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d^5* OREGON

Environmental Laboratory Accreditation Program

TestAmerica Denver 4025

4955 Yarrow St. ,Arvada, CO 80002 ! '

IS GRANTED APPROVAL BY ORELAP UNDER THE 2009 TNI STANDARDS, TO PERFORM ANALYSES ON ENVIRONMENTAL SAMPLES IN MATRICES AS LISTED BELOW :

J;^?i§rmS0f

NELAP Recognized

Air Drinking WaterNon Potable

WaterSolids and

Cbem. Waste Tissue

Chemistry Chemistry Chemistry

AND AS RECORDED IN THE LIST OF APPROVED ANALYTES, METHODS, ANALYTICAL TECHNIQUES, AND FIELDS OF TESTING ISSUED CONCURRENTLY WITH THIS CERTIFICATE AND REVISED AS NECESSARY.

ACCREDITED STATUS DEPENDS ON SUCCESSFUL ONGOING PARTICIPATION IN THE PROGRAM AND CONTINUED COMPLIANCE WITH THE STANDARDS. ,

CUSTOMERS ARE URGED TO VERIFY THE LABORATORY’S CURRENT ACCREDITATION STATUS IN OREGON.v/ J sJ~<Pr'

Gary fc'. Ward, MS Oregon State Public Health Laboratory ORELAP Administrator 3150 NW. 229th Ave, Suite 100 Hillsboro, OR 97124

EFFECTIVE DATE : 01/9/2017

EXPIRATION DATE : 01/8/2018

Certificate No : 4025 - 006

ES/teS'StEltet

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>r;4 In£?frf%s~ziiu

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«ELiOREGON


ORELAP Fields of Accreditation

TestAmerica Denver

4955 Yarrow St.

Arvada, CO 80002

ORELAP ID: 4025

C000026EPA CODE:

Certificate: 4025-006

Issue Date: 1/9/2017 Expiration Date: 1/8/2018

As of 1/9/2017 this list supercedes all previous lists for this certificate number.

MATRIX Reference Code Analyte Code DescriptionDrinkingWater DV-LC-0012 i 60036035 TestAmerica Denver - PFOA in NPW

and SCM by HPLC-MS-MS

7044 Ammonium Perfluorooctanoate (APFO)

6911 Perfluorobutane Sulfonate (PFBS)

6915 Perfluorobutyric acid (PFBA)

9562 Perfluorodecane Sulfonate (PFDS)

6905 Perfluorodecanoic acid (PFDA)

6903 Perfluorododecanoic (PFDDA)

6908 Perfluoroheptanoic acid (PFHA)

6910 Perfluorohexane Sulfonate (PFHS)

6913 Perfluorohexanoic acid (PFHXA)

6906 Perfluorononanoic acid (PFNA)

6917 Perfluorooctane Sulfonamide (PFOSA)

6912 Perfluorooctanoic acid (6909 Perfluorooctanoic Sulfonate (PFOS)

6914 Perfluoropentanoic acid (PFPEA)

6902 Perfluorotetradecanoic acid (PFTDA)

9563 Perfluorotridecanoic (PFTRIA)

6904 Perfluoroundecanoic acid (PFUDA)

Non-Potable ASTM D5057- 30032134 Screening Apparent Specific GravityWater 10 and Bulk Density of Waste

8042 Specific Gravity (Relative Density)

ASTM D7065- 30032918 Nonylphenol by GC/MS06

6513 4-Nonylphenol

9466 4-Nonylphenol diethoxylate

6512 4-tert-Octylphenol

9301 Bisphenol A

9592 Nonyl phenol monoethoxylate

CA HML 939-M 90016765 Determination of Organic LeadCompounds by Graphite FurnaceAbsorption Spectrometry

1208 Organic Lead

D1429-08 30023439 Standard Test Methods for SpecificGravity of Water and Brine

8042 Specific Gravity (Relative Density)

DV-LC-0012 60036035 TestAmerica Denver - PFOA in NPW .and SCM by HPLC-MS-MS M

7044 Ammonium Perfluorooctanoate (APFO)



Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 1 Of 70

OREGONEnvironmental Laboratory Accreditation Program

ORELAP Fields of Accreditation ORELAP ID: 4025

TestAmerica Denver

4955 Yarrow St.

Arvada, CO 80002

EPACODE: C000026

Certificate: 4025 - 006


As of 1/9/2017 this list supercedes all previous lists for this certificate number.Perfluorodecane Sulfonate (PFDS)

Perfluorodecanoic acid (PFDA)

Perfluorododecanoic (PFDDA)

,J)f(----- ItJ .

Non- DV-LC-0012 9562

Potable 6905

Water 6903

6908

6910

6913

6906

r in ’ fr - f6910 Perflubrohexarie-Sulfonate (PFHS)/

^ 691.7 .Vtr

'^',6912^

i'. '6909

’6914

>Perfluorooctane Sulfonamide (PFOSA)

Perfluorooctanoic acid

Perfluorooctanoic Sulfonate (PFOS)

Perfluoropentanoic acid (PFPEA)

'dj f/t\ O

!; / /[/J- Z7, i'V, <HV.


V—’-V9563 Perfluorotridecanoic (PFTRIA)


DV-LC-0020 3

6119 Disodium Inimodiacetate

60036013 TestAmerica Denver - Disodium Iminodiacetate (IDA) by LC/MS/MS (modified EPA 8321 A)

DV-WC-0077

9378 1,1-Dimethyl hydrazine

60036046 TestAmerica Denver - Determination of Hydrazine, Monomethyl Hydrazine, and Unsymmetrical Dimethylhydrazine by IC

9486 Hydrazine

9495 Methyl hydrazine (MMH)

EPA 1010 10116606 Pensky-Martens Closed-Cup Method for Determining Ignitability

" \(L.!0 ' 1780 IgnitabilityEPA 1010A SJV~

K10234807 , i Pensky-Martens Closed-Cup Method for

Determining Ignitability? 1780':., Ignitability

EPA 1311 ^ j , S- "0)

8031 ■ - -T--•- Extraction'/l?i;eparation;L j ‘| ,/?”V

10118806r-A ^

- "Toxicity Characteristic Leaching Procedure

EPA 1312 j'U-fj 11 Ij.'i -',' - J 13 10119003 Synthetic Precipitation Leaching Procedure

8031 Extraction/Preparation

EPA 160.4

1947 Residue - Fixed

10010409 Total Volatile Solids, ignition @ 550 C.

1948 Residue - Fixed, Nonfilterable (FSS)

2070 Volatile suspended solids

EPA 160.4

1970 Residue-volatile


EPA1664A(HEM)

1803 n-Hexane Extractable Material (O&G)

10127807 N-Hexane Extractable Material (Oil and Grease) by Extraction and Gravimetry

Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division

2 of 70

oEL«CESS* OREGONEnvironmental Laboratory Accreditation Program

ORELAP Fields ofAccreditation ORELAP ID: 4025

TestAmerica Denver EPA CODE: C000026

4955 Yarrow St. Certificate: 4025- 006

Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018

As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- Potable Water

EPA 1664A (HEM)

1860 Oil & Grease

EPA 1664A 10261606 Silica Gen Treated N-Hexane(SGT-HEM)

2050

Tr?'- pi—, fT"- ” /v’tn

TotaLPetroleum-Hydrocarbons (TPW) )1Extractable Material (Oil and Grease)

EPA1664B i V“-‘- i/, —3 \

V-J/ /.<•( I fjN-Hexane Extractable Material (Oil and Grease) by Extraction and Gravimetry

. 1803 n-Hexane Extractable Material (O&G)U I £j .

yv 1860 - Oil & Grease ' .e r.

EPA1664B CO 10260628 \ Silica Gel Treated n-Hexane Extractable(SGT-HEM)---- o'- X' vMaterial(Oil & Grease)

‘ - 2050 Total Petroleum Hydrocarbons (TPH)

EPA 180.1 2 10011800 Tur6jdity: Nephelometric

2055 Turbidity

EPA 200.7 4.4

1000 Aluminum

10013806 ICP - metals

1005 Antimony 11010 Arsenic

1015 Barium

1020 Beryllium

1025 Boron

1030 Cadmium

1035 Calcium

1040 Chromium

1050 Cobalt

Qy* . 1055 Copperi: r 1760 Hardness (calc.) '•x-

- f |1070 Iron , r—.

1075 5 •'.Lead /h;:

1080// /Lithium ' __ '

1085 ‘ Magnesium / ,J / ; ~1 f.fi 'r~i H i ^ | ’t 'i .•4

1090 Manganese-' ; .; i 1 '

1100 Molybdenum

1105 Nickel

1910 Phosphorus, total

1125 Potassium

1140 Selenium

1990 Silica as Si02

1145 Silicon

1150 Silver 11155 Sodium

1160 Strontium

2017 Sulfur

Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 3 of 70

oEUo'SSS OREGONEnvironmental Laboratory Accreditation Program


TestAmerica Denver

4955 Yarrow St.

Arvada, CO 80002

ORELAP ID: 4025

EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non-PotableWater

EPA 200.7 4.4

EPA 200.8 5.4

1165

1175

1180

1185

1190

i1005

.1010.»■> \.10.15

’1*620

1030

Thallium

Tin

Titanium

Vanadium

Zinc-!:

. \

Antimony ^ Arsenic

Barium

Beryllium

Cadmium

to fft -SI, ‘I I If l ff'I. !■ -- „[i, •■lL'LIjJ:, 'lin ifp0014605 Metals by ICP-MS

/>

\SC. Oi H

1040

1050

Chromium

Cobalt■A A

>->- —1/

1055 Copper

1075 Lead

1090 Manganese

1100 Molybdenum

1105 Nickel

1140 Selenium

1150 Silver

1165 Thallium

1170 Thorium

1175 Tin

3035 Uranium h

1185 Vanadium

-.1190 ZincEPA 245.1 3 ^ 10036609. . Z ^Mercury by Cold Vapor Atomic

, Absorption

-1,095 C J,Mercury

EPA 300.0 ' i'

1540'■Cj, 1 - ,1 f 1 ^ i-v T.t- cr-Brorhide-'/ <,( )' 1 Jr]-!: i

i ! 10053006' Ion chromatography - anions.

1! 7 ■ f Aii- -

1575 Chloride vl !•;' AA 1 i_.' ---

1730 Fluoride

1810 Nitrate as N

1820 Nitrate-nitrite

1840 Nitrite as N

1870 Orthophosphate as P

2000 Sulfate

EPA 3005A 10133207 Acid Digestion of waters for TotalRecoverable or Dissolved Metals


EPA 3010A 10133605 Acid Digestion of Aqueous samples and Extracts for Total Metals



4 of 70



TestAmerica Denver EPACODE: C000026

4955 Yarrow St. Certificate: 4025 - 006



EPA 3020A


10134404 Acid Digestion of Aqueous samples and Extracts for Total Metals for Analysis by GFAA

EPA 335.1 _ ^ - t— (V"' S 10060001i | i>^ "'p

Cyanides, amenable to chlorination

1510 t Amenable cyanide'O

EPA 335.4 I

t VL L.\ ,1 J S'. »-- < -■ *1' 1645 Total cyanide

!‘s4.0061402 ,r> Methods for the Determination of ,»lnorganic Substances in Environmental .'‘Samples

EPA 350.1 2 10063602 ' Ammonia Nitrogen - Colorimetric, Auto Rhe'nate':

-O 1515 Ammonia as N '• j

EPA 351.2 2

1795 Kjeldahl nitrogen - total

10065404 Total Kjeldahl Nitrogen - Block Digest, Phenate_; v

EPA 351.2 minus EPA

10238207 Organic Nitrogen by AutomatedPhenate (Calculated)

350.1 1865 Organic nitrogen •EPA 3510C


10138202 Separatory Funnel Liquid-liquid extraction

EPA 3520C


10139001 Continuous Liquid-liquid extraction

EPA 353.2 2 10067604 Nitrate/Nitrite Nitrogen - Automated, Cadmium

- 1810 Nitrate as N•

- 1820 Nitrate-nitrite ^ --

M 1825 Total nitrate+nitrite_

:EPA 3535A rV

L /.10139409 ~ ,'Solid-Phase Extraction (SPE)

9822' ' Extraction/Preparation'’.'s'.y''"

EPA 3580A J 1 . J J • 1 .l.. 10143007 Waste Dilution

8031 ' / ’ • ' 1 j' ‘lExtraction/Pfepal'dtion 1 11 1 ilr ' S:

EPA 3620B


10145809 Florisil Cleanup

EPA 365.1 2


10070005 Phosphorous - Colorimetric, Automated persulfate


EPA 3660B 10148400 Sulfur cleanup

8031 Extraction/Preparation £

EPA 3665A 10148808 Sulfuric Acid / permanganate Cleanup



oELt OREGONEnvironmental Laboratory Accreditation Program





As of 1/9/2017 this list supercedes all previous lists for this certificate number._________Non-PotableWater

EPA 410.4 2 10077404 Chemical Oxygen Demand ■ Colorimetric, Automated.

1565 Chemical oxygen demand

EPA 420.1

1905 Total phenolics pp

10079400-ftdn , „'fr$ —

U . ! 'V -

Phenolics - Spectrophotometric, manual.

EPA 420.4

S?•V*19,05

F i Jw b ~-J ^3 ~

ir.T ^,-pTotal phenolics

J [ [10080203.1 J | jTH~(/M

il- / S

Phenolics, Total Recoverable by Semi- Automated Colorimetry

vEPA 5030B -A

'OO't/ \r

,9822 Extraction/Preparation

10153409 :3/. .Burge and trap for aqueous samples

EPA 5030C V. 10284603 Purge-ancHTrap for Aqueous Samples


EPA 6010B

1000 Aluminum

10155609 ICP - AES '

1005 Antimony

1010 Arsenic

1015 Barium

1020 Beryllium

1025 Boron

1030 Cadmium

1035 Calcium

1040 Chromium

1050 Cobalt

1055 Copper

r1070

1075"[1080

1085'

Iron

Lead

>_ Lithium

Pd, MagnesiumJ; Manganese

Molybdenbrp,!

j

’v. r*"'V>: r

1090

1100

.. V"’

1105

1910

Nickel [[ [I,

Phosphorus, total

It 3-

1125 Potassium

1140 Selenium

1990 Silica as Si02

1145 Silicon

1150 Silver

1155 Sodium

1160 Strontium

2017 Sulfur

1165 Thallium

1175 Tin


6 of 70

oEU(CT4 OREGON


ORELAP Fields of ^„I_1 _Accreditation ORELAP ID: 4025




As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 6010B 1180 Titanium

Potable 1185 Vanadium

Water 1190 Zinc

EPA 6010C^ fOi

1000r'

Aluminuhii f r-y\: \ 1*, M

1005 \ ^Antimony

1010 ' Arsenic^Barium

,, ■. .1020' Beryllium__ .”'1025

/ - jBoron

1030 Cadmium

1035 Calcium

1040 Chromium

1050 Cobalt

1055 Copper

1070 Iron

1075 Lead

1080 Lithium

1085 Magnesium

1090 Manganese

1100 Molybdenum

1105 Nickel


1125 Potassiumr,l- 1140 Selenium

-1990 Silica as Si02^ >145

Silicon! 1150. . . Silver

} -1155: Sodjum1160 lj ^Strontium

2017 Sulfur ■ r} i | ’

Thallium i >1165

1175 Tin

1180 Titanium

1185 Vanadium

1190 Zinc

_ J10155803

f(p/>H J .1 j t

ICP - AES

riM:

EPA 6010D 10155916 Metals by ICP - AES

1000 Aluminum

1005 Antimony

1010 Arsenic

1015 Barium

1020 Beryllium

1025 Boron




TestAmerica Denver

4955 Yarrow St.

Arvada, CO 80002 Issue Date: 1/9/2C

As of 1/9/2017 this list supercedes all previous lists for thiiNon- EPA 6010D 1030 Cadmium

Potable 1035 Calcium

Water 1040 Chromium

1050 Cobalt

1055 Copper .

1070 Iron

1075 Lead •'

1080 Lithium

1085 Magnesium

1090 Manganese

1100 Molybdenum

1105 Nickel


1125 Potassium

1140 Selenium

1990 Silica as Si02( 1145 Silicon

1150 Silver

1155 Sodium

1160 Strontium

2017 Sulfur

1165 Thallium

1175 Tin

1180 Titanium

1185 Vanadium

1190 Zinc

EPA 602

4610 1,2-Dichlorobenzene



4375 Benzene

4475 Chlorobenzene

4765 Ethylbenzene

5240 m+p-xylene

5000 Methyl tert-butyl ether (MTBE)

5250 o-Xylene

5140 Toluene

5260 Xylene (total)

ORELAP ID: 4025

EPA CODE: C000026


EPA 6020

10102202 Purgeable Aromatics by GC/PID Purge & Trap

10156000 Inductively Coupled Plasma-Mass Spectrometry

1005

1010

1015

Antimony

Arsenic

Barium


fH OREGONEnvironmental Laboratory Accreditation Program


ORELAP ID:

TestAmerica Denver

4955 Yarrow St.

Arvada, CO 80002

4025

C000026EPA CODE:


Expiration Date: 1/8/2018Issue Date: 1/9/2017

As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 6020 1020 Beryllium

Potable 1030 Cadmium

Water 1040 Chromium

1050 Cobalt

1055 Copper

1075 Lead

1090 Manganese

1100 Molybdenum

1105 Nickel

1140 Selenium

1150 Silver

1165 Thallium

1170 Thorium

1175 Tin

3035 Uranium

1185 Vanadium

| 1190 Zinc

EPA 6020A

1005 Antimony

1010 Arsenic

1015 Barium

1020 Beryllium

1030 Cadmium

1040 Chromium

1050 Cobalt

1055 Copper

1075 Lead

1090 Manganese

1100 Molybdenum

1105 Nickel

1140 Selenium

1150 Silver

1165 Thallium

1170 Thorium

1175 Tin

3035 Uranium

1185 Vanadium

1190 Zinc

>EPA 6020B2014

1005 Antimony

1010 Arsenic

1015 Barium

i‘










EPA 6020B 2014

1020

1030

1040

1050

1055

1075

1090

1100

1105

1140

1150

1165

1170

1175

3035

1185

1190

Beryllium

Cadmium

Chromium

Cobalt ,

Copper

Lead

Manganese

Molybdenum

Nickel

Selenium

Silver

Thallium

Thorium

Tin

Uranium

Vanadium

Zinc

EPA 608 10103603

7355 4,4'-DDD

7360 4,4-DDE

7365 4,4-DDT

7025 Aldrin

7110 alpha-BHC (alpha-Hexachlorocyclohexane)

7240 alpha-Chlordane

8880 Aroclor-1016 (PCB-1016)

8885 Aroclor-1221 (PCB-1221)

8890 . Aroclor-1232 (PCB-1232)

8895 Aroclor-1242 (PCB-1242)

8900 Aroclor-1248 (PCB-1248)

8905 Aroclor-1254 (PCB-1254)

8910 Aroclor-1260 (PCB-1260)

7115 beta-BHC (beta-Hexachlorocyclohexane)

7250

7105

7470

7510

7515

7520

7540

7530

7535

Chlordane (tech.)

delta-BHC

Dieldrin

Endosulfan I

Endosulfan II

Endosulfan sulfate

Endrin

Endrin aldehyde

Endrin ketone

Organochlorine Pesticides & PCBs by GC/ECD


10 of 70






As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 608PotableWater

7120

7245

7685

gamma-BHC (Lindane, gamma- HexachlorocyclohexanE)

gamma-Chlordane

Heptachlor

7690 Heptachlor epoxide

7810 Methoxychlor , .

8250 Toxaphene (Chlorinated camphene)

EPA 610 (HPLC)

10297004 , Polynuclear Hydrocarbons by HPLC/UV-VIS

6380 1-Methylnaphthalene


5500 Acenaphthene

5505 Acenaphthylene

5555 Anthracene

5575 Benzo(a)anthracene

5580 Benzo(a)pyrene

_ 5590 Benzo(g,h,i)perylenew 5600 Benzo(k)fluoranthene

5585 Benzo[b]fluoranthene

5855 Chrysene

5895 Dibenz(a.h) anthracene

6265 Fluoranthene

6270 Fluorene

6315 lndeno(1,2,3-cd) pyrene

5005 Naphthalene

6615 Phenanthrene

6665 Pyrene

EPA 614 10105201 Organophosphorous Pesticides by Liquid/Liquid Extraction and GC/NPD

7075 Azinphos-methyl (Guthion)

7410 Diazinon

8625 Disulfoton

7770 Malathion

7825 Methyl parathion (Parathion, methyl)

7955 Parathion, ethyl

EPA 614 10105201 Organophosphorous Pesticides by Liquid/Liquid Extraction and GC/NPD

7390 Demeton

7395 Demeton-o

7385 Demeton-s

EPA 624 10107207 Volatile Organic Compounds by purge and trap GC/MS

5105 1,1,1,2-Tetrachloroethane

5160 1,1,1 -Trichloroethane



11 Of 70

aEU OREGONEnvironmental Laboratory Accreditation Program





As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 624 5165 1,1,2-Trichloroethane

Potable 4630 1,1-Dichloroethane

Water 4640 1,1 -Dichloroethylene

5180 1,2,3-Trichloropropane

4570 1,2-Dibromo-3-chloropropane (DBCP)

4585 1,2-Dibromoethane (EDB, Ethylene, dibromide)


4635 1,2-Dichloroethane (Ethylene dichloride)

4655 1,2-Dichloropropane



4735 1,4-Dioxane (1,4- Diethyleneoxide)

4410 2-Butanone (Methyl ethyl ketone, MEK)

4500 2-Chloroethyl vinyl ether

4860 2-Hexanone (MBK)

4995 4-Methyl-2-pentanone (MIBK)

4315 Acetone

4325 Acrolein (Propenal)

4340 Acrylonitrile

4375 Benzene

4395 Bromodichloromethane

4400 Bromoform

4450 Carbon disulfide

4455 Carbon tetrachloride

4475 Chlorobenzene

4575 Chlorodibromomethane

4485 . Chloroethane (Ethyl chloride)

4505 Chloroform

4645 cis-1,2-Dichloroethylene

4680' cis-1,3-Dichloropropene

4595 Dibromomethane (Methylene bromide)

4625 Dichlorodifluoromethane (Freon-12)

4765 Ethylbenzene

5240 m+p-xylene

4950 Methyl bromide (Bromomethane)

4960 Methyl chloride (Chloromethane)


4975 Methylene chloride (Dichloromethane)

5005 Naphthalenei 4855 n-Hexane

5250 o-Xylene

5100 Styrene

5115 Tetrachloroethylene (Perchloroethylene)


o!SS5o OREGONEnvironmental Laboratory Accreditation Program

ORELAP Fields of A r,Accreditation ORELAP ID: 4025




As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 624 5140 Toluene

Potable 5205 Total trihalomethanes

Water 4700 trans-1,2-Dichloroethylene

4685 trans-1,3-Dichloropropylene 4

5170 Trichloroethene (Trichloroethylene)

5175 Trichlorofluoromethane -(Fluorotrichloromethane, Freon 11)

5225 . Vinyl acetate

5235 Vinyl chloride

5260 Xylene (total)

EPA 625

6715 1,2,4,5-Tetrachlorobenzene

5155 1,2,4-Trichlorobenzene


6221 1,2-Diphenylhydrazine


\ 4620 1,4-Dichlorobenzene


4659 2,2-Oxybis(1 -chloropropane)

6835 2,4,5-T richlorophenol

6840 2,4,6-Trichlorophenol

5880 2,4-Diaminotoluene

6000 2,4-Dichlorophenol

6130 2,4-Dimethylphenol

6175 2,4-Dinitrophenol

6185 2,4-Dinitrotoluene (2,4-DNT)

6183 2,6-Diaminotoluene



5795 2-Chloronaphthalene

5800 2-Chlorophenol

6360 2-Methyl-4,6-dinitrophenol (4,6-Dinitro-2 -methylphenol)

6400 2-Methylphenol (o-Cresol)

6490 2-Nitrophenol

6412 3 & 4 Methylphenol

5945 3,3'-Dichlorobenzidine

5660 4-Bromophenyl phenyl ether (BDE-3)

5700 4-Chloro-3-methylphenol

5825 4-Chlorophenyl phenylether

I 6410 4-Methylphenol (p-Cresol)

6500 4-Nitrophenol

5500 Acenaphthene

5505 Acenaphthylene

10300002 Base/Neutrals and Acids by GC/MS


13 Of 70

oEUOW4 OREGON



TestAmerica Denver

4955 Yarrow St.

Arvada, CO 80002 Issue Date: 1/9/2017

ORELAP ID: 4025

EPACODE: C000026


Expiration Date: 1/8/2018

As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 625

Potable Water

5510 Acetophenone

4330 Acrylamide

6700 alpha-Terpineol

5545 Aniline

5555 Anthracene

5562 Azobenzene - -

5565 Benzal chloride

5595 Benzidine


5580 Benzo(a)pyrene

5590 Benzo(g,h,i)perylene

5600 Benzo(k)fluoranthene


5610 Benzoic acid

5760 bis(2-Chloroethoxy)methane

5765 bis(2-Chloroethyl) ether

5780 bis(2-Chloroisopropyl) ether

5670 Butyl benzyl phthalate

5680 Carbazole

7210 Carbofuran phenol

5855 Chrysene

6065 Di(2-ethylhexyl) phthalate (bis(2- Ethylhexyl)phthalate, DEHP)

5895 Dibenz(a,h) anthracene

6070 Diethyl phthalate

6135 Dimethyl phthalate

5925 Di-n-butyl phthalate

6200 Di-n-octyl phthalate

6265 Fluoranthene

6270 Fluorene

6275 Hexachlorobenzene

4835 Hexachlorobutadiene

6285 Hexachlorocyclopentadiene

4840 Hexachloroethane


6320 Isophorone

5005 Naphthalene

5875 n-Decane

5015 Nitrobenzene

6530 n-Nitrosodimethylamine

6545 n-Nitrosodi-n-propylamine

6535 n-Nitrosodiphenylamine

6580 n-Octadecane

6590 Pentachlorobenzene





4955 Yarrow st. Certificate: 4025 - 006


As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 625 6605 Pentachlorophenol

Potable 6615 Phenanthrene

Water 6625 Phenol

6640 Phthalic anhydride

6665 Pyrene , l5095 Pyridine . • ■5200 Triethylamine

EPA 6860

1895 Perchlorate

10304800 ' Perchlorate in Water, Soils and Solid Wastes Using Ion Chromatography/Electrospray

‘ lonization/Mass Spectrometry

EPA7196A

1045 Chromium VI

10162400 Chromium Hexavalent colorimetric

EPA 7470A

1095 Mercury

10165807 Mercury in Liquid Waste by Cold Vapor Atomic Absorption

• EPA 8011 10173009 1,2-Dibromoethane and 1,2-Dibromo-3- chloropropane by Microextraction and GC/ECD


4585 1,2-Dibromoethane (EDB, Ethylene dibromide)

4580 Dibromochloropropane

EPA 8015B

9369 Diesel range organics (DRO)

10173601 Non-halogenated organics usingGC/FID

4750 Ethanol

9408 Gasoline range organics (GRO)

4875 . Isobutyl alcohol (2-Methyl-1-propanol)

4895 •Isopropyl alcohol (2-Propanol, Isopropanol)

9488 Jet Fuel

4930 Methanol

9499 Motor Oil

4425 n-Butyl alcohol (1-Butanol, n-Butanol)

5055 n-Propanol

EPA8015C 10173805 Non-halogenated organics using GC/FID

9369

4720

4750

4785

9408

4875

Diesel range organics (DRO)

Diethylene glycol (2,2-Oxybisethanol)

Ethanol

Ethylene glycol

Gasoline range organics (GRO)

Isobutyl alcohol (2-Methyl-1 -propanol)


aEUOW4 OREGON



TestAmerica Denver

ORELAP ID: 4025

EPACODE: C000026

4955 Yarrow St. Certificate: 4025-006


As of 1/9/2017 this list supercedes all previous lists for this certificate number.EPA8015C

PotableWater

4895

9488

4930

Isopropyl alcohol (2-Propanol,Isopropanol)

Jet Fuel

Methanol

9499 Motor Oil |


5055 ; ; n-Propanol

6657 Propylene Glycol

9646 Triethylene Glycol

EPA8015D 10305609 Nonhalogenated Organics UsingGC/FID


4750 Ethanol


4875 Isobutyl alcohol (2-Methyl-1-propanol)

4895 Isopropyl alcohol (2-Propanol,Isopropanol)

) 9488 Jet Fuel

4930 Methanol

9499 Motor Oil

4425 n-Butyl alcohol (1 -Butanol, n-Butanol)

5055 n-Propanol

EPA 8021B 10174808 Aromatic and Halogenated Volatiles byGC with PID and/or ECD Purge & Trap




4375 Benzene

4475 Chlorobenzene

4765 Ethylbenzene

5240 m+p-xylene

5000 Methyl tert-butyl ether (MTBE) ;

5005 Naphthalene

5250 o-Xylene

5140 Toluene

5260 Xylene (total)

EPA 8081A 10178606 Organochlorine Pesticides by GC/ECD

8580 2,4'-DDD

8585 2,4-DDE

8590 2,4-DDT

7355 4,4-DDD9

7360 4,4-DDE

7365 4,4'-DDT

7025 Aldrin




TestAmerica Denver

4955 Yarrow St.


As of 1/9/2017 this list supercedes all previous lists for this cerEPA 8081A 7110 alpha-BHC (alpha-

PotableHexachlorocyclohexane)

7240 aloha-ChlordaneWater 7115 beta-BHC (beta-

Hexachlorocyclohexane)

7250 Chlordane (tech.)

7260 Chlorobenzilate

7300 Chlorpyrifos

7105 delta-BHC

7405 Diallate

7460 Dicofol

7470 Dieldrin

7510 Endosulfan I

7515 Endosulfan II

7520 Endosulfan sulfate

7540 Endrin

7530 Endrin aldehyde1

7535 Endrin ketone

7120 gamma-BHC (Lindane, gamma- HexachlorocyclohexanE)

7245 gamma-Chlordane

7685 Heptachlor



6280 Hexachlorocyclohexanes

7725 Isodrin

7740 Kepone

7810 Methoxychlor

7870 Mirex

8045 Propachlor (Ramrod)


EPA 8081B

8580 2,4-DDD

8585 2,4-DDE

8590 2,4-DDT

7355 4,4-DDD

7360 4,4'-DDE

7365 4,4'-DDT

7025 Aldrin

7110 alpha-BHC (alpha- Hexachlorocyclohexane)

¥ 7240 alpha-Chlordane

7115 beta-BHC (beta- Hexachlorocyclohexane)


EPACODE: C000026



10.178800 Organochlorine Pesticides by GC/ECD


oEL« OREGONEnvironmental Laboratory Accreditation Program


Test America Denver

4955 Yarrow St.


As of 1/9/2017 this list supercedes all previous lists for this cerEPA 8081B 7260 Chlorobenzilate

Potable 7300 Chlorpyrifos

Water 7105 delta-BHC

7405 Diallate r ; ,

7460 DicofOl ' ;

7470 ■ - Dieldrin - - --- -

7510 Endosulfan I

7515 Endosulfan II


7540 Endrin

7530 Endrin aldehyde

7535 Endrin ketone



7685 Heptachlor

j 7690 Heptachlor epoxide



7725 Isodrin

7740 Kepone

7810 Methoxychlor

7870 Mirex

8045 Propachlor (Ramrod)


EPA 8082

8880 Aroclor-1016 (PCB-1016)

8885 Aroclor-1221 (PCB-1221)

8890 Aroclor-1232 (PCB-1232)

8895 Aroclor-1242 (PCB-1242)

8900 Aroclor-1248 (PCB-1248)

8905 Aroclor-1254 (PCB-1254)

8910 Aroclor-1260 (PCB-1260)

8912 Aroclor-1262 (PCB-1262)

8913 Aroclor-1268 (PCB-1268)

ORELAP ID: 4025

EPA CODE: C000026



10179007 Polychlorinated Biphenyls (PCBs) by GC/ECD

EPA 8082A 10179201 Polychlorinated Biphenyls (PCBs) by GC/ECD

8880 Aroclor-1016 (PCB-1016)

8885 Aroclor-1221 (PCB-1221)

8890 Aroclor-1232 (PCB-1232)

8895 Aroclor-1242 (PCB-1242)

8900 Aroclor-1248 (PCB-1248)

8905 Aroclor-1254 (PCB-1254)



ORELAP Fields ofAccreditation ORELAP ID. 4025





EPA 8082A

EPA 8141A

/‘f'V-

%

8910

8912

8913

7045

7065

7070

7075.

, 7125

;> 7220

7300

7315

7390

7395

7385

7410

8610

7475

8625

7550

7570

7580

7600

7605

7770

'7785

•7825

Aroclor-1260 (PCB-1260)



Cr’,-Anilazine:

-k

I”T—'*^1XO:-' f10182000

g)'Atrazihe

iljjiziriphos-ethyl (Ethyl guthion)

' Azinphos-methyl (Guthion)

Bolstar (Sulprofos)

Carbophenothion

Chlorpyrifos

Coumaphos

Demeton

Demeton-o

Demeton-s

Diazinon

Dichlorovos (DDVP, Dichlorvos)

Dimethoate

Disulfoton

EPN

Ethoprop

Famphur

Fensulfothion

Fenthion

Malathion

Merphos

Methyl parathion (Parathion, methyl)

Organophosphorous Pesticides by GC/NPD

m tif.nr ,fSIT-

_r:_s

Crib -VI.

a

!!>7850V^'Mevinphos

7905)

8290

7955

7985

8000

8060

8110

8125

8155

8200

8235

8245

8275

ji ii Naled . ti r-

6,0,0/Triethyl phosphorothioateA

If 4> I.

Q l;. I:

■ fi JParathion,"ethyl

Phorate

Phosmet (Imidan)

Propazine

Ronnel

Simazine

Sulfotepp

Tetrachlorvinphos (Stirophos, Gardona) Z-isomer

Thionazin (Zinophos)

Tokuthion (Prothiophos)

Trichloronate


19 Of 70

o£S5* OREGONEnvironmental Laboratory Accreditation Program


TestAmerica Denver

4955 Yarrow St.

Arvada, CO 80002

EPACODE: C000026




EPA8141B 10182204 Organophosphorous Pesticides by GC/NPD

7045 Anilazine

7065 AtrazineT '-..si,Azinphos-ethy) .(Ethyl

£ p~-7070 guthion)f

7075 Azinphos-methyl (Gut

7125^ ^Bolstaf^Sulprofos)

„ 7220f.-f V-;:• . 7300.

Carbophenothion-TV

Chlorpyrifos^'’.^7315 CoumaphosXl ;: 7390 Demeton

7395 Demeton-o

7385 Demeton-s

7410 Diazinon

8610 Dichlorovos (DDVP, Dichlorvos)

7475 Dimethoate

8625 Disulfoton

7550 EPN

7570 Ethoprop

7580 Famphur

7600 Fensulfothion

7605 Fenthion

7770 Malathion

7785 Merphos


7850 Mevinphos

‘ 7905 Naled

. L , 79551 i7985‘

Parathion, ethyl

' Phorate

^ lit

/ J"/

8000 i

8110

8125

8155

8200

8235

8245

8275

Phosrpet (Imidan)

Rorinel f'\-- SimStzine 'V ' I i Tfi.V' •*i ‘tSulfotepp ;i. j 1

Tetrachlorvinphos (Stirophos, Gardona) Z-isomer

Thionazin (Zinophos)

Tokuthion (Prothiophos)

Trichloronate

EPA 8151A 10183207 Chlorinated Herbicides by GC/ECD

8655

8545

8560

8555

8595

2,4,5-T

2.4- D

2.4- DB

Dalapon

Dicamba


ttEUOREGON



TestAmerica Denver

4955 Yarrow St.


ORELAP ID: 4025

EPACODE: C000026




EPA 8151A 8605

8620

7775

7780

8645

8650

Dichloroprop (Dichlorprop)

Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP)

MCPA

MCPB—,

EPA 8260B •t^tA"

'V

^Picloram'.!w...... .!jSilvexL{2,4,5-TP) vu A

——i!" A I I j'v101848024///

?

N.’

%-■ Q 'if

:5,105■‘'5185

5160

5110

5195

5165

5167

5172

5171

4630

4640

4670

5150

5180

5182

5155

,5210

4570

’• l, *3 f v //4695 J

i4697

4610

4635

4655

6800

5215

4615

4660

4675

4620

4735

4919

4510

1.1.1.2- Tetrachloroethane

1,1,1 -Trichloro-2,2,2-trifluoroethane

1.1.1- Trichloroethane

1.1.2.2- Tetrachloroethane

1.1.2- Trichloro-1,2,2-trifluoroethane (Freon 113)

1.1.2- T richloroethane

1.1.2- Trichlorofluoroethane

1.1.2- Trifluoroethane

1.1- Dichloro-1-fluoroethane

1.1- Dichloroethane

1.1- Dichloroethylene

1.1- Dichloropropene

1.2.3- Trichlorobenzene

1.2.3- Trichloropropane

1.2.3- T rimethylbenzene

1.2.4- T richlorobenzene

1.2.4- Trimethylbenzene

1.2- Dibromo-3-chloropropane (DBCP)

1.2- Dibromoethane (EDB, Ethylene 'T’dibromide)

",1\2-Dichloro-1,1,2,2-tetrafluoroethane(^reon‘11'4) J IT-.-, c-p |.\

fluoroethane ] f l 7.!u y

/.Volatile Organic Compounds by purge •' and trap GC/MS

'S-v

Yi.

cc,

Vl

■ i • i i f J — r,-J F-7., cr pj L it,',2-DjchjQtbr1,1,2j-trifluprpethanp ] ; I. _; “t (Y i'1' £ ji'7 J ’i,i Tj

1('-. I < '• if —1.2- DichlorobenzeneT ~t-

1.2- Dichloroethane (Ethylene dichloride)

1.2- Dichloropropane



1.3- Dichlorobenzene




1.4- Dioxane (1,4- Diethyleneoxide)

1 -Chloro-1,1 -difluoroethane

1-Chlorohexane

- 5 --,Af'^ji t - jyM"1


«EUOREGON



TestAmerica Denver

4955 Yarrow St.


EPACODE: C000026




EPA 8260B 5222

4665

4410

4411

4500

4535

-v 4860^ 50201

O’. 5045

Ly 4540

4910

4995

4315

4320

4325

4340

4355

4375

4385

4390

4395

4400

4450

4455

4475

4575

4577 '4485

; :

U

2.2- Dichloro-1,1,1 -trifluoroethane (Freon 123)


2-Butanone (Methyl ethylketone. MEK)2-Chloro-1,1,1-trif|.uoroethanie tf?

r v-1, ■; . i;.p~ fl 'r'_- 2-Chjoraethyl yinvhgther ~ ' y ,

'.grChlorotoluene

'l 2-Hexanone (MBK)

• 2-Nitropropane

2-Pentanone

4-Chlorotoluene

4-lsopropyltoluene (p-Cymene)

4-Methyl-2-pentanone (MIBK)

Acetone

Acetonitrile

Acrolein (Propenal)

Acrylonitrile

Allyl chloride (3-Chloropropene)

Benzene

Bromobenzene

Bromochloromethane

Bromodichloromethane

Bromoform

Carbon disulfide

Carbon tetrachloride

Chlorobenzene

Chlorodibromomethane

Chlorodifluoromethane (Freon-22)

- Chloroethane (Ethyl chloride)

1/ ; l, /?,L.L;—I / rVf r /e

ii/yy

r •i'-yt. ■

44861, - . ’ ' 'nChlorqfluoromethane4505'J Chloroform .. — y,

4522- — i . * ,i t , f , ■1 j ( l. i L <Chloropentafluorbethane || I1.’

4525 Chloroprene (2-Chldro-1,3-butadiene)

4526 Chlorotrifluoroethene

4705 cis & trans-1,2-Dichloroethene


4680 cis-1,3-Dichloropropene

4600 cis-1,4-Dichloro-2-butene

4555 Cyclohexane

4560 Cyclohexanone



4627 Dichlorofluoromethane (Freon 21)

4725 Diethyl ether




TestAmerica Denver

4955 Yarrow St.


ORELAP ID: 4025

EPACODE: C000026




EPA 8260B 9375

4750

4755

4810

4765

4795

4770

Di-isopropylether (DIPE)

Ethanol

Ethyl acetate

Ethyl methacrylate, pp3EthyJbgnzenelO':-' ij p? iff

A7

77't

-1-- \ V ^$Tlpr-4835

4870

4875

4895

4900

5240

4925

4940

4950

4960

4990

5000

4965

4975

5245

5005

-4425Vi4435

V ^yieh#bxide^J ««--- 'H“J-'■‘feVH ^ ^\!iEthyJ^f-fautyIether (ETBE) (2-Ethoxy-2- ’S^rV/Y | 7?

' Sjr 1It! 7

(fs:

Ijriethylpropane)

Fluoromethane (Freon 41)

Hexachlorobutadiene

lodomethane (Methyl iodide)

Isobutyl alcohol (2-Methyl-1-propanol)

Isopropyl alcohol (2-Propanol, Isopropanol)

Isopropylbenzene (Cumene)

m+p-xylene

Methacrylonitrile

Methyl acetate

Methyl bromide (Bromomethane)

Methyl chloride (Chloromethane)

Methyl methacrylate

Methyl tert-butyl ether (MTBE)

Methylcyclohexane

Methylene chloride (Dichloromethane)

m-Xylene

Naphthalene

n-Butyl alcohol (1-Butanol, n-Butanol)

n-Butylbenzene

\sOil

s?

48550. n-Hexane

50965250t-Y

5035

5080

9579

5255

9607

4440

5100

4370

4420

4445

5115

5120

9574

n^P-ropylbenzene

i o-Xylene - f jr _n- | |Pentachloroethane

O fp, fl,/3,\ f i -Propionitrile(Ethyl cySnide)1:'

Propylene oxide

p-Xylene

sec-Butyl Alcohol (2-Butanol)

sec-Butylbenzene

Styrene

T-amylmethylether (TAME)

tert-Butyl alcohol

tert-Butylbenzene

Tetrachloroethylene (Perchloroethylene)

Tetrahydrofuran (THF)

Tetrahydrothiophene

ff*-.X 7

;s


23 of 70

ItELtOREGON






As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA8260B 5140 Toluene

Potable 4027 Total BTEX

Water 5205 Total trihalomethanes

4700 trans-1,2-Dichloroethylgne'r, 1’■ i* ;,.. f’:r~ '

4685 tranp=1,3-Dichjoropropylenelj ^ jl s4605 r '.trans;13-Dichloro-2-butene J V----

hVv i1 Trichloroethene (Trichloroethylene)5170

y- Si'75 ,.,oT richlorofluoromethaneV,r (Fluorotrichloromethane, Freon 11)

! -’5225 Vinyl acetate

.f—5235 Vinyl chloride

5237 Vinyl Fluoride

5260 Xylene (total)

EPA 8260B SIM


4570 1,2-Dibromo-3-chloropropane (DBCP)




4340 Acrylonitrile

4375 Benzene

4925 Methacrylonitrile

4420 tert-Butyl alcohol

- - .I 5235 Vinyl chloride

EPA 8270C y 'u' . — •

I, i ’t-,6703 1,1-Biphenyl (BZ-0)


5155,1, 1,2,4-Trichlorobenzene4610 1,2-Dichldrobe’nzepe , ■ , —p| V6221 1,2-DipheriyihVd^azine ] || 1 '

6885 1,3,5-Trinitroberizene (1 ;3,5-TNB)


6160 1,3-Dinitrobenzene (1,3-DNB)

4679 1,3-phenylenediamine


6165 1,4-Dinitrobenzene


6420 1,4-Naphthoquinone

6630 1,4-Phenylenediamine

5790 1 -Chloronaphthalene

6380 1 -Methylnaphthalene

6425 1-Naphthylamine

!'■ Cs Jf ■'t \:-J , /r; !

' 1 1 l j

wI '1.

10184904 Volatile Organic Compounds by purge and trap GC/MS-SIM

10185805 -Semivolatile Organic compounds by -GC/MS

’tW'/h

Department ol Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 24 of 70

oELd OREGONEnvironmental Laboratory Accreditation Program





As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 8270C 4659 2,2-Oxybis(1 -chloropropane)

Potable 6735 2,3,4,6-Tetrachlorophenol

Water 6835 2,4,5-T richlorophenol

6840 2,4,6-Trichlorophenolf:>^„ s-n,--- ri—i • rpfr

6000 VCAL. {* i

6130 rt2i4-pirnethylph^inol-- ’ ■ - ~ *^3 Xr—'X1

6175 r';2;4jDinitrophenol -«j?2,4-Dinitrotoluene (2,4-DNT)6185

2,6-Dichlorophenol1 <0:61 90 2,6-Dinitrotoluene (2,6-DNT)

V-—-' 5515 2-Acetylaminofluorene

9322 2-Butoxyethanol


5800 2-Chlorophenol

5866 2-Ethoxyethanol (cellosolve)


P5145 2-Methylaniline (o-Toluidine)




6460 2-Nitroaniline

6490 2-Nitrophenol

5050 2-Picoline (2-Methylpyridine)


5945 3,3'-Dichlorobenzidiner>' j—~ •„• // 6J20

'4 .-6355 ,f .^6405^

3,3'-Dimethylbenzidine

3-Methylcholanthrene

' “| 3-Methylphenol (m-Cresol)

6465 J f:'^3-Nitroaniline

6365“1 ;V4,4':Methylenebis(2-chloroaniline)^

4-AminobipKenyf j j | llf'.1^' J"'! J J ,1

4-Bromophenyl phehyl ether! (BDE-3) “5540

5660


5745 4-Chloroaniline


6105 4-Dimethyl aminoazobenzene

6410 4-Methylphenol (p-Cresol)

6470 4-Nitroaniline

6500 4-Nitrophenol\

6510 4-Nitroquinoline 1 -oxide

6570 5-Nitro-o-toluidine

6112 6-Methylchrysene

6115 7,12-Dimethylbenz(a) anthracene

' ! J iE?- -/7|

f '■& ,1* r _\x.

\\U -r t

\ - —'V

- V "■VI

& i?







As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 8270C 6125 a-a-Dimethylphenethylamine

Potable 5500 Acenaphthene

Water 5505 Acenaphthylene

5510 Acetophenone.—4330 Acrylamide lj r=’ l[{

7005 r'^AIacKlori ’ \

I i V-5. 1 '4357 1'alplja-Methylstyrene

,y>: 5545 ^ciAnlline r -■ y

,/j' . \ . ' I r J' / ‘•y 6555 ^ Anthracene v" __1

/P

■\n c . V-1WH,/=w

,5560 Aramite

7065 Atrazine

5562 Azobenzene

5570 Benzaldehyde

5567 Benzenethiol (Phenylmercaptan)

5595 Benzidine


5580 Benzo(a)pyrene

5605 Benzo(e)pyrene




5610 Benzoic acid

5630 Benzyl alcohol





--<*,

03 O Caprolactam

5680 y Carbazole7210,’i

1Carbofuran phenol

7260 - Chlorobenzilate \ r PP

5855• 1 t • ‘ 1 ’ ItChrysene \ i • _ ^ II , i

5862 Cresols, Total


7405 Diallate

9354 Dibenzfa, h) acridine

5900 Dibenz(a, j) acridine


5890 Dibenzo(a.e) pyrene

5905 Dibenzofuran


7475 Dimethoate



oEUO’SiJo OREGONEnvironmental Laboratory Accreditation Program


TestAmerica Denver

4955 Yarrow St.


EPACODE: C000026




EPA 8270C

y0

-----fi!

5925

6200

8620

6205

8625

62607580

6265;

6270

6275

4835

6285

4840

6295

6312

6315

7725

6320

6325

6345

6375

7825

5010

5005

5875

63000 - ■A y5015

('6525^

Di-n-butyl phthalate

Di-n-octyl phthalate

Dinoseb (2-sec-butyl-4,6-dinitrophenol DNBP) _ j—,

Diphenylaminei; j,? I j—-j iff' ' ff y.DisulfoJtqn ^ g Ll ^!,Ethyl methanesulfonate

i^Famphur

Fluoranthene

Fluorene

Hexachlorobenzene

Hexachlorobutadiene

Hexachlorocyclopentadiene

Hexachloroethane

Hexachloropropene

Indene

lndeno(1,2,3-cd) pyrene

Isodrin

Isophorone

Isosafrole

Methapyrilene

Methyl methanesulfonate

Methyl parathion (Parathion, methyl)

n, n-Dimethyl formamide

Naphthalene

n-Decane

n-Hexadecane

Nitrobenzene

y n-Nitrosodiethylamine

"1

00)

.A

cV/?=..■< v-'

6530 5025!

6545

6535

6550

6555

6560

6565

8290

5550

5553

7955

6590

5035

6600

$ n-Nitrosodimethylamine

fi;Nitroso-di-njbutylamine t—-p

n-Nitrosddi-n{pro,plylamihe jn-Nitrosodiphenylamihell'i t

n-Nitrosomethylethalamine

n-Nitrosomorpholine

n-Nitrosopiperidine

n-Nitrosopyrrolidine

o,o,o-Triethyl phosphorothioate

o-Anisidine

Octachlorostyrene

Parathion, ethyl

Pentachlorobenzene

Pentachloroethane

Pentachloronitrobenzene

'',f0A

jj


oEUOREGON



TestAmerica Denver

4955 Yarrow St.

Arvada, CO 80002

ORELAP ID: 4025

C000026

Issue Date: 1/9/2017

EPA CODE:



As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA8270C 6605 Pentachlorophenol

Perylene

Phenacetin

Phenanthren^-—-

Phe^'-'

PotableWater

6608

6610

6615

6625

7985 r Phofate-Yi .nr..

/?

EPA 8270C SIM

6635 *1 V v

Phthalic acid

^ 6640 ^ iPhthalic anhydride

s---> 9663- ' p-Phenylenediamine

.6650 Pronamide (Kerb)

- 6665 Pyrene

5095 Pyridine

6670 Quinoline

6685 Safrole

8155 Sulfotepp

8235 Thionazin (Zinophos)

8262 Tributyl phosphate

5200 Triethylamine

8310 tris-(2,3-Dibromopropyl) phosphate (tris- BP)




5500 Acenaphthene

\ 5505 Acenaphthylene

5555 Anthracene' [ 5575.';. Benzo(a)anthracene

5580 . Benzo(a)pyrene

5605-J Benzo’(e)pyrene y - -

5590 Benzd(g,h,i)perylene ;' )" ' I 1 'f

5600 Benzo(k)fluorantheri!S — ; j >! -



5855 Chrysene



5905 Dibenzofuran





'// f 7

'{fr,

/ je'S

%./ _..'V

10242407 Semivolatile Organic GC/MS Selective Ion

compounds by Monitoring




Test America Denver EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non-Potable

EPA 8270CSIM

6265

6270

Fluoranthene

Fluorene

Water 6315 lndeno(1,2,3-cd) pyrene

5005 Naphthalene, f

6525 n-Nitrosodiethylamine

6530 : n-Nitrosodimethylamine—‘



6615 Phenanthrene

6665 Pyrene

EPA 8270D.

6703 1,1'-Biphenyl (BZ-0)


5155 1,2,4-T richlorobenzene


6221 1,2-DiphenylhydrazineP

6885 1,3,5-Trinitrobenzene (1,3,5-TNB)




6165 1,4-Dinitrobenzene


6420 1,4-Naphthoquinone


5790 1 -Chloronaphthalene



4659 2,2-Oxybis(1 -chloropropane)

6735 2,3,4,6-Tetrachlorophenol


6840 2,4,6-Trichlorophenol ' s







5515 2-Acetylaminofluorene

5795 2-Chloronaphthalene| 5800 2-Chlorophenol


5145 2-Methylaniline (o-Toluidine)

10186002 Semivolatile Organic compounds by GC/MS


oELtOW4 OREGON



TestAmerica Denver

4955 Yarrow St.


As of 1/9/2017 this list supercedes all previous lists for this certNon- EPA 82700 6385 2-Methylnaphthalene

Potable 6400 2-Methylphenol (o-Cresol)

Water 6430 2-Naphthylamine

6460 2-Nitroaniline,

6490 2-Nitrophenol




6120 3,3'-Dimethylbenzidine

6355 3-Methylcholanthrene

6405 3-Methylphenol (m-Cresol)

6465 3-Nitroaniline

6365 4,4-Methylenebis(2-chloroaniline)

5540 4-Aminobiphenyl







6470 4-Nitroaniline

6500 4-Nitrophenol

6510 4-Nitroquinoline 1-oxide



6125 a-a-Dimethylphenethylamine

5500 Acenaphthene

5505 Acenaphthylene

5510 Acetophenone

5545 Aniline

5555 Anthracene

5560 Aramite

5562 Azobenzene

5570 Benzaldehyde

5595 Benzidine


5580 Benzo(a)pyrene




5610 Benzoic acid

5630 Benzyl alcohol


ORELAP ID: 4025

EPACODE: C000026









As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 8270D 5765 bis(2-Chloroethyl) ether

Potable 5780 bis(2-Chloroisopropyl) ether

Water 5670 Butyl benzyl phthalate

7180 Caprolactam, ,

5680 Carbazole

7260 Chlorobenzilate - ■

5855 Chrysene

8906 Coelution - 3-Chlorophenol + 4- Chlorophenol

5862 Cresols, Total


7405 Diallate



5905 Dibenzofuran


• 7475 Dimethoate




8620 Dinoseb (2-sec-butyl-4,6-dinitrophenol DNBP)

6205 Diphenylamine

8625 Disulfoton

6260 Ethyl methanesulfonate

7580 Famphur

6265 Fluoranthene

6270' Fluorene





6295 Hexachloropropene


7725 Isodrin

6320 Isophorone

6325 Isosafrole

6345 Methapyrilene

6375 Methyl methanesulfonate

•7825 Methyl parathion (Parathion, methyl)

5005 Naphthalene

5015 Nitrobenzene



31 Of 70


ORELAP Fields ofAccreditation

TestAmerica Denver

4955 Yarrow St.


As of 1/9/2017 this list supercedes all previous lists for this ceNon- epa 82700 6530 n-Nitrosodimethylamine

Potable 5025 n-Nitroso-di-n-butylamine

Water 6545 n-Nitrosodi-n-propylamine


6550 n-Nitrosomethylethalamine

6555 n-Nitrosomorpholine

6560 n-Nitrosopiperidine

6565 n-Nitrosopyrrolidine

8290 0,0,0-Triethyl phosphorothioate



5035 Pentachloroethane

6600 Pentachloronitrobenzene

6605 Pentachlorophenol

6610 Phenacetin

6615 Phenanthrene

6625 Phenol

7985 Phorate

9663 p-Phenylenediamine

6650 Pronamide (Kerb)

6665 Pyrene

5095 Pyridine

6685 Safrole

8155 Sulfotepp


EPA 8270DSIM




5500 Acenaphthene

5505 Acenaphthylene

5555 Anthracene


5580 Benzo(a)pyrene





5855 Chrysene



5905 Dibenzofuran

ORELAP ID: 4025

EPACODE: C000026



10242509 Semivolatile Organic compounds by GC/MS Selective Ion Monitoring




TestAmerica Denver

4955 Yarrow St.

Arvada, CO 80002

ORELAP ID: 4025

EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 8270D 6070 Diethyl phthalate

SIMPotableWater

Dimethyl phthalate


Di-n-octyl phttjalate Fluoranthene IQ.;

6135

5925

6200

6265 . . ..6270 rfiFJuoferie'1 Ui

6315

5005 ,jy ,,V . -v6530-'

I ./L>. S t-]. !lndeno(-l ,2,3-cd) pyreneh r

^Naphthalene

n-Nitrosodimethylamine

EPA 8310

."-.6535 n-Nitrosodiphenylamine

L 6615 Phenanthrene

6665 Pyrene



5500 Acenaphthene

5505 Acenaphthylene

5555 Anthracene


5580 Benzo(a)pyrene




5855 Chrysene


! “ 6265 Fluoranthene

, *46270''ff1 6315*

r~_

s Fluorene■J,-Q~Hndeno(1 ,2,3-cd) pyrene

10187607 Polynuclear Aromatic Hydrocarbons by HPLC/UVrVIS

6615

6665

NaphthaleneiPheninthfanei!:

Pyrene-

%

%.

:v)i .jL“L -fZ

EPA 8321A "" M 7 Li ’!4 " '



6014 2,3-Dinitrotoluene

8655 2,4,5-T

9651 2,4,6-Trinitrotoluene (2,4,6-TNT)

8545 2,4-D

8560 2,4-DB



9303 2-Amino-4,6-dinitrotoluene (2-am-dnt)

10189001 Solvent Extractable non-volatile compounds by HPLC/TS/MS




TestAmerica Denver

4955 Yarrow St. I

Arvada, CO 80002 Issue Date: 1/9/2017 E

As of 1/9/2017 this list supercedes all previous lists for this certiNon- EPA 8321A 9507 2-Nitrotoluene

Potable 9510 3-Nitrotoluene

Water 9306 4-Amino-2,6-dinitrotoluene (4-am-dnt)

9513 4-Nitrotoluene

7010 Aldicarb (Temjk)

7040 Aminocarb

7195 Carbaryl (Sevin)

7205 Carbofuran (Furaden)

7275 Chloropropham

8555 Dalapon

8595 Dicamba

8605 Dichloroprop (Dichlorprop)

8620 Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP)

7505 Diuron

7610 Fenuron

7630 Fluometuron

7765 Linuron (Lorox)

7775 MCPA

7780 MCPP

7800 Methiocarb (Mesurol)

7805 Methomyl (Lannate)

6415 Methyl-2,4,6-trinitrophenylnitramine (tetryl)

7855 Mexacarbate

7885 Monuron

7915 Neburon

5015 Nitrobenzene

6485 Nitroglycerin

9522 Octahydro-1,3,5,7-tetranitro-1,3,5,7- tetrazocine (HMX)


9558 Pentaerythritoltetranitrate (PETN)

8075 Propham

8080 Propoxur (Baygon)

9432 RDX (hexahydro-1,3,5-trinitro-1,3,5- triazine)

8120 Siduron

8650 Silvex (2,4,5-TP)

EPA 8321B




8655 2,4,5-T

ORELAP ID: 4025

EPACODE: C000026

tificate: 4025 - 006



c8S5* OREGONEnvironmental Laboratory Accreditation Program


TestAmerica Denver

4955 Yarrow St.

Arvada, CO 80002

ORELAP ID: 4025

EPACODE: C000026


Expiration Date: 1/8/2018Issue Date: 1/9/2017

As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 8321B 9651 2,4,6-Trinitrotoluene (2,4,6-TNT)

Potable 8545 2,4-D

Water 8560 2,4-DB

6185 2,4-Dinitrotoluene (2,4-DNT) "



9507 2-Nitrotoluene

9510 3-Nitrotoluene


9513 4-Nitrotoluene

7010 Aldicarb (Temik)

7040 Aminocarb



7275 Chloropropham

8555 Dalapon( 8595 Dicamba



7505 Diuron

7610 Fenuron

7630 Fluometuron


7775 MCPA

7780 MCPP




7855 Mexacarbate ,

7885 Monuron ’

7915 Neburon

5015 Nitrobenzene

6485 Nitroglycerin




8075 Propham

| 8080 Propoxur (Baygon)¥ 9432 RDX (hexahydro-1,3,5-trinitro-1,3,5-

triazine)

8120 Siduron

8650 Silvex (2,4,5-TP)


«EL«OREGON


6160 1,3-Dinitroberizene (1,,3-DNB)


5882 2,4-diamino-6-nitrotoluene



6190 2,6-Dinitrotoiuene (2,6-DNT)


9507 2-Nitrotoluene

9510 3-Nitrotoluene


9513 4-Nitrotoluene

7046 Ammonium Picrate

6415 Methyl-2,4,6-trinitrophenylnitramine(tetryl)

5015 Nitrobenzene

6485 Nitroglycerin



1899 Picric Acid (2,4,6-Trinitrophenol)










9507 2-Nitrotoluene

6150 3,5-Dinitroaniline

9510 3-Nitrotoluene


9513 4-Nitrotoluene


6415 Methyl-2,4,6-trinitrophenylnitramine(tetryl)

5015 Nitrobenzene


TestAmerica Denver

4955 Yarrow St.


EPACODE: C000026



EPA 8330A 10190008 Nitroaromatics and Nitramines by HighPerformance Liquid Chromatography (HPLC)


EPA 8330B 10308006 Nitroaromatics, Nitramines and NitrateEsters by High Performance Liquid Chromatography (HPLC)


ow-o OREGONEnvironmental Laboratory Accreditation Program


TestAmerica Denver

4955 Yarrow St.

ORELAP ID: 4025

EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 8330B 6485 Nitroglycerin

Potable 9522 Octahydro-1,3,5,7-tetranitro-1,3,5,7- tetrazocine (HMX)

Water9558 Pentaerythritoltetranitrate (PETN)


9432 RDX (hexahydro-1,3,5-tr!nitro-1,3,5- triazine)

i

• ' i

EPA 9012A 10193405 Total and Amenable Cyanide (automated colorimetric with off-line

■ distillation)

1510 Amenable cyanide ' '

_1645 Total cyanide

EPA 9012B

1510 Amenable cyanide

10243206 Total and Amenable Cyanide (automated colorimetric with off-line distillation)

1645 Total cyanide

EPA 9020B 10194408 Total Organic Halides

• 2045 Total organic halides (TOX)

EPA 9030B

2005 Sulfide

10195605 Acid-Soluble and Acid-Insoluble sulfides: Distillation

EPA 9034

2005 Sulfide

10196006 Titrimetric Procedure for Acid-Soluble and Acid-Insoluble Sulfides

EPA 9040B

1900 pH

10197203 pH Electrometric Measurement

EPA 9040C

,1900 pH

10244403 pH Electrometric Measurement

EPA 9050A

1610 Conductivity

10198808 Specific Conductance

EPA 9056

1540 Bromide

10199005 Determination of Inorganic Anions byIon Chromatography

1575 Chloride

1730 Fluoride

1805 Nitrate

1835 Nitrite


2000 Sulfate

_1825 Total nitrate+nitrite

• EPA 9056A

1540 Bromide


1575 Chloride


«ELdOREGON



TestAmerica Denver



As of 1/9/2017 this list supercedes all previous lists for this certificate number.EPA 9056A 1730 Fluoride

Potable 1805 Nitrate

Water 1820 Nitrate-nitrite

1835 Nitrite


2000 Sulfate

EPA 9060

1710 Dissolved organic carbon (DOC)

10200201 Total Organic Carbon

2040 Total organic carbon

EPA 9060A




EPA 9066

1905 Total phenolics

10200609 Phenolics (Colorimetric, Automated 4- AAP with Distillation)

EPA RSK-175 10212905 Methane, Ethane, and Ethene in water(GC-FID)

4323 Acetylene

by Headspace GC/FID

4747 Ethane

4752 Ethene

4877 Isobutylene

4926 Methane

5007 n-Butane

5028 n-Pentane

5029 n-Propane

FLDEP SOP 90015820 Calculation of Un-ionized Ammonia in02/12/01

2058 Un-ionized Ammonia

Fresh Water

NWTPH-Dx


90018409 Oregon DEQ TPH Diesel Range

9499 Motor Oil

9506 Residual Range Organics (RRO)

2050 Total Petroleum Hydrocarbons (TPH)

NWTPH-Gx


90018603 Oregon DEQ TPH Gasoline RangeOrganics by GC/FID-PID Purge & Trap

SM 2120 B- 2001 online

1605 Color

20039309 Color by Visual Comparison

SM 2120 B- 20039310 Color2011

1605 Color •SM 2310 B-97 online

1500 Acidity, as CaC03

20044604 Acidity by Titration Method




TestAmerica Denver

4955 Yarrow St.

ORELAP ID: 4025

EPACODE: C000026




SM 2320 B- 2011

1505 Alkalinity as CaC03


Water SM 2320 B-97 online

1505i ,

Alkalinity as CaC03 ,

20045607 Alkalinity by Titration Method

SM 2340 B- 2011

1750

• _ ■ * • *

Hardness

20046611 Hardness

SM 2340 B-97 online

1550 Calcium hardness as CaC03

20046600 Hardness by calculation

- 1750 Hardness

1755 Total hardness as CaC03

SM 2340 C-97 online

1755 Total hardness as CaC03

20047603 Hardness by EDTA Titration Method

SM 2510 B-97 online

1610 Conductivity

20048606 Conductivity by Probe

§ SM 2540 B-97 online

1950 Residue-total

20049405 Total Solids Dried at 103 - 105C

SM 2540 C- 2011

1955 Residue-filterable (TDS)


SM 2540 C-97 online


20050402 Total Dissolved Solids Dried at 180C

SM 2540 D-97 online

1960 Residue-nonfilterable (TSS)

20051201 Total Suspended Solids Dried at 103 - 105C’

SM 2540 F-97 online

1965 Residue-settleable

20052204 Settleable Solids

SM 3500-Cr B- 2009 online

1045 Chromium VI

20066255 Chromium by Colorimetric Method

SM 3500-Cr D 19th ED

1045 Chromium VI

20067009 Chromium by Colorimetric Method

SM 3500-Fe B 20th ED

1070 Iron

20068604 Iron by Colorimetric Method

SM 3500-Fe B- 97 online

1070 Iron

20069005 Iron by Phenanthroline Method

£

SM 3500-Fe D 19th ED

1070 Iron

20069209 Iron by Phenanthroline Method

SM 4500-CN E- 20096417 Cyanide by Colorimetric Method1999

1645 Total cyanide


OW4 OREGONEnvironmental Laboratory Accreditation Program






SM 4500-CN E- 2011 2011

1645 Total cyanide

20096428 Cyanide by Colormetric Method

Water SM 4500-CN G- 1999 online

1510 Amenable cyanide

20097216 Cyanide Amenable to Chlorination after Distillation

SM 4500-CN' C-97 online

20095607 Cyanide by Total Cyanide afterDistillation

1645 Total cyanide

SM 4500-CN' I- 97 online

2074 Weak Acid Dissociable Cyanide

20098004 Cyanide by Weak Acid Dissociable Cyanide

SM 4500-H+ B- 2000 online

1900 pH

20105219 pH Value by Electrometric Method .

SM 4500-H+ B- 2011

1900 pH

20105220 pH - Electrometric Measurement

SM 4500-N02" B-2000 online

1835 Nitrite

20113104 Nitrite by Colorimetric Determination

1840 Nitrite as N

SM 4500-S2 D- 2000

2005 Sulfide

20125853 Sulfide by Methylene Blue Method

SM 4500-S2' F-2000 online

2005 Sulfide

20126652 Sulfide by lodometric Method

SM 4500-S03' B-2000 online

2015 Sulfite-S03

20130625 Sulfite by lodometric Method

SM 5210 B- 2001 online

1530 Biochemical oxygen demand

20135255 Biochemical Oxygen Demand (BOD), 5- Day

1555 Carbonaceous BOD, CBOD

SM 5210 B- 2011

1530 Biochemical oxygen demand

20135266 Biochemical Oxygen Demand (5 days @ 20 C).

SM 5310 B- 2000


20137819 Total Organic Carbon (TOC) by Combustion Infra-red Method


SM 5310 B- 2011 2011


20137820 TOC by High-Temperature Combustion Method

Solids

ASTM D2216- 10 10

8641 Percent Moisture

30025106 Standard Test Methods for Laboratory Determination of Water (Moisture)Content of Soil and Rock by Mass



ORELAP Fields of AAccreditation ORELAP ID: 4025




CA HML 939-M

1208 Organic Lead

90016765 Determination of Organic Lead Compounds by Graphite Furnace Absorption Spectrometry

DV-LC-0012

7044 • Ammonium Perfluorooctanoate (APFO)

60036035 TestAmerica Denver - PFOA in NPW and SCM by HPLC-MS-MS



9562 Perfluorodecane Sulfonate (PFDS)

6905 Perfluorodecanoic acid (PFDA)

6903 Perfluorododecanoic (PFDDA)

6908 Perfluoroheptanoic acid (PFHA) -

6910 Perfluorohexane Sulfonate (PFHS)

6913 Perfluorohexanoic acid (PFHXA)

6906 Perfluorononanoic acid (PFNA)

6917 Perfluorooctane Sulfonamide (PFOSA)

6912 Perfluorooctanoic acid

6909 Perfluorooctanoic Sulfonate (PFOS)

6914 Perfluoropentanoic acid (PFPEA)


9563 Perfluorotridecanoic (PFTRIA)


DV-LC-0020 3

6119 Disodium Inimodiacetate

60036013 TestAmerica Denver - Disodium Iminodiacetate (IDA) by LC/MS/MS (modified EPA 8321 A)

DV-WC-0077

9378 1,1-Dimethyl hydrazine

60036046 TestAmerica Denver - Determination of Hydrazine, Monomethyl Hydrazine, and Unsymmetrical Dimethylhydrazine by IC

9486 Hydrazine

9495 Methyl hydrazine (MMH)

EPA 1010

1780 Ignitability

10116606 Pensky-Martens Closed-Cup Method for Determining Ignitability

EPA 1010A

1780 Ignitability

10234807 Pensky-Martens Closed-Cup Method for Determining Ignitability

EPA 1311


10118806 Toxicity Characteristic Leaching Procedure

EPA 1312


10119003 Synthetic Precipitation Leaching Procedure

Solids


oEUOWO OREGON



TestAmerica Denver

4955 Yarrow St.

Arvada, CO 80002

EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 160.4

1970 Residue-volatile


EPA 3050B

9822-Extradion/Preparation (— !

10135601

ff

Acid Digestion of Sediments, Sludges, and soils

EPA 335.4

//'V\

■-1645-

L i x \ i

..J”" "

Total cyanide

V'-Lt;1 110061208'v._J i/r>\'■oh

L

Methods for the Determination of j-, Inorganic Substances in Environmental '/ ^Samples

EPA 350.1 , v \

1515 Ammonia as N

10063204' Jc \Ammbnia Nitrogen - Colorimetric, AutoVPhenate,

v/t-i S

EPA 350.1 2 10063602 Ammonia Nitrogen - Colorimetric, Auto Phenate j i

1515 Ammonia as N —

EPA 351.2

1790 Kjeldahl nitrogen

10065006 Total Kjeldahl Nitrogen - Block Digest, Phenate

M

EPA 353.2 2


10067604 Nitrate/Nitrite Nitrogen - Automated, ^

Cadmium

1825 Total nitrate+nitrite

EPA 3540C


10140202 Soxhlet Extraction

EPA 3546


10141205 Microwave Extraction

EPA 3550C . • .Kt‘ /' . -

10142004 ^Ultrasonic Extraction

I r8031 Extraction/Preparation

EPA 3580A ‘ l I , 10143007 ‘ Waste Dilution

8031 '1, Extraction/Preparation i -i ■ ■

EPA 3620B "ji 1 ,,^0145809 Florisil Cleanup

8031■ — -■ / I ' -1! i '

Extradion/Preparation •_ ■Ij ‘'7.7

EPA 3660B


10148400 Sulfur cleanup

EPA 3665A


10148808 Sulfuric Acid / permanganate Cleanup

EPA 5035 10154004 Closed-System Purge-and-Trap and Extraction for Volatile Organics in Soil and Waste Samples

9822 Extraction/Preparation M

EPA 5035A


10284807 Closed-System Purge-and-Trap and ^ Extraction for Volatile Organics in Soil and Waste Samples







As of 1/9/2017 this list supercedes all previous lists for this certificate number. _______SolidS EPA 6010B 10155609 ICP - AES

1000 Aluminum

1005 Antimony

1010 Arsenic ' -

1015 Barium

1020 Beryllium

1025 Boron ’

1030 Cadmium

1035 Calcium

1040 Chromium

1050 Cobalt

1055 Copper

1070 Iron

1075 Lead

1080 Lithium

1085 Magnesium

1090 Manganese

1100 Molybdenum

1105 Nickel


1125 Potassium

1140 Selenium

1990 Silica as Si02

1145 Silicon

1150 Silver

1155 Sodium

1160 Strontium

2017- Sulfur

1165 Thallium

1175 Tin ,

1180 Titanium

1185 Vanadium

1190 Zinc

EPA 6010C 10155803 ICP - AES

1000 Aluminum

1005 Antimony

1010 Arsenic

1015 Barium

1020 Beryllium

1025 Boron

1030 Cadmium

1035 Calcium

1040 Chromium


«EL«OREGON



TestAmerica Denver

4955 Yarrow St.

Arvada, CO 80002

EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 6010C 1050 Cobalt

EPA 6010D

1105 " Nickel

.1910 Phosphorus, total

1125 Potassium

1140 Selenium

1990 Silica as Si02

1145 Silicon

1150 Silver

1155 Sodium

1160 Strontium

2017 Sulfur

1165 Thallium

1175 Tin

1180 Titanium

1185 Vanadium

1190 Zinc

1000 Aluminum

.1005 Antimony

r.1010 Arsenic

1015 Bariumf02*)* Beryllium

1025 -J Boron,Cadmium t .i111 |1030

1035 Calcium u ! i

1040 Chromium

1050 Cobalt

1055 Copper

1070 Iron

1075 Lead

1080 Lithium

1085 Magnesium

1090 Manganese

1100 Molybdenum

1105 Nickel


10155916 Metals by ICP - AES

7-;--

;k1: r ir. i >

I Si, ~;-r'







As of 1/9/2017 this list supercedes all previous lists for this certificate number. Solids EPA 6010D

EPA 6020

EPA 6020A

1125 Potassium

1140 Selenium

1990 Silica as Si02

1145 Silicon

1150 Silver

1155 Sodium

1160 Strontium

2017 Sulfur

1165 Thallium

1175 Tin

1180 Titanium

1185 Vanadium

1190 Zinc

1005 Antimony

1010 Arsenic

1015 Barium

1020 Beryllium

1030 Cadmium

1040 Chromium

1050 Cobalt

1055 Copper

1075 Lead

1090 Manganese

1100 Molybdenum

1105 Nickel

1140 , Selenium

1150 Silver

1165 Thallium

1170 Thorium

1175 Tin

3035 Uranium

1185 Vanadium

1190 Zinc

1005 Antimony

1010 Arsenic

1015 Barium

1020 Beryllium

1030 Cadmium

1040 Chromium

1050 Cobalt

10156000

10156408

Inductively Coupled Plasma-Mass Spectrometry



45 of 70






As of 1/9/2017 this listSoMdS ERA 6020A

EPA 6020B 2014

supercedes all previous lists for this certificate number.1055 Copper

1075 Lead

1090 Manganese

1100 Molybdenum

1105 Nickel

1140 Selenium - -

1150 Silver •

1165 Thallium

1170 Thorium

1175 Tin

3035 Uranium

1185 Vanadium

1190 Zinc

10156420

1005 Antimony

1010 Arsenic

1015 Barium

1020 Beryllium

1030 Cadmium

1040 Chromium

1050 Cobalt

1055 Copper

1075 Lead

1090 Manganese

1100 Molybdenum

1105 Nickel

1140 Selenium

1150 Silver

1165 Thallium

1170 Thorium

1175 Tin

3035 Uranium

1185 Vanadium

1190 Zinc


EPA 6860

1895 Perchlorate

10304800 Perchlorate in Water, Soils and Solid Wastes Using Ion Chromatography/Electrospray lonization/Mass Spectrometry

EPA 7471A

1095 Mercury

IUIDOCUO mercury in ounu was it? uyAtomic Absorption




TestAmerica Denver

4955 Yarrow St.

Arvada, CO 80002

EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 7471B

1095 Mercury

10166402 Mercury by Cold Vapor AtomicAbsorption

EPA 8011;•

10173009 1,2-Dibromoethane and 1,2-Dibromo-3- chloropropane by Microextraction and GC/ECD

5180 1,2,3-Trichloropropane - ■


4580 Dibromochloropropane

EPA 8015B



4750 Ethanol



4895 Isopropyl alcohol (2-Propanol, Isopropanol)

9488 Jet Fuel

4930 Methanol

9499 Motor Oil


5055 n-Propanol

EPA 8015C



4720 Diethylene glycol (2,2-Oxybisethanol)

4750 Ethanol

4785 Ethylene glycol



4895 Isopropyl alcohol (2-Propanol, Isopropanol)

9488 Jet Fuel

4930 Methanol

9499 Motor Oil


5055 n-Propanol

6657 Propylene Glycol

9646 Triethylene Glycol

EPA 8015D


10305609 Nonhalogenated Organics UsingGC/FID

4750 Ethanol




47 Of 70






As of 1/9/2017 this listSolidS EPA8015D

EPA 8021B

EPA 8081A

supercedes all previous lists for this certificate number.4895 Isopropyl alcohol (2-Propanol,

Isopropanol)

9488 Jet Fuel

4930 Methanol

9499 Motor Oil


5055 n-Propanol

10174808




4375 Benzene

4475 Chlorobenzene

4765 Ethylbenzene

5240 m+p-xylene


5005 Naphthalene

5250 o-Xylene

5140 Toluene

5260 Xylene (total)

10178606

8580 2,4'-DDD

8585 2,4'-DDE

8590 2,4'-DDT

7355 4,4-DDD

7360 4,4'-DDE

7365 4,4'-DDT

7025 Aldrin

7110 alpha-BHC (alpha-Hexachlorocyclohexane)


7115 beta-BHC (beta-Hexachlorocyclohexane)



7105 delta-BHC

7405 Diallate

7470 Dieldrin

7510 Endosulfan I

7515 Endosulfan II


7540 Endrin


Aromatic and Halogenated Volatiles by GC with PID and/or ECD Purge & Trap

Organochlorine Pesticides by GC/ECD


o*“2U OREGONEnvironmental Laboratory Accreditation Program

ORELAPID: 4025ORELAP Fields of Accreditation

TestAmerica Denver

4955 Yarrow St.


EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 8081A 7535 Endrin ketone


7245 gamma-Chlordane ,

7685 Heptachlor

7690 Heptachlor epoxide^



7725 Isodrin

7740 Kepone

7810 Methoxychlor

7870 Mirex


8310 tris-(2,3-Dibromopropyl) phosphate (tris-BP)

EPA 8081B 10178800 Organochlorine Pesticides by GC/ECD

8580 2,4'-DDD

8585 2,4'-DDE

8590 2,4'-DDT

7355 4,4-DDD

7360 4,4'-DDE

7365 4,4-DDT

7025 Aldrin

7110 alpha-BHC (alpha- Hexachlorocyclohexane)


7115 beta-BHC (beta- Hexachlorocyclohexane)



7105 delta-BHC

7405 Diallate

7470 Dieldrin

7510 Endosulfan I

7515 Endosulfan II


7540 Endrin


7535 Endrin ketone



7685 Heptachlor




nELt OREGONEnvironmental Laboratory Accreditation Program


TestAmerica Denver

4955 Yarrow St.

ORELAP ID: 4025

EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 8081B

EPA 8082


7725 Isodrin

7740 Kepone

7810 Methoxychlor

7870 Mirex


8310 tris-(2,3-Dibromopropyl) phosphate (tris-BP)

10179007

8880 Aroclor-1016 (PCB-1016)

8885 Aroclor-1221 (PCB-1221)

8890 Aroclor-1232 (PCB-1232)

8895 Aroclor-1242 (PCB-1242)

8900 Aroclor-1248 (PCB-1248)

8905 Aroclor-1254 (PCB-1254)

8910 Aroclor-1260 (PCB-1260)

8912 Aroclor-1262 (PCB-1262)

8913 Aroclor-1268 (PCB-1268)

EPA 8082A 10179201

8880

8885

8890

8895

8900

8905

8910

8912

_________________ 8913

EPA 8141A










10182000

7045 Anilazine

7065 Atrazine

7070 Azinphos-ethyl (Ethyl guthion)


7125 Bolstar (Sulprofos)

7220 Carbophenothion

7300 Chlorpyrifos

7315 Coumaphos

7390 Demeton

7395 Demeton-o

7385 Demeton-s

7410 Diazinon


Polychlorinated Biphenyls (PCBs) by GC/ECD

Polychlorinated Biphenyls (PCBs) by GC/ECD

Organophosphorous Pesticides byGC/NPD







As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 8141A

EPA 8141B

7475 Dimethoate

8625 Disulfoton

7550 EPN

7570 Ethoprop , '

7580 Famphur

7600 Fensulfothion 1

7605 Fenthion

7770 Malathion

7785 Merphos


7850 Mevinphos

7905 Naled

8290 0,0,0-Triethyl phosphorothioate


7985 Phorate

8000 Phosmet (Imidan)

8060 Propazine

8110 Ronnel

8125 Simazine

8155 Sulfotepp

8200 Tetrachlorvinphos (Stirophos, Gardona) Z-isomer


8245 Tokuthion (Prothiophos)

8275 Trichloronate

7045 Anilazine

7065 Atrazine

7070 Azinphos-ethyl (Ethyl guthion)


7125 Bolstar (Sulprofos)

7220 Carbophenothion

7300 Chlorpyrifos

7315 Coumaphos

7390 Demeton

7395 Demeton-o

7385 Demeton-s

7410 Diazinon


7475 Dimethoate

8625 Disulfoton

7550 EPN

7570 Ethoprop

10182204 Organophosphorous Pesticides by GC/NPD


51 of 70



Test America Denver EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 8141B 7580 Famphur

7600 Fensulfothion

7605 Fenthion

7770 Malathion

7785 Merphos >


7850 Mevinphos

7905 Naled


7985 Phorate

8000 Phosmet (Imidan)

8110 Ronnel

8125 Simazine

8155 Sulfotepp

8200 Tetrachlorvinphos (Stirophos, Gardona) Z-isomer


8245 Tokuthion (Prothiophos)

8275 Trichloronate

EPA 8151A

8655 2,4,5-T

10183207

8545 2,4-D

8560 2,4-DB

8555 Dalapon

8595 Dicamba


7775 MCPA

7780 MCPP

8645 Picloram

8650 Silvex (2,4,5-TP)

Chlorinated Herbicides by GC/ECD

EPA 8260B


5185 1,1,1 -T richloro-2,2,2-trifluoroethane

5160 1,1,1-Trichloroethane

5110 1,1,2,2-T etrachloroethane

5195 1,1,2-Trichloro-1,2,2-trifluoroethane(Freon 113)

5165 1,1,2-Trichloroethane

5167 1,1,2-Trichlorofluoroethane

5172 1,1,2-Trifluoroethane

5171 1,1-Dichloro-1-fluoroethane

4630 1,1-Dichloroethane

4640 1,1 -Dichloroethylene

10184802 Volatile Organic Compounds by purge and trap GC/MS


«EU OREGONEnvironmental Laboratory Accreditation Program


TestAmerica Denver

4955 Yarrow St.


ORELAP ID: 4025

EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number. SolidS EPA8260B 4670 1,1-Dichloropropene

1,2,3-T richlorobenzene

1.2.3- T richloropropane

1.2.3- Trimethylbenzene1.2.4- Trichloroberizene •- ') i

‘1,2,4-Trimethylbenzene ' ' -

1,2rDibromo-3-chloropropane (DBCP)

1.2- Dibromoethane (EDB, Ethylene dibromide)

1.2- Dichloro-1,1,2,2-tetrafluoroethane (Freon-114)

1.2- Dichloro-1,1,2-trifluoroethane


1.2- Dichloroethane (Ethylene dichloride)









1 -Chloro-1,1 -difluoroethane

1-Chlorohexane

2,2-Dichloro-1,1,1 -trifluoroethane (Freon 123)

4665 2,2-Dichloropropane

4410 2-Butanone (Methyl ethyl ketone, MEK)

4411 2-Chloro-1,1,1-trifluoroethane

4500 2-Ghloroethyl vinyl ether ;

4535 2-Chlorotoluene

4860 2-Hexanone (MBK)

5020 2-Nitropropane

5045 2-Pentanone

4540 4-Chlorotoluene

4910 4-lsopropyltoluene (p-Cymene)

4995 4-Methyl-2-pentanone (MIBK)

4315 Acetone

4320 Acetonitrile


4340 Acrylonitrile

4355 Allyl chloride (3-Chloropropene)

4375 Benzene

4385 Bromobenzene

5150

5180

5182

51555210'

4570

4585

4695

4697

4610

4635

4655

6800

5215

4615

4660

4675

4620

4735

4919

4510

5222


53 Of 70

aEL4

ORELAPID: 4025






As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 8260B 4390 Bromochloromethane

4395 Bromodichloromethane

4400 Bromoform

„ 4450 Carbon disulfide ,r

4455 Carbon tetrachloride i .

4475 Chlorobenzene, -- ~ V ,

4575 Chlorodibromomethane

4577 Chlorodifluoromethane (Freon-22)

4485 Chloroethane (Ethyl chloride) _ .

4486 Chlorofluoromethane

4505 Chloroform

4522 Chloropentafluoroethane

4525 Chloroprene (2-Chloro-1,3-butadiene)

4526 Chlorotrifluoroethene /

4705 cis & trans-1,2-Dichloroethene


4680 cis-1,3-Dichloropropene

4600 cis-1,4-Dichloro-2-butene

4555 Cyclohexane

4560 Cyclohexanone



4627 Dichlorofluoromethane (Freon 21)

4725 Diethyl ether

9375 Di-isopropylether (DIPE)

4750 Ethanol

4755 Ethyl acetate

4810 Ethyl methacrylate

4765 Ethylbenzene

4795 Ethylene oxide

4770 Ethyl-t-butylether (ETBE) (2-Ethoxy-2- methylpropane)

4772 . Fluoromethane (Freon 41)


4870 lodomethane (Methyl iodide)


4895 Isopropyl alcohol (2-Propanol,Isopropanol)

4900 Isopropylbenzene (Cumene)

5240 m+p-xylene

4925 Methacrylonitrile

4940 Methyl acetate

4950 Methyl bromide (Bromomethane)

4960 Methyl chloride (Chloromethane)


54 Of 70

ow« OREGONEnvironmental Laboratory Accreditation Program


TestAmerica Denver

4955 Yarrow St.

ORELAP ID: 4025

EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number.SoMdS EPA8260B 4990 Methylmethacrylate


4965 Methylcyclohexane

4975 Methylene chloride (Dichloromethane)

5245 m-Xylene ‘ ( ; ~

5005 Naphthalene


; 4435 n-Butylbenzene

4855 n-Hexane

EPA 8260B SIM

5090 n-Propylbenzene

5250 o-Xylene

5035 Pentachloroethane

5080 Propionitrile (Ethyl cyanide)

9579 Propylene oxide

5255 p-Xylene

9607 sec-Butyl Alcohol (2-Butanol)

4440 sec-Butylbenzene

5100 Styrene

4370 T-amylmethylether (TAME)

4420 tert-Butyl alcohol

4445 tert-Butylbenzene

5115 Tetrachloroethylene (Perchloroethylene)

5120 Tetrahydrofuran (THF)

9574 Tetrahydrothiophene

5140 Toluene

4027 Total BTEX

5205 Total trihalomethanes

4700 trans-1,2-Dichloroethylene

4685 irans-1,3-Dichloropropylene

4605 trans-1,4-Dichloro-2-butene

5170 Trichloroethene (Trichloroethylene)

5175 Trichlorofluoromethane(Fluorotrichloromethane, Freon 11)

5225 Vinyl acetate

5235 Vinyl chloride

5237 Vinyl Fluoride

5260 Xylene (total)

10184904


EPA 8270C 10185805

6703 1,1'-Biphenyl (BZ-0)


Volatile Organic Compounds by purge and trap GC/MS-SIM

Semivolatile Organic compounds by GC/MS


55 Of 70

oEU

ORELAPID: 4025


ORELAP Fields of^Accreditation




As of 1/9/2017 this list supercedes all previous lists for this certificate number.SolidS EPA8270C. 5155 1,2,4-Trichlorobenzene


6221 1,2-Diphenylhydrazine

6885 1,3,5-Trinitrobenzene'(1,3,5-TNB)

4615 1,3-Dichlorobenzene :

6160 1,3-Dinitrobenzene (1,3-DNB)-

4620 1,4-Dichlorobenzene , , /

/ 6165 1,4-Dinitrobenzene .

4735 1,4-Dioxane (1,4-Diethyleneoxide)

. 6420 1,4-Naphthoquinone





4659 2,2-Oxybis(1-chloropropane)

6735 2,3,4,6-Tetrachlorophenol


6840 2,4,6-TrichlOrophenol







5515 2-Acetylaminofluorene

9322 2-Butoxyethanol


5800 2-Chlorophenol

5866 2-Ethoxyethanol (cellosolve)

6360 2-Methyl-4,6-dinitrophenol (4,6-Dinitro-2-methylphenol)

5145 2-Methylaniline (o-Toluidine)1




6460 2-Nitroaniline

6490 2-Nitrophenol







6465 3-Nitroaniline


56 Of 70

HEUOWO OREGON


ORELAP Fields of „noi:Accreditation ORELAP ID: 4025




As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 8270C 6365 4,4-Methylenebis(2-chloroaniline)

5540 4-Aminobiphenyl

5660 4-Bromophenyl phenyl ether (BDE-


5745 4-Chloroaniline -

5825 ) \4-Chlorophenyl phenylether

6105 4-Dimethyt aminoazobenzene

6410 . 4-Methylphenol (p-Cresol)

6470 4-Nitroaniline

6500 4-Nitrophenol

6510 4-Nitroquinoline 1 -oxide


6112 6-Methylchrysene



5500 Acenaphthene

5505 Acenaphthylene

5510 Acetophenone

4330 Acrylamide

7005 Alachlor

4357 alpha-Methytstyrene

5545 Aniline

5555 Anthracene

5560 Aramite

7065 Atrazine

5562 Azobenzene

5570 Benzaldehyde

5567 Benzenethiol (Phenylmercaptan)

5595 Benzidine


5580 Benzo(a)pyrene

5605 Benzo(e)pyrene




5610 Benzoic acid

5630 Benzyl alcohol





7180 Caprolactam

5680 Carbazole


57 of 70

HELt0^sb3* OREGONEnvironmental Laboratory Accreditation Program


TestAmerica Denver

4955 Yarrow St.


ORELAP ID: 4025

EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA8270C 7210 Carbofuran phenol


5855 Chrysene

5862 Cresols, Total -


7405 Diallate

9354 , Dibenz(a, h) acridine



5890 Dibenzo(a.e) pyrene

5905 Dibenzofuran


7475 Dimethoate





6205 Diphenylamine

8625 Disulfoton


7580 Famphur

6265 Fluoranthene

6270 Fluorene

6275 Hexachiorobenzene





6312 Indene


7725 Isodrin

6320 Isophorone

6325 Isosafrole

6345 MethapyrileneI6375 Methyl methanesulfonate


5010 n, n-Dimethyl formamide

5005 Naphthalene

5875 n-Decane

6300 n-Hexadecane

5015 Nitrobenzene



58 Of 70



TestAmerica Denver

4955 Yarrow St.

Arvada, CO 80002

ORELAP ID: 4025

EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number.SoMdS EPA8270C 6530

5025

6545

6535

6550

6555

6560

6565

8290

5550

5553

7955

6590

5035

6600

6605

6615

6625

7985

6635

6640

9663

6650

6665

6670

6685

8155

8235

5200

8310

EPA 8270C SIM

n-Nitrosodimethyl amine

n-Nitroso-di-n-butyl amine

n-Nitrosodi-n-propylamine

n-Nitrosodiphenylamirie , . n-Nitrosomethylethalamine ' , -,

n-Nitrosomorpholirie' '—’ ' - ,x - " \ \ - ■n-Nitrosopiperidine ■ , .

n-Nitrosopyrrolidine ,

o,o,o-Triethyl phosphorothioate

o-Anisidine

Octachlorostyrene

Parathion, ethyl

Pentachlorobenzene '

Pentachloroethane

Pentachloronitrobenzene

Pentachlorophenol

Perylene

Phenacetin

Phenanthrene

Phenol

Phorate

Phthalic acid

Phthalic anhydride

p-Phenylenediamine

Pronamide (Kerb)

Pyrene

Pyridine

Quinoline

Safrole

Sulfotepp

Thioriazin (Zinophos) .

Triethylamine

tris-(2,3-Dibromopropyl) phosphate (tris- BP)

10242407

4735

6380

6385

5500

5505

5555

5575

5580

1,4-Dioxane (1,4- Diethyleneoxide)

1 -Methylnaphthalene

2-Methylnaphthalene

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene

Semivolatile Organic compounds by GC/MS Selective Ion Monitoring


59 of 70

oELd OREGONEnvironmental Laboratory Accreditation Program


TestAmerica Denver

4955 Yarrow St.

ORELAP ID: 4025

EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number.SoMdS EPA8270C 5605 Benzo(e)pyrene

SIM 5590 Benzo(g,h,i)perylene


5585 Benzo[b]fluoranthene'


5855 Chrysene ' ' • ' ■ • ’ - .


5895

5905

6070

6135

5925

6200

6265

6270

6315

5005

6525

6530

6545

6535

6615

6665

Dibenz(a,h) anthracene

Dibenzofuran

Diethyl phthalate

Dimethyl phthalate


Di-n-octyl phthalate

Fluoranthene

Fluorene

lndeno(1,2,3-cd) pyrene

Naphthalene ^

n-Nitrosodiethylamine

n-Nitrosodimethylamine

n-Nitrosodi-n-propyl amine

n-Nitrosodiphenylamine

Phenanthrene

Pyrene

EPA 8270D 10186002

6703

6715

5155

4610

6221

6885

4615

6160

4620

6165

4735

6420

6630

5790

6380

6425

4659

6735

1,1’-Biphenyl (BZ-0)

1,2,4,5-Tetrachlorobenzene



1.2- Diphenylhydrazine

1.3.5- Trinitrobenzene (1,3,5-TNB)


1.3- Dinitrobenzene (1,3-DNB)


1.4- Dinitrobenzene


1.4- Naphthoquinone

1.4- Phenylenediamine

1 -Chloronaphthalene


1-Naphthylamine

2,2-Oxybis(1 -chloropropane)

2,3,4,6-Tetrachlorophenol

Semivolatile Organic compounds by GC/MS


60 Of 70



TestAmerica Denver

4955 Yarrow St.


ORELAP ID: 4025

EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number.SoMdS EPA8270D 6835 2,4,5-Trichlorophenol



6130 2,4-Dimethylphenol ;


6185 2,4-Dinitrotoluene (2,4-DNT) - ' ; . ' ■'

6005 ■ 2,6-Dichlorophenol

6190 ' 2,6-Dinitrotoluene (2,6-DNT)

5515 2-Acetylaminofluorene /


5800 2-Chlorophenol


5145 2-Methylaniline (o-Toluidine)




6460 2-Nitroaniline

6490 2-Nitrophenol



5945 3,3’-Dichlorobenzidine




6465 3-Nitroaniline

6365 4,4-Methylenebis(2-chloroaniline)

5540. 4-Aminobiphenyl




5825 4-Chlorophenyl phenylether ■



6470 4-Nitroaniline

6500 4-Nitrophenol

6510 4-Nitroquinoline 1-oxide




5500 Acenaphthene

5505 Acenaphthylene

5510 Acetophenone

5545 Aniline


61 Of 70

owo OREGONEnvironmental Laboratory Accreditation Program

ORELAPID: 4025ORELAP Fields of Accreditation

TestAmerica Denver

4955 Yarrow St.


EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number.SoMdS EPA 8270D

5560 Aramite

5562 Azobenzene

5570 Benzaldehyde .

5595 Benzidine

5575 Benzo(a)anthracene ---- -

5580 Benzo(a)pyrene




5610 Benzoic acid

5630 Benzyl alcohol





7180 Caprolactam

5680 Carbazole


5855 Chrysene

8906 Coelution - 3-Chlorophenol + 4- Chlorophenol

5862 Cresols, Total


7405 Diallate



5905 Dibenzofuran


7475 Dimethoate





6205 Diphenylamine

8625 Disulfoton


7580 Famphur

6265 Fluoranthene

6270 Fluorene




62 Of 70

HEU OREGONEnvironmental Laboratory Accreditation Program


TestAmerica Denver

4955 Yarrow St.

Arvada, CO 80002

ORELAP ID: 4025

EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA8270D 6285 Hexachlorocyclopentadiene



6315 lndeno(1,2.3-cd) pyrene .. .....

7725 Isodrin ' '6320 Isophorone -----J . ' y';

6325 Isosafrole

, 6345 Methapyrilene

x 6375 Methyl methanesulfonate


- 5005 Naphthalene

5015 Nitrobenzene



5025 n-Nitroso-di-n-butylamine


6535 n-NitrosodiphenylamineI 6550 n-Nitrosomethylethalamine

6555 n-Nitrosomorpholine

6560 n-Nitrosopiperidine

6565 n-Nitrosopyrrolidine

8290 o,o,o-Triethyl phosphorothioate



5035 'Pentachloroethane

6600 Pentachloronitrobenzene


6610 Phenacetin

6615 Phenanthrene

6625 Phenol ,

7985 Phorate .

9663 p-Phenylenediamine

6650 Pronamide (Kerb)

6665 Pyrene

5095 Pyridine

6685 Safrole

8155 Sulfotepp


EPA8270D 10242509SIM

4735

6380

6385

5500

1,4-Dioxane (1,4- Diethyleneoxide)


2-Methylnaphthalene

Acenaphthene

Semivolatile Organic compounds by GC/MS Selective Ion Monitoring


63 Of 70

owo OREGONEnvironmental Laboratory Accreditation Program


TestAmerica Denver

4955 Yarrow St.


ORELAP ID: 4025

EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 8270D

SIM5505 Acenaphthylene

EPA 8310

5555 Anthracene


5580 Benzo(a)pyrene I f


5600 Benzo(k)fluoranthene ~ - -

5585 Berizo[b]fluoranthene


5855 Chrysene



5905 Dibenzofuran





6265 Fluoranthene

6270 Fluorene


5005 Naphthalene



6615 Phenanthrene

6665 Pyrene



5500 Acenaphthene

5505 Acenaphthylene

5555 Anthracene r


5580 Benzo(a)pyrene




5855 Chrysene


6265 Fluoranthene

6270 Fluorene


5005 Naphthalene

6615 Phenanthrene

10187607 Polynuclear Aromatic Hydrocarbons by HPLC/UV-VIS


64 Of 70






As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 8310 6665 Pyrene

EPA 8321A

6885 1,3,5-Tririitrobehzene (1,3,5-TNB) /

6160 7 1,3-Dinitrobenzene (1;3-DNB) ~ - V

6014 ’ 2,3-Dinitrotoluene

/-, 8655 . - 2,4,5-T

' 9651 2,4,6-Trinitrotoluene (2,4,6-TNT)

8545 2,4-D

~ 8560 2,4-DB




9507 2-Nitrotoluene

9510 3-Nitrotoluene


9513 4-Nitrotoluene


, 7040 Aminocarb



7275 Chloropropham

8555 Dalapon

8595 Dicamba



7505 ': Djuron

7610 1 Fenuron

7630 Fluometuron

7765 Linuron (Lorox) ' '

7775 MCPA •:

7780 MCPP




7855 Mexacarbate)

7885 Monuron

7915 Neburon

5015 Nitrobenzene

6485 Nitroglycerin





TestAmerica Denver

4955 Yarrow St.


ORELAP ID: 4025

EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids ERA 8321A 9522 Octahydro-1,3,5,7-tetranitro-1,3,5,7-

tetrazocine (HMX)

EPA 8321B


9558 Pentaeryth ritoltetran itrate (P ETN)

8075 Propham •

8080 Propoxur (Baygon) .;


.8120 ; Siduron

8650 Silvex (2,4,5-TP)

6885 1,3,5-Trinitrobenzene(1,3,5-TNB)



8655 2,4,5-T


8545 2,4-D

8560 2,4-DB




9507 2-Nitrotoluene

9510 3-Nitrotoluene


9513 4-Nitrotoluene


7040 Aminocarb



7275 , Chloropropham

8555 Dalapon

8595 Dicamba



7505 Diuron

7610 Fenuron

7630 Fluometuron


7775 MCPA

7780 MCPP





66 Of 70

aELa OREGONEnvironmental Laboratory Accreditation Program



4955 Yarrow st. Certificate: 4025-006


As of 1/9/2017 this list supercedes all previous lists for this certificate number.SoMdS EPA 8321B 6415 Methyl-2,4,6-trinitrophenylnitramine

(tetryl)

7855 Mexacarbate

7885 Monuron

7915 Neburon

5015 Nitrobenzene ___ i '

6485 Nitroglycerin


6605' Pentachlorophenol


8075 Propham

8080 Propoxur (Baygon)


8120 Siduron

8650 Silvex (2,4,5-TP)

EPA 8330A 10190008

6885

6160

9651

5882

6185

6181

6190

9303

9507

9510

9306

9513

7046

6415

5015

6485

9522

9558

1899

9432

1.3.5- Trinitrobenzene (1,3,5-TNB)

1.3- Dinitrobenzene (1,3-DNB)

2.4.6- Trinitrotoluene (2,4,6-TNT)

2.4- diamino-6-nitrotoluene

2.4- Dinitrotoluene (2,4-DNT)

2.6- diamino-4-nitrotoluene

2.6- Dinitrotoluene (2,6-DNT)

2-Amino-4,6-dinitrotoluene (2-am-dnt)

2- Nitrotoluene

3- Nitrotoluene

4- Amino-2,6-dinitrotoluene (4-am-dnt)

4-Nitrotoluene

Ammonium Picrate

Methyt-2,4,6-trinitrophenylnitramine — (tetryl)

Nitrobenzene

Nitroglycerin

Octahydro-1,3,5,7-tetranitro-1,3,5,7- tetrazocine (HMX)

Pentaerythritoltetranitrate (PETN)

Picric Acid (2,4,6-Trinitrophenol)

RDX (hexahydro-1,3,5-trinitro-1,3,5- triazine)

Nitroaromatics and Nitramines by High Performance Liquid Chromatography (HPLC)

)


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«EU OREGONEnvironmental Laboratory Accreditation Program


TestAmerica Denver



As of 1/9/2017 this list supercedes all previous lists for this certificate number._________

ORELAP ID: 4025

EPACODE: C000026

Solids EPA 8330B 10308006 Nitroaromatics, Nitramines and Nitrate Esters by High Performance Liquid Chromatography (HPLC)


6160 1,3-Dinitrobenzene (1',3-DNBj,

9651 2,4,6-Trinitrotoluene (2,4,6-TNT) /' - -5882 , 2,4-diamino-6-nitrotoluene

6185 2,4-Dinitrotoluene (2,4-DNT)' 6181 2,6-diamino-4-nitrotoluene

v 6190 2,6-Dinitrotoluene (2,6-DNT)


9507 2-Nitrotoluene

6150 3,5-Dinitroaniline j

9510 3-Nitrotoluene


9513 4-Nitrotoluene


6415 Methyl-2,4,6-trinitrophenylnitr amine (tetryl)

5015 Nitrobenzene

6485 Nitroglycerin




>' ,9432 RDX (hexahydro-1,3,5-trinitro-1,3,5-

triazine)

EPA 9012A -

1645 : Total cyanide

10193405 Total and Amenable Cyanide (automated colorimetric with off-line distillation)

EPA 9012B • ' % .10243206 Total and Amenable Cyanide (automated colorimetric with off-linedistillation)

1645 Total cyanide

EPA 9030BJ

10195605 Acid-Soluble and Acid-Insoluble sulfides: Distillation

2005 Sulfide

EPA 9034

2005 Sulfide

10196006 Titrimetric Procedure for Acid-Soluble and Acid-Insoluble Sulfides

EPA 9045C

1900 pH

10198400 Soil and Waste pH

EPA 9045D

1900 pH

10244607 Soil and Waste pH


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ORELAP ID: 4025

TestAmerica Denver

4955 Yarrow St.

EPACODE: C000026



As of 1/9/2017 this list supercedes all previous lists for this certificate number.SoMdS EPA 9050A

1610 Conductivity

10198808 Specific Conductance

EPA 9056r " ■. rv ■-


1540 Bromide '• ' ' • ~ . j ' ;

1575 Chloride ..... /N

1730 t fluoride "■ ' j «' -... 1805 Nitrate

1835 Nitrite


2000 Sulfate

1825 Total nitrate+nitrite

EPA 9056A

1540 Bromide


1575 Chloride

1730 Fluoride

•1805 Nitrate


1835 Nitrite


2000 Sulfate

EPA 9060



EPA 9060A '

I 2040 Total organic carbon


EPA 9071B-

10201602 Oil and Grease Extraction Method for sludge and sediment samples

1803 n-Hexane Extractable Material (O&G)

1860 Oil & Grease

EPA 9095A

9822 Extraction/Preparation .

10204203 Paint Filter Liquids Test

NWTPH-Dx


90018409 Oregon DEQ TPH Diesel Range

9499 Motor Oil

8641 Percent Moisture

9506 Residual Range Organics (RRO)

2050 Total Petroleum Hydrocarbons (TPH)

NWTPH-Gx

•90018603 Oregon DEQ TPH Gasoline Range

Organics by GC/FID-PID Purge & Trap



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SM 2320 B-97 online


20045607 Alkalinity by Titration Method

SM 251 OB-97 online

1610 Conductivity '< ; ‘ ' /

20048606 Conductivity by Probe

SM 2540 B-97 online

1950 Residue-total

, , ; , 20049405 Total Solids Dried at 103 - 105C

SM 4500-CN C- 1999

1635 Cyanide

20095652/ Cyanide (Total) after Distillation/

SM 4500-CN E- 1999 ' "

1645 Total cyanide

20096417 Cyanide by Colorimetric Method

SM 4500-CN E- 2011 2011

1645 Total cyanide

20096428 Cyanide by Colormetric Method

SM 4500-CN'C-97 online

1645 Total cyanide

20095607 Cyanide by Total Cyanide afterDistillation

SM 4500-N02" 20113104 Nitrite by Colorimetric DeterminationB-2000 online

1835 Nitrite

1840 Nitrite as N


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TestAmericaTHE LEADER IN ENVIRONMENTAL TESTING

TestAmerica Denver

Electronic Document Cover

The electronic copy of this document, as maintained on the TestAmerica Denver computer network, is the controlled copy. Any printed copy becomes uncontrolled,

and all work performed should ultimately reference the controlled electronic version.

Any printed or electronic copy of this document that is distributed external to TestAmerica Denver becomes uncontrolled; To arrange for automatic updates to

this document, contact TestAmerica Denver.

TestAmerica Laboratories, Inc. TestAmerica Denver 4955 Yarrow Street Arvada, CO 80002

Phone: 303-736-0100 Fax: 303-431-7171

DenverTestAmericaTHE LEADER IN ENVIRONMENTAL TESTING

SOP No. DV-QA-003P, Rev. 11Effective Date: 10/31/2016

Page No.: 1 of 35

Electronic Copy Only

Title: Quality Control Program

Copyright Information:This documentation has been prepared by TestAmerica Laboratories, Inc. and its affiliates (“TestAmerica”), solely for their own use and the use of their customers in evaluating their qualifications and capabilities in connection with a particular project. The user of this document agrees by its acceptance to return it to TestAmerica upon request and not to reproduce, copy, lend, or otherwise disclose its contents, directly or indirectly, and not to use it for any other purpose other than that for which it was specifically provided. The user also agrees that where consultants or other outside parties are involved in the evaluation process, access to these documents shall not be given to said parties unless those parties also specifically agree to these conditions.

THIS DOCUMENT CONTAINS VALUABLE CONFIDENTIAL AND PROPRIETARY INFORMATION. DISCLOSURE, USE OR REPRODUCTION OF THESE MATERIALS WITHOUT THE WRITTEN AUTHORIZATION OF TESTAMERICA IS STRICTLY PROHIBITED. THIS UNPUBLISHED WORK BY TESTAMERICA IS PROTECTED BY STATE AND FEDERAL LAW OF THE UNITED STATES. IF PUBLICATION OF THIS WORK SHOULD OCCUR THE FOLLOWING NOTICE SHALL APPLY:

©COPYRIGHT 2016 TESTAMERICA LABORATORIES, INC. ALL RIGHTS RESERVED.

Facility Distribution No. Distributed To:


Page No.: 2 of 35

1.0 Purpose /

1.1 The purpose of this policy is to describe TestAmerica Denver’s program of routine analytical quality control (QC) activities. The objective is to generate QC data that demonstrate that the analytical process is in control and that the data meet client and method requirements.

1.2 The policy outlines QC requirements for a variety of regulatory programs, with the stipulation that lacking specific direction from our clients, TestAmerica Denver will default to routine “commercial” QC requirements as described in this policy.

2.0 Scope

2.1 This procedure provides a consistent approach for evaluating and maintaining routine analytical QC activities. This document has been prepared to assure compliance with The NELAC Institute (TNI) Standard, dated 2009, Volume 1 Modules 2 and 4, and the ISO/IEC Guide 17025:2005(E). All requirements established here are to be enforced and followed throughout the laboratory.

2.2 Every staff member at TestAmerica Denver plays an integral part in quality control activities and is held responsible and accountable for the quality of their work. It is, therefore, required that all laboratory personnel are trained and agree to comply with applicable procedures and requirements established by this document.

2.3 Federal program requirements are not covered in this procedure. SOP DV-QA- 024P, Requirements for Federal programs provides specific requirements for the Department of Defense Environmental Accreditation Program (DoD ELAP) and the Department of Energy (DOE) programs. When performing analyses for DoD ELAP, or DOE projects, DV-QA-024P shall be consulted to ensure that program- specific requirements are met.

3.0 Safety

3.1 There are no specific safety hazards associated with this SOP.

3.2 During the course of performing this procedure it may be necessary to go into laboratory areas to consult with appropriate staff members, therefore employees performing this procedure must be familiar with the Laboratory Health & Safety Plan, and take appropriate precautions and wear appropriate attire and safety glasses.

4.0 Definitions

4.1 Acceptance Criteria: The specified limits placed on characteristics of an item, process, or service defined in requirement documents.

4.2 Accuracy: The degree of agreement between an observed value and anaccepted reference value. Accuracy includes a combination of random error (precision) and systematic error (bias) components which are due to sampling and analytical operations; a data quality indicator.

COMPANY CONFIDENTIAL AND PROPRIETARY


Page No.: 3 of 35■©

4.3 Batch: Environmental samples that are prepared and/or analyzed together with the same process and personnel, using the same lot(s) of reagents.

4.3.1 A preparation batch is composed of one (1) to twenty (20) environmental samples of the same quality systems matrix, meeting the above mentioned criteria and with a maximum time between the start of processing of the first and last sample in the batch to be twenty-four (24) hours. When a batch is closed and a new batch is opened, QC samples must not be shared across multiple LIMS batch numbers that are prepared at different times. Each LIMS preparation batch must have its own QC samples.

NOTE 1: Field samples prepared at different dilutions (initial volume < nominal volume specified in the method) are not duplicates and must be counted as separate samples toward the batch count of20.

NOTE 2: For some procedures where the analytical results from the same extract can be reported using different analysis method codes, the samples are prepared in the same QC batch and then assigned to a different TALS prep batch number. Traceability to the analyst, original reagents, materials, and equipment must be maintained.

NOTE 3: When samples need to be filtered by the lab, the samples and associated batch QC must all be filtered. A filtration batch must not exceed 20 samples.

4.3.2 An analytical batch is composed of prepared environmental samples (extracts, digestates or concentrates) which are analyzed together as a group. An analytical batch can include prepared samples originating from various quality system matrices and can exceed twenty (20) samples. (Analyses with no separate preparation are limited to 20 field samples.)

4.4 QC Batch: The QC batch is a set of up to 20 field samples plus associatedlaboratory QC samples (both positive and negative controls) that are similar in composition (matrix) and that are processed within the same time period using the same reagents and standard lots. )

4.5 Calibration: A set of operations that establish, under specified conditions, the relationship between values of quantities indicated by a measuring instrument or measuring system, or values represented by a material measure or a reference material, and the corresponding values realized by standards.

4.6 Corrective Action: The action taken to eliminate the causes of an existingnonconformity, defect, or other undesirable situation in order to prevent recurrence.

4.7 Detection Limits and Quantitation Limits

NOTE: DoD ELAP program delineates three detections limits (DL, LOD and LOQ) see SOP DV-QA-024P for additional information.


4.7.1 Limit(s) of Detection (LOD) [a.k.a., Method Detection Limit (MDL)]: Alaboratory's estimate of the minimum amount of an analyte in a given matrix that an analytical process can reliably detect in their facility. This is defined as the minimum concentration of a substance (an analyte) that can be measured and reported with 99% confidence that the analyte concentration is greater than zero and is determined from analysis of a sample in a given matrix containing the analyte.

4.7.2 Limit(s) of Quantitation (LOQ) [a.k.a., Reporting Limit]: The minimum levels, concentrations, or quantities of a target variable (e.g., target analyte) that can be reported with a specified degree of confidence.

4.7.3 Lower Limit of Quantitation (LLOQ): The lowest concentration at which the laboratory has demonstrated target analytes can be reliably measured and reported with a certain degree of confidence, which must be > the lowest point in the calibration curve. The LLOQ is equivalent to the standard reporting limit. The required LLOQ verification is performed at a concentration of 1-2 times the LLOQ (or RL).

4.8 Instrument/Calibration Blank: A clean sample (e.g., distilled water, hexane, methylene chloride, etc.) processed through the instrumental steps of the measurement process; used to determine instrument contamination.

NOTE: For procedures without a separate preparation step for aqueous samples, an instrument blank is equivalent to the method blank, and serves the same purpose.

4.9 Laboratory Control Sample (however named, such as laboratory fortified blank, spiked blank, or QC check sample): A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes, taken through all preparation and analysis steps of the procedure unless otherwise noted in a reference method. It is generally used to establish intra-laboratory or analyst specific precision and bias or to assess the performance of all or a portion of the measurement system.

, 4.9.1 An LCS shall be prepared at a minimum of one per batch of 20 or fewersamples per matrix type per sample extraction or preparation method.

4.9.2 QC samples are purchased and used as an LCS for methods that are not easily spiked into solution such as total suspended solids, total dissolved solids, pH or turbidity.

4.9.3 Sample duplicates serve as the batch QC for methods where spiking solutions are not available such as total volatile solids, total solids, color, dissolved oxygen, settable solids or moisture. An LCS is not prepared for these methods.

4.10 Laboratory Control Sample Duplicate (LCSD): A duplicate laboratory control sample must be prepared if there is insufficient sample volume received to prepare and analyze an MS/MSD pair or sample duplicate. Some clients may require an


Page No.: 4 of 35


LCSD to be reported for their samples. LCS/LCSD pairs provide information regarding the precision of the measurement process.

4.11 Matrix Spike (spiked sample or fortified sample): A sample prepared, takenthrough all sample preparation and analytical steps of the procedure unless otherwise noted in a referenced method, by adding a known amount of target analyte to a specified amount of a field sample for which an independent test result of targetanalyte concentration is available. Matrix spikes are used, for example, to determine the effect of the matrix on a method's recovery efficiency..

4.12 Matrix Spike Duplicate (spiked sample or fortified sample duplicate): Areplicate matrix spike prepared and analyzed to obtain a measure of the precision of the recovery for each analyte.

NOTE: Due to the potential variability of the matrix of each sample, the MS and MSD results may not have immediate bearing on any samples except the one spiked and possible for samples from the same site.

4.13 Measurement System: An analysis or test method, as implemented at aparticular laboratory, which includes the equipment and reagents used to perform the method.

4.14 Method Blank: A sample of a matrix similar to the batch of associated samples (when available) that is free from the analytes of interest and is processed simultaneously with and under the same conditions as samples through all steps of the analytical procedures, and in which no target analytes or interferences are present at concentrations that impact the analytical results for sample analyses.

4.15 Precision: The degree to which a set of observations or measurements of the same property obtained under similar conditions, conform to themselves; a data quality indicator. Precision is usually expressed as standard deviation, variance or range, whether absolute or in relative terms.

4.16 Sample Duplicate: A sample duplicate is a second aliquot of a field sample, taken from the same sample container when possible, that is processed with the first aliquot of that sample. That is, sample duplicates, using the same size aliquot from the sample container for each replicate, are processed as independent samples within the same QC batch. The sample duplicate does not count toward the maximum batch count of 20 samples. The sample and duplicate results are compared to determine the effect of the sample matrix on the precision of the analytical process.

NOTE: Field samples that go thorough a preparation process at different dilutions are not considered duplicates and must be counted as separate samples toward the batch count of 20.

4.17 Spike: A known amount of target analyte added to a blank sample or sub-sample; used to determine recovery efficiency or for other quality purposes.


Page No.: 5 of 35


4.18 Surrogate: A substance with properties that mimic the analyte of interest. It is unlikely to be found in environment samples and is added to them for quality control purposes.

4.18.1 Surrogate compounds must be added to air samples, standards, and blanks, for all organic chromatography methods except when the matrix precludes its use or when a surrogate is not available. Poor surrogate recovery may indicate a problem with sample composition and shall be reported to the client whose sample produced poor recovery.

4.19 Working Range: The difference between the Limit of Quantitation and the upper limit of measurement system calibration.

Procedure

5.1 Assessments of QC data relative to established control limits determine the acceptability of sample test results. Whenever control criteria are not met, the data must be evaluated to determine appropriate corrective action. Corrective action decisions, particularly whether or not to reanalyze samples, should be done in consultation with the client to the extent possible when operating under project- specific QA plans.

5.2 TestAmerica Denver’s standard QC program shall be communicated to the client prior to acceptance of work. Alternative QC procedures may be required depending on the clients’ special project requirements. In the event that alternative QC procedures are not specified by our clients, the standard QC protocols specified in this policy must be followed to ensure the generation of legally and scientifically defensible analytical data.

5.3 TestAmerica Denver’s QC Program applies to the following:

5.3.1 RCRA and SW-846 Projects - All routine analytical projects performed using SW-846 methods must comply with the requirements described in TestAmerica Denver’s Quality Assurance Manual (QAM) and this policy. The Quality Control sections of analytical standard operating procedures (SOPs) referencing SW-846 methods must be consistent with the requirements in this policy.

5.3.2 CWA and 40 CFR Part 136 Projects - Any analytical work conducted in support of an NPDES permit or other Clean Water Act (CWA) compliance activities, must meet applicable quality control specifications as summarized in the QAM. The quality control requirements listed in the QAM define the minimum requirements that must be given in laboratory analytical SOPs.

5.3.3 Method specific QC requirements that are more restrictive than the requirements defined in this policy take precedence. For example, a method that requires the MS/MSD be performed every 10 samples sets the number of samples in the QC batch to 10, not 20.

SOP No. DV-QA-003P, Rev. 11Effective Date: 10/31 /2016

Page No.: 6 of 35


Other Programs or Projects with Clearly Defined QC Requirements

5.4.1 The differences between TestAmerica Denver’s standard QC program and special project requirements must be specified in project documents. These documents may include Quality Assurance Project Plans (QAPPs), Sampling and Analysis Plans (SAPs), project-specific Quality Assurance Summaries (QASs), SOPs, contracts, protocols, or other approved documents.

NOTE: Specific requirements for federal programs are not covered in this document and can be found in TestAmerica Denver’s SOP DV- QA-024P QA/QC Requirements for Federal Programs.

5.4.2 Documents describing special project requirements must be reviewed and approved by appropriate QA and operations staff.

5.4.3 If the special project requirements appear to result in modifications that contradict TestAmerica policies or procedures, a variance must be requested in writing and communicated to the client. A record of this communication and acceptance of the variance must be retained as a permanent part of the project file.

5.4.4 Any special client’s project requirements must be communicated to TestAmerica Denver’s analysts in advance of releasing samples for analysis, and the work must be clearly differentiated in the analytical documentation, otherwise this policy’s requirements will be followed.

Laboratory QC Method Requirements

NOTE: Analytical SOPs must include a quality control section that addresses these general QC requirements as well as method-specific requirements. Method-specific requirements are given precedence to these general requirements and are noted accordingly.

5.5.1 The proficiency of a method is defined by its precision, bias (accuracy), limit of quantitation, limit of detection, and working range.

5.5.2 The limit of quantitation (LOQ) is established as the standard reporting limit at the time of calibration and is typically defined as the lowest level standard that is used in the method calibration. Alternatively, the LOQ may be defined in relation to an established lower limit of detection (LOD), i.e., method detection limit (MDL). See SOP DV-QA-009P, Reporting Limits, for additional information.

5.5.3 The working range is established by the difference between the Limit of Quantitation and the upper limit of measurement system calibration.

5.5.4 The method detection limit (MDL) must be initially determined in accordance with Policy DV-QA-005P. The MDL must be verified annually at a minimum. Quarterly verification is required for specific programs (DOD ELAP and Texas TRRP).


Page No.: 7 of 35

* COMPANY CONFIDENTIAL AND PROPRIETARY

5.5.5 Prior to using a method for actual samples and at any time there is a change in instrument type, personnel, or test method, a NELAC-compliant demonstration of capability (IDOC) must be performed by the analyst(s) who will be performing the method in accordance with SOP DV-QA-0024. The analyst must analyze spiked control samples and achieve recoveries within prescribed acceptance criteria. For methods where spiked samples are not appropriate, the DOC consists of demonstration of a properly performed QC batch. Acceptable results from analysis of blind PTs or QC samples may also be used for the CDOC. Analysts performing a method must demonstrate their continued proficiency annually.

5.5.6 Evaluation of LCS data over the long term establishes the precision and bias of the analytical method free of any matrix interference. See section5.9 for details on the determination of limits.

Batch QC Elements and Batch Processing

5.6.1 A QC batch is designed to allow assessment of the quality, in terms of accuracy and precision, of the analytical results obtained for a group of up to 20 field samples. Every batch must include both accuracy and precision. With some exceptions as described in Sections 5.6.6 and 5.6.7 below, the minimum QC elements for each QC batch consist of the following:

• one method blank (MB),

• one laboratory control sample (LCS),

• one sample duplicate (DUP) [where applicable],

• one matrix spike (MS), and

• one matrix spike duplicate (MSD).

NOTE: If there is insufficient sample for an MS/MSD or sample duplicate, an LCSD must be performed.

5.6.2 The identity of each QC batch must be documented and traceable, i.e., each batch of field samples must be clearly associated with the applicable QC samples.

5.6.3 To the extent possible, samples that require a preparation step should be analyzed together with their associated QC samples. If the samples in a given QC batch require separate analytical runs, the minimum batch QC in each run is an acceptable MB or instrument/calibration blank. To the extent possible, the QC samples should not be analyzed independently of the field samples on a different instrument.

5.6.4 For analytical procedures that do not include a separate extraction or digestion (e.g., volatile organic analysis by purge and trap), the QC batch must be analyzed sequentially using the same instrument and instrument configuration within the same calibration event. That is, the same calibration curve, calibration factors, or response factors must be in effect throughout the analysis.


Page No.: 8 of 35


5.6.5 Field QC samples (e.g., trip blanks, equipment rinsates, and field duplicates) count as individual samples, therefore, they add to the QC batch count. Samples that require simple reanalysis (e.g., dilutions to adjust a sample extract to the working range of the instrument), as opposed to re-extraction or digestion and reanalysis, do not count as additional samples in the QC batch. For procedures without a separate preparation, a reanalysis within the same calibration event (as defined in Section 5.6.4) does not add to the batch count.

5.6.6 Although MS/MSD pairs are the preferred measure of precision, they are not the only acceptable means of demonstrating precision.

5.6.6.1 As requested by clients or as method required, batch precision may also be demonstrated through the analysis of sample duplicates. The client should be advised that a sample duplicate is less likely to provide usable precision statistics depending on the likelihood of finding concentrations above reporting limits.

5.6.6.2 A duplicate LCS (LCSD) may be used to demonstrate method batch precision independent of the client’s matrix. LCSDs may be prepared at the client’s request, but must be used when there is no client specified MS and MSD, or sample duplicate in the batch.

5.6.6.3 On-going monitoring of LCS results can be used to determine long-term precision and accuracy for a method independent of matrix effects.

5.6.6.4 MS and MSDs are to be prepared, analyzed and reported at the same dilution as the parent sample.

5.6.7 Some methods, including isotope-dilution methods, pH, and ignitability, for example, do not use all of the QC elements listed in Section 5.6.1. Method exceptions to these requirements are listed in the laboratory’s analytical SOPs.

5.6.8 Deviations from these QC elements must be noted either in project planning documents (QAPPs, SAPs, SOWs, QAS, or equivalent) or in a nonconformance memo (see SOP DV-QA-0031 for details).

Data Evaluation and Corrective Action)

5.7.1 General Guidelines\

5.7.1.1 Any QC component that fails acceptance criteria is considered an out-of-control event. All out-of-control events must be documented and the associated data evaluated. Depending on the specific circumstances, evaluation can lead to a variety of actions. The following sections and the flowcharts (Figures 1-4) describe the appropriate corrective actions for the most common QC failures. However, it is not possible to address all possible data evaluation scenarios in this policy. The guiding principle for

SOP No. DV-QA-003P, Rev. 11i Effective Date: 10/31/2016

Page No.: 9 of 35


all evaluations is that the data and corrective action decisions must be defensible using TestAmerica Denver policies, procedures, or scientific evidence, and justified in the project records.

5.7.1.2 If reanalysis for QC failures is conducted and the second analysis confirms a QC problem that is outside of the laboratory’s control, further testing is not necessary. The problem must be documented and the data properly qualified in. the analytical report.

5.7.1.3 QC failures that require reanalysis are documented in TestAmerica Denver’s electronic nonconformance system, as described in SOP DV-QA-0031.

5.7.1.4 QC failures due to sample matrix interferences (particularly sample duplicate, and sample surrogate failures) must be documented and the data properly qualified in the analytical report.

5.7.1.5 The laboratory does not control on MS/MSD recoveries or RPDs. However, the laboratory must ensure that significant failures are not due to laboratory error such as a missed spike, double spike or incorrect integration. MS/MSD failures due to laboratory error must be corrected. See Section 5.7.6.2 for additional corrective actions.

5.7.1.6 When ongoing, systematic problems are identified, work must stop until it can be demonstrated that the system is in control again.

5.7.2 Method Blank (MB) Evaluation (see Figure 1)

5.7.2.1 Method Blank Acceptance Criteria

5.7.2.1.1 When appropriate for the specific analytical method, the results of the method blank shall be one of the QC measures used to assess batch acceptance. SW-846 guidance is to have no detectable contaminants in the method blank, i.e., the method blank result must be less than or equal to the MDL for each target analyte. However, this may not be practically achievable in a laboratory setting, and method blank contamination between the MDL and the laboratory’s reporting limit may not have an adverse affect on data quality. Each method blank must be critically evaluated as to the nature of the interference and the effect on the analysis of each sample in the batch.

5.7.2.1.2 TestAmerica Denver policy is that the method blank is acceptable as long as all analytes of interest are less than one-half the laboratory’s reporting limit (RL) for


Page No.: 10 of 35


organic, metals, and some wet chemistry analyses, unless otherwise specified by specific projects or clients or listed here.

5.7.2.1.3 For the following list of wet chemistry analytes, a method blank is acceptable if the analytes of interest are less than the reporting limit:

AlkalinityBODCODHEMHEM SGT TDSTOC soils

5.7.2.1.4 When the method blank result is above the acceptance limit, the results for the associated samples may be accepted with qualification if the method blank meets one of the following criteria, unless otherwise prescribed by project-specific requirements:

• The concentration of the analyte of concern in the method blank is less than or equal to 10% (1/10) of the regulatory limit for that analyte, or

• The concentration of the analyte of concern in the method blank is less than or equal to 10% (1/10) of the measured concentration of that analyte in the sample, or

• The same analyte was not detected above the MDL in the associated samples (and therefore the apparent contamination in the blank did not represent corresponding elevated values in the samples).

NOTE: Positive method blank results slightly below thereporting limit should still be evaluated by the analyst for potential impact on sample results at or near the reporting limit.

5.7.2.2 Corrective Action for Method Blank Failure

5.7.2.2.1 If the method blank does not meet the acceptance criteria, the source of contamination must be investigated and measures taken to correct, minimize, or eliminate the problem.


Page No.: 11 of 35


5.7.2.2.2 Samples associated with the contaminated blank shall be reprocessed for analysis or may be reported as qualified (qualifier flags or narrative comments).

5.7.2.2.3 If the contaminant is a common laboratory contaminant (see the table below) and the MB concentration is less than 5 times the RL for organics or less than the RL for metals samples may be reported.

NOTE: Some programs do not recognize common laboratorycontaminants.

Common Laboratory Contaminants


Page No.: 12 of 35

Analyte Method

Methylene Chloride Volatile Organics (GC or GC/MS)

Acetone Volatile Organics (GC or GC/MS)

2-Butanone Volatile Organics (GC or GC/MS)

Phthalate Esters Semi-Volatile Organics (GC or GC/MS)

Calcium Metals (ICP)

Sodium Metals (ICP)

Zinc Metals (ICP or ICP-MS)

Iron Metals (ICP or ICP-MS)

5.7.3 Laboratory Control Samples (LCS) Evaluation (see Figure 2)

5.7.3.1 LCS Acceptance Criteria

5.7.3.1.1 The LCS recovery for the control analytes must be within established control limits. Unless otherwise specified in a reference method or project requirements, the control limits are set at ± 3 standard deviations around the mean of the historical data. Regardless of the calculated limit, the limit should be no tighter than the Calibration Verification (CCV) [unless the analytical method specifies a tighter limit],

5.7.3.1.2 An LCS that is determined to be within acceptance criteria effectively demonstrates that the analytical system is in control and validates system performance for the samples in the associated batch.

5.7.3.1.3 The LCS percent recovery is calculated as follows:

, „ _ measured valueLCS Percent Recovery =-------------------- x 100%

expected value



Page No.: 13 of 35

5.7.3.2 Marginal Exceedance

5.7.3.2.1 If there are a large number of reported analytes in the LCS, as is the case for many organic analyses, then NELAC allows a specified number of results to fall beyond the LCS control limit (3 standard deviations), but within the marginal exceedance (ME) limits.

5.7.3.2.2 Marginal exceedance limits are set at ± 4 standard deviations around the mean of historical data (marginal exceedance limits are posted in the Outlook public folders under Public FoldersNAII Public Folders\Analytical\Denver\NELAC-Marginal Exceedance Tables.

5.7.3.2.3 The number of marginal exceedances is based on the number of reported analytes in the LCS, as shown in the following table:

Marginal Exceedance Allowances

# of Reported Analytes in LCS

# of Allowed Marginal Exceedances

>90 5

71 -90 4

51-70 3

31 -50 2

11-30 1

<11 0

5.7.3.2.4 If more analytes exceed the LCS control limits than is allowed, or if any analyte exceeds the ME limits, the LCS fails and corrective action is necessary.

5.7.3.2.5 Marginal exceedances must be random. If the same analyte repeatedly fails the LCS control limits, it is an indication of a systematic problem. The source of the error must be identified and corrective action taken.

5.7.3.3 Corrective Action for LCS Failure

5.7.3.3.1 Samples analyzed along with an LCS that is determined to be “out of control” are considered suspect and the samples must be reprocessed and reanalyzed, or the data reported with appropriate data qualification. If the LCS result does not fall within statistical control limits, check calculations, check instrument performance, reanalyze the LCS, and if still


outside of control limits, re-prepare and reanalyze all samples in the QC batch.

5.7.3.3.2 It is acceptable to report the data if the LCS recovery is out high and any analyte of concern was not detected in any of the samples.

5.7.3.3.3 In the case of volatile analyses, if the LCS fails, a new LCS may be re-prepared and reanalyzed within the same tune period.

5.7.3.3.4 In the case where all target requested analytes are within control, but some other LCS compounds are out of control, the LCS may still be considered acceptable for reporting.

5.7.3.3.5 See Figure 2 for additional detail.

5.7.4 Duplicate Laboratory Control Samples (LCSD or DCS) Evaluation (see Figure 2) ,

5.7.4.1 LCS/LCSD Acceptance Criteria

5.7.4.1.1 The recovery for each analyte in the LCS and LCSD must be within established control limits as described in Section 5.7.3.1. If either LCS fails, the samples must be reprocessed and reanalyzed, or the data reported with appropriate data qualification. LCS and/or LCSD failures must be described in the final report if samples are not reanalyzed.

5.7.4.1.2 The LCS precision is calculated as the relative percent difference (RPD) between the LCS and LCSD and must not exceed the established limit. Unless otherwise specified in the reference method or in project requirements, the limit is set at the mean of the historical RPD data plus three standard deviations. The RPD between the LCS and LCSD is calculated as follows:


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Where:

RPD =\LCS - LCSD]

{LCS + LCSD)x!00%

LCS = measured concentration for the LCS

LCSD = measured concentration for the duplicate LCS

5.7.4.2 Corrective Action for LCS/LCSD Recovery (Accuracy) Failure


See Section 5.7.3.3 for corrective actions for LCS recovery failures.

NOTE: If either the LCS or the LCSD spike fails and the batch cannot be reprepared and/or reanalyzed, the failure must be documented and noted in the final report.

5.7.4.3 Corrective Action for LCS/LCSD Precision Failure

Because the LCS/LCSD precision limits are based on the standard deviation of data collected over time and include longterm precision, it would be unusual to fail precision limits while meeting accuracy limits. If this occurs with any frequency, control limits should be reevaluated. For any single precision failure, check calculations; verify, if possible, that the LCS and LCSD were spiked correctly; check instrument performance; and if the RPD is out of control but both accuracy recoveries are within acceptance criteria, prepare an NCM, and qualify the reported results.

5.7.5 Surrogate Evaluation (see Figure 3)

5.7.5.1 Acceptance Criteria

Surrogate recovery must be within established control limits. Unless otherwise specified in a reference method or project requirements, the control limits are set at ± 3 standard deviations around the mean of the historical data for QC samples. Method QC (MB, LCS, and/or LCSD) results are not acceptable unless the surrogate recoveries for those QC samples are within control limits. If MS/MSD, duplicate, or field samples require dilutions beyond the threshold stated in the analytical SOPs, routine surrogate control limits do not apply and recoveries are not evaluated. This should be noted in the final report. The surrogate recovery is calculated as follows:


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Surrogate Percent Recovery =measured value

expected valuexl00%

5.7.5.2 Corrective Action for Surrogate Failure

Corrective action must be considered for any surrogate failure. Analysts and data reviewers must review specific project instructions to be certain that the required actions are taken. Lacking instructions to the contrary, the following guidelines apply:

• Check calculations and instrument performance.

• Failed Surrogates in QC Samples: Evaluate the surrogate results together with the QC sample results for all QC samples in the batch to determine whether associated samples should


be re-prepared and reanalyzed. Refer to Figures 1 through 4 for details. For example, consistent surrogate failures in all the QC samples in a batch indicate a method failure. Surrogate failures in only one QC sample in a batch may indicate a problem with that one sample only, especially if surrogate recoveries fall within limits for all other samples in the batch. Document the failure and evaluation in the final report.

• Failed Surrogates in Field Samples: Refer to Figure 3.

5.7.6 Matrix Spike and Matrix Spike Duplicates (MS/MSD) Evaluation (see Figure 4)

5.7.6.1 MS/MSD Acceptance Criteria

The MS and MSD recoveries for control analytes should be within established control limits, which are either mandated in the published methods or regulatory programs, or are set at ± 3 standard deviations around the mean of historical LCS data. In addition, the relative percent difference (RPD) between the MS and MSD results should be less than or equal to the established upper control limit. If MS or MSD samples require dilutions


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MS or MSD %Recovery = 'SSR-SR'

K SA ,x!00%

beyond the threshold stated in the analytical SOPs, routine control limits do not apply and recoveries are not evaluated, but this should be noted in the final report. The RPD between the MS and MSD is calculated the same way as the RPD between the LCS and LCSD, as shown in Section 5.7.4.1.2. The MS and MSD recoveries are calculated using observed concentrations (except as noted below):

Where:

SSR = observed concentration in spiked sample

SR = observed concentration in unspiked sample

SA = concentration of spike added to sample

NOTES:

1. If the sample result is ND, then SR = 0 when no values are reported below RL.

2. If the sample result is reported as a value less than the RL, then SR = the reported value.

3. CLP forms software uses observed recovery, not concentrations.



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5.7.6.2 Over Range Matrix Spikes

5.7.6.2.1 When the parent sample result and the MS/MSD concentration are above the linear range, the MS/MSD and parent sample MUST be reanalyzed at a dilution. These samples must be analyzed at the same dilution.

5.7.6.2.2 If the analyte concentration in the parent sample is greater than four times the concentration of spike added, then spike recovery results are not compared to control limits. The recovery is either reported as “NC” (not calculated) or with a qualifier flag to indicate that the spike was swamped by the native analyte concentration in the sample. If the analyte concentration in the parent sample is greatly above the spike concentration such that the dilution may cause the spike to be less than two times the reporting limit, the matrix spike does not need to be diluted and is reported as “NC” (not calculated).

5.7.6.3 Parent Sample is within Working Range and Matrix Spike(s) are Over Range - No client requested MS/MSD in Batch

When the parent sample result is within the working range of the method and the matrix spikes are over range and the MS/MSD serves as batch QC for all samples in the batch (no client requested MS/MSD) the laboratory will report the result for the sample from the original analysis together with the spike result qualified to indicate that it was an over range measurement (e.g., E-flag qualifier).

5.7.6.4 Parent Sample is within Working Range and Matrix Spike(s) are Over Range - Client-requested MS/MSD in Batch

When the parent sample result is within the working range of the method and the matrix spikes are over range and the MS/MSD was client-requested the laboratory will reanalyze the parent samples and MS/MSDs at the same dilution. If the analyte concentration in the parent sample is greater than four times the concentration of spike added, then spike recovery results are not compared to control limits. The recovery is either reported as “NC” (not calculated) or with a qualifier flag to indicate that the spike was swamped by the native analyte concentration in the sample.

5.7.6.5 For multi-analyte tests, if only a few of the target analytes are in the upper half of the curve causing a few of the MS/MSD to be over-range, diluting the sample may result in loss of information in the MS/MSD for all but one or a few analytes. Consult with the PM if needed to assure that the client receives data that serves their needs.


5.7.6.6 Corrective Action for MS/MSD Recovery (Accuracy) Failure

As noted previously, matrix spike data are meaningful only for the sample in which they are prepared and possibly for samples from the same site. The information obtained from MS data are sample/matrix specific and are not normally used to determine the validity of the entire batch. If the MS and/or MSD recovery falls outside of the established control limits, the bracketing CCV and batch LCS recoveries must be within control limits in order to accept results for the associated samples. The following corrective actions are required for MS/MSD recovery failures to rule out lab error:

• Check calculation and instrument performance;

• Verify, if possible, that the MS and MSD were spiked correctly (e.g., very low or very high recoveries);

• Consider objective evidence of matrix interference (e.g., heterogeneous sample, interfering peaks seen on chromatograms, or interference demonstrated by prior analyses);

• Flag the data for any results outside of acceptance limits.

• For any single RPD failure, check calculations; verify, if possible, that the MS and MSD were spiked correctly; check instrument performance; consider objective evidence of matrix interference or sample inhomogeneity; and flag the data.

• If both the parent sample and associated matrix spike results are over range the parent and the spikes shall be diluted by the same amount and the results from the reanalysis reported for both. If the analyte concentration in the parent sample is greater than four times the concentration of spike added, then spike recovery results are not compared to control limits, and the recovery is either reported as “NC” (not calculated) or with a qualifier flag to indicate that the spike was less than four times the analyte concentration in the sample. If the dilution will cause the spike to be less than two times the reporting limit, the MS/MSD do not need to be diluted and the recovery reported as “NC” (not calculated).

• For MS/MSD that serve as batch QC, if the parent sample result is within the calibration range and the MS/MSD results are above the calibration range, the results are reported with the MS/MSD result being flagged as an over-range measurement (e.g., the E-flag qualifier).

• If the MS/MSD are client requested, the parent sample result is within calibration range and the MS/MSD results are above the calibration range, the sample and spike should be diluted, keeping in mind that we need to assess whether or not the dilution will best serve the client’s needs. Consult with the PM as needed. Both the parent sample and MS/MSD samples


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must have the same dilution factor. Some EDDs do not accept data that are at different dilution factors.

• If the native analyte concentration in the MS/MSD sample exceeds 4 times the spike level for that analyte, the recovery data are reported as NC (i.e., not calculated) and the appropriate qualifier flags are added.

• See Figure 4 for additional detail.

NOTE: See Denver Policy Memorandum P16-001 and Corporate Policy Memorandum CA-Q-QM-013 for more detail.

NOTE: Some client programs require reanalysis to confirm matrix interferences. Check special project requirements for this corrective action.

5.7.6.7 Corrective Action for MS/MSD Precision Failure

For any single precision failure, check calculations; verify, if possible, that the MS and MSD were spiked correctly; check instrument performance; consider objective evidence of matrix interference or sample inhomogeneity; and flag the data if no lab errors are found. If lab errors are identified take appropriate corrective action to resolve the error.

5.7.7 Sample Duplicate

5.7.7.1 Sample Duplicate Acceptance Criteria

The RPD between the sample and its duplicate must be within established control limits. The RPD between the sample and its duplicate is calculated the same way as the RPD between the LCS and its duplicate, as shown in Section 5.7.4.1.2.

5.7.7.2 Corrective Action for Duplicate Failure

For any single precision failure, check calculations and instrument performance. Document the QC failure in an NCM and note it on the final report.

Reporting Uncertainty with Measurements

It is the responsibility of the project manager to notify the appropriate laboratory personnel whenever the uncertainty for a given analyte is to be' reported. It is the responsibility of the laboratory personnel to calculate and report the uncertainty for each analyte requested in accordance with the procedures in this section

NOTE: The laboratory does not have an automated reporting mechanism for reporting the uncertainty associated with each measurement. Reporting


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this information would require project-specific arrangements to accommodate manual calculation and manual reporting.

5.8.1 Procedure

5.8.1.1 Determine the average and standard deviation of a minimum of twenty recovery results. Calculate the relative standard deviation (RSD) as follows:

5.8.1.2 The average percent recovery (Xavg) and the standard deviation (SD) can be derived from the control limits (at the 99% confidence interval):

Where: UCL=upper control limit, LCL= lower control limit

5.8.1.3 Calculate the uncertainty (U(X)) associated with an analytical result as follows:

5.8.2 Example Calculation

The analytical result for phenol is 120 pg/L. The control limits for phenol are 33-122%. The average recovery for phenol is 77.5% with a standard deviation of 14.8%. The average percent recovery and the standard deviation can be derived from the control limits (at the 99% confidence interval).

1) Calculate the average percent recovery:

RSD = SD /Xavg

Xavg = (UCL + LCL)/2

#U (X) = C+ (2 X RSD X C)

Where: C = Sample Concentration

Xavg= (122+33)/2 = 77.5

2) Calculate the Standard Deviation:

SD = 14.8

Standard Deviation



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where:

s = series number

7 = point number in series s

m = number of series for point y in chart

n - number of points in each series

X® = data value of series s and the ith point

Ny - total number of data values in all series

M = arithmetic mean

3) Calculate the RSD: 14.8/77.5=0.19

4) Calculate the uncertainty of the analytical result

U (x) = 120 + (2 x 0.19 x 120) = 165.6

U (x) = 120 - (2 x 0.19 x 120) = 74.4

5) Report the analytical result as 120 pg/L with an uncertainty range of74.4 pg/L to 165.6 pg/L at the 95% confidence interval.

Establishing QC Acceptance Limits

5.9.1 Initial Control Limits

For new procedures, published method limits can be used until sufficient QC data are acquired (a minimum of 20 to 30 data points recommended). However, the published limits may not be appropriate if they are based on a single-operator or single-laboratory study. In this case, the QA Manager may establish default limits until enough data are collected to calculate statistical limits.

5.9.2 TALS Control Chart Program

5.9.2.1 Evaluating control charts is an important first step in considering new control limits. Control charts are generated by TALS Control Chart program. The program collects a specified set of QC data, calculates the mean and three standard deviation control limits, compares those limits to the existing limits in the LIMS, and generates an l-type control chart (ref. ASTM D 6299). This control chart is a plot of results, in chronological order, to which existing control limits and a centerline have been added. The control chart aids in the examination of the data to be sure that it is representative and appropriate for use in setting new limits. See the TALS User Guide (Training Brief CW-l-T-001) Control Charts

for complete details on how to pull control charts. Some specific requirements include the following:



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5.9.2.2 Select QC Type Options

QC Type Description

MB Used to evaluate method baselines, laboratory background levels or possible issues with laboratory contamination. This may also be used to set MDLs.

LCS/LCSD Used to establish LCS/LCSD/MS/MSD control limits.

MS/MSD Used to assess matrix-specific control limits. This is used for evaluation purposes only. MS/MSD limits are set based on LCS/LCSD control limits.

MB/LCS/LCSDSurrogates

This option will produce a pooled set of LCS/LCSD and MB recoveries. There is an option to include or not include client samples. In addition control charts can be generated for just client samples.

5.9.2.3 Representative Time Period

The appropriate time period depends bn the frequency with which the test is performed and the frequency of other events, such as calibrations and standards preparation. A minimum of three months is desirable to capture data from multiple instruments, multiple instrument tunes, multiple calibrations, and multiple standard preparations. For infrequent tests, it may be necessary to collect nine months or more of data. However, collecting more than 100 data points is normally unnecessary, makes the control charts hard to read, and may result in abnormally tight control limits.

5.9.2.4 Documentation of Control Chart Review

When the control chart is obtained, select the “Save Log” button and answer “YES” to the two successive questions that are presented. This should be done any time control charts are reviewed, regardless of whether limits need to be changed, as described below.

5.9.3 Grubbs’Test for Outliers

5.9.3.1 The Control Limits program automatically runs the Grubbs’ test for

5.9.3.2

outliers using a 5% level of significance, i.e., the risk of falsely rejecting a data point. The initial assumption is made that the data are normally distributed. The Grubbs’ test detects one outlier at a time, eliminates that outlier, and repeats the test until all outliers are eliminated. The test should not be used for sample sizes of six or less.

The test is defined for the hypothesis H0, there are no outliers in the data set, and Ha, there is at least one outlier in the data set.


The test statistic “G” is calculated as the ratio of the difference between the suspect point and the mean value to the calculated standard deviation, as follows:


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maxG =

Y-Y

Where:

Yi = the point being considered for rejection

Y = the mean value of the data set

s = the standard deviation

5.9.3.3 The hypothesis of no outliers, and consequently the suspect point, is rejected if

G >(n- l)-In l|

t,(al{2N),N-2)

N-2 + t,(al{2N),N-2)

Where:

N = number of points

t(a/(2N),N-2) = the critical value of the t-distribution with (N- 2)/2 degrees of freedom and a significance level of a/(2N).

NOTE: Tables for critical values of t are given in John Taylor, QualityAssurance of Chemical Measurements, Lewis Publishers; 1987. For a complete discussion of the Grubbs’ Test for Outliers also see NIST/SEMATECH e-Handbook of Statistical Methods, Section 4.3.5.1.7:http://www.itl.nist.gov/div898/handbook/eda/section3/eda35h.htm.

5.10 Evaluating and Investigating Collected Data

Assuming that an adequate amount of data are collected, the next step involves determining that the data set is representative of the laboratory’s performance, and therefore provides a useful prediction of future performance. A key part of the process is examining the data for bias, discontinuities, and/or trends. Ideally, if conditions are constant over the time period selected and existing limits are appropriate, the data will be evenly distributed around the centerline, with very few points outside control limits (i.e., less than 1 point in 100 should lie beyond the 3 standard deviation control limits). The reasons for deviations from the ideal should be investigated to be sure that the collected data are appropriate. Specific conditions requiring further investigation include data sets with no outliers, data with significant bias relative to existing limits, excessive number of outliers, discontinuous patterns, and upward or downward sloping trends


5.10.1 The laboratory must review the control charts annually for trends and/or changes in the system to evaluate whether or not a change in control limits is required. If the recalculated limits are consistent with the historical limits (±5%), the historical limits may remain unchanged.

NOTE: DoD QSM requires a quarterly review of a subset ofrepresentative analytes. See SOP DV-QA-024P for additional details.

5.10.2 No Outlier Data

If there are no outlier data and little or no data outside the 2-standard-deviation warning limits, then one of the following is true:

5.10.2.1 Insufficient data have been collected, which can be tested by generating charts using a longer time period.

5.10.2.2 Outlier data are being censored (not entered into TALS). Check with the analysts to verify this. Analysts should be told that not omitting statistical outliers (not blunders) is essential to avoid generating even tighter limits.

5.10.2.3 Existing limits are much too wide (possibly because the performance of the analytical system has significantly improved) and should be changed immediately (see Section5.11 on Establishing New Control Limits below).

NOTE: When evaluation is made relative to the warning limits, if thelimits were set using the CCV limits, the mean shown will not be the statistical mean of the data set but the midpoint of the limits. Hence the mean and warning limits do not reflect the statistical dataset.

5.10.3 Bias Relative to Existing Limits

If there are a significant majority of QC results falling on one side of thecenterline, then consider the following:

5.10.3.1 The procedure, equipment, or calibration may have changed. Verify the accuracy of the SOP with analysts.

5.10.3.2 The analyst’s skill level may have changed. Check with the supervisor to find out if new analysts might account for the bias.

5.10.3.3 Equipment may have been changed. Check with supervisor.

5.10.3.4 The standards used for calibration, including those used for internal standards, may have changed or may have been incorrectly prepared.


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5.10.3.5

V

SOP No. DV-QA-003P, Rev. 11 Effective Date: 10/31/2016

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The time since the limits were last set may be longer than six months, and an update to the control limits is overdue.

NOTE: When evaluation is made relative to the center line, if the limits were set using the CCV limits, the mean shown will not be the statistical mean of the data set but the midpoint of the limits. Hence the mean does not reflect the statistical dataset.

5.10.4 Excessive Number of Outliers

If significantly more than 1 point in 100 is outside the control limits, the following should be considered:

5.10.4.1 The variability in the analytical system may have changed significantly, either as the result of a specific event, or degradation in the instrumentation.

5.10.4.2 The existing limits may not be statistically based. Review control limits records to check the basis of the old limits.

5.10.4.3 Audit the method to verify the accuracy of the SOP, competency of the analysts, and reliability of the instrumentation.

5.10.4.4 Consult with the supervisor.

5.10.4.5 Compare laboratory’s performance to other laboratories. The Tri-Agency QSM limits is one source of limits by competent laboratories, other TestAmerica laboratories is another, and method limits have to be considered as well. Limits should not be widened if the laboratory’s performance is not consistent with other labs.

5.10.5 Discontinuous Pattern

If the data appear to run for a period at one mean recovery and then suddenly jump to a different level, then the following should be considered:

5.10.5.1 The accuracy of the analytical system experienced a statistically significant change, and most likely there is an event that caused that change, such as recalibration, change in instrument or instrument settings, change in calibration standards, change in methodology, or a change in analyst.

5.10.5.2 Consult with the supervisor.

5.10.5.3 Unless the discontinuity is characteristic of the method somehow, a decision will usually need to be made as to which mode of operation is the best predictor of future performance. A selective time period may be used for calculating


representative limits if no errors in standards, instrument performance, etc., are identified.

5.10.6 Upward or Downward Sloping Pattern

An upward or downward trend is typically indicative of an unstable instrument, a standard or reagent that is degrading sooner than its current expiration period or progressive changes in background or contamination levels. Such trends are early warning that the analytical system will soon be out of control. When a trend is detected, investigate as follows:

5.10.6.1 Consult with the supervisor, and have the supervisor consider the condition of standards, reagents and maintenance of equipment.

5.10.6.2 Review the SOP and check the proficiency of the analysts.

5.10.6.3 Reliable control limits cannot be set using data during an unstable period. Maintaining the old limits until a stable period is documented is probably the best course.

5.11 Establishing New Control Limits

Having collected sufficient data and determined that the data are representative, the next step is to establish the new limits. See Work Instruction WI-DV-0097

Control Limit Review and Updating for additional details. Control limits are set at ± 3 standard deviations around the mean of the collected data with the following exceptions:

5.11.1 If the calculated 3-standard-deviation limits are tighter than the method calibration verification criteria (e.g., CCV acceptance limits for ICP are ± 10% of the expected value), then the new limits are set to the mean value ± the calibration acceptance limits.

5.11.2 If the calculated limits are wider than method or program requirements, then the laboratory’s performance should be reconsidered. If the limits are marginally wider, inspect the control chart to estimate the frequency of failures using the program limits. If, based on the control chart, the failure rate is predicted to be low (less than 2% is normally acceptable), then program limits might be adopted. Otherwise the laboratory will need to either not offer the test or request a variance.

5.11.3 If the lower control limit is very low, e.g., less than 10%, there is a concern about accepting data that is not quantitatively reliable. The minimum lower control limit must be elevated to 10%. If inspection of the control chart data indicates that the failure rate will be high at a LCL of 10%, the method should be evaluated for improvements that may mitigate a high failure rate. An exception to the lower limit of 10% is benzidine which is set to a minimum acceptance limit of 5%.


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5.11.4 If the upper control limit is less than 100% recovery plus the method calibration verification acceptance limit, then adjust the upper limit to 100% plus the calibration acceptance limit. For example, if CCV acceptance limits are ± 10% of the expected value, then set the upper control limit to 110%.

5.11.5 The basis of the new control limits must be documented Additionally, annotation may be made directly on the printed control charts or control limits reports, and must be signed and dated or the information conveyed to the QA Manager in an email.

5.12 Communicating and Implementing New Control Limits

5.12.1 When the group leader identifies a need to update limits, a request is sent by email to the QA department for a review of the limits.

5.12.2 The email should contain the control chart data (or location of the file), identification of analytes that require updates, and rationale for the change.

5.12.3 A member of the QA group will review the request and update the appropriate method limit group with the new limits (if necessary).

5.12.4 The QA department and the group leader will confirm a date that the instrument data systems and the LIMS will be updated. The CSO group will be notified of the changes.

5.13 Reporting QC Data

QC data that are routinely reported with sample results include the LCS, method blank, and surrogate standards. Client reporting format requirements are negotiable and documented as part of the project records. Ultimately, all reporting decisions should accommodate the client’s requirements as long as data integrity is maintained.

Responsibilities

6.1 Successful implementation of this QC program requires that it is clearly understood by all TestAmerica staff. Training based on this policy will be conducted periodically and provided to new personnel as appropriate for their functions.

6.2 Project Managers

6.2.1 The laboratory project managers (PMs) serve as a liaison between the clients and the laboratory staff to ensure that requirements are properly communicated in writing to both parties.

6.2.2 The PM communicates any QC problems to clients and documents decisions made with clients.


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6.3 Analytical Groups

6.3.1 The analytical groups are responsible for the evaluation of control limits, frequently in conjunction with data review software and/or senior analysts or supervisors.

6.3.2 Analytical groups shall review control chart data and notify QA when limits need to be updated as needed.

6.4 QA Group

6.4.1 The QA manager can establish default control limits until enough data points are collected to calculate statistical limits.

6.4.2 The QA staff shall review the statistical limits when the analytical groups request for updates to the control limits.

6.4.3 After coordinating a date and time with the analytical groups, the QA staff will update the control limits in the TestAmerica Denver LIMS system. See WI-DV-0097 Control Limit Updates.

6.4.4 The QA staff will evaluate all limits on an annual basis to ensure that appropriate limits are set and as a verification of the reviews performed by the laboratory groups.

6.4.5 The QA staff will verify and track the quarterly control chart reviews completed by the analytical groups. The reviewer shall document the date of review and notify the group leader and operations manager when reviews are past due.

References / Cross-References

7.1 Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, USEPA SW-846, 3rd Edition, with promulgated updates, Chapter One, Quality Control.

7.2 2009 TNI Standard, Management and Technical Requirements for Laboratories Performing Environmental Analysis, Volume 1, The NELAC Institute.

7.3 A2LA Guidance for the Estimation of Uncertainty for testing” Thomas Adams, July 2002 (from the A2LA website)

7.4 ASTM D 6299, Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance, Volume 5.03.

7.5 John Taylor, Quality Assurance of Chemical Measurements, Lewis Publishers; 1987.

7.6 NIST/SEMATECH e-Handbook of Statistical Methods, http://www.itl.nist.gov/div898/handbook/eda/section3/eda35h.htm, April 1,2012.



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8.0 Attachments

Figure 1: Method Blank EvaluationFigure 2: LCS/LCSD EvaluationFigure 3: Surrogate Evaluation xFigure 4: Matrix Spike/Matrix Spike Duplicate Evaluation

9.0 Revision History

• Revision 11, dated 31 October 2016

o Removed references to AFCEE throughout o Removed reference to DV-QA-020P as this SOP was discontinued, o Added definition of Lower Limit of Quantitation6 Added requirement for assessment for batch precision by use of MS/MSD, sample

duplicate or LCS/LCSD throughouto Modified section 4.9.1 and added sections 4.9.2 and 4.9.3 - clarification/detail on

LCSso Added Calcium to the Common Laboratory Contaminants table in section 5.7.2.2.3 o Added Sections 5.7.6.2-5.7.6.4 to describe how to handle parent sample and

MS/MSD dilutions; renumbered remainder of sections o Revised Section 5.7.6.6 to describe corrective actions for MS/MSD recovery

failures to rule out lab erroro Added notes to Sections 5.10.2 and 5.10.3 to caution that when limits set to CCV

limits the mean and warning limits displayed on the control chart do not reflect the statistically determined limits

o Added reference to work instruction WI-DV-0097 Control Limit Review and Updating to section 5.11

o Added section 6.4.5 to state QA responsibility to track compliance with quarterly control chart review

o Editorial and formatting changes throughout

• Revision 10, dated 31 October 2015

o Revised Section 4.3.1 to clarify assignment of samples from one prep batch to accommodate different analysis method codes that use the same prep and extract for analysis

o Added detail to section 4.10 to identify when LCSD is prepared, o Updated section 5.7.2.1.3 to include TOC soilso Updated reference to TALS User Guide on how to generate control charts in

Section 5.9.2o Added suggestion in Section 5.10.6 that a sloping pattern may result from standard

or reagent degradation and should be evaluated, o Added section 6.4.4 to QA Group responsibilities to review limits annually in

addition to analytical group review.

• Revision 9, dated 31 August 2014 N

o Changed title of SOP o Formatting and editorial changes throughouto Re-arranged document sections for consistency, better flow and easier

comprehension and corrected section references throughout o Added references to SOP DV-QA-024P and CW-l-T-001 where appropriate


o Split up original paragraph in Section 1 to be Sections 1.1 and 1.2. o Revised Section 2.0 to reflect the scope of the current document o Updated/revised definitions - aligned with QAM o Split up Section 4.3 to correct format and information o Updated Section 4.3.1 to reflect separate QC for separate batch numbers o Added note to Sections 4.7 and 4.16 o Removed previous Section 5.3 reference to DoD o Deleted previous Section 5.4.3 - SDWA reference o Added note to Section 5.4.1 o Added Section 5.7.3.2 o Deleted previous Section 5.6.5.1.2 o Revised Sections 5.6.6, 5.7.11, and 5.7.2.2 through 5.7.4 o Updated Section 5.9 o Updated Table 5.9.2.1 o Added Section 5.9.2.4o Integrated previous Attachment 1 information into the text of the SOP o Deleted previous Attachment 1 o Deleted previous Sections 5.6.5.3 and 5.6.5.4 o Added current Sections 5.10 through 5.11 o Updated current Section 5.12 to reflect current practices o Updated Section 5.13 that client requests for reporting QC data are followed so

long as data integrity is maintained, o Updated Section 6 to reflect current practices o Updated Figures 1 through 4 to current practices

Revision 8, dated 31 May 2013

o Revised section 4.3 to reflect current practiceo Clarified section 4.4 regarding differentiating what samples count toward the batch

count.o Added section 5.1.4 to clarify that method QC requirements take precedence over

this policy.o Revised 5.6.1.5 to reflect use of DOCs for tests without an LCS. o Revised section 5.6.3.2.1 to clarify method blank acceptance criteria for wet

chemistry methods.o Updated Section 5.6.3.2 DoD requirements to match QSM 4.2 o Corrected reference to public folders in section 5.6.3.3.1o Updated sections 5.6.3.6.2, 5.6.3.6.3 and Figure 4 to reflect policy change to flag

MS/MSD results rather than write NCM o Revised Sections 5.6.4.1 and 5.6.5.1.2 for clarity o Revised Figures to reflect changes to policy o Relabeled Figure 5 as Attachment 2 and updated form o Added references cited in text of SOP o Formatting and editorial changes throughout

Revision 7.3, dated 06 July 2012

o Removed criteria that the LOQ to be at least three times the LOD. o Updated sections 5.3.1.6 and 5.3.1.7 to meet current procedures, o Added requirement for limits to be reviewed annually by QA to section 5.3.1.6 and

5.3.1.7.o Updated Figures 2,3 and 4.


Page No.: 30 of 35


o Removed section 5.3.3.5.2.2 which pertained to DoD requirements for surrogate failures. Can be found in the DoD specific SOP.

o Updated surrogate section 5.3.5.2.1 to meet current LIMS. o Updated section 5.3.5.1.2 for new procedure.

• Revision 7.2, dated 01 March 2011

o Updated references to TALS.

Earlier revision histories have been archived and are available upon request.


Page No.: 31 of 35



Page No.: 32 of 35

Figure 1. Method Blank Evaluation



Page No.: 33 of 35

Figure 2. LCS Failure



Page No.: 34 of 35

Figure 3. Surrogate Failures



Page No.: 35 of 35

Figure 4. MS/MSD Failure


SCOPE OF ACCREDITATION TO ISO/IEC 17025:2005

TEST AMERICA DENVER 4955 Yarrow Street Arvada, CO 80002

Margaret S. Sleevi Phone: 303-736-0100 www.testamericainc.com

ENVIRONMENTAL

Valid To: October 31, 2017 Certificate Number: 2907.01

In recognition of the successful completion of the A2LA evaluation process, (including an assessment of the laboratory's compliance with ISO IEC 17025:2005, the 2009 TNI Environmental Testing Laboratory Standard, the requirements of the DoD Environmental Laboratory Accreditation Program (DoD ELAP) as detailed in version 5.0 of the DoD Quality Systems Manual for Environmental Laboratories), and for the test methods applicable to the Wyoming Storage Tank Remediation Laboratory Accreditation Program, accreditation is granted to this laboratory to perform recognized EPA methods using the following testing technologies and in the analyte categories identified below:

Testing Technologies

Atomic Absorption/ICP-AES Spectrometry, ICP/MS, Gas Chromatography, Gas Chromatography/Mass Spectrometry, Gravimetry, High Performance Liquid Chromatography, Ion Chromatography, Misc.- Electronic Probes (pH, O2), Oxygen Demand, Hazardous Waste Characteristics Tests, Spectrophotometry (Visible), Spectrophotometry (Automated),Titrimetry, Total Organic Carbon, Total Organic Halide

Parameter/Analvte Non-Potable Water Solid Hazardous Waste ("Water) Solid Hazardous Waste ("Solid)

MetalsAluminum EPA 6010B/6010C EPA 6010B/6010CAntimony EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020AArsenic EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020ABarium EPA 6010B/6010C/6020/6020A EPA 6010B/6010/6020/6020ABeryllium EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020ABoron EPA 6010B/6010C EPA 6010B/6010CCadmium EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020ACalcium EPA 6010B/6010C EPA 6010B/6010CChromium EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020ACobalt EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/ 6020/6020ACopper EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/ 6020/6020AIron EPA 6010B/6010C EPA 6010B/6010CLead EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/ 6020/6020A

^jthium EPA 6010B/6010C EPA 6010B/6010C^^gnesium EPA 6010B/6010C EPA 6010B/6010CManganese EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/ 6020/6020AMercury EPA 7470A EPA 7471 A/747 IB

(A2LA Cert. No. 2907.01) Revised 09/15/2016 ------ C. ^3—^ Page 1 of 12

5202 Presidents Court Suite 220 I Frederick, MD 21703-8398 I Phone: 301 644 3248 I Fax: 240 454 9449 I wwwA21_A.org

Parameter/Analvte Non-Potable Water Solid Hazardous Waste (Water) Solid Hazardous Waste (Solid)

Molybdenum EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/ 6020/6020AEckel EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020A

'otassium EPA 6010B/6010C EPA 6010B/6010CSelenium EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020ASilica EPA 6010B/6010C EPA 6010B/6010CSilicon EPA 6010B/6010C EPA 6010B/6010CSilver EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020ASodium EPA 6010B/6010C EPA 6010B/6010CStrontium EPA 6010B/6010C EPA 6010B/6010CThallium EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020ATin EPA 6010B/6010C EPA 6010B/6010CTitanium EPA 6010B/6010C EPA 6010B/6010CVanadium EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020AZinc EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020A

NutrientsNitrate (as N) By calculation EPA 9056/9056A/300.0

By calculation________EPA 9056/9056A By calculation

Nitrate-nitrite (as N) EPA 353.2 EPA 353.2/9056/ 9056A/300.0 EPA 9056/9056ANitrite (as N) SM 4500-N02 B SM 4500-N02 B

EPA 9056/9056A/300.0EPA 9056/9056A

Orthophosphate (as P) EPA 9056/9056A/300.0 EPA 9056/9056ATotal Phosphorus EPA 6010B/6010C EPA 6010B/6010C

mandsbtal Organic Carbon EPA 9060/9060A EPA 9060/9060A

Total Organic Halides EPA 9020B

Wet ChemistryAlkalinity(Total Bicarbonate, Carbonate, and Hydroxide Alkalinty)

SM 2320 B-1997 SM 2320 B SM 2320 B

Ammonia EPA 350.1 EPA 350.1Biological Oxygen Demand SM 5210B SM 5210BBromide EPA 9056/9056A/300.0 EPA 9056/9056AChloride EPA 9056/905 6A/3 00.0 EPA 9056/9056AChemical Oxygen Demand EPA 410.4 EPA 410.4Conductivity EPA 9050/9050A EPA 9050/9050ACyanide 9012A/9012B 9012A/9012BFerrous iron SM 3500 Fe B, D SM 3500 Fe B, DFluoride EPA 9056/9056A300.0 EPA 9056/9056AFlexavalent chromium EPA7196A2H EPA 9040B/9040C EPA 9045C/9045DOil and Grease (HEM and SGT-HEM)

EPA 1664A/1664B EPA907IB

Percent moisture ASTMD2216Perchlorate EPA 6860 EPA 6860

enols EPA 9066lids, total SM 2540 B SM 2540 B SM 2540 B

Solids, Total Suspended SM 2540 D SM 2540 D SM 2540 DSolids, Total Dissolved SM 2540 C SM 2540 C SM 2540 C

(A2LA Cert. No. 2907.01) Revised 09/15/2016 c. Jbb Page 2 of 12


Sulfatem

EPA 9056/905 6A/300.0 EPA 9056/9056Alfide, total EPA 9034 EPA 9034

ulfide EPA 9030B EPA 903 0BTotal Kjeldahl Nitrogen EPA 351.2

Purgeable Organics(volatiles-)Acetone EPA 8260B EPA 8260BAcetonitrile EPA 8260B EPA 8260BAcrolein EPA 8260B EPA 8260BAcrylonitrile EPA 8260B EPA 8260BAllyl Chloride EPA 8260B EPA 8260Btert-Amyl Methyl EtherBenzene EPA 8260B/8021B//8260B SIM

AK101/OK DEQ GRO________EPA 8260B/8021B/ AK101/OK DEQ GRO

Bromobenzene EPA 8260B EPA 8260BBromochloromethane EPA 8260B EPA 8260BBromodichloromethane EPA 8260B EPA 8260BBromoform EPA 8260B EPA 8260BBromomethane EPA 8260B EPA 8260B2-Butanone EPA 8260B EPA 8260Bn-Butyl alcohol EPA 8260B/8015B/8015C EPA 8260B/8015B/8015Ctert-Butyl alcohol (2-Methyl-2-propanol)

EPA 8260B/8260B SIM EPA 8260B

mutylbenzene EPA 8260B EPA 8260Bc-Butylbenzene EPA 8260B EPA 8260B

tert-Butylbenzene EPA 8260B EPA 8260BCarbon disulfide EPA 8260B EPA 8260BCarbon tetrachloride EPA 8260B EPA 8260BChlorobenzene EPA 8260B/8021B EPA 8260B/8021B2-Chloro-1,3 -butadiene EPA 8260B EPA 8260BChloroethane EPA 8260B EPA 8260B2-Chloroethyl vinyl ether EPA 8260B EPA 8260BChloroform EPA 8260B EPA 8260B1-Chlorohexane EPA 8260B EPA 8260BChloromethane EPA 8260B EPA 8260BChloroprene EPA 8260B EPA 8260B4-Chlorotoluene EPA 8260B EPA 8260B2-Chlorotoluene EPA 8260B EPA 8260BCyclohexane EPA 8260B EPA 8260BCyclohexanone EPA 8260B EPA 8260BDibromochloromethane EPA 8260B EPA 8260B1,2-Dibromo-3 -chloropropane (DBCP)__________________

EPA 8260B/8011 EPA 8260B/8011

Dibromochloromethane EPA 8260B EPA 8260BDichlorodifluoromethane EPA 8260B EPA 8260BDibromomethane EPA 8260B EPA 8260B

Dibromoethane (EDB) EPA 8260B/8011 EPA 8260B/8011

i-Dichlorobenzene EPA 8260B/8021B EPA 8260B/8021B1,3-Dichlorobenzene EPA 8260B/8021B EPA 8260B/8021B1,4-Dichlorobenzene EPA 8260B/8021B EPA 8260B/8021B

(A2LA Cert. No. 2907.01) Revised 09/15/2016 <=^f. C. Page 3 of 12


cis-1,4-Dichloro-2-butene EPA 8260B EPA 8260B^ns-1,4-Dichloro-2-butene EPA 8260B EPA 8260B

T, 1 -Dichloroethane EPA 8260B EPA 8260B1,2-Dichloroethane EPA 8260B EPA 8260B1,1 -Dichloroethene EPA 8260B EPA 8260B1,2-Dichloroethene EPA 8260B EPA 8260Bcis-1,2-Dichloroethene EPA 8260B EPA 8260Btrans-1,2-Dichloroethene EPA 8260B EPA 8260BDichlorofluoromethane EPA 8260B EPA 8260B1,2-Dichloropropane EPA 8260B EPA 8260B1,3-Dichloropropane EPA 8260B EPA 8260B2,2-Dichloropropane EPA 8260B EPA 8260B1,1 -Dichloropropene EPA 8260B EPA 8260B1,3 -Dichloropropene EPA 8260B EPA 8260Bcis-1,3 -Dichloropropene EPA 8260B EPA 8260Btrans-1,3-Dichloropropene EPA 8260B EPA 8260BDiethyl ether EPA 8260B EPA 8260BDi-isopropylether EPA 8260B EPA 8260B1,4-Dioxane EPA 8260B/8260B SIM EPA 8260B/8260B SIMEthanol EPA 8260B/8015B/8015C EPA 8260B/8015B/8015CEthyl acetate EPA 8260B EPA 8260BEthyl benzene EPA 8260B/8021B/

AK101/OK DEQ GROEPA 8260B/8021B/ AK101/OK DEQ GRO

Ethyl methacrylate EPA 8260B EPA 8260B|hyl tert-butyl ether

fthylene glycol EPA8015C EPA 8015CGas Range Organics (GRO)___________

EPA 8015B/8015C/8015D/ AK101/OK DEQ GRO

EPA 8015B/8015C/8015D/ AK101/OK DEQ GRO

Hexane EPA 8260B EPA 8260B2-Hexanone EPA 8260B EPA 8260BHexachlorobutadiene EPA 8260B EPA 8260BIsobutyl alcohol (2-Methyl-1 -propanol)

EPA 8260B/8015B/8015C EPA 8260B/8015B/8015C

Isopropyl alcohol EPA 8260B EPA 8260BI sopropy lbenzene EPA 8260B EPA 8260B1,4-Isopropyltoluene EPA 8260B EPA 8260BIodomethane EPA 8260B EPA 8260BMethacrylonitrile EPA 8260B EPA 8260BMethanol EPA 8015B/8015C EPA 8015B/8015CMethyl acetate EPA 8260B EPA 8260BMethyl cyclohexane EPA 8260B EPA 8260BMethylene chloride EPA 8260B EPA 8260BMethyl ethyl ketone (MEK) EPA 8260B EPA 8260BMethyl isobutyl ketone EPA 8260B EPA 8260BMethyl methacrylate EPA 8260B EPA 8260BMethyl tert-butyl ether (MtBE) EPA 8260B/8021B/

OK DEQ GROEPA 8260B/8021B/ OK DEQ GRO

|Methyl-2-pentanone EPA 8260B EPA 8260Baphthalene EPA 8260B/QK DEQ GRO EPA 8260B/QK DEQ GRO

2-Nitropropane EPA 8260B EPA 8260B2,2’ Oxybisethanol EPA 8015C EPA8015C

(A2LA Cert. No. 2907.01) Revised 09/15/2016 r. Page 4 of 12

Parameter/Analyte Non-Potable Water Solid Hazardous Waste (Water) Solid Hazardous Waste (Solid)

2-Pentanone EPA 8260B EPA 8260Bjpionitrile EPA 8260B EPA 8260B

^PPropylbenzene EPA 8260B EPA 8260BPropylene glycol EPA8015C EPA 8015CStyrene EPA 8260B EPA 8260B1,1,1,2-T etrachloroethane EPA 8260B EPA 8260B1,1,2,2-Tetrachloroethane EPA 8260B EPA 8260BT etrachloroethene EPA 8260B EPA 8260BTetrahydrofiiran EPA 8260B EPA 8260BToluene EPA 8260B/8021B/

AK101/OK DEQGROEPA 8260B/8021B/ AK101/OK DEQ GRO

Total Petroleum Elydrocarbons (TPH)____________________

EPA 1664A/1664B EPA 1664A/1664B

1,2,3-Trichlorobenzene EPA 8260B EPA 8260B1,1,1 -Trichloroethane EPA 8260B EPA 8260B1,1,2-Trichloroethane EPA 8260B EPA 8260BTrichloroethene EPA 8260B/8260B SIM EPA 8260BTrichlorofluoromethane EPA 8260B EPA 8260B1,2,3-Trichlorobenzene EPA 8260B EPA 8260B1,2,4-Trichlorobenzene EPA 8260B EPA 8260B1,2,3-Trichloropropane EPA 8260B/8011 EPA 8260B/80111,1,2-Trichloro-1,2,2- trifluoroethane

EPA 8260B EPA 8260B

Triethylene glycol EPA 8015C EPA 8015C,3-Trimethylbenzene EPA 8260B EPA 8260B

P,2,4-T rimethylbenzene EPA 8260B EPA 8260B1,3,5-Trimethylbenzene EPA 8260B EPA 8260BVinyl acetate EPA 8260B EPA 8260BVinyl chloride EPA 8260B/8260B SIM EPA 8260BXylenes, total EPA 8260B/8021B/

AK101/OK DEQ GROEPA 8260B/8021B/ AK101/OK DEQ GRO

1,2-Xylene EPA 8260B/8021B/ AK 101/OK DEQGRO

EPA 8260B/8021B/ AK101/OK DEQ GRO

M+P-Xylene EPA 8260B/8021B/ AK101/OK DEQ GRO

EPA 8260B/8021B/ AK101/KDEQ GRO

Methane RSK-175Ethane RSK-175Ethylene (Ethene) RSK-175Acetylene RSK-175Acetylene ethane RSK-175

Extractable Organics(semivolatiles)Acenaphthene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMAcenaphthylene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMAcetophenone EPA 8270C/8270D EPA 8270C/8270D2-Acetylaminofluorene EPA 8270C/8270D EPA 8270C/8270Ddachlor EPA 8270C/8270D EPA 8270C/8270DyAminobiphenyl EPA 8270C/8270D EPA 8270C/8270D

Aniline EPA 8270C/8270D EPA 8270C/8270DAnthracene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIM

(A2LA Cert. No. 2907.01) Revised 09/15/2016 r. Page 5 of 12

Parameter/Analvte Non-Potable Water Solid Hazardous Waste (Water) Solid Hazardous Waste ('Solid)

Aramite EPA 8270C/8270D EPA 8270C/8270Dirazine EPA 8270C/8270D EPA 8270C/8270D

izobenzene EPA 8270C/8270D EPA 8270C/8270DBenzaldehyde EPA 8270C 8270D EPA 8270C/8270DBenzidine EPA 8270C/8270D EPA 8270C/8270DBenzoic acid EPA 8270C/8270D EPA 8270C/8270DBenzo (a) anthracene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMBenzo (b) fluoranthene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMBenzo (k) fluoranthene EPA 82 70C/82 70D/8270D SIM EPA 8270C/8270D/8270D SIMBenzo (ghi) perylene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMBenzo (a) pyrene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMBenzyl alcohol EPA 8270C/8270D EPA 8270C/8270Dbis (2-Chloroethoxy) methane EPA 8270C/8270D EPA 8270C/8270Dbis (2-Chloroethyl) ether EPA 8270C/8270D EPA 8270C/8270Dbis (2-Chloroisopropyl) ether (2,2’Oxybis( 1 -chloropropane)

EPA 8270C/8270D EPA 8270C/8270D

bis (2-Ethylhexyl) phthalate EPA 8270C/8270D EPA 8270C/8270D4-Bromophenyl phenyl ether EPA 8270C/8270D EPA 8270C/8270Dbutyl Benzyl phthalate EPA 8270C/8270D EPA 8270C/8270D2-sec-butyl-4,6-Dinitrophenol EPA 8270C/8270D EPA 8270C/8270DCarbazole EPA 8270C/8270D EPA 8270C/8270D4-Chloroanilene EPA 8270C/8270D EPA 8270C/8270DChlorobenzilate EPA 8270C/8270D EPA 8270C/8270D4-ch loro-3 -Methy lphenol EPA 8270C/8270D EPA 8270C/8270D

kChloronaphthalene EPA 8270C/8270D EPA 8270C/8270D^Ch loronaphthalene EPA 8270C/8270D EPA 8270C/8270D2-Chlorophenol EPA 8270C/8270D EPA 8270C/8270D4-Chlorophenyl phenyl ether EPA 8270C/8270D EPA 8270C/8270DChrysene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMCresols EPA 8270C/8270D EPA 8270C/8270DDiallate EPA 8270C/8270D EPA 8270C/8270DDibenzo (a,h) anthracene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMDibenzofuran EPA 8270C/8270D EPA 8270C/8270D1,2-Dichlorobenzene EPA 8270C/8270D EPA 8270C/8270D1,3-Dichlorobenzene EPA 8270C/8270D EPA 8270C/8270D1,4-Dichlorobenzene EPA 8270C/8270D EPA 8270C/8270D3,3’-Dichlorobenzidine EPA 8270C/8270D EPA 8270C/8270D2,4-Dichlorophenol EPA 8270C/8270D EPA 8270C/8270D2,6-Dichlorophenol EPA 8270C/8270D EPA 8270C/8270DDiethyl phthalate EPA 8270C/8270D EPA 8270C/8270DDimethoate EPA 8270C/8270D EPA 8270C/8270D3,3-Dimethylbenzidine EPA 8270C/8270D EPA 8270C/8270Dp-Dimethylaminoazobenzene EPA 8270C/8270D EPA 8270C/8270D7,12-Dimethylbenz(a)anthracene

EPA 8270C/8270D EPA 8270C/8270D

alpha-,alpha- Dimethylphenethylamine

EPA 8270C/8270D EPA 8270C/8270D

k4-Dimethylphenol EPA 8270C/8270D EPA 8270C/8270D"methyl phthalate EPA 8270C/8270D EPA 8270C/8270D

di-n-butyl Phthalate EPA 8270C/8270D EPA 8270C/8270Ddi-n-octyl Phthalate EPA 8270C/8270D EPA 8270C/8270D

r. ^5-(A2LA Cert. No. 2907.01) Revised 09/15/2016 Page 6 of 12

Parameter/Analyte Non-Potable Water Solid Hazardous Waste (Water-) Solid Hazardous Waste (Solid)

1,3 -Dinitrobenzenem

EPA 8270C/8270D EPA 8270C/8270D-Dinitrobenzene EPA 8270C/8270D EPA 8270C/8270D

,4-Dinitrophenol EPA 8270C/8270D EPA 8270C/8270D2,4-Dinitrotoluene EPA 8270C/8270D EPA 8270C/8270D2,6-Dinitrotoluene EPA 8270C/8270D EPA 8270C/8270D1,4-Dioxane EPA 8270C/8270D EPA 8270C/8270DDiphenylamine EPA 8270C/8270D EPA 8270C/8270D1,2-Diphenylhydrazine EPA 8270C/8270D EPA 8270C/8270DDisulfoton EPA 8270C/8270D EPA 8270C/8270DDiesel Range Organics (DRO) EPA 8015B/8015C/

AK102/8015D/OK DEQ DROEPA 8015B/8015C/AK102/8015D/OK DEQ DRO

ethyl Methanesulfonate EPA 8270C/8270D EPA 8270C/8270DFamphur EPA 8270C/8270D EPA 8270C/8270DFluoroanthene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMFluorene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMHexachlorobenzene EPA 8270C/8270D EPA 8270C/8270DHexachlorobutadiene EPA 8270C/8270D EPA 8270C/8270DHexachlorocyclopentadiene EPA 8270C/8270D EPA 8270C/8270DHexachloroethane EPA 8270C/8270D EPA 8270C/8270DHexachloropropene EPA 8270C/8270D EPA 8270C/8270DIndeno (1,2,3-cd) pyrene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMIsodrin EPA 8270C/8270D EPA 8270C/8270DIsophorone EPA 8270C/8270D EPA 8270C/8270DIsosafrole EPA 8270C/8270D EPA 8270 C/8270D

fethapyrilene EPA 8270C/8270D EPA 8270C/8270D"Methylcholanthrene EPA 8270C/8270D EPA 8270C/8270D2-methyl-4,6-Dinitrophenol EPA 8270C/8270D EPA 8270C/8270Dmethyl Methane sulfonate EPA 8270C/8270D EPA 8270C/8270D1 -Methylnaphthalene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIM2-Methylnaphthalene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIM2-Methylphenol EPA 8270C/8270D EPA 8270C/8270D3 +4-Methy lphenol EPA 8270C/8270D EPA 8270C/8270DNaphthalene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIM1,4-Naphthoquinone EPA 8270C/8270D EPA 8270C/8270D1-Naphthylamine EPA 8270C/8270D EPA 8270C/8270D2-Naphthylamine EPA 8270C/8270D EPA 8270C/8270D2-Nitroaniline EPA 8270C/8270D EPA 8270C/8270D3-Nitroaniline EPA 8270C/8270D EPA 8270C/8270D4-Nitroaniline EPA 8270C/8270D EPA 8270C/8270DNitrobenzene EPA 8270C/8270D EPA 8270C/8270D2-Nitrophenol EPA 8270C/8270D EPA 8270C/8270D4-Nitrophenol EPA 8270C/8270D EPA 8270C/8270DNitroquinoline-1 -oxide EPA 8270C/8270D EPA 8270C/8270DN-Nitrosodiethylamine EPA 8270C/8270D EPA 8270C/8270DN-Nitrosodimethylamine EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMN-Nitrosodi-n-butylamine EPA 8270C/8270D EPA 8270C/8270DN-Nitrosodi-n-propylamine EPA 8270C/8270D EPA 8270C/8270D

rNitrosodiphenylamine EPA 8270C/8270D EPA 8270C/8270D*Nitrosomethylethylamine EPA 8270C/8270D EPA 8270C/8270D

N-Nitrosomorpholine EPA 8270C/8270D EPA 8270C/8270DN-Nitrosopiperidine EPA 8270C/8270D EPA 8270C/8270D

(A2LA Cert. No. 2907.01) Revised 09/15/2016 — r. ^3 Page 7 of 12


N-Nitrosopyrrolidine

Iitro-o-Toluidine2-oxybis( 1 -chloropropane)

Parathion, methylParathion, ethylPentachlorobenzenePentachloroethanePentachloronitobenzenePentachlorophenol

Phenacetin________________Phenanthrene______________Phenol___________________Phorate________________ _2-Picoline_________________Pronamide________________Pyrene ________________Pyridine__________________Safrole___________________Sulfotepp_________________1.2.4.5- Tetrachlorobenzene2.3.4.6- TetrachlorophenolThionazin_________________o-Toluidine_______________

I|2,4-Trichlorobenzene______,r4,5-Trichlorophenol

2,4,6-Trichlorophenol_______0,0,0-triethyl Phosphorothioate1,3,5-Trinitrobenzene_______Motor Oil (Residual Range Organics)_________________

EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D/ 8321 A/8321B____________________EPA 8270C/8270D__________EPA 8270C/8270D/8270D SIMEPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D/8270D SIMEPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D_______ __EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8015B/8015C/8015D/AK103/QK DEQRRO_______

EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D/ 8321 A/8321B____________________EPA 8270C/8270D__________EPA 8270C/8270D/8270D SIMEPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D/8270D SIMEPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D_________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8015B/ 8015C/8015D/ AK103/ OK DEQRRO

Pesticides/Herbicides/PCBsAldrin__________________Atrazine________________Azinophos ethyl__________Azinophos methyl_________alpha-BHC______________beta-BHC_______________delta-BHC_______________gamma-BHC_____________Bolstar_________________alpha-Chlordane__________gamma-Chlordane________Chlordane (technical)______Chloropyrifos______ _____Coumaphos______________

^4-DValapclapon

2,4-DB 4,4’-DDD

EPA 8081 A/808 IB EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8141 A/814IB EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8141A/8141B EPA 8141A/8141B EPA 8151A/8321A EPA 8151A/8321A EPA 8151A/8321A EPA 8081 A/808 IB

EPA 8081 A/808 IB EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8081A/8081B EPA 8081A/8081B EPA 8081A/8081B EPA 8081A/8081B EPA 8141A/8141B EPA 8081 A/808 IB EPA 8081A/8081B EPA 8081 A/808 IB EPA 8141A/8141B EPA 8141A/8141B EPA 8151A/8321A EPA 8151 A/8321 A EPA 8151A/8321A EPA 8081 A/808 IB

(A2LA Cert. No. 2907.01) Revised 09/15/2016 r. ^5 Page 8 of 12

Parameter/ Analvte Non-Potable Water Solid Hazardous Waste (Water) Solid Hazardous Waste (Solid)

4,4’-DDE1’-DDT

emeton-0Demeton-SDemeton, totalDiazinonDicambaDichlorovosDichloropropDieldrinDimethoateDinosebDisulfotonEndosulfan IEndosulfan IIEndonsulfan sulfateEndrinEndrin aldehydeEndrin ketoneEPNEthopropEthyl ParathionFamphurFensulfothion

Inthioneptachlor

Heptachlor epoxideHexachlorobenzeneMalathionMCPAMCPPMerphosMethoxychlorMethyl parathionMevinphosNaledPCB-1016 (Arochlor)PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260PCB-1262PCB-1268Total PCBsPhorate

aosmetropazine

RonnelSimazine

EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8141A/8141B EPA 8141 A/8141 B EPA 8141A/8141B EPA 8141 A/8141B EPA 8151A/8321A EPA 8141A/8141B EPA 8151 A/8321 A EPA 8081 A/808 IB EPA 8141 A/8141B EPA 8151 A/8321 A EPA 8141A/8141B EPA 8081A/8081B EPA 8081A/8081B EPA 8081 A/808 IB EPA 8081 A/808IB EPA 8081 A/808 IB EPA 8081A/8081B EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8081A/8081B EPA 8141A/8141B EPA 8151A/8321A EPA 8151A/8321A EPA 8141A/8141B EPA 8081 A/808 IB EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B

EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8141A/8141B EPA 814IA/8141B EPA 8141A/8141B EPA 8141 A/8141B EPA 8151 A/8321 A EPA 8141A/8141B EPA 8151A/8321A EPA 8081 A/808 IB EPA 8141 A/8141B EPA 8321A EPA 8141 A/8141B EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8081A/8081B EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8141 A/8141B EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8141 A/8141B EPA 8151 A/8321 A EPA 8151A/8321A EPA 8141 A/8141B EPA 8081A/8081B EPA 8141A/8141B EPA 8141A/8141B EPA 8141 A/8141B EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8141 A/8141B EPA 8141A/8141B

(A2LA Cert. No. 2907.01) Revised 09/15/2016r. ^5 Page 9 of 12


Stirophos ^lfotepp~

?T4;5-TThionazinTokuthion2,4,5-TP__________________Toxaphene________________Trichloronate______________o,o,o-triethylphos Phorothioate

Exylostt£&

1,3,5-Trinitrobenzene

1,3-Dinitrobenzene

2,4,6-Trinitrotoluene

3,5-Dinitroaniline2,4-Dinitrotoluene

2,6-Dinitroltoluene

2-amino-4,6-Dinitrotoluene

kNitrotoluene

3-Nitrotoluene

4-amino-2,6-Dinitrotoluene

4-Nitrotoluene

Nitrobenzene

Nitroglycerin

octahydro-1,3,5,7-tetrabitro- 1,3,5,7-Tetrazocine (HMX) Pentaerythritoltetranitrate(PETN)________ ,___________Picric acid______________ _RDX (hexahydro-l,3,5-trinitro-1,3,5-Triazine)_____________Tetryl (methyl 2,4,6- Trinitrophenylnitramine______

Perfluorinated Hydrocarbons

EPA 8141A/8141B EPA 8141A/8141B EPA 8151 A/8321A EPA 8141A/8141B EPA 8141A/8141B EPA 8151A/8321A EPA 8081A/8081B EPA 8141A/8141B EPA 8141A/8141B

EPA 8141A/8141B EPA 8141A/8141B EPA 8151A/8321A EPA 8141 A/8141B EPA 8141A/8141B EPA 8151A/8321A EPA8081 A/808IB EPA 8141A/8141B EPA 8141A/8141B

EPA 8330A/8330B/8321A/8321B________________ _EPA 833 0A/833OB/8321 A/8321B_________________EPA 833 0A/833OB/8321 A/832 IB_________________EPA 83 3 OB_____________EPA 8330A/8330B/8321A/8321B__________ .EPA 8330A/8330B/8321AJ

832 IB_________________EPA 8330A/8330B/8321A/832IB_________________EPA 8330A/8330B/8321A/8321B___________^

EPA 8330A/8330B/8321A/832IB_________________EPA 8330A/8330B/8321A/832 IB_____________ __EPA 8330A/8330B/8321A/832 IB_________________EPA 8330A/8330B/8321A/8321B_________________EPA 8330A/8330B/8321A/8321B_________________EPA 8330A/8330B/8321A/8321B_________________EPA 8330A/8330B/8321 A/832 IB_______ _______ __EPA 8330A/8330B______EPA 8330A/8330B/8321A/8321B_________________EPA 8330A/8330B/8321A/ 8321B

EPA 8330A/8330B/ 8321A/8321B_________________EPA 8330A/8330B/ 8321A/8321B_________________EPA 8330A/8330B/ 8321A/832 IB_________________EPA 83 3 OB_____________EPA 8330A/8330B/ 8321 A/8321B_________________EPA 8330A/8330B/ 8321A/8321B_________________EPA 8330A/8330B/ 8321A/8321B_________________EPA 8330A/8330B/ 8321A/8321B_________________EPA 8330A/8330B/ 8321 A/8321B_________________EPA 8330A/8330B/ 8321A/8321B_________________EPA 8330A/8330B/ 8321 A/832 IB_________________EPA 8330A/8330B/ 8321 A/8321B_________________EPA 8330A/8330B/ 8321 A/8321B_________________EPA 8330A/8330B/ 8321A/8321B_________________EPA 8330A/8330B/ 8321A/8321B_________________EPA 8330A/8330B_______EPA 8330A/8330B/ 8321A/8321B_________________EPA 8330A/8330B/ 8321 A/ 8321B

and Perfluorinated Sulfonates

Irfluorobutanoic aciderfluoropentanoic acid

Perfluorohexanoic acid

SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012



(A2LA Cert. No. 2907.01) Revised 09/15/2016 r. Jb> Page 10 of 12


Perfluoroheptanoic acidfcrfluorooctanoic acid_____rerfluorononanoic acid____Perfluorodecanoic acid____Perfluoroundecanoic acid Perfluorododecanoic acid Perfluorotridecanoic acid Perfluorotetradecanoic acid Perfluorobutane sulfonate Perfluorohexane sulfonate Perfluorooctane sulfonate Perfluorodecane sulfonate Perfluorooctane sulfonamide

SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012



Hazardous WasteCharacteristics_________Conductivity____________Corrosivity_____________Ignitibility______Paint filter liquids test Synthetic Precipitation Leaching Procedure (SPLP) Toxicity Characteristic

EPA 1010/1010 A

EPA 9050A EPA 9040B/9040C EPA 1010/1010A. EPA 9095A EPA1312

EPA1311

EPA 9050A EPA 9045C/9045D EPA 1010/1010 A EPA 9095A EPA 1312

EPA 1311Leaching Procedure

Organic Prep Methods Separatory funnel liquid-liquidextraction_________________Continuous liquid-liquid

EPA3510C

EPA 3520Cextraction___________Soxhlet extraction____Microwave extraction Ultrasonic extractionWaste dilution_______Solid phase extraction Volatiles purge and trap

EPA 3 5 80A EPA 3535A EPA 5 03 0B

EPA 3540CEPA 3546_______EPA 3550B/3550C EPA3580A

EPA 5030A/5035A/5035

Organic Cleanup ProceduresFlorisil cleanup_____________Florisil cleanup_____________Sulfur cleanup______________Sulfuric acid/Permanganate cleanup___________________

Metals DigestionAcid digestion total recoverable

EPA 3620B EPA 3620C EPA 3660A EPA 3 665A

EPA 3620B EPA 3620C EPA 3660A EPA 3665A

EPA 3005Aor dissolved metals

icid digestion for total metalsid digestion for total metals

cid digestion of sediments, sludges and soils

EPA3010A EPA 3020A

EPA 3050B

(A2LA Cert. No. 2907.01) Revised 09/15/2016 r. Jb Page 11 of 12

In recognition of the successful completion of the A2LA evaluation process, (including an assessment of the laboratory's compliance with ISO IEC 17025:2005, and for the test methods applicable to the Wyoming Storage Tank Remediation laboratory Accreditation Program), accreditation is granted to this laboratory to perform recognized EPA methods using the following testing technologies and in the analyte categories identified below:

Wyoming Storage Tank Program

Parameter/Analyte Method(s)

MetalsCadmium EPA6010CChromium EPA 6010CLead EPA 6010C

Wet ChemistryHexavalent chromium EPA 7196A

Pureable Organics (volatiles!tert-Amyl Methyl Ether EPA 8260BBenzene EPA8260B/ 02IBtert-Butyl alcohol EPA 8260B(2-Methyl-2-propanol)1,2-Dichloroethane EPA 8260BDi-isopropylether EPA 8260BEthyl benzene EPA 8260B/8021BEthyl tert-butyl ether EPA 8260BGas Range Organics (GRO) EPA8015CMethyl tert-butyl ether (MtBE) EPA 8260B/8021BNaphthalene EPA 8260B/8021BToluene EPA 8260B/8021BXylenes, total EPA 8260B/8021B1,2-Xylene EPA 8260B/8021BM+P-Xylene EPA 8260B/8021B

Extractable Organics (semivolatileslDiesel Range Organics (DRO) EPA 8015C (WY: C10-C32)

Organic PreD MethodsVolatiles purge and trap EPA 5030B (water) /5030A (solids)

(A2LA Cert. No. 2907.01) Revised 09/15/2016 ------c. Jb Page 12 of 12

Accredited LaboratoryA2LA has accredited

TESTAMERICA DENVERArvada, CO

/ for technical competence in the field of

Environmental Testing j

In recognition of the successful completion of the A2LA evaluation process that includes an assessment of the laboratory's compliance with ISO/IEC 17025:2005, the 2009 TNI Environmental Testing Laboratory Standard, and the requirements of the

Department of Defense Environmental Laboratory Accreditation Program (DoD ELAP) as detailed in version 5.0 of the DoD Quality System Manual for Environmental Laboratories (QSM), accreditation is granted to this laboratory to perform recognized EPA

methods as defined on the associated A2LA Environmental Scope of Accreditation. This accreditation demonstrates technical competence for this defined scope and the operation of a laboratory quality management system

(refer to joint ISO-ILAC-IAF Communique dated 8 January 2009).

v

For the tests to which this accreditation applies, please refer to the laboratory's Environmental Scope of Accreditation.

EXHIBIT B.3

Canon City Milling Facility/Lincoln ParkSuperfund SiteJuly 2017

Cotter Corporation (N.S.L.)QAPP Version 1.0

NEW YORKSTATE OF OPPORTUNITY.

.-.ANDREW M. CUOMO ’ # Governor

HOWARD A. ZUCKER, M.D., J.D.Commissioner# _ m

SALLY ORESLiN, M.S., R.N.Executive Deputy Commissioner

‘

:12042 April 01, =f f== -=

JYifCTRYGGVE RONNQVIST LANDAUER NORDIC AB PO BOX 6522 SE-751 38 M UPPSALA, SWEDEN Certificate Expiration Date:

April

Dear Mr. Ronnqvlst,

Enclosed are certificate(s) of approval issued to your environmental laboratory for the current permit year. The certificate(s) supersede(s) any previously issued one(s) and is{are) in effect through the expiration date listed. Please carefully examine the certificate(s) to insure that the categories, subcategories, analytes, and methods for which your laboratory is approved are correct. In addition, verify that your laboratory’s name, address, lead technical director, and identification number are accurate. pH wp|

Pursuant to NYCRR Subpart 55-2.2, original certificates must be posted conspicuously intheleboratory and copies shall be made availablejaany client of the laboratory upon request.

Pursuant to NYCRR Subpart 55-2.6, any misrepresentation of the fields of accreditation (category - method - analyte) for which your laboratory is approved may result in denial, suspension, or revocation of your i certification. Anyuseqhthe Environmental Laboratory Approval Program (ELAP) or National Environmental Laboratory Accreditation Program (NELAP) name, reference to the laboratory's approval status, and/or using the NELAP Ipgp fo any catalogs, advertising, business solicitations, proposals, quotations, laboratory analytical reports, or other materials must Include the laboratory's ELAP identification number and distinguish between testing for which the laboratory is approved and testing for which the laboratory is not approved.

If you have any questions, please contact ELAP at the New York State Department of Health (NYS.DOH), Wadsworth Center, PO Box 509, Albany NY, 12201-0509; by phone at (518) 485-5570; by facsimile at (518) 485-5568; and by email at [email protected], • § •

Victoria Pretti Director -iEnvironmental Laboratory Approval Program

|t fi H'-V

, Atwny. NY 12237 |h«ft)uiy.g(W

NEW YORK STATE DEPARTMENT OF HEALTH • WADSWORTH CENTER

Expires 12:01 AM April 01,2018 Issued April 01,2017

CERTIFICATE <

Issued In accordance with and pursuant to section 502 Public Health Law of New York State

MR. TRYGGVE RONNQVIST LANDAUER NORDIC AB RAPSGATAN 25, SE-754 50 UPPSALA, SWEDEN % 1

NY Lab Id No: 12042

Miscellaneous

Radon 1

is hereby APPROVED as an Environmental Laboratory in conformance with theStandards (2003) for the category

ENVIRONMENTAL ANALYSES AIR AND EMISSIONS 4All approved analytes are listed below:

Alpha Track

=r~ -J. ~ '• 3=s ■ LsssiiiHF

1

t iL

SeriHl^.L46372

Property of the New York Slate Department of Health. Certificates are valid only at the address shown, must be conspicuously posted, and are printed on secure paper. Continued accreditation depends on successful ongoing participation In the Program. Consumers are urged to call (618) 485-5570 to Yerify the laboratory's accreditation status, 4 * *= 4 m mVL E

1

sWw-

SWEDACStyrcKcn Rirm.lmxlin-rins cH'Ivtckmik kcmirnll

SwwiMi Ikwrd lor Aunxlilntinn umi Conformity AsscssnuMil

MV/ fio.o DAC"

Scope of accreditationLa ndauer Nordic AB Uppsala

CORRECTION

Scope corrected on parameter "Radon Canada"/2017-01-23 Maria Wallin

Measuring activityTechnical area Parameter |jMethod

1\\

Radon SS-ISO 11665-4:2012

Radon, worksites SSMMethod description - Radon worksites in 2004:01

Radon, Ireland SS-ISO 11665-4:2012/RPII, Protocol for measurement of radon in homes, October 2010

Radon, Canada EPA, Protocols for Radon Measurement in Homes, 1993

Measuring principle

, Trace film measuring, 'image analysis

■ Trace film measuring, !jimage analysis

Trace film measuring, image analysis

Trace film measuring,

'Trace film measuring,

f image analysis

Trace film measuring,

j___

Pa gel (3)

22/12/201 2016/1841

Accreditation Number 1489

A003783-001

Appendix 2Date Name

Measuring range

; 10-25000 Bq/m3 ;(3 month exp).

10-30000 kBq/m3 ’I (80-250000 Bq/m3

:120 month exp.)if

] 50-150000 Bq/m3 i (7 days exp.).1

j 20-25000 Bq/m3 ■j(3 month exp.]

if

; 10-25000 Bq/m3 ,(3month exp.)

‘ 50-150000 Bq/m3 i (7 days exp.)

15-25000 Bq/m3 (3 month exp.),

;37-100000 Bq/m3 (10 days exp.)

Test type;j

Hex Reid ....... . 1Note

i Air■I■f

No No

j Air'ii

i!

;IAiri * ‘

No

No

No

_No

Two position detectors- Duotrak(not USA/Canada)

Air No No |

i Air No No

Air

Air

pr,r pA/iSWEDACStyrclven Rfrackri-tliatring orh Utkmtk ktmtrnll

Swedish Board tor Autreilitalion and Confurmity Assessment

Technical area \ Parameterl!

I Radon, long-term

measurement,(housing.

Method

SSMmethod description - Radon in housing, 2013

Measuring principle

Trace film measuring, ; image analysis

Radon, Norway j! SS-ISO 11665-4:2012/ Measuring Trace film measuring,procedure for radon in housing, image analysis2013 .Trace film measuring,

image analysis

SS-ISO 11665-4:2012/ Measuring Trace film measuring, procedure for radon in schools image analysis and daycare facilities, 2015

;; Radon, (personal

" Radon, current, j! short-term

'(measuring, (housing

i.I!

( Internal method: Manual ( measuring of radio in indoor jjair with trace film, SFMANM

iiSSM

method description - Radon in '(housing, 2013

| Radon, Great | SS-ISO 11665- 4:2012/HPA-

i BritainiI;

RPD047

Radon, USA1.

jlEPA, Protocols for Radon Measurement in Homes, 1993




Trace film measuring, ,image analysis



Page2 (3)

Appendix 2Date Name

22/12/201 2016/1841

Measuring range Test type jjflex Field :Note

ii !|

20-25000 Bq/m3 (3 month exp).

Air No1;Ii

|Sno

:■ i'

10-20000 Bq/m3

(3 month exp).Air (No

(iN° ii

50-150000 Bq/m3 (7 days exp.)

(Air ! No1

n- i

i‘

10-20000 Bq/m3 (3 month exp). 50-150000 Bq/m3 (7 days exp.)

Air Nor[

No t,ii !,!: !'! 1

40-50000 kBqh/m3 Air No rNo !

i [

50-150000 Bq/m3 (7 days exp.)

Air No

|

No \

f j

i

10-25000 Bq/m3 (3 month exp).

(Air '! Noji

!

! i

i ;■t

_.. .1

o

:

50-150000 Bq/m3

(7 days exp.)Air No

;l

No |(i jii! j;

0.4-650 pCi/l (3 month exp).

(Air Noii

No :!t (

f

1-2500 pCi/l (10 days exp.)

Air rNo 'No I1

SWEDACStyroKcn fit rnckivdiur ring ot:h tokuUk knntroll

Swedish Hoard for Aicmlilntion and Omfcrmitv Asscssmcnl

Appendix 2

Date Name

22/12/201 2016/1841

Technical area Parameter Method iMeasuring .Measuring rangeprinciple ;j

Test type Flex Field Note

iFood analysis Cesium, Cs-137 ■Gamma spectrometry a >0.4Bq (1 h meal)

:i (2 Bq/kg for 200 g sample)

r

:Ashes

i

No No .

Gamma spectrometry " >0.4Bq (1 h meal)•1 " (2 Bq/kg for 200g sample)

■ Biological Nomaterial/biota ;i

J. . J JNo

Gamma spectrometry >3 Bq (1 min measure time)■ j(15 Bq/kg for 200 g sample)

Ashes■-

No No 1jl

iGamma spectrometry ! > 3 Bq (1 min measure time)

■; (15 Bq/kg for 200 g sample)Biologicalmaterial/biota

No No

Water analysis Radon Analy si s of radon i n wate r - method description, Swedish Radiation Safety Authority 2013

jlGamma spectrometry !! > 4 Bq (15 min measure time)* i;(20 Bq/kg for 200 ml sample)i! i!p ^

5 1

!j Drinking water

1

No No

Testing Is not covered by the accreditation. If the laboratory still performs the testing, the testing is not covered by the accreditation.

Modified scope is marked in bold.

Page3 (3)

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