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ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Denver4955 Yarrow StreetArvada, CO 80002Tel: (303)736-0100

TestAmerica Job ID: 280-54917-1Client Project/Site: Semi Annual Waste Water

For:Intel Corporation / eProcurement4100 Sara RoadMail Stop RR5-491Rio Rancho, New Mexico 87124

Attn: Jeff Rudnik

Authorized for release by:5/19/2014 10:16:27 AM

DiLea Griego, Project Manager I(303)[email protected]

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents

Client: Intel Corporation / eProcurementProject/Site: Semi Annual Waste Water

TestAmerica Job ID: 280-54917-1

Page 2 of 38TestAmerica Denver

5/19/2014

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30

Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37

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Case NarrativeClient: Intel Corporation / eProcurement TestAmerica Job ID: 280-54917-1

Project/Site: Semi Annual Waste Water

Job ID: 280-54917-1

Laboratory: TestAmerica Denver

Narrative

CASE NARRATIVE

Client: Intel Corporation / eProcurement

Project: Semi Annual Waste Water

Report Number: 280-54917-1

With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no

problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control

limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of

the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,

the reporting limits are adjusted relative to the dilution required.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the

individual sections below.

RECEIPT

The samples were received on 05/01/2014; the samples arrived in good condition, properly preserved and on ice. The temperatures of

the coolers at receipt time were 0.5º C and 3.0º C.

The 1-Methyl-2-pyrrilidinone analysis by method 8270C was subcontracted to the TestAmerica Canton laboratory located at, 4101 Shuffel

Street NW, North Canton, OH 44720.

The Butyl Carbitol analysis by method 8015C was subcontracted to the TestAmerica Savannah laboratory located at, 5102 LaRoche

Avenue, Savannah, GA 31404.

VOLATILE ORGANIC COMPOUNDS (GC-MS) - METHOD 8260B

No difficulties were encountered.

SEMIVOLATILE ORGANIC COMPOUNDS (GC-MS) - METHOD 8270C

Samples SV-01 - SV-10 (280-54917-1)[200X] and SV-01 - SV-10 (280-54917-1)[400X] required dilution prior to analysis due to high analyte

concentrations. As such, the surrogate recovery could not be calculated, because the extract was diluted beyond the ability to quantitate a

recovery. The reporting limits have been adjusted accordingly.

The LCS associated with analysis batch 280-129793 exhibited a percent recovery above the QC control limits for 2-Nitrophenol. This is an

indicator that data may be biased high. As no detectable concentrations are present in the associated samples, corrective action is

deemed unnecessary. Usability of the sample data is not compromised.

Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate duplicate (MS/MSD) associated with prep batch

280-129221. The acceptable LCS analyte recoveries provide evidence that the laboratory is performing the method within acceptable

guidelines.

No other difficulties were encountered.

NONHALOGENATED ORGANIC USING GC/FID (DIRECT AQUEOUS INJECTION) - METHOD 8015C


TOTAL METALS - METHOD 6010B


TOTAL RECOVERABLE METALS - METHOD 6020


GENERAL CHEMISTRY

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Case NarrativeClient: Intel Corporation / eProcurement TestAmerica Job ID: 280-54917-1


Job ID: 280-54917-1 (Continued)

Laboratory: TestAmerica Denver (Continued)

Sample SV-01 - SV-10 (280-54917-1)[20X] required dilution prior to analysis for Ammonia, due to high analyte concentrations. The

reporting limits have been adjusted accordingly.

Sample SV-01 - SV-10 (280-54917-1)[10X] required dilution prior to analysis for Total Phosphorus, due to high analyte concentrations.

The reporting limits have been adjusted accordingly.

Sample SV-01 - SV-10 (280-54917-1)[10X] required dilution prior to analysis for COD, due to high analyte concentrations. The reporting

limits have been adjusted accordingly.

The matrix spike / matrix spike duplicate (MS/MSD) samples associated with analysis batch 280-226205 were performed on a sample

from another job and exhibited recoveries outside control limits for Ammonia. The presence of the '4' qualifier in the data indicates

analytes where the concentration in the unspiked sample exceeded four times the spiking amount. Method precision and accuracy have

been verified by the acceptable LCS/LCSD analysis data; therefore, corrective action is deemed unnecessary.

The matrix spike / matrix spike duplicate (MS/MSD) samples associated with analysis batch 280-224839 were performed on SV-01 -

SV-10 (280-54917-1) and exhibited recoveries outside control limits for Total Phosphorus as PO4. The presence of the '4' qualifier in the

data indicates analytes where the concentration in the unspiked sample exceeded four times the spiking amount. Method precision and

accuracy have been verified by the acceptable LCS/LCSD analysis data; therefore, corrective action is deemed unnecessary.

The matrix spike / matrix spike duplicate (MS/MSD) samples associated with analysis batch 280-225201 were performed on a sample

from another job and the MSD exhibited recoveries outside control limits for COD. Method precision and accuracy have been verified by

the acceptable LCS/LCSD analysis data; therefore, corrective action is deemed unnecessary.

No other difficulties were encountered.


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Definitions/GlossaryTestAmerica Job ID: 280-54917-1Client: Intel Corporation / eProcurement


Qualifiers

GC/MS Semi VOA

Qualifier Description

X Surrogate is outside control limits

Qualifier

* LCS or LCSD exceeds the control limits

General Chemistry

Qualifier Description

F1 MS and/or MSD Recovery exceeds the control limits

Qualifier

4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not

applicable.

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Detection SummaryTestAmerica Job ID: 280-54917-1Client: Intel Corporation / eProcurement


Client Sample ID: SV-01 - SV-10 Lab Sample ID: 280-54917-1

1-Methyl-2-pyrrilidinone

RL

3800 ug/L

MDLAnalyte Result Qualifier Unit Dil Fac D Method Prep Type

Total/NA4007500 8270C

Copper 0.010 mg/L Total/NA10.075 6010B

Molybdenum 0.020 mg/L Total/NA10.030 6010B

Nickel 0.0020 mg/L Total

Recoverable

10.0025 6020

Fluoride 0.50 mg/L Total/NA15.9 300.0

Nitrate as N 0.50 mg/L Total/NA17.2 300.0

Ammonia 2.0 mg/L Total/NA2058 350.1

Phosphorus, Total 0.50 mg/L Total/NA108.2 365.1

Total Phosphorus as PO4 1.5 mg/L Total/NA1025 365.1

Chemical Oxygen Demand 200 mg/L Total/NA10280 410.4

Total Dissolved Solids 20 mg/L Total/NA11500 SM 2540C

Total Suspended Solids 4.0 mg/L Total/NA112 SM 2540D

Client Sample ID: TRIP BLANK Lab Sample ID: 280-54917-8

No Detections.

Client Sample ID: COMPOSITE (SV-11 - SV-16) Lab Sample ID: 280-54917-9

Acetone

RL

100 ug/L

MDLAnalyte Result Qualifier Unit Dil Fac D Method Prep Type

Total/NA11400 8260B

TestAmerica Denver

This Detection Summary does not include radiochemical test results.

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Method SummaryTestAmerica Job ID: 280-54917-1Client: Intel Corporation / eProcurement


Method Method Description LaboratoryProtocol

SW8468260B Volatile Organic Compounds (GC/MS) TAL DEN

SW8468270C Semivolatile Organic Compounds (GC/MS) TAL CAN

SW8468015C Nonhalogenated Organic using GC/FID (Direct Aqueous Injection) TAL SAV

SW8466010B Metals (ICP) TAL DEN

SW8466020 Metals (ICP/MS) TAL DEN

1664A1664A HEM and SGT-HEM TAL DEN

MCAWW300.0 Nitrate TAL DEN

40CFR136A300.0 Fluoride TAL DEN

MCAWW350.1 Nitrogen, Ammonia TAL DEN

EPA365.1 Determination of Phosphorus by Semi-Automated Colorimetry TAL DEN

MCAWW410.4 COD TAL DEN

SMSM 2540C Solids, Total Dissolved (TDS) TAL DEN

SMSM 2540D Solids, Total Suspended (TSS) TAL DEN

SMSM5210B BOD, 5 Day TAL DEN

Protocol References:

1664A = EPA-821-98-002

40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater", 40CFR, Part 136, Appendix A, October 26, 1984 and

subsequent revisions.

EPA = US Environmental Protection Agency

MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.

SM = "Standard Methods For The Examination Of Water And Wastewater",

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL CAN = TestAmerica Canton, 4101 Shuffel Street NW, North Canton, OH 44720, TEL (330)497-9396

TAL DEN = TestAmerica Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL (303)736-0100

TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858

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Sample SummaryTestAmerica Job ID: 280-54917-1Client: Intel Corporation / eProcurement


Lab Sample ID Client Sample ID ReceivedCollectedMatrix

280-54917-1 SV-01 - SV-10 Water 04/30/14 09:00 05/01/14 09:30

280-54917-8 TRIP BLANK Water 04/30/14 00:00 05/01/14 09:30

280-54917-9 COMPOSITE (SV-11 - SV-16) Water 04/30/14 00:00 05/01/14 09:30

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Client Sample ResultsTestAmerica Job ID: 280-54917-1Client: Intel Corporation / eProcurement


Method: 8260B - Volatile Organic Compounds (GC/MS)

Lab Sample ID: 280-54917-8Client Sample ID: TRIP BLANK

Matrix: WaterDate Collected: 04/30/14 00:00

Date Received: 05/01/14 09:30RL MDL

Acetone ND 10 ug/L 05/13/14 16:36 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

1.0 ug/L 05/13/14 16:36 1Benzene ND

1.0 ug/L 05/13/14 16:36 1Bromoform ND

1.0 ug/L 05/13/14 16:36 1Bromomethane ND

5.0 ug/L 05/13/14 16:36 12-Butanone (MEK) ND

1.0 ug/L 05/13/14 16:36 1Carbon tetrachloride ND

1.0 ug/L 05/13/14 16:36 1Chlorobenzene ND

1.0 ug/L 05/13/14 16:36 1Chloroethane ND

1.0 ug/L 05/13/14 16:36 1Chloroform ND

1.0 ug/L 05/13/14 16:36 1Chloromethane ND

1.0 ug/L 05/13/14 16:36 1cis-1,3-Dichloropropene ND

1.0 ug/L 05/13/14 16:36 11,1-Dichloroethane ND

1.0 ug/L 05/13/14 16:36 11,2-Dichloroethane ND

1.0 ug/L 05/13/14 16:36 1Bromodichloromethane ND

1.0 ug/L 05/13/14 16:36 11,1-Dichloroethene ND

1.0 ug/L 05/13/14 16:36 11,2-Dichloroethene, Total ND

1.0 ug/L 05/13/14 16:36 11,2-Dichloropropane ND

1.0 ug/L 05/13/14 16:36 1Carbon disulfide ND

1.0 ug/L 05/13/14 16:36 1Ethylbenzene ND

5.0 ug/L 05/13/14 16:36 12-Hexanone ND

1.0 ug/L 05/13/14 16:36 1Dibromochloromethane ND

1.0 ug/L 05/13/14 16:36 1Methylene Chloride ND

5.0 ug/L 05/13/14 16:36 14-Methyl-2-pentanone (MIBK) ND

1.0 ug/L 05/13/14 16:36 1Styrene ND

1.0 ug/L 05/13/14 16:36 11,1,2,2-Tetrachloroethane ND

1.0 ug/L 05/13/14 16:36 1Tetrachloroethene ND

1.0 ug/L 05/13/14 16:36 1Toluene ND

1.0 ug/L 05/13/14 16:36 1trans-1,3-Dichloropropene ND

1.0 ug/L 05/13/14 16:36 11,1,1-Trichloroethane ND

1.0 ug/L 05/13/14 16:36 11,1,2-Trichloroethane ND

1.0 ug/L 05/13/14 16:36 1Trichloroethene ND

1.0 ug/L 05/13/14 16:36 1Vinyl chloride ND

1.0 ug/L 05/13/14 16:36 1Xylenes, Total ND

5.0 ug/L 05/13/14 16:36 1Tetrahydrofuran ND

4-Bromofluorobenzene (Surr) 105 78 - 120 05/13/14 16:36 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

Dibromofluoromethane (Surr) 114 05/13/14 16:36 177 - 120

1,2-Dichloroethane-d4 (Surr) 113 05/13/14 16:36 170 - 127

Toluene-d8 (Surr) 106 05/13/14 16:36 180 - 125

Lab Sample ID: 280-54917-9Client Sample ID: COMPOSITE (SV-11 - SV-16)



Acetone 1400 100 ug/L 05/14/14 00:48 1


10 ug/L 05/14/14 00:48 1Benzene ND

10 ug/L 05/14/14 00:48 1Bromoform ND

10 ug/L 05/14/14 00:48 1Bromomethane ND

50 ug/L 05/14/14 00:48 12-Butanone (MEK) ND

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Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)

Lab Sample ID: 280-54917-9Client Sample ID: COMPOSITE (SV-11 - SV-16)



Carbon tetrachloride ND 10 ug/L 05/14/14 00:48 1


10 ug/L 05/14/14 00:48 1Chlorobenzene ND

10 ug/L 05/14/14 00:48 1Chloroethane ND

10 ug/L 05/14/14 00:48 1Chloroform ND

10 ug/L 05/14/14 00:48 1Chloromethane ND

10 ug/L 05/14/14 00:48 1cis-1,3-Dichloropropene ND

10 ug/L 05/14/14 00:48 11,1-Dichloroethane ND

10 ug/L 05/14/14 00:48 11,2-Dichloroethane ND

10 ug/L 05/14/14 00:48 1Bromodichloromethane ND

10 ug/L 05/14/14 00:48 11,1-Dichloroethene ND

10 ug/L 05/14/14 00:48 11,2-Dichloroethene, Total ND

10 ug/L 05/14/14 00:48 11,2-Dichloropropane ND

10 ug/L 05/14/14 00:48 1Carbon disulfide ND

10 ug/L 05/14/14 00:48 1Ethylbenzene ND

50 ug/L 05/14/14 00:48 12-Hexanone ND

10 ug/L 05/14/14 00:48 1Dibromochloromethane ND

10 ug/L 05/14/14 00:48 1Methylene Chloride ND

50 ug/L 05/14/14 00:48 14-Methyl-2-pentanone (MIBK) ND

10 ug/L 05/14/14 00:48 1Styrene ND

10 ug/L 05/14/14 00:48 11,1,2,2-Tetrachloroethane ND

10 ug/L 05/14/14 00:48 1Tetrachloroethene ND

10 ug/L 05/14/14 00:48 1Toluene ND

10 ug/L 05/14/14 00:48 1trans-1,3-Dichloropropene ND

10 ug/L 05/14/14 00:48 11,1,1-Trichloroethane ND

10 ug/L 05/14/14 00:48 11,1,2-Trichloroethane ND

10 ug/L 05/14/14 00:48 1Trichloroethene ND

10 ug/L 05/14/14 00:48 1Vinyl chloride ND

10 ug/L 05/14/14 00:48 1Xylenes, Total ND

50 ug/L 05/14/14 00:48 1Tetrahydrofuran ND



Dibromofluoromethane (Surr) 101 05/14/14 00:48 177 - 120

1,2-Dichloroethane-d4 (Surr) 99 05/14/14 00:48 170 - 127

Toluene-d8 (Surr) 117 05/14/14 00:48 180 - 125

Method: 8270C - Semivolatile Organic Compounds (GC/MS)

Lab Sample ID: 280-54917-1Client Sample ID: SV-01 - SV-10



1-Methyl-2-pyrrilidinone 7500 3800 ug/L 05/05/14 07:57 05/13/14 11:30 400


2,4,6-Tribromophenol (Surr) 0 X 21 - 110 05/05/14 07:57 05/12/14 16:45 200


2,4,6-Tribromophenol (Surr) 0 X 05/05/14 07:57 05/13/14 11:30 40021 - 110

2-Fluorobiphenyl (Surr) 149 X 05/05/14 07:57 05/12/14 16:45 20020 - 110

2-Fluorobiphenyl (Surr) 0 X 05/05/14 07:57 05/13/14 11:30 40020 - 110

2-Fluorophenol (Surr) 122 X 05/05/14 07:57 05/12/14 16:45 20010 - 110

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Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)



Date Received: 05/01/14 09:30

2-Fluorophenol (Surr) 0 X 10 - 110 05/05/14 07:57 05/13/14 11:30 400


Nitrobenzene-d5 (Surr) 162 X 05/05/14 07:57 05/12/14 16:45 20021 - 110

Nitrobenzene-d5 (Surr) 0 X 05/05/14 07:57 05/13/14 11:30 40021 - 110

Phenol-d5 (Surr) 92 05/05/14 07:57 05/12/14 16:45 20021 - 110

Phenol-d5 (Surr) 0 X 05/05/14 07:57 05/13/14 11:30 40021 - 110

Terphenyl-d14 (Surr) 75 05/05/14 07:57 05/12/14 16:45 20024 - 110

Terphenyl-d14 (Surr) 0 X 05/05/14 07:57 05/13/14 11:30 40024 - 110

Method: 8015C - Nonhalogenated Organic using GC/FID (Direct Aqueous Injection)




Butyl carbitol ND 5.0 mg/L 05/09/14 00:02 1


Method: 6010B - Metals (ICP)




Arsenic ND 0.010 mg/L 05/02/14 07:30 05/13/14 01:40 1


0.010 mg/L 05/02/14 07:30 05/13/14 01:40 1Copper 0.075

0.0030 mg/L 05/02/14 07:30 05/13/14 01:40 1Lead ND

0.020 mg/L 05/02/14 07:30 05/13/14 01:40 1Molybdenum 0.030

0.0050 mg/L 05/02/14 07:30 05/13/14 01:40 1Silver ND

Method: 6020 - Metals (ICP/MS) - Total Recoverable




Nickel 0.0025 0.0020 mg/L 05/02/14 07:30 05/02/14 17:42 1


General Chemistry




HEM ND 5.0 mg/L 05/13/14 14:56 05/13/14 18:43 1


6.1 mg/L 05/13/14 14:56 05/13/14 18:43 1SGT-HEM ND

0.50 mg/L 05/01/14 20:16 1Fluoride 5.9

0.50 mg/L 05/01/14 20:16 1Nitrate as N 7.2

2.0 mg/L 05/15/14 16:54 20Ammonia 58

0.50 mg/L 05/06/14 09:57 05/07/14 16:01 10Phosphorus, Total 8.2

1.5 mg/L 05/06/14 09:57 05/07/14 16:10 10Total Phosphorus as PO4 25

200 mg/L 05/10/14 09:11 10Chemical Oxygen Demand 280

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General Chemistry (Continued)




Total Dissolved Solids 1500 20 mg/L 05/02/14 12:40 1


4.0 mg/L 05/02/14 16:50 1Total Suspended Solids 12

2.0 mg/L 05/01/14 16:51 1Biochemical Oxygen Demand ND

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QC Sample ResultsTestAmerica Job ID: 280-54917-1Client: Intel Corporation / eProcurement


Method: 8260B - Volatile Organic Compounds (GC/MS)

Client Sample ID: Method BlankLab Sample ID: MB 280-225443/6

Matrix: Water Prep Type: Total/NA

Analysis Batch: 225443

RL MDL

Acetone ND 10 ug/L 05/13/14 08:04 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

ND 1.0 ug/L 05/13/14 08:04 1Benzene

ND 1.0 ug/L 05/13/14 08:04 1Bromoform

ND 1.0 ug/L 05/13/14 08:04 1Bromomethane

ND 5.0 ug/L 05/13/14 08:04 12-Butanone (MEK)

ND 1.0 ug/L 05/13/14 08:04 1Carbon tetrachloride

ND 1.0 ug/L 05/13/14 08:04 1Chlorobenzene

ND 1.0 ug/L 05/13/14 08:04 1Chloroethane

ND 1.0 ug/L 05/13/14 08:04 1Chloroform

ND 1.0 ug/L 05/13/14 08:04 1Chloromethane

ND 1.0 ug/L 05/13/14 08:04 1cis-1,3-Dichloropropene

ND 1.0 ug/L 05/13/14 08:04 11,1-Dichloroethane


ND 1.0 ug/L 05/13/14 08:04 1Bromodichloromethane

ND 1.0 ug/L 05/13/14 08:04 11,1-Dichloroethene

ND 1.0 ug/L 05/13/14 08:04 11,2-Dichloroethene, Total

ND 1.0 ug/L 05/13/14 08:04 11,2-Dichloropropane

ND 1.0 ug/L 05/13/14 08:04 1Carbon disulfide

ND 1.0 ug/L 05/13/14 08:04 1Ethylbenzene

ND 5.0 ug/L 05/13/14 08:04 12-Hexanone

ND 1.0 ug/L 05/13/14 08:04 1Dibromochloromethane

ND 1.0 ug/L 05/13/14 08:04 1Methylene Chloride

ND 5.0 ug/L 05/13/14 08:04 14-Methyl-2-pentanone (MIBK)

ND 1.0 ug/L 05/13/14 08:04 1Styrene

ND 1.0 ug/L 05/13/14 08:04 11,1,2,2-Tetrachloroethane

ND 1.0 ug/L 05/13/14 08:04 1Tetrachloroethene

ND 1.0 ug/L 05/13/14 08:04 1Toluene

ND 1.0 ug/L 05/13/14 08:04 1trans-1,3-Dichloropropene

ND 1.0 ug/L 05/13/14 08:04 11,1,1-Trichloroethane


ND 1.0 ug/L 05/13/14 08:04 1Trichloroethene

ND 1.0 ug/L 05/13/14 08:04 1Vinyl chloride

ND 1.0 ug/L 05/13/14 08:04 1Xylenes, Total

ND 5.0 ug/L 05/13/14 08:04 1Tetrahydrofuran


MB MB

Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery

106 05/13/14 08:04 1Dibromofluoromethane (Surr) 77 - 120

101 05/13/14 08:04 11,2-Dichloroethane-d4 (Surr) 70 - 127

102 05/13/14 08:04 1Toluene-d8 (Surr) 80 - 125

Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-225443/4



Benzene 5.00 5.01 ug/L 100 74 - 135

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Carbon tetrachloride 5.00 5.01 ug/L 100 67 - 135

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Chlorobenzene 5.00 5.54 ug/L 111 76 - 135

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Chloroform 5.00 5.09 ug/L 102 76 - 120

1,1-Dichloroethane 5.00 4.98 ug/L 100 75 - 135

Bromodichloromethane 5.00 4.96 ug/L 99 73 - 135

1,1-Dichloroethene 5.00 4.59 ug/L 92 71 - 136

1,2-Dichloropropane 5.00 5.18 ug/L 104 71 - 120

Carbon disulfide 5.00 4.55 ug/L 91 34 - 150

Ethylbenzene 5.00 5.56 ug/L 111 72 - 120

Methylene Chloride 5.00 5.21 ug/L 104 54 - 141

Tetrachloroethene 5.00 5.32 ug/L 106 70 - 135

Toluene 5.00 5.32 ug/L 106 73 - 120

1,1,1-Trichloroethane 5.00 5.08 ug/L 102 70 - 135

Trichloroethene 5.00 5.18 ug/L 104 73 - 135

4-Bromofluorobenzene (Surr) 78 - 120

Surrogate

94

LCS LCS

Qualifier Limits%Recovery

105Dibromofluoromethane (Surr) 77 - 120

961,2-Dichloroethane-d4 (Surr) 70 - 127

109Toluene-d8 (Surr) 80 - 125

Client Sample ID: Matrix SpikeLab Sample ID: 280-54928-R-4 MS



Benzene ND 5.00 4.97 ug/L 99 74 - 135

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Carbon tetrachloride ND 5.00 5.38 ug/L 108 67 - 135

Chlorobenzene ND 5.00 5.49 ug/L 110 76 - 135

Chloroform ND 5.00 5.21 ug/L 104 76 - 120

1,1-Dichloroethane ND 5.00 5.24 ug/L 105 75 - 135

Bromodichloromethane ND 5.00 5.21 ug/L 104 73 - 135

1,1-Dichloroethene ND 5.00 4.69 ug/L 94 71 - 136

1,2-Dichloropropane ND 5.00 5.23 ug/L 105 71 - 120

Carbon disulfide ND 5.00 4.80 ug/L 96 34 - 150

Ethylbenzene ND 5.00 5.45 ug/L 109 72 - 120

Methylene Chloride ND 5.00 3.79 ug/L 76 54 - 141

Tetrachloroethene ND 5.00 5.21 ug/L 104 70 - 135

Toluene ND 5.00 5.35 ug/L 107 73 - 120

1,1,1-Trichloroethane ND 5.00 5.25 ug/L 105 70 - 135

Trichloroethene ND 5.00 5.29 ug/L 106 73 - 135


Surrogate

101

MS MS





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Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-54928-R-4 MSD



Benzene ND 5.00 5.14 ug/L 103 74 - 135 3 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Carbon tetrachloride ND 5.00 5.33 ug/L 107 67 - 135 1 21

Chlorobenzene ND 5.00 5.74 ug/L 115 76 - 135 4 20

Chloroform ND 5.00 5.35 ug/L 107 76 - 120 3 20

1,1-Dichloroethane ND 5.00 5.32 ug/L 106 75 - 135 1 21

Bromodichloromethane ND 5.00 5.19 ug/L 104 73 - 135 0 20

1,1-Dichloroethene ND 5.00 4.79 ug/L 96 71 - 136 2 20

1,2-Dichloropropane ND 5.00 5.37 ug/L 107 71 - 120 3 20

Carbon disulfide ND 5.00 4.98 ug/L 100 34 - 150 4 20

Ethylbenzene ND 5.00 5.60 ug/L 112 72 - 120 3 26

Methylene Chloride ND 5.00 3.98 ug/L 80 54 - 141 5 20

Tetrachloroethene ND 5.00 5.41 ug/L 108 70 - 135 4 20

Toluene ND 5.00 5.53 ug/L 111 73 - 120 3 20

1,1,1-Trichloroethane ND 5.00 5.35 ug/L 107 70 - 135 2 20

Trichloroethene ND 5.00 5.42 ug/L 108 73 - 135 2 20


Surrogate

107

MSD MSD








RL MDL

Acetone ND 10 ug/L 05/13/14 21:38 1

MB MB


ND 1.0 ug/L 05/13/14 21:38 1Benzene

ND 1.0 ug/L 05/13/14 21:38 1Bromoform

ND 1.0 ug/L 05/13/14 21:38 1Bromomethane

ND 5.0 ug/L 05/13/14 21:38 12-Butanone (MEK)

ND 1.0 ug/L 05/13/14 21:38 1Carbon tetrachloride

ND 1.0 ug/L 05/13/14 21:38 1Chlorobenzene

ND 1.0 ug/L 05/13/14 21:38 1Chloroethane

ND 1.0 ug/L 05/13/14 21:38 1Chloroform

ND 1.0 ug/L 05/13/14 21:38 1Chloromethane

ND 1.0 ug/L 05/13/14 21:38 1cis-1,3-Dichloropropene



ND 1.0 ug/L 05/13/14 21:38 1Bromodichloromethane

ND 1.0 ug/L 05/13/14 21:38 11,1-Dichloroethene

ND 1.0 ug/L 05/13/14 21:38 11,2-Dichloroethene, Total

ND 1.0 ug/L 05/13/14 21:38 11,2-Dichloropropane

ND 1.0 ug/L 05/13/14 21:38 1Carbon disulfide

ND 1.0 ug/L 05/13/14 21:38 1Ethylbenzene

ND 5.0 ug/L 05/13/14 21:38 12-Hexanone

ND 1.0 ug/L 05/13/14 21:38 1Dibromochloromethane

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RL MDL

Methylene Chloride ND 1.0 ug/L 05/13/14 21:38 1

MB MB


ND 5.0 ug/L 05/13/14 21:38 14-Methyl-2-pentanone (MIBK)

ND 1.0 ug/L 05/13/14 21:38 1Styrene

ND 1.0 ug/L 05/13/14 21:38 11,1,2,2-Tetrachloroethane

ND 1.0 ug/L 05/13/14 21:38 1Tetrachloroethene

ND 1.0 ug/L 05/13/14 21:38 1Toluene

ND 1.0 ug/L 05/13/14 21:38 1trans-1,3-Dichloropropene



ND 1.0 ug/L 05/13/14 21:38 1Trichloroethene

ND 1.0 ug/L 05/13/14 21:38 1Vinyl chloride

ND 1.0 ug/L 05/13/14 21:38 1Xylenes, Total

ND 5.0 ug/L 05/13/14 21:38 1Tetrahydrofuran


MB MB

Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery

108 05/13/14 21:38 1Dibromofluoromethane (Surr) 77 - 120

107 05/13/14 21:38 11,2-Dichloroethane-d4 (Surr) 70 - 127

118 05/13/14 21:38 1Toluene-d8 (Surr) 80 - 125




Benzene 5.00 4.14 ug/L 83 74 - 135

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Carbon tetrachloride 5.00 4.44 ug/L 89 67 - 135

Chlorobenzene 5.00 4.50 ug/L 90 76 - 135

Chloroform 5.00 4.42 ug/L 88 76 - 120

1,1-Dichloroethane 5.00 4.44 ug/L 89 75 - 135

Bromodichloromethane 5.00 4.18 ug/L 84 73 - 135

1,1-Dichloroethene 5.00 4.15 ug/L 83 71 - 136

1,2-Dichloropropane 5.00 4.32 ug/L 86 71 - 120

Carbon disulfide 5.00 3.81 ug/L 76 34 - 150

Ethylbenzene 5.00 4.58 ug/L 92 72 - 120

Methylene Chloride 5.00 4.25 ug/L 85 54 - 141

Tetrachloroethene 5.00 4.69 ug/L 94 70 - 135

Toluene 5.00 4.42 ug/L 88 73 - 120

1,1,1-Trichloroethane 5.00 4.73 ug/L 95 70 - 135

Trichloroethene 5.00 4.65 ug/L 93 73 - 135


Surrogate

104

LCS LCS





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Client Sample ID: Matrix SpikeLab Sample ID: 280-54959-D-8 MS



Benzene ND 5.00 4.19 ug/L 84 74 - 135

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Carbon tetrachloride ND 5.00 4.36 ug/L 87 67 - 135

Chlorobenzene ND 5.00 4.57 ug/L 91 76 - 135

Chloroform ND 5.00 4.48 ug/L 90 76 - 120

1,1-Dichloroethane ND 5.00 4.47 ug/L 89 75 - 135

Bromodichloromethane ND 5.00 4.05 ug/L 81 73 - 135

1,1-Dichloroethene ND 5.00 4.15 ug/L 83 71 - 136

1,2-Dichloropropane ND 5.00 4.25 ug/L 85 71 - 120

Carbon disulfide ND 5.00 4.09 ug/L 82 34 - 150

Ethylbenzene ND 5.00 4.64 ug/L 93 72 - 120

Methylene Chloride ND 5.00 3.66 ug/L 73 54 - 141

Tetrachloroethene ND 5.00 4.70 ug/L 94 70 - 135

Toluene ND 5.00 4.41 ug/L 88 73 - 120

1,1,1-Trichloroethane ND 5.00 4.70 ug/L 94 70 - 135

Trichloroethene ND 5.00 4.59 ug/L 92 73 - 135


Surrogate

107

MS MS





Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-54959-D-8 MSD



Benzene ND 5.00 4.75 ug/L 95 74 - 135 13 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Carbon tetrachloride ND 5.00 4.90 ug/L 98 67 - 135 12 21

Chlorobenzene ND 5.00 5.18 ug/L 104 76 - 135 12 20

Chloroform ND 5.00 5.01 ug/L 100 76 - 120 11 20

1,1-Dichloroethane ND 5.00 4.94 ug/L 99 75 - 135 10 21

Bromodichloromethane ND 5.00 4.61 ug/L 92 73 - 135 13 20

1,1-Dichloroethene ND 5.00 4.64 ug/L 93 71 - 136 11 20

1,2-Dichloropropane ND 5.00 4.83 ug/L 97 71 - 120 13 20

Carbon disulfide ND 5.00 4.56 ug/L 91 34 - 150 11 20

Ethylbenzene ND 5.00 5.25 ug/L 105 72 - 120 12 26

Methylene Chloride ND 5.00 4.27 ug/L 85 54 - 141 15 20

Tetrachloroethene ND 5.00 5.22 ug/L 104 70 - 135 10 20

Toluene ND 5.00 4.95 ug/L 99 73 - 120 12 20

1,1,1-Trichloroethane ND 5.00 5.33 ug/L 107 70 - 135 13 20

Trichloroethene ND 5.00 5.19 ug/L 104 73 - 135 12 20


Surrogate

105

MSD MSD




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Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-54959-D-8 MSD



Toluene-d8 (Surr) 80 - 125

Surrogate

116

MSD MSD


Method: 8270C - Semivolatile Organic Compounds (GC/MS)

Client Sample ID: Method BlankLab Sample ID: MB 240-129221/21-A


Analysis Batch: 129793 Prep Batch: 129221

RL MDL

1-Methyl-2-pyrrilidinone ND 10 ug/L 05/05/14 07:57 05/08/14 17:04 1

MB MB


2,4,6-Tribromophenol (Surr) 82 21 - 110 05/08/14 17:04 1

MB MB

Surrogate

05/05/14 07:57

Dil FacPrepared AnalyzedQualifier Limits%Recovery

81 05/05/14 07:57 05/08/14 17:04 12-Fluorobiphenyl (Surr) 20 - 110

84 05/05/14 07:57 05/08/14 17:04 12-Fluorophenol (Surr) 10 - 110

90 05/05/14 07:57 05/08/14 17:04 1Nitrobenzene-d5 (Surr) 21 - 110

92 05/05/14 07:57 05/08/14 17:04 1Phenol-d5 (Surr) 21 - 110

99 05/05/14 07:57 05/08/14 17:04 1Terphenyl-d14 (Surr) 24 - 110

Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-129221/22-A



1,2,4-Trichlorobenzene 20.0 14.2 ug/L 71 35 - 110

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

2,4,6-Trichlorophenol 20.0 19.7 ug/L 99 45 - 110

2,4-Dichlorophenol 20.0 20.0 ug/L 100 41 - 110

2,4-Dimethylphenol 20.0 15.1 ug/L 76 32 - 110

2,4-Dinitrophenol 40.0 40.9 ug/L 102 10 - 110

2,4-Dinitrotoluene 20.0 20.5 ug/L 103 53 - 110

2,6-Dinitrotoluene 20.0 20.8 ug/L 104 54 - 110

2-Chloronaphthalene 20.0 16.8 ug/L 84 43 - 110

2-Chlorophenol 20.0 19.5 ug/L 97 29 - 110

2-Nitrophenol 20.0 23.4 * ug/L 117 40 - 110

2,4,6-Tribromophenol (Surr) 21 - 110

Surrogate

105

LCS LCS


872-Fluorobiphenyl (Surr) 20 - 110

892-Fluorophenol (Surr) 10 - 110

100Nitrobenzene-d5 (Surr) 21 - 110

101Phenol-d5 (Surr) 21 - 110

106Terphenyl-d14 (Surr) 24 - 110

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Method: 8015C - Nonhalogenated Organic using GC/FID (Direct Aqueous Injection)




RL MDL

Butyl carbitol ND 5.0 mg/L 05/08/14 22:18 1

MB MB





Butyl carbitol 40.0 33.2 mg/L 83 50 - 150

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 680-328335/3



Butyl carbitol 40.0 39.0 mg/L 98 50 - 150 16 50

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

Client Sample ID: SV-01 - SV-10Lab Sample ID: 280-54917-1 MS



Butyl carbitol ND 40.0 22.6 mg/L 57 50 - 150

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: SV-01 - SV-10Lab Sample ID: 280-54917-1 MSD



Butyl carbitol ND 40.0 32.0 mg/L 80 50 - 150 34 50

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Method: 6010B - Metals (ICP)




RL MDL

Arsenic ND 0.010 mg/L 05/02/14 07:30 05/13/14 00:51 1

MB MB


ND 0.010 mg/L 05/02/14 07:30 05/13/14 00:51 1Copper

ND 0.0030 mg/L 05/02/14 07:30 05/13/14 00:51 1Lead

ND 0.020 mg/L 05/02/14 07:30 05/13/14 00:51 1Molybdenum

ND 0.0050 mg/L 05/02/14 07:30 05/13/14 00:51 1Silver




Arsenic 1.00 1.02 mg/L 102 88 - 110

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

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Method: 6010B - Metals (ICP) (Continued)




Copper 0.250 0.255 mg/L 102 86 - 112

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Lead 0.500 0.502 mg/L 100 89 - 110

Molybdenum 1.00 1.05 mg/L 105 90 - 110

Silver 0.0500 0.0511 mg/L 102 86 - 115

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-223813/3-A



Arsenic 1.00 1.05 mg/L 105 88 - 110 3 20

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

Copper 0.250 0.264 mg/L 106 86 - 112 4 20

Lead 0.500 0.513 mg/L 103 89 - 110 2 20

Molybdenum 1.00 1.05 mg/L 105 90 - 110 1 20

Silver 0.0500 0.0529 mg/L 106 86 - 115 3 20

Client Sample ID: Matrix SpikeLab Sample ID: 280-54935-A-13-B MS



Arsenic ND 1.00 1.06 mg/L 106 84 - 124

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Copper ND 0.250 0.264 mg/L 105 82 - 129

Lead ND 0.500 0.485 mg/L 97 89 - 121

Molybdenum ND 1.00 1.05 mg/L 105 83 - 109

Silver ND 0.0500 0.0533 mg/L 107 75 - 141

Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-54935-A-13-C MSD



Arsenic ND 1.00 1.06 mg/L 106 84 - 124 0 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Copper ND 0.250 0.265 mg/L 105 82 - 129 1 20

Lead ND 0.500 0.490 mg/L 98 89 - 121 1 20

Molybdenum ND 1.00 1.05 mg/L 105 83 - 109 0 20

Silver ND 0.0500 0.0533 mg/L 107 75 - 141 0 20

Method: 6020 - Metals (ICP/MS)


Matrix: Water Prep Type: Total Recoverable


RL MDL

Nickel ND 0.0020 mg/L 05/02/14 07:30 05/02/14 17:09 1

MB MB


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Method: 6020 - Metals (ICP/MS) (Continued)




Nickel 0.0400 0.0407 mg/L 102 85 - 119

Analyte

LCS LCS


Spike

Added

%Rec.

Limits




Nickel 0.0025 0.0400 0.0406 mg/L 95 85 - 119

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits




Nickel 0.0025 0.0400 0.0427 mg/L 101 85 - 119 5 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Method: 1664A - HEM and SGT-HEM




RL MDL

HEM ND 5.0 mg/L 05/13/14 14:56 05/13/14 18:43 1

MB MB


ND 6.0 mg/L 05/13/14 14:56 05/13/14 18:43 1SGT-HEM




HEM 40.0 34.0 mg/L 85 78 - 114

Analyte

LCS LCS


Spike

Added

%Rec.

Limits




HEM 40.0 35.2 mg/L 88 78 - 114 3 18

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD




HEM ND 40.4 35.5 mg/L 81 78 - 114

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

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Method: 1664A - HEM and SGT-HEM (Continued)




HEM ND 41.0 37.7 mg/L 85 78 - 114 6 18

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Method: 300.0 - Nitrate




RL MDL

Nitrate as N ND 0.50 mg/L 05/01/14 11:19 1

MB MB





Nitrate as N 5.00 4.77 mg/L 95 90 - 110

Analyte

LCS LCS


Spike

Added

%Rec.

Limits




Nitrate as N 5.00 4.79 mg/L 96 90 - 110 0 10

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

Client Sample ID: Lab Control SampleLab Sample ID: MRL 280-223698/3



Nitrate as N 0.200 ND mg/L 107 50 - 150

Analyte

MRL MRL


Spike

Added

%Rec.

Limits

Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-54926-P-1 MSD



Nitrate as N 0.77 5.00 6.08 mg/L 106 80 - 120 2 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Client Sample ID: Matrix SpikeLab Sample ID: 280-54926-Q-1 MS



Nitrate as N 0.77 5.00 5.93 mg/L 103 80 - 120

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

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Method: 300.0 - Nitrate (Continued)

Client Sample ID: DuplicateLab Sample ID: 280-54926-R-1 DU



Nitrate as N 0.77 0.782 mg/L 1 15

Analyte

DU DU

DUnitResult Qualifier

Sample

Result

Sample

Qualifier LimitRPD

RPD

Method: 300.0 - Fluoride




RL MDL

Fluoride ND 0.50 mg/L 05/01/14 11:19 1

MB MB





Fluoride 5.00 5.21 mg/L 104 90 - 110

Analyte

LCS LCS


Spike

Added

%Rec.

Limits




Fluoride 5.00 5.23 mg/L 105 90 - 110 0 10

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

Client Sample ID: Lab Control SampleLab Sample ID: MRL 280-223699/3



Fluoride 0.200 ND mg/L 109 50 - 150

Analyte

MRL MRL


Spike

Added

%Rec.

Limits

Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-54926-P-1 MSD



Fluoride 0.75 5.00 6.29 mg/L 111 80 - 120 2 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Client Sample ID: Matrix SpikeLab Sample ID: 280-54926-Q-1 MS



Fluoride 0.75 5.00 6.19 mg/L 109 80 - 120

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

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Method: 300.0 - Fluoride (Continued)

Client Sample ID: DuplicateLab Sample ID: 280-54926-R-1 DU



Fluoride 0.75 0.767 mg/L 3 15

Analyte

DU DU


Sample

Result

Sample

Qualifier LimitRPD

RPD

Method: 350.1 - Nitrogen, Ammonia




RL MDL

Ammonia ND 0.10 mg/L 05/15/14 19:49 1

MB MB





RL MDL

Ammonia ND 0.10 mg/L 05/15/14 16:34 1

MB MB





Ammonia 2.50 2.41 mg/L 96 90 - 110

Analyte

LCS LCS


Spike

Added

%Rec.

Limits




Ammonia 2.50 2.50 mg/L 100 90 - 110

Analyte

LCS LCS


Spike

Added

%Rec.

Limits




Ammonia 2.50 2.57 mg/L 103 90 - 110 7 10

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD




Ammonia 2.50 2.45 mg/L 98 90 - 110 2 10

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

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Method: 350.1 - Nitrogen, Ammonia (Continued)

Client Sample ID: Matrix SpikeLab Sample ID: 280-55261-A-15 MS



Ammonia 97 20.0 108 4 mg/L 57 90 - 110

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-55261-A-15 MSD



Ammonia 97 20.0 113 4 mg/L 80 90 - 110 4 10

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Method: 365.1 - Determination of Phosphorus by Semi-Automated Colorimetry




RL MDL

Phosphorus, Total ND 0.050 mg/L 05/06/14 09:57 05/07/14 14:19 1

MB MB





RL MDL

Total Phosphorus as PO4 ND 0.15 mg/L 05/06/14 09:57 05/07/14 16:10 1

MB MB





Phosphorus, Total 0.500 0.515 mg/L 103 90 - 110

Analyte

LCS LCS


Spike

Added

%Rec.

Limits




Total Phosphorus as PO4 1.53 1.55 mg/L 101 90 - 110

Analyte

LCS LCS


Spike

Added

%Rec.

Limits




Phosphorus, Total 0.500 0.522 mg/L 104 90 - 110 1 10

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

TestAmerica Denver

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Method: 365.1 - Determination of Phosphorus by Semi-Automated Colorimetry (Continued)




Total Phosphorus as PO4 1.53 1.59 mg/L 104 90 - 110 3 10

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD




Phosphorus, Total 8.2 0.500 7.99 mg/L -33 90 - 110

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits




Total Phosphorus as PO4 25 1.53 24.5 4 mg/L -30 90 - 110

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits




Phosphorus, Total 8.2 0.500 8.21 mg/L 12 90 - 110 3 10

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD




Total Phosphorus as PO4 25 1.53 25.3 4 mg/L 20 90 - 110 3 10

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Method: 410.4 - COD




RL MDL

Chemical Oxygen Demand ND 20 mg/L 05/10/14 09:11 1

MB MB





Chemical Oxygen Demand 100 102 mg/L 102 90 - 110

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

TestAmerica Denver

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Method: 410.4 - COD (Continued)




Chemical Oxygen Demand 100 96.1 mg/L 96 90 - 110 6 11

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

Client Sample ID: Matrix SpikeLab Sample ID: 280-54800-B-8 MS



Chemical Oxygen Demand ND 50.0 54.4 mg/L 96 90 - 110

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-54800-B-8 MSD



Chemical Oxygen Demand ND 50.0 50.8 F1 mg/L 89 90 - 110 7 11

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Method: SM 2540C - Solids, Total Dissolved (TDS)




RL MDL

Total Dissolved Solids ND 10 mg/L 05/02/14 12:40 1

MB MB





Total Dissolved Solids 500 471 mg/L 94 86 - 110

Analyte

LCS LCS


Spike

Added

%Rec.

Limits




Total Dissolved Solids 500 489 mg/L 98 86 - 110 4 20

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

Client Sample ID: SV-01 - SV-10Lab Sample ID: 280-54917-1 DU



Total Dissolved Solids 1500 1510 mg/L 2 10

Analyte

DU DU


Sample

Result

Sample

Qualifier LimitRPD

RPD

TestAmerica Denver

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Method: SM 2540D - Solids, Total Suspended (TSS)




RL MDL

Total Suspended Solids ND 4.0 mg/L 05/02/14 16:50 1

MB MB





Total Suspended Solids 100 89.0 mg/L 89 86 - 114

Analyte

LCS LCS


Spike

Added

%Rec.

Limits




Total Suspended Solids 100 92.0 mg/L 92 86 - 114 3 20

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

Client Sample ID: DuplicateLab Sample ID: 280-54941-G-2 DU



Total Suspended Solids 26 24.8 mg/L 6 10

Analyte

DU DU


Sample

Result

Sample

Qualifier LimitRPD

RPD

Method: SM5210B - BOD, 5 Day




RL MDL

Biochemical Oxygen Demand ND 2.0 mg/L 05/01/14 16:50 1

MB MB





Biochemical Oxygen Demand 198 204 mg/L 103 85 - 115

Analyte

LCS LCS


Spike

Added

%Rec.

Limits




Biochemical Oxygen Demand 198 205 mg/L 104 85 - 115 0 20

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

TestAmerica Denver

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Method: SM5210B - BOD, 5 Day (Continued)

Client Sample ID: SV-01 - SV-10Lab Sample ID: 280-54917-1 DU



Biochemical Oxygen Demand ND ND mg/L NC 20

Analyte

DU DU


Sample

Result

Sample

Qualifier LimitRPD

RPD

TestAmerica Denver

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QC Association SummaryTestAmerica Job ID: 280-54917-1Client: Intel Corporation / eProcurement


GC/MS VOA


Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 8260B280-54917-8 TRIP BLANK Total/NA

Water 8260B280-54928-R-4 MS Matrix Spike Total/NA

Water 8260B280-54928-R-4 MSD Matrix Spike Duplicate Total/NA

Water 8260BLCS 280-225443/4 Lab Control Sample Total/NA

Water 8260BMB 280-225443/6 Method Blank Total/NA



Water 8260B280-54917-9 COMPOSITE (SV-11 - SV-16) Total/NA

Water 8260B280-54959-D-8 MS Matrix Spike Total/NA

Water 8260B280-54959-D-8 MSD Matrix Spike Duplicate Total/NA

Water 8260BLCS 280-225628/6 Lab Control Sample Total/NA

Water 8260BMB 280-225628/7 Method Blank Total/NA

GC/MS Semi VOA

Prep Batch: 129221


Water 3520C280-54917-1 SV-01 - SV-10 Total/NA

Water 3520CLCS 240-129221/22-A Lab Control Sample Total/NA

Water 3520CMB 240-129221/21-A Method Blank Total/NA



Water 8270C 129221LCS 240-129221/22-A Lab Control Sample Total/NA

Water 8270C 129221MB 240-129221/21-A Method Blank Total/NA



Water 8270C 129221280-54917-1 SV-01 - SV-10 Total/NA



Water 8270C 129221280-54917-1 SV-01 - SV-10 Total/NA

GC VOA



Water 8015C280-54917-1 SV-01 - SV-10 Total/NA

Water 8015C280-54917-1 MS SV-01 - SV-10 Total/NA

Water 8015C280-54917-1 MSD SV-01 - SV-10 Total/NA

Water 8015CLCS 680-328335/2 Lab Control Sample Total/NA

Water 8015CLCSD 680-328335/3 Lab Control Sample Dup Total/NA

Water 8015CMB 680-328335/5 Method Blank Total/NA

TestAmerica Denver

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Metals

Prep Batch: 223803


Water 3005A280-54917-1 SV-01 - SV-10 Total Recoverable

Water 3005A280-54917-1 MS SV-01 - SV-10 Total Recoverable

Water 3005A280-54917-1 MSD SV-01 - SV-10 Total Recoverable

Water 3005ALCS 280-223803/2-A Lab Control Sample Total Recoverable

Water 3005AMB 280-223803/1-A Method Blank Total Recoverable

Prep Batch: 223813


Water 3010A280-54917-1 SV-01 - SV-10 Total/NA

Water 3010A280-54935-A-13-B MS Matrix Spike Total/NA

Water 3010A280-54935-A-13-C MSD Matrix Spike Duplicate Total/NA

Water 3010ALCS 280-223813/2-A Lab Control Sample Total/NA

Water 3010ALCSD 280-223813/3-A Lab Control Sample Dup Total/NA

Water 3010AMB 280-223813/1-A Method Blank Total/NA



Water 6020 223803280-54917-1 SV-01 - SV-10 Total Recoverable

Water 6020 223803280-54917-1 MS SV-01 - SV-10 Total Recoverable

Water 6020 223803280-54917-1 MSD SV-01 - SV-10 Total Recoverable

Water 6020 223803LCS 280-223803/2-A Lab Control Sample Total Recoverable

Water 6020 223803MB 280-223803/1-A Method Blank Total Recoverable



Water 6010B 223813280-54917-1 SV-01 - SV-10 Total/NA

Water 6010B 223813280-54935-A-13-B MS Matrix Spike Total/NA

Water 6010B 223813280-54935-A-13-C MSD Matrix Spike Duplicate Total/NA

Water 6010B 223813LCS 280-223813/2-A Lab Control Sample Total/NA

Water 6010B 223813LCSD 280-223813/3-A Lab Control Sample Dup Total/NA

Water 6010B 223813MB 280-223813/1-A Method Blank Total/NA

General Chemistry



Water 300.0280-54917-1 SV-01 - SV-10 Total/NA

Water 300.0280-54926-P-1 MSD Matrix Spike Duplicate Total/NA

Water 300.0280-54926-Q-1 MS Matrix Spike Total/NA

Water 300.0280-54926-R-1 DU Duplicate Total/NA

Water 300.0LCS 280-223698/4 Lab Control Sample Total/NA

Water 300.0LCSD 280-223698/5 Lab Control Sample Dup Total/NA

Water 300.0MB 280-223698/6 Method Blank Total/NA

Water 300.0MRL 280-223698/3 Lab Control Sample Total/NA




Water 300.0280-54926-P-1 MSD Matrix Spike Duplicate Total/NA

Water 300.0280-54926-Q-1 MS Matrix Spike Total/NA

TestAmerica Denver

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Analysis Batch: 223699 (Continued)


Water 300.0280-54926-R-1 DU Duplicate Total/NA




Water 300.0MRL 280-223699/3 Lab Control Sample Total/NA



Water SM5210B280-54917-1 SV-01 - SV-10 Total/NA

Water SM5210B280-54917-1 DU SV-01 - SV-10 Total/NA

Water SM5210BLCS 280-223818/4 Lab Control Sample Total/NA

Water SM5210BLCSD 280-223818/5 Lab Control Sample Dup Total/NA

Water SM5210BMB 280-223818/6 Method Blank Total/NA



Water SM 2540D280-54917-1 SV-01 - SV-10 Total/NA

Water SM 2540D280-54941-G-2 DU Duplicate Total/NA

Water SM 2540DLCS 280-223828/1 Lab Control Sample Total/NA

Water SM 2540DLCSD 280-223828/2 Lab Control Sample Dup Total/NA

Water SM 2540DMB 280-223828/3 Method Blank Total/NA



Water SM 2540C280-54917-1 SV-01 - SV-10 Total/NA

Water SM 2540C280-54917-1 DU SV-01 - SV-10 Total/NA

Water SM 2540CLCS 280-224006/2 Lab Control Sample Total/NA

Water SM 2540CLCSD 280-224006/3 Lab Control Sample Dup Total/NA

Water SM 2540CMB 280-224006/1 Method Blank Total/NA

Prep Batch: 224404


Water 365.2/365.3/365280-54917-1 SV-01 - SV-10 Total/NA

Water 365.2/365.3/365280-54917-1 MS SV-01 - SV-10 Total/NA

Water 365.2/365.3/365280-54917-1 MSD SV-01 - SV-10 Total/NA

Water 365.2/365.3/365LCS 280-224404/3-A Lab Control Sample Total/NA

Water 365.2/365.3/365LCSD 280-224404/4-A Lab Control Sample Dup Total/NA

Water 365.2/365.3/365MB 280-224404/5-A Method Blank Total/NA



Water 365.1 224404280-54917-1 SV-01 - SV-10 Total/NA

Water 365.1 224404280-54917-1 SV-01 - SV-10 Total/NA

Water 365.1 224404280-54917-1 MS SV-01 - SV-10 Total/NA

Water 365.1 224404280-54917-1 MS SV-01 - SV-10 Total/NA

Water 365.1 224404280-54917-1 MSD SV-01 - SV-10 Total/NA

Water 365.1 224404280-54917-1 MSD SV-01 - SV-10 Total/NA

Water 365.1 224404LCS 280-224404/3-A Lab Control Sample Total/NA

Water 365.1 224404LCS 280-224404/3-A Lab Control Sample Total/NA

Water 365.1 224404LCSD 280-224404/4-A Lab Control Sample Dup Total/NA

Water 365.1 224404LCSD 280-224404/4-A Lab Control Sample Dup Total/NA

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Analysis Batch: 224839 (Continued)


Water 365.1 224404MB 280-224404/5-A Method Blank Total/NA

Water 365.1 224404MB 280-224404/5-A Method Blank Total/NA



Water 410.4280-54800-B-8 MS Matrix Spike Total/NA

Water 410.4280-54800-B-8 MSD Matrix Spike Duplicate Total/NA





Prep Batch: 225584


Water 1664A280-54917-1 SV-01 - SV-10 Total/NA

Water 1664A280-54917-1 MS SV-01 - SV-10 Total/NA

Water 1664A280-54917-1 MSD SV-01 - SV-10 Total/NA

Water 1664ALCS 280-225584/2-A Lab Control Sample Total/NA

Water 1664ALCSD 280-225584/3-A Lab Control Sample Dup Total/NA

Water 1664AMB 280-225584/1-A Method Blank Total/NA



Water 1664A 225584280-54917-1 SV-01 - SV-10 Total/NA

Water 1664A 225584280-54917-1 MS SV-01 - SV-10 Total/NA

Water 1664A 225584280-54917-1 MSD SV-01 - SV-10 Total/NA

Water 1664A 225584LCS 280-225584/2-A Lab Control Sample Total/NA

Water 1664A 225584LCSD 280-225584/3-A Lab Control Sample Dup Total/NA

Water 1664A 225584MB 280-225584/1-A Method Blank Total/NA




Water 350.1280-55261-A-15 MS Matrix Spike Total/NA

Water 350.1280-55261-A-15 MSD Matrix Spike Duplicate Total/NA







TestAmerica Denver

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Lab ChronicleClient: Intel Corporation / eProcurement TestAmerica Job ID: 280-54917-1


Client Sample ID: SV-01 - SV-10 Lab Sample ID: 280-54917-1Matrix: WaterDate Collected: 04/30/14 09:00


Prep 3520C KEC05/05/14 07:57 TAL CAN129221

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 1040 mL 2.0 mL

Analysis 8270C 200 130216 05/12/14 16:45 JMG TAL CANTotal/NA 1040 mL 2.0 mL

Prep 3520C 129221 05/05/14 07:57 KEC TAL CANTotal/NA 1040 mL 2.0 mL

Analysis 8270C 400 130407 05/13/14 11:30 JMG TAL CANTotal/NA 1040 mL 2.0 mL

Analysis 8015C 1 328335 05/09/14 00:02 AJMC TAL SAVTotal/NA 1 mL 1 mL

Prep 3010A 223813 05/02/14 07:30 SEJ TAL DENTotal/NA 50 mL 50 mL

Analysis 6010B 1 225521 05/13/14 01:40 JKH TAL DENTotal/NA 50 mL 50 mL

Prep 3005A 223803 05/02/14 07:30 SEJ TAL DENTotal Recoverable 50 mL 50 mL

Analysis 6020 1 224168 05/02/14 17:42 LMT TAL DENTotal Recoverable 50 mL 50 mL

Prep 1664A 225584 05/13/14 14:56 CML TAL DENTotal/NA 991 mL 1000 mL

Analysis 1664A 1 225623 05/13/14 18:43 CML TAL DENTotal/NA 991 mL 1000 mL

Analysis 300.0 1 223698 05/01/14 20:16 TLP TAL DENTotal/NA 10 mL 10 mL

Analysis 300.0 1 223699 05/01/14 20:16 TLP TAL DENTotal/NA 10 mL 10 mL

Analysis 350.1 20 226205 05/15/14 16:54 AFH TAL DENTotal/NA 10 mL 10 mL

Prep 365.2/365.3/365 224404 05/06/14 09:57 AJS TAL DENTotal/NA 50 mL 50 mL

Analysis 365.1 10 224839 05/07/14 16:01 AJS TAL DENTotal/NA 50 mL 50 mL

Prep 365.2/365.3/365 224404 05/06/14 09:57 AJS TAL DENTotal/NA 50 mL 50 mL

Analysis 365.1 10 224839 05/07/14 16:10 AJS TAL DENTotal/NA 50 mL 50 mL

Analysis 410.4 10 225201 05/10/14 09:11 CCJ TAL DENTotal/NA 2 mL 2 mL

Analysis SM 2540C 1 224006 05/02/14 12:40 CML TAL DENTotal/NA 50 mL 100 mL

Analysis SM 2540D 1 223828 05/02/14 16:50 MW1 TAL DENTotal/NA 250 mL 250 mL

Analysis SM5210B 1 223818 05/01/14 16:51 MRB TAL DENTotal/NA 300 mL

Client Sample ID: TRIP BLANK Lab Sample ID: 280-54917-8Matrix: WaterDate Collected: 04/30/14 00:00


Analysis 8260B MRM05/13/14 16:361 TAL DEN225443

Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 20 mL 20 mL

Client Sample ID: COMPOSITE (SV-11 - SV-16) Lab Sample ID: 280-54917-9Matrix: WaterDate Collected: 04/30/14 00:00


Analysis 8260B ADD05/14/14 00:481 TAL DEN225628

Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 2 mL 20 mL

Laboratory References:

TAL CAN = TestAmerica Canton, 4101 Shuffel Street NW, North Canton, OH 44720, TEL (330)497-9396

TAL DEN = TestAmerica Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL (303)736-0100

TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858

TestAmerica Denver

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Login Sample Receipt Checklist

Client: Intel Corporation / eProcurement Job Number: 280-54917-1

Login Number: 54917

Question Answer Comment

Creator: Knauf, James R

List Source: TestAmerica Denver

List Number: 1

TrueRadioactivity wasn't checked or is </= background as measured by a survey

meter.

TrueThe cooler's custody seal, if present, is intact.

TrueSample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or

tampered with.

TrueSamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time.

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

N/ASample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested

MS/MSDs

TrueContainers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.


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Login Sample Receipt Checklist

Client: Intel Corporation / eProcurement Job Number: 280-54917-1

Login Number: 54917

Question Answer Comment

Creator: West, Lauren H

List Source: TestAmerica Savannah

List Creation: 05/02/14 09:12 AMList Number: 681

N/ARadioactivity wasn't checked or is </= background as measured by a survey

meter.

TrueThe cooler's custody seal, if present, is intact.

TrueSample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or

tampered with.

TrueSamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

N/AIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time.

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

N/ASample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested

MS/MSDs

TrueContainers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.


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