Introduction Lab 1
-
Upload
ameerrashid -
Category
Documents
-
view
214 -
download
0
Transcript of Introduction Lab 1
-
8/18/2019 Introduction Lab 1
1/2
INTRODUCTION
Gaseous diffusivity or gas dispersion apparatus, which involves diffusion with
bulk flow, is one of the laboratory equipment that have been designed to allow
measurement of molecular diffusivities. From this model, it will make the students
become more familiar with the basic notions or concepts of mass transfer theory. This
apparatus is a bench mounted apparatus for the determination of diffusion coefficients of
a vapour in air, which uses the method of measuring the rate of evaporation of a liquid
through a stagnant layer into a flowing air stream, comprising a precision bore capillary
tube, which may be filled from a syringe and the top of which means are provided to pass
air (or an inert gas) stream to remove vapour. The apparatus also consist an air pump, a
travelling microscope with accurate focus adustment and mounted for vertical a!is
movement against a "ernier scale and a thermostatically controlled water bath, in which
to place the capillary tube, capable of accurate temperature control.
Figure #$ Gas %iffusion &pparatus
The e!perimental capabilities of this apparatus are direct measurement of mass
transfer rates in the absence convective effects. Gas laws was used to calculate
concentrations differences in terms of partial pressures while Fick's aw was used to
measure diffusion coefficients in the presence of a stationary gas, measurement of the
effect of temperature on diffusion coefficients and gaining familiarity with the use of
laboratory instruments to achieve accurate measurements of data required for industrial
process design.
-
8/18/2019 Introduction Lab 1
2/2
The diffusivity of the vapour of a volatile liquid in air can be conveniently
determined by inklemann's method in which liquid is contained in a narrow diameter
vertical tube, maintained at a constant temperature, and an air stream is passed over the
top of the tube to ensure the partial pressure of the vapour is transferred from the surface
of the liquid to the air stream by molecular diffusion. The molecular diffusivity, %, is a
kinetic parameter associated with static and dynamic conditions of a process. &ll the
comple!ity and unwieldiness of many calculations is, indeed, connected with the
determination of this quantity.