Atmos Lab's Eliquid Analysis 10/2012 GR

Atmos L

ab

Finest Gree

k Eliquids

ITANEITIL.THMIO KPHTHL. TMHMA IATPIKHI:

UNIVERSI1Y OF CRETE MEDICAL SCHOOL

T.e. 2208 HpciKAuo Kpirtq P.O.Box 2208 Heraklion Crete, Greece

EPfA~1'8PIO TO!UCOAOfiAt Llu:uOuv-rl]<;: KaOTJYll-riJ<; ApLa-rEt6T)<; M. Taa-raaKT)<;

Tel +30 2810 394870, Fax +30 2810 542098 e-mail: [email protected] http://ctoxres.med.uoc.qr

Epyam:~plO - nl.r1Po¢oplE<; : 2810 394687 - 394681 - 394794, Fax: +30 281 0 39 46 88

IHETOTIOIHTIKO ANAAY:EH:E* KAI TASINOMH:EH:E TOY AIAAYMATO:E ANATIAHP!!:EH:E AGRINIO

ETAIPIA: ATMOS LAB EMDOPIKH ONOMAI:IA YTPOY ANAIIAHP!!l:Hl:: AGRINIO API@MOI: TIAPTIAAI:: 01/AGRINIO 112

TIOIOTIKOI: TIPOl:AIOPil:MOl: AIAA YMATOI: ANATIAHP!!l:Hl: E<DAPMOZOMENH ANAAYTIKH TEXNIKH: A£ptoc; XpcoJlaToypacpia-<DacrJlaTOJlcTpia Masac; (Gas Chromatography -Mass Spectrometry) Kat ··vypi] XpcoJlawypacpia-<DacrJlUTOJlcTpia Masac; (Liquid Chromatography-Mass Spectrometry)

TIOI:OTIKOI: TIPOI:AIOPII:MOI: MEXPI TIOI:Ol:TOY 99,9997%

ATIOTEAEI:MAT A TiivaKac; 1.

Opw llo<JOTtKoiJ

0\l<Jl(l llo<JO<JTO llpo<J()wpt<f!lOil (%w/v) Mt9o()o1.l (LOQ)

( m)

propylene glycol 3,21 0,198

glycerol 83,59 I ,187

water 11,6997

nicotine 1,5 0,1

l:i>vol..o 99,9997

Acv mstVOJlf:lLClt

Acv mstVOJlf:lLat

Oscia wstKo•11m 1 oscia wstKO'tTJm 3

Xp6vta LOStKOLTJTU 2 cr£ uop6~taUS opyavtcrJlOUS

• To Epyacrn']pw To~tKoA.oyiac; q>EpEt mcrronoiT]<YTJ crU!lq>wva llE to ISO: 17025 yta nc; 8tabtKao-iEc; napaA.ap~c;. 8taxEiptcrT]c;, Kamypa<p~c; Kat apxEw9tTTJ<rTJc; twv bEtY!l6.twv Kat AEttoupyEi llE 8taKptPwlltvEc; crucrKEutc; Kat 6pyava. •• H opyavoA.oyia LC-MS q>EpEt btaKpipwcr'l Kat&. ISO: 17025 llE nEbio Eq>apllOY~c; tT]V aviXVEU<YTJ vapKwnKv oucrtffiv crtTJV tpixa.

Atmos L

ab

Finest Gree

k Eliquids

TASINOMH!:H TOY YrPOY ANAITAHP!11:H1: AGRINIO

Ms ~acrrt trtv AXL 265/2002, <DEK 1214/B' /19.9.2002, trtv ra~tv61J.rtcrrt tcov !J.c!J.OVco!J.EVcov auatanKffiv tou !J.dy!J.atO<; Kat ~acrrt tou Kavovtcr!J.OU 1272/2008 (EK) to AGRINIO (Apt81J.6<; I1aptioa<;: 01/AGRINI0/12) IJ.c 99,9997% O"Ucrtacrrt nou ava<ptpstat crtov I1ivaKa 1, ta~tvO!J.chat co<; !lll smKivouvo yta trtv av8pffimvrt uyda, yta to nspt~aA.A.ov Kat !J.c ~acrrt n<; <pUatKOXll!J.tKE<; tou t8t6trtt£<;. Emnp6a8sta, yta trt XPTt<Jrt tou otaA.u~J.atO<; avanA.ftpcocrrt<; an6 tO rtA£KtpovtK6 tcrtyapo, to !J.ctY!J.U £tcrnvs61J.CVCOV at!J.WV nou ansA.su8spffivstat XP£ta~£tat ta~tv61J.rtcrrt AUIJ.~avovta<; un' 6\j/rt trtv £Katocrnaia aucrtacrrt tcov at!J.WV nou napayovtat !J.c trtV svspyonoirtcrrt tou !lllXUVta!J.OU Ut!J.07tOtrt<Jll<; !J.EXPt 7tcptcKTIKOtrtta<; 0.1 o/o ~~~ 0"£ IJ.c!J.OVCOIJ.EVO <JUO"taTIKO, Ka8ffi<; Kat t1l auyKcKpt!J.EYll XPTt<Jll autffiv.

ANIXNEY!:H NITPOZAMINQN !:TO AIAA YMA ANAllAHP!11:H1:

EAPMOZOMENH ANAA YTIKH TEXNIKH ··: Yypf] XpcoJ.la'toypa<pia-<l>acrJ.lU'tOJ.lE'tpia Masac; (Liquid

Chromatography -Mass Spectrometry)

ANIXNEYOMENE!: OY!:IE!:

To OtaAUIJ.U avanA.ftpcocrrt<; AGRINIO (Apt81J.6<; I1aptioa<;:Ol/AGRINIO 112) c~ctacr8rtK£ yta trtv

avi:x;veucrrt -rcov napaKa-rco vnpo~a!J.tvffiv, ITivaKa<; 2.

IIivaKaS 2.

4-(Methylnitrosamino )-1-(3-pyridyl)-1-butanol 4'-(nitrosomethylarnino )-1-(3-pyridyl)-1-butanone N-nitrosoanatabine

N-nitrosoanabasine

AllOTEAE!:MATA

(ppm)

ND*

ND ND ND

'Opw lloO'O'TlKOU llpoo-(hoptO'f.10U ME06()ol) (LOQ)

(ppm)

0,01

0,01 0,05 0,01

ANIXNEY!:H llOA YKYKAIKQN AP!!MATIKQN Y APOrONAN0PAKQN !:TO

AIAA YMA ANAllAHP!11:H1:

EAPMOZOMENH ANAA YTIKH TEXNIKH : A£pta XpffiJ.lU'toypa<pia- <l>acrJ.lU'tOJ.lE'tpia Masac; (Gas


Atmos L

ab

Finest Gree

k Eliquids

ANIXNEYOMENE1: OY1:IE1:

To 8u:iA.ufla avanA.i)procrT]<; AGRINIO (Apt8f.l6<; f1ap-ri8a<;:O 11 AGRINI0/12) E~E-racr8T]KE yta 'tT]Y

aviX,VEUO"TJ -rrov napaKa-rro noA.uKUKAtKrov aprof.!anKrov u8poyovav8paKrov (PAHs), ITivaKa<; 3.

llivaKaS 3.

acenaphtylene fluorene

phenanthrene

anthracene pyrene

benzo(a)anthracene

chrysene benzo(k)fluoranthene benzo(b )fluoranthene benzo(g,h,i)perylene

di benzo( a,h )anthracene indeno( 1 ,2,3-CD)pyrene

AllOTEAE1:MATA

Opto lloao-rtKoil 1: uyKtv-r pro mt llpoa~wptaJ.a.oil MtOo~ou

(LOQ) (ppm) (ppm)

ND* 0,005

ND 0,010

ND 0,005

ND 0,006

ND 0,003 ND 0,003

ND 0,003

ND 0,060

ND 0,006

ND 0,014

ND 0,021

ND 0,022

*NO: ~£V UVt:XV£U811KUV 1tOAUKUKAtKOt apCOf..l.U'ttKOt u8poyovav8paK£<; O"Uf..l.q>COVU f..l.£ TU ava<p£p0f..1.£VU 6pta aviXV£U<J11<;·

Ka91JY'lnl~ To!;tKoJ..oyia~ laTfHKou TJ.lt}JlaToc;

Aum9uvn\<; Epya<rt"flpiou la-rpoou~a<t'ttKrov EnLGTlJJlrov & Movaoac; To;tKol..oyia:;

Atmos L

ab

Finest Gree

k Eliquids

ITANEITIL.THMI 0 KPHTHL. TMHMA IATPIKHL.


T.e. 2208 HpaKAuo Kpirtq P.O.Box 2208 Heraklion Crete, Greece

EPI'AJ:TRPtO TO!lKOAOflAJ: Llu:u0uvn1<;: KaOT)ytr~i]<; ApuJT£L6T)<; M. TaaTaUKT)<;

-.. Tel +30 2810 394870, Fax +30 2810 542098 e-mail: [email protected] http://ctoxres.med.uoc.qr Epyacrr~plO - nl.f1po¢oplE<; : 2810 394687- 394681 - 394794, Fax: +30 281 0 39 46 88

IIIETOIIOIHTIKO ANAAYEHI:* KAI TASINOMHI:HI: TOY AIAAYMATOI: ANAIIAHPQI:HI:APACHE

ETAIPIA: ATMOS LAB EMTIOPIKH ONOMA!:IA YrPOY ANATIAHP!l!:H!:: APACHE API0MO!: TIAPTIAA!:: 011 APACHE /12

TIOIOTIKO!: TIPO!:AIOPI!:MO!: AIAAYMATO!: ANATIAHP!l!:H!: E<l>APMOZOMENH ANAA YTIKH TEXNIKH: A£pta<; Xpcu)la:roypa.<pia-<l>a.cr)la.'toJ..I£-rpia. Mat;;a.<; (Gas Chromatography -Mass Spectrometry) Kat **Yypij Xpcu~ta.-roypa.<pia.-<l>a.cr)lU'tOJlC'tpia Mat;;a.<; (Liquid Chromatography-Mass Spectrometry)

IIO!:OTIKO!: TIPO!:AIOPI!:MO!: MEXPI TIO!:O!:TOY 99,9944%

ATIOTEAE!:MAT A IlivaKa<; 1.

'Opto Jioo-O'TlKOU

Ovo-ia Iloo-oo-'TO Ilpoaatopto-Jlou (%w/v) MtOoaov (LOQ)

( m)


glycerol 84,93 1,187

water 9,7144

nicotine 1,3 0,1

!:uvoJ.o 99,9944

~£v 'tUStVOf.1£ha.t

~£V 'tUStVOJlChUt

Ostia. -rostK6'tlJm I Ostia. wstK6-rlJm 3

Xp6vta. 'tOStKO'tTJ'tU 2 cr£ uop6~taUS opya.vtcr)lOUS

• To Epyacr1~pto To~tKoA.oyiac; <pl':pct mcrwnoi'l<Hl crUfl<pWva flc 10 ISO: 17025 yta nc; 8ta8tKacricc; napaA.a~~c;. 8ta;tcipta'lc;, Kamypa<p~c; Kat apxct08ET'lCJ'lc; 1wv 8ctyfllhwv Kat A.ctToupyci flc 8taKpt~WflEvcc; crucrKcuf:c; Kat 6pyava. •• H opyavoA.oyia LC-MS <pf:pct 8taKpi~WCJ'l KaTa ISO: 17025 flE 7tc8io c<papfloy~c; T'lV avi;x:vcucr'l vapKwnKwv oucrtwv cr1'lv 1pixa.

Atmos L

ab

Finest Gree

k Eliquids

TASINOMH:EH TOY YrPOY ANAllAHP!!:EH:E APACHE

ME pacrYJ TllY AXE 265/2002, <DEK 1214/B'/19.9.2002, TllY -ca~tv6J..LTJO"TJ To.w J..LEJ..LovroJ..Ltvrov crucrTanKmv Tou J.!EtYJ..lUToc; Kat pacrYJ wu KavovtcrJ..LOU 1272/2008 (EK) TO APACHE (Apt8J..L6c; llapTi8ac;: 01/APACHE/12) J..l€ 99,9944% O"UO""CUO"TJ7WU avaq>EpETUl O"TOV llivaKa 1, TU~tVOJ..lELTUl roc; J..lll EmKiv8uvo yta TTJY av8pmmv11 uyda, yta To 7tEptPaA.A.ov Kat J.!E pacrYJ Tt<; cpumKOXTJJ..ltKE<; Tou t8t6TTJTE<;. Em7tp6cr8ETa, yta TTJ XPTJO"TJ Tou 8taAUJ..lUTO<; ava7tA.ijprocrYJc; a1t6 TO TJAEKTpovtK6 Tcrtyapo, w J..lEtYJ..la Etcr1tYEOJ..lEVrov aTJ..lmv 1tou a7tEA.Eu8EpmvETm XPEtasETm Ta~tvOJ..lTJO"TJ A.aJ..lPavovmc; u1t' 0\j/TJ TllY EKUTOO"Ttaia crUO""CUO"TJ TCDV UTJ..lWV 1tOU 7tapayOVTUl J..l€ TllV EYEpyo7tOlTJO"TJ TOU J..lTJXUYlO"J..lOU aTJ..lo1toiYJcrTJc; J..lEXPt 1tEptEKnK6TYJTac; 0.1% p;p crE J..LEJ..lovroJ..ltvo crucrTanK6, Ka8mc; Kat TTJ <ruyKEKplJ..lEVTJ XPTJO"TJ UUTWV.

ANIXNEY:EH NITPOZAMIN!!N :ETO AIAA YMA ANAllAHP!!:EH:E

EAPMOZOMENH ANAAYTIKH TEXNIKH ** : Yyp'i) Xprof..t.a-toypacpia-<l>acrJlaTOJlt-rpia Masac; (Liquid


ANIXNEYOMENE:E OY:EIE1:

To 8taAUJ..lU ava7tA.ijprocrYJ<; APACHE (Apt8J..L6<; llapTi8ac;:Ol/APACHE/12) E~ETacr8YJKE yta TTJV

avixvwcrYJ Trov 7tapaKaTro vnposaJ..ltvmv, llivaKac; 2.

TiivaKas 2.

AKpO>VUf.llO

4-(Methylnitrosamino )-1-(3-pyridyl)-1-butanol 4'-(nitrosomethylamino )-1-(3-pyridyl)-1-butanone

N -nitrosoanatabine

N -nitrosoanabasine

AllOTEAE1:MA T A

(ppm)

ND*

ND ND ND

'Opw lloO'O'TlKOU llpoO"(hoptO'f.lOU Mt96oou (LOQ)

(ppm)

0,01

0,01 0,05 0,01

ANIXNEY1:H llOAYKYKAIK!!N AP!!MATIK!!N YAPOrONAN0PAK!!N 1:TO

AIAA YMA ANAllAHP!!1:H1:

EAPMOZOMENH ANAA YTIKH TEXNIKH : A£pta XproJlawypacpia- <l>acrJlUWfltTpia Masac; (Gas


Atmos L

ab

Finest Gree

k Eliquids

ANIXNEYOMENKE OYEIKE

To 8uiAUJ.!a avanA.flprocrllc; APACHE (Apt8J.!6c; ITap·ri8ac;:01/APACHEI12) c~c-r6.cr811K£ yta 't'llV

avi:x;vcucr11 -rrov napaK6.-rro noA.uKUKAtKffiv aproJ.!attKffiv u8poyovav8p6.Krov (PAHs ), ITivaKac; 3.

llivaKClS 3.

AKprovi>Jno


phenanthrene anthracene

pyrene benzo(a)anthracene


dibenzo( a,h )anthracene indeno( 1 ,2,3-CD)pyrene

AUOTEAEI:.MATA

Dpw UoaonKoi> I:.uyKEVTpro<Jll UpoaowptaJ.loi> MEOooou

(LOQ) (ppm) (ppm)

ND* 0,005 ND 0,010 ND 0,005 ND 0,006 ND 0,003 ND 0,003 ND 0,003 ND 0,060 ND 0,006 ND 0,014 ND 0,021 ND 0,022

*ND: Do£V ClVlXV£U9TJKUV 7tOAUKUKAlKOt apffiJ..LU'tlKOt UOpoyovav9paK£t; O'UJ..L<pffiVU J..LE '!U UVU<pEpOJ..LEVU 6pta UVtXVEUO'TJt;.

/ AptoT£1.0'1<;; M. TonToaKtls ·-- --~ MSc (Org Chern), PhD (Chern), DSc (Bioi), ERT (Eur Registered Toxicologist)

KaO'I"f'ITtl<;; T ol;tKol.oyiac; laTplKou TJltlJUIToc;

daEU9-u\"t'i)<;; EpyaO'TT)piou laTpOOLKa<ntKcilv Ento't"'lf.lOlV & Movaoac; Tol;tKol..oyiac;

Atmos L

ab

Finest Gree

k Eliquids

ITANEITIL.THMIO KPHTHL. TMHMA IATPIKHZ:


T.9. 2208 HptiKA&to Kpq1:q P.O.Box 2208 Heraklion Crete, Greece

EPtAt1'8PIQ TO!IKOAOfiAt 4u:u0uvu1<;: KaOT)YTlTTt<; ApLaTt:t6T)<; M. Taa-rartKT)<;

Tel +30 2810 394870, Fax +30 2810 542098 e-mail: [email protected] http://ctoxres.med.uoc.qr Epyam~plo - nAr)pocpoplE<;: 2810 394687 - 394681 - 394794, Fax: +30 281 0 39 46 88

1111:TOIIOIHTIKO ANAA Y1:H1:* KAI T ASINOMH1:H1: TOY AIAA YMAT01: ANAIIAHPQ1:H1:BARBARA

ETAIPIA: ATMOS LAB EMDOPIKH ONOMAI:IA YrPOY ANAllAHP!li:HI:: BARBARA API0MOI: llAPTIAAI:: 01/BARBARA /12

llOIOTIKOI: llPOI:AIOPII:MOI: AIAA YMA TO I: ANADAHPQI:HI: E<DAPMOZOMENH ANAA YTIKH TEXNIKH: AEpto<; Xpw)lawypa<pia-<Dacr)laTO)lE-rpia Masas (Gas Chromatography -Mass Spectrometry) Kat **Yypf] Xpw)lawypa<pia-<Dacr)laTO~tE-rpia Masas (Liquid Chromatography-Mass Spectrometry)

DOI:OTIKOI: llPOI:AIOPII:MOI: MEXPI llOI:OI:TOY 99,9976%

AllOTEAEI:MA T A llivaKa~ 1.

'Opto IIOGO'TlKOU

Ou«Jia Ilo«JOGTO IlpoGcltoplGJ.lOU (%w/v) MtOoclo\l (LOQ)

( m)



water 15,0376

nicotine 1,1 0,1

I:ilvolo 99,9976

DoEV 'tUSlVO)lEhat

DoEV 'tUSlVO)lEt'tal

OsEia -rostK6-rqm t OsEia wstK6TIJm 3

Xp6vta -rostKOTTJTU 2 crE u8p6~tou<; opyavtcr)lOUS

*To Epyac:n~pto Tol;tKoA.oyiw; q>£p~::tmcrwrroilJc:H] c:rUJlq>wva JlE TO ISO: 17025 yta n<; iltailtmcriE<; rrapaA.a~~ <;. iltaxEiptcrTJ<;, Kamypaq>~<; Kat apx~::to9£TTJGTJS Twv il~::tyJlc:iTwv Kat A.~::noupy~::i JlE iltaKpt~WJlEvE<; crucrKEu£<; Kat 6pyava. ** H opyavoA.oyia LC-MS q>£pEt btaKpi~WO"TJ KaTa ISO: 17025 JlE rr~::ilio Eq>apJlOY~S TTJV avixv~::ucrlJ vapKwnKcilV oucrt<Ov O"TTJV Tpixa.

Atmos L

ab

Finest Gree

k Eliquids

T AEINOMH:EH TOY YrPOY ANAIIAHP!l:EH:E BARBARA

Me ~acrT] tT]Y AXI: 265/2002, EK 1214/B'/19.9.2002, 'tTJY ta~tvO!J.TJO"T] tcov !J.c!J.OYCO!J.EVCOV crucrtanKrov 'tOU !J.clY!J.UtOc; Kat ~acr11 'tOU KavovtO"!J.OU 1272/2008 (EK) 'tO BARBARA (Apt8!J.6c; I1apti8ac;: 01/BARBARA/12) !J.c 99,9976% crucrtaO"T] nou ava<pEpctat O"'tOV IlivaKa 1, ta~tvO!J.chat coc; llll cmKiv8uvo yta 'tT]V av8promvT] uyda, yta to ncpt~aA.A.ov Kat !J.c ~acrT] nc; qmcrtKOXT]!J.tKEc; wu t8t6tT]tcc;. Emnp6cr8cta, yta 'tTJ XPllO"TJ tou 8taA.u~J.atoc; avanA.ijpcocrT]c; an6 to T]AcKtpovtK6 tmyapo, to !J.ctY!la ctcrnvc6~J.cvcov at~J.rov nou ancA.cu8cprovcmt XPctasctat m~tYO!J.TJO"TJ A.a11~avovmc; un' 0\j/T] 'tT]Y cKU'tOO"'ttaia O"UO"'tUO"T] 'tCOV U't!J.cDY 1tOU napayov'tat !J.c 'tT]V cVcpyonOiT]O"T] 'tOU !J.T]XUVlO"!J.OU at~J.onoiT]crT]c; !J.EXPt ncptcKnK6'tT]tac; 0.1 % p;~ crc !J.c!J.OYCO!J.EVO crucrtanK6, Ka8roc; Kat 'tTJ cruyKcKpt!J.EYT] XPllO"TJ autrov.

ANIXNEY:EH NITPOZAMIN!!N :ETO AIAA YMA ANAIIAHP!l:EH:E

EAPMOZOMENH ANAA YTIKH TEXNIKH ** : YypfJ XpmllaToypaq>ia-<l>acr!la'tO!lc'tpia Mat;ac; (Liquid


ANIXNEYOMENE:E OY:EIE:E

To 8taA.u!J.a avanA.ijpcocrT]c; BARBARA (Apt8!J.6c; I1apti8ac;:Ol/BARBARA/12) c~ctacr8T]K£ yta 'tT]Y

avixvcucrTJ tcov napaKatco vt'tposa~J.tvffiv, IlivaKac; 2.

llivaKas 2.

4-(Methylnitrosamino )-1-(3-pyridyl)-1-butanol 4'-(nitrosomethylarnino )-1-(3-pyridyl)-1-butanone

N -nitrosoanatabine

N -ni trosoanabasine

AIIOTEAE:EMA T A

(ppm)

ND*

ND ND

ND

Dpw IIo(JOTlKOU llpo(JblOpt(Jf.lOU Mt06()ou (LOQ)

(ppm)

0,01

0,01 0,05 0,01

ANIXNEY:EH IIOA YKYKAIKQN AP!!MATIKQN YAPOrONAN0PAKQN :ETO

AIAA YMA ANAIIAHP!l:EH:E

EAPMOZOMENH ANAA YTIKH TEXNIKH : A£pta Xpm11amypacpia- <l>acr!la'to!lc'tpia Mai:;ac; (Gas


Atmos L

ab

Finest Gree

k Eliquids

To 8ui:AuJla avan:Aflpcocrllc; BARBARA (Apt8J.16c; Ilap-ri8ac;:Ol/BARBARA/12) £~£T<icr811K£ yta TllV

UVl:XV£U0"11 TCOV napaKUTCO 7rOAUKUKAlKcOV apCOflUTlKcOV u8poyovav8paKCOV (PAHs), IlivaKac; 3.

IlivaKaS 3.

acenaphty1ene

fluorene


pyrene benzo( a)anthracene

chrysene benzo(k)fluoranthene

benzo(b )fluoranthene benzo(g,h,i)pery1ene

di benzo( a,h )anthracene indeno( 1 ,2,3-CD )pyrene

AIIOTEAE:EMA T A

'Opto IIOGO'tlKOV I: 'UYKEVT piDGl} IlpoG(hoptGtto'6 Mt96oo'U

(LOQ)

(ppm) (ppm)

ND* 0,005 NO 0,010

NO 0,005

ND 0,006

ND 0,003

ND 0,003

ND 0,003

ND 0,060 ND 0,006 NO 0,014

ND 0,021

ND 0,022

*ND: L\~::v UVtXVEUEhjKUV 1tOAUKUKAtKOt apCO!lU'ttKOt u8poyovuv8paKEc; CJU!!<pffiVU !!€ "CU ava<p€p0!1€VU 6pta avixv~::ucrlJc; .

/ Apto-n:iora~ M. ToaToaKTI.; ·--. -- ____:_..-'

MSc (Org Chern), PhD (Chern), DSc (Bioi), ERT (Eur Registered Toxicologist)

Ka9lJY'lritc; To/;tKo#.oyiac; laTptKo\i TJLTII.laToc;;

l\u;u9l>\'Tl\c; Epya<J't'1lplol> la-rpolhKa«nlKrov EntoT1Wrov & Movaoac; T o;tKoA.oyiac;

Atmos L

ab

Finest Gree

k Eliquids

ITANEITI~THMIO KPHTH~ TMHMA IATPIKHL.


T.e. 2208 HpciKA£to Kpirtq P.O.Box 2208 Herak.lion Crete, Greece

EPfAt'tlliPIO TO!IKOAOflAt Llu:u0uv·n1«;: KaOlJYTinl«; ApuJT£L6T)«; M. Taa-raaKT)«;

Tel +30 2810 394870, Fax +30 2810 542098 e-mail: [email protected] http://ctoxres.med.uoc.qr Epyam~plO - nXr1Po¢oplE<;: 2810 394687 - 394681 - 394794, Fax: +30 281 0 39 46 88

IIIETOIIOIHTIKO ANAA Y~H~* KAI T AEINOMH~H~ TOY AIAA YMATO~ ANAIIAHPQ~H~BEBECA

ET AlP lA: A TMOS LAB

EMTIOPIKH ONOMAl:IA YrPOY ANADAHP!!l:Hl:: BEBECA API0MOl: IIAPTIAAl:: OI/BEBECNI2

llOIOTIKOl: IIPOl:AIOPil:MOl: AIAA YMATOl: ANADAHP!!l:Hl: E<DAPMOZOMENH ANAA YTIKH TEXNIKH: Atptoc; Xpco).tmoypa.cpia.-<Da.crJ..La.TO~u::-rpia. Mal;a.c; (Gas Chromatography -Mass Spectrometry) Kat **Yypi] XpcoJ..La.-roypa.cpia.-<Da.crJ..LUTOJ..LcTpia. Mal;a.c; (Liquid Chromatography-Mass Spectrometry)

llOl:OTIKOl: IIPOl:AIOPil:MOl: MEXPI llOl:Ol:TOY 99,9992%

llivaKa~ 1.

Ouaia

methyl cyclopentenolone

ethyl maltol

ethyl vanillin

propylene glycol

glycerol

water

nicotine

l:i>voA.o

AllOTEAEl:MAT A

Iloaoa-ro (%w/v)

0,503

1,130

0,004

9,35

85,86

1,6522

1,5

99,9992

'Opto IloaonKou Ilpoaowptaf.lOU Mt960o'U (LOQ)

( m) 0,121

0,135

0,032

0,198

l , 187

0,1

Acv -ra.stvoJ..LEha.t

ostia. -rostKOTIJTU a.n:a cr-r6J..La.TOc;, Ka.TIJyopia. 4 ostia. -rostKOTIJTU a.n:o

cr-r6J..LaTO<;, Ka.TIJyopia. 4 Epc8tcrJ..LO<; bEpJ..LUTO<;,

Ka.TIJyopia. 2 Epc8tcrJ..L6c; ocp8a.A.J..Lffiv

Ka.TIJyopia. 2 Et8tKi] TOStKOTIJTU crta.

6pya.va.-cr-r6xouc; ccpan:a.s EK8c<rrJ Ka.nwopia. 3

Acv ta.StVOJ..LEha.t

Acv ta.StVOJ..Lcha.t

ostia. TOStKOTIJTU 1 ostia. -rostKOTIJ'tU 3

Xp6vta. TOStKOTIJta. 2 cr£ u8p6pwus opya.vtcrgous

Atmos L

ab

Finest Gree

k Eliquids

• To EpyacrT~pto To~tKoA.oyia~ q>EpEt mcrwn:oiTJOTJ <ril!J.q>mva IJ.E w ISO: 17025 yta n~ 8ta8tKacriE~ n:apaA.ap~~. 8taxEiptaTJ~, Kamypaq>~~ Kat apx~::to8ETTJO"TJ~ Tmv OEtYflUTffiV Kat A.~::twupy~::i flE 8taKptPmiJ.EvE~ crucrKru£~ Kat 6pyava. •• H opyavoA.oyia LC-MS q>£p~::t 8taKpipmcrTJ KaTa ISO: 17025 IJ.E n:~::8io Eq>Up!J.OY~~ TTJV avixvrucrTJ vapKmnKffiv oucrtffiv crTTJV Tpixa.

T AEINOMHl:H TOY YrPOY ANATIAHP!!l:Hl: BEBECA

ME ~UO'TJ TIJY AXL 265/2002, EK 1214/B'/19.9.2002, TIJV 'ta~tVOJ.!TJO'TJ 't(J)V J.!EJ.!OV(J)J.!EvffiV crucr-ranKffiv wu J.!El'YJ.ta-roc; Kat ~UO'TJ -rou KavovtcrJ.!OU 1272/2008 (EK) -ro BEBECA (Apt8J.t6c; ITap-ri8ac;: 01/BEBECA/12) J.!E 99,9992% O'Ucr-mcrTJ nou ava<pEpE-rat cr-rov ITivaKa 1, -ra~tVOJ.!Ehat ffic; !lll Emriv8uvo yta TIJY av8pffimVTJ uyda, yta -ro nEpt~aA.A.ov Kat J.!E ~acrll nc; <pumKOXTJJ.!tKEc; wu t8t6-rTJ-rEc;. Emnp6cr8na, yta Til XPllO'TJ -rou 8taA.uJ.tawc; avanA.flpfficrTJc; an6 w TJA.EK-rpovtK6 wtyapo, -ro J.!El'YJ.!a EtcrnvEOJ.!EVffiv a-rJ.tffiv nou anEA.Eu8EpffivE-mt XPEta~E-mt -ra~tVOJ.!TJO'TJ A.aJ.t~avov-mc; un' 0\j/TJ TIJY EKa-rocrnaia crUO''taO'TJ 'tffiV U'tJ.!WV 7tOU napayov-rat J.!E TIJV EVEpyonOtTJO'TJ 'tOU J.!TJXUVtO'J.!OU U'tJ.!07tOtTJO'TJc; J.!EXPt 7tEptEK'ttKOTIJ'tac; 0.1% W~ O'E J.!EJ.!OVffiJ.!EVO O'UO''ta'ttKO, Ka8ffic; Kat 'tll cruyKEKptJ.!EYTJ XPllO'TJ au-rffiv.

ANIXNEYl:H NITPOZAMIN!!N l:TO AIAA YMA ANATIAHP!!l:Hl:

EAPMOZOMENH ANAA YTIKH TEXNIKH ** : Yyp1l XpcoflaLOypa<pia-acrlla·ro!l£'tpia Masa<; (Liquid


ANIXNEYOMENEl: OYl:IEl:

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aviXVEUO'TJ -rffiv napaKa-rffi vnpo~aJ.ttvffiv, ITivaKac; 2.

llivaKaS 2.

AKproVUfltO


N-ni trosoanatabine

N -nitrosoanabasine

AllOTEAEl:MATA

(ppm)

ND*

ND ND ND

'Opto llo<JOTlKOU llpo<J~hopt<JflOU Mt9o&ou (LOQ)

(ppm)

0,01

0,01 0,05 0,01

*ND: ~£V UVtXV£U8rjKUV Vtrposa!ltV£<; crUfl<j>COVU !l£ 'tU ava<p£p0!-L£VU 6pta UVtXV£U<JT}<;.

ANIXNEYl:H llOAYKYKAIK!!N AP!!MATIK!!N YAPOrONAN0PAK!!N l:TO

AIAA YMA ANATIAHP!!l:Hl:

EAPMOZOMENH ANAA YTIKH TEXNIKH : Aepta Xpco!laLOypacpia- <l>acr!la'tO!l£-rpia Masa<; (Gas


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ab

Finest Gree

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To 8ui/..:uj.la avan/...i)proo-r1<; BEBECA (Apt8j.!6<; Tiap-ri8a<;:01/BEBECA/12) £~£Ta<J8'flKE yta T'flV

avi:XVEU<J'fl TCDV napaKaTro 7tOAUKUKAlKWV aproj.!UTlKWV u8poyovav8paKroV (PAHs), TiivaKa<; 3.

llivaKUS 3.

AKpOOVVfllO

acenaphtylene

fluorene

phenanthrene

anthracene

pyrene

benzo(a)anthracene

chrysene

benzo(k)fluoranthene

benzo(b )fl uoranthene

benzo(g,h,i)perylene

dibenzo(a,h)anthracene

indeno( 1 ,2,3-CD)pyrene

AIIOTEAE:EMA T A

Opto IloaonKoi> l: vyKEV'T proa11 Ilpoaowpt<YflOil ME90001>

(LOQ)

(ppm) (ppm)

ND* 0,005 ND 0,010

ND 0,005

ND 0,006 ND 0,003

ND 0,003 ND 0,003 ND 0,060 ND 0,006 ND 0,014 ND 0,021 ND 0,022

*ND: i1EV UVtXVEU811KUV 7tOAUKUKAtKOt aproj.!U'ttKOt Ubpoyovav8pa.KES <JUf,Hprova. j.!E 'tU a.va.<pEpOj.!EVU 6pta. a.VtXVEU<J'flS·

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Ka91JY'1nl<; To~lKoloyiac; luTplKOU TJLiiJ.laToc;

~u:-u9'll\"Ti)c; Epyu~pio'll luTpOOlKti~lKc:ilv EnLOTTJJHilv & Movaoac; To!;tKoA.oyiac;

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ITANEITIL:THMI 0 KPHTHL: TMHMA IATPIKHL.


T.e. 2208 Hpcuuuo Kpirtll P.O.Box 2208 Heraklion Crete, Greece

.IPrAtTHPIO TO!lKOAOr tAt Llu:u0uv·n1<;: KaOT)YTITTJ<; ApuJTt:L6T)<; M. TaaT<JUKT)<;

Tel +30 2810 394870, Fax +30 2810 542098 e-mail: [email protected] http://ctoxres.med.uoc.qr Epyam:~pto - nXr)po<j>oplE<;: 2810 394687 - 394681- 394794, Fax: +30 281 0 39 46 SlSl

IllETOIIOIHTIKO ANAA Yl:Hl:* KAI TASINOMHl:Hl: TOY AIAA ANAIIAHPfil:Hl:BEBECA18mg

ETAIPIA: ATMOS LAB

EMTIOPIKH ONOMAEIA YrPOY ANAITAHP!!EHE: BEBECA 18mg

API0MOE IIAPTIAAI:: 01/ BEBECA 18mg/12

IIOIOTIKOE IIPOEAIOPII:MOE AIAA YMATOI: ANAIIAHPQI:HI: EAPMOZOMENH ANAA YTIKH TEXNIKH: A£ptoc; Xpmlla·roypaq>ia-acrlla•o!l£'tpia Masac; (Gas Chromatography -Mass Spectrometry) Kat **YypfJ Xpmllawypaq>ia-acrlla•o!l£•pia Masac; (Liquid Chromatography-Mass Spectrometry)

IIOEOTIKOI: IIPOEAIOPIEMOI: MEXPI IIOI:OI:TOY 99,9999%

IltVIlKil 1.

0\l(Jl(l

propylene glycol

glycerol

ethyl vanillin

nicotine

Methyl cyclopentonolone

Ethyl maltol

water

EuvoA.o

AIIOTEAEI:MA T A

no(JO(JTO (o/ow/v)

2,73

93,15

0,006

1,6

0,525

1,152

0,8369

99,9999

OplO no(JOTLKOU npo(JOlOpt(Jf!OU Mseooou (LOQ)

( m)

0,198

1 '187

0,032

0,1

0,121

0,135

L'l£V 'tU~tVO!!EtLUt

L'l£V 'tU~tVO!l£tLUt

O~cia •o~tKO'tllLU, an:o cr•611a•oc;, Kanwopia 4 Ep£Eltcr!l6c; 'tOU 8£p!lU'tO<;

(Kanwopia 2) Ep£Eltcr!l6c; 'tffiV oq>ElaA.11ciw

(Kanwopia 2) EtOtKTj LO~tKOLll'tU am

6pyava cr•6xouc;-£q>an:a~ £KEl£crT) (Kanwopia 3) 0~£ia LO~tKO'tllLU 1 O~cia LO~tKOLll'tU 3

Xp6vta 'tO~tKOLllLU 2 cr£ uop6Ptous opyavtcr11ous

0~£ia LO~tKOLllLU, an:o cr•611a•oc;, Kanwopia 4

Atmos L

ab

Finest Gree

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· To Epyaar~pto To~tKoA.oyiac; <p£pst maronoirJO"ll mJflq>Wva flE ro ISO: 17025 yta nc; 8ta8tmaisc; napaA.ap~c;, 8taXEipwllc;, Karaypa<p~c; Kat apxsto8ET110"1lt; TWV 8EtyflCLTWV Kat AEtroupyd flE 8taKptPWJlEVEt; <JU<JKEUEt; Kat 6pyava. • H opyavoA.oyia LC-MS <p£pst 8taKpipwall Kara ISO: 17025 flE ns8io s<papfloy~c; r11v avixvrua11 vapKWnK<iw ouatv

ar11v rpixa.

TASINOMH:EH TOY YrPOY ANAIIAHPQ:EH:E BEBECA 18mg

M~:: ~acr11 'tllV AXI 265/2002, <DEK 1214/B'/19.9.2002, 'tllV 'ta~w6J..lllcrll 'trov J..lEJ..lOVroJ..l~rov crucr'tanKrov 'tOU J..lEtYJ..lU'toc; Kat ~acr11 'tou KavovtcrJ..lOU 1272/2008 (EK) 'tO BEBECA 18mg (Apt8f..l6c; Tiapn8ac;: 011 BEBECA 18mg/12) J..lE 99,9999% cri>cr'tacr11nou ava<p€pE'tat cr'tov TiivaKa 1, 'ta~tVOJ..lEhat roc; J..lll ~::mKiv8uvo yta 'tllV av8promv11 uy~::ia, yta 'to n~::pt~aA.A.ov Kat J..lE ~acr11 nc; qmcrtKOXllf..ltK€c; 'tOU t8t6'tll'tEc;. Enmp6cr8~::m, yta 'tll XPTJ<Jll wu 8taAUJ..lU'toc; avanA.iJprocrllc; an6 'tO TlAEK'tpOVtKO 'tcrtyapo, 'tO J..lElYJ..lU Et<J1tVEOJ..lEVffiV U'tJ..lcDV 7t0U U7tEAEU8EpcDVE'tat XPEtaSE'tat m~WOf..lll<Jll AUJ..l~avov'tac; un' O\j/11 'tllV EKa'tocrnaia cri>crmcr11 'trov U'tf..lcDV nou napayovmt J..lE 'tllV EVEpyonOlll<Jll 'tOU J..lllXUVt<Jf..lOU U'tf..l01t0tll<Jllc; J..lEXPt 1tEptEK'ttKO'tll'tUc; 0.1% ~~~ crE J..lEJ..lOVffiJ..lEVO <JU<J'tUTIKO, Ka8roc; Kat 'tll cruyKEKptf..lEVll XPTJ<Jll UU'tcDV.

ANIXNEY:EH NITPOZAMINQN :ETO AIAA YMA ANAIIAHPQ:EH:E

E<l>APMOZOMENH ANAA YTIKH TEXNIKH ··: Yypij XpCDflCLToypa<pia-<l>uaf.!CLLO~LE-rpia Mat;ac; (Liquid



To 8taAUJ..la avanA.iJprocrllc; BEBECA 18mg (Apt8f..l6c; Tiap'ti8ac;:Oll BEBECA 18mg/12) E~E'tacr811KE yta 'tllV avixvwcr11 'trov napaKa'tro vt-rposaJ..ltvrov, TiivaKac; 2.

llivaKUS 2.

AKpCOVUJllO

4-(Methylnitrosamino )-1-(3-pyridyl)-1-butanol 4'-(nitrosomethylamino )-1-(3-pyridyl)-1-butanone N-nitrosoanatabine N-nitrosoanabasine

AIIOTEAE:EMA T A

(ppm)

ND*

ND ND ND

Opw Iloao-rtKou Ilpoa&toplGJlOU ME06&ou (LOQ)

(ppm)

0,01

0,01 0,05 0,01

ANIXNEY:EH IIOA YKYKAIKQN APQMATIKQN YAPOrONAN0PAKQN :ETO

AIAA YMA ANAIIAHPQ:EH:E

2

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ab

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EAPMOZOMENH ANAA YTIKH TEXNIKH : A£ptu Xprof..tmoypu<piu- <l>ucrf..LU'Wf..I.£Tpiu Masuc; (Gas


ANIXNEYOMENEI: OYI:IEI: I

To 8uiA.uf..La avanA.T)pwcr11c; BEBECA 18mg(Apt8f.l6c; I1apTi8ac;:Oll BEBECA 18mg/12) E~ETacr811KE yta TllV UVtXVEUO"ll TWV napaKUTW 7tOAUKUKAtKWV apWf.lUTtKWV u8poyovav8paKWV (PAHs), I1i.vaKac; 3.

TiivaKas 3.

AKprovilt.tw

acenaphtylene

fluorene phenanthrene

anthracene pyrene

benzo(a)anthracene

chrysene benzo(k)fluoranthene

benzo(b )fluoranthene benzo(g,h,i)perylene


indeno( 1 ,2,3-CD )pyrene

AllOTEAEI:MATA

'Opw lloaonKoiJ I:uyKtv-rproo-11 llpoaowptat.toil MdMoou

(LOQ) (ppm) (ppm)

ND* 0,005 ND 0,010 ND 0,005 ND 0,006 ND 0,003

ND 0,003 ND 0,003 ND 0,060 ND 0,006 ND 0,014 NO 0,021 ND 0,022

*NO: f..ev UVtXV£U9l]KUV 1tOAUKUKAtKOt UpUlf..I.UTtKOt UOpoyovav9pUK£c; CJUf..l.<j>UlVU f.!£ TU UVU<p£p0f..1.£VU 6ptU uvixveucrl]c;.

3

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ab

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T.e. 2208 HpaKAuo Kpirtq


P.O.Box 2208 Heraklion Crete, Greece

DI:I:TODOIHTIKO ANAA Y:I:H:I: META ADO :I:YMDYKNQ:I:H* KAI T AEINOMH:I:H:I: EI:I:DNEOMENOY ATMOY DOY DPOKYDTEI ADO THN

ATMODOIH:I:H YrPOY ANADAHP!!:I:H:I: BEBECA 18mg

ETAIPIA: ATMOS LAB

EMTIOPIKH ONOMA~IA YrPOY ANAIIAHP.Q~H~: BEBECA 18mg

API0MO~ IIAPTIAA~: 01/ BEBECA 18mg /12

ITOIOTIKO~ IIPO~t.\IOPI~MO~ EI~NEOMENOY ATMOY MET A AllO ~YMTIHKN.Q~H E<DAPMOZOMENH ANAA YTIKH TEXNIKH: A£ptoc; Xpco)lamypa<pia-<Dacr)laTO)l£-rpia Mul;ac; (Gas Chromatography -Mass Spectrometry) Kat ··vypij Xpco)lamypa<pia-<Dacr)laTO)l£Tpia Mul;ac; (Liquid Chromatography-Mass Spectrometry)

llO~OTIKO~ IIPO~AIOPI~MO~ MEXPI ITO~O~TOY 99,97%

llivaKaS 1.

Ouo-ia

propylene glycol

glycerol

nicotine

Methyl cyclopentanolone

Ethyl vanillin

Ethyl maltol

water

~uvoJ...o

AITOTEAE~MAT A

noo-OO"TO (%w/v)

9,89

75,94

1,6

0,801

0,008

1,785

9,95

99,97

Opw noO"OTlKOU n poo-~hoptO"f.lOU Me961>ou (LOQ)

( m)

0,198

1,187

0,1

0,121

0,032

0,135

~£V TU~tvO)l£tTat

~£V TU~tVO)l£tTUt

O~Eia TO~tKOTTJTU I , 8aVIlTTJq>OpO <JE £1W<pTJ f.lE TO

8f:pf.11l O~sia TO~tKOTTJTU 3,To~tK6 o£

1tEpt1tTWO"TJ KllT<l1tOOTJ<; Xp6vta TO~tKOTTJTU 2 o£ u8p6PtOus opyavtof.1ous

O~sia TO~tKOTTJTil, an6 oT6f.1aTO<;, Kanwopia 4 Eps9tof.16<; TOU bEpf.1aro<;

(Kantyopia 2) Epe9tof.16<; TWV o<p9aA.f.1WV

(Ka<TJyopia 2) EtiltKTJ TO~tKOTTJTU om 6pyava

o<6xou<;-s<pana~ EK9EoTJ (KaTTJyopia 3)-MnopEi va 1tpOKilAE<JEl Ep£9t<Jf.10 O"TTJV

avanvo O~sia TO~tKOTTJTU, an6 o<6f.1a<os, Kanwopia 4

Atmos L

ab

Finest Gree

k Eliquids

· To Epya<n~pLO To~tKoA.oyiac; q>f:pEtm<norroiT]<HJ <ril!lq>wva 1-LE to ISO: 17025 yta nc; 8ta8tKacri£c; rrapaA.ap~c;, btaXEiptcrT]c;, Kamypaq>~c; Kat apx~>to8£TT]<JT]c; 1wv b£lY!lCL1WV Kat A£noupy£i !l£ 8taKptPw!l£v~>c; crucrK£u£c; Kat 6pyava.

T ASINOMHI:.H TOY EII:.DNEOMENOY ATMOY

M£ ~acr11 -rT)V AX~ 265/2002, <DEK 1214/B'/19.9.2002 Kat 'CT)V -ca~tVOf.!T)<JT) -ccov f.!£f.!OVCOf.!8vcov crDcrmnKrov -roD f.!ElYf.!a-coc; ~acr£t -coD Kavovtcrf.!OD 1272/2008 (EK), -co f.!ElYf.!U £tcrnv£6f.!£VOD a-rf.!OD 1WD nporim£t an6 TTJV a-rJ.!onoi.T)<JT) -roD Dypou avanA.T]pcocrT)c; BEBECA 18mg (Apt8f.!6c; ITap-ci.8ac;: 011 BEBECA 18mg/12) f.!£ crucr-cacr11 99,97% 6ncoc; avaq>£p£-rat cr-cov ITi.vaKa 1, m~tVOf.!Ehat coc; noA.u -co~tK6 (T + )cr£ nEpi.n-ccocrT) EITA<D'Hc; ME TO .6.'EPMA KAI nc; EITIBAAB'Ec; (Xn) <J£ 7t£pt7t'CCO<JT) KU'CUJtO<JT)c; Ka-canOcrT)c; .

ANIXNEYI:.H NITPOZAMINQN I:.TON EII:.DNEOMENO ATMO MET A ADO

I:.YMDYKN!!I:.H

E<l>APMOZOMENH ANA/\ YTIKH TEXNIKH ··: Yypf] XpcoJlaLOypa<pia-<l>acrJlaTOJlETpia Ma.t~a~ (Liquid


ANIXNEYOMENEI:. OYI:.IEI:.

0 £t<J7tV£0f.!£VOc; U'rf.!Oc; JtOD npoKDm£t an6 'CT)V U'Cf.!07tOtT)<JT) 'COD 8taAUf.!U'rOc; avanA_TjpcocrT)c; BEBECA 18mg (Apt8f.!6c; ITap-ci.8ac;:Oll BEBECA 18mg /12) £~£-racr8T)K£ yta 'CT)V avi.xvwcr11 -ccov napaKa-rco vupo~af.!tvrov, ITi.vaKac; 2.

llivaKas 2.

4-(Methylnitrosamino )-1-(3-pyridy1)-1-butanol 4'-(nitrosomethylamino )-1-(3-pyridyl)-1-butanone

N -nitrosoanatabine N -nitrosoanabasine

ADOTEAEI:.MA T A

(ppm)

ND*

ND ND ND

'Opto DoGO'TlKOU DpoGblOplGJlOU ME9obou (LOQ)

(ppm)

0,01

0,01 0,05 0,01

ANIXNEYI:.H DOA YKYKAIKQN AP!!MA TIKQN Y APOrONAN0PAK!!N I:.TON

EII:.DNEOMENO ATMO META ADO I:.YMDYKNQI:.H

E<l>APMOZOMENH ANA/\ YTIKH TEXNIKH : A£pta XpcoJlaToypa<pia- <l>acrJlUTOJlC:Tpia Mat;a~ (Gas


2

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ANIXNEYOMENKE OV:EIEI:

0 Etmrw:6jlEVOt; Utjl6t; nou npOKU7rtEt an6 TT]V Utjl07r0tr]CH] 'LOU DtaA:UjlUtOt; avanA.ijprocrT]t; BEBECA 18mg (Apt8jl6t; ITapti8at;:O 11 BEBECA 18mg I 12) E~Etacr8T]KE yta "CT]V avixvwcrT] trov napaKatro noA.uKUKAtKffiv aprojlanKci:>v u8poyovav8p6.Krov (PAHs ), ITivaKa<; 3.

llivaKaS 3.




chrysene benzo(k)fluoranthene benzo(b )fl uoranthene benzo(g,h,i)perylene

dibenzo(a,h)anthracene indeno( 1 ,2,3-CD)pyrene

AIIOTEAEI:MA T A

Opto IloooTtKou I:uyKEV'Tp<Ooll Ilpoo(hoptoJlOU ME96()ou

(LOQ)

(ppm) (ppm)

ND* 0,005 NO 0,010 ND 0,005 ND 0,006 ND 0,003 ND 0,003 NO 0,003 ND 0,060 ND 0,006 NO 0,014 ND 0,021 ND 0,022

*ND: ~EV llVtXVEU8TJKUV 1tOAUKUKAtKOt a.pffi~LU'ttKOt u8poyovav8pa.KE<; O"Ujl<pffiVU jlE TU a.va.<pcpOjlcVU 6pta. a.vixvcucrTJ<;.

,.,.,,. .... "' .; i' . "'\.~ .

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" / ,. / \ ,

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/ Apto'Td011S M. TonT«niKTJ.; --~ MSc (Org Chern), PhD (Chern), DSc (Bioi), ERT (Eur Registered Toxicologist)

Kn9l)YlJnlS T o~tKol.oyia<; hnptKoi> T JlltJl«Toc:;

At&llltu~"Tl\s Epya<J"t'11piou la'Tpo()tK«MLKrov E7ttGT1)Jlrov & Movuoac:; To;tKoA.oyiac;

3

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ab

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TIANETIIl:THMIO KPHTHl: TMHMA IATPIKHL:


T.9. 2208 Hpiuuo.&\0 Kpi)"tl) P.O.Box 2208 Heraklion Crete, Greece

EPfAli:THPIO TO!IKOAOfiAli:

L\u:u9uv-ri)<;: Ka9T)YTJ-ri)<; ApLaTt:t6T)<; M. Taa-raaKT)<; Tel +30 2810 394870, Fax +30 2810 542098 e-mail: [email protected] http://ctoxres.med.uoc.qr

Epyaot~plO - nt .. r]po<j>oplE<; : 2810 394687- 394681 - 394794, Fax: +30 281 0 39 46 88

lllETOllOIHTIKO ANAA YEHE* KAI TASINOMHEHE TOY AIAA YMATOE ANAllAHP!!EHE CAMILA

ETAIPIA: ATMOS LAB EMTIOPIKH ONOMAI:IA YrPOY ANATIAIIP.QI:HI: : CAMILA API0MOI: TIAPTIAAI:: 011 CAMILA /I2

TIOIOTIKOI: TIPOI:AIOPII:MOI: AIAA YMATOI: ANATIAIIP.QI:HI: E<l>APMOZOMENH ANA/\ YTIKH TEXNIKH: Atptos; Xpffi!la:roypacpia-<l>acrlla.To!l£-rpia Masas; (Gas Chromatography -Mass Spectrometry) Kat **Yypl) Xpffi!la-roypacpia-<l>acr!la.LO!lf:Tpia Masas; (Liquid Chromatography-Mass Spectrometry)

TIOI:OTIKOI: TIPOI:AIOPII:MOI: MEXPI TIOI:OI:TOY 99,9983%

TiivaKa<; 1.

ethyl vanillin

propylene glycol

glycerol

water

nicotine

I:l>voA.o

ATIOTEAEI:MA TA

llO(JO(J'TO (%w/v)

0,001

15,52

80,70

2,2773

1,5

99 9983

'Opto llO(JO'TlKOU llpo(J(hopt(JflOU Mt96aov (LOQ)

( m)

0,032

0,198

I, I87

0, I

O~cia TO~tK6-tT]TU an6 crT6!la.TOs;, Ka.TT]yopia 4

Epc8tcr!l6s; Mp!la.Tos;, Ka.TT]yopia 2

Epc8tcr!l6s; ocp8a.A.!lciw Ka.TT]yopia 2

Et8tK1) -ro~tKOTllTU crm 6pyava-cr-r6xous; Eq>ana~

tK8c(JT] Kanwopia 3 .t.cv m~tYO!lchat

.t.cV TU~tV0!1£hat

O~cia -ro~tKOTT]TU I O~cia TO~tK6TT]m 3

Xp6vta TO~tKOTT]TU 2 crc u8p6pwus; opyavtcr!lous;

• To EpyaoT~pLO To~tKoA.oyiac; q>EpEt rrt<JT07tOtT)<JT) <JlJf.lq>rova f.lE TO ISO: 17025 yta nc; 8ta8tKaoi~::c; napaA.a~~c;, 8taxEiptoT)c;, Kamypaq>~c; Kat apx~::to9€TTJOTJc; Trov 8~::tyf.l<lTrov Kat A.~::noupy~::i f.lE 8taKpt~rof1€v~::c; ouoKED€c; Kat 6pyava. •• H opyavoA.oyia LC-MS q>€p~::t 8taKpi~rooT) KaTa ISO: 17025 f.lE n~::8io ~::q>apf.Loy~c; TTJV avixvEDoTJ vapKronKffiv oumffiv on1v tpixa.

Atmos L

ab

Finest Gree

k Eliquids

T AEINOMH:EH TOY YrPOY ANATIAHPU:EH:E CAMILA

M~:: ~U<JT] TT]V AX~ 265/2002, <DEK 1214/B'/19.9.2002, TT]V Ta~tVOf.!Tj<JTj TffiV j..lf:j..lOVffij..lEVffiV crucr-rauKmv Tou f.!ctYf.!UTOS Kat ~acrTJ TOU Kavovtcrf.!OU 1272/2008 (EK) TO CAMILA (Apt8f.!6S ITapn8ac;: 011 CAMILA 112) f.!l:': 99,9983% crU<JTa<JT] nou ava<p£p~::Tat crTov ITivaKa 1, -ra~tvOf.!l:':hat roc; f.!T] ~::mKiv8uvo yta TT]V av8pcD1ttVT] uycia, yta TO 1tl::pt~UAAOV Kat j..lf: ~U<JT] TtS <pUcrtKOXT]f.!lKES TOU t8t6TT]Tf:t;. Enmp6cr8~::Ta, yta TTJ XPTJ<JT] Tou 8taA.uf.!UTOS avanA.i]pmcrTJs an6 TO T]Af:KTpovtK6 Tcrtyapo, TO j..lctyj..la f:t(J1tVf:Oj..lf:VffiV UTj..lcDV 1tOU U1tf:AGU8~::provf:Tat XPI::tasf:Tat Ta~tVOf.!Tj<JT] AUj..l~UVOVTUS un' 0\j/Tj TT]V f:KUTO<JTtata crU<JTa<JT] TffiV UTj..lcDV 1tOU napayOVTat j..lf: TT]V GVI::pyo7tOtTj<JTj TOU f.!TJXUVt<Jj..lOU UTj..l01tOtTj<JT]S f.!EXPl 1tl::pti::KTtKOTT]TaS 0.1% W~ <Jf: j..lf:j..lOVffij..lEVO <JU<JTaTtKO, Ka8roc; Kat TT] cruyK~::Kptf.!EVTJ XPTJ<JT] auTmv.

ANIXNEY:EH NITPOZAMINQN :ETO AIAA YMA ANATIAHPU:EH:E

E<l>APMOZOMENH ANAA YTIKH TEXNIKH **: Yypi] Xpffif.!a:roypa<pia-<l>aof.!UTOf.!cTpia Masac; (Liquid



To 8taAUf.!U avanA.i]pmcrT]c; CAMILA (Apt8f.!6S ITapTi8ac;:Oll CAMILA /12) ~::~~::Tacr8T]Kf: yta TTJV

avixvcucr11 Trov napaKaTm vnposaJ..ttvrov, ITivaKac; 2.

IlivaKas 2.

AKprov'UfllO

4-(Methy1nitrosamino )-1-(3-pyridyl)-1-butanol 4'-(nitrosomethylamino )-1-(3-pyridyl)-1-butanone N -nitrosoanatabine

N -nitrosoanabasine

ATIOTEAE:EMAT A

(ppm)

ND*

ND ND

ND

'OptO llO(JOTlKO'U llpo(J&10pt(Jf.10'U Mt9o&ol) (LOQ)

(ppm)

0,01

0,01 0,05

0,01

ANIXNEY:EH TIOAYKYKAIKUN APUMATIKQN YAPOrONAN0PAK!1N :ETO

AIAA YMA ANATIAHPU:EH:E

E<l>APMOZOMENH ANAAYTIKH TEXNIKH: A£pta Xpffi~ta-roypaq>ia- <l>aof.!UTOf.!cTpia Masac; (Gas


Atmos L

ab

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ANIXNEYOMENEI: OYI:IEI:

To 8ui/..u11a avarr/..ijprocr11c; CAMILA (Apt9!l6c; ITapri8ac;:O 11 CAMILA I 12) E~E-cacr911KE yta "ClJV

avixvcucr11 -crov rrapaKa-cro rrof..uKUKAtKcOV apro!lanKmv u8poyovav9paKrov (PAHs), ITivaKac; 3.

TiivaKas 3.

acenaphty1ene

fluorene

phenanthrene

anthracene

pyrene

benzo(a)anthracene

chrysene


benzo(b )fluoranthene


dibenzo( a,h )anthracene


AIIOTEAEI:MAT A

'Opto IloaonKo-6 I:uyKEVTpOOO"TJ Ilpoa&wptof.10'6 ME96&ou

(LOQ) (ppm) (ppm)

ND* 0,005

ND 0,010

ND 0,005

ND 0,006

ND 0,003

ND 0,003

ND 0,003

ND 0,060

ND 0,006

ND 0,014

ND 0,021

ND 0,022

*ND: ~Ev avtxv€'U8TJKUV noA.uKUKAtKoi apcof..LanKoi u8poyovav8paKE<; <n)f..L<pcova f..L€ m ava<p€p6p.tva 6pta UVLXV€UGTJ<;.

0 .:1tcu9uvri)<; wu Epyg. · piou, /

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Ka91JYTJn1c; To;tKoJ..oyiac; laTptKou TJ.LiltJaToc;

~uro9ll\'Ti)<; EpyaOT1Jpioll laTpOOtKaOTtKrov EmoTTJfJWV & Movaow; T o;tKol..oyia;

Atmos L

ab

Finest Gree

k Eliquids

Atmos L

ab

Finest Gree

k Eliquids

ITANEITI~THMIO KPHTH~ TMHMA IATPIKHL:


T.e. 2208 HpciKAEto Kpi)"tl) P.O.Box 2208 Heraklion Crete, Greece

EPfA~THPlO TO!lKOAOflA~

Llu:uOuvTT]<;: KaOT)YTITtl<; ApuJT£L6T)<; M. TaaT<JUKT)<; Tel +30 2810 394870, Fax +30 2810 542098 e-mail: [email protected] http://ctoxres.med.uoc.qr

Epyam~plO - m .. l'jpo¢oplc:c;: 2810 394687 - 394681- 394794, Fax: +30 281 0 39 46 SUl

llii:TOllOIHTIKO ANAA YI:HI:* KAI TASINOMHI:HI: TOY AIAA ANADAHP!!I:HI: GINA 18mg

ETAIPIA: ATMOS LAB

EMIIOPIKH ONOMAEIA YrPOY ANAITAHP!ll:Hl:: GINA 18mg

API0MOI: IIAPTIAAI:: 02/ GINA 18mg/12

TIOIOTIKOI: TIPOI:AIOPII:MOI: AIAA YMA TO I: ANATIAHP!ll:Hl: EAPMOZOMENH ANAA YTIKH TEXNIKH: A£ptat; Xpffif..Lawypa<pia-<l>acrf..LaTofJ£-rpia M6.1;at; (Gas Chromatography -Mass Spectrometry) Kat **Yypl) Xpffif..Lawypmpia-<l>acr~ta'tOf..LETpia Mal;a<; (Liquid Chromatography-Mass Spectrometry)

TIOI:OTIKOI: TIPOI:AIOPII:MOI: MEXPI TIOI:Ol:TOY 99,9999%

IlivaKa 1.

Ouaia

propylene glycol

glycerol

ethyl vanillin


nicotine

water

l:uvow

ATIOTEAEI:MA T A

llOCJOCJTO (%w/v)

53,36

38,90

0,006

0,001

1,6

6,1329

99,9999

OpLO noaOTlKOU llpoaowptCJf.lOU M~:66oou (LOQ)

( m)

0,198

1,187

0,032

0,121

0,1

~eV 'ta~tVOfl£hat

~EV 't(l~tVOfl£hat

O~eia w~tKO'tTJTU, ano cr-r6f..La-rot;, KaTTJyopia 4 Epe8tcrf..L6t; -rou 8£pf..LU"CCt;

(Ka-rTJyOpia 2) Epe8tcrf..L6t; -rffiv o<p8aA.f..LOW

(KaTTJyopia 2) Et8tK1l w~tKO'tTJTU cr-ra

6pyava cr-r6xom;-e<pana~ £K8ECJTJ (KaTTJyopia 3)

O~eia -ro~tKO'tTJ'tU 1 O~eia -ro~tKO'tTJTU 3

Xp6vta w~tKO'tTJ'tU 2 cr£ u8p6pwus opyavtcrf..Lous

Atmos L

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*To Epyacrri]pto Toi;tKoA.oyia~ q>£p£t mcrrorroiT]cr'l mJ!lq>cova !1£ ro ISO: 17025 yta n~ OtaOtKacri£~ rrapaA.api]~, otaxsiptcrT]~ , Karaypaq>i]~ Kat apxsto8ETT]O"T]~ TCOV 0£tYilUTCOV Kat A£ttoupy£i !1£ OtaKptPCO!lEV£~ crucrK£UE~ Kat 6pyava. ** H opyavoA.oyia LC-MS q>f:pst otaKpipcocrT] Kara ISO: 17025 !1£ rrsoio scpawoyi]~ TT]V avixvsucr'l vapKconKwv oucrtwv crrTJV rpixa.

T AEINOMHI:H TOY YrPOY ANAIIAHPQI:HI: GINA 18mg

M£ ~U(JYJ TYJV AXL 265/2002, <DEK 1214/B'/19.9.2002, TI)V Ta~tVOJ..t.Yj<JYJ TOW Jlf:J..I.OV(J)J..t.EV(J)V crucr-ranKffiv -rou J..t.£iYJ..t.aTO<; Kat ~acrYJ TOU KavovtcrJ..t.OU 1272/2008 (EK) TO GINA 18mg (Apt8J..t.6<; ITapTiba<;: 02/ GINA 18mg/12) J..t.£ 99,9999% <JUcr-racrYJ nou avac:p£p£Tat cr-rov ITivaKa 1, -ra~tvOJ..t.£hat ro<; J..I.YJ £ntKivbuvo yta TYJV av8pffimVYJ uy£ia, yta TO 7t£pt~UAAOV Kat Jlf: ~U<JYJ n<; c:pucrtKOXYJJltK£<; -rou tbtOTI)T£<;. Emnp6cr8£Ta, yta •YJ XPTJ<JYJ Tou btaAUJlaTo<; avanA.i]procrYJ<; an6 w YJAEKLpOVtKO Tcrtyapo, TO J..t.£iYJ..t.a £tcr1tV£0J..t.£VffiV a1:J..t.WV 7tOU a7t£A£U8£pffiV£1:at XP£ta~£Tat -ra~tvOJ..t.YJ<JYJ AaJ..t.~avovTa<; un' O\j/YJ TYJV £KaTocrnaia crucrTacrYJ Trov aT)lffiv nou napayov-rat J..I.E TI)V £V£pyonOtYj<JTj TOU JlYJXaVt<JJ..t.OU aTJ..t.07tOtYj<JYJ<; JlEXPt 7t£pt£KTtKOTYJTa<; 0.1% ~~~ <J£ Jlf:J..I.OVWJ..t.EVO crucrTanK6, Ka8ffi<; Kat TTJ cruyK£KptJ..t.EVYJ XPTJ<JYJ auTffiv.

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E<l>APMOZOMENH ANAA YTIKH TEXNIKH ** : Yypl) Xpffi~w:roypa<pia-<l>acrllaTO!l£•pia Mal;w; (Liquid



To btaAUJla avanA.i]procrYJ<; GINA 18mg (Apt8J..t.6<; I1apTiba<;:02/ GINA 18mg/12) £~£Tacr8YJK£ yta TTJV avixvwcrYJ Trov napaKaTro vnpo~aJ..t.tvffiv, ITivaKa<; 2.

IlivaKas 2.

AKproVUJltO

4-(Methy1nitrosamino )-1-(3-pyridyl)-1-butanol 4'-(nitrosomethylarnino )-1-(3-pyridyl)-1-butanone

N -nitrosoanatabine

N -nitrosoanabasine

AIIOTEAEI:MA T A

(ppm)

ND*

ND

ND

ND

Opw IloaoTtKou IlpoaowptO'JlOU Mt96oou (LOQ)

(ppm)

0,01

0,01 0,05 0,01

ANIXNEYI:H IIOA YKYKAIKQN APQMATIKQN Y APOrONAN0PAKQN I:TO

AIAA YMA ANAIIAHPQI:HI:

E<l>APMOZOMENH ANAA YTTKH TEXNIKH : A£pta Xpffillawypac:pia- <l>acr!laTO!l£-rpia Mal;w; (Gas


2

Atmos L

ab

Finest Gree

k Eliquids

ANIXNEYOMENEI:. OYI:.IEI:.

To 8uiA.u11a avanA.i)pcocrrv; GINA 18mg(Apt8!l6t; ITap-ri8at;:02/ GINA 18mgll2) £~nacr8T)K£ yta -rT)V avixvcucrT) -rcov napaKa-rco noA.uKUKAtKffiv apco!lanKffiv u8poyovav8paKcov (PAHs), ITivaKat; 3.

IlivllKilS 3.

AKprovilt.tto

acenaphtylene

fluorene

phenanthrene

anthracene

pyrene

benzo(a)anthracene

chrysene

benzo(k)fl uoranthene





AIIOTEAEI:.MA T A

'Opto Ilo(JO'TlKoil l:'UyKEVTpW(Jl} Ilpo(JOlOpt(JflOil Ms9oOo'U

(LOQ) (ppm) (ppm)

ND* 0,005

ND 0,010

ND 0,005

ND 0,006

ND 0,003

ND 0,003

ND 0,003

ND 0,060

ND 0,006

ND 0,014

ND 0,021

ND 0,022

*ND: Llev UVtXV£U8TJKUV 1tOAUKUKAtKOt a.pCOIJ.UHKOt u8poyovuv8pa.K£S <JUj..lq>ffiVU j..l£ La. a.va.cpep6~teva. 6pta. a.vixveumlS·

3

Atmos L

ab

Finest Gree

k Eliquids

ITANEITIL.THMI 0 KPHTHL. TMHMA IATPIKHL:

T.9. 2208 HpciKA~:to Kpip:q



* lli~TOllOIHTIKO ANAA Y~H~ MET A AllO ~YMllYKN!!~H KAI T A2INOMH~H~ EI~llNEOMENOY ATMOY llOY llPOKYllTEI AllO THN

ATMOllOIH~H YrPOY ANAllAHP!!~H~ GINA 18mg

ETAIPIA: ATMOS LAB

EMllOPIKH ONOMA.EIA YrPOY ANAIIAHPQ.EH.E: GINA 18mg

API0MO.E IIAPTIAA.E: 01/ GINA 18mg 112

TIOIOTIKO.E TIPO.EAIOPI.EMO.E EI.ETINEOMENOY ATMOY MET A ATIO .EYMTIYKNQ.EH E<DAPMOZOMENH ANA/\ YTIKH TEXNIKH: Atpto~ Xpw!lawypa<pia-<Dacr!la'W!-LETpia Musa~ (Gas Chromatography -Mass Spectrometry) Kat **Yyp1) Xpw!lawypa<pia-<Dacr~ta'tO!!ETpia Musa~ (Liquid Chromatography-Mass Spectrometry)

TIO.EOTIKO.E TIPO.EAIOPI.EMO.E MEXPI TIO.EO.ETOY 99,98%

TiivaKa 1.

Ouaia

propylene glycol

Glycerol

Nicotine


Ethyl vanillin

Water

.Ei>vol..o

ATIOTEAE.EMA TA

noaoaT6 (%w/v)

68,70

28,25

1,6

0,027

0,007

1,4

99,98

Opw noaOTlKOU npoaOlOptGflOU Mt96oou (LOQ)

( m)

0,198

1,187

0,1

0,121

0,032

~EV TU~tVO!!£hat

~EV TU~tVO!!£hUt

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i>f:pfla O~cia TO~tKOTTJTa 3, To~tK6 aE

7rEpt7rTffiO"T] KllT<l7rOO"T]~ Xp6vta TO~tKOTT]Ta 2 O"E uop6~tOUS opyavtO"flOUS

O~cia TO~tKOTT]Til arr6 TOU O"TOflaTo~, KaTT]yopia 4 EpE9lO"fl0~ TOU OEpflllTO~

(KaTT]yopia 2) EpE9tO"fl6~ Tmv oq>9aA.fl<llV

(KaTT]yopia 2) EtotK~ TO~tKOTTJTa am 6pyava

aT6xou~-Eq>arra~ £K9EO"TJ, Mrropci va rrpoKaA.£aEt

EpE9tO"flO TT]~ avarrvEUO"TlK~~ OOOU (KaTT]yOpia 3)

· To EpyaaT~pto To~tKoA.oyia~ q>EpEt maTorroiT]O"TJ aUf.Lq>mva f.LE TO ISO: 17025 yta n~ otaotKaai£~ rrapaA.a~~~, OtllXEiptaT]~, Kamypaq>~~ Kat apxEta9ETTJO"TJ~ Tmv OEtYflUTmv Kat A.t:tmupyci f.LE otaKpt~ffiflEvE~ O"UO"KEUE~ Kat 6pyava.

Atmos L

ab

Finest Gree

k Eliquids

TASINOMHI:H TOY EII:IINEOMENOY ATMOY

M~:: ~<icrTJ 'tTJV AXL: 265/2002, <DEK 1214/B'/19.9.2002 KaJ 'tTJV -ra~tVOflTJCJTJ -rwv JlEJ.lOVWJ.lEvwv crucrwnKrov -rou JlclYJ.law<; ~acr~::t -rou KavovtcrJ.lOU 1272/2008 (EK), -ro JlclYJ.la ~::wn:E6JlEVou a-rJ.lou n:ou n:porin:-r~::t an:6 'tTJV a'tJ.lOn:OiTJcrTJ uypou avan:A.ftpwcrTJ<; GINA 18mg (Apt8fl6<; flapri8ac;: 01/ GINA 18mg/ 12), JlE crucrwcrTJ 99,98% 6n:w<; ava<p£pcwt cr-rov ITivaKa 1, w~tVOJ.lEhat roc; n:oA.u 'tO~lKO (T +) CJE 1tcpin:-rwcrTJ En:a<pf}<; Jlc 'tO bEpJ.la Kat w<; Em~Aa~£<; (Xn) CJE 1tcpimwcrTJ KU'tU1tOCJTJ<;.

ANIXNEYI:H NITPOZAMIN.QN I:TON EII:IINEOMENO ATMO MET A AIIO

I:YMIIYKN .QI:H

E<l>APMOZOMENH ANAA YTIKH TEXNIKH ** : Yypij Xpw~tawypaq>ia-<l>acrJ.lULOf.!£-rpia Masac; (Liquid



0 Etcrn:vc6JlEVO<; a-rJ.l6<; n:ou n:porin:-rEt an:6 'tTJV a-rJ.lon:oiTJCJTJ uypou avan:A.ftpwcrTJc; GINA 18mg (Apt8Jl6<; flap-ri8ac;:Oll GINA 18mg /12) E~E-racr8TJKE yta 'tTJV avixvcucrTJ -rrov n:apaKa-rro vt-rpo~aJ.ltvmv, ITivaKa<; 2.

IlivaKas 2.

4-(Methylnitrosamino )-1-(3-pyridyl)-1-butanol 4'-(nitrosomethylamino )-1-(3-pyrid yl)-1-butanone

N -nitrosoanatabine

N-nitrosoanabasine

AIIOTEAEI:MA TA

(ppm)

ND*

ND ND ND

'Opw Iloao'TlKO'U IlpoaowptaJ!Oll M~::OooolJ (LOQ)

(ppm)

0,01

0,01

0,05

0,01

ANIXNEYI:H IIOA YKYKAIK.QN AP.QMATIK.QN Y APOrONAN0PAK.QN I:TON

EII:IINEOMENO ATMO META AIIO I:YMIIYKN!!I:H

E<l>APMOZOMENH ANAA YTIKH TEXNIKH : A£pta Xpwf.!awypaq>ia- <l>acrJ.lU'Wf.lE'tpia Masac; (Gas



0 EtcrnvE6JlEVO<; a-rJ.l6c; n:ou n:porin:-rct an:6 LTJV a-rJ.lon:oiTJCJTJ uypou avan:A.ftpwcrTJ<; GINA 18mg (Apt8Jl6c; flap-ri8ac;:Oll GINA 18mg /12) E~E-racr8TJKE yta 'tTJV avixv~::ucrTJ -rwv n:apaKa-rw n:oA.uKUKAtKffiv apwJ.lanKmv u8poyovav8paKwv (PARs), ITivaKac; 3.

2

Atmos L

ab

Finest Gree

k Eliquids

llivaKas 3.

acenaphtylene

fluorene

phenanthrene

anthracene

pyrene

benzo(a)anthracene

chrysene




di benzo( a,h )anthracene


AIIOTEAEI:.MA T A

Opw IloaoTtKoi> 1:,1)yKEVT proa11 Ilpoac)wptaJLOU Mt06()o1)

(LOQ) (ppm) (ppm)

ND* 0,005

ND 0,010

ND 0,005

ND 0,006

ND 0,003

ND 0,003

ND 0,003

ND 0,060

ND 0,006

ND 0,014

ND 0,021

ND 0,022

*ND: ~Ev avtxvcu811Kav noA.uKUKAtKoi apco).la:nKoi u8poyovav8paK£<; cru).l<pcova )1£ -ra ava<pt:p6)1£va 6pta avixvcucr11c;.

0 ~umeuvn;c; Tou tP"{g. · piou

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.,. / \ "" -...~1~' / \ ' ~ 'l I~\' " ' '

. i':.-, \:) "--' '-.• ctJ ":" --

/ AptoTEiBra; M. ToaTaaKtJc;. ·~ '~ MSc (Org Chern), PhD (Chern), DSc (Bioi), ERT (Eur Registered Toxicologist)

Ka9ttYTtnl<; To~tKo)..oyia,;; laTptKoi> TJ.LftJUITo<;

£\um9'U\'Ttl<; EpyaG't'llpio1) la'tpoBtK«OTtKrov E7ttO't11J1WV & Movaoa.c; To~tKol..oyia:;

3

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Atmos L

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ITANEITI~THMIO KPHTH~ TMHMA IATPIKHL.


T.9. 2208 HpaKAuo Kpirtll P.O.Box 2208 Heraklion Crete, Greece

EPrAl:TRPlO TO!IKOAOriAl: L\u:uOuvTi)«;: KaOT)YTITTJ«; Apl<JT£L6T)«; M. TaaT<JrtKT)«;

Tel +30 2810 394870, Fax +30 2810 542098 e-mail: [email protected] http://ctoxres.med.uoc.qr Epyacn:~plO- nArJPo¢>oplEc;: 2810 394687- 394681 - 394794, Fax: +30 281 0 39 46 su~

lllETOllOIHTIKO ANAA Yl:Hl:* KAI T AEINOMHI:Hl: TOY AIAA ANAIIAHP!!l:Hl: HABANA 18mg

ET AIPIA: A TMOS LAB

EMllOPIKH ONOMAI:IA YrPOY ANAITAHP.Qr.Hr.: HABANA 18mg

API0MOr. IIAPTIAAr.: 02/ HABANA 18mg/12

IIOIOTIKOr. IIPOr.AIOPir.MOr. AIAA YMA TOr. ANAIIAHP.Qr.Hr. E<l>APMOZOMENH ANAA YTIKH TEXNIKH: A£ptoc; XpCD!!CL'Wypuq>iu-<l>uof..Ul'tO!!ETpiu Mu~uc; (Gas Chromatography -Mass Spectrometry) Kat **Yypft XpCDf..tmoypuq>iu-<l>uo!!CL'W!!E'rpiu Mu~uc; (Liquid Chromatography-Mass Spectrometry)

IIOr.OTIKOr. IIPOr.AIOPir.MOr. MEXPI IIOr.Or.TOY 99,9999%

IlivaKUS 1.

propylene glycol

glycerol

ethyl vanillin

nicotine


Ethyl alcohol

water

r.uvoJ...o

AllOTEAEr.MA T A

flOO'OO'TO (%w/v)

69,72

27,49

0,007

1,6

0,002

0,92

0,2609

99,9999

OplO flOO'OTlKOU llpoaowptO'I.lOU Meeooou (LOQ)

( m)

0,198

l, 187

0,032

0, l

0,121

l gr/Lt

• ~EV 'tU~tVO!l£LLCLl

~EV 'tU~tVO!!ELLUt

O~eiu w~tKOTllTU, uno OTO!!U'Wc;, KuTllyopiu 4 Epe8to116c; •ou o£p!luwc;

(KuTllyopiu 2) Epe8to116c; TCDv oq>8uA.wbv

(Kunwopiu 2) EtotKft w~tK6Tllm om

6pyuvu o-r6xouc; -£q>ana~ £K8£<n] (Kunwopiu 3) O~eia TO~tKOTllLCL 1 O~eiu 'W~tKOTllLCL 3

Xp6vtu 'W~tKOTllTU 2 o£ uop6ptouc; opyuvtO!!OUc;

Atmos L

ab

Finest Gree

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*To Epyacrn'jpto To~tKoA.oyiac; q>EpEt mcnonoill<HJ <J1Jflq>wva flE to ISO: 17025 yta nc; l'itabtKacriEc; napaA.ap~c;, l'itaxEiptcrllc;, Kamypaq>~c; Kat apxEto8£tllcrllc; twv l'iEtyfl<'nwv Kat A.EttoupyEi flE l'itaKptPWflEvEc; crucrKw£c; Kat 6pyava. •• H opyavoA.oyia LC-MS q>£pEt l'itaKpipwcrll Kata ISO: 17025 flE nEI'iio Eq>apfloy~c; tllv avixvwcr11 vapKwttKffiv oumwv crt11v tpixa.

T ASINOMHI:H TOY YrPOY ANAllAHP!!l:Hl: HABANA 18mg

Me ~acr11 TllY AXL 265/2002, <DEK 1214/B'/19.9.2002, TllY Ta~tYO)lll01l TO)V )lcflOYmJ.lEYmv crucrmnKffiY Tou JlclYJ.lUTO<; Kat ~acr11 TOU KaYOYt0JlOU 1272/2008 (EK) TO HABANA 18mg (Apt8)l6<; I1apTi8ac;: 02/ HABANA 18mg/12) Jlc 99,9999% 0UcrTU0111tOU aYa<p£pcTat crTOY

IliYaKa 1, Ta~tYOJ.lchat me; llll cmKiY8uYo yta TllY aY8pffimY11 uycia, yta TO 7tcpt~aAAOY Kat Jlc ~acr11 n<; <pUcrtKOXllfllKE<; Tou t8t6Tl1Tc<;. Em7tp6cr8cTa, yta Tll XPTJ011 Tou 8taAu)laTo<; aYa1tAijpmcr11<; a1t6 TO llAcKTpOYtKO Tcrtyapo, TO JlclYJ.lU cl01tVcO)lcYffiY UT)lcOY 1tOU U1tcAcU8cpffiYcTat XPctascmt TU~tv0)l11011 AU)l~UYOYTU<; U1t' 0\jfll TllY cKUTOcrnaia crU0TU01l TillY UT)lcOY 1tOU 1tapayOYTat )lc TllY CVcpy07t0l11011 TOU llllXUYl0)lOU UT)l01t0t11011<; JlEXPt 1tcptcKHKOTllTU<; 0.1% ~~~ 0c )lc)lOYffi)lEVO crucrTanK6, Ka8ffi<; Kat Tll cruyKcKpt)lEYll XPTJ01l auTffiY.

ANIXNEYI:H NITPOZAMIN!!N l:TO AIAA YMA ANAllAHP!!l:Hl:

E<DAPMOZOMENH ANA!\ YTIKH TEXNIKH ** : Yypij Xpffi)latoypa<pia-<Daa)laTOJ.IEtpia Masac; (Liquid



To 8taAUJ.la aYa1tA.ijpmcr11<; HABANA 18mg (Apt8)l6<; I1apTi8ac;:02/HABANA 18mg/12) c~cTacr811Kc yta TllY UVlX)'cU011 TillY 1tapaKaTm YtTPOSU)llYWY, IliYaKa<; 2.

llivaKas 2.

AKpO>VUJUO

4-(Methylnitrosarnino )-1-(3-pyridyl)-1-butanol 4'-(nitrosomethylarnino )-1-(3-pyridyl)-1-butanone

N-nitrosoanatabine

N-ni trosoanabasine

AllOTEAEI:MAT A

(ppm)

ND*

ND

ND

ND

'OplO llOGOTlKOU llpoG~lOplGJ.lOU ME00~01) (LOQ)

(ppm)

0,01

0,01 0,05 0,01

ANIXNEYI:H llOA YKYKAIK!!N AP!!MA TIK!!N Y APOrONAN0PAK!!N l:TO

AIAA YMA ANAllAHP!!l:Hl:

2

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ab

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E<DAPMOZOMENH ANAAYTIKH TEXNIKH: A£pta Xpcof..La-roypa<pia- <Dacrf..LUTOfl£Tpia Masac; (Gas


ANIXNEYOMENE'E OY'EIE'E

To 8uiA.u11a ava1tA.ijpcocr11~ HABANA 18mg(Apt8!l6~ I1ap-d8a~:02/ HABANA 18mg/12) cSc'r<icr811Kc yta TllV avi:X,VcUO"ll TCOV 1tapaKIXTCO 1tOAUKUKAtKcDV apCO!lUTtKcDV u8poyovav8paKCOV (PAHs), TiivaKa~ 3 ..

IlivaKas3.




chrysene benzo(k)fluoranthene benzo(b )fluoranthene benzo(g,h,i )perylene


AllOTEAE'EMAT A

Opw llo<JoTtKoi> 'I:uyKtVTpO>Gll llpoG(hoptGf.lOU M£965ou

(LOQ) (ppm) (ppm)


*ND: ~C:V aVt:X,VC:U8TJKUV n:OAUKDKAtKOi apCDf..LUTtKOt ubpoyovav8paKC:S CJUf..Lij>CDVa f..LC: Ta ava!pC:pOfl£VU 6pta avi:x,vc:ucr11c;.

3

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ab

Finest Gree

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ITANEITIL:THMI 0 KPHTHL: TMHMA IATPIKH2:

T.e. 2208 HpciKAuo KpirtrJ

UNIVERSI'IY OF CRETE MEDICAL SCHOOL


IIIETOIIOIHTIKO ANAA Yl:H:E META ADO l:YMDYKN.Ql:H * KAI T AEINOMHI:Hl: Ell:IINEOMENOY A TMOY IIOY IIPOKYIITEI ADO THN

ATMODOIHI:H YrPOY ANADAHP!!l:Hl: HAVANA 18mg


EMIIOPIKH ONOMAI:IA YrPOY ANAIIAHP!li:HI:: HAVANA 18mg

API0MOI: IIAPTIAAI:: 011 HAVANA 18mg /12

IIOIOTIKOI: IIPOI:AIOPII:MOI: l:TON Ell:DNEOMENO A TMO META ADO l:YMDYKN.Ql:H E<DAPMOZOMENH ANAAYTIKH TEXNIKH: A£ptoc; Xpffi~w:roypa<pia-<Dacr11a1:o~tE1:pia Masac; (Gas Chromatography -Mass Spectrometry) Kat **Yypll Xpffillawypa<pia-<DacrllULOflE'Lpia Masac; (Liquid Chromatography-Mass Spectrometry)

IIOI:OTIKOI: IIPOI:AIOPII:MOI: MEXPI IIOI:OI:TOY 99,97%

IlivaKa 1.

Ouuia

propylene glycol

Glycerol

Nicotine


Ethyl vanillin

Water

I:uvolo

AIIOTEAEI:MA TA

nouOCJTO (o/ow/v)

65,96

32,00

I, I

0,002

0,006

0,90

99,97

Opto nouOTLKOU n poulhoptuf.10U Mt96oou (LOQ)

( m)

0,198

1' 187

0,1

0,121

0,032

LlEV "CU~lVOilf:LLUl

LlEV LU~lVOilf:LLUl

O~tia w~tK6nrra I, 8avatT]<p6po cre ma<pi] flt 1:0 8£pfla

O~Eia TO~tKOTT]Ta 3, To~tK6 crE n~:pirrw.>crT] KatcmocrT]~

Xp6vta TO~tKOTTJTU 2 crE u8p6~wu~

O~cia TO~tKOTT]TU arr6 wu crt6flUTO~ , KaTT]yopia 4 Epcf.llCJflO~ TOU OEpflUTO~

(KatT]yopia 2) Epc8tcrfl6~ nov o<p9aAflWV

{KatT]yopia 2) Et8tKij TO~tKOTTJTU crm 6pyava

crtoxou~-E<parra~ £K8EcrTJ , Mrropci va rrpOKUAEcrEt Epc8tCJflO CJTT(V

avarrv~:ucrnK1 oM (Kanwopia 3)

*To Epyacrti]pto To~tKoA.oyia~ <p£pEt mcrwrroiTJGTJ CJUfl<prova flE TO ISO: 17025 yta n~ 8ta8tKacriE~ napaA.a~i]~. 8taxciptcrTJ~, Kamypa<pi]~ Kat apx~:w8£tTJGTJ~ trov OEtyfl<ltrov Kat A.~:noupyci flE 8taKpt~WflEvE~ crucrKE\JE~ Kat 6pyava.

Atmos L

ab

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TASINOMHI:H TOY EII:IINEOMENOY ATMOY

Me ~acr11 tl)V AXL 265/2002, <DEK 1214/B'/19.9.2002 Kal "Cl)V m~tVOf.ll)O"ll tcov f.lcf.lOVCOf.lEVcov crucrmnKffiv tou f.lclYf.lUtoc; ~<icr£t tou KuvovtO"f.lOU 1272/2008 (EK), w f.lclYf.lU £tmrv£Of.l£Vou Utf.lOU nou nporunt£t uno"Cl)v Utf.!Onoil)O"ll uypou uvunA.ijpcocrl)c; HAVANA 18mg (Apt8f.loc; I1upti8uc;: 011 HAVANA 18mg/12) f.l£ O"Ucrmcr11 99,97% oncoc; uvuq>Epcmt crtov ITivuKu 1, tu~tvOf.lchat coc; nolcu w~tKo (T +) a£ n£pimcocrl) £nu<pijc; f.l£ to 8Epf.lU Kat coc; £m~AU~Ec; (Xn) a£ n£pintCOO"l) KUtUnOO"l)c;.

ANIXNEYI:H NITPOZAMIN.QN I:TON EII:IINEOMENO ATMO META AIIO

I:YMIIYKN.QI:H

E<DAPMOZOMENH ANAAYTIKH TEXNIKH ** : Yyp1l Xprof.laToypa<pia-<Dacrf.!a:rof.!cTpia Masa<; (Liquid



0 £tcrnv£Of.l£Voc; Utf.loc; nou nporim£t uno "Cl)V Utf.!Onoil)O"ll uypou uvunA.ijpcocrl)c; HAVANA 18mg (Apt8f.loc; I1upti8uc;:Ol/ HAVANA 18mg /12) £~£t<icr8l)K£ ytu "Cl)V uvixvcuO"l) tcov nupuK<itco vnposuf.ltvffiv, ITivuKuc; 2.

ll(vaKas 2.

4-(Methylnitrosamino )-1-(3-pyridyl)-1-butanol 4'-(nitrosomethylarnino )-1-(3-pyridyl)-1-butanone

N-nitrosoanatabine N -nitrosoanabasine

AIIOTEAEI:MAT A

(ppm)

ND*

ND ND ND

'OplO IIOGOTlKOU Ilpoa~lOplGJlOU

MtOo~o'U (LOQ) (ppm)

0,01

0,01

0,05 0,01

ANIXNEYI:H IIOA YKYKAIK.QN AP.QMATIK.QN Y APOrONAN0PAK.QN I:TON

EII:IINEOMENO A TMO MET A AIIO I:YMIIYKN.QI:H

E<DAPMOZOMENH ANAA YTIKH TEXNIKH: AEpta Xprof.!awypa<pia- <Dacrf.!UTOf.lETpia Masa<; (Gas



0 £mnv£Of.l£Voc; Utf.loc; nou nporunt£t uno tl)V Utf.lonoil)O"ll uypou uvunA.Tjpcocrl)c; HAVANA 18mg (Apt8f.loc; I1upti8uc;:Ol/ HAVANA 18mg /12) £~£t<icr8l)K£ ytu tl)V uviXV£UO"l) -rcov nupuK<itco noAUKUKAtKffiv upcof.lUTIKffiv u8poyovuv8p<iKcov (PAHs), ITivuKuc; 3.

2

Atmos L

ab

Finest Gree

k Eliquids

TiivaKas 3.

Acenaphtylene Fluorene

Phenanthrene Anthracene

Pyrene benzo(a)anthracene

Chrysene benzo(k)fluoranthene

benzo(b )fl uoranthene benzo(g,h,i)perylene


AllOTEAEI:MA T A

'Opto llo<JO'TlKOU 1: U"{KEVT pro <Jfl llpo<J(hopt<JJ.wi> MEOooou

(LOQ) (ppm) (ppm)

ND* 0,005 ND 0,010

ND 0,005 ND 0,006

ND 0,003 ND 0,003

ND 0,003 ND 0,060 ND 0,006 ND 0,014 ND 0,021 ND 0,022

*NO: ll£V aVtXV£U811KUV 1tOAUKUKAtKOt apco~LaTtKOt u8poyovav8paK£<; <JU).Hj>COVa ~L£ La ava<pcpO~LCVa opta avixvcucr11s-

0 lltEU8uvni<; -rou Ep·yg. · piou,

/ /

/' _,/

~/~~:~ / \ '-..•'c:tJ

/ ' "-.,

/ Aplo't£Lo11c; M. TCJaT<JaKTJ.:; --- --~ MSc (Org Chern), PhD (Chern), DSc (Bioi), ERT (Eur Registered Toxicologist)

Ka9l)Y1Jnl<; To~LKO).oyia.:; IrnplKoi> Tf.Li}J!«Toc;

.iu:u9'Uvn1c; EpyafJ't'Tipiou la-rpOOlKUO'ttKrov EnlOTlJJ!WV & Movaoac; To;LKol.oyias;

3

Atmos L

ab

Finest Gree

k Eliquids

ITANEITIL:THMIO KPHTHL: TMHMA IATPIKH~


T.e. 2208 HpciKAuo KpQl:IJ P.O.Box 2208 Heraklion Crete, Greece

EPrA~TlttlO TO!IItOAOflAt L\u:uOuvTI)<;: KaOTJYTJTTt<; ApLaT£L6TJ<; M. Taa-raaKTJ<;

"' Tel +30 2810 394870, Fax +30 2810 542098 e-mail: [email protected] http://ctoxres.med.uoc.qr Epyam:~plO- m .. l']po<!>oplE<; : 2810 394687- 394681- 394794, Fax: +30 281 0 39 46 88

III.ETOIIOIHTIKO ANAA Y.EH.E* KAI TAEINOMH.EH.E TOY AIAA YMATO.E ANAIIAHPQ.EH.EKAPNOS

ETAIPIA: ATMOS LAB EMIIOPIKH ONOMAI:IA YTPOY ANAIIAHPQI:HI:: KAPNOS API0MOI: IIAPTIAAI:: 01/KAPNOS/12

IIOIOTIKOI: IIPOI:AIOPII:MOI: AIAA YMATOI: ANAIIAHPQI:HI: E<DAPMOZOMENH ANAAYTlKH TEXNIKH: Aepto~ XpwJ..La-roypa<pia-<DacrJ..LU'toJ.!ETpia Masa~ (Gas Chromatography -Mass Spectrometry) Kat **Yypi] XpwJ.!aTOypa<pia-<DacrJ..LUTOJ.!ETpia Masa~ (Liquid Chromatography-Mass Spectrometry)


AIIOTEAEI:MATA IlivaKac; 1.

'Opw IIO<JOTlKOU

Ouaia Iloaoa-r6 Ilpoa<hopt<J!lOU (%w/v) Mt06oou (LOQ)

( m)



water 5,6996

nicotine 1,4 0,1

I:uvol.o 99,9896

f1£V TU~lVOJ.!ElTUl

AEV TU~lVOJ.!ElTUl

O~Eia TO~tKOTIFU 1 O~Eia TO~tKOTTJTU 3

Xp6vta TO~tKOTTJTU 2 cr£ u8p6Pwus opyavtcrJ..Lous

* To EpyaoT~ptO To~tKoA.oyiac; <ptpEt rctowrcoiT]OTJ OU!l<pffiva llE TO ISO: 17025 yta nc; 8ta8tKaoicc; rcapaA.ap~c;, 8taxciptcrT]c;, Kamypa<p~c; Kat apxcw8ETTJcrTJc; Tffiv OEtYilUTffiV Kat A.ctToupyci llE 8taKptPffillEYEc; crucrKwtc; Kat 6pyava. ** H opyavoA.oyia LC-MS <ptpct 8taKpipfficrTJ KaTa ISO: 17025 llE rc£8io E<papllOY~c; TTJV aviXVEDOTJ vapKffinK6:JV oucrtffiv O"TTJV Tpixa.

Atmos L

ab

Finest Gree

k Eliquids

TASINOMHl:H TOY YrPOY ANAIIAHP!ll:Hl: KAPNOS

ME ~cicrT] TTJV AXL 265/2002, EK 1214/B'/19.9.2002, TTJV Ta~tVOJ..I.T]crTJ nov J..I.EJ..I.OVo:>J..I.Evo:>V crucrTanKrov Tou J..I.ElYJ..I.UTOc; Kat ~cicrT] wu KavovtcrflOU 1272/2008 (EK) TO KAPNOS (Apt8J..1.6c; TiapTi8ac;: 01/KAPNOS/12) J..I.E 99,9896% crucrTacrTj 1tOU ava<pEpEmt crTOV TiivaKa 1, m~tVOJ..I.Ehat o:>c; J..I.Tj E1tlKtV8UVO yta TT]V av8pro1tlVT] uyda, yta TO 1tEpt~UAAOV Kat J..I.E ~UcrTj nc; <j)UcrlKOXTJJ..llKEc; TOU t8t6TT]TEc;. Emnp6cr8Em, yta TTJ :xpftcrTJ TOU 8taAUJ..laTOc; avan'Aftpo:>crT]c; an6 TO TJAEKTpovtK6 Tcrtycipo, To J..I.EtYJ..la EtcrnvE6J..1.Evo:>v aTJ..lcOV nou anE'AEu8EprovETat :xpEtci~ETat m~lVOJ..I.TJcrTJ 'AaJ..l~avovmc; un' 0\j/Tj TT]V EKUTOcrnaia crucrTacrTj To:>V UTJ..lcOV 1tOU 7tapciyOVTat J..I.E TT]V EVEpyo7tOtTjcrTj TOU J..I.TJXUVtcrJ..I.OU UTJ..l01tOtTjcrT]c; J..I.E:xpt 1tEptEK'!lKOTT]Tac; 0.1 % ~~~ crE J..I.EJ..I.OVo:>J..I.EVO crucrmnK6, Ka8roc; Kat TTj

cruyKEKptJ..I.EVTJ :xpftcrTJ auTrov.

ANIXNEYl:H NITPOZAMIN!!N l:TO AIAA YMA ANAIIAHP!ll:Hl:

E<DAPMOZOMENH ANAA YTIKH TEXNIKH .. : Yypl'l Xpwf.!atoypa<pia-<Dacrf.!atOflt:tpia Mal;ac; (Liquid


ANIXNEYOMENEl: OYl:IEl:

To otci'AuJ..la avan'Aftpo:>crT]c; KAPNOS (Apt8J..1.6c; TiapTi8ac;:Ol/KAPNOS/12) E~ETcicr8TjKE yta TTJV

aviXVEUcrTJ -rwv napaKci-rw vnpo~aJ..ltvrov, TiivaKac; 2.

IlivaKas 2.

4-(Methylnitrosarnino )-1-(3-pyridyl)-1-butanol 4'-(nitrosomethylarnino )-1-(3-pyridyl)-1-butanone

N -nitrosoanatabine

N-nitrosoanabasine

AIIOTEAEl:MA T A

(ppm)

ND*

ND

NO ND

'Opto IIO(JO'TlKOU Ilpo(J<>topt(Jf.10U MdM<>ou (LOQ)

(ppm)

0,01

0,01 0,05 0,01

ANIXNEYl:H IIOA YKYKAIK!!N AP!!MATIK!!N Y APOrONAN0PAK!!N l:TO

AIAA YMA ANAIIAHP!ll:Hl:

E<DAPMOZOMENH ANAA YTIKH TEXNIKH : A€pta Xpwf.!atoypa<pia- <Dacrf.!atof.!Ctpia Mal;ac; (Gas


Atmos L

ab

Finest Gree

k Eliquids

To 8uiAUJ.!U avanA.iJpwoTJ<; KAPNOS (Apt8J.!6<; I1ap-ri.8ac;:Oll KAPNOS 112) E~E-racr8YJKE yta 'tTJV

UVtXVEU<JTj 'tWV napaKU't(l) 1tOAUKUKAtKWV apWJ.!U'ttKWV u8poyovav8paKWV (PAHs), Tii.vaKa<; 3.

llivaKUS 3.

acenaphtylene

fluorene

phenanthrene

anthracene

pyrene benzo( a)anthracene

chrysene benzo(k)fluoranthene benzo(b )fluoranthene benzo(g,h,i )perylene

dibenzo( a,h )anthracene


AllOTEAEI:MATA

Opto lloGonKou l:l)yKEVTpiDGT) llpoG&toptGJlOU Mc06&o1)

(LOQ) (ppm) (ppm)

ND* 0,005

ND 0,010

ND 0,005

ND 0,006

ND 0,003 ND 0,003

ND 0,003 ND 0,060 ND 0,006 ND 0,014

ND 0,021 ND 0,022

*ND: ~£v avtxvd>811Kav noA.uKUKA.tKoi apcoJlanKoi uopoyovav8paK£<; cn)Jl<pcova !l£ -ra avacpcp6!1£va 6pta avixvcu<>ll<;-

Atmos L

ab

Finest Gree

k Eliquids

Atmos L

ab

Finest Gree

k Eliquids

ITANEITIL:THMI 0 KPHTHL: TMHMA IATPIKHL,


T.9. 2208 HpciKAuo KpquJ P.O.Box 2208 Heraklion Crete, Greece

EPfA.tTHPIO TO!IKOAOflAt Llu:uOuvTi)«;: KaOTIYTITTJ«; ApuJTt:L6ll«; M. TaaTaaKll«;

Tel +30 2810 394870, Fax +30 2810 542098 e-mail: [email protected] http://ctoxres.med.uoc.qr Epyam:~plO- m .. l')po¢>oplEc;: 2810 394687 - 394681 - 394794, Fax: +30 281 0 39 46 su~

IIII:TOIIOIHTIKO ANAA YI:HI:* KAI TASINOMHI:HI: TOY AIAA ANAIIAHP!!I:HI: MAXXX 18mg

ETAIPIA: ATMOS LAB

EMDOPIKH ONOMA.EIA YrPOY ANADAHP!l..EH.E: MAXXX 18mg

API0MO.E DAPTIAA.E: 02/ MAXXX 18mg/l2

DOIOTIKO.E DPO.EAIOPI.EMO.E AIAA YMA TO.E ANADAHP!l..EH.E E<l>APMOZOMENH ANA/\ YTIKH TEXNIKH: AEpto<; Xpffijlamypa<pia-<l>acrjla'tOjle'tpia Masas (Gas Chromatography -Mass Spectrometry) Kat **Yypi] Xpffijla-roypa<pia-<l>acrjla'tOjle-rpia Masas (Liquid Chromatography-Mass Spectrometry)

DO.EOTIKO.E DPO.EAIOPI.EMO.E MEXPI DO.EO.ETOY 99,9999%

llivaKa 1.

Ouaia

propylene glycol

glycerol

ethyl vanillin

nicotine


Ethyl maltol

water

.Ei>vol.o

ADOTEAE.EMA T A

noaoaT6 (o/ow/v)

68,77

28,91

0,004

1,6

0,214

0,010

0,4919

99,9999

Opto noaOTlKOU n poaO lOp lGJlOU ME96oou (LOQ)

( m)

0,198

1,187

0,032

0,1

0,121

0,135

~eV 'tU~tVOjlClLUt

~eV 'tU~tVOjlClLUt

O~eia m~tKO'tll'ta, ano cr-r6jla-ros, Ka-r1nopia 4 Epe8tcrjl6<; -rou bEpjlUTOS

(Ka-r1nopia 2) Epe8tcrjl6<; 'tffiV o<p8aAjlWV

(Ka'tllyopia 2) Et8t!d] 'tO~tKO'tll'tU <J'tU

6pyava cr-r6xou<;-e<pana~ EK8ecr11 (Kannopia 3) O~eia -ro~tKO'tll'ta 1 O~eia TO~tKO'tll'tU 3

Xp6vta -ro~tKO'tll'tU 2 cre u8p6~wus opyavtcrjlOUS

O~eia -ro~tKO'tll'ta, ano cr-r611a-ros, Kannopia 4

Atmos L

ab

Finest Gree

k Eliquids

·To EpyaoTijpto To~tKoA.oyiac; q>EpEt moTorroiT]<JT] <JlJjlq>WVCL jl£ TO ISO: 17025 ym nc; 8m8tKCL<Ji£c; rrapaA.api]c;, 8mxEipwTJc;, Kamypaq>i]c; Kill apx~:to8ETTJcrTJc; Twv 8~:tyll<iTwv Kill AEtToupyEi llE 8taKptPwllEvEc; cruoK~:ul;c; Kill 6pyava. ** H opyavoA.oyia LC-MS q>EpEt btCLKpipwoT] KCLTU ISO: 17025 jl£ rr£8io Eq>CLpjloyi]c; TTJV avixvcuoT] vapKWnKv oucrtffiv <JTT]V TPlXCL.

T ASINOMHI:H TOY YrPOY ANAllAHPQI:HI: MAXXX 18mg

M£ ~<icrll TllY AX.L 265/2002, <l>EK 1214/B'/19.9.2002, LllY m~tYOI!llGll TWY 1!£~-LOYW~-L~WY crucrmnKffiY TOU ~-LctY~-LUTO<; Kat ~<iG'Il TOU KaYOYtcr~!OD 1272/2008 (EK) TO MAXXX 18mg (Apt8~-L6<; ITapTiOa<;: 02/ MAXXX 18mg/12) 1-L£ 99,9999% cri>crTacrll7tOU aYa<p£p£tat crroY ITiYaKa 1, m~tvO~-L£hat m<; ~ill £mKiYOUYO yta TllY aY8pffimYll uyda, yta TO n£pt~aA.A.oY Kat ~-L£ ~<icrll Tt<; cpucrtKOXll~-LtK£<; rou t8t6tllt£<;. Emnp6cr8£ta, yta Tll XPTJGll rou 8taA.i>~-Lato<; aYanA.i)pmcrll<; an6 ro llA£KrpoYtK6 rmyapo, ro ~-LctY~-La £tcr1tV£6~-L£YWY ar11ffiY nou an£A.cu8cpffiY£mt XP£t<is£Tat ta~tYOI!llGll AU~!~UYOYLU<; U1t' 0\(/ll 'IllY f:KaTocrnaia cri>crracrll TWY UTI!WY 1tOU napayOYLat l!f: TllY f:YcpyonoillGll 'IOU 1-LllXUYtGI!OD U'I1!01t0lllGll<; ~i£XPt 1t£pt£KLtKO'Illta<; 0.1% ~~~ G£ l!f:I!OYW~-L£Yo crucrTattK6, Ka8ffi<; Kat tll cruyK£KPt~-L£Yll XPTJGll aurffiY.

ANIXNEYI:H NITPOZAMINQN I:TO AIAA YMA ANAllAHPQI:HI:

E<DAPMOZOMENH ANAA YTIKH TEXNIKH ** : Yypij XpcoJ.l.a'tOypaq>ia-<DacrJ.l.UTOJ.l.ETpia Mal;ac.; (Liquid



To 8taA.u11a aYanA.i)pwcrll<; MAXXX 18mg (Apt8~-L6<; I1apri8a<;:02/ MAXXX 18mg/12) £~£racr8llK£ yta 'IllY aYixvcucrll rmY napaKarm Ytrposa~-LtYffiY, ITiYaKa<; 2.

IlivaKUS 2.

AKpmVUf.UO


N -nitrosoanatabine N-ni trosoanabasine

ATIOTEAEI:MATA

'Opw llOO'OTlKOU l;l)yKEVTpffiO'll Tipoaowptaf.lOU

ME0000l) (LOQ) (ppm) (ppm)

ND* 0,01

ND 0,01

ND 0,05

ND 0,01

*NO: ~£V UVtXV£U8rjKUV vnpoi;UJ.l.LV£c; crUJ.l.(j>COVU J.l.E Til avaq>£p6p..cva 6pta UVLXV£UO"ll'.;·

ANIXNEYI:H TIOA YKYKAIKQN APQMATIKQN Y APOrONAN0PAKQN I:TO

AIAA YMA ANAllAHPQI:HI:

2

Atmos L

ab

Finest Gree

k Eliquids

E<l>APMOZOMENH ANAA YTIKH TEXNIKH : A£pta XproJ..Lawypa<pia- <l>aoJ..LU'tOJ..L£-rpia Mai;m; (Gas



To 8taA.u/-la avanA.iJpro011c; MAXXX 18mg(Apt8!-l6c; Ilap·ri8ac;:02/ MAXXX 18mg/12) E~Eni0811KE yta 't11V aviX,VED0"11 rrov napaKatro noA.uKUKA.tKrov apro/-lanKrov u8poyovav8paKrov (PAHs ), fHvaKac; 3.

IIivaKilS 3.

acenaphty1ene fluorene



chrysene benzo(k)fluoranthene benzo(b )fluoranthene benzo(g,h ,i )pery lene


AIIOTEAE:EMAT A

'Opto IIOGO'TlKOU !: UYKEVT pro Gfl IIpoGotoptGflOU MEOooou

(LOQ)

(ppm) (ppm)

ND* 0,005 NO 0,010 ND 0,005 ND 0,006 ND 0,003 ND 0,003 ND 0,003 ND 0,060 ND 0,006 ND 0,014 NO 0,021 ND 0,022

*NO: ~£V ClVtXV£U811K!lV 7tOAUKUKAtKOl aproJ..L!l-rLKOt ubpoyovav8paK£<; m)~L<pffiV!l f..L£ -ra ava<p£p0f..L£V!l 6pta aviXV£U011S·

()/;;-~ / AptoniOllS M. ToanHiKTJ.:; ·- - -~


Ka911Yllnl<; To;tKol.oyiac; I«TfHKou TfllJflllTO<;

L\u;o9uvn't.:; EpyaG't'Tipiou laTpOOtK«<rTlKrov EnlOT1JJlWV & Movaoac; To;tKoA.oyias;

3

Atmos L

ab

Finest Gree

k Eliquids

ITANEITIL.THMIO KPHTHL. TMHMA IATPIKHL:

T.e. 2208 HpciKAuo KpirtiJ



IHETOIIOIHTIKO ANAA YEH:E META AIIO :EYMIIYKNQ:EH * KAI TAEINOMH:EH:E EI:EIINEOMENOY ATMOY IIOY IIPOKYIITEI AIIO THN

ATMOIIOIH:EH YrPOY ANAIIAHPQ:EH:E MAXXX18mg

ETAIPIA: ATMOS LAB

EMDOPIKH ONOMA~IA YrPOY ANADAHPQ~H~: MAXXX 18mg

API0MO~ DAPTIAA~: 01/ MAXXX 18mg /12

IIOIOTIKO~ DPO~AIOPI~MO~ EI~DNEOMENOY ATMOY META ADO ~YMDYKNQ~H E<DAPMOZOMENH ANAA YTIKH TEXNIKH: A£ptoc; Xpffi~Lawypaq>ia-<Dacr!lcrroJ..LE-rpia Masac; (Gas Chromatography -Mass Spectrometry) KaL ··vypll Xpffi!lawypaq>ia-<Dacr!laTo!lETpia Masac; (Liquid Chromatography-Mass Spectrometry)

DO~OTIKO~ DPO~AIOPI~MO~ MEXPI IIO~O~TOY 99,97%

llivaKa 1.

propylene glycol

glycerol

nicotine


Ethyl vanillin

Ethyl maltol

water

~i>vol..o

ADOTEAE~MAT A

fioGOGT6 (%w/v)

66,58

24,96

1,6

0,265

0,005

0,014

6,55

99,97

Opto fiO!JO'TlKOU fipomStoplGf.lOU ME86&ou (LOQ)

( m)

0,198

I, 187

0,1

0,121

0,032

0,135

L'lEV TU~tVOJ..LELTaL

f..EV TU~tVO!lElTUl 0/;Eia to/;tKOtl]Ta I ,

0aVUll]q>OpO O"E E7IU(j>~ J..LE tO o£pJ..La

OI;Eia to/;tKOtl]ta 3, Tol;tK6 crE 1IEpi1ItWO"l] KUtU7IOOT]c; Xp6vta tol;tKOtl]Ta 2 crE uopopwus opyavtcrflOUc;

OI;Eia •ol;tKOtl]Ta an6 tou crt6J..Latoc;, Katl]yopia 4 EpE8tcrJ..L6c; tou o£pJ..Lawc;

(Katl]yopia 2) EpE8tcrJ..L6c; twv oq>8UAJ..LWV

(Katl]yopia 2) EtOtK~ tol;tKOtl]ta crta 6pyava

crtoxouc; -Eq>anas £K8EcrlJ (Kat yo ia 3)

0/;Eia to/;tKOtl]tU an6 tOU crt6J..Latos. Katl]yopia 4

• To Epyacrt~pto Tol;tKoA.oyiac; q>£pEt mcrwnoil]crl] crUJ..Lq>wva J..LE to ISO: 17025 yta nc; otaOtKacriEc; napaA.ap~c;. otaxEiptcrl]c;, Karaypaq>~c; Kat apxEto8£tl]crl]c; twv OEtyJ..Latwv Kat AEttoupyEi J..LE OtaKptPwJ..LtvEc; crucrKEu£c; Kat 6pyava.

Atmos L

ab

Finest Gree

k Eliquids

TAEINOMH~H TOY EI~IINEOMENOY ATMOY

ME ~acr11 'tTJV AXL 265/2002, <l>EK 1214/B'/19.9.2002 KOI 'tTJV -ra~tvO!lTJO"TJ -rrov !lE!lOYro!l£vrov crucr-ranKffiv -rou !lEiY!la-roc; ~acrEt -rou Kavovtcr!lOU 1272/2008 (EK), -ro !lEiY!la Et0"1tEO!lEVOU a-r!lOU nou npoKl>n-rEt an6 'tTJY a-r!l07tOtTJO"TJ uypou avanA.i)procrT]c; MAXXX 18mg (Apt8116c; I1apri8ac;: 01/ MAXXX 18mg/ 12), !lE crl>cr-racr11 99,97% 6nroc; ava<p£pE-rat cr-rov IlivaKa 1, -ra~tYO!lEhat roc; noA.u 'tO~tKO (T +) O"E 1tEpimrocrTj EJta<pi)c; !lE 'tO 8£p11a Kat roc; E1tt~Aa~£c; (Xn) O"E 1tEpin-rrocrTj Ka'tU1tOO"T]c;.

ANIXNEY~H NITPOZAMIN!!N ~TON EI~IINEOMENO ATMO META AIIO

~YMIIYKN!!~H

E<l>APMOZOMENH ANAA YTIKH TEXNIKH ** : YypiJ Xpwflatoypacpia-<l>acrflato~Lc'tpta Ma/;a~ (Liquid


ANIXNEYOMENE~ OY~IE~

0 Etcr1tVEO!lEvoc; a-r116c; nou npoKl>mEt an6 1TJV a-rllonoiT]crTJ uypou avanA.i)procrTJc; MAXXX 18mg (Apt8!l6c; I1ap-ri8ac;:Ol/ MAXXX 18mg 112) E~E-racr8T]KE yta 1TJV aviX,VEUO"TJ -rrov napaKa-rw vnposa!ltvffiv, IlivaKac; 2.

IHvaKas 2.

AKpffiVllJllO

4-(Meth ylnitrosamino )-1-(3-pyridyl)-1-butanol 4'-(nitrosomethylarnino )-1-(3-pyridyl)-1-butanone


AIIOTEAE~MATA

(ppm)

ND*

ND ND ND

'Opto Ilo«JOTlKOll Ilpom)topt«JJlOll Mc06()ou (LOQ)

(ppm)

0,01

0,01

0,05 0,01

ANIXNEY~H IIOA YKYKAIK!!N AP!!MA TIK!!N Y APOrONAN0PAK!!N ~TON

EI~IINEOMENO ATMO MET A AIIO ~YMIIYKN!!~H

E<l>APMOZOMENH ANAA YTIKH TEXNIKH : A£pta Xpw~tatoypacpia- <l>acrf.!atoflc'tpta Mal;a~ (Gas


2

Atmos L

ab

Finest Gree

k Eliquids

0 ctcr7tVc6J..LcVoc; a-rJ..L6c; 1tou 1tp01c6mct a1t6 TTJV aTJ..l01tOillcr11 uypou ava1tA.ijprocrlls MAXXX 18mg (Apt8J..L6c; ITap-ri8ac;:Oll MAXXX 18mg 112) c~c-racr811Kc yta TTJV avixvcucr11 -rrov 7tapaKa-rro 1tOAUKUKAtKffiv aproJ..LanKffiv u8poyovav8paKrov (PAHs ), ITivaKac; 3.

llivaKUS 3.

AKpOOVUJUO

acenaphtylene

fluorene phenanthrene

anthracene pyrene

benzo(a)anthracene

chrysene benzo(k)fluoranthene benzo(b )fluoranthene

benzo(g,h,i )perylene


AIIOTEAE:EMA T A

OplO IIOO'OTlKOU :EuyKEV'TpOOO'll IIpoO"owptO"Jloil MEOooou

(LOQ) (ppm) {ppm)

ND* 0,005

NO 0,010

ND 0,005

ND 0,006 ND 0,003 ND 0,003

NO 0,003 ND 0,060 ND 0,006 ND 0,014

ND 0,021 ND 0,022

*NO: Ll£V UVtXV£U811KUV 7tOAUKUtcAtKOt a.pCO)..lUTtKOt uopoyovav8pa.K£t; <JU)..l<j>COVU ~L£ TU UVU<p£pO~L£VU 6pta.

UVtXV£U<J11S·

Ka0TtYTJnl~ To;tKol.oyia~ IUTfHKou TJ..LiiJ.laToc:;

~uru9uvn')c:; Epya<J'Tl"'piou laTpOOlK«O"TtKrov E7tlO'TllflWV & Movaoa~ To;tKoA.oyiac:;

3

Atmos L

ab

Finest Gree

k Eliquids

Atmos L

ab

Finest Gree

k Eliquids

UNIVERS11Y OF CRETE MEDICAL SCHOOL

T.e. 2208 HpciKA&to Kpirtq P.O.Box 2208 Heraklion Crete, Greece

EPfAiTRPlO TO!lKOA.OflAi Llu:u0uvn1<;: KaOrrYTJTTJ<; ApuJT£L6T)<; M. TaaTaaKT)<;

,. Tel +30 2810 394870, Fax +30 2810 542098 e-mail: [email protected] http://ctoxres.med.uoc.qr Epyacn:~plO- nf..rlPo¢oplE<;: 2810 394687 · 394681· 394794, Fax: +30 281 0 39 46 SHl

lliETOllOIHTIKO ANAA Yl:H:E* KAI TASINOMHl:Hl: TOY AIAA ANAIIAHP!l:EHl: RY69 18mg


EMDOPIKH ONOMAEIA YrPOY ANAllAHPQEHE: RY69 18mg

API0MOE IIAPTI~AE: 011 RY69 18mg/12

IIOIOTIKOE IIPOE~IOPIEMOE ~IAA YMA TOE ANAIIAHPQEHI: E<l>APMOZOMENH ANA/\ YTIKH TEXNIKH: A£pta<; XpCDJla'toypa<pia-<l>acrJla'tOJle'tpia Masa<; (Gas Chromatography -Mass Spectrometry) Kat **YypfJ XpCDJla'toypa<pia-<l>acrJla'toJ.!E•pia Masas (Liquid Chromatography-Mass Spectrometry)

IIOI:OTIKOI: IIPOI:~IOPII:MOI: MEXPI IIOI:OI:TOY 99,9999%

IlivaKas 1.

OuGia

propylene glycol

glycerol

ethyl vanillin

Ethyl maltol


nicotine

water

I:uvolo

AIIOTEAEI:MAT A

00GOGTO (o/ow/v)

64,86

29,94

0,006

0,585

0,425

1,7

2,4839

99,9999

Upto floGonKou flpoGotoplGI.lOU Mt96ooll (LOQ)

( m)

0,198

1,187

0,032

0,135

0,121

0,1

!lev w~tVOJ.!Ehat

fleV 'tU~tVOJ.!ElLClt

O~eia 'tO~tK6nrra, ano cr'tOJla'tO<;, Ka'tT)yopia 4 Epe8tcrJ.!OS 'tOU bEpJlU'tO<;

(KanJYopia 2) Epe8tcrJlOS 'tCDV o<p8aAJlcOV

(Ka'tT)yopia 2) Et8tKTj 'tO~tKOTT)'tU O""CU

6pyava O'tOXOU<;-e<pana~ £K8e<Yl] (Kanwopia 3) O~cia 'tO~tKOTTJ'tU, ano cr't6Jla't0s, Kanwopia 4

!lev 'ta~tVOJ.!Ehat

O~cia 'tO~tKOTTJ'tU I O~eia 'tO~tKOTTJ'ta 3

Xp6vta 'tO~tK6ntw 2 cre u8p6pwus opyavtcrJlous

Atmos L

ab

Finest Gree

k Eliquids

·To Epyacrn)pto To~tKoA.oyiac; <p£p£t mcrT07WtTJ<J'l m)~<pwva ~£TO ISO: 17025 yta nc; 8ta8tKacri£c; napaA.ap~c;, 8tax£iptc:rTJc;, Kamypa<p~c; Kat apx£to9£TTJ<JTJc; rwv 8£ty~arwv Kat A£tmupy£i ~£ 8taKptPw~£v£c; crucrK£Utc; Kat 6pyava. •· H opyavoA.oyia LC-MS q>EpEt 8taKpipwcr'l Kara ISO: 17025 ~£ n£8io £<pap~oy~c; TTJV avixv£U<JTJ vapKwnKwv oucrtwv <JTTJV Tpixa.

TASINOMH1:H TOY YrPOY ANAIIAHP.Q1:H1: RY69 18mg

Me ~acrT) TT)V AXL 265/2002, <DEK 1214/B'/19.9.2002, TT)V -ra~tvO!!T)<JT) Tcov !!E!!OVCO!!Evcov <rucrTanKrov TOU !!ctY!!UToc; Kat ~acrT) TOU Kavovtcr!!OD 1272/2008 (EK) TO RY69 18mg (Apt8!!6c; ITapTi8ac;: 01/ RY69 18mg/12) !!E 99,9999% crDcrTacrT) 1rou avacp£pETat crTOV ITivaKa 1, TU~lVO!!Ehat coc; !!11 E1tlKtVbUVO yta TT)V av8pffimVT) uycia, yta TO 1tcpt~UAAOV Kat !!E ~U<JT) nc; q>UcrtKOXT)!!lKEc; TOU tbtOTT)Tcc;. Em1tp6cr8ETa, yta TT) XPTJ<JT) TOU 8taAD!!UToc; ava1tATJpCOcrT)c; a1t6 TO T)AEKTpOVlKO Tcrtyapo, TO !!clY!!U El<J1tVEO!!EVCOV UT!!WV 1tOU U1tEAEU8cpcOVELal XPEtasE-rat TU~lVO!!T)<JT) AU!!~UVOV-rac; U1t' 0\j/T) TT)V EKUTO<JTtata <JU<JLU<JT) TCOV UT!!WV 1tOU 1tapayOVTat !!E TT)V EVEpyo1tOtT)<JT) TOU !!T)XUVtcr!!OD UT1!01tOtT)<JT)c; !!EXPl1tcplEKTtKOTT)TUc; 0.1 o/o ~~~ <JE !!E!!OVCO!!EYO crucrTanK6, Ka8roc; Kat TT) ouyKEKPt!!EVT) XPiJcrTt auTv.

ANIXNEY1:H NITPOZAMIN.QN 1:TO L\IAA YMA ANAIIAHP.Q1:H1:

EAPMOZOMENH ANAAYTIKH TEXNIKH ** : Yyp11 XpcoJ.La:roypacpia-<l>acrJ.La-roJ.L£Tpia Masac; (Liquid


ANIXNEYOMENE1: OY1:IE1:

To 8taA.u!!a ava7tA.ijpcocrT)c; RY69 18mg (Apt8!!6c; ITapTi8ac;:Oll RY69 18mg/12) E~ETacr8T)KE yta TT)V avixvcucrT) Tcov 7tapaKaTco vtTposa!!tvrov, ITivaKac; 2.

llivaKClS 2.

AKpO>vU~lO

4-(Methylnitrosarnino )-1-(3-pyridyl)-1-butanol 4'-(nitrosomethylamino )-1-(3-pyridyl)-1-butanone


AIIOTEAE1:MAT A

(ppm)

ND*

ND

ND

ND

'Opw IloaOTlKOU Ilpoa(hopta~ou

Mc96()ol) (LOQ) (ppm)

0,01

0,01

0,05 0,01

ANIXNEY1:H IIOA YKYKAIK.QN AP.QMA TIK.QN Y L\POrONAN0P AK.QN 1:TO

L\IAA YMA ANAIIAHP.Q1:H1:

2

Atmos L

ab

Finest Gree

k Eliquids

E<l>APMOZOMENH ANAAYTIKH TEXNIKH: Af:pta Xpwf..La·wypa<pia- <l>acrJ..LaTOJ..LE-rpia Masac; (Gas


ANIXNEYOMENE:E OYEIE'E

To 8taAU!la avanA.flprocrT]<; RY69 18mg(Apt8!l6<; I1apTi8a<;:Ol/ RY69 18mg!l2) £~£Tacr8T]K£ yta TT]V avixvcucr11 Trov napaKaTro noA.uKUKAtKmv apro!laTtKmv u8poyovav8paKrov (PAHs), ITivaKa<; 3.

llivaKUS 3.

AKprovi>t.uo





dibenzo(a,h)anthracene indeno( 1 ,2,3-CD )pyrene

ATIOTEAE:EMA T A

Opw TioaonKoi> l:uyKEVTpOO<Jfl Tipoa~wpt<JflOU Mt96~ou

(LOQ)

(ppm) (ppm)

ND* 0,005 ND 0,010 ND 0,005 ND 0,006 ND 0,003 ND 0,003 NO 0,003 ND 0,060 NO 0,006 ND 0,014 ND 0,021 ND 0,022

*ND: ~EV UVtXVEU8TJKUV 7tOAUKUKAtKOt apWf..LU'ttKOi uopoyovav8paKE<; GUJ..L<pffiVU f..LE -ra ava<pEpOJ..LEVU 6pta aviXVEUcrTJc;.

0 ~1cu8uvn')c; "COU .Epy. · piou, /

----

&/~/ / ' \ <_:·<13

/ ApLoTdO'IS M. ToaT<f(iKflc;;·, '--,


Ka911Y'InlS To~lKol.oyiac; laTplKou Tf.LTJJlflToc;;

~u:l)&u\•Tftc; EpyaOTflp{ol) laTpOOLKCIOTlKcilv EnlOTflf!IDV & Movaoac; To;tKoJ.oyia;

3

Atmos L

ab

Finest Gree

k Eliquids

ITANEITII:THMIO KPHTHI: TMHMA IATPIKHL.

T.9. 2208 HpciKAEto KpiJul



DII:TODOIHTIKO ANAA YI:HI: MET A ADO I:YMDYKN!!I:H * KAI T ASINOMHI:HI: EII:DNEOMENOY ATMOY DOY DPOKYDTEI ADO THN

ATMODOIHI:H YrPOY ANADAHP!!I:HI: RY6918mg

ETAIPIA: ATMOS LAB

EMllOPIKH ONOMAI:IA YrPOY ANATIAHPQI:HI:: RY69 18mg

API0MOI: llAPTIAAI:: 01/ RY69 18mg /12

llOIOTIKOI: llPOI:AIOPII:MOI: EII:llNEOMENOY A TMOY MET A AllO I:YMllYKNQI:H E<DAPMOZOMENH ANA/\. YTIKH TEXNIKH: A£pwc; XpcoJ.la'tOypa<pia-<DacrJ.lU'tof.lETpia Masac; (Gas Chromatography -Mass Spectrometry) Kat ''Yypi] Xpco~ta-roypa<pia-<DacrJ.lU'tOf.lETpia Masac; (Liquid Chromatography-Mass Spectrometry)

llOI:OTIKOI: llPOI:AIOPII:MOI: MEXPI llOI:OI:TOY 99,97%

llivaKa 1.

Oua(a

propylene glycol

glycerol

nicotine


Ethyl vanillin

Ethyl maltol

Water

I:uvol..o

AllOTEAEI:MA TA

noaO<JTO (o/ow/v)

66,66

28,08

1,4

0,387

0,006

0,499

2,94

99,97

OplO noaOTlKOU n poaowptaflOU Me86oou (LOQ)

( m)

0,198

1,187

0,1

0,121

0,032

0,135

Ac:v -ra~tVOJ.lEhat

Ac:v TU~tVOf.lEhat

OI;Eia tol;tK6tT]TU I , 8avatT]<p6po <JE f:7t(l<p~ f.LE tO Of:pf.La

Ol;c:ia tol;tK6tT]TU 3, Tol;tK6 crc: 7rEpi7rtW<JT] KUtU7rO<JT]<;

Xp6vta tO/;tKOtT]tU 2 ()f: uop6pwuc;

OI;Eia tol;tK6tT]TU an6 tou crt6f.Latoc;, KatT]yopia 4 Epc:9tcrf16c; tou oEpf.Latoc;

(KatT]yopia 2) Epc:9tcrf16c; twv o<p9aA.wi>v

(KatT]yopia 2) EtotK~ to/;tKOtT]tU crm 6pyava

crt6xouc;-c:<panas EK9E<JT], MnopEi VU 7rpOKUAE<JEl EpE9t<Jf10 <JtT]V

UVU7rV01 (Katl)yopia 3) Ol;c:ia to/;tK6tT]tU an6 tou

crt6f!UtOS, KatT]yopia 4

' To Epyacrt~pto Tol;tKoA.oyiac; <ptpc:t mcrtonoiT]<JTJ crUf.L<pwva f.LE to ISO: 17025 yta nc; otaotKacric:c; napaA.ap~c;, otaxEiptmlc;, Kataypa<p~c; Kat apxc:to9EtT]<JT]<; tWV OElYf!UtWV Kat AEttoupyEi f.LE OlUKptPWf!EvE<; <JU<JKEUE<; Kat 6pyava.

Atmos L

ab

Finest Gree

k Eliquids

TASINOMH:EH TOY EI:ETINEOMENOY ATMOY

ME ~U<Jll TllV AXL 265/2002, <l>EK 1214/B'/19.9.2002 KOI TllV TU~tvOflll<Jll TroY f.!Ef.!OVrof.!EVrov OU<JTUTtKWV TOU f.!ElYflUTOc; ~a<JEt TOU Kavovt<Jf.!OU 1272/2008 (EK), TO f.!Etyfla Et<J1tVEOf.!EVOU UTflOU nou np01c6n-rEt an6 T'llV UTfl07tOtll<Jll uypou avanA.iJprocrllc; RY 69 18mg (Apt8f.!6c; I1ap-ri8ac;: 011 RY69 18mg/12), f.!E crucrmcr11 99,97% 6nroc; ava<p£pETat cr-rov ITivaKa 1, -ra~tVOf.!Ehat roc; no/..u TO~tKO (T +) <JE 7tEpt7tTro<Jll Ena<.pftc; f.!E TO 8£pfla Kat roc; E7tt~Aa~£c; (Xn) <JE 1tEpin-rrocr11 KUTU7t0<Jllc;.

ANIXNEY:EH NITPOZAMIN!!N :ETON EI:ETINEOMENO ATMO META ATIO :EYMTIYKN!!:EH E<l>APMOZOMENH ANAA YTIKH TEXNIKH ··: Yyp1) XpwJlaTOypa<pia-<l>acrJlaTOflETpia Mal;;a<; (Liquid



0 Et<J1tVEOf.!Evoc; a-rf.!6c; nou nporimEt an6 TllV aTf.!07tOtll<Jll uypou avanA.iJprocrllc; RY69 18mg (Apt8f.!6c; I1ap·d8ac;:Ol/ RY69 18mg /12) E~E-racr811KE yta TllV avixvwcr11 -rrov napaKa-rro vnposaf.!tvffiv, ITivaKac; 2.

IltVClKClS 2.


N-ni trosoanatabine

N -nitrosoanabasine

ATIOTEAE:EMAT A

(ppm)

ND*

ND

ND

ND

'OplO floGO'tlKOU UpoG()wptGJ.lOU ME9o()ol) (LOQ)

(ppm)

0,01

0,01 0,05 0,01

*ND: ~ev avtxveu8l]Kav vt-rpo/;;af.liV£<; crUJl<pCDva ~L£ -ra ava<pep6fl£Va 6pta avix;veuml<;·

ANIXNEY:EH UOA YKYKAIK!!N AP!!MATIK!!N Y APOrONAN0PAK!!N :ETON

EI:EUNEOMENO ATMO MET A ADO :EYMUYKN!!:EH

E<l>APMOZOMENH ANAA YTIKH TEXNIKH : A£pta XpCDJla-roypa<pia- <l>acrJlUTOflETpia Ma/;;a<; (Gas



0 EtcrnvEOf.!EVoc; a-rf.!6c; nou nporinTEt an6 TllV aTf.!07tOtll<Jll uypou avanA.iJprocrllc; RY69 18mg (Apt8f.!6c; I1ap-ri8ac;:O 11 RY69 18mg I 12) E~E-racr811KE yta TllV avixvwcr11 -rrov napaKa-rro noA.uKUKAtKffiv aprof.!anKffiv u8poyovav8paKrov (PAHs), ITivaKac; 3.

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TiivaKaS 3.

AKpO>VVf.llO






ATIOTEAEI:MAT A

'OplO llO<JO'TlKOV l:lY'fKEV'tpO><JT) Tipo<J&wpt<Jf.lOil MtOo&ou

(LOQ)

(ppm) (ppm)


*ND: ~EV UVlXVEU811KUV 1tOAUICU1CAlKOi apCOI!UTlKOi uopoyov6.v8paK£~ OUI!<f>COVU 1-LE La avacpEp011£VU 6pta avi:XVEUOll~·

~»~~/ .- / . 1- ,

/ '. '-...'0':]

/ Apto't'£l01}<; M. TociToaK1}.; '·---~- ___;__.--'


Ka01)Y1}n\<; To~lKoJ..oyiac; laTplKOU TJ..Lt\J..LaTo<;

t:\u:1)9'U\'Tit<; Epy«O't'T)piou laTpOOLK«O't'tKrov E1tlOT1)J1WV & Movaow; To;ucoA.oyiac;

3

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ab

Finest Gree

k Eliquids

Atmos L

ab

Finest Gree

k Eliquids

IIANEIIIl:THMI 0 KPHTHl: TMHMA IATPIKH~


T.e. 2208 HpaKAuo Kpircq P.O.Box 2208 Heraklion Crete, Greece

EPfA~THPlO TO:tUtOAOflA~

Llu:uOuvTft<;: Ka01JYTITTt<; AptaTEL6T)<; M. TaaTaUKT)<; Tel +30 2810 394870, Fax +30 2810 542098 e-mail: aris(Q)med.uoc.ar http://ctoxres.med.uoc.qr

Epyam:~plO - nXr)po<(>oplE<;: 2810 394687 - 394681- 394794, Fax : +30 281 0 39 46 RR

TilETOTIOIHTIKO ANAA Y:EH:E* KAI TAEINOMH:EH:E TOY AIAA ANATIAHPQ:EH:E MINT 18mg

ETAIPIA: ATMOS LAB

EMTIOPIKH ONOMAI:IA YrPOY ANAIIAHPQI:HI:: MINT18mg

API0MOI: IIAPTIL\AI:: 01/ MINT 18mgll2

IIOIOTIKOI: IIPOI:I\IOPII:MOI: 1\IAA YMA TO I: ANAIIAHPQI:HI: E<l>APMOZOMENH ANA/\ YTlKH TEXNIKH: A£pto<; XpwJ..lawypa<pia-<l>aoJ..laWJ..lETpia Masa<; (Gas Chromatography -Mass Spectrometry) Kat .. YypiJ XpwJ..lawypa<pia-<l>ao~LUWJ..lETpia Masa<; (Liquid Chromatography-Mass Spectrometry)


IlivaKas 1.

Ouaia

propylene glycol

glycerol

nicotine

water

I:uvoA.o

AIIOTEAEI:MA T A

Ooao1no (%w/v)

47,66

49,78

1,8

0,759

99,999

Upto noaOTtKOU npoaowptaJ.tOil ME96oou (LOQ)

( m)

0,198

1 '187

0,1

~EV LU~tVOJ..lElLUl

~EV TU~tvOJ..lElLUt

O~Eia -ro~tKOTI]LU 1 O~Eia -ro~tKOTI]LU 3

Xp6vta -ro~tKOTI]LU 2 o£ u8p6~wus opyavtoJ..lous

• To Epycwr~pw Tol;tKoA.oyiac; q>i:pEtnt<nonoiT]<HJ <JD!lq>mva !-IE ro ISO: 17025 yw nc; 8ta8tKacriEc; napaA.a~~c;, 8taxEiptcrT]c;, Karaypaq>~c; Kat apxEw8i:rT]crT]c; rcov 8Ety!larmv Kat A.EtroupyEi !!E 8taKpt~m!1i:vEc; crucrKrni:c; Kat 6pyava. •• H opyavoA.oyia LC-MS q>i:pEt 8taKpi~mcrl] Kara ISO: 17025 !!E nE8io Eq>ap!loy~c; TT]V avi;zyrncrl] vapKmnKwv oucrtwv crr11v rpixa.

Atmos L

ab

Finest Gree

k Eliquids

TASINOMH~H TOY YrPOY ANAIIAHP!l~H~ MINT 18mg

ME pacrYJ -rYJv AXI: 265/2002, <DEK 1214/B'/19.9.2002, -rYJv -ra~tv61!YJO"TJ -row 1-LEI!OVffii!EVffiv crucr-ranKrov mu I!ElYI!amc; Kat pacrYJ mu Kavovtcr11ou 1272/2008 (EK) m MINT 18mg Apt9~-L6<; ITap-rioac;: 011 MINT 18mg /12) 1-LE 99,999% <JUcr-racrYJ 1tou avacp£pE-rat crmv ITivaKa 1, 'ta~tvOI!Ehat ffi<; 1-LTJ E7tlKlVOUVO yta 'tT]V av9pc07ttVYJ uyEia, yta 'tO 7tEptpaAAOV Kat 1-LE pacrYj n<; cpucrtKOXYJI!lKE<; -rou tot6'tT]-rE<;. Em7tp6cr9E-ra, yta 'tTJ XPll<JT] mu otaAUI!a-ro<; ava7tAllPffi<JT]<; a1t6 -ro YJAEK'tpOVlKO -rmyapo, 'tO ~!ElYI!U El<J7tVE01!EVffiV U'tl!cOV 7tOU U7tEAEU9EpcOVE'tal XPElUSE'tat -ra~tvOI!TJO"TJ Aai!P<ivov-rac; u1t' O\j/TJ 'tTJV EKamcrnaia crucr-racrYJ -rffiv a-r11rov 1tou 7tapayov-rat 1-LE 'tTJV EVEpyo7tOtT]<JT] mu 1-LYJXUVt<J~-LOU a-ri!07tOtT]<JT]<; 1-LEXPt 7tEptEKnK6-rYJ-ra<; 0.1% PIP <JE 1-LEI!OVffii!EVO crucr-ranK6, Ka9roc; Kat •TJ cruyKEKPt~-LEVYJ XPllO"TJ au-rrov.

ANIXNEY~H NITPOZAMIN!lN ~TO AIAA YMA ANAIIAHP!l~H~

E<DAPMOZOMENH ANAAYTIKH TEXNIKH ** : YypfJ Xpffi~a:roypacpia-<Dacr~aTo~£Tpia Mu~ac; (Liquid


ANIXNEYOMENE~ OY~IEI:

To otaAulla ava7tAllPffi<JT]<; MINT 18mg (Apt9~-L6<; ITap-rioac;:Ol/ MINT18mg /12) E~E-racr9YJKE yta TTJV aviXVED<JTJ -rffiv 7tapaKa-rffi vnposalltvrov, ITivaKa<; 2.

lltVUKUS 2.

4-(Meth ylnitrosamino )-1-(3-pyridyl)-1-butanol 4'-(nitrosomethylamino )-1-(3-pyridyl)-1-butanone N-nitrosoanatabine N-nitrosoanabasine

AIIOTEAE~MATA

(ppm)

ND*

ND ND ND

Dpw IloGOTlK01) IlpoG~iloptGJ!OU

M~:Oo()ou (LOQ) (ppm)

0,01

0,01 0,05 0,01

ANIXNEY~H IIOA YKYKAIK!lN AP!lMATIK!lN Y APOrONAN0PAK!lN ~TO

AIAA YMA ANAIIAHP!l~H~

E<DAPMOZOMENH ANAA YTIKH TEXNIKH: A£pta XpffiJ..tmoypacpia- <Dacr~aTo~£Tpia Mu~ac; (Gas


2

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To ouiA.ufla avanA.ftpwcrrJ<; MINT 18mg (Apt8fl6<; ITap-rioac;:Ol/ MINT 18mgl12) E~E-racr8TJKE yta 'rl]V aviXVEDGT] 'r(J)V napaKU'r(J) TCOAUKUKAtKWV apWflUTtKWV uopoyovavepaKWV (PAHs), ITivaKa<; 3.

llivaKas 3.


phenanthrene

anthracene pyrene

benzo(a)anthracene



indeno( 1 ,2,3-CD )pyrene

AIIOTEAEI:MA T A

'Opto IloaO'TlKOU l;l)yKEV'TpOOGll Ilpoa(hoptGf.lOU Mt960o1)

(LOQ) (ppm) (ppm)

ND* 0,005 NO 0,010

NO 0,005

ND 0,006 ND 0,003 ND 0,003

ND 0,003 ND 0,060 ND 0,006 ND 0,014

NO 0,021 ND 0,022

*ND: ~ev avtxveu811Kav noA.uKUKAtKoi apw~LanKoi u8poyovav8paK£<; cru~L<pwva ~£ m ava<pep6~va 6pta avixvwcr11<;.

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ab

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ab

Finest Gree

k Eliquids

Atmos Lab's Eliquid Analysis 10/2012 GR

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Transcript of Atmos Lab's Eliquid Analysis 10/2012 GR