CRYOGEN-FREE MAGNETS FOR SOLID STATE NMR · CRYOGEN-FREE MAGNETS FOR SOLID STATE NMR ... Z2, X, Y,...

4
www.cryogenic.co.uk CRYOGEN-FREE NMR PRODUCTS CRYOGEN-FREE MAGNETS FOR SOLID STATE NMR 500 MHz and 600 MHz wide bore products Special bore sizes available on request Variable temperature inserts down to 2 K Superconducting sweep coils Custom magnets tailored to DNP CF 600 MHz wide bore installed in Université Paris-Sud XI 2009 (*) 17 O-NMR spectrum of Cu 3 Zn(OH) 6 Cl 2 collected by sweeping main magnetic field over 6000 G about 12.9 T (*) As-NMR spectrum of Sr 2 VO 3 FeAs pnictide at room temperature in magnetic field of 13 T. (*) (*)courtesy Prof. P. Mendels and Dr. H. Alloul, Université Paris-Sud XI

Transcript of CRYOGEN-FREE MAGNETS FOR SOLID STATE NMR · CRYOGEN-FREE MAGNETS FOR SOLID STATE NMR ... Z2, X, Y,...

Page 1: CRYOGEN-FREE MAGNETS FOR SOLID STATE NMR · CRYOGEN-FREE MAGNETS FOR SOLID STATE NMR ... Z2, X, Y, C2, S2, ZX, ZY Z1, Z2, X, Y, C2, S2, ZX, ZY ... Compressor Water cooled, 3 phase

www.cryogenic.co.uk

CRYOGEN-FREE NMR PRODUCTS

CRYOGEN-FREE MAGNETS FOR SOLID STATE NMR

500 MHz and 600 MHz wide bore products

Special bore sizes available on request

Variable temperature inserts down to 2 K

Superconducting sweep coils

Custom magnets tailored to DNP

CF 600 MHz wide bore installed in Université Paris-Sud XI 2009 (*)

17O-NMR spectrum of Cu3Zn(OH)6Cl2 collected by sweeping main magnetic field over 6000 G about 12.9 T (*)

As-NMR spectrum of Sr2VO3FeAs pnictide at room temperature in magnetic field of 13 T. (*)

(*)courtesy Prof. P. Mendels and Dr. H. Alloul, Université Paris-Sud XI

Page 2: CRYOGEN-FREE MAGNETS FOR SOLID STATE NMR · CRYOGEN-FREE MAGNETS FOR SOLID STATE NMR ... Z2, X, Y, C2, S2, ZX, ZY Z1, Z2, X, Y, C2, S2, ZX, ZY ... Compressor Water cooled, 3 phase

CRYOGEN-FREE NMR PRODUCTS

CRYOGEN-FREE MAGNETS FOR SOLID STATE NMR

(*) Homogeneity measured by plotting field over 1 cm long x 1 cm diameter cylinder and specified assuming cryo-shims and room temperature shim settings have been optimized.

Technical Specifications

Product CF 600/89 AS CF 500/89 AS

Field strength 600 MHz (14.1T) 500 MHz (11.7T)

Homogeneity (*)

<0.1 ppm <0.1 ppm

Cryo-shims Z1, Z2, X, Y, C2, S2, ZX, ZY Z1, Z2, X, Y, C2, S2, ZX, ZY

Drift 0.1 ppm/hr 0.1 ppm/hr

Room Temperature bore

89 mm 89 mm

Field sweep -14.1 to 14.1 T - 11.7 to 11.7 T

Cryocooler 1.5 W pulse tube 1.5 W pulse tube

Compressor Water cooled, 3 phase power

Water cooled, 3 phase power

Cooldown time 48 hours 36 hours

www.cryogenic.co.uk

Cryogenic Limited

Unit 30

Acton Park Industrial Estate

London W3 7QE

United Kingdom

Tel: +44 (0)20 8743 6049

Email: [email protected]

www.cryogenic.co.uk

No cryogenic experience required

Turn-key operation

Overnight cool-down

Low cost of ownership

Minimal maintenance

Minimal quench hazards

Key Benefits of Cryogen-Free Technology

Leaving you to focus on the science

Page 3: CRYOGEN-FREE MAGNETS FOR SOLID STATE NMR · CRYOGEN-FREE MAGNETS FOR SOLID STATE NMR ... Z2, X, Y, C2, S2, ZX, ZY Z1, Z2, X, Y, C2, S2, ZX, ZY ... Compressor Water cooled, 3 phase

www.cryogenic.co.uk

CRYOGEN-FREE NMR PRODUCTS

CRYOGEN-FREE DESK-TOP NMR SYSTEMS

300 MHz and 400 MHz desk-top products

Variable temperature inserts

Superconducting sweep coils

Cryo-coolers with air-cooled compressors which run off single phase mains

Product features

Compact 7 T and 9.4 T cryogen-free magnets

NMR-grade homogeneity provided by cryo-shims and room temperature shims

NMR-grade drift

LabVIEW® based temperature diagnostics

Magritek Kea2 spectrometer with direct digital transmission & detection

Optional high stability oven-controlled oscillator for spectrometer

ProspaNMRsoftwarewithuser-configurable pulse programmer

The photograph shows an early prototype while the drawing illustrates our new product design

Page 4: CRYOGEN-FREE MAGNETS FOR SOLID STATE NMR · CRYOGEN-FREE MAGNETS FOR SOLID STATE NMR ... Z2, X, Y, C2, S2, ZX, ZY Z1, Z2, X, Y, C2, S2, ZX, ZY ... Compressor Water cooled, 3 phase

www.cryogenic.co.uk

CRYOGEN-FREE NMR PRODUCTS

CRYOGEN-FREE DESK-TOP NMR SYSTEMS

(*) Homogeneity measured by plottingfieldover1 cmlongx1cmdiametercylinderandspecifiedassuming cryo-shims and room temperature shim settings have been optimized.

Technical Specifications

Product CF 300/52 CF 400/52

Field strength 300 MHz (7T) 400 MHz (9.4T)

Homogeneity (*)

<0.1ppm <0.1ppm

Cryo-shims Z1,Z2,X,Y,C2,S2,ZX,ZY Z1,Z2,X,Y,C2,S2,ZX,ZY

Drift 0.1ppm/hr 0.1ppm/hr

Room Temperature Bore

52 mm 52 mm

Field sweep -7 to +7 T -9.4 to +9.4 T

Cryocooler 100mWGM 250 mW pulse tube

Compressor Air-cooled,singlephase Air-cooled,singlephase

Cooldown time Overnight Overnight

Cryogenic Limited

Unit 30

Acton Park Industrial Estate

London W3 7QE

United Kingdom

Tel: +44 (0)20 8743 6049

Email: [email protected]

www.cryogenic.co.uk

No cryogenic experience required

Turn-key operation

Overnight cool-down

Low cost of ownership

Minimal maintenance

Minimal quench hazards

Key Benefits of Cryogen-Free Technology

Leaving you to focus on the science