition on ReceipN(eg. broken, no ice, Chain-of-Custoay-etc.)
(Phone)
mphng Date:Extractable
(W ret J^ed. OTuJwiMw{, CJLULtoalLu, ftt^J^JUk.•tf^M ^e nJb, rrvtTAfJl
Begin) (End)Extiactable
3 Shipping Information Extradable
,1 VOAUnpreserved
Name o( Shipper:VOA Unpreserved(Duplicate)
Date Shipped:
Airbill Number:
T) Description of Sample Location:
® Special Handling Instructions:(e g.. safety prr'caununs, hi,curcioua nature)
07106018
LAB COPY FOR RETURN TO SMO
BSD ORGANICS TRAFFIC REPORT IMtrrq(T) Case Number
.^^
Sample Site Name/Code:
@ Regional Office:Sampling Personnel:
f - , ' ) , - • • / '. • .-'. . . ; . , f ,1 / , / < ^ / / / ' / < ,••;.//••/(Name)
.."0 < "•" 7! - i ? I(Phone)
Sampling Date::' ' /' "/ .'•...--• f
(Begin) (End)
(J) Shipping Infonnation
7'.. .T^...,-' Name of Shipper
Date Shipped-'
» .— •— ~ -T• - : ' . ' * ^ > ,' '\
Aubill Number:
(7) Description of Sample Location:
'/ - • • ' / ^ -^
(^) Special Handling Instructions:(ea,, aaiety precautions, haaardousnuturB)
07106019» ^
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Somple Condition on Beoeipt(e.g. broken, no ice, Chain-ofOistody, etc.)
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ORGANICS TRAFnC REPORTSample Number
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Sample Site Name/Cede:
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(Name)
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Sampling Date:Extractable
DateSampled
(J) Analysis Lab:Rec'dby: ^i^ ^ ^iOUDate/TimeRec'd •7/3/^ //»7
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(6) Shipping Intormation Extractable
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PO Box818.A!».y.md™,Vinwin2231^-7Cl3 557.2490'FTS 557-2490
ORGANICS TRAFnC REPORTSample Number
F 0567
©Case Number:s^-o
Somple Site Name /Code:
©
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— RunOff
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(Name)
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Sampling Date:Extractable
DateSampled
?-.,• -/ • I/
(J) Analysis Lab: ^Reed by: A^* ^ f »Date/rime Rec'd / //^
Sample Condition on Beceipt(e.g. broken, no ice, Chain-ofOistody, etc.)
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VOA Unpreserved
Name ot ShipperVOAUnpreserved(Duplicate)
Date Shipped:
Airbill Number
(7) Description of Sample Location:
./ '
(J) Special Handling Instructions:(e i;., safety precautions, hciairdous notui'e) 07106021
U.S. ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office }PaBcx8l3.A^xan.^i.V^nra<-i22313 703 b57^.4'JO-t-TS -W 2.190 \
ORGANICS TRAFnC REPORT© Case Number:
.cs'c?
Sample Site Name /Code:
©2) Sample Type: (Check One)
— RunOff
WeH
Receiving Water
Leachate
Effluent
Ofher (specify)
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Sampling Personnel;
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(j) Mark Volume Level on Sample Botfle
DateSampled
(Name)
^ - -^/Extractable
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Sample Conditional Receipt(eg. broken, no ice, Chain-of-Custody, e
0. ..(Phone)
Sampling Date:Extractable
(Begin) (End)Extractable
(^) Shipping Information Extractable
"T' / VOA Unpreserved
Name of ShipperVOA Unpreserved(Duplicate)
Date Shipped:
.- ,A ,.—" ^ --, —'' .-'• -1 3 / -?
Airbill Number
(7) Description of Sample Location:
® Special Handling Instructions:(e.g., anfety precautions, h<,-!znrdous nature)
I An ^~-r~'nv T-^M-. •
o^o^^T"07106022
U.S. ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office557 -2490 •FTS 557-2490
ORGANICS TRAFFIC REPORTSample Number
Sample Site Name/Code:
(?) Sample Type: (Check One)
—— RunOif
^S- Well
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——— Leachate
—— Effluent
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Date/Time Rec'd ^ft' ^^
Sample Condition on Receipt(e.g. broken, no ice, Chain-of-fiystody, etc.)
(Phone)
Sampling Date:Extractable
(Begin) (End)Extractable
(6) Shipping Information Extractable
VOA Unpreserved
Name of Shipper:VOA Unpreserved(Duplicate)
Date Shipped:
Airbill Number.
(T) Description of Sample Looation:
® Special HandUng Instructions:(eg., sulcty pnscautions, hcizardous natiire)
T ^ n f^/^PV r'/ o r'T~"-r m^r 'T\- i
wwsesz-^07106023
U.S. ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management OfficeP.O Ecx8i8 AieKTn'Inci.Vir-iini.'i;^!^ . ".":• '-^•-^ffl-F'lS 55774^)
ORGANICS TRAFnC REPORTSample Number >
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— RunOff
WeU
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Leachate
Effluent
Other (spedfy)
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(Name)^7/ J'// - .' 7r-/ Extractable
(Phone)
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Sampling Date:• /. 'C / ~a~
(Begin) (End)Extractable
(J) Shipping Information Extractable
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^^ -J / i
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^<1-0^105^33—
07106024i ^ R r^uv mp Rrrr TPM TV-^ CM^I
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ORGANICS TRAFnC REPORTSample Number
F 0571
0 Case Number:
5^0_©
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2) Sample Type: (Check One)
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(Phone)
Sampling Date:Extractable
(Begin) (End)ExtractaHe
(6) Shipping Information Extractable
/ •? VOAUnpreserved
Name of Shipper:VOAUnpreserved(Duplicate)
Date Shipped:
Airbill Number
: (7) Description of Sample Location:
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I AR (-OPY FOR RF-n fRN TO ?MO
(3<1_—
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07106025
ORGANICS TRAFFIC REPORT(T) Case Number:
^
Sample Site Name/Code:
JL
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• ^ l f ] - - S i St-^t
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Name of Shipper:
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VOAUnpreserved(Duplicate)
Date Shipped:
Airbill Number
(7) Description of Sample Location:
Lab ^t^^
\J[) Special Handling Instructions:(e.g., safety precautions, hazardous nature)
REGIONAL OFFICE FILE COPY
bample No: t-UbbbLab Standard ID:
TRACE Ml 52 & 4153
STD I . D . TRACE #4151
U . S . ENVIRONMENTAL PROTECTION AGENCY
HWI SAMPLE MANAGEMENT OFFICE
QUALITY CONTROL REPORTB. DUPLICATE ANALYSIS
Lab Mame-.HEST COAST TECHNICAL SERVICE. INC.Report No:______^fi________Page 5___ of ___5_____
0<l
Ss
ft
:OMPOUNO (including surroqates)
P. P. %
<i
\
\
<
^his'QC Report also covers the following sample numbers: F0535. F0536, F0564-F0571. C0592-C0596, G0360-G0364i ., 00 4-^—3—Z————
4
3
k
«»^
S——3..
\
4 V
COMPOUND NAME
METHYLENE CHLORIDE
BENZENE-D6
1-CHLORO-2-BROMOPROPANE
TOLUENE-D8
PESTICIDES NONE DETECTED
CONCENTRATION (uq /1 )
Aliquot 1 (D,)
20
49
44
46
ND
Aliquot 2 (D^)
19
49
45
48
ND
Relative PercentDifference
(RPD)*
5
0
2
4
0
(D, - OJ*RPD = - , 1 — 2 X 100pnpn)^^
Ldu JLdilualu m. V U A 1 5 0 I KrtLL t f 4 1 b U
STD I.D.; TRACE #4159HMI SAMPLE MANAGEMENT OFFICE Report No:
Page 4 of
QUALITY CONTROL REPORTA. MATRIX SPIKE ANALYSIS
0lk^^
^cM
COMPOUND (including surrogates)
P. P. #
- . . „ „ „ . , ^, y.ii . - . i .-...-L - rnR^K cnRQC cncc/1 cnK7i rr>CQO rncoc fnicn nnic/i
4
0
8
0
4
4
6
7
V
V
V
V
COMPOUND NAME
METHYLENE CHLORIDE
BENZENE
TOLUENE
CHLOROBENZENE
BENZENE-06
1-CHLORO-2-BROMOPROPANE
TOLUENE-08
HEPTACHLOR
ALDRIN
DIELDRIN
4,4 ' -DOT
SampleResult (SR)
20
ND
NO
NO
49
44
46
ND
NO
ND
ND
CONCENTRATION (ug/1)Spiked SampleResult (SSR)
21
24
21
46
48
46
51
3.3
2.9
4.4
4.4
SpikeAdded (SA)
0
25
25
25
50
50
50
4.9
5.0
5.0
4.6
%Recovery*
96
84
184
96
92
102
67
58
88
95
0 0 1 6 3 b* Recovery = ^"^ x 100
(SA)
^dillple No:_____hUbb4___Lab Standard~TDlPHEN353
U.S. ENVIRONMENTAL PROTECTION AGENCY
HWI SAMPLE MANAGEMENT OFFICE
QUALITY CONTROL REPORTB. DUPLICATE ANALYSIS
Lab Name:NEST COAST TECHNICAL SERVICE. INC.Report No:____36__________Page 5 of 5_____
i—i<^J
ca-cy;
:OMPOUMD (including surrogates)
P. P. #
6
3
2
c,
1
1
A
A
A
COMPOUND NAME
PHENOL
2,4-DICHLOROPHENOL
2,4.6-TRICHLOROPHENOL
PHENOL-05
DIETHYLPHTHALATE
DI-N-BUTYLPHTHALATE
BIS(2-ETHYLHEXYL)PHTHALATE
1,2,4-TRICHLOROBENZENE
NITROBENZENE D5
2-FLUOROBIPHENYL
NAPHTHALENE D8
2-FLUOROPHENOL
CONCENTRATION (uq/1)
Aliquot 1 (D,)
1
1 4
2
103
1
2
1 1
ND
52
64
59
84
Aliquot 2 (0^)
ND
14
2
109
1
2
8
1
57
67
63
89
Relative PercentDifference
(RPD)*
100
0
0
6
0
0
,32
100
9
5
7
6
This QC Report also covers the following sample numbers: F0535, F0536.-F0564-F0571, C0592-F0596, G0360-G0364———————————————————————______—001 639———————————
*RPD(0^ - D^)
[(TT.-T-D^X 100
Hiu JLauuuiu iu. t^hLllJO-.) HNI SAMPLE MANAGEMENT OFFICE Report No:'Page 4 of
QUALITY CONTROL REPORTA . MATRIX SPIKE ANALYSIS
S<2^0W0u
:OMPOUND (includinq surroqates)
P. P. #
6
3
2
2
2
5
1
1
2
4
A
A
A
A
A
COMPOUND NAME
PHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
PENTACHLOROPHENOL
4-CHLORO-M-CRESOL
2-CHLOROPHENOL
PHENOL-Df)
4-NTTROPHFNOI
2-FLUOROPHENOL
1.2.4-TRICHLOROBEN7FNE
ACENAPHTHFNE
2.6-DINITROTOLUENE
DI-N-BUTYLPHTHALATE
PYRENE
N-NITROSO-DI-N-PROPYLAMINE
1,4-DICHLOROBENZENE
NITROBENZENE
2-FLUOROBIPHENYl
NAPHTHALENE D8
SampleResult (SR)
1
1 4
2
ND
ND
ND
103
ND
84
ND
ND
ND
2
ND
ND
ND
52
64
59
.
CONCENTRATION (uq/1)Spiked SampleResult (SSR)
27
9
ND
24
23
29
65
737
53
32
37
35
6
32
27
30
67
69
67
SpikeAdded (SA)
52
-
-
52
51
54
103
536
100
51
51
50
53
50
51
51
101
101
101
%Recovery*
50
-
46
45
54
63
138
53
63
73
70
8
64
53
59
66
68
66
This QC Report also covers the following sample numbers: F0535' F0536' F0564-F0571, C0592-C0596, G0360-G0364
0 0 1 6 4 0* Recovery - (SSR-SR) , IQO W^^-
(SA)
saagi
SAMt
LAB
DATE
STD
CONC
Vola-
2V
3V
4V
6V
7V
10V
11V
13V
14V
15V
16V
n^mmwmiMw^mmwwnnmn19V23V
29V
30V
32V
33V
38V
44V
45V
46V
47V
48V
49V
50V
51V
85V
86V
87V
88V
Ul WEST COAST T€CHNICAL
'LE ID LAB BLANK
ID 21881V14
; INJECTED 8/6/81
ID BFB36 VOA157
:. FACTOR ————--
tiles
acrolein
acrylonitrile
benzene
carbon tetrachloride
chlorobenzene
1,2-dichloroethane
1,1,1-trichloroethane
1,1-dichloroethane
1,1,2-trichloroethane
1,1,2,2-tetrachloroethane
chloroethane
2-chloroethylvinyl ether
chloroform
1,1-dichloroethylene
1,2-trans-dichloroethylene
1,2-dichloropropane
1,3-dichloropropylene
ethylbenzene
methylene chloride
methyl chloride
methyl bromide -
bromoform
dichlorobromo methane
trichlorofluoromethane
dichlorodifluoromethane
chlorodibromomethane
tetrachloroethylene
toluene
trichloroethylene
vinyl chloride
SERVI
ug/1
NO
,NDND
ND
ND
ND
. ND
NDNnND
Nn
ND
ND
ND
ND
ND
ND
ND
14
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
C61NC
SAM!
LAB
DAT!
DAT!
STD
CON(
Pest
89P
90P
91P
92P
93P
94P
95P
96P
97P
98P
99P
100P
101P
102P
103P
104P
105P
106P
107P
108P
109P
HOP
HIP
112P
113P
* =
(PND =** ^
. INDUSTRIAL CATEGORY
^E ID NO SAMPLE
ID
; EXTRACTED
; INJECTED
ID
:. FACTOR
icides
aldrin
dieldrin
chlordane
4,4'-DDT
4,4 '-DDE
4,4'-DDD
alpha-endosulfan
beta-endosulfan
endosulfan sulfate
endrin
endrin aldehyde
heptachlor
heptachlor epoxide
alpha-BHC
beta-BHC
gamma-BHC
delta-BHC
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
toxaphene
Less than 10 ug/1
esticides less than 5 ug/1)
Not detected
Not confirmed by GCMSvr+ifli
ug/1NA
NA
NA
NA
^A
^A
^NA
r^A
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
5032(5^—
17605 Fabrica Way. Suite D Cerritos, Caltfornia 90701 213/921-9831
WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3
QC Report No:_ 36Sample Number
LAB BLANK
A. SURROGATE SPIKE RESULTS
COMPOUND
Benzene - d6
l-Chloro-2-Bromopropane
Toluene - d8
2-Fluorophenol
Phenol - d5
Nitrobenzene - d5
2-Fluorobiphenyl
Naphthalene-DS
Fraction
VOA
VOA
VOA
ACID
ACID
B/N
B/N
B/N
C o n e . ( u g / 1 )
43 I
42
45
66
79
46
55
54
(Surrogates only)Soi ke
Added (uq /1)
50
50
50
100
103
101
101
101
%Recovery
86
84
90
66
77 C\J
45 ^
54 "
53 o
B . TENTATIVELY IDENTIFIED COMPOUNDS0
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
1 1 .
12.
13.
14.
15 .
16.
17.
18.
19.
20.
CAS # COMPOUND NAME FRACTION
% Maximum Score Attained
Mass Matching Routine: FIT(specify)
.
0710603-
0^10^642
i-r-.n', r-,]-ir'rn Wnv Sl i i tpD Cprrjtos. California qf)701 ? 1 3 ' 0 2 1 - 9 8 3 1
SSSf^
SAMP
LAB
DATE
STD •
CONC
Volat
2V
3V
4V
6V
7V
10V
11V
13V
14V
15V
16V
)l»MXXMX^KX»^W©tX^XDOXMDtMiXXXXXXXXXn
19V
23V
29V
30V
32V
33V
38V
44V
45V
46V
47V
48V
49V
50V
51V
85V
86V
87V
88V
a W€ST COAST TECHNICAL
LE ID LAB BLANK
ID 21881V1
INJECTED 8/5/81
ID BFB34 VOA156TrAC""mR
iles
acrolein
acrylonitrile
benzene
carbon tetrachloride
chlorobenzene
1,2-dichloroethane
1,1,1-trichloroethane
1,1-dichloroethane
1,1,2-trichloroethane
1,1,2,2-tetrachloroethane
chloroethane
2-chlorpethylvinyl ether
chloroform
1,1-dichloroethylene
1,2-trans-dichloroethylene
1,2-dichloropropane
1,3-dichloropropylene
ethylbenzene
methylene chloride
methyl chloride
methyl bromide
bromoform
dichlorobromomethane
trichlorofluoromethane
dichlorodifluoromethane
chlorodibromomethane
tetrachloroethylene
toluene
trichloroethylene
vinyl chloride
.SGRVIQ
ug/1
ND
ND
N D
ND
N D
ND
ND
N D '
ND
N D
ND
ND
ND
ND
ND
ND
N D
ND
19
ND
ND
ND
ND
ND
ND
ND*
NDND
ND
E I N C .
SAMP
LAB
DATE
DATE
STD '.
CONC
Pesti.
89P
90P
91P
92P
93P
94P
95P
96P
97P
98P
99P
100P
101P
102P
103P
104P
105P
106P
107P
108P
109P
HOP
HIP
112P
113P
A = I
(p.
ND =•A" '^
INDUSTRIAL CATEGORY
LE ID METHOD BLANK
ID TRACE #4142
EXTRACTED 7/31/81
INJECTED 8/6/81
[D TRACE #4140
. FACTOR 100
cides
aldrin
dieldrin
chlordane
4,4 ' -DDT
4,4 ' -DDE
4,4 ' -DDD
alpha-endosulfan
beta-endosulfan
endosulfan sulfate
endrin
endrin aldehyde
heptachlor
heptachlor epoxide
alpha-BHC
beta-BHC
- gamma-BHC
delta-BHC
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
toxaphene
..ess than 10 ug/1
•sticides less than 5 ug/1)
Not detected 0'«'10
Not confirmed by GCMS
0^102643
,
ug/1
ND
ND
ND
^D
3°^A-/JjD
OStD
^D
ND
N D
N D
N D
ND
ND
ND
ND
ND
ND
N D
ND
ND
ND
ND
N D
ND
6034
^
WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
SAMP
LAB •
DATE
DATE
STD 1
CONC
Acid
21A
22A
24A
31A
34A
SPA
58A
59A
60A
64A
65A
Base/
1B
5B
8B
9B
12B
18B
20B
25B
26B
27B
28B '
35B
36B
37B
39B
40B
LE ID METHOD B L A N K
ID 21881A1
EXTRACTED 8/1/81
INJECTED 8/9/81
;D SENS176 PHEN353
FACTOR 1000
Compounds u,
2,4,6-trichlorophenol
p-chloro-m-cresol
2-chlorophenol
2,4-dichlorophenol
2,4-dimethylphenol
2-nitrophenol
4-nitrophenol
2,4-dinitrophenol
4,6-dinitro-o-cresol
pentachlorophenol
phenol
Neutral Compounds
acenaphthene
benzidine
1,2,4-trichlorobenzene
hexachlorobenzene
hexachloroethane
bis(2-chloroethyl)ether
2-chloronapthalene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
3,3'-dichlorobenzidine
2,4-dinitrotoluene
2,6-dinitrotoluene
1,2-diphenylhydrazine
(as azobenzene)
f luoranthene
4-chlorophenyl phenyl ether
g/1
ND
ND
ND
ND
NONDN D
ND
ND
ND
ND
ND
ND
N D
ND
N D
NDND
ND
N D
ND
ND
ND
ND
NDND
ND
SAMPI
LAB I
DATE
DATE
STD I:
CONC
Base/
41B
42B
43 B
52B
53B
54B
55 B• 56B
61B62B
63B
66B
67B
68B
69B
70B
71B
72B
73B
74B
75B
76B
77B
78B
79B
SOB
81B
82B
83B
84 B
129B
p-dio;
-I
D
E
I
D
F
N.
4-bromophenyl phenyl ether
bis(2-chloroisopropyl) ether
bis (2-chloroethoxy) methane
N-nitrosodi-n-propylamine
bis (2-ethylhexyl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
dl-n-octyl phthala te
diethyl phthalate
dimethyl phthalate
b e n z o ( a ) anthracene
benzo(a)pyrene
3, 4-benzofluoranthene
b e n z o ( k ) f l u o r a n t h e n e
benzo(gh l )pe ry l ene
d i b e n z o ( a , h ) a n t h r a c e n e
indeno( 1,2,3-cd)pyrene N D
pyrene wn f\^n^ii-—i-i—————————u «'.1U<JU«J5—2,3,7,8-tetrachlorodibenzo-
<in QW^Wr
^ ID METHOD B L A N K
21881B1
:XTRACTED 7/31/81
NJECTED 8/13/^1
BENZ397 BNSTD414
'ACTOR 1000
eutral Compounds u
hexachlorobutadiene
hexachlorocyclopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodimethylamine
N-nitrosodiphenylamine
chrysene
acenaphthylene
anthracene
fluorene
phenanthrene
g/1
N D
ND
ND
^
fffi)
Nt)
W<BD
N D
ND
ND
N DND*
ND
*
N D
ND
ND
NDN D
NDN DN DN D
N DNnN D
N D
s-' '
"ND
WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3
QC Report No: 36Sample Number
F0571 Cont.
A. SURROGATE SPIKE RESULTS
COMPOUND
Benzene - d6
l-Chloro-2-Bromopropane
Toluene - d8
2-Fluorophenol
Phenol - d5
Nitrobenzene - d5
2-Fluorobiphenyl
Naphthalene-DS
Fraction
VOA
VOA
VOA
ACID
ACID
B/N
B/N
B/N
Cone.(ug/1)
(Surrogates only)Spike
Added (uq/1)%
Recovery
in«^v0
<-)
B . TENTATIVELY IDENTIFIED COMPOUNDS0
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
1 1 .
12.
13.
14.
15.
16.
17 .
18.
19.
20.
CAS # COMPOUND NAME
CHLOROPHENOL
TRICHLOROMETHOXY-
BENZENE
UNKNOWN
HYDROCARBON
HYDROCARBON
HYDROCARBON
HYDROCARBON
FRACTION
B/N # 2 1 3
B/N #301
B/N #334
B/N #456
B/N #489
B/N #509
B/N # 5 1 8
% Maximum Score Attained
Mass Matching Routine: FIT(specify)
GENERAL FIT
GENERAL FIT
NO GOOD FIT
GENERAL FIT
GENERAL FIT
GENERAL FIT
GENERAL FIT
.
07106036
WW^c^-
~n W,-.v P.ntp 0 Corritn?;. Cnlifornin P0701 p^.-n^ i^i-n '
WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3
QC Report No: 36Sample Number
F0571
A. SURROGATE SPIKE RESULTS
COMPOUND
Benzene - d6
l-Chloro-2-Bromopropane
Toluene - d8
2-Fluorophenol
Phenol - d5
Nitrobenzene - d5
2-Fluorobiphenyl
Naphthalene-DS
Fraction
VOA
VGA
VOA
ACID
ACID
B/N
B/N
B/N
C o n e . ( u g / 1 )
54
42
54
50
75
105
91
88
(Surrogates only)Spike
Added ( u q / 1 )
50
50
50
100
103
101
101
101
%Recovery
108
84
108
50
73 ^0
104 ^
90 \0
87 ^
B . TENTATIVELY IDENTIFIED COMPOUNDS0
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
1 1 .
12.
13.
14.
15 .
16.
17.
18.
19.
20.
CAS # COMPOUND NAME
ACETONE
2-METHYLPROPANAL
BUTANAL
PENTANE
CYCLOHEXANE
1-BUTANOL
3-METHYLHEXANE
2-METHYLHEXANE
4-CHLOROPHENOL
UNKNOWN
',4,5-TRICHLOROPHENOL
4,5-DICHLORO-2-METHOXY
PHENOL
DICHLOROPHENOL
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
CHLORO-METHYL-BENZENE
2-ETHYL-1-HEXANOL
FRACTION
VOA #88
VOA # 1 3 5
VOA # 1 5 8
VOA #184
VOA #193
VOA #208
VOA #337
VOA #346
ACID #92
ACID # 1 9 4
ACID #208
ACID #229
ACID #265
ACID #287
AICD # 3 1 9
ACID #454
B/N #47
B/N # 1 0 6
B/N # 1 2 6
% Maximum Score Attained
Mass Matching Routine: FIT(specify)
965
874
983
935
987
973
985
990
792
NO GOOD FIT
696
935
GENERAL FIT
NO GOOD FIT
NO GOOD FIT
NO GOOD FIT
NO GOOD FIT 071060.37
GENERAL FIT
963 0^^646 c^—
' ' • ,11 .10 n rnrritnr r'-ihfnrnn nnpm in n^i-omi
WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
SAMPLE ID F0571 • SAMPLE ID FQ571
LAB ID 21881V18 & 21881V19 LAB ID TRACE #4158
DATE INJECTED 8/6/81 DATE EXTRACTED 7/31/81
STD ID BFB36 VOA157 DATE INJECTED 8/7/81
CONC. FACTOR ----- STD ID TRACE #4156
Volatiles
2V acrolein
3V acrylonitrile
4V benzene
6V carbon tetrachloride
7V chlorobenzene
10V 1,2-dichloroethane
11V 1,1,1-trichloroethane
13V 1,1-dichloroethane
14V 1,1, 2-trichloroethane
15V 1,1,2,2-tetrachloroethane
l6V chloroethane
)imxx»max^)^3^x)^i)^<mxxxxxxxxx19V 2-chloroethylvinyl ether
23V chloroform
29V 1,1-dichloroethylene
30V 1,2-trans-dichloroethylene
32V 1,2-dichloropropane
33V 1,3-dichloropropylene
38V ethylbenzene
44V methylene chloride
45V methyl chloride
46V methyl bromide
47V bromoform
48V dichlorobromomethane
49V tr ichlorofluoromethane
50V dichlorodifluoromethane
51V chlorodibromomethane
85V tetrachloroethylene
86V toluene
87V trichloroethylene
88V vinyl chloride
ug/1
ND
ND
124
ND
*
ND
ND
N D
ND
N D
ND
N D
*
*
ND
ND
N D*
13
ND
ND
ND
ND
ND
ND
ND
N D
27000*
ND
CONC. FACTOR 100
Pesticides
89P aldrin
90P dieldrin
91P chlordane
92P 4 ,4 ' -DDT
93P 4 ,4 ' -DDE
94P 4 , 4 ' - D D D
95P alpha-endosulfan
9oP beta-endosulfan
97P endosulfan sulfate
98P endrin
99P endrin aldehyde
100P heptachlor
101P heptachlor epoxide
102P alpha-BHC
103P beta-BHC
104P gamma-BHC
105P delta-BHC
106P PCB-1242
107P PCB-1254
108P PCB-1221
109P PCB-1232
HOP PCB-1248
HIP PCB-1260
112P PCB-1016
113P toxaphene
* = Less than 10 ug/1
(pesticides less than 5
ND = Not detected
** = Not confirmed by GC
VOA ND = less than 2 ug/1fWi-9
ug/1
N D
ND
ND
NID~
N^^0
ND
Nto
N<P
ND
N D
N D
N D
ND
ND
N D
ND
ND
ND
N D
ND
ND
ND
N D
N D
N D
ug/1)
^ W106038-i
W€5T COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
SAMP
LAB
DATE
DATE
STD •
CONC
Acid
21A
22A
24A
31A
34A
57A
58A
59A
60A
64A
65A
Base/
1B
5B
8B
9B
12B
18B
20B
25B
26B
27B
28B
35B
36B
37B
39B
40B
LE ID F0571
ID 21881A11 & 21881A12
EXTRACTED 8/1/81
INJECTED 8/10/81
ID SENS177 PHEN354
FACTOR 1000 & 20
Compounds
2,4,6-trichlorophenol
p-chloro-m-cresol
2-chlorophenol
2,4-dichlorophenol
2,4-dimethylphenol
2-nitrophenol
4-nitrophenol
2,4-dinitrophenol
4,6-dinitro-o-cresol
pentachlorophenol
phenol
^Neut ra l Compounds
acenaphthene
benzidine
1,2,4-trichlorobenzene
hexachlorobenzene
hexachloroethane
bis(2-chloroethyl)ether
2-chloronapthalene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
3,3'-dichlorobenzidine
2,4-dinitrotoluene
2,6-dinitrotoluene
1,2-diphenylhydrazine
(as azobenzene)
f luoranthene
4-chlorophenyl phenyl e t h e r N D
ug/1
2400
ND
4000
14000
NO
ND
N D
ND
ND
ND
1200
ND
ND
33
ND
N D
ND
ND*
ND*
ND
NO
ND
NDN D
SAMP
LAB
DATE
DATE
STD •
CONC
Base/
41B
42B
43B
52B
53B
54B
55B56 B
61B
62 B
63 B
66B
67B
68B
69B
70B
71B
72B
73B
74B
75B
76B
77B
78B
79B
80 B
81B
82B
83B
84B
129B
p-dic
LE ID F0571
ID 21881B12
EXTRACTED 7/31/81
INJECTED 8/21/81
ID BENZ401 BNSTD418
FACTOR 1000
''Neutral Compounds u
4-bromophenyl phenyl ether
bis (2-chloroisopropyl) ether
bis (2-chloroethoxy) methane
hexachlorobutadiene
hexachlorocyclopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodi methyl a mine
N-nitrosodiphenylamine
N-nitrosodi-n-propylamine
bis (2-ethylhexyl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
di-n-octyl phthalate
diethyl phthalate
dimethyl phthalate
b e n z o ( a ) anthracene
benzo(a)pyrene
3, 4-benzofluoranthene
benzo (k ) f luoranthene
chrysene
acenaphthylene
anthracene
benzo(gh i )pe ry lene
fluorene
phenanthrene
d ibenzo (a ,h )an th racene
indeno( 1,2,3-cd)pyrene
pyrenen»"(-
2,3,7,8-tetrachlorodibenzo-"—
>xin WW£f^K~
g/1
ND
ND
ND
NEto
ND^
ND^
Nt^
NOD
N D
ND
ND
17•k
*
*
*
ND
ND
ND
NPN D
NDNONDNONnNO
NnN nN D
l06(^
N D
WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3
QC Report No:Sampte Number
F0570
A. SURROGATE S P I K E RESULTS
COMPOUND
Benzene - d6
l-Chloro-2-Bromopropane
Toluene - d8
2-Fluorophenol
Phenol - d5
Nitrobenzene - d5
2-Fluorobiphenyl
Naphthalene-DS
Fraction
VOA
VOA
VOA
ACID
ACID
B/N
B/N
B/N
C o n e . ( u g / 1 )
56
49
52
2
2
62
75
70
(Surrogates only)Spike
Added (ug /1)
50
50
50
100
103
101
101
101
%Recovery
112
98
104
2
2 C
61
74 \
69 <
r\f0
3
B . TENTATIVELY IDENTIFIED COMPOUNDS
1.2.
3.
4.
5.
6.
7.
8.
9.
10.
1 1 .
12.
13 .
14.
15 .
16.
17 .
18.
19.
20.
CAS # COMPOUND NAME
TETRAHYDROFURAN
UNKNOWN
FRACTION
VOA # 1 3 1
VOA #421
% Maximum Score Attained
Mass Matching Routine: FIT(specify)
928
NO GOOD FIT
———————————071060^
c^w^u^——
W€5T COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
SAMP
LAB
DATE
STD •
CONC
Volat
2V
3V
4V
6V
7V
10V
11V
13V
14V
15V
l6V
>imxxmxm»)^)^x^xx^iwomxxxxxxxx19V23V
29V
30V
32V
33V38V44V45V46V
47V
48V
49V
50V51V
85V
86V
87V
88V
LE ID F0570
ID 21881V17
INJECTED 8/6/81
ID BFB36 VOA157f A r'TC^D
iles
acrolein
acrylonitrile
benzene
carbon tetrachloride
chlorobenzene
1,2-dichloroethane
1,1,1-trichloroethane
1,1-dichloroethane
1,1, 2-trichloroethane
1,1,2, 2-tetrachloroethane
chloroethane
2-chloroethylvinyl ether
chloroform
1,1-dichloroethylene
1,2-trans-dichloroethylene
1,2-dichloropropane
1,3-dichloropropylene
ethylbenzene
methylene chloride
methyl chloride
methyl bromide
bromoform
dichlorobromo methane
trichlorofluoromethane
dichlorodifluoromethane
chlorodibromomethane
tetrachloroethylene
toluene
trichloroethylene
vinyl chloride
ug/1
NO
N D
NO
ND
ND
N D
ND
N D
N D
N D
ND
N D
ND
ND
ND
ND
ND
ND
13
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
SAMP
LAB
DATE
DATE
STD :
CONC
Pesti
89P
90P
91P
92P
93P94P
95P96P
97P98P
99P
100P
101P
102P
103P
104P
105P
106P
107P
108P
109P
HOP
HIP
112P
113P
* = 1
( P ^ND =-«- •,': ^
LE ID F057D
ID TRACE N157
EXTRACTED 7/31/81
INJECTED 8/7/81
ID TRACE #4156
. FACTOR 100
cides u
aldrin
dieldrin
chlordane
4,4 ' -DDT
4 , 4 ' - D D E
4 , 4 ' - D D D
alpha-endosulfan
beta-endosulfan
endosulfan sulfate
endrin
endrin aldehyde
heptachlor
heptachlor epoxide
alpha-BHC
beta-BHC
gamma-BHC
delta-BHC
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
toxaphene
-.ess than 10 ug/1
isticides less than 5 ug/1)
Not detected O'HOeNot confirmed by GCMS ," .
(meseso-
g/iND
ND
ND
ND=>
^'sO
ND
ND^>
NCP
ND
N D
N D
N D
ND
ND
N D
ND
N D
N D
N D
ND
ND
ND
N D
N D
N D
;041
WSfSa^.
SAMP
LAB •
DATE
DATE
STD 1
CONC
Acid
21A
22A
24A
31A
34A
SPA
58A
59A
60A
64A
65A
Base/
1B
5B
8B
9B
12B
18B
20B
25B
26B
27B
28B
35B
36B
37B
39B
40B
H W6ST COAST TECHNICAL
LE ID F0570
ID 21881A10
EXTRACTED 8/1/81
INJECTED 8/10/81
:D SENS177 PHEN354
FACTOR 1000
Compounds u
2,4,6-trichlorophenol
p-chloro-m-cresol
2-chlorophenol
2,4-dichlorophenol
2,4-dimethylphenol
2-nitrophenol
4-nitrophenol
2,4-dinitrophenol
4,6-dinitro-o-cresol
pentachlorophenol
phenol
^Neut ra l Compounds
acenaphthene
benzidine
1,2,4-trichlorobenzene
hexachlorobenzene
hexachloroe thane
bis(2-chloroethyl)ether
2-chloronapthalene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
3,3'-dichlorobenzidine
2,4-dinitrotoluene
2,6-dinitrotoluene
1,2-diphenylhydrazine
(as azobenzene)
f luoranthene
4-chlorophenyl phenyl ether
5€F
g/1
NO
ND
ND*
N nNDNnNn'N nNnNn
ND
N D
N D
ND
N D
NDND
NDN H*
N H
ND
NH
NnND
ND
•- p
<vice INC.SAMP
LAB
DATE
DATE
STD ID BENZ398 mSTD415
CONC
Base/Neutral Compounds us
41B
42B
43B
52B
53B
54B
55B
56 B
61B
62 B
63B
66B
67B
68B
69B
70B
71B
72B
73B
74B
75B
76B
77B
78B
79B
80B
81B
82B
83B
84B
129B
p-dio
i",, -1., ^ .--i.i,,
INDUSTRIAL CATEGORY
LE ID F0570
ID 21881B11
EXTRACTED 7/31/81
INJECTED 8/13/81
FACTOR 1000
4-bromophenyl phenyl ether
bis(2-chloroisopropyl) ether
bis (2-chloroethoxy) methane
hexachlorobutadiene
hexachlorocyclopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodi methyl a mine
N-nitrosodiphenylamine
N-nitrosodi-n-p ropy la mine
bis (2-ethylhexyl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
di-n-octyl phthalate
diethyl phthalate
dimethyl phthalate
b e n z o ( a ) anthracene
benzo(a )py rene
3,4-benzofluoranthene
benzo(k ) f luo ran thene
chrysene
acenaphthylene
anthracene
benzo(gh i )pe ry lene
fluorene
phenanthrene
d i b e n z o ( a , h ) a n t h r a c e n e
indeno( 1 ,2,3-cd)pyrene
pyrene
2,3,7,8-tetrachlorodiberyy^Og
xin
.,,^^ ,.,,,gai0^&3r-^^
^iN D
N D
ND
ND^
NanND^
NC^
NDo
ND
ND
ND*
N D*
ND*
ND
N D
ND
NDN D
N DN DN D
N HNnN nN nN nN D
042N D
WeST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3
QC Report No: 36Sample Number
F0569
A. SURROGATE S P I K E RESULTS
COMPOUND
Benzene - d6
l-Chloro-2-Bromopropane
Toluene - d8
2-Fluorophenol
Phenol - d5
Nitrobenzene - d5
2-Fluorobiphenyl
Naphthalene-DS
Fraction
VOA
VOA
VOA
ACID
ACID
B/N
B/N
B/N
C o n e . ( u g / 1 )
48
45
47
0
2
72
81
74
(Surrogates only)Spike
Added ( u g / 1 )
50
50
50
100
103
101
101
101
/,Recovery
96
90
94
0
2 C\J
71 ^
80 \u
73 c
B . TENTATIVELY IDENTIFIED COMPOUNDS
1.2.
3.
4.
5.
6.
7.
8.
9.
10.
1 1 .
12.
13.
14.
15 .
16.
17.
18.
19.
20.
CAS # COMPOUND NAME
TOLUENE
CHLOROBENZENE
TRICHLOROBENZENE
FRACTION
3/N H3
B/N #68
B/N #209
% Maximum Score Attained
Mass Matching Routine: FIT(specify)
999
991
GENERAL FIT
(m06043
. -»
WlOUim'1^————
WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
SAMPLE ID F0569
LAB ID 21881V12 & 21881V16
DATE INJECTED 8/5/81 & 8/6/81
STD ID BFB35 VOA156 & BFB36 VOA157
CONC. FACTOR ---- & 1/10 D i l u t i o n
Volatiles u
2V acrolein
3V acrylonitrile
4V benzene
6V carbon tetrachloride
7V chlorobenzene
10V 1,2-dichloroethane
11V 1,1,1-trtchloroethane
13V 1,1-dichloroethane
14V 1,1,2-trichloroethane
15V 1,1,2,2-tetrachloroethane
l6V chloroethane
)imxxm^m^)^x^x)^-X(Xixxxxxxxxxxx19V 2-chloroethylvinyl ether
23V chloroform
29V 1,1-dichloroethylene
30V 1,2-trans-dichloroethylene
32V 1,2-dichloropropane
33V 1,3-dichloropropylene
38V ethylbenzene
44V methylene chloride
45V methyl chloride
46V methyl bromide
47V bromoform
48V dichlorobromomethane
49V tr ichlorofluoromethane
50V dichlorodifluoromethane
51V chlorodibromomethane
85V tetrachloroethylene
86V toluene
87V trichloroethylene
88V vinyl chloride
LAB ID TRACE #4155
DATE EXTRACTED 7/31/81
g/1
ND
N D*
ND
392
ND
ND
N D
ND
N D
ND
ND
ND
ND
ND
ND
ND
ND
20
ND
ND
ND
ND
ND
ND
ND
ND
16ND
ND
SAMPLE ID F0569
DATE INJECTED 8/7/81
STD ID TRACE #4156
CONC. FACTOR 100
Pesticides
89P aldrin
90P dieldrin
91P chlordane
92P 4 ,4 ' -DDT
93P 4 ,4 ' -DDE
94P 4 ,4 ' -DDD
95P alpha-endosulfan
96P beta-endosulfan
97P endosulfan sulfate
98P endrin
99P endrin aldehyde
100P heptachlor
101P heptachlor epoxide
102P alpha-BHC
103P beta-BHC
104P gamma-BHC
105P delta-BHC
106P PCB-1242
107P PCB-1254
108P PCB-1221
109P PCB-1232
HOP 'PCB-1248
HIP PCB-1260
112P PCB-1016
113P toxaphene
'"" = Less than 10 ug/1
(pesticides less than 5 ug/1)
ND = Not detected ^i
-;.-* ^ ^Q^ confirmed by GCMS
fyTfT
ug/1
ND
ND
ND
NO^
Nl!^
^
ND^
NO
ND
N D
N D
N D
ND
0.1**
0.3**
ND
0.2**
N D
N D
N D
ND
ND
N D
N D
N D
^106044/'?
s'71 1
) WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
E ID F0569
3 21881A9
EXTRACTED 8/1/81
INJECTED 8/9/81
3 SENS176 PHEN353
FACTOR 1000
Compounds
2,4,6-trichlorophenol
p-chloro-m-cresol
2-chlorophenol
2, A-dichlorophenol
2,A-dimethylphenol
2-nitrophenol
^-nitrophenol
2,^-dinitrophenol
4,6-dinttro-o-cresol
pentachlorophenol
phenol
' /Neutral Compounds
acenaphthene
benzidine
1,2,4-trichlorobenzene
hexachlorobenzene
hexachloroethane
bis (2-chloroethyDether
2-chloronapthalene
1,2-dichlorobenzene
1,3-dichlorobenzene
i 1,4-dichlorobenzene
i 3,3 '-dichlorobenzidine
3 2,4-dinitrotoluene
3 2,6-dinitrotoluene
3 1,2-diphenylhydrazine
(as azobenzene)
3 f luoranthene
B 4-chlorophenyl phenyl
ug/1*
ND
ND
21
NOND
NnN0NnN0*
ND
NO
29
ND
ND
ND
ND30
50
493
ND
NnNO
NOND
e t h e r N D
SAMP
LAB
DATE
DATE
STD •
CONC
Base/
41B
42B
43B
52B
53B
54B
55B
56B61B
62B
63B
66B
67B
68B
69 B
70B
71B
72B
73B
74B
75B
76B
77B
78B
79B
SOB
81B
82B
83B
84B
129B
p-dic
LE ID F0569
ID 21881B10 & 21881B13
EXTRACTED 7/31/81
INJECTED 8/13/81 8/21/81
ID BENZ398 BNSTD415/BENZ401 BNSTD418
FACTOR 1000 & 100
Neutral Compounds u;
^-bromophenyl phenyl ether
bis(2-chloroisopropyl) ether
bis (2-chloroethoxy) methane
hexachlorobutadiene
hexachlorocyclopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodi methyl a mine
N-nitrosodiphenylamine
N-nitrosodi-n-p ropy la mine
bis (2-ethylhexyl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
di-n-octyl phthalate
diethyl phthalate
dimethyl phthalate
benzo(a ) anthracene
benzo(a)pyrene
3,4-benzofluoranthene
benzo (k ) f luo ran thene
chrysene
acenaphthylene
anthracene
benzo(ghi )pery lene
fluorene
phenanthrene
d ibenzo (a ,h )an th racene
indeno(1,2 ,3-cd)pyrene
pyrene
2,3,7,8-tetrachlorodibenzo-
,xin -WIO^S^Q
sZlN D
ND
ND
ND
ND
ND
ND
ND
N D,:*
ND*
N D*
ND*
ND
ND
ND
ND
N D
ND
ND
NO
NO
ND
NnNnN HN D
c:
WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
SAMP
LAB
DATE
STD '
CONC
Volat
2V
3V
4V
6V
7V
10V
11V
13V
14V
15V
16V
)imxxM^Km»)^x^xMi^mxxxxxxxxx19V
23V
29V
30V
32V
33V
38V
44V
45V
46V
47V
48V
49V
50V
51V
85V
86V
87V
88V
LE ID F0568
ID 21881V15
INJECTED 8/6/81
ID BFB36 VOA157V A PTnD
iles
acrolein
acrylonitrile
benzene
carbon tetrachloride
chlorobenzene
1,2-dichloroethane
1,1,1-trichloroethane
1,1-dichloroethane
1,1, 2-trichloroethane
1,1, 2,2-tetrachloroethane
chloroethane
2-chloroethylvinyl ether
chloroform
1,1-dichloroethylene
1,2-trans-dichloroethylene
1,2-dichloropropane
1,3-dichloropropylene
ethylbenzene
methylene chloride
methyl chloride
methyl bromide
bromoform
dichlorobromomethane
trichlorofluoromethane
dichlorodifluoromethane
chlorodibromomethane
tetrachloroethylene
toluene
trichloroethylene
vinyl chloride
ug/1
ND
ND
N D
ND
ND
ND
ND
N D
ND
N D
ND
ND
ND
ND
ND
ND
ND
N D13
ND
ND
ND
ND
ND
ND
ND
N D
ND
N D
ND
SAMP
LAB
DATE
DATE
STD
CONC
Pesti
89P
90P
91P
92P
93P94P95P96P
97P
98P
99P
100P
101P
102P
103P
104P
105P
106P
107P
108P
109P
HOP
HIP
112P
113P
* = ]
( p <
ND =
LE ID
ID
EXTRACTED
INJECTED
ID
. FACTOR
cides
aldrin
dieldrin
chlordane
4,4 ' -DDT
4,4 ' -DDE
4 , 4 ' - D D D
alpha-endosulfan
beta-endosulfan
endosulfan
endrin
endrin aldehyde
heptachlor
heptachlor
alpha-BHC
beta-BHC
gamma-BHC
delta-BHC
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
toxaphene
Less than 10
'sticides less
Not detected
Not confirme
F0568
TRACE #4154
7/31/81
8/7/81
TRACE #4151
100
sulfate
epoxide
ug/1
than 5 ug/1)
d by GCMS07106<• /
ug/1
ND
ND
ND
^
^
NiP
ND^
N&>
ND
N D
N D
N D
ND
ND
ND
ND
N D
N D
N D
NOND
ND
ND
ND
N D
347
W€5T COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
SAMP
LAB
DATE
DATE
STD
CONC
Acid
21A
22A
24A
31A
34A
57A
58A
59A
60A
64A
65A
Base,
1B
5B
8B
9B
12B
18B
20B
25B
26B
27B
28B
35B
36B
37B
39B
40B
LE ID F0568
ID 21881A8
EXTRACTED 8/1/81
INJECTED 8/9/81
ID SESN176 PHEN353
FACTOR 1000
Compounds u,
2, 4 , 6-trichlorophenol
p-chloro-m-cresol
2-chlorophenol
2,4-dichlorophenol
2,4-dimethylphenol
2-nitrophenol
4-nitrophenol
2,4-dinitrophenol
4,6-dinitro-o-cresol
pentachlorophenol
phenol
/Neutral Compounds
acenaphthene
benzidine
1,2, 4-trichlorobenzene
hexachlorobenzene
hexachloroethane
bis(2-chloroethyl)ether
2-chloronapthalene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
3,3'-dichlorobenzidine
2,4-dinitrotoluene
2,6-dinitrotoluene
1,2-diphenylhydrazine
(as azobenzene)
f luoranthene
4-chlorophenyl phenyl ether
g/1
*
ND
ND26
ND
ND
ND
ND
NDND
N D
ND
ND
N D
ND
ND
ND
N D
ND
N D
ND
ND
ND
ND
NnND
ND
SAMP
LAB
DATE
DATE
STD
CONC
Base/
41B
42B
43B
52B
53B
54B
55B
56B
61B
62B
63B
66 B
67B68B
69 B
70B
71B
72B
73B
74B
75B
76B
77B
78B
79B
80B
81B
82B
83B
84B
129B
p-dic
LE ID F0568
ID 21881B9
EXTRACTED 7/31/81
INJECTED 8/13/81
ID BENZ398 BNSTD415
FACTOR 1000
Neutral Compounds u j
4-bromophenyl phenyl ether
bis(2-chloroisopropyl) ether
bis (2-chloroethoxy) methane
hexachlorobutadiene
hexachlorocyclopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodi methyl a mine
N-nitrosodiphenylamine
N-nitrosodi-n-propylamine
bis (2-ethylhexyl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
di-n-octyl phthalate
diethyl phthalate
dimethyl phthalate
benzo (a ) anthracene
benzo(a)pyrene
3,4-benzofluoranthene
benzo(k) f luoran thene
chrysene
acenaphthylene
anthracene
benzo(gh i )pe ry l ene
fluorene
phenanthrene
d ibenzo (a ,h ) an th racene
indeno( 1,2,3-cd)pyrene
pyrene ND ^
2,3,7,8-tetrachlorodibenzoy *
>xin
0'ywwy
g/1
N D
ND
ND
^0NDinND^
ND""0
ND^
ND
ND
ND
18
N D*
ND
N D
N D
ND
ND
NDN D
ND
ND
N D
N D
N D
Nn
Nn
N n
ND^ „
WEST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3
QC Report No: 36Sample Number
F0567
A. SURROGATE SPIKE RESULTS
COMPOUND
Benzene - d6
l-Chloro-2-Bromopropane
Toluene - d8
2-Fluorophenol
Phenol - d5
Nitrobenzene - d5
2-Fluorobiphenyl
Naphthalene-DS
Fraction
VOA
VGA
VOA
ACID
ACID
B/N
B/N
B/N
C o n e . ( u q / 1 )
44
43
46
40
2
60
68
60
(Surrogates only)Spike
Added ( u g / 1 )
50
50
50
100
103
101
101
101
%Recovery
88
86
92
40
2 r59 L
67 \
59 '
B . TENTATIVELY IDENTIFIED COMPOUNDS
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
1 1 .
12 .
13.
14.
15.
16.
17.
18.
1 9 .
20.
CAS # COMPOUND NAME
ACETONE
TETRAHYDROFURAN
DICHLOROPHENOL
CHLOROPHENOL
2,4,5^TRICHLOROPHENOL
DICHLOROPHENOL
UNKNOWN
UNKNOWN
2-ETHYL-1-HEXANOL
TRICHLOROMETHOXYBENZENi
UNKNOWN
UNKNOWN
FRACTION
VOA #86
VOA # 1 3 0
ACID #146
ACID # 1 9 6
ACID #207
ACID #264
ACID #492
ACID # 5 1 5
B/N #142
; B/N #296
B/N #324
B/N #330
% Maximum Score Attained
Mass Matching Routine: FIT(specify)
835
993
GENERAL FIT
GENERAL FIT
966
GENERAL FIT
NO GOOD FIT
NO'^GOOD FIT
942
GENERAL FIT
NO'tSOOD FIT
NO GOOD FIT
—————————————071060
C————————W10WSQ——
Alf .» t Ja '4 .
SAMP
LAB
DATE
STD •
CONC
Volat
2V
3V
4V
6V
7V
10V
11V
13V
14V
15V
16V
)imxxmxxmK»)^x^x)4xi)tMixxxxxxxxxxx19V
23V
29V
30V
32V
33V
38V
44V
45V
46V
47V
48V
49V
50V
51V
85V
86V
87V
88V
H WEST COAST TECHNICAL
LE ID F0567
ID 21881V10
INJECTED 8/5/81
ID BFB35 VOA156
. r A^. 1 UK
lies
acrolein
acrylonitrile
benzene
carbon tetrachloride
chlorobenzene
1,2-dichloroethane
1,1,1-trichloroethane
1,1-dichloroethane
1,1,2-trichloroethane
1,1,2,2-tetrachloroethane
chloroethane
2-chloroethylvinyl ether
chloroform
1,1-dichloroethylene
1,2-trans-dichloroethylene
1,2-dichloropropane
1,3-dichloropropylene
ethylbenzene
methylene chloride
methyl chloride
methyl bromide
bromoform
dichlorobromomethane
trichlorofluoromethane
dichlorodifluoromethane
chlorodibromomethane
tetrachloroethylene
toluene
trichloroethylene
vinyl chloride
.56RVK
ug/1
ND
ND
N D
ND
ND
ND
N D
N D
ND
N D
ND
N D
ND
ND
ND
ND
ND
N D
20ND
ND
ND
N D
ND
ND
ND
ND
ND
ND
ND
:6 INC.
SAMP
LAB
DATE
DATE
STD :
CONC
Pesti
89P
90P
91P
92P
93P
94P
95P96P
97P98P
99P
100P
101P
102P
103P
104P
105P
106P
107P
108P
109P
HOP
HIP
112P
113P
* = ]
( P <ND --;.- * ^
INDUSTRIAL CATEGORY
LE ID F0567
ID TRACE #41
EXTRACTED 7/31/81
INJECTED 8/6/81
ID TRACE #41
. FACTOR 100
cides
aldrin
dieldrin
chlordane
4,4 ' -DDT
4,4 ' -DDE
4,4 ' -DDD
alpha-endosulfan
beta-endosulfan
endosulfan sulfate
endrin
endrin aldehyde
heptachlor
heptachlor epoxide
alpha-BHC
beta-BHC
gamma-BHC
delta-BHC
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
toxaphene
l.ess than 10 ug/1
'sticides less than 5 ug/1
Not detected
Not confirmed by GCMS
46
43
ug/1
ND
. ND
ND
N D
ND°——————tf\
NDn
ND-
NtP
ND^
ND
N D
N D
ND
ND
N D
ND
N D
N D
N D
ND
N D
ND
N D
N D
N D
)
07106050
/-''/iy^wse^
213/921-983117605 Fabrics Way. Suite D Cerntos. California 90701
WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
SAMP
LAB '
DATE
DATE
STD I
CONC
Acid
21A
22A
2^A
31A
34A
57A
58A
59A60A
6AA
65A
Base/
1B
5B
8B
9B
12B
l8B
20B
25B
26B
27B
28B
35B
36B
37B
39B
Z^OB
LE ID F0567
CD 21881
EXTRACTED 8/1/8
INJECTED 8/9/8
.D SENS176
FACTOR 1000
Compounds
2,4,6-trichlorophenol
p-chloro-m-cresol
2-chlorophenol
2,4-dichlorophenol
2,4-dimethylphenol
2-nitrophenol
4-nitrophenol
2,4-dinitrophenol
4,6-dinitro-o-cresol
pentachlorophenol
phenol
'Neutral Compounds
acenaphthene
benzidine
1,2,4-trichlorobenzene
hexachlorobenzene
hexachloroethane
bis(2-chloroethyl)ether
2-chloronapthalene
1,2-dichlorobenzene
1,3-dichlorobenzene
1, Zt-dichlorobenzene
3,3'-dichlorobenzidine
2,4-dinitrotoluene
2,6-dinitrotoluene
1,2-diphenylhydrazine
(as azobenzene)
f luoranthene
4-chlorophenyl phenyl
A7
1
1
PHEN353
ug/1
7S
ND
154
153
ND
ND
ND
N0
NnNnNn
ND
ND*
ND
ND
ND
ND
ND
N D
ND
ND
ND
ND
NnND
e t h e r N D
SAMP]
LAB 1
DATE
DATE
STD I
CONC
Base/
41B
42B
43B
52B
53B
54B
55B
56B
61B
62B
63B
66B67B68B
69B
70B
71B
72B
73B
74B
75B
76B
77B
78B
79B
80B
81B
82B
83B
84B
129B
p-dio
.E ID F0567
.D 21881B8
EXTRACTED 7/31/81
INJECTED 8/13/81
D BENZ398 !£NSTD415
FACTOR 1000
Neutral Compounds ui
4-bromophenyl phenyl ether
bis(2-chloroisopropyl) ether
bis (2-chloroethoxy) methane
hexachlorobutadiene
hexachlorocyclopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodimethylamine
N-nitrosodiphenylamine
N-nitrosodi-n-propylamine
bis (2-ethylhexyl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
di-n-octyl phthalate
diethyl phthalate
dimethyl phthalate
benzo(a ) anthracene
benzo(a)pyrene
3,4-benzofluoranthene
benzo(k) f luoran thene
chrysene
acenaphthylene
anthracene
benzo(ghi )pery lene
fluorene
phenanthrene
d ibenzo(a ,h )an th racene
indeno( 1,2,3-cd)pyrene
pyrene
2,3,7,8-tetrachlorodibenzo-
xin
1ND
ND
ND
NDC^
^LHND^o
ND-^-
N D 0
0ND
ND
ND
29
ND
ND
ND
ND
N D
ND
ND
ND
N D
ND
N D
N D
ND
Nn
NnNnNnN D
L06051N D
WEST COAST TECHNICAL S6RVIC6 INC. INDUSTRIAL CATEGORY
SAMP
LAB
DATE
STD
CONC
Volat
2V
3V
4V
6V
7V
10V
11V
13V
14V
15V
16V
>imxxm^Km»)tm^xxsm<Mxxxxxxxxxx19V
23V
29V
30V
32V
33V
38V
44V
45V
46V
47V
48V
49V
50V
51V
85V
86V
87V
88V
LE ID R0566
ID 21881V9
INJECTED 8/5/81
ID BFB35 VOA156 DATE INJECTED 8/6/81
. FACTOR -------
:iles ui
acrolein
acrylonitrile
benzene
carbon tetrachloride
chlorobenzene
1,2-dichloroethane
1,1,1-trichloroethane
1,1-dichloroethane
1,1, 2-trlchloroethane
1,1,2,2-tetrachloroethane
chloroethane
2-chloroethylvinyl ether
chloroform
1,1-dlchloroethylene
1,2-trans-dichloroethylene
1,2-dichloropropane
1,3-dichloropropylene
ethylbenzene
methylene chloride
methyl chloride
methyl bromide
bromoform
dichlorobromo methane
tr ichlorofluoromethane
die hlorodifluorome thane
chlorodibromomethane
tetrachloroethylene
toluene
trichloroethylene
vinyl chloride
17605 Fabrica Way, Suite D
LAB ID TRACE #4145
DATE EXTRACTED 7/31/81
STD ID TRACE #4143
1ND
N D
N D
N D
N D
N D
N D
N D
N D
N D
ND
ND
ND
ND
ND
N D
ND
N D
18
ND
N D
N D
N D
ND
ND
N D
N D
NP
N D
N D
Cen
SAMPLE ID F0566
CONC. FACTOR 100
Pesticides
89P aldrin
90P dieldrin
91P chlordane
92P 4 ,4 ' -DDT
93P 4 , 4 ' - D D E
94P 4 , 4 ' - D D D
95P alpha-endosulfan
96P beta-endosulfan
97P endosulfan sulfate
98P endrin
99P endrin aldehyde
100P heptachlor
101P heptachlor epoxide
102P alpha-BHC
103P beta-BHC
104P gamma-BHC
105P delta-BHC
106P PCB-1242
107P PCB-1254
108P PCB-1221
109P PCB-1232
HOP PCB-1248
HIP PCB-1260
112P PCB-1016
113P toxaphene
* = Less than 10 ug/1
(pesticides less than 5 ug/1)
ND = Not detected
-"-* = Not confirmed by GCMS
0'
(mo^entos. C a l i f o r n i a 90701 213/921-9831
Ug/1
N D
. ND
ND
ND
^——<©•^W-
N9
NV
N D
N D
ND
ND
ND
ND
ND
N D
N D
N D
N D
ND
ND
N D
ND
N D
10^053
^
EST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
i F0566
21881A6
^ACTED 8/1/81
CTED 8/9/81
SENS176 PHEN353
TOR 1000
rounds u'
6-trichlorophenol
iloro-m-cresol
^lorophenol
-dichlorophenol
-dimethylphenol
i.trophenol
itrophenol
-dinitrophenol
-dinitro-o-cresol
.tachlorophenol
"nol
:tral Compounds
^naphthene
^zidine
2,4-trichlorobenzene
xachlorobenzene
<achloroethane
;(2-chloroethyl)ether
:hloronapthalene
2-dichlorobenzene
3-dichlorobenzene
4-dichlorobenzene
3'-dichlorobenzidine
^-dinitrotoluene
6-dlnitrotoluene
2-diphenylhydrazine
is azobenzene)
•Joranthene
-chlorophenyl phenyl ether
g/1
NO
ND
NO
NO
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
N D
ND
ND
ND
ND
NnND
ND
SAMP
LAB
DATE
DATE
STD
CONC
Base,
41B
42B
^3B
52B
53B54B
55 B
56B61B62B
63B
66B67B68B69B
70B
71B
72B
73B
7AB
75B
76B
77B
78B
79BSOB
81B
82B
83B
84B
129B
p-di<
LE ID F0566
ID 21881B7
EXTRACTED 7/31/81
INJECTED 8/13/81
ID BENZ397 BNSTD414
FACTOR 1000
/Neutral Compounds u
4-bromophenyl phenyl ether
bis(2-chloroisopropyl) ether
bis (2-chloroethoxy) methane
hexachlorobutadiene
hexachlorocyclopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodi methyl a mine
N-nitrosodiphenylamine
N-nitrosodi-n-propylamine
bis (2-ethylhexyl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
di-n-octyl phthalate
diethyl phthalate
dimethyl phthalate
benzo(a ) anthracene
benzo(a)pyrene
3,4-benzofluoranthene
benzo(k) f luoranthene
chrysene
acenaphthylene
anthracene
benzo(ghi )pery lene
fluorene
phenanthrene
dibenzo(a ,h)an thracene
indenod, 2,3-cd)pyrene
pyrene
2,3,7,8-tetrachlorodibenzo-
?xin (TW^f^S^
g/1
NDND
ND
ND
ND
ND
ND
ND
ND
ND
ND
12
ND*
ND*
ND
ND
ND
ND
N D
ND
ND
ND
N D
ND
Nn
N DNnN D
i^
iber
only)%
:overy
98
38
52
1
1 ^
i7 ^0
.5 \0
-4 Z
.1. W6ST COAST TECHNICAL
SAMPLE ID F0565
LAB ID 21881V4
DATE INJECTED 8/5/81
STD ID BFB35 VOA156
CONC. FACTOR - ----
Volatiles
2V acrolein
3V acrylonitrile
4V benzene
6V carbon tetrachloride
7V chlorobenzene
10V 1,2-dichloroethane
11V 1,1,1-trichloroethane
13V 1,1-dichloroethane
14V 1,1,2-trichloroethane
15V 1,1,2,2-tetrachloroethane
l6V chloroethane
)imXXM^m^»mWXXiXl^(fXimXXXXXXXX
19V 2-chloroethylvlnyl ether
23V chloroform
29V 1,1-dichloroethylene
30V 1,2-trans-dichloroethylene
32V 1,2-dichloropropane
33V 1,3-dichloropropylene
38V ethylbenzene
44V methylene chloride
45V methyl chloride
46V methyl bromide
47V bromoform
48V dichlorobromomethane
49V tr ichlorofluoromethane
50V dichlorodifluoromethane
51V chlorodibromomethane
85V tetrachloroethylene
86V toluene
87V trichloroethylene
88V vinyl chloride
SERVICE
LAB ID TRACE #4152
DATE EXTRACTED 7/31/81
DATE INJECTED 8/7/81
ug/1
ND
ND
N D
N D .
ND
ND
ND
N D
N D
N D
ND
ND
ND
ND
ND
ND
N D
N D
2D
N D
ND
N D
ND
ND
ND
ND
N D
N D
N D
N D
INC INnU^TRlAl L AT^GQRY
SAMPLE ID F0565
STD ID TRACE #4151
CONC. FACTOR 50
Pesticides u
89P aldrin
90P dieldrin
91P chlordane
92P 4 ,4 ' -DDT
93P 4.4 '-DDE
94P 4 ,4 ' -DDD
95P alpha-endosulfan
96P beta-endosulfan
97P endosulfan sulfate
98P endrin
99P endrin aldehyde
100P heptachlor
101P heptachlor epoxide
102P alpha-BHC
103P beta-BHC
104P gamma-BHC
105P delta-BHC
106P PCB-1242
107P PCB-1254
108P PCB-1221
109P PCB-1232
HOP PCB-1248
HIP PCB-1260
112P PCB-1016
113P toxaphene
* = Less than 10 ug/1
(pesticides less than 5 ug/1)
ND = Not detected
-.'•-* = Not confirmed by GCM&ingQgg
g/1
N D
ND
ND
ND
1^Ww-N^>
N?
N D
N D
N D
ND
ND
ND
ND
ND
N D
N D
ND
ND
ND
ND
ND
ND
17605 Fabnca Way, Suite D Cerntos, California 90701 213/921-9831
W€ST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
SAMP
LAB
DATE
DATE
STD
CONC
Acid
21A
22A
2^A
31A
34A
SPA
58A
59A
60A64A65A
Base,
1B
5B
8B
9B
12B
18B
20B
25B
26B
27B
28B
35B
36B
37B
39B
40B
LE ID F0565
ID 21881A5
EXTRACTED 8/1/81
INJECTED 8/9/81
ID SENS176 PHEN353
FACTOR 1000
Compounds u;
2, , 6-trichlorophenol
p-chloro-m-cresol
2-chlorophenol
2,4-dichlorophenol
2,4-dimethylphenol
2-nitrophenol
4-nitrophenol
2,^-dinitrophenol
4,6-dinitro-o-cresol
pentachlorophenol
phenol
/Neutral Compounds
acenaphthene
benzidine
1,2,/r-trichlorobenzene
hexachlorobenzene
hexachloroethane
bis(2-chloroethyl)ether
2-chloronapthalene
1,2-dichlorobenzene
1,3-dichlorobenzene
1, /t-dichlorobenzene
3,3'-dichlorobenzidine
2, Zt-dinitrotoluene
2,6-dinitrotoluene
1,2-diphenylhydrazine
(as azobenzene)
f luoranthene
4-chlorophenyl phenyl ether
g/1
ND
ND
NONDNDNDND
NnNDNnNn
ND
ND
ND
ND
ND
ND
ND
ND
N DNDND
NnND
NDND
ND
SAMP
LAB
DATE
DATE
STD :
CONC
Base/Neutral Compounds U j
41B
Z»2B
^3B
52B
53B
54B
55B
56B61B62B
63B
66B67B
68B
69B70B
71B
72B
73B
74B
75B
76B
77B
78B
79B
80 B
81B
82B
83B
84B
129B
p-dic
LE ID F0565
ID 21881B6
EXTRACTED 7/31/81
INJECTED 8/13/81
[D BENZ397 BNSTD414
FACTOR 1000
^-bromophenyl phenyl ether
bis(2-chloroisopropyl) ether
bis (2-chloroethoxy) methane
hexachlorobutadiene
hexachlorocyclopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodimethylamine
N-nitrosodiphenylamine
N-nitrosodi-n-propylamine
bis (2-ethylhexyl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
di-n-octyl phthalate
diethyl phthalate
dimethyl phthalate
benzo(a) anthracene
benzo(a)pyrene
3,4-benzofluoranthene
benzo(k)f luoranthene
chrysene
acenaphthylene
anthracene
benzo(ghi)perylene
fluorene
phenanthrene
dibenzo(a ,h)an thracene
indeno( 1,2,3-cd)pyrene
pyrene
2,3,7,8-tetrachlorodibenzo-07j0^)xln nffltf>yfifift
^1N D
ND
ND
ND
N D ^——•<£)ND^n
ND^-
ND 0
ND
ND
ND
10
ND*
ND*
N D
ND
ND
ND
N D
ND
N D
ND
N D
Nn
N nN nNnN D
106057ND
h^.Y ;-';*•'
SAMP
LAB
DATE
STD •
CONC
Volat
2V
3V
4V
6V
7V
10V
11V
13V
14V
15V
16V
)imxxm^Km»)^jWX)^Mixxxxxxxxxxx19V
23V
29V
30V
32V
33V
38V
44V
45V
46V
47V
48V
49V
50V
51V
85V
86V
87V
88V
^ WEST COAST TECHNICAL
LE ID F0564
ID 21881V3
INJECTED 8/5/81
ID BFB35 VOA156T- A f~"rr\'D
lies
acrolein
acrylonitrile
benzene
carbon tetrachloride
chlorobenzene
1,2-dichloroethane
1,1,1-trichloroethane
1,1-dichloroethane
1,1, 2-trichloroethane
1,1,2,2-tetrachloroethane
chloroethane
2-chloroethylvinyl ether
chloroform
1,1-dichloroethylene
1,2-trans-dichloroethylene
1,2-dichloropropane
1,3-dichloropropylene
ethylbenzene
methylene chloride
methyl chloride
methyl bromide
bromoform
dichlorobromomethane
trie hlorofluoro methane
dichlorodifluoromethane
chlorodibromomethane
tetrachloroethylene
toluene
trichloroethylene
vinvl chloride
.S6RVIC
ug/1
ND
ND
N D
ND
N D
N D
ND
N D
ND
N D
ND
ND*
ND
ND
N D
N D
N D
20
ND
ND
ND
ND
ND
ND
ND
10
N D
N D
N D
:(= INC.
SAMP
LAB
DATE
DATE
STD
CONC
Pesti
89P
90P
91P
92P
93P
94P
95P
96P
97P
98P
99P
100P
101P
102P
103P
104P
105P
106P
107P
108P
109P
HOP
HIP
112P
113P
* = 1
( P ^ND =* -A- ^
INDUSTRIA
LE ID
ID
EXTRACTED
INJECTED
ID
. FACTOR
cides
aldrin
dieldrin
chlordane
4 ,4 ' -DDT
4,4 ' -DDE
4 , 4 ' - D D D
alpha-endosulfan
beta-endosulfan
endosulfan
endrin
endrin aldehyde
heptachlor
heptachlor
alpha-BHC
beta-BHC
gamma-BHC
delta-BHC
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
toxaphene
l.ess than 10
isticides less
Not detected
Not confirme
L. i-ATt=(30RY
F0564
TRACE #4144
7/31/81
8/6/81
TRACE N143
50
2.5**
sulfate
epoxide
0.7**
ug/1
than 5 ug/1)
0710<d by GCMS
n^v^fw-ev-a
ug/1
0:1**
N D
1.6**
N^YO
^
o.y*NP
^0.1**
1.0**
N D
ND
0.6**
1.5**
1.8**
ND
N D
ND
ND
ND
N D
N D
N D
5059
17605 Fabnca Way. Suite D Cerntos, California 90701 213/921-9831
WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
SAMP
LAB •
DATE
DATE
STD 1
CONC
Acid
21A
22A
24A
31A
34A
SPA
58A
59A60A
64A
65A
Base/
1B
5B
8B
9B
12B
18B
20B
25B
26B
27B
28B
35B
36B
37B
39B
LOB
LE ID F0564ID 21881A2
EXTRACTED 8/1/81
INJECTED 8/9/81
ID SENS176 PHEN353
FACTOR 1000
Compounds u
2,4,6-trichlorophenol
p-chloro-m-cresol
2-chlorophenol
2,4-dichlorophenol
2,4-dimethylphenol
2-nitrophenol
4-nitrophenol
2,4-dinitrophenol
4,6-dinitro-o-cresol
pentachlorophenol
phenol
Neutral Compounds
acenaphthene
benzidine
1,2,4-trichlorobenzene
hexachlorobenzene
hexachloroethane
bis(2-chloroethyl)ether
2-chloronapthalene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
3,3'-dichlorobenzidine
2,4-dinitrotoluene
2,6-dinitrotoluene
1,2-diphenylhydrazine
(as azobenzene)
fluoranthene
4-chlorophenyl phenyl ether
g/1*
ND
ND
14
ND
ND
N D
ND
ND
ND*
ND
ND
N D
ND
ND
ND
ND
ND
N D
ND
ND
ND
ND
NDND
ND
SAMP
LAB •
DATE
DATE
STD ]
CONC
Base/
41B
42B
43 B
52B
53B
54B
55B
•56B61B62B
63B
66 B67B68B
69B
70B
71B
72B
73B
74B
75B
76B
77B
78B
79B80B
81B
82B
83B
84B
129B
p-dio
LE ID F0564
ID 21881B3
EXTRACTED 7/31/81
INJECTED 8/13/81
^D BENZ397 BNSTD414
FACTOR 1000
''Neutral Compounds u,
4-bromophenyl phenyl ether
bis(2-chloroisopropyl) ether
bis (2-chloroethoxy) methane
hexachlorobutadiene
hexachlorocyclopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodimethylamine
N-nitrosodiphenylamine
N-nitrosodi-n-propylamine
bis (2-ethylhexyl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
di-n-octyl phthalate
.diethyl phthalate
dimethyl phthalate
benzo(a) anthracene
benzo(a)pyrene
3,4-benzofluoranthene
benzo(k) f luoran thene
chrysene
acenaphthylene
anthracene
benzo(ghi)perylene
fluorene
phenanthrene
dibenzo(a ,h)anthracene
indeno( l ,2 ,3-cd)pyrene
pyrene
2,3,7,8-tetrachlorodibenz(9-^H
xin 0' U*5WQ
gZlN D
ND
ND
ND
^ND^
ND--
ND0
N D
ND
ND
11
ND*
ND*
N D
ND
ND
ND
N D
N DN D
N D
ND
ND
N D
N D
N D
N D
96060'ND
WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY
SAMF
LAB
DATE
STD
CONC
Volal
2V
3V
4V
6V
7V
10V
11V
13V
14V
15V
16V
)™xxmxax^)^3»xx^x<mxxxxxxxxx19V23V
29V
30V
32V
33V
38V
44V
45V
46V
47V
48V
49V
50V
51V
85V
86V
87V
88V
'LE ID F0536
ID 21881V2
: INJECTED 8/5/81
ID BFB35 VOA156
:. FACTOR -----
tiles i
acrolein
acrylonitrile
benzene
carbon tetrachloride
chlorobenzene
1,2-dichloroethane
1,1, l-trichloroethane
1,1-dichloroethane
1,1,2-trichloroethane
1,1,2,2-tetrachloroethane
chloroethane
2-chloroethylvinyl ether
chloroform
1,1-dichloroethylene
1,2-trans-dichloroethylene
1,2-dichloropropane
1,3-dichloropropylene
ethylbenzene
methylene chloride
methyl chloride
methyl bromide
bromoform
dichlorobromomethane
trichlorofluoro me thane
dichlorodifluorome thane
chlorodibromo methane
tetrachloroethylene
toluene
trichloroethylene
vinyl chloride
17605 Fabrica Way. Suite
Llg/1
ND
N D
N D
ND
N D
N D
ND
N D
N D
N D
ND
ND
13
N D
ND
N D
N D
N D
19
ND
N D
N D
N D
ND
ND
N D*
N D
N D
ND
D Cen
SAMF
LAB
DATE
DATI
STD
CONC
Pesti
89P
90P
91P
92P
93P
94P
95P
96P
97P98P
99P100P
101P
102P
103P
104P
105P
106P
107P
108P
109PHOP
HIP
112P
113P
-"-
(P 1
ND =^- ^
ntos. Ca l i f
'LE ID F053
ID TRAC
; EXTRACTED 7/31
; INJECTED 8/6/
ID TRAC
;. FACTOR 50
Icides
aldrin
dieldrin
chlordane
4,4 ' -DDT
4,4 ' -DDE
4,4 ' -DDD
alpha-endosulfan
beta-endosulfan
endosulfan sulfate
endrin
endrin aldehyde
heptachlor
heptachlor epoxide
alpha-BHC
beta-BHC
gamma-BHC
delta-BHC
PCB-1242
PCB-1254
PCB-1221
PCB-1232
PCB-1248
PCB-1260
PCB-1016
toxaphene
Less than 10 ug/1
esticides less than 5
Not detected
Not confirmed by GC
ornia 90701 213/921-9831
[6
;E N141
/81
'81
;E N140
ug/1
N D
. ND
ND
ND
<W
^00
^
^(ffp
N D
N D
N D
ND
ND
ND
ND
N D
N D
N D
N D
N D
ND
N D
N D
ND
ug/1)
^ 07106062
n "i nvc. fnV *A<J»<.io/JL
vss/e^t
SAMP
LAB :
DATE
DATE
STD 1
CONC
Acid
21A
22A
24A
31A
34A
SPA
58A
59A60A
64A
65A
Base/
1B
5B
8B
9B
12B
18B
20B
25B
26B
27B
28B
35B
36B
37B
39B
40B
D WGSTCOASi ,^. 1CAL
LE ID F0536
[D 21881A13
EXTRACTED7/31/81
INJECTED 8/17/81
•'D SENS178 PHEN355
FACTOR 1000
Compounds u
2,4,6-trichlorophenol
p-chloro-m-cresol
2-chlorophenol
2,4-dichlorophenol
2,4-dimethylphenol
2-nitrophenol
4-nitrophenol *
2,4-dinitrophenol
4,6-dinitro-o-cresol
pentachlorophenol
phenol
'Neutral Compounds
acenaphthene
benzidine
1,2,4-trlchlorobenzene
hexachlorobenzene
hexachloroethane
bis(2-chloroethyl)ether
2-chloronapthalene
1,2-dichlorobenzene
1,3-dichlorobenzene
1,4-dichlorobenzene
3,3'-dichlorobenzidine
2,4-dinitrotoluene
2,6-dinitrotoluene
1,2-diphenylhydrazine
(as azobenzene)
f luoranthene
4-chlorophenyl phenyl ether
S6RVK
g/lNO
ND
ND
ND
ND
ND
ND
NO*
117
ND
ND
ND
ND
ND
NDND
N D
N D
N D
ND
ND
ND
NnND
ND
C€ INC.
SAMP]
LAB 1
DATE
DATE
STD I
CONC
Base/
41B
42B
43B
52B
53B
54B
55B
56 B
61B
62B63B
66 B
67B
68B
69B
70B
71B
72B
73B
74B
75B
76B
77B
78B
79B
80B
81B
82B
83 B
84B
129B
p-dio
INDUSTRIAL CATEGORY
-E ID FOMfi
•D ?1RR1R?
EXTRACTED 7/.'n/fii
INJECTED f i /n /Ri
D RFN7.W RNSTn^U
FACTOR mnn
Neutral Compounds u^
4-bromophenyl phenyl ether
bis(2-chloroisopropyl) ether
bis (2-chloroethoxy) methane
hexachlorobutadiene
hexachlorocyclopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodi methyl a mine
N-nitrosodiphenylamine
N-nitrosodi-n-propylamine
bis (2-ethylhexyl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
di-n-octyl phthalate
diethyl phthalate
dimethyl phthalate
benzo(a) anthracene
benzo(a)pyrene
3,4-benzofluoranthene
benzo(k) f luoran thene
chrysene
acenaphthylene
anthracene
benzo(ghi)perylene
fluorene
phenanthrene
d ibenzo(a ,h )an th racene
indeno( 1,2,3-cd)pyrene
pyrene
2,3,7,8-tetrachlorodiben0»y^()<xln n^Tmnrw
g/lND
ND
ND
ND
N^T- e-NtbN&-
NP
NP
ND
ND
ND
ND*
ND*
ND
ND
ND
NDN D
mND
N D
N D
N n
NnNnN nN D
K063.ND
W6ST COAST TECHNICAL SERVICE INC.ORGANICS ANALYSIS DATA SHEET - Page 3
QC Report No: 28Sample Number
LAB BLANK & BFB
A. SURROGATE SPIKE RESULTS
COMPOUND
Benzene - d6
l-Chloro-2-Bromopropane
Toluene - d8
2-Fluorophenol
Phenol - d5
Nitrobenzene - d5
2-Fluorobiphenyl
Naphthalene-DS
Fraction
VOA
VOA
VOA
ACID
ACID
B/N
B/N
B/N
C o n e . ( u g / 1 )
52
52
55
96
62
58
68
2
(Surrogates only)Spike
Added (ug /1 )
50
50
50
142
10298
100
102
%Recovery
104
104
110
68
———^-^59 .r
68 ^
2 ^
B . TENTATIVELY IDENTIFIED COMPOUNDS 0
1.2.
3.
4.
5.
6.
7.
8.
9.
10.
1 1 .
12.
13.
14.
15.
16.
17.
18.
19.
20.
CAS # COMPOUND NAME
UNKNOWN
UNKNOWN
UNKNOWN
FRACTION
B/N #221
B/N #317
B/N #330
% Maximum Score Attained
Mass Matching Routine: FIT(specify)
NO GOOD FIT
NO GOOD FIT
NO GOOD FIT
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07106064
—————————QWWmr-^