Atmos Lab's Tobacco Flavour Analysis EN
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Transcript of Atmos Lab's Tobacco Flavour Analysis EN
IIANEHil:HIMION 0EI:I:AAIAI: TMHMA BIOXHMEIAI: & BIOTEXNOAOrJAE HAOYT!!NOE 26 41221 AAPIEA
THAIFAX. (2410) 565277/90 Email: [email protected] ATJ!JtiTPTJ~ Kouptm~ Ku01Jy,Ttj~
UNIVERSITY OF THESSAL Y BIOCHEMISTRY & BIOTECHNOLOGY DEPT
PLOUTONOS 26 LARISSA, 41221-GREECE
TEL/FAX. (302410) 565277/90 Email: [email protected]
Demetrios Kouretas Professor
CERTIFICATE OF ANALYSIS AND CLASSIFICATION OF AGRINIO
COMPANY: ATMOS LAB COMMERCIAL NAME OF THE PRODUCT: AGRINIO TOTAL NUMBER: 01/AGRINIO 112
ANALYSIS (Gas Chromatography -Mass Spectrometry and Liquid Chromatography-Mass Spectrometry)
RESULTS
table 1.
percentage Limit of analysis
substance (%w/v) (LOQ) classification ( m)
propylene glycol 3,21 0,198 no
glycerol 83,59 1,187 no
water II ,6997 Acute toxicity 1
nicotine 1,5 0,1 Acute toxicity 3
Chronic toxicity 2 in aquatic organisms
total 99,9997
Classification of the liquid Agrinio
According to Greek regulation ( FEK 1214/B'/19.9.2002), classification of particular ingredients of the mixture and according to EU Regulation 1272/2008 this product with 99.9991% composition, is classified as non hazardous for human health, environment and according to its physicochemical properties.
NYTROZAMINE ANALYSIS
(Liquid Chromatography -Mass Spectrometry)
table 2. name
4-(Methylnitrosamino )-1-(3-pyridyl)-1-butanol 4'-(nitrosomethylamino )-1-(3-pyridyl)-1-butanone N-nitrosoanatabine N-nitrosoanabasine
RESULTS
concentration (ppm)
ND*
ND ND ND
(LOQ) (ppm)
0,01
0,01 0,05 0,01
POLYCYCLIC AROMATIC HYDROCARBONS (PAHs) ANALYSIS
(Gas Chromatography -Mass Spectrometry)
RESULTS
table 3. name Concentration (LOQ)
(ppm) (ppm)
acenaphtylene ND* 0,005 fluorene ND 0,010
phenanthrene ND 0,005 anthracene ND 0,006
pyrene ND 0,003 benzo(a)anthracene ND 0,003
chrysene ND 0,003 benzo(k)fluoranthene ND 0,060 benzo(b )fluoranthene ND 0,006 benzo(g,h,i)perylene ND 0,014
dibenzo(a,h)anthracene ND 0,021 indeno( 1 ,2,3-CD)pyrene ND 0,022
Demetrios Kouretas, PhD
Professor
Biochemical Toxicology
DANEnn:ntMION 0EI:I:AAIAI: TMHMA BIOXHMEIAI: & BIOTEXNOAOrlAI: DAOYTflNOI: 26 41221 AAPII:A
THA/FAX. (2410) 565277/90 Email: [email protected] AqJ.niTPil~ KouptTa~ KaO,yljTij~
UNIVERSITY OF THESSAL Y BIOCHEMISTRY & BIOTECHNOLOGY DEPT
PLOUTONOS 26 LARISSA, 41221-GREECE
TEL/FAX. (302410) 565277/90 Email: [email protected]
Demetrios Kouretas Professor
CERIFICATE OF ANALYSIS AND CLASSIFICATIONS OF APACHE
COMPANY: ATMOS LAB COMMERCIAL NAME OF THE PRODUCT: APACHE TOTAL NUMBER: 011 APACHE 112
ANALYSIS (Gas Chromatography -Mass Spectrometry and Liquid Chromatography-Mass Spectrometry)
RESULTS table 1.
substance persentage
Limit of analysis (LOQ)
( m)
propylene glycol
glycerol
water
nicotine
total
Classification of the liquid Apache
(%w/v)
4,05
84,93
9,7144
1,3
99,9944
0,198
I ,187
0,1
classification
no
no
Acute toxicity 1 Acute toxicity 3
Chronic toxicity 2 in aquatic organisms
According to Greek regulation ( FEK 1214/B'/19.9.2002), classification of particular ingredients of the mixture and according to EU Regulation 1272/2008 this product with 99.9991 % composition, is classified as non hazardous for human health, environment and according to its physicochemical properties.
NYTROZAMINE ANALYSIS
(Liquid Chromatography -Mass Spectrometry)
table 2. name
4-(Methylnitrosamino )-1-(3-pyridyl)-1-butanol 4'-(nitrosomethylarnino )-1-(3-pyridyl)-1-butanone N -nitrosoanatabine N -nitrosoanabasine
RESULTS
concentration (ppm)
ND*
ND
ND ND
(LOQ) (ppm)
0,01
0,01 0,05
0,01
POLYCYCLIC AROMATIC HYDROCARBONS (PAHs) ANALYSIS
(Gas Chromatography -Mass Spectrometry)
RESULTS
table 3. name conentration (LOQ)
(ppm) (ppm)
acenaphtylene ND* 0,005
fluorene ND 0,010 phenanthrene ND 0,005
anthracene ND 0,006 pyrene ND 0,003
benzo(a)anthracene ND 0,003
chrysene ND 0,003 benzo(k)fluoranthene ND 0,060 benzo(b )fluoranthene ND 0,006
benzo(g,h,i)perylene ND 0,014 dibenzo(a,h)anthracene ND 0,021
indeno( 1 ,2,3-CD )pyrene ND 0,022
Demetrios Kouretas, PhD
Professor
Biochemical Toxicology
nANEnt:!:::TIIMION 0EI:I:AAIAI: TMHMA BIOXHMEIAI: & BIOTEXNOAOriAI: nAOYT!!NOI: 26 41221 AAPII:A
TIIAIFAX. (2410) 565277/90 Email: [email protected] Al]lliJTP'l~ KouptTU~ Ka01]y1JT1~
UNIVERSITY OF THESSAL Y BIOCHEMISTRY & BIOTECHNOLOGY DEPT
PLOUTONOS 26 LARISSA, 41221-GREECE
TEL/FAX. (302410) 565277/90 Email: [email protected]
Demctrios Kouretas Professor
CERTIFICATE OF ANALYSIS AND CLASSIFICATON OF BARBARA
COMPANY: ATMOS LAB COMMERCIAL NAME OF THE PRODUCT: BARBARA TOTAL NUMBER: OJ/BARBARA /12
ANALYSIS (Gas Chromatography -Mass Spectrometry and Liquid Chromatography-Mass Spectrometry)
table 1.
substance
propylene glycol
glycerol
water
nicotine
total
RESULTS
percentage (%w/v)
3,67
80,19
15,0376
1,1
99,9976
Limit of analysis (LOQ) ( m)
0,198
I ,187
0,1
Classification of the liquid Barbara
classification
no
no
Acute toxicity 1 Acute toxicity 3
Chronic toxicity 2 in aquatic organisms
According to Greek regulation ( FEK 1214/B'/19.9.2002) , classification of particular ingredients of the mixture and according to EU Regulation 1272/2008 this product with 99.9991 % composition, is classified as non hazardous for human health, environment and according to its ph ysicochernical properties.
NYTROZAMINE ANALYSIS
(Liquid Chromatography -Mass Spectrometry)
RESULTS
table 2. name concentration (LOQ)
(ppm) (ppm) 4-(Methylnitrosamino )-1-(3-pyridyl)-1-butanol ND* 0,01 4'-(nitrosomethylamino )-1-(3-pyridyl)-1-butanone ND 0,01 N-ni trosoanatabine ND 0,05 N -nitrosoanabasine ND 0,01
POLYCYCLIC AROMATIC HYDROCARBONS (PAHs) ANALYSIS
(Gas Chromatography -Mass Spectrometry)
RESULTS
Table 3. name concentration (LOQ)
(ppm) (ppm)
acenaphtylene ND* 0,005
fluorene ND 0,010 phenanthrene ND 0,005
anthracene ND 0,006
pyrene ND 0,003 benzo(a)anthracene ND 0,003
chrysene ND 0,003 benzo(k)fluoranthene ND 0,060 benzo(b )fluoranthene ND 0,006 benzo(g,h,i)perylene ND 0,014
dibenzo( a,h )anthracene ND 0,021
indeno( 1 ,2,3-CD)pyrene ND 0,022
Demetrios Kouretas, PhD
Professor
Biochemical Toxicology
fiANEOJI:TIIMION 0EI:I:AAIAI: TMHMA BIOXHMEIAI: & BIOTEXNOAOriAI: fiAOYT!!NOI: 26 41221 AAPII:A
THA/FAX. (2410) 565277/90 Email: [email protected] AIJfJJlTPll~ KouptTU~ KaOtJ'YIJTJl~
UNIVERSITY OF THESSAL Y BIOCHEMISTRY & BIOTECHNOLOGY DEPT
PLOUTONOS 26 LARISSA, 41221-GREECE
TEL/FAX. (302410) 565277/90 Email: [email protected]
Demetrios Kouretas Professor
CERTIFICATE OF ANALYSIS AND CLASSIFICATION OFBEBECA
COMPANY: ATMOS LAB
COMMERCIAL NAME OF PRODUCT: BEBECA TOTAL NUMBER: 01/BEBECA/12
ANALYSIS (Gas Chromatography -Mass Spectrometry and Liquid Chromatography-Mass Spectrometry)
table 1.
substance
methyl cyclopentenolone
ethyl maltol
ethyl vanillin
propylene glycol
glycerol
water
nicotine
total
RESULTS
Percentage (%w/v)
0,503
1,130
0,004
9,35
85,86
1,6522
1,5
99,9992
Limit of analysis (LOQ) ( m) 0,121
0,135
0,032
0,198
1,187
0,1
classification
no
Oral acute toxicity group 4
Skin irritation group 2
Eye irritation group 2
Special toxicity in target organs group 3
no
no
Acute toxicity 1 Acute toxicity 3
Chronic toxicity 2 in aquatic organisms
Classification of the liquid Bebeca
According to Greek regulation ( FEK 1214/B'/19.9.2002), classification of particular ingredients of the mixture and according to EU Regulation 1272/2008 this product with 99.9991% composition, is classified as non hazardous for human health, environment and according to its physicochemical properties
NYTROZAMINE ANALYSIS
(Liquid Chromatography -Mass Spectrometry)
table 2. name
4-(Methylnitrosamino )-1-(3-pyridyl)-1-butanol 4'-(nitrosomethylamino )-1-(3-pyridyl)-1-butanone N -nitrosoanatabine
N -nitrosoanabasine
RESULTS
concentration (ppm)
ND*
ND ND
ND
(LOQ) (ppm)
0,01
0,01 0,05 0,01
POLYCYCLIC AROMATIC HYDROCARBONS (PAHs) ANALYSIS
(Gas Chromatography -Mass Spectrometry)
RESULTS
table 3. name concentration (LOQ)
(ppm) (ppm)
acenaphtylene ND* 0,005
fluorene ND 0,010
phenanthrene ND 0,005
anthracene ND 0,006
pyrene ND 0,003
benzo(a)anthracene ND 0,003
chrysene ND 0,003
benzo(k)fluoranthene ND 0,060
benzo(b )fluoranthene ND 0,006
benzo(g,h,i )perylene ND 0,014
dibenzo(a,h)anthracene ND 0,021
indeno( 1 ,2,3-CD )pyrene ND 0,022
Demetrios Kouretas, PhD
Professor
Biochemical Toxicology
nANEniETHMION 0EEEAAIAE TMHMA BIOXHMEIAE & BIOTEXNOAOrtAE nAOYT!!NOE 26 41221 AAPIEA
THAIFAX. (2410) 565277/90 Email: [email protected] Al]Jl1JTP1]~ KouptTa~ Ka91)YlJTtj~
UNIVERSITY OF THESSAL Y BIOCHEMISTRY & BIOTECHNOLOGY DEPT
PLOUTONOS 26 LARISSA, 41221-GREECE
TEL/FAX. (302410) 565277/90 Email: [email protected]
Demetrios Kouretas Professor
CERTIFICATE OF ANALYSIS AND CLASSIFICATION OFCAMILA
COMPANY: ATMOS LAB COMMERCIAL NAME OF PRODUCT: CAMll..A TOTAL NUMBER: 011 CAMILA 112
ANALYSIS (Gas Chromatography -Mass Spectrometry and Liquid Chromatography-Mass Spectrometry)
RESULTS
Table 1.
Percentage Limit of analysis
substance (%w/v)
(LOQ) classification ( m)
Oral acute toxicity group 4
Skin irritation group 2
ethyl vanillin 0,001 0,032 Eye irritation group 2
Special toxicity in target organ group 3
propylene glycol 15,52 0,198 no
gl~cerol 80,70 1,187 no
water 2,2773 Acute toxicity 1
nicotine 1,5 0,1 Acute toxicity 3
Chronic toxicity 2 in aguatic organisms
total 99,9983
Classification of the liquid CAMILA
According to Greek regulation ( FEK 1214/B'/19.9.2002), classification of particular ingredients of the mixture and according to EU Regulation 1272/2008 this product with 99.9991% composition, is classified as non hazardous for human health, environment and according to its physicochemical properties.
NYTROZAMINE ANALYSIS
(Liquid Chromatography -Mass Spectrometry)
table 2. name
4-(Methylnitrosamino )-1-(3-pyridyl)-1-butanol 4'-(nitrosomethylarnino )-1-(3-pyridyl)-1-butanone N -nitrosoanatabine N -nitrosoanabasine
RESULTS
concentration (ppm)
ND*
ND ND ND
(LOQ) (ppm)
0,01
0,01 0,05 0,01
POLYCYCLIC AROMATIC HYDROCARBONS (PAHs) ANALYSIS
(Gas Chromatography -Mass Spectrometry)
RESULTS
total 3. name concentration (LOQ)
(ppm) (ppm)
acenaphtylene ND* 0,005 fluorene ND 0,010
phenanthrene ND 0,005
anthracene ND 0,006 pyrene ND 0,003
benzo(a)anthracene ND 0,003
chrysene ND 0,003
benzo(k)fluoranthene ND 0,060
benzo(b )fluoranthene ND 0,006
benzo(g,h,i )pery lene ND 0,014
dibenzo(a,h)anthracene ND 0,021
indeno( 1 ,2,3-CD )pyrene ND 0,022
Demetrios Kouretas, PhD
Professor
Biochemical Toxicology
flANEllll:THMION 0EI:I:AAIAI: TMHMA BIOXHMEIAI: & BIOTEXNOAOriAI: nAOYT!!NOI: 26 41221 AAPII:A
THAIFAX. (2410) 565277/90 Email: [email protected] AlJJltJTPlJ~ Kollptm~ Ko01JY1JTtJ~
UNIVERSITY OF THESSAL Y BIOCHEMISTRY & BIOTECHNOLOGY DEPT
PLOUTONOS 26 LARISSA, 41221-GREECE
TEL/FAX. (302410) 565277/90 Email: [email protected]
Demetrios Kouretas Professor
CERTIFICATE OF ANALYSIS AND CLASSIFICATION OFKAPNOS
COMPANY: ATMOS LAB COMMERCIAL NAME OF THE PRODUCT: KAPNOS TOTAL NUMBER: 0 1/KAPNOS/ 12
ANALYSIS (Gas Chromatography -Mass Spectrometry and Liquid Chromatography-Mass Spectrometry)
table 1.
substance
propylene glycol
glycerol
water
nicotine
total
RESULTS
percentage (%w/v)
3,28
89,61
5,6996
1,4
99,9896
Limit of analysis (LOQ) ( m) 0,198
1,187
0,1
Classification of the liquid KAPNOS
classification
no
no
Acute toxicity 1 Acute toxicity 3
Chronic toxicity 2 in aquatic organisms
According to Greek regulation ( FEK 1214/B '119 .9 .2002) , classification of particular ingredients of the mixture and according to EU Regulation 1272/2008 this product with 99.9991 % composition, is classified as non hazardous for human health, environment and according to its physicochemical properties.
NYTROZAMINE ANALYSIS
(Liquid Chromatography -Mass Spectrometry)
RESULTS
table 2. name concentration (LOQ)
(ppm) (ppm) 4-(Methylnitrosamino )-1-(3-pyridyl)-1-butanol ND* 0,01 4'-(nitrosomethylamino )-1-(3-pyridyl)-1-butanone ND 0,01
N -nitrosoanatabine ND 0,05
N -nitrosoanabasine ND 0,01
POLYCYCLIC AROMATIC HYDROCARBONS (PAHs) ANALYSIS
(Gas Chromatography -Mass Spectrometry)
RESULTS
table 3. name concentration (LOQ)
(ppm) (ppm)
acenaphtylene ND* 0,005 fluorene ND 0,010
phenanthrene ND 0,005
anthracene ND 0,006
pyrene ND 0,003 benzo(a)anthracene ND 0,003
chrysene ND 0,003 benzo(k)fluoranthene ND 0,060 benzo(b )fluoranthene ND 0,006 benzo(g,h,i )perylene ND 0,014
dibenzo(a,h)anthracene ND 0,021
indeno( 1 ,2,3-CD)pyrene ND 0,022
Demetrios Kouretas, PhD
Professor
Biochemical Toxicology