NOORUL ISLAM UNIVERSITY DEPARTMENT OF CHEMISTRY · PDF fileantacids, inorganic drugs in dental...

NOORUL ISLAM CENTRE FOR HIGHER EDUCATION

M.PHIL. CHEMISTRY


NOORUL ISLAM UNIVERSITY

DEPARTMENT OF CHEMISTRY

M.PHIL. CHEMISTRY

CURRICULUM & SYLLABUS

SEMESTER - I

SL.No.

SUBJECTCODE SUBJECT L T P C

THEORY

1. GE401 Teaching Methodology 4 1 0 5

2. CH401 Research Methodology in Chemistry 4 1 0 5

3. CH402 Biomaterials and its Characterization 4 1 0 5

TOTAL 12 3 0 15


M.PHIL. CHEMISTRY

GE401 TEACHING METHODOLOGY 4 1 0 5

OBJECTIVES1. To understand the concepts and Practices of Teaching Methodology in Higher Education2. To understand the Concept and Practices of Educational Psychology3. To develop the awareness in modern teaching practices and evaluation4. To provide systematic knowledge about motivation and emotion

UNIT - I 15Higher Education - Teaching Technology: Objectives and Role of Higher Education-Learningand Learning Hierarchy - Information Processing – Learning Events and Outcomes. TeachingTechnology - Meaning, concept and scope – Instructional Designs: Objectives based, Skillbased, Competency based, Learning style based and Model based Large Group Techniques:Lecture, Modified Lecture, Panel Discussion, Team Teaching, Project Approach and Workshop– Simulation, Role Playing, Brain Storming, Case formulation, analysis and Discussion.Concept of Micro – teaching - Steps - Micro-teaching Cycle - Rationale of Micro-teachingProcedure - Phase of Micro-teaching.

UNIT – II 10Educational Evaluation: Methods of Evaluation -Self Evaluation – Analysis of Teaching-Identification of Teaching Skills - Core Teaching Skills-Teaching Skills and their Specification-Teacher Evaluation- Methods. The measurement and evaluation process - concept - scope andneed - Basics - characteristics of good measuring instruments - validity - Objectivity - reliabilityusability and norms. Models in educational evaluation - 3d model - total reflection model andindividual judgment model. - scores and methods of feed back to students - new trends inevaluation.

UNIT –III 10Educational Psychology : Meaning and Definition - modern psychology - Study of psychology:Structuralism, Functionalism, and Behaviorism. - Branches of Psychology - EducationalPsychology -Concepts, Nature and Scope - Importance of Educational Psychology for theTeacher. Key perspectives in psychology: The facets of behavior - New trends in psychology -Research methods in psychology: Observation, Correlation and the Experimental method -Ethical issues in psychological research. Group Dynamics- Competition and Co-operation –Group Behaviour- Leadership Traits – Classroom Climate.

UNIT – IV 15Motivation and Emotion : Motivation and Learning - Functions of Motives - Kinds of Motives -Theories of Motivation - Hull's Drive education, Maslow's Hierarchy of Needs, Achievement -Motivation - Carl Rogers: self theory – McClelland: Achievement Motivation - Components -Fear of Failure and Hope of Success - Motivation in the classroom context - Praise and Blame,Rewards and Punishments - Feedback / Knowledge of Results - Level of Aspiration -


M.PHIL. CHEMISTRY

Achievement Motivation - Emotions, Expression and Impact - Relationship between emotionand cognition. - Levels of aspiration and its psychological implications.

UNIT – V 10ICT Enabled Teaching – Meaning and Scope. Electronic Media in Education: Concept,Selection, Use and Variety-e-Learning Resources: e-Learning, e-books, e-journals etc-Web-based Learning: Access and Teaching Issues. Conducting lessons using interactive whiteboards /Electronic Board – conducting an online class / online discussion - virtual Classroom – Videoconferencing – Building Animation Tools

TOTAL HOURS: 60REFERENCE BOOKS:1. Aggarwal.J.C. (2008) Essentials of Educational Psychology (2nd Edition) Vikas Publishing

House Pvt. Ltd., New Delhi.2. Baron A. Robert (2000) Psychology. Prentice-Hall of India, New Delhi.3. Chauhan. S. S. (2007) Advanced Educational Psychology (7th Edition), Vikas Publishing

House Pvt. Ltd. New Delhi.4. Dennis Child (1973) Psychology and the Teacher. Holt Rinehart and Winston, New York.5. Hurlock B. Elizabeth (1980) Adolescent Development. Tata McGraw Hill, New Delhi.6. Hurlock B.Elizabeth (1980) Developmental Psychology. Tata McGraw Hill, New Delhi.7. John.W.Santrock (2006) Educational Psychology, Mc graw-hill Higher Education,

New Delhi.8. Mangal. S. K (2007) Advanced Educational Psychology (2nd Edition), Prentice-Hall of

India Pvt. Ltd., New Delhi9. Vedanayagam, E.G. (1989) Teaching Technology for College Teachers. New Delhi: Sterling

Publishers (p) Ltd.10. Rajasekar, S. (2005) Computer Education and Educational Computing, Hyderabad:

Neelkamal Publications.11. Kumar, K. L. (1997) Educational Technology, New Delhi: New Age International (p) Ltd.12 SampathKumar, K. Paneerselvam, A and Santhanam, S. (1990) Introduction to Educational

Technology, New Delhi: Sterling Publishers (Pvt) Ltd.13. Tony Bates, A.W. (2005) Technology, e-Learning and Distance Education, New York:

Routlede.

CH401 RESEARCH METHODOLOGY IN CHEMISTRY 4 1 0 5

UNIT -I LITERATURE SURVEYSurvey of literature including patents – primary sources – secondary sources including reviews,treatise and monographs – Literature survey– possible ways of getting oneself familiar withcurrent literature – abstraction of research papers.Computer basic literature search – chemical data bases-protein data bank – patent searchWeb sources – E-journals - citation index – impact factor – H index – science direct – Scopus –scirus


M.PHIL. CHEMISTRY

UNIT -II CHOICE OF A RESEARCH PROBLEMIdentification of research problem – assessing the status of the problem – guidance from thesupervisor – actual investigation analysis of experimental results, conclusion, presentingscientific seminar – publication of scientific work - reporting the results in the form ofcommunication, paper – email operation and online submission of manuscripts for publication -writing a thesis - preparing research proposals for grants.

UNIT -III C PROGRAMMINGData types – Variables and Scope – operators – program selection: if – else, logical operators,ternary operator switch statement – repetition: While, do-while and for loops- Function, Arrays.Applications in chemistry- computation of vander Waals equation, pH titration, kinetics,radioactive decay- Evaluation of lattice energy and ionic radii from experimental data , Linearregression, Rate constant computations.

UNIT- IV CHEMICAL SAFETY AND SEPARATION TECHNIQUESSafe working procedure and protective environment, protective apparel, emergency procedureand first aid, laboratory ventilation, Safe storage and use of hazardous chemicals, procedure forlaboratory disposal of explosives, disposal of chemicals in the sanitary sewer system.Techniques: TLC, PC, Column , GLC, HPLC, DCCC – gel electrophoresis – GC – MS, LC-MS

UNIT - V ANALYTICAL TECHNIQUESPrinciple and Instrumentation: TEM, SEM, AFM (for characterization of solid samples - Thinfilms and nano materials).Multinuclear - 1H, 13C, 19F, 31P NMR- INDOR, DEPT, INEPT and 2D-COSY, NOESY, NMRfor structural determination.

REFERENCES:1. P. Rajammal, Devadas, A Hand book of Methodology of Research, S.R.K. Vidyalaya,

Chennai, 1976.2. J. Anderson, B.H. Durstan and M. Poole, Thesis and assignment writing, Wiley Eastern,

New Delhi, 1977.3. R.O. Butlet, Preparing thesis and other manuscript.4. Balagrusamy, Programming in C.5. K.V. Raman, Computers in Chemistry, Tata McGraw Hill, New Delhi, 1993.6. J. Banett, J.Mendham and R.C. Denney, Vogel’s Textbook of Quantitative Chemical

Analysis, ELBS, 5th Edition, Reprint 1991.7. D.C. Harris, W.H. Freeman , Quantitative Chemical Analysis.8. R.T. Bottle , The use of chemical literature.9. Chemical safety matters – IUPAC –IPCS- Cambridge Univ. Press.10. Spectroscopy methods in organic chemistry, William D.H. Flamming McGraw Hill.11. Hand book of Instyrumental Techniques for Analytical Chemistry – Frenk Settle.


M.PHIL. CHEMISTRY

12. H.H. Willard, L.L. Merrit, J.A. Dean and F.A. Settle, Instrumental Methods of Analysis,6th Edn., CBS publishers, 1986.

13. W. Kemp, Organic Spectroscopy, Macmillan Press Ltd, 1996.14. Harald Gunther, NMR spectroscopy, 2nd Edn., Basic principles, concepts, application in

Chemistry, John Willey & Sons Publishing (1984).

CH402 BIOMATERIALS AND ITS CHARACTERIZATION 4 1 0 5

UNIT I SYNTHESIS AND STRUCTURAL ELUCIDATION:a) Synthesis: Retrosynthetic analysis – synthon and disconnection approach-

chemoselectivity, regioselectivity and stereoselectivity in organic synthesis – solid phasepeptide synthesis- micro wave mediated organic synthesis – green solvent reactions –solvent free reactions

b) Structural elucidation of organic molecules by a combined use of Mass, UV-Vis., IR, 1HNMR, 13C-NMR, ORD and CD.

UNIT II NANO PARTICLES AND STRUCTURAL MATERIALSSynthesis, characterization and physical properties-optical and electronic properties-nanoclusters-nano devices-applications: water purification, Catalysis, solar cells, information storage,nano medicine.

UNIT III BIOINORGANIC CHEMISTRYMetalloproteins and enzymes - blue copper proteins – non-heme iron proteins-role ofmanganese in photo system – role of molybdenum in nitrogenase in the fixation of atmosphericnitrogen – (Na+-K+) Ion pump, ATPase – structure of DNA and DNA targeted drugs – metal ioninduced toxicity and detoxification by chelation therapy – Metallotherapy – ligand therapy –Applications of inorganic chemistry in different medical fields such as inorganic compounds asantacids, inorganic drugs in dental care, clinical disorders with alkali and alkaline earth metalsand their remedies and lithium therapy in psychiatric practice.

UNIT IV POLYMERS AND BIO-PHYSICAL CHEMISTRYPolymer structure, physical property relationship and polymer utilization- Characterization ofpolymers. Conducting Polymers: synthesis, properties, types and applications of conductingpolymer.Optical emission ,spectral methods for protein conformation, protein substrate interaction byFRET, ESR spin-labelling and spin-trapping techniques – principle and applications of MRI

UNIT V GROUP THEORYGroup theory and spectroscopy – defining properties of groups – symmetry elements andoperations – products of symmetry operation – symmetry point groups – classification ofmolecules into point groups – character table – orthogonility theorem – direct product.


M.PHIL. CHEMISTRY

Application of group theory to IR and Raman spectroscopy- symmetry of normal vibrations –selection rules for fundamental vibrations- splitting levels and term in a chemical environment.

REFERENCES

1. S. Warren, Designing Organic Synthesis- A programmed Introduction to the SynthesisApproach, John Wiley & Sons, 1978.

2. Chromatographic Methods, Stock and Rice.3. W. Kemp, Organic Spectroscopy, Macmillan Press Ltd, 1996.4. R.M. Silverstein, G.C. Bassler and T.C. Morrill, Spectrometric Identification of Organic

compounds, John Wiley & Sons, Inc., New York, 1991.5. C.N.R. Rao, Nano Chemistry, Wiley-Interscience, New York.6. G. Ozin, A. Arscnault, Nano Chemistry: A Chemical approach to nanomaterials,

Elsevier, Amsterdam, 2005.7. J.E. Huheey , E.A. Keiter and R.L. Keiter, Inorganic Chemistry, Harper and Row, 4th

Edn., 1993.8. S.J. Lippard and J.M. Berg, Basic concept of Bioinorganic Chemistry, University Science

Books, California.9. A.K. Das, A Text book on Medicinal aspects of Bio-Inorganic Chemistry, CBS

publishers, 1st Edn., 1990.10. Polymer Chemistry, Billmeger, et al.11. Introductory polymer chemistry, G.S. Mistra, , et al12. R.S. Dargo, Physical Methods in Chemistry, W.B. Saunders, 1977.13. Alan Cooper, Biophysical Chemistry, Royal Society of Chemistry Publication, 2004.14. Application of Group theory, Battacharya.15. Chemical application of Group theory, F.A. Cotton.16. Group theory, Bishop.17. Ligand Fields, Figgis, et al.


M.PHIL. CHEMISTRY




M.PHIL. CHEMISTRY

CURRICULUM & SYLLABUS

SEMESTER - II

SL.No.

SUBJECTCODE

SUBJECT L T P C

THEORY

1. XxEx1ELECTIVE – 1(In depth study of published literaturein Chemistry)

4 1 0 5

PROJECT

2. CH4P1 Dissertation 0 0 30 15

TOTAL 4 1 30 20


M.PHIL. CHEMISTRY




M.PHIL. CHEMISTRY

LIST OF ELECTIVES

SL.No.

SUBJECTCODE SUBJECT L T P C

THEORY

1. CH4A1Indepth Study of Published Literaturein Medicinal Plants

4 1 0 5

2. CH4A2Indepth Study of Published Literaturein Phytoconstituents

4 1 0 5

3. CH4A3Indepth Study of Published Literaturein Metal Complex

4 1 0 5

4. CH4A4Indepth Studies on ConductingPolyaniline Composites

4 1 0 5

5. CH4A5Indepth Study of Published Literatureon Metal Complexes with Drugs

4 1 0 5


M.PHIL. CHEMISTRY

CH4A1 INDEPTH STUDY OF PUBLISHED LITERATURE IN MEDICINAL PLANTS

UNIT 1Antimicrobial activity and phytochemical analysis of selected Indian folk medicinal plants.Evaluation of antimicrobial activity and phytochemical analysis of Citrus limon.

UNIT IIPhytochemical screening of eight traditionally used Ethnomedicinal plants from akola district(ms) india. Cultural and biochemical characteristics Of acinetobacter spp. Strains isolated Fromhospital units.

UNIT IIIPhytochemical and antimicrobial evaluations of Some medicinal plants of nepal. Antibacterial,antifungal and phytochemical analysis of selected medicinal Plants.

UNIT IVComparative analysis of antioxidant activity and phytochemical screening of some indianmedicinal plants. Screening of Crude Phytochemicals and Antimicrobial Activities of SelectedMedicinbal Plants of Peshawar Region Khyber Pakhtoon Khawa Pakistan.

UNIT VPhytochemical and antimicrobial studies on vernonia blumeoides hook. Fil. (asteraceae) ethanolextract. Gas Chromatography-Mass Spectrometry Analysis and Phytochemical Screening ofMethanolic Fruit Extract of Momordica charantia.

REFERENCES

1. Mohamed Sham Shihabudeen et. al. / International Journal of Pharma Sciences andResearch (IJPSR). Vol.1(10), 2010, 430-434.

2. Amit Pandey et al., Journal of pharmaceutical and biomedical sciences, 2011, 13 (17)3. Dipak koche et al., International Journal of Pharma and Bio Sciences. Vol.1/Issue-4/Oct-

Dec.2010.4. Sofia et al., The journal of preventive medicine. 2004; 12 (3-4): 35-42.

5. Himal Paudel Chhetri et al., Kathmandu university journal of science, engineering andtechnology. Vol. I, no. V, september 2008, pp 49-54.

6. Lali Growther et al., J. Nat. Prod. Plant Resour., 2012, 2 (6):644-6487. Kumar et al. Int J Pharm Pharm Sci, Vol 4, Issue 3, 291-2958. Farhat Ali Khan et al., Middle-East Journal of Scientific Research 9 (2): 200-208, 2011.9. Ibrahim et al., Nig. Journ. Pharm. Sci., March, 2011 Vol. 10 No.1, P. 50– 56.10. Singh et al., J Rec Adv Agri 2012, 1(4): 122-127.


M.PHIL. CHEMISTRY

CH4A2 INDEPTH STUDY OF PUBLISHED LITERATURE IN PHYTOCONSTITUENTS

UNIT IPhytochemical analysis and in vitro antibacterial activity of root peel extract of Raphanus

sativus L. var niger. Phytochemical, antioxidant and antibacterial activities of medicinal plantsused in Northern Thailand as postpartum herbal bath recipes by the Mien (Yao) community.

UNIT IIPhytochemical investigations and antibacterial activity of some medicinal plants againstpathogenic bacteria. Antimicrobial activity and phytochemical analysis of Sanseiveriaroxburghiana leaf.

UNIT IIIAntimicrobial activity and Phytochemical analysis of Andrographis alata Nees fromSouthern India. Preliminary Phytochemical screening of seeds of Pseoralea corylifolia

UNIT IVPhytochemical Screening of Some Pakistanian Medicinal Plants. Analysis of the PhytochemicalContent and Anti-microbial Activity of Plectranthus glandulosis Whole Plant.

UNIT VPhytochemical screening and TLC profiling of plant extracts of Cyathea gigantea (Wall. Ex.Hook.) Haltt. and Cyathea brunoniana. Wall. ex. Hook. (Cl. & Bak). Analysis of phytochemicalcomponents and anti-microbial activity of the toxic plant -Thevetia Peruviana.

REFERENCE

1. Safia Janjua et al., Advancement in Medicinal Plant Research. Vol. 1(1), pp. 1-7, January2013.

2. Kannika Panyaphu et al., Phytopharmacology 2012, 2(1) 92-105.3. Jayalakshmi et al., Journal of Applied Pharmaceutical Science 01 (05); 2011: 124-128.4. Jeeva et al., Asian Journal of Plant Science and Research, 2012, 2 (1):41-44.5. Chinnappan Alagesaboopathi. International Journal of PharmTech Research, Vol.3,

No.3,pp 1322-1328,6. Mohammed Rafiq Khan et al IRJP 2013, 4 (1).7. Iqbal et al., Middle-East Journal of Scientific Research 8 (3): 575-578, 2011.8. Egwaikhide et al., Middle-East Journal of Scientific Research 2 (3-4): 135-138, 2007.9. Das Talukdar et al., Assam University Journal of Science & Technology :Biological and

Environmental Sciences. Vol. 5 Number I.70-74, 2010.10. Mathuravalli et al., Indian J. Innovations Dev., Vol. 1, No. 2 (Feb 2012).


M.PHIL. CHEMISTRY

CH4A3 INDEPTH STUDY OF PUBLISHED LITERATURE IN METAL COMPLEX

UNIT 1

1. Synthesis, characterization and biological studies of schiff bases metal complexes Co(II),Zn(II), Ni(II), and Mn(II) derived from amoxicillin trihydrate with various aldehydes.

2. Synthesis, characterization and anti microbial activity of various schiff bases complexesof Zn(II) and Cu(II) ions

UNIT II1. Synthesis and characterization of Cu(II) complexes derived from acyl pyrazolone and 2-

amino phenol2. Synthesis, characterization, X-Ray and Thermal studies of some Schiff Base Metal

Complexes

UNIT III1. Synthesis, structural characterization and antimicrobial activities of some transition metal

complexes containing 2- acetonaphthone2. Cobalt(II) and Zinc(II) compounds with unsaturated ligands derived from 2-

aminobenzothiazole

UNIT IV1. Synthesis structural characterization & antibacterial studies of some biosensitive mixed

ligand copper(II) complexes2. Synthesis and physicochemical characterization of some schiff base complexes of

chromium(III)

UNIT V1. 1H NMR, IR and Uv/Vis spectroscopic studies of some schiff bases derived from 2-

aminobenzothiazole and 2-amino-3-hydroxypyridine2. Synthesis of pharmaceutically important 1,3,4-thiadiazole and imidazolinone derivatives

as antimicrobials

REFERENCES

1. Sunil joshi/international journal of pharma and bio sciences/vol 2/issue1/jan-march 20112. Venkatesh p /asian journal of pharmaceutical & health sciences/vol1/issue1/ jan- march

20113. N. P. Moorjani, k . M. Vyas and r. N. Jadeja/ prajñā - journal of pure and applied

sciences, vol. 18: 68 - 72 (2010)4. A.p. mishra and neha sharma/ j. Ind. Council chem./ vol. 26, no. 2, 2009, pp. 125-129


M.PHIL. CHEMISTRY

5. A.p. mishra and d.k. mishra, international journal of pharma and bio sciences//vol2/issue3/ july- sept 2011

6. Fabiola te´llez, angelina flores-parra, nora´h barba-behrens, rosalinda contreras,polyhedron 23 (2004) 2481–2489

7. N. Raman, indian journal of chemistry, vol 46a/oct 2007/pp. 1611-16148. R.k. dubey, indian journal of chemistry, vol 47a/aug 2008/pp. 1208-12129. Raafat m. Issa, abdalla m. Khedr and helen rizk, journal of the chinese chemical society,

2008, 55, 875-88410. Mohd amir, arun kumar,isrsr ali & s a khan/ indian journal of chemistry, vol 48b/sept

2009/pp. 1288-1293

CH4A4 Indepth studies on conducting polyaniline composites

Unit I

Polymers- introduction to conducting polymers- Synthesis, characterization andapplications of the conducting polymer: Polyaniline- Studies on electrical property ofpolyaniline.

Unit II

Polyaniline clay composites- their improved structure property relations compared topristine polyaniline- structure and characterization of phyllosilicates with specialemphasis to laponite clay.

Unit III

Self assembly approach for the synthesis of electromagnetic functionalized Fe3O4/polyaniline nanocomposites and photocatalytic polyaniline/ laponite/ titanate composites.Effect of dopant on the properties.

Unit IV

Visible light induced photocatalytic degradation of methylene blue with polyaniline-sensitized TiO2 composite photocatalysts.

Magnetic, electric and thermal properties of soluble polyaniline- ferrite composites

Unit V


M.PHIL. CHEMISTRY

Characterization techniques for polyaniline composites: Structural characterization: UV-vis, FT-IR, XRD, Morphology: SEM, TEM Conductivity: four probe conductivitymeterThermal Analysis:TGA, DSC, Magnetic property: magnetometer.

References

1. Preparation of a conducting Polymer: Polyaniline, Pure Appl Chem, 74, 2002,857-867

2. Preparation, characterization and photochemical degradation of dyes under UVirradiation by inorganic – organic nanocomposites, Materials Science insemiconductor processing 16, 2013, 1904-1911

3. Polyaniline conducting polymer composite materials:, Fabrication andphotocatalytic property, Inorganic Chemistry Communications 35, 2013, 260-264.

4. Synthesis of polymer/ Laponite nanocomposite latex paricles via emulsionpolymerisation using silyated and cation exchanged Laponite clay platelets,Progress in Solid state chemistry 34, 200, 121- 137.

5. Polyaniline: TiO2 Nanocomposites: Synthesis and characterization, Archives ofApplied Science Research, 2010, 2, 194-201.

6. Visible light induced photocatalytic degradation of methylene blue withpolyaniline- sensitized TiO2 composite photocatalysts. Superlattices andMicrostructures 48, 2010, 170-180.

7. Electrical, thermal, photocatalytic and antibacterial studies of metallic oxidenanocomposites doped polyaniline. J. Mater. Sci. Technol. 2013, 29, 795-800.

8. Preparation of PANI- TiO2 nanocomposites and their solid- phase photocatalyticaldegradation, Polymer degradation and stability, 91, 2006, 2213-2219.

9. Synthesis and properties of polyaniline/ ferrite nanocomposites Int. J.Electrochem. Sci. 6, 2011, 206-221.

10. Ferrite- grafted polyaniline nanofibers as electromagnetic shielding Materials. J.Mater. Chem. C, 2013, 1, 2851-59.

11. Formation, mechanism and magnetic properties of hollow Fe3O4 nanospheresynthesize without surfactant. Crys. Eng. Comm, 2012, 14, 858-63.

12. Water dispersible multifunctional polyaniline- laponite- keggin ironnanocomposites through a template approach. J. Mater. Chem, 21, 2011, 16642-50.

13. Micelle assisted synthesis of polyaniline/ magnetite nanorods by in situ self-assembly process, J. Colloids and interface science 320, 2008, 341- 345.


M.PHIL. CHEMISTRY

14. Self assembly approach for the synthesis of electromagnetic functionalizedFe3O4/ Polyaniline nanocomposites: Effect of dopant on the properties. Colloidsand surfaces A: Physicochem. Eng. Aspects 320, 2008, 49-56.

15. Synthesis of a soluble polyaniline- ferrite composite: magnetic and electricproperties. J. Mater. Sci 42, 2007, 7062- 68.

16. Composites of polyaniline containing iron oxides Physica B 354, 2004, 224-227.

CH4A5 Indepth Study of Published Literature on Metal Complexes with Drugs

UNIT -1; Coordination chemistry

Introduction, Nomenclature and terminology, Geometry, isomerism,opticalisomerism,structural

isomerism, electronic properties, colour of transition metal complexes

Unit -II

IR spectroscopy; Vibrational modes, strectching frequencies of various functional frequencies,

Instrumenation and working and applications , isomerism ,metal carbonyls , organometallic

compounds , minerals

Unit – III: UV-Visible spectroscopy;

Instrumentation , working and applications, Structural elucidation by electronic spectroscopy

Unit –IV: NMR spectroscopy, Structural elucidation by 1H, 13C NMR technique, chemical shift, Spin-

Spin Coupling

Unit –V: Application of metal complexes in biological studies. Anti- microbial studies, Anti-

inflammatory Activity, Anti-tuberculosis activity, DNA binding studies – Viscosity method, cyclic

voltammetry, Thermal denaturation studies.

REFERENCES

1. Cotton, Frank Albert Geoferry, Wilkinson, Carlos Murillo(1999), Advanced Inorganic Chemistry,

P 1355 ,ISBN, 978 -0-471199957-1


M.PHIL. CHEMISTRY

2. Instrumental methods of analysis - Hobart H.Willard Lynne L.Meritt, John. A. Dean, Frank.

A.SetleJr

3. Bio inorganic chemistry K. Hussian Reddy, New age international 01-Jan 2007

4. S.K.Kulkarni,Handbook of experimental pharmacology 2nd ed , Vallabh Prakashan , Delhi (1999)p123-128

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