“Material Characterisation of Polyurethane-BasedDLR - Overview -7.700 employee are working at 32...

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www.DLR.de Chart 1 Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013 “Material Characterisation of Polyurethane-Based Paper Honeycomb Sandwich Structures” 16 th International Conference on Experimental Mechanics 7 th 11 th July 2014, Cambridge - UK Authors: Dipl.-Ing. Gerhard Kopp (DLR) Dr.-Ing. Jan Kuppinger (Fraunhofer ICT) Prof. Dr.-Ing. Horst E. Friedrich (DLR)

Transcript of “Material Characterisation of Polyurethane-BasedDLR - Overview -7.700 employee are working at 32...

Page 1: “Material Characterisation of Polyurethane-BasedDLR - Overview -7.700 employee are working at 32 research institutes and facilities in n 9 locations 7 branch offices -International

www.DLR.de • Chart 1 Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

“Material Characterisation of Polyurethane-Based

Paper Honeycomb Sandwich Structures” 16th International Conference on Experimental Mechanics 7th – 11th July 2014, Cambridge - UK Authors:

Dipl.-Ing. Gerhard Kopp (DLR)

Dr.-Ing. Jan Kuppinger (Fraunhofer ICT)

Prof. Dr.-Ing. Horst E. Friedrich (DLR)

Page 2: “Material Characterisation of Polyurethane-BasedDLR - Overview -7.700 employee are working at 32 research institutes and facilities in n 9 locations 7 branch offices -International

DLR - Overview

- 7.700 employee are working at 32 research institutes and facilities in

n 9 locations

7 branch offices

- International Branch Offices in Brussels, Paris and Washington

- Partner of

European Transsonic Wind Tunnel (ETW)

German Dutch Wind Tunnels (DNW)

www.DLR.de • Chart 2

SPACE AERONAUTICS TRANSPORT ENERGY

SECURITY

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

Page 3: “Material Characterisation of Polyurethane-BasedDLR - Overview -7.700 employee are working at 32 research institutes and facilities in n 9 locations 7 branch offices -International

DLR - Overview

DLR Institute of Vehicle Concepts (DLR FK)

Department of Lightweight and Hybrid Design Methods

Pfaffenwaldring 38 – 40

D – 70569 Stuttgart

Germany

www.DLR.de • Chart 3

SPACE AERONAUTICS TRANSPORT ENERGY

SECURITY

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

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Outline

- Introduction and motivation

- Sandwich characterization

- Approach

- Face sheet material

- Core material

- Sandwich configuration in bending

- Conclusion

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

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www.DLR.de • Chart 5

Introduction and motivation

Sandwich manufacturing processes

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

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Introduction and motivation

Sandwich manufacturing processes

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

Basic raw material

Intermediate step Manufacturing method

Direct process, e.g.

Integral foam

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www.DLR.de • Chart 7

Introduction and motivation

Sandwich manufacturing processes

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

Basic raw material

Face sheet

Joining technology

Core structure

Intermediate step

Sandwich bonding,

welding, brazing, …

Manufacturing method

Direct process, e.g.

Integral foam

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www.DLR.de • Chart 8

Introduction and motivation

Sandwich manufacturing processes

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

Basic raw material

Face sheet

Joining technology

Core structure

Core structure with joining

technology

Intermediate step

Sandwich bonding,

welding, brazing, …

Hot joining, Foam

molding

Manufacturing method

Direct process, e.g.

Integral foam

Page 9: “Material Characterisation of Polyurethane-BasedDLR - Overview -7.700 employee are working at 32 research institutes and facilities in n 9 locations 7 branch offices -International

www.DLR.de • Chart 9

Introduction and motivation

Sandwich manufacturing processes

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

Face sheet with joining

technology

Basic raw material

Face sheet

Joining technology

Core structure

Core structure with joining

technology

Intermediate step

Wet-in-wet procedure

Sandwich bonding,

welding, brazing, …

Hot joining, Foam

molding

Manufacturing method

Direct process, e.g.

Integral foam

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Overview of the polyurethane fibre spraying process

www.DLR.de • Chart 10

Introduction and motivation

Sandwich

configuration

Textile reinforcements

and core structures

Source: [1]

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

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Overview of the polyurethane fibre spraying process

www.DLR.de • Chart 11

Introduction and motivation

Sandwich

configuration

Textile reinforcements

and core structures

Robot and

Spraying

deposition

Polyurethane high

pressure dosing unit

Source: [1]

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

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Overview of the polyurethane fibre spraying process

www.DLR.de • Chart 12

Introduction and motivation

Sandwich

configuration

Textile reinforcements

and core structures

Robot and

Spraying

deposition

Sandwich structure

Compression moulding

Polyurethane high

pressure dosing unit

Source: [1]

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

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Introduction and motivation

Challenges for the future development and

application of the process

- Detail analyze of the sandwich and material

properties, depending of the manufacturing

process

- Examination of the relevant mode of failure

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

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Sandwich characterization

Approach

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

Approach in dependence on: [2] and [3]

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Sandwich characterization

Approach

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

Property characterisation of face sheet and

core structure in tension, compression and shear

Source: Fraunhofer ICT

Approach in dependence on: [2] and [3]

Page 16: “Material Characterisation of Polyurethane-BasedDLR - Overview -7.700 employee are working at 32 research institutes and facilities in n 9 locations 7 branch offices -International

www.DLR.de • Chart 16

Sandwich characterization

Approach

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

Property characterisation of face sheet and

core structure in tension, compression and shear

Derive correlations between the core densities and

the core material properties

Source: Fraunhofer ICT

Approach in dependence on: [2] and [3]

Page 17: “Material Characterisation of Polyurethane-BasedDLR - Overview -7.700 employee are working at 32 research institutes and facilities in n 9 locations 7 branch offices -International

www.DLR.de • Chart 17

Sandwich characterization

Approach

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

Property characterisation of face sheet and

core structure in tension, compression and shear

Derive correlations between the core densities and

the core material properties

Derived failure mode maps with analytical formula

and analyse the relevant modes of failure in

bending

Source: Fraunhofer ICT

Approach in dependence on: [2] and [3]

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www.DLR.de • Chart 18

Sandwich characterization

Face sheet material

- The face sheet thickness was measured with the

computer tomograph (CT) also for different glass

fiber mats

- In a wide range the material properties were

independent of the mass of deposit polyurethane

Source: Fraunhofer ICT

300 g/m² 450 g/m² 600 g/m² 900 g/m²

Face sheet thickness [mm] 340 430 545 781

Standard deviation [μm] 31 26 32 38

Young modulus [N/mm²] 10300 12300 13200 13300

Standard deviation [N/mm²] 510 530 560 850

Tensile strength [N/mm²] 152 169 212 212

Standard deviation [N/mm²] 9,1 11,0 6,3 10,3

Source: Fraunhofer ICT

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

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Sandwich characterization

Variations of the sandwich structure

- Chopped glass strand mats with a mass per unit

area of 600 g/m² in each cover as reinforcements

for the faces

- Paper honeycomb core (A-wave, Testliner III,

Density ca. 55 kg/m³ and A-wave, Testliner II,

Density ca. 75 kg/m³ )

- Polyurethane spraying deposition of 600 g/m² on

the face sheets

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

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www.DLR.de • Chart 20

Sandwich characterization

Core material

- The core properties were measured in

plane and out of plane

- Measurement based on DIN53291,

DIN53292 and DIN53294

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

Direction

Direction

Direction

Page 21: “Material Characterisation of Polyurethane-BasedDLR - Overview -7.700 employee are working at 32 research institutes and facilities in n 9 locations 7 branch offices -International

www.DLR.de • Chart 21

Sandwich characterization

Core material

- The core properties were measured in

plane and out of plane

- Measurement based on DIN53291,

DIN53292 and DIN53294

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

Direction

Direction

Direction

Page 22: “Material Characterisation of Polyurethane-BasedDLR - Overview -7.700 employee are working at 32 research institutes and facilities in n 9 locations 7 branch offices -International

www.DLR.de • Chart 22

Sandwich characterization

Core material

- The core properties were measured in

plane and out of plane

- Measurement based on DIN53291,

DIN53292 and DIN53294

- Examples:

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

Material

properties

Correlation in tension and

compression

Tension strenght

out of plane 𝜎𝐶,𝑡𝑒𝑛𝑠𝑖𝑜𝑛,𝑧𝑧

𝜎𝑆=

𝜌𝐶𝜌𝑆

Strenght in

compression

out of plane

𝜎𝐶,𝑃𝑟𝑒𝑠𝑠𝑢𝑟𝑒,𝑧𝑧𝜎𝑆

=𝜌𝐶𝜌𝑆

Material

properties

Correlation in shear

Shear strenght

out of plane

L-direction

𝜏𝐶,𝑥𝑧,𝐿𝜏𝑆

= 1,348 ∙𝜌𝐶𝜌𝑆

Shear stiffness

out of plane

L-direction

𝐺𝐶,𝑥𝑧,𝐿𝐺𝑆

= 0,763 ∙𝜌𝐶𝜌𝑆

Direction

Direction

Direction

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www.DLR.de • Chart 23

Sandwich characterization

Sandwich configuration in bending

- Relevant mode of failure:

- Face sheet failure

- Core shear failure

- Locale indentation

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

Page 24: “Material Characterisation of Polyurethane-BasedDLR - Overview -7.700 employee are working at 32 research institutes and facilities in n 9 locations 7 branch offices -International

www.DLR.de • Chart 24

Sandwich characterization

Sandwich configuration in bending

- Failure mode maps

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

-0,02

-0,1

Rela

tive

den

sit

y r

c/r

s [

-]

-10-4 -10-3

-0,4

Face thickness / span tF / l2 [-]

-10-2

Face fracture

(Compression)

Wrinkling

Core Shear

Local

Indentation

3-point-bending, L-direction

Page 25: “Material Characterisation of Polyurethane-BasedDLR - Overview -7.700 employee are working at 32 research institutes and facilities in n 9 locations 7 branch offices -International

www.DLR.de • Chart 25

Sandwich characterization

Sandwich configuration in bending

- Failure mode maps

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

-0,02

-0,1

Rela

tive

den

sit

y r

c/r

s [

-]

-10-4 -10-3

-0,4

Face thickness / span tF / l2 [-]

-10-2

Face fracture

(Compression)

Wrinkling

Core Shear

Local

Indentation

3-point-bending, L-direction

Page 26: “Material Characterisation of Polyurethane-BasedDLR - Overview -7.700 employee are working at 32 research institutes and facilities in n 9 locations 7 branch offices -International

www.DLR.de • Chart 26

Sandwich characterization

Sandwich configuration in bending

- Failure mode maps

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

-0,02

-0,1

Rela

tive

den

sit

y r

c/r

s [

-]

-10-4 -10-3

-0,4

Face thickness / span tF / l2 [-]

-10-2

4-point-bending, L-direction

Face fracture

(Compression)

Wrinkling

Core Shear

Local

Indentation

Page 27: “Material Characterisation of Polyurethane-BasedDLR - Overview -7.700 employee are working at 32 research institutes and facilities in n 9 locations 7 branch offices -International

Material Characterisation of Polyurethane-Based Paper Honeycomb

Sandwich Structures

- Basic material parameters were determined from sandwich structures

produced using the polyurethane fibre spraying process

- Furthermore, the critical failure modes were determined using bending

tests

- These results were used to design and simulate such sandwich

components with FEM

www.DLR.de • Chart 27

Conclusion

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013

Page 28: “Material Characterisation of Polyurethane-BasedDLR - Overview -7.700 employee are working at 32 research institutes and facilities in n 9 locations 7 branch offices -International

Thank you very much for your attention.

Contact:

DLR Institute of Vehicle Concepts (DLR FK)

Dipl.-Ing. Gerhard Kopp

[email protected]

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www.DLR.de • Chart 29

Source

[1] - Cageao, R.A.; Lorenzo, J.M.; Franken, K.: Studies of Composites made with Baypreg F:

Component Selection of Optimal Mechanical Properties, in: Polyurethanes, 2004

[2] - Triantafillou, T.; Gibson, L.: Failure Mode Maps for Foam Core Sandwich Beams, in:

Materials Science and Engineering, Vol. 98, 1987, p. 37 - 53

[3] Petras, A.; Sutcliffe, M.: Failure mode maps for honeycomb sandwich panels, in: Composite

Structures, Vol 44, 1999, p. 237 - 252

Material Characterisation Polyurethane-Based Paper Honeycomb Sandwich > Gerhard Kopp > 07.07.2013