ANALYTICAL REPORT 6 - Energy.gov · 2016-09-26 · ANALYTICAL REPORT TestAmerica Laboratories, Inc....

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica St. Louis13715 Rider Trail NorthEarth City, MO 63045Tel: (314)298-8566

TestAmerica Job ID: 160-18570-2Client Project/Site: ORNL Y-12 Outfall 200 Characterization

For:Alliant Corporation320 N Cedar Bluff RoadSuite 200Knoxville, Tennessee 37923

Attn: Doug Milloway

Authorized for release by:9/26/2016 3:18:59 PM

Erika Gish, Project Manager II(314)[email protected]

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents

Client: Alliant CorporationProject/Site: ORNL Y-12 Outfall 200 Characterization

TestAmerica Job ID: 160-18570-2

of 52TestAmerica St. Louis

9/26/2016

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

Subcontract Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

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Case NarrativeClient: Alliant Corporation TestAmerica Job ID: 160-18570-2Project/Site: ORNL Y-12 Outfall 200 Characterization

Job ID: 160-18570-2

Laboratory: TestAmerica St. Louis

Narrative

CASE NARRATIVE

Client: Alliant Corporation

Project: ORNL Y-12 Outfall 200 Characterization

Report Number: 160-18570-2

With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control

limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses

performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmerica’s operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions

to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a % solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and

disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.”

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPTThe samples were received on 8/10/2016 9:20 AM; the samples arrived in good condition, properly preserved. The temperature of the

cooler at receipt was 0.7º C.

Receipt Exceptions

The container label for the following sample did not match the information listed on the Chain-of-Custody (COC): YMTFA 32 SO 002 (160-18570-8). The container labels lists YMTFA 32 SO 010, while the COC lists YMTFA 32 SO 002. Sample was logged per CoC.

CommentsPlease see attached subcontract report for analyses performed at TestAmerica Richland.

RADIUM-226 BY ALPHA SPECTROMETRYSamples YMTFA 42 SO 030 (160-18570-1), YMTFA 42 SO 030D (160-18570-2), YMTFA 43 SO 030 (160-18570-3), YMTFA 43 SO 030D

(160-18570-4), YMTFA 49 SO 005 (160-18570-5), YMTFA 36 SO 002 (160-18570-6), YMTFA 35 SO 002 (160-18570-7), YMTFA 32 SO 002 (160-18570-8) and YMTFA 34 SO 002 (160-18570-9) were analyzed for Radium-226 by Alpha Spectrometry in accordance with

TestAmerica St. Louis of 52 9/26/2016

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Case NarrativeClient: Alliant Corporation TestAmerica Job ID: 160-18570-2Project/Site: ORNL Y-12 Outfall 200 Characterization

Job ID: 160-18570-2 (Continued)

Laboratory: TestAmerica St. Louis (Continued)

ST-RC-0301. The samples were dried on 08/10/2016, prepared on 08/22/2016 and analyzed on 09/15/2016 and 09/16/2016.

The At-217 tracer recovery for the following samples was low outside the QC limits of 30%: LCS 160-266021/2-A: 28.2%. The DOE/DOD

Quality Systems Manual for Environmental Laboratories (QSM Rev. 5.0) allows for reporting results as quantitative when tracer recoveries

are below 30% if a) the relative uncertainty associated with the tracer recovery is less than 10% (2 sigma), b) spectral resolution requirements are met and there are no indications of spectral interferences, and c) detection limit requirements are met. All three of these

criteria are met for these samples: a) a minimum of 400 counts (which leads to 10% count uncertainty at 2 sigma) in the tracer peak, b) resolution of < 100 keV is met for all peaks, and c) the activity in the sample is well above the MDC. The data have been qualified and

reported.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.


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Login Sample Receipt Checklist

Client: Alliant Corporation Job Number: 160-18570-2

Login Number: 18570

Question Answer Comment

Creator: Clarke, Jill C

List Source: TestAmerica St. Louis

List Number: 1

TrueRadioactivity wasn't checked or is </= background as measured by a survey meter.

N/AThe cooler's custody seal, if present, is intact.

N/ASample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

TrueSamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

FalseThere are no discrepancies between the containers received and the COC. Sample #8 COC and container do not match. Logged per container.

TrueSamples are received within Holding Time (excluding tests with immediate HTs)

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

N/AContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.


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Definitions/GlossaryTestAmerica Job ID: 160-18570-2Client: Alliant Corporation

Project/Site: ORNL Y-12 Outfall 200 Characterization

Qualifiers

Rad

Qualifier Description

S Tracer is outside acceptance limits.

Qualifier

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Method SummaryTestAmerica Job ID: 160-18570-2Client: Alliant Corporation


Method Method Description LaboratoryProtocol

TAL-STLST-RC-0301 Radium-226 (Alpha Spectrometry) TAL SL

NONEAm-241 General Sub Contract Method TAL RCH

NONEC-14 General Sub Contract Method TAL RCH

NONENp-237 General Sub Contract Method TAL RCH

NONEPu-238,

Pu-239/240

General Sub Contract Method TAL RCH

NONETh-228, Th-230,

Th-232


NONEU-233/234,

U-235/236, U-238


Protocol References:

NONE = NONE

TAL-STL = TestAmerica Laboratories, St. Louis, Facility Standard Operating Procedure.

Laboratory References:

TAL RCH = TestAmerica Richland, 2800 George Washington Way, Richland, WA 99352, TEL (509)375-3131

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566


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Sample SummaryTestAmerica Job ID: 160-18570-2Client: Alliant Corporation


Lab Sample ID Client Sample ID ReceivedCollectedMatrix

160-18570-1 YMTFA 42 SO 030 Solid 08/09/16 09:20 08/10/16 09:20

160-18570-2 YMTFA 42 SO 030D Solid 08/09/16 09:20 08/10/16 09:20

160-18570-3 YMTFA 43 SO 030 Solid 08/09/16 10:50 08/10/16 09:20

160-18570-4 YMTFA 43 SO 030D Solid 08/09/16 10:50 08/10/16 09:20

160-18570-5 YMTFA 49 SO 005 Solid 08/09/16 13:00 08/10/16 09:20

160-18570-6 YMTFA 36 SO 002 Solid 08/09/16 13:05 08/10/16 09:20

160-18570-7 YMTFA 35 SO 002 Solid 08/09/16 14:01 08/10/16 09:20

160-18570-8 YMTFA 32 SO 002 Solid 08/09/16 14:48 08/10/16 09:20

160-18570-9 YMTFA 34 SO 002 Solid 08/09/16 15:10 08/10/16 09:20


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Client Sample ResultsTestAmerica Job ID: 160-18570-2Client: Alliant Corporation


Lab Sample ID: 160-18570-1Client Sample ID: YMTFA 42 SO 030Matrix: SolidDate Collected: 08/09/16 09:20

Date Received: 08/10/16 09:20

Method: ST-RC-0301 - Radium-226 (Alpha Spectrometry)

Analyte

Radium-226 1.66

(2σ+/-)

0.291

(2σ+/-)

109/15/16 10:1908/22/16 18:53pCi/g0.1391.00

RL MDC

0.255

Dil FacAnalyzedPreparedUnitResult Qualifier

Count Total

Uncert. Uncert.

At-217 30 - 110

Tracer

08/22/16 18:53 09/15/16 10:19 1

Dil FacAnalyzedPreparedQualifier Limits%Yield

43.2

Lab Sample ID: 160-18570-2Client Sample ID: YMTFA 42 SO 030DMatrix: SolidDate Collected: 08/09/16 09:20



Analyte

Radium-226 1.53

(2σ+/-)

0.246

(2σ+/-)

109/15/16 10:1908/22/16 18:53pCi/g0.09251.00

RL MDC

0.210


Count Total

Uncert. Uncert.

At-217 30 - 110

Tracer

08/22/16 18:53 09/15/16 10:19 1


55.1




Analyte

Radium-226 1.57

(2σ+/-)

0.253

(2σ+/-)

109/15/16 10:1908/22/16 18:53pCi/g0.07041.00

RL MDC

0.216


Count Total

Uncert. Uncert.

At-217 30 - 110

Tracer

08/22/16 18:53 09/15/16 10:19 1


49.1

Lab Sample ID: 160-18570-4Client Sample ID: YMTFA 43 SO 030DMatrix: SolidDate Collected: 08/09/16 10:50



Analyte

Radium-226 1.62

(2σ+/-)

0.260

(2σ+/-)

109/15/16 10:1908/22/16 18:53pCi/g0.07151.00

RL MDC

0.222


Count Total

Uncert. Uncert.

At-217 30 - 110

Tracer

08/22/16 18:53 09/15/16 10:19 1


50.5


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Analyte

Radium-226 1.48

(2σ+/-)

0.241

(2σ+/-)

109/15/16 10:1908/22/16 18:53pCi/g0.02151.00

RL MDC

0.206


Count Total

Uncert. Uncert.

At-217 30 - 110

Tracer

08/22/16 18:53 09/15/16 10:19 1


49.2




Analyte

Radium-226 0.537

(2σ+/-)

0.158

(2σ+/-)

109/15/16 10:1908/22/16 18:53pCi/g0.1161.00

RL MDC

0.152


Count Total

Uncert. Uncert.

At-217 30 - 110

Tracer

08/22/16 18:53 09/15/16 10:19 1


40.3




Analyte

Radium-226 1.83

(2σ+/-)

0.278

(2σ+/-)

109/16/16 10:1708/22/16 18:53pCi/g0.05601.00

RL MDC

0.232


Count Total

Uncert. Uncert.

At-217 30 - 110

Tracer

08/22/16 18:53 09/16/16 10:17 1


50.2




Analyte

Radium-226 1.72

(2σ+/-)

0.278

(2σ+/-)

109/16/16 10:1708/22/16 18:53pCi/g0.07731.00

RL MDC

0.238


Count Total

Uncert. Uncert.

At-217 30 - 110

Tracer

08/22/16 18:53 09/16/16 10:17 1


46.2


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Analyte

Radium-226 1.25

(2σ+/-)

0.244

(2σ+/-)

109/15/16 10:1908/22/16 18:53pCi/g0.1211.00

RL MDC

0.220


Count Total

Uncert. Uncert.

At-217 30 - 110

Tracer

08/22/16 18:53 09/15/16 10:19 1


39.4


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QC Sample ResultsTestAmerica Job ID: 160-18570-2Client: Alliant Corporation



Client Sample ID: Method BlankLab Sample ID: MB 160-266021/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 270177 Prep Batch: 266021

Radium-226

Analyte

109/15/16 10:2008/22/16 18:53pCi/g0.0787

MDC

1.00

RL

0.09560.0942

(2σ+/-) (2σ+/-)

MB

0.1953

MB

Dil FacPrepared AnalyzedUnitResult Qualifier

Uncert.

Count

Uncert.

Total

Tracer

At-217 30 - 110 08/22/16 18:53 09/15/16 10:20 1

Dil FacPrepared AnalyzedQualifier Limits%Yield

36.5

MB MB

Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-266021/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 270178 Prep Batch: 266021

Radium-226

Analyte

130-7011714.0712.1 1.47 1.00 0.103

RL MDC(2σ+/-)

LCS LCS

pCi/g

UnitResult Qual %RecAdded

Spike

Limits

%Rec.Uncert.

Total

At-217

Tracer

S 30 - 110

LCS

Qualifier Limits%Yield

28.2

LCS

Client Sample ID: DuplicateLab Sample ID: 160-18504-F-1-Q DUMatrix: Solid Prep Type: Total/NAAnalysis Batch: 270180 Prep Batch: 266021

Radium-226

Analyte

10.310.65920.772 0.171 1.00 0.152

RL MDC(2σ+/-)

DU DU

pCi/g

UnitResult Qual LimitResult

Sample Sample

Qual

Uncert.

Total

RER

RER

At-217

Tracer

30 - 110

DU

Qualifier Limits%Yield

50.0

DU


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QC Association SummaryTestAmerica Job ID: 160-18570-2Client: Alliant Corporation


Rad

Leach Batch: 263919

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid Dry and Grind160-18504-F-1-Q DU Duplicate Total/NA

Leach Batch: 264331


Solid Dry and Grind160-18570-1 YMTFA 42 SO 030 Total/NA

Solid Dry and Grind160-18570-2 YMTFA 42 SO 030D Total/NA


Solid Dry and Grind160-18570-4 YMTFA 43 SO 030D Total/NA






Prep Batch: 266021


Solid DPS-0 264331160-18570-1 YMTFA 42 SO 030 Total/NA

Solid DPS-0 264331160-18570-2 YMTFA 42 SO 030D Total/NA


Solid DPS-0 264331160-18570-4 YMTFA 43 SO 030D Total/NA






Solid DPS-0MB 160-266021/1-A Method Blank Total/NA

Solid DPS-0LCS 160-266021/2-A Lab Control Sample Total/NA

Solid DPS-0 263919160-18504-F-1-Q DU Duplicate Total/NA


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Tracer/Carrier SummaryTestAmerica Job ID: 160-18570-2Client: Alliant Corporation


Method: ST-RC-0301 - Radium-226 (Alpha Spectrometry)Prep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (30-110)

At-217

50.0160-18504-F-1-Q DU

Percent Yield (Acceptance Limits)

Duplicate

43.2160-18570-1 YMTFA 42 SO 030

55.1160-18570-2 YMTFA 42 SO 030D

49.1160-18570-3 YMTFA 43 SO 030

50.5160-18570-4 YMTFA 43 SO 030D

49.2160-18570-5 YMTFA 49 SO 005

40.3160-18570-6 YMTFA 36 SO 002

50.2160-18570-7 YMTFA 35 SO 002

46.2160-18570-8 YMTFA 32 SO 002

39.4160-18570-9 YMTFA 34 SO 002

28.2 SLCS 160-266021/2-A Lab Control Sample

36.5MB 160-266021/1-A Method Blank

Tracer/Carrier Legend

At-217 = At-217


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Analytical Data Package Prepared For

Radiochemical Analysis By

TESTAMERICA ST. LOUIS

TestAmerica Inc

2800 G.W. Way, Richland Wa, 99354, (509)-375-3131.

Data Package Contains ______ Pages

Assigned Laboratory Code: TA-RL

Client Sample ID (List Order) Lot-Sa No. Work OrderSDG No.

Report No.: 69364

Order No. Report DB ID Batch No.

Results in this report relate only to the sample(s) analyzed.

YMTFA 32 SO 002(160-

18570-8)

9M84VV1051961 J6H180408-8 M84VV1AE 6231057

YMTFA 32 SO 002(160-

18570-8)

9M84VV10J6H180408-8 M84VV1AG 6231058

YMTFA 32 SO 002(160-

18570-8)

9M84VV10J6H180408-8 M84VV1AC 6231059

YMTFA 32 SO 002(160-

18570-8)

9M84VV10J6H180408-8 M84VV1AF 6231060

YMTFA 32 SO 002(160-

18570-8)

9M84VV10J6H180408-8 M84VV1AA 6231061

YMTFA 32 SO 002(160-

18570-8)

9M84VV10J6H180408-8 M84VV1AD 6231062

YMTFA 34 SO 002(160-

18570-9)

9M84VW10J6H180408-9 M84VW1AE 6231057

YMTFA 34 SO 002(160-

18570-9)

9M84VW10J6H180408-9 M84VW1AG 6231058

YMTFA 34 SO 002(160-

18570-9)

9M84VW10J6H180408-9 M84VW1AC 6231059

YMTFA 34 SO 002(160-

18570-9)

9M84VW10J6H180408-9 M84VW1AF 6231060

YMTFA 34 SO 002(160-

18570-9)

9M84VW10J6H180408-9 M84VW1AA 6231061

YMTFA 34 SO 002(160-

18570-9)

9M84VW10J6H180408-9 M84VW1AD 6231062

YMTFA 35 SO 002(160-

18570-7)

9M84VR10J6H180408-7 M84VR1AE 6231057

YMTFA 35 SO 002(160-

18570-7)

9M84VR10J6H180408-7 M84VR1AG 6231058

YMTFA 35 SO 002(160-

18570-7)

9M84VR10J6H180408-7 M84VR1AC 6231059

TestAmerica Inc

rptSTLRchTitle v3.73

TestAmerica Laboratories, Inc. 1

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Report No.: 69364



YMTFA 35 SO 002(160-

18570-7)

9M84VR1051961 J6H180408-7 M84VR1AF 6231060

YMTFA 35 SO 002(160-

18570-7)

9M84VR10J6H180408-7 M84VR1AA 6231061

YMTFA 35 SO 002(160-

18570-7)

9M84VR10J6H180408-7 M84VR1AD 6231062

YMTFA 36 SO 002(160-

18570-6)

9M84VQ10J6H180408-6 M84VQ1AE 6231057

YMTFA 36 SO 002(160-

18570-6)

9M84VQ10J6H180408-6 M84VQ1AG 6231058

YMTFA 36 SO 002(160-

18570-6)

9M84VQ10J6H180408-6 M84VQ1AC 6231059

YMTFA 36 SO 002(160-

18570-6)

9M84VQ10J6H180408-6 M84VQ1AF 6231060

YMTFA 36 SO 002(160-

18570-6)

9M84VQ10J6H180408-6 M84VQ1AA 6231061

YMTFA 36 SO 002(160-

18570-6)

9M84VQ10J6H180408-6 M84VQ1AD 6231062

YMTFA 42 SO 030(160-

18570-1)

9M84VK10J6H180408-1 M84VK1AE 6231057

YMTFA 42 SO 030(160-

18570-1)

9M84VK10J6H180408-1 M84VK1AG 6231058

YMTFA 42 SO 030(160-

18570-1)

9M84VK10J6H180408-1 M84VK1AC 6231059

YMTFA 42 SO 030(160-

18570-1)

9M84VK10J6H180408-1 M84VK1AF 6231060

YMTFA 42 SO 030(160-

18570-1)

9M84VK10J6H180408-1 M84VK1AA 6231061

YMTFA 42 SO 030(160-

18570-1)

9M84VK10J6H180408-1 M84VK1AD 6231062

YMTFA 42 SO 030D(160-

18570-2)

9M84VL10J6H180408-2 M84VL1AE 6231057

YMTFA 42 SO 030D(160-

18570-2)

9M84VL10J6H180408-2 M84VL1AG 6231058

YMTFA 42 SO 030D(160-

18570-2)

9M84VL10J6H180408-2 M84VL1AC 6231059

YMTFA 42 SO 030D(160-

18570-2)

9M84VL10J6H180408-2 M84VL1AF 6231060

YMTFA 42 SO 030D(160-

18570-2)

9M84VL10J6H180408-2 M84VL1AA 6231061

YMTFA 42 SO 030D(160-

18570-2)

9M84VL10J6H180408-2 M84VL1AD 6231062

YMTFA 43 SO 030(160-

18570-3)

9M84VM10J6H180408-3 M84VM1AE 6231057

TestAmerica Inc


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Report No.: 69364



YMTFA 43 SO 030(160-

18570-3)

9M84VM1051961 J6H180408-3 M84VM1AG 6231058

YMTFA 43 SO 030(160-

18570-3)

9M84VM10J6H180408-3 M84VM1AC 6231059

YMTFA 43 SO 030(160-

18570-3)

9M84VM10J6H180408-3 M84VM1AF 6231060

YMTFA 43 SO 030(160-

18570-3)

9M84VM10J6H180408-3 M84VM1AA 6231061

YMTFA 43 SO 030(160-

18570-3)

9M84VM10J6H180408-3 M84VM1AD 6231062

YMTFA 43 SO 030D(160-

18570-4)

9M84VN10J6H180408-4 M84VN1AE 6231057

YMTFA 43 SO 030D(160-

18570-4)

9M84VN20J6H180408-4 M84VN2AG 6231058

YMTFA 43 SO 030D(160-

18570-4)

9M84VN10J6H180408-4 M84VN1AC 6231059

YMTFA 43 SO 030D(160-

18570-4)

9M84VN10J6H180408-4 M84VN1AF 6231060

YMTFA 43 SO 030D(160-

18570-4)

9M84VN10J6H180408-4 M84VN1AA 6231061

YMTFA 43 SO 030D(160-

18570-4)

9M84VN10J6H180408-4 M84VN1AD 6231062

YMTFA 49 SO 005(160-

18570-5)

9M84VP10J6H180408-5 M84VP1AE 6231057

YMTFA 49 SO 005(160-

18570-5)

9M84VP10J6H180408-5 M84VP1AG 6231058

YMTFA 49 SO 005(160-

18570-5)

9M84VP10J6H180408-5 M84VP1AC 6231059

YMTFA 49 SO 005(160-

18570-5)

9M84VP10J6H180408-5 M84VP1AF 6231060

YMTFA 49 SO 005(160-

18570-5)

9M84VP10J6H180408-5 M84VP1AA 6231061

YMTFA 49 SO 005(160-

18570-5)

9M84VP10J6H180408-5 M84VP1AD 6231062

TestAmerica Inc



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Certificate of Analysis

September 23, 2016


13715 Rider Trail North

Earth City, MO 63045

Attention: Erika Gish

Date Received in Lab : August 18, 2016

Sample Type : Nine (9) Solid

SDG Number : 51961

Job Number : 160-18570-1

Project Number/Name : 16005502/ORNL Y-12 Outfall 200 Characterization

CASE NARRATIVE

I. Introduction

On August 18, 2016, nine solid samples were received at the TestAmerica Richland laboratory for

radiochemical analysis. Upon receipt the samples were assigned to Lot Number J6H180408 with the

laboratory ID number corresponding to the client ID as shown on the cover page.

II. Sample Receipt

The samples were received in good condition; no anomalies were noted upon check-in.

III. Analytical Results/Methodology

The analytical results for this report are presented by laboratory sample ID. Each set of data includes

sample identification information; analytical results and the appropriate associated statistical

uncertainties.

The analyses requested were:

Alpha Spectroscopy

Americium 241 by method RL-ALP-003

Neptunium-237 by method RL-ALP-013

Plutonium-238, -239/240 by method RL-ALP-002

Thorium-228,230,232 by method RL-ALP-001

Uranium 234, 235 and 238 by method RL-ALP-004

Liquid Scintillation Counting

Carbon-14 by method RL-LSC-008


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September 23, 2016

IV. Quality Control

The analytical result for each analysis performed includes a minimum of one laboratory control sample

(LCS), and one reagent blank sample analysis. Any exceptions have been noted in the “Comments”

section.

V. Comments

Alpha Spectroscopy

Americium 241 by method RL-ALP-003:

The LCS, batch blank, sample duplicate and sample results are within acceptance limits.

Neptunium-237 by method RL-ALP-013:


Plutonium-238, -239/240 by method RL-ALP-002:


Thorium-228,230,232 by method RL-ALP-001


Uranium 234, 235 and 238 by method RL-ALP-004


Liquid Scintillation Counting

Carbon-14 by method RL-LSC-008:


I certify that this Certificate of Analysis is in compliance with the SOW and/or NELAC, both technically

and for completeness, for other than the conditions detailed above. The Laboratory Manager or a

designee, as verified by the following signature has authorized release of the data contained in this hard

copy data package.

Reviewed and approved:

____________________________

Roger A. Stringer

Project Manager I

TestAmerica Laboratories, Inc. 5

Roger A. StringerDigitally signed by Roger A. Stringer

DN: cn=Roger A. Stringer, o, ou,

[email protected], c=US

Date: 2016.09.23 11:40:33 -07'00'

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DRINKING WATER ASTM METHOD CROSS REFERENCES

Referenced Method Isotope(s) TestAmerica Richland's SOP No.

EPA 901.1 Cs-134, I-131 RL-GAM-001

EPA 900.0 Alpha & Beta RL-GPC-001

EPA 00-02 Gross Alpha (Coprecipitation) RL-GPC-002

EPA 903.0 Total Alpha Radium (Ra-226) RL-RA-002

EPA 903.1 Ra-226 RL-RA-001

EPA 904.0 Ra-228 RL-RA-001

EPA 905.0 Sr-89/90 RL-GPC-003

ASTM D5174 Uranium RL-KPA-003

EPA 906.0 Tritium RL-LSC-005

TestAmerica Richland has adopted the internationally accepted approach to estimating

uncertainties described in “NIST Technical Note 1297, 1994 Edition”. The approach, "Law of Propagation

of Errors", involves the identification of all variables in an analytical method which are used to derive a

result. These variables are related to the analytical result (R) by some functional relationship, R = constants

* f(x,y,z,...). The components (x,y,z) are evaluated to determine their contribution to the overall method

uncertainty. The individual component uncertainties (ui) are then combined using a statistical model that

provides the most probable overall uncertainty value. All component uncertainties are categorized as type

A, evaluated by statistical methods, or type B, evaluated by other means. Uncertainties not included in the

components, such as sample homogeneity, are combined with the component uncertainty as the square root

of the sum-of-the-squares of the individual uncertainties. The uncertainty associated with the derived result

is the combined uncertainty (uc) multiplied by the coverage factor (1,2, or 3).

When three or more sample replicates are used to derive the analytical result, the type A

uncertainty is the standard deviation of the mean value (S/?n), where S is the standard deviation of the

derived results. The type B uncertainties are all other random or non-random components that are not

included in the standard deviation.

The derivation of the general "Law of Propagation of Errors" equations and specific example are

available on request.

Uncertainty Estimation

Drinking Water Method Cross References


rptGeneralInfo v3.72

TestAmerica Inc


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Action Lev An agreed upon activity level used to trigger some action when the final result is greater than or equal to the Action

Level. Often the Action Level is related to the Decision Limit.

Batch The QC preparation batch number that relates laboratory samples to QC samples that were prepared and analyzed

together.

Bias Defined by the equation (Result/Expected)-1 as defined by ANSI N13.30.

COC No Chain of Custody Number assigned by the Client or TestAmerica.

Count Error (#s) Poisson counting statistics of the gross sample count and background. The uncertainty is absolute and in the same

units as the result. For Liquid Scintillation Counting (LSC) the batch blank count is the background.

CSU (#s)

uc Combined

Standard Uncert.

All known uncertainties associated with the preparation and analysis of the sample are propagated to give a measure

of the uncertainty associated with the result, uc the combined standard uncertainty. The uncertainty is absolute and

in the same units as the result.

(#s), Coverage

Factor

The coverage factor defines the width of the confidence interval, 1, 2 or 3 standard deviations.

CRDL (RL) Contractual Required Detection Limit as defined in the Client’s Statement Of Work or TestAmerica “default”

nominal detection limit. Often referred to the reporting level (RL)

Lc Decision Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume

associated with the sample. The Type I error probability is approximately 5%. Lc=(1.645 *

Sqrt(2*(BkgrndCnt/BkgrndCntMin)/SCntMin)) * (ConvFct/(Eff*Yld*Abn*Vol) * IngrFct). For LSC methods the

batch blank is used as a measure of the background variability. Lc cannot be calculated when the background count

is zero.

Lot-Sample No The number assigned by the LIMS software to track samples received on the same day for a given client. The

sample number is a sequential number assigned to each sample in the Lot.

MDC|MDA|MDL Detection Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume

with a Type I and II error probability of approximately 5%. MDC = (4.65 *

Sqrt((BkgrndCnt/BkgrndCntMin)/SCntMin) + 2.71/SCntMin) * (ConvFct/(Eff * Yld * Abn * Vol) * IngrFct). For

LSC methods the batch blank is used as a measure of the background variability.

Primary Detector The instrument identifier associated with the analysis of the sample aliquot.

Ratio U-234/U-238 The U-234 result divided by the U-238 result. The U-234/U-238 ratio for natural uranium in NIST SRM 4321C is

1.038.

Rst/MDC Ratio of the Result to the MDC. A value greater than 1 may indicate activity above background at a high level of

confidence. Caution should be used when applying this factor and it should be used in concert with the qualifiers

associated with the result.

Rst/TotUcert Ratio of the Result to the Total Uncertainty. If the uncertainty has a coverage factor of 2 a value greater than 1 may

indicate activity above background at approximately the 95% level of confidence assuming a two-sided confidence

interval. Caution should be used when applying this factor and it should be used in concert with the qualifiers

associated with the result.

Report DB No Sample Identifier used by the report system. The number is based upon the first five digits of the Work Order

Number.

RER The equation Replicate Error Ratio = (S-D)/[sqrt(TPUs2 + TPUd2)] as defined by ICPT BOA where S is the original

sample result, D is the result of the duplicate, TPUs is the total uncertainty of the original sample and TPUd is the

total uncertainty of the duplicate sample.

SDG Sample Delivery Group Number assigned by the Client or assigned by TestAmerica upon sample receipt.

Sum Rpt Alpha

Spec Rst(s)

The sum of the reported alpha spec results for tests derived from the same sample excluding duplicate result where

the results are in the same units.

Work Order The LIMS software assign test specific identifier.

Yield The recovery of the tracer added to the sample such as Pu-242 used to trace a Pu-239/40 method.

Report Definitions

rptGeneralInfo v3.72

TestAmerica Inc


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22-Sep-16Date:

Parameter MDLUnits

Client Id

Work Order

Report No. : 69359

Result +- CSU ( s) Tracer

Yield

51966SDG No:

TestAmerica Inc TA-RL

Qual

Sample Results Summary

Ordered by Method, Batch No., Client Sample ID.

2 RER2CRDLBatch

6231051 L4SO

YMTFA60 SO 010(160-18615-6)

5.88E-02PLUTONIUM-238 PCI_GM840L1AE -3.04E-03 96% +- 2.5E-02 1.00E+00U

5.49E-02PLUTONIUM-239/240 PCI_G1.06E-02 96% +- 2.5E-02 1.00E+00U

YMTFA61 SO 010(160-18615-5)

8.02E-02PLUTONIUM-238 PCI_GM840K1AE 7.83E-03 93% +- 3.0E-02 1.00E+00U

5.53E-02PLUTONIUM-239/240 PCI_G1.44E-02 93% +- 3.0E-02 1.00E+00U

YMTFA62 SO 010(160-18615-4)

7.30E-02PLUTONIUM-238 PCI_GM840J1AE 9.32E-03 94% +- 2.9E-02 1.00E+00U

5.74E-02PLUTONIUM-239/240 PCI_G-1.16E-03 94% +- 2.9E-02 1.00E+00U

YMTFA67 SO 010(160-18615-3)

9.70E-02PLUTONIUM-238 PCI_GM840G1AE -8.75E-03 67% +- 3.7E-02 1.00E+00U


YMTFA69 SO 010(160-18615-2)

6.65E-02PLUTONIUM-238 PCI_GM840E1AE 1.09E-02 87% +- 2.9E-02 1.00E+00U


YMTFA70 SO 010(160-18615-1)

8.11E-02PLUTONIUM-238 PCI_GM84X91AE 7.92E-03 95% +- 3.1E-02 1.00E+00U

5.59E-02PLUTONIUM-239/240 PCI_G0.00E+00 95% +- 3.0E-02 1.00E+00U

YMTFA70 SO 010(160-18615-1) DU

5.47E-02PLUTONIUM-238 PCI_GM84X91AH 1.63E-02 104% 0.4 +- 3.0E-02 1.00E+00U

4.36E-02PLUTONIUM-239/240 PCI_G-1.26E-03 104% 0.1 +- 2.1E-02 1.00E+00U

6231052 C0SR

YMTFA60 SO 010(160-18615-6)

9.64E-02URANIUM-233/234 PCI_GM840L1AG 2.19E-01 56% +- 1.5E-01 1.00E+00

8.15E-02URANIUM-235/236 PCI_G4.35E-02 56% +- 6.3E-02 1.00E+00U

8.15E-02URANIUM-238 PCI_G1.55E-01 56% +- 1.2E-01 1.00E+00

YMTFA61 SO 010(160-18615-5)

5.98E-02URANIUM-233/234 PCI_GM840K1AG 2.42E-01 89% +- 1.3E-01 1.00E+00

5.27E-02URANIUM-235/236 PCI_G-5.74E-04 89% +- 2.9E-02 1.00E+00U


YMTFA67 SO 010(160-18615-3)

6.19E-02URANIUM-233/234 PCI_GM840G1AG 2.53E-01 75% +- 1.4E-01 1.00E+00

6.19E-02URANIUM-235/236 PCI_G0.00E+00 75% +- 3.4E-02 1.00E+00U


YMTFA69 SO 010(160-18615-2)

6.13E-02URANIUM-233/234 PCI_GM840E1AG 3.71E-01 84% +- 1.7E-01 1.00E+00

5.70E-02URANIUM-235/236 PCI_G1.55E-02 84% +- 3.1E-02 1.00E+00U


TestAmerica Inc

U Qual - Analyzed for but not detected above limiting criteria, Mdc/Mda/Mdl, Total Uncert, RDL or not identified by gamma scan

software.

RER2 - Replicate Error Ratio = (S-D)/[sqrt(sq(TPUs)+sq(TPUd))] as defined by ICPT BOA.

rptTALRchSaSum

mary2 V5.6 A2002


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Parameter MDLUnits

Client Id

Work Order

Report No. : 69359


Yield

51966SDG No:


Qual



2 RER2CRDLBatch

6231052 C0SR

YMTFA70 SO 010(160-18615-1)

7.07E-02URANIUM-233/234 PCI_GM84X91AG 3.81E-01 85% +- 1.7E-01 1.00E+00

5.44E-02URANIUM-235/236 PCI_G-5.93E-04 85% +- 3.0E-02 1.00E+00U


YMTFA70 SO 010(160-18615-1) DU

5.43E-02URANIUM-233/234 PCI_GM84X91AJ 3.84E-01 70% 0.0 +- 1.6E-01 1.00E+00

5.05E-02URANIUM-235/236 PCI_G-5.50E-04 70% 0.0 +- 2.8E-02 1.00E+00U

5.43E-02URANIUM-238 PCI_G2.74E-01 70% 0.6 +- 1.3E-01 1.00E+00

6231053 L4SX

YMTFA60 SO 010(160-18615-6)

7.24E-02AMERICIUM-241 PCI_GM840L1AC 1.98E-02 101% +- 3.8E-02 1.00E+00U

YMTFA61 SO 010(160-18615-5)

6.77E-02AMERICIUM-241 PCI_GM840K1AC 1.11E-02 94% +- 2.9E-02 1.00E+00U

YMTFA62 SO 010(160-18615-4)

7.29E-02AMERICIUM-241 PCI_GM840J1AC -6.14E-03 101% +- 2.8E-02 1.00E+00U

YMTFA67 SO 010(160-18615-3)

6.63E-02AMERICIUM-241 PCI_GM840G1AC -1.91E-03 77% +- 3.2E-02 1.00E+00U

YMTFA69 SO 010(160-18615-2)

7.54E-02AMERICIUM-241 PCI_GM840E1AC 4.58E-02 95% +- 5.5E-02 1.00E+00U

YMTFA70 SO 010(160-18615-1)

8.49E-02AMERICIUM-241 PCI_GM84X91AC -8.15E-03 93% +- 3.2E-02 1.00E+00U

YMTFA70 SO 010(160-18615-1) DU

5.95E-02AMERICIUM-241 PCI_GM84X91AK 1.70E-02 92% 1.1 +- 3.2E-02 1.00E+00U

6231054 L4S1

YMTFA60 SO 010(160-18615-6)

5.22E-02THORIUM-228 PCI_GM840L1AF 4.84E-01 94% +- 1.9E-01 1.00E+00

5.02E-02THORIUM-230 PCI_G2.46E-01 94% +- 1.2E-01 1.00E+00


YMTFA61 SO 010(160-18615-5)

7.14E-02THORIUM-228 PCI_GM840K1AF 7.19E-01 94% +- 2.5E-01 1.00E+00



YMTFA62 SO 010(160-18615-4)

5.99E-02THORIUM-228 PCI_GM840J1AF 6.93E-01 93% +- 2.3E-01 1.00E+00



YMTFA67 SO 010(160-18615-3)

7.57E-02THORIUM-228 PCI_GM840G1AF 4.74E-01 64% +- 2.2E-01 1.00E+00

TestAmerica Inc


software.


rptTALRchSaSum

mary2 V5.6 A2002


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Parameter MDLUnits

Client Id

Work Order

Report No. : 69359


Yield

51966SDG No:


Qual



2 RER2CRDLBatch

6231054 L4S1

YMTFA67 SO 010(160-18615-3)

7.83E-02THORIUM-230 PCI_GM840G1AF 3.55E-01 64% +- 1.9E-01 1.00E+00


YMTFA69 SO 010(160-18615-2)

4.88E-02THORIUM-228 PCI_GM840E1AF 2.58E-01 92% +- 1.2E-01 1.00E+00



YMTFA70 SO 010(160-18615-1)

8.19E-02THORIUM-228 PCI_GM84X91AF 5.42E-01 91% +- 2.2E-01 1.00E+00



YMTFA70 SO 010(160-18615-1) DU

5.85E-02THORIUM-228 PCI_GM84X91AL 5.60E-01 91% 0.1 +- 2.0E-01 1.00E+00

5.33E-02THORIUM-230 PCI_G2.69E-01 91% 0.0 +- 1.3E-01 1.00E+00

4.95E-02THORIUM-232 PCI_G3.64E-01 91% 0.0 +- 1.5E-01 1.00E+00

6231056 E7XW

YMTFA60 SO 010(160-18615-6)

3.35E-02NEPTUNIUM-237 PCI_GM840L1AD -6.77E-04 91% +- 1.7E-02 1.00E+00U

YMTFA61 SO 010(160-18615-5)

1.85E-02NEPTUNIUM-237 PCI_GM840K1AD 4.67E-03 92% +- 9.5E-03 1.00E+00U

YMTFA62 SO 010(160-18615-4)

2.86E-02NEPTUNIUM-237 PCI_GM840J1AD 5.49E-03 92% +- 1.3E-02 1.00E+00U

YMTFA67 SO 010(160-18615-3)

3.11E-02NEPTUNIUM-237 PCI_GM840G1AD 3.61E-03 89% +- 1.2E-02 1.00E+00U

YMTFA69 SO 010(160-18615-2)

3.05E-02NEPTUNIUM-237 PCI_GM840E1AD -1.57E-03 94% +- 1.3E-02 1.00E+00U

YMTFA70 SO 010(160-18615-1)

2.71E-02NEPTUNIUM-237 PCI_GM84X91AD -9.93E-04 88% +- 1.2E-02 1.00E+00U

YMTFA70 SO 010(160-18615-1) DU

3.94E-02NEPTUNIUM-237 PCI_GM84X91AN -1.45E-03 87% 0.0 +- 1.8E-02 1.00E+00U

6231049 RL-LSC-008

YMTFA60 C(160-18613-1) DUP

1.88E-01CARBON-14 PCI_GM84XV1AM 3.99E-02 100% 0.1 +- 9.7E-02 1.00E+01U

YMTFA60 SO 010(160-18615-6)

1.93E-01CARBON-14 PCI_GM840L1AA -5.27E-02 100% +- 9.6E-02 1.00E+01U

YMTFA61 SO 010(160-18615-5)

1.89E-01CARBON-14 PCI_GM840K1AA -8.97E-02 100% +- 9.3E-02 1.00E+01U

YMTFA62 SO 010(160-18615-4)

TestAmerica Inc


software.


rptTALRchSaSum

mary2 V5.6 A2002


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Parameter MDLUnits

Client Id

Work Order

Report No. : 69359


Yield

51966SDG No:


Qual



2 RER2CRDLBatch

6231049 RL-LSC-008

YMTFA62 SO 010(160-18615-4)

1.85E-01CARBON-14 PCI_GM840J1AA -7.21E-02 100% +- 9.2E-02 1.00E+01U

YMTFA67 SO 010(160-18615-3)

1.88E-01CARBON-14 PCI_GM840G1AA -5.48E-02 100% +- 9.4E-02 1.00E+01U

YMTFA69 SO 010(160-18615-2)

1.88E-01CARBON-14 PCI_GM840E1AA -3.31E-02 100% +- 9.4E-02 1.00E+01U

YMTFA70 SO 010(160-18615-1)

1.92E-01CARBON-14 PCI_GM84X91AA -7.75E-02 100% +- 9.5E-02 1.00E+01U

74No. of Results:

TestAmerica Inc


software.


rptTALRchSaSum

mary2 V5.6 A2002


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23-Sep-16Date:

Parameter MDLUnits

Batch

Work Order

Report No. : 69364


Yield

51961SDG No.:


Qual

QC Results Summary

LCS

Recovery Bias

Ordered by Method, Batch No, QC Type,.

2

L4SO

6231057 BLANK QC,

6.46E-02PLUTONIUM-238 PCI_GM842A1AA 93% 1.62E-02 +- 3.3E-02 U

4.56E-02PLUTONIUM-239/240 PCI_G 93% 1.06E-02 +- 2.3E-02 U

6231057 LCS,

5.08E-02PLUTONIUM-239/240 PCI_GM842A1AC 90% 97% 0.03.26E+00 +- 7.0E-01

C0SR

6231058 BLANK QC,

4.79E-02URANIUM-233/234 PCI_GM842C1AA 95% 5.14E-03 +- 1.9E-02 U

3.82E-02URANIUM-235/236 PCI_G 95% -1.10E-03 +- 1.8E-02 U

4.13E-02URANIUM-238 PCI_G 95% -1.83E-03 +- 1.8E-02 U

6231058 LCS,

4.13E-02URANIUM-233/234 PCI_GM842C1AC 105% 88% -0.11.89E+00 +- 4.1E-01

3.52E-02URANIUM-238 PCI_G 105% 86% -0.11.93E+00 +- 4.2E-01

L4SX

6231059 BLANK QC,

9.56E-02AMERICIUM-241 PCI_GM842D1AA 62% 2.61E-02 +- 5.0E-02 U

6231059 LCS,

1.50E-01AMERICIUM-241 PCI_GM842D1AC 35% 104% 0.03.44E+00 +- 1.0E+00

L4S1

6231060 BLANK QC,

5.53E-02THORIUM-228 PCI_GM842E1AA 97% 9.82E-03 +- 2.5E-02 U

4.32E-02THORIUM-230 PCI_G 97% 1.18E-02 +- 2.4E-02 U

4.32E-02THORIUM-232 PCI_G 97% -4.71E-04 +- 2.4E-02 U

6231060 LCS,

6.29E-02THORIUM-230 PCI_GM842E1AC 71% 78% -0.21.30E+00 +- 3.7E-01

E7XW

6231062 BLANK QC,

4.95E-02NEPTUNIUM-237 PCI_GM842G1AA 78% -1.43E-03 +- 2.4E-02 U

6231062 LCS,

5.60E-02NEPTUNIUM-237 PCI_GM842G1AC 73% 99% 0.01.25E+00 +- 4.4E-01

RL-LSC-008

6231061 BLANK QC,

1.91E-01CARBON-14 PCI_GM842F1AA 100% -3.38E-02 +- 9.5E-02 U

6231061 LCS,

1.92E-01CARBON-14 PCI_GM842F1AC 100% 99% 0.07.24E+00 +- 5.1E-01

18No. of Results:

TestAmerica Inc

U Qual - Analyzed for but not detected above limiting criteria, Mdc/Mda/Mdl, Total Uncert, RDL or not identified by gamma scan software.

Bias - (Result/Expected)-1 as defined by ANSI N13.30.

rptSTLRchQcSum

mary V5.6 A2002


1

2

3

4

5

6

7

8

9

10

11

12

13

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ID

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5.2

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17

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9M

84V

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ID

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4.7

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AM

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6231060

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9M

84V

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ID

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1

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1.9

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9/2

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rptS

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Sam

ple

V5.6

A2002

TestA

merica L

abora

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Inc.

13

of 52 9/26/2016

1

2

3

4

5

6

7

8

9

10

11

12

13

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No

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9M

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Rep

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DB

ID

:E

7X

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ple

V5.6

A2002

TestA

merica L

abora

tories,

Inc.

14

of 52 9/26/2016

1

2

3

4

5

6

7

8

9

10

11

12

13

Lo

t-S

am

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No

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SD

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YM

TF

A 3

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6 1

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Rep

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DB

ID

:L4S

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9.1

0E

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3.5

E-0

29

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6231058

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h:

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Ord

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9M

84V

W10

Rep

ort

DB

ID

:C

0S

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2.7

3E

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1.4

E-0

16

.36

E-0

27

8%

UR

AN

IUM

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34

PC

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9/1

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218

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1.3

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9/1

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2.4

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AN

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PC

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9/1

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6231059

Batc

h:

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Ord

er:

9M

84V

W10

Rep

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DB

ID

:L4S

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1.7

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3.8

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AM

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M-2

41

PC

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9/1

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420

g

0.2

3

0.9

1

U

1.0

0E

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01

.59

E-0

2

6231060

Batc

h:

M84V

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Ord

er:

9M

84V

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Rep

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DB

ID

:L4S

1

4.0

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1.7

E-0

16

.23

E-0

29

8%

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9/2

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Level

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on

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me.

rptS

TL

Rch

Sam

ple

V5.6

A2002

TestA

merica L

abora

tories,

Inc.

15

of 52 9/26/2016

1

2

3

4

5

6

7

8

9

10

11

12

13

Lo

t-S

am

ple

No

.:

SD

G:

YM

TF

A 3

4 S

O 0

02(1

60-1

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)

51961

Matr

ix:

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Receiv

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Date

:8/1

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01

6 1

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Date

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69364

Rst/

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22

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9/2

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6231061

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Ord

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9M

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Rep

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ID

:R

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4E

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21

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PC

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9/3

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2

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Inc.

18

of 52 9/26/2016

1

2

3

4

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6

7

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2

3

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9M

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Ord

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2

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ID

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2

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2

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1

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32

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2

3

4

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6

7

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10

11

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0 p

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62

31

06

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ID

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1

9.8

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25

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29

7%

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6 1

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9/2

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6

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7

0.9

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33

of 52 9/26/2016

1

2

3

4

5

6

7

8

9

10

11

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13

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34

of 52 9/26/2016

1

2

3

4

5

6

7

8

9

10

11

12

13

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ID

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73

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ID

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71

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s:

75

12

5

6231057

Batc

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Ord

er:

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ID

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90

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0

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7%

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imit

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75

12

5

6231059

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ER

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12

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7N

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Inc.

35

of 52 9/26/2016

1

2

3

4

5

6

7

8

9

10

11

12

13


1

2

3

4

5

6

7

8

9

10

11

12

13

ANALYTICAL REPORT 6 - Energy.gov · 2016-09-26 · ANALYTICAL REPORT TestAmerica Laboratories, Inc....

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Transcript of ANALYTICAL REPORT 6 - Energy.gov · 2016-09-26 · ANALYTICAL REPORT TestAmerica Laboratories, Inc....