1 2 3 4 5 ANALYTICAL REPORT 6 - Naperville Park District · 2017-12-07 · ANALYTICAL REPORT...
Transcript of 1 2 3 4 5 ANALYTICAL REPORT 6 - Naperville Park District · 2017-12-07 · ANALYTICAL REPORT...
ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Chicago2417 Bond StreetUniversity Park, IL 60484Tel: (708)534-5200
TestAmerica Job ID: 500-46374-1TestAmerica Sample Delivery Group: 500-46374-1Client Project/Site: Naperville Sportsman Club
For:Shaw Environmental & Infrastructure, Inc1607 East Main StreetSuite ESaint Charles, Illinois 60174
Attn: Jeffrey Cademartori
Authorized for release by:5/24/2012 4:50:47 PMCindy PritchardProject Mgmt. [email protected]
Designee for
Richard WrightProject Manager [email protected]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Shaw Environmental & Infrastructure, IncProject/Site: Naperville Sportsman Club
TestAmerica Job ID: 500-46374-1SDG: 500-46374-1
Page 2 of 39TestAmerica Chicago
5/24/2012
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39
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Case NarrativeClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-46374-1
Project/Site: Naperville Sportsman Club SDG: 500-46374-1
Job ID: 500-46374-1
Laboratory: TestAmerica Chicago
Narrative
Job Narrative
500-46374-1
Comments
No additional comments.
Receipt
The samples were received on 5/16/2012 7:00 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 4.0º C.
GC/MS Semi VOA
Method(s) 8270C: The following sample was diluted due to the abundance of target analytes: G19 (0-6") (500-46374-5). Elevated
reporting limits (RLs) are provided.
No other analytical or quality issues were noted.
Metals
Method(s) 7471A: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for 500-46374-1 were outside control limits for Hg. The
associated laboratory control sample (LCS) recovery met acceptance criteria.
No other analytical or quality issues were noted.
General Chemistry
No analytical or quality issues were noted.
Organic Prep
No analytical or quality issues were noted.
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Detection SummaryTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Client Sample ID: E24 (0-6") Lab Sample ID: 500-46374-1
☼Benzo[b]fluoranthene
RL
0.043 mg/Kg
MDL
0.0084
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J0.011
☼Chrysene 0.043 mg/Kg0.0098 Total/NA8270C10.020 J
☼Arsenic 1.2 mg/Kg0.26 Total/NA6010B123
☼Barium 1.2 mg/Kg0.14 Total/NA6010B161
☼Cadmium 0.24 mg/Kg0.060 Total/NA6010B10.36
☼Chromium 1.2 mg/Kg0.20 Total/NA6010B120
☼Copper 1.2 mg/Kg0.33 Total/NA6010B136
☼Lead 0.60 mg/Kg0.21 Total/NA6010B119
☼Selenium 1.2 mg/Kg0.35 Total/NA6010B10.47 J
☼Zinc 2.4 mg/Kg0.83 Total/NA6010B165
☼Mercury 0.021 mg/Kg0.0064 Total/NA7471A10.035
pH 0.200 SU0.200 Total/NA9045C17.76
Client Sample ID: G9 (0-6") Lab Sample ID: 500-46374-3
☼Benzo[a]pyrene
RL
0.045 mg/Kg
MDL
0.0083
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J0.0089
☼Benzo[b]fluoranthene 0.045 mg/Kg0.0088 Total/NA8270C10.014 J
☼Chrysene 0.045 mg/Kg0.010 Total/NA8270C10.011 J
☼Antimony 2.6 mg/Kg0.34 Total/NA6010B11.7 J B
☼Arsenic 1.3 mg/Kg0.28 Total/NA6010B16.3
☼Barium 1.3 mg/Kg0.15 Total/NA6010B194
☼Cadmium 0.26 mg/Kg0.064 Total/NA6010B10.23 J
☼Chromium 1.3 mg/Kg0.22 Total/NA6010B115
☼Copper 1.3 mg/Kg0.35 Total/NA6010B120
☼Lead 0.65 mg/Kg0.22 Total/NA6010B147
☼Zinc 2.6 mg/Kg0.89 Total/NA6010B151
☼Mercury 0.021 mg/Kg0.0063 Total/NA7471A10.040
pH 0.200 SU0.200 Total/NA9045C17.22
Client Sample ID: G19 (0-6") Lab Sample ID: 500-46374-5
☼Acenaphthene
RL
0.51 mg/Kg
MDL
0.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA5J0.19
☼Anthracene 0.51 mg/Kg0.12 Total/NA8270C50.29 J
☼Benzo[a]anthracene 0.51 mg/Kg0.11 Total/NA8270C53.1
☼Benzo[a]pyrene 0.51 mg/Kg0.093 Total/NA8270C54.7
☼Benzo[b]fluoranthene 0.51 mg/Kg0.099 Total/NA8270C56.0
☼Benzo[g,h,i]perylene 0.51 mg/Kg0.17 Total/NA8270C52.6
☼Benzo[k]fluoranthene 0.51 mg/Kg0.12 Total/NA8270C52.2
☼Chrysene 0.51 mg/Kg0.11 Total/NA8270C53.9
☼Dibenz(a,h)anthracene 0.51 mg/Kg0.14 Total/NA8270C50.66
☼Fluoranthene 0.51 mg/Kg0.21 Total/NA8270C53.9
☼Fluorene 0.51 mg/Kg0.12 Total/NA8270C50.13 J
☼Indeno[1,2,3-cd]pyrene 0.51 mg/Kg0.17 Total/NA8270C52.5
☼Phenanthrene 0.51 mg/Kg0.21 Total/NA8270C51.2
☼Pyrene 0.51 mg/Kg0.18 Total/NA8270C53.9
☼Antimony 6.4 mg/Kg0.85 Total/NA6010B14.2 J B
☼Arsenic 3.2 mg/Kg0.70 Total/NA6010B113
☼Barium 3.2 mg/Kg0.38 Total/NA6010B185
☼Cadmium 0.64 mg/Kg0.16 Total/NA6010B10.64
☼Chromium 3.2 mg/Kg0.54 Total/NA6010B115
☼Copper 3.2 mg/Kg0.87 Total/NA6010B11600
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Detection SummaryTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Client Sample ID: G19 (0-6") (Continued) Lab Sample ID: 500-46374-5
☼Lead
RL
1.6 mg/Kg
MDL
0.55
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B Total/NA1190
☼Selenium 3.2 mg/Kg0.92 Total/NA6010B11.2 J
☼Zinc 6.4 mg/Kg2.2 Total/NA6010B1810
☼Mercury 0.049 mg/Kg0.015 Total/NA7471A10.045 J
pH 0.200 SU0.200 Total/NA9045C17.63
Client Sample ID: I9 (0-6") Lab Sample ID: 500-46374-7
☼Benzo[a]anthracene
RL
0.055 mg/Kg
MDL
0.012
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J0.017
☼Benzo[a]pyrene 0.055 mg/Kg0.010 Total/NA8270C10.022 J
☼Benzo[b]fluoranthene 0.055 mg/Kg0.011 Total/NA8270C10.031 J
☼Benzo[k]fluoranthene 0.055 mg/Kg0.013 Total/NA8270C10.015 J
☼Chrysene 0.055 mg/Kg0.013 Total/NA8270C10.024 J
☼Fluoranthene 0.055 mg/Kg0.023 Total/NA8270C10.034 J
☼Pyrene 0.055 mg/Kg0.020 Total/NA8270C10.030 J
☼Antimony 2.9 mg/Kg0.39 Total/NA6010B133 B
☼Arsenic 1.5 mg/Kg0.32 Total/NA6010B139
☼Barium 1.5 mg/Kg0.17 Total/NA6010B1100
☼Cadmium 0.29 mg/Kg0.073 Total/NA6010B10.32
☼Chromium 1.5 mg/Kg0.25 Total/NA6010B115
☼Copper 1.5 mg/Kg0.40 Total/NA6010B121
☼Lead 0.73 mg/Kg0.25 Total/NA6010B15400
☼Selenium 1.5 mg/Kg0.42 Total/NA6010B10.89 J
☼Zinc 2.9 mg/Kg1.0 Total/NA6010B164
☼Mercury 0.027 mg/Kg0.0081 Total/NA7471A10.050
pH 0.200 SU0.200 Total/NA9045C17.55
Client Sample ID: I18 (0-6") Lab Sample ID: 500-46374-9
☼Benzo[a]anthracene
RL
0.047 mg/Kg
MDL
0.010
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J0.014
☼Benzo[a]pyrene 0.047 mg/Kg0.0087 Total/NA8270C10.021 J
☼Benzo[b]fluoranthene 0.047 mg/Kg0.0093 Total/NA8270C10.028 J
☼Chrysene 0.047 mg/Kg0.011 Total/NA8270C10.032 J
☼Pyrene 0.047 mg/Kg0.017 Total/NA8270C10.019 J
☼Antimony 2.9 mg/Kg0.38 Total/NA6010B10.70 J B
☼Arsenic 1.4 mg/Kg0.31 Total/NA6010B12.2
☼Barium 1.4 mg/Kg0.17 Total/NA6010B172
☼Cadmium 0.29 mg/Kg0.071 Total/NA6010B10.25 J
☼Chromium 1.4 mg/Kg0.24 Total/NA6010B115
☼Copper 1.4 mg/Kg0.39 Total/NA6010B118
☼Lead 0.71 mg/Kg0.25 Total/NA6010B169
☼Zinc 2.9 mg/Kg0.98 Total/NA6010B149
☼Mercury 0.022 mg/Kg0.0069 Total/NA7471A10.027
pH 0.200 SU0.200 Total/NA9045C18.21
Client Sample ID: J4 (0-6") Lab Sample ID: 500-46374-11
☼Benzo[a]anthracene
RL
0.069 mg/Kg
MDL
0.015
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J0.023
☼Benzo[a]pyrene 0.069 mg/Kg0.013 Total/NA8270C10.017 J
☼Benzo[b]fluoranthene 0.069 mg/Kg0.013 Total/NA8270C10.025 J
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Detection SummaryTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Client Sample ID: J4 (0-6") (Continued) Lab Sample ID: 500-46374-11
☼Chrysene
RL
0.069 mg/Kg
MDL
0.016
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J0.032
☼Fluoranthene 0.069 mg/Kg0.028 Total/NA8270C10.057 J
☼Phenanthrene 0.069 mg/Kg0.029 Total/NA8270C10.12
☼Pyrene 0.069 mg/Kg0.025 Total/NA8270C10.039 J
☼Antimony 4.2 mg/Kg0.55 Total/NA6010B11.6 J B
☼Arsenic 2.1 mg/Kg0.45 Total/NA6010B111
☼Barium 2.1 mg/Kg0.25 Total/NA6010B1110
☼Cadmium 0.42 mg/Kg0.10 Total/NA6010B10.23 J
☼Chromium 2.1 mg/Kg0.35 Total/NA6010B118
☼Copper 2.1 mg/Kg0.56 Total/NA6010B124
☼Lead 1.0 mg/Kg0.36 Total/NA6010B140
☼Selenium 2.1 mg/Kg0.60 Total/NA6010B10.70 J
☼Zinc 4.2 mg/Kg1.4 Total/NA6010B199
☼Mercury 0.034 mg/Kg0.010 Total/NA7471A10.049
pH 0.200 SU0.200 Total/NA9045C17.78
Client Sample ID: J13 (0-6") Lab Sample ID: 500-46374-13
☼Benzo[a]anthracene
RL
0.068 mg/Kg
MDL
0.014
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA10.081
☼Benzo[a]pyrene 0.068 mg/Kg0.013 Total/NA8270C10.12
☼Benzo[b]fluoranthene 0.068 mg/Kg0.013 Total/NA8270C10.17
☼Benzo[g,h,i]perylene 0.068 mg/Kg0.023 Total/NA8270C10.072
☼Benzo[k]fluoranthene 0.068 mg/Kg0.016 Total/NA8270C10.062 J
☼Chrysene 0.068 mg/Kg0.016 Total/NA8270C10.12
☼Fluoranthene 0.068 mg/Kg0.028 Total/NA8270C10.14
☼Indeno[1,2,3-cd]pyrene 0.068 mg/Kg0.023 Total/NA8270C10.064 J
☼Phenanthrene 0.068 mg/Kg0.029 Total/NA8270C10.075
☼Pyrene 0.068 mg/Kg0.025 Total/NA8270C10.14
☼Antimony 3.6 mg/Kg0.48 Total/NA6010B146 B
☼Arsenic 1.8 mg/Kg0.39 Total/NA6010B192
☼Barium 1.8 mg/Kg0.22 Total/NA6010B170
☼Cadmium 0.36 mg/Kg0.090 Total/NA6010B11.1
☼Chromium 1.8 mg/Kg0.30 Total/NA6010B1510
☼Copper 1.8 mg/Kg0.49 Total/NA6010B1580
☼Lead 0.91 mg/Kg0.31 Total/NA6010B16400
☼Selenium 1.8 mg/Kg0.52 Total/NA6010B12.3
☼Silver 0.91 mg/Kg0.11 Total/NA6010B10.48 J
☼Zinc 3.6 mg/Kg1.2 Total/NA6010B167
☼Mercury 0.032 mg/Kg0.0099 Total/NA7471A10.040
pH 0.200 SU0.200 Total/NA9045C17.72
Client Sample ID: J15 (0-6") Lab Sample ID: 500-46374-15
☼Acenaphthene
RL
0.062 mg/Kg
MDL
0.019
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J0.050
☼Anthracene 0.062 mg/Kg0.015 Total/NA8270C10.047 J
☼Benzo[a]anthracene 0.062 mg/Kg0.013 Total/NA8270C10.65
☼Benzo[a]pyrene 0.062 mg/Kg0.011 Total/NA8270C11.1
☼Benzo[b]fluoranthene 0.062 mg/Kg0.012 Total/NA8270C11.3
☼Benzo[g,h,i]perylene 0.062 mg/Kg0.021 Total/NA8270C10.53
☼Benzo[k]fluoranthene 0.062 mg/Kg0.015 Total/NA8270C10.54
☼Chrysene 0.062 mg/Kg0.014 Total/NA8270C10.77
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Detection SummaryTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Client Sample ID: J15 (0-6") (Continued) Lab Sample ID: 500-46374-15
☼Dibenz(a,h)anthracene
RL
0.062 mg/Kg
MDL
0.017
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA10.16
☼Fluoranthene 0.062 mg/Kg0.025 Total/NA8270C10.74
☼Fluorene 0.062 mg/Kg0.014 Total/NA8270C10.026 J
☼Indeno[1,2,3-cd]pyrene 0.062 mg/Kg0.021 Total/NA8270C10.50
☼Naphthalene 0.062 mg/Kg0.012 Total/NA8270C10.012 J
☼Phenanthrene 0.062 mg/Kg0.026 Total/NA8270C10.28
☼Pyrene 0.062 mg/Kg0.022 Total/NA8270C10.82
☼Antimony 3.6 mg/Kg0.48 Total/NA6010B115 B
☼Arsenic 1.8 mg/Kg0.40 Total/NA6010B130
☼Barium 1.8 mg/Kg0.22 Total/NA6010B157
☼Cadmium 0.36 mg/Kg0.090 Total/NA6010B10.67
☼Chromium 1.8 mg/Kg0.30 Total/NA6010B127
☼Copper 1.8 mg/Kg0.49 Total/NA6010B127
☼Lead 0.91 mg/Kg0.31 Total/NA6010B13000
☼Selenium 1.8 mg/Kg0.52 Total/NA6010B11.3 J
☼Silver 0.91 mg/Kg0.11 Total/NA6010B10.31 J
☼Zinc 3.6 mg/Kg1.2 Total/NA6010B153
☼Mercury 0.028 mg/Kg0.0084 Total/NA7471A10.040
pH 0.200 SU0.200 Total/NA9045C17.76
Client Sample ID: J24 (0-6") Lab Sample ID: 500-46374-17
☼Antimony
RL
2.5 mg/Kg
MDL
0.33
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B Total/NA1J B0.39
☼Arsenic 1.3 mg/Kg0.27 Total/NA6010B17.6
☼Barium 1.3 mg/Kg0.15 Total/NA6010B1110
☼Cadmium 0.25 mg/Kg0.062 Total/NA6010B10.16 J
☼Chromium 1.3 mg/Kg0.21 Total/NA6010B124
☼Copper 1.3 mg/Kg0.34 Total/NA6010B129
☼Lead 0.63 mg/Kg0.22 Total/NA6010B120
☼Selenium 1.3 mg/Kg0.36 Total/NA6010B10.82 J
☼Zinc 2.5 mg/Kg0.86 Total/NA6010B163
☼Mercury 0.021 mg/Kg0.0064 Total/NA7471A10.063
pH 0.200 SU0.200 Total/NA9045C17.70
Client Sample ID: K7 (0-6") Lab Sample ID: 500-46374-19
☼Benzo[a]anthracene
RL
0.075 mg/Kg
MDL
0.016
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J0.035
☼Benzo[a]pyrene 0.075 mg/Kg0.014 Total/NA8270C10.046 J
☼Benzo[b]fluoranthene 0.075 mg/Kg0.015 Total/NA8270C10.058 J
☼Benzo[k]fluoranthene 0.075 mg/Kg0.018 Total/NA8270C10.026 J
☼Chrysene 0.075 mg/Kg0.017 Total/NA8270C10.050 J
☼Fluoranthene 0.075 mg/Kg0.031 Total/NA8270C10.081
☼Phenanthrene 0.075 mg/Kg0.032 Total/NA8270C10.046 J
☼Pyrene 0.075 mg/Kg0.027 Total/NA8270C10.068 J
☼Antimony 4.6 mg/Kg0.61 Total/NA6010B12.2 J B
☼Arsenic 2.3 mg/Kg0.50 Total/NA6010B115
☼Barium 2.3 mg/Kg0.28 Total/NA6010B1120
☼Chromium 2.3 mg/Kg0.39 Total/NA6010B185
☼Copper 2.3 mg/Kg0.63 Total/NA6010B1320
☼Lead 1.2 mg/Kg0.40 Total/NA6010B11900
☼Selenium 2.3 mg/Kg0.66 Total/NA6010B12.2 J
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Detection SummaryTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Client Sample ID: K7 (0-6") (Continued) Lab Sample ID: 500-46374-19
☼Zinc
RL
4.6 mg/Kg
MDL
1.6
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B Total/NA173
☼Mercury 0.038 mg/Kg0.011 Total/NA7471A10.052
pH 0.200 SU0.200 Total/NA9045C17.77
Client Sample ID: K11 (0-6") Lab Sample ID: 500-46374-21
☼Antimony
RL
2.9 mg/Kg
MDL
0.39
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B Total/NA1J B1.6
☼Arsenic 1.5 mg/Kg0.32 Total/NA6010B17.0
☼Barium 1.5 mg/Kg0.17 Total/NA6010B1150
☼Cadmium 0.29 mg/Kg0.072 Total/NA6010B10.073 J
☼Chromium 1.5 mg/Kg0.24 Total/NA6010B123
☼Copper 1.5 mg/Kg0.39 Total/NA6010B121
☼Lead 0.73 mg/Kg0.25 Total/NA6010B138
☼Selenium 1.5 mg/Kg0.42 Total/NA6010B10.62 J
☼Zinc 2.9 mg/Kg1.0 Total/NA6010B159
☼Mercury 0.024 mg/Kg0.0073 Total/NA7471A10.060
pH 0.200 SU0.200 Total/NA9045C17.71
Client Sample ID: L5 (0-6") Lab Sample ID: 500-46374-23
☼Benzo[b]fluoranthene
RL
0.052 mg/Kg
MDL
0.010
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J0.013
☼Chrysene 0.052 mg/Kg0.012 Total/NA8270C10.012 J
☼Antimony 3.0 mg/Kg0.40 Total/NA6010B10.66 J B
☼Arsenic 1.5 mg/Kg0.33 Total/NA6010B13.8
☼Barium 1.5 mg/Kg0.18 Total/NA6010B178
☼Cadmium 0.30 mg/Kg0.075 Total/NA6010B10.24 J
☼Chromium 1.5 mg/Kg0.25 Total/NA6010B115
☼Copper 1.5 mg/Kg0.41 Total/NA6010B123
☼Lead 0.75 mg/Kg0.26 Total/NA6010B130
☼Zinc 3.0 mg/Kg1.0 Total/NA6010B149
☼Mercury 0.025 mg/Kg0.0076 Total/NA7471A10.045
pH 0.200 SU0.200 Total/NA9045C18.27
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Method SummaryTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Method Method Description LaboratoryProtocol
SW8468270C Semivolatile Organic Compounds (GC/MS) TAL CHI
SW8466010B Metals (ICP) TAL CHI
SW8467471A Mercury (CVAA) TAL CHI
SW8469045C pH TAL CHI
EPAMoisture Percent Moisture TAL CHI
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200
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Sample SummaryTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
500-46374-1 E24 (0-6") Solid 05/09/12 10:31 05/16/12 07:00
500-46374-3 G9 (0-6") Solid 05/09/12 12:20 05/16/12 07:00
500-46374-5 G19 (0-6") Solid 05/09/12 16:08 05/16/12 07:00
500-46374-7 I9 (0-6") Solid 05/09/12 13:22 05/16/12 07:00
500-46374-9 I18 (0-6") Solid 05/07/12 15:45 05/16/12 07:00
500-46374-11 J4 (0-6") Solid 05/09/12 14:40 05/16/12 07:00
500-46374-13 J13 (0-6") Solid 05/07/12 13:40 05/16/12 07:00
500-46374-15 J15 (0-6") Solid 05/07/12 13:00 05/16/12 07:00
500-46374-17 J24 (0-6") Solid 05/09/12 11:00 05/16/12 07:00
500-46374-19 K7 (0-6") Solid 05/07/12 16:30 05/16/12 07:00
500-46374-21 K11 (0-6") Solid 05/07/12 14:25 05/16/12 07:00
500-46374-23 L5 (0-6") Solid 05/09/12 15:20 05/16/12 07:00
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Client Sample ResultsTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-1Client Sample ID: E24 (0-6")Matrix: SolidDate Collected: 05/09/12 10:31
Percent Solids: 74.2Date Received: 05/16/12 07:00
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.043 0.043 0.013 mg/Kg ☼ 05/18/12 07:14 05/20/12 20:37 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.043 0.010 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Acenaphthylene <0.043
0.043 0.010 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Anthracene <0.043
0.043 0.0091 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Benzo[a]anthracene <0.043
0.043 0.0079 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Benzo[a]pyrene <0.043
0.043 0.0084 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Benzo[b]fluoranthene 0.011 J
0.043 0.015 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Benzo[g,h,i]perylene <0.043
0.043 0.010 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Benzo[k]fluoranthene <0.043
0.043 0.0098 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Chrysene 0.020 J
0.043 0.012 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Dibenz(a,h)anthracene <0.043
0.043 0.018 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Fluoranthene <0.043
0.043 0.0099 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Fluorene <0.043
0.043 0.015 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Indeno[1,2,3-cd]pyrene <0.043
0.043 0.0084 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Naphthalene <0.043
0.043 0.018 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Phenanthrene <0.043
0.043 0.016 mg/Kg 05/18/12 07:14 05/20/12 20:37 1☼Pyrene <0.043
2-Fluorobiphenyl 78 30 - 119 05/18/12 07:14 05/20/12 20:37 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 76 05/18/12 07:14 05/20/12 20:37 130 - 115
Terphenyl-d14 96 05/18/12 07:14 05/20/12 20:37 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony <2.4 2.4 0.32 mg/Kg ☼ 05/17/12 08:40 05/18/12 18:24 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.2 0.26 mg/Kg 05/17/12 08:40 05/18/12 18:24 1☼Arsenic 23
1.2 0.14 mg/Kg 05/17/12 08:40 05/18/12 18:24 1☼Barium 61
0.24 0.060 mg/Kg 05/17/12 08:40 05/18/12 18:24 1☼Cadmium 0.36
1.2 0.20 mg/Kg 05/17/12 08:40 05/18/12 18:24 1☼Chromium 20
1.2 0.33 mg/Kg 05/17/12 08:40 05/18/12 18:24 1☼Copper 36
0.60 0.21 mg/Kg 05/17/12 08:40 05/18/12 18:24 1☼Lead 19
1.2 0.35 mg/Kg 05/17/12 08:40 05/18/12 18:24 1☼Selenium 0.47 J
0.60 0.072 mg/Kg 05/17/12 08:40 05/18/12 18:24 1☼Silver <0.60
2.4 0.83 mg/Kg 05/17/12 08:40 05/18/12 18:24 1☼Zinc 65
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.035 0.021 0.0064 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:12 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.76 0.200 0.200 SU 05/16/12 16:39 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-3Client Sample ID: G9 (0-6")Matrix: SolidDate Collected: 05/09/12 12:20
Percent Solids: 70.5Date Received: 05/16/12 07:00
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.045 0.045 0.014 mg/Kg ☼ 05/18/12 07:14 05/20/12 20:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.045 0.010 mg/Kg 05/18/12 07:14 05/20/12 20:53 1☼Acenaphthylene <0.045
0.045 0.011 mg/Kg 05/18/12 07:14 05/20/12 20:53 1☼Anthracene <0.045
0.045 0.0095 mg/Kg 05/18/12 07:14 05/20/12 20:53 1☼Benzo[a]anthracene <0.045
0.045 0.0083 mg/Kg 05/18/12 07:14 05/20/12 20:53 1☼Benzo[a]pyrene 0.0089 J
0.045 0.0088 mg/Kg 05/18/12 07:14 05/20/12 20:53 1☼Benzo[b]fluoranthene 0.014 J
0.045 0.015 mg/Kg 05/18/12 07:14 05/20/12 20:53 1☼Benzo[g,h,i]perylene <0.045
0.045 0.011 mg/Kg 05/18/12 07:14 05/20/12 20:53 1☼Benzo[k]fluoranthene <0.045
0.045 0.010 mg/Kg 05/18/12 07:14 05/20/12 20:53 1☼Chrysene 0.011 J
0.045 0.013 mg/Kg 05/18/12 07:14 05/20/12 20:53 1☼Dibenz(a,h)anthracene <0.045
0.045 0.019 mg/Kg 05/18/12 07:14 05/20/12 20:53 1☼Fluoranthene <0.045
0.045 0.010 mg/Kg 05/18/12 07:14 05/20/12 20:53 1☼Fluorene <0.045
0.045 0.015 mg/Kg 05/18/12 07:14 05/20/12 20:53 1☼Indeno[1,2,3-cd]pyrene <0.045
0.045 0.0088 mg/Kg 05/18/12 07:14 05/20/12 20:53 1☼Naphthalene <0.045
0.045 0.019 mg/Kg 05/18/12 07:14 05/20/12 20:53 1☼Phenanthrene <0.045
0.045 0.016 mg/Kg 05/18/12 07:14 05/20/12 20:53 1☼Pyrene <0.045
2-Fluorobiphenyl 66 30 - 119 05/18/12 07:14 05/20/12 20:53 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 60 05/18/12 07:14 05/20/12 20:53 130 - 115
Terphenyl-d14 90 05/18/12 07:14 05/20/12 20:53 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 1.7 J B 2.6 0.34 mg/Kg ☼ 05/17/12 08:40 05/18/12 18:31 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.3 0.28 mg/Kg 05/17/12 08:40 05/18/12 18:31 1☼Arsenic 6.3
1.3 0.15 mg/Kg 05/17/12 08:40 05/18/12 18:31 1☼Barium 94
0.26 0.064 mg/Kg 05/17/12 08:40 05/18/12 18:31 1☼Cadmium 0.23 J
1.3 0.22 mg/Kg 05/17/12 08:40 05/18/12 18:31 1☼Chromium 15
1.3 0.35 mg/Kg 05/17/12 08:40 05/18/12 18:31 1☼Copper 20
0.65 0.22 mg/Kg 05/17/12 08:40 05/18/12 18:31 1☼Lead 47
1.3 0.37 mg/Kg 05/17/12 08:40 05/18/12 18:31 1☼Selenium <1.3
0.65 0.078 mg/Kg 05/17/12 08:40 05/18/12 18:31 1☼Silver <0.65
2.6 0.89 mg/Kg 05/17/12 08:40 05/18/12 18:31 1☼Zinc 51
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.040 0.021 0.0063 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:23 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.22 0.200 0.200 SU 05/16/12 16:41 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-5Client Sample ID: G19 (0-6")Matrix: SolidDate Collected: 05/09/12 16:08
Percent Solids: 30.8Date Received: 05/16/12 07:00
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene 0.19 J 0.51 0.15 mg/Kg ☼ 05/18/12 07:14 05/20/12 21:10 5
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.51 0.12 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Acenaphthylene <0.51
0.51 0.12 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Anthracene 0.29 J
0.51 0.11 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Benzo[a]anthracene 3.1
0.51 0.093 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Benzo[a]pyrene 4.7
0.51 0.099 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Benzo[b]fluoranthene 6.0
0.51 0.17 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Benzo[g,h,i]perylene 2.6
0.51 0.12 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Benzo[k]fluoranthene 2.2
0.51 0.11 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Chrysene 3.9
0.51 0.14 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Dibenz(a,h)anthracene 0.66
0.51 0.21 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Fluoranthene 3.9
0.51 0.12 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Fluorene 0.13 J
0.51 0.17 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Indeno[1,2,3-cd]pyrene 2.5
0.51 0.098 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Naphthalene <0.51
0.51 0.21 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Phenanthrene 1.2
0.51 0.18 mg/Kg 05/18/12 07:14 05/20/12 21:10 5☼Pyrene 3.9
2-Fluorobiphenyl 71 30 - 119 05/18/12 07:14 05/20/12 21:10 5
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 60 05/18/12 07:14 05/20/12 21:10 530 - 115
Terphenyl-d14 96 05/18/12 07:14 05/20/12 21:10 536 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 4.2 J B 6.4 0.85 mg/Kg ☼ 05/17/12 08:40 05/18/12 18:37 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
3.2 0.70 mg/Kg 05/17/12 08:40 05/18/12 18:37 1☼Arsenic 13
3.2 0.38 mg/Kg 05/17/12 08:40 05/18/12 18:37 1☼Barium 85
0.64 0.16 mg/Kg 05/17/12 08:40 05/18/12 18:37 1☼Cadmium 0.64
3.2 0.54 mg/Kg 05/17/12 08:40 05/18/12 18:37 1☼Chromium 15
3.2 0.87 mg/Kg 05/17/12 08:40 05/18/12 18:37 1☼Copper 1600
1.6 0.55 mg/Kg 05/17/12 08:40 05/18/12 18:37 1☼Lead 190
3.2 0.92 mg/Kg 05/17/12 08:40 05/18/12 18:37 1☼Selenium 1.2 J
1.6 0.19 mg/Kg 05/17/12 08:40 05/18/12 18:37 1☼Silver <1.6
6.4 2.2 mg/Kg 05/17/12 08:40 05/18/12 18:37 1☼Zinc 810
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.045 J 0.049 0.015 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:25 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.63 0.200 0.200 SU 05/16/12 16:43 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-7Client Sample ID: I9 (0-6")Matrix: SolidDate Collected: 05/09/12 13:22
Percent Solids: 59.2Date Received: 05/16/12 07:00
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.055 0.055 0.017 mg/Kg ☼ 05/18/12 07:14 05/20/12 21:27 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.055 0.013 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Acenaphthylene <0.055
0.055 0.013 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Anthracene <0.055
0.055 0.012 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Benzo[a]anthracene 0.017 J
0.055 0.010 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Benzo[a]pyrene 0.022 J
0.055 0.011 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Benzo[b]fluoranthene 0.031 J
0.055 0.019 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Benzo[g,h,i]perylene <0.055
0.055 0.013 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Benzo[k]fluoranthene 0.015 J
0.055 0.013 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Chrysene 0.024 J
0.055 0.015 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Dibenz(a,h)anthracene <0.055
0.055 0.023 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Fluoranthene 0.034 J
0.055 0.013 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Fluorene <0.055
0.055 0.019 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Indeno[1,2,3-cd]pyrene <0.055
0.055 0.011 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Naphthalene <0.055
0.055 0.023 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Phenanthrene <0.055
0.055 0.020 mg/Kg 05/18/12 07:14 05/20/12 21:27 1☼Pyrene 0.030 J
2-Fluorobiphenyl 64 30 - 119 05/18/12 07:14 05/20/12 21:27 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 57 05/18/12 07:14 05/20/12 21:27 130 - 115
Terphenyl-d14 83 05/18/12 07:14 05/20/12 21:27 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 33 B 2.9 0.39 mg/Kg ☼ 05/17/12 08:40 05/18/12 18:43 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.5 0.32 mg/Kg 05/17/12 08:40 05/18/12 18:43 1☼Arsenic 39
1.5 0.17 mg/Kg 05/17/12 08:40 05/18/12 18:43 1☼Barium 100
0.29 0.073 mg/Kg 05/17/12 08:40 05/18/12 18:43 1☼Cadmium 0.32
1.5 0.25 mg/Kg 05/17/12 08:40 05/18/12 18:43 1☼Chromium 15
1.5 0.40 mg/Kg 05/17/12 08:40 05/18/12 18:43 1☼Copper 21
0.73 0.25 mg/Kg 05/17/12 08:40 05/18/12 18:43 1☼Lead 5400
1.5 0.42 mg/Kg 05/17/12 08:40 05/18/12 18:43 1☼Selenium 0.89 J
0.73 0.088 mg/Kg 05/17/12 08:40 05/18/12 18:43 1☼Silver <0.73
2.9 1.0 mg/Kg 05/17/12 08:40 05/18/12 18:43 1☼Zinc 64
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.050 0.027 0.0081 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:27 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.55 0.200 0.200 SU 05/16/12 16:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-9Client Sample ID: I18 (0-6")Matrix: SolidDate Collected: 05/07/12 15:45
Percent Solids: 66.7Date Received: 05/16/12 07:00
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.047 0.047 0.014 mg/Kg ☼ 05/18/12 07:14 05/20/12 21:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.047 0.011 mg/Kg 05/18/12 07:14 05/20/12 21:44 1☼Acenaphthylene <0.047
0.047 0.011 mg/Kg 05/18/12 07:14 05/20/12 21:44 1☼Anthracene <0.047
0.047 0.010 mg/Kg 05/18/12 07:14 05/20/12 21:44 1☼Benzo[a]anthracene 0.014 J
0.047 0.0087 mg/Kg 05/18/12 07:14 05/20/12 21:44 1☼Benzo[a]pyrene 0.021 J
0.047 0.0093 mg/Kg 05/18/12 07:14 05/20/12 21:44 1☼Benzo[b]fluoranthene 0.028 J
0.047 0.016 mg/Kg 05/18/12 07:14 05/20/12 21:44 1☼Benzo[g,h,i]perylene <0.047
0.047 0.011 mg/Kg 05/18/12 07:14 05/20/12 21:44 1☼Benzo[k]fluoranthene <0.047
0.047 0.011 mg/Kg 05/18/12 07:14 05/20/12 21:44 1☼Chrysene 0.032 J
0.047 0.013 mg/Kg 05/18/12 07:14 05/20/12 21:44 1☼Dibenz(a,h)anthracene <0.047
0.047 0.020 mg/Kg 05/18/12 07:14 05/20/12 21:44 1☼Fluoranthene <0.047
0.047 0.011 mg/Kg 05/18/12 07:14 05/20/12 21:44 1☼Fluorene <0.047
0.047 0.016 mg/Kg 05/18/12 07:14 05/20/12 21:44 1☼Indeno[1,2,3-cd]pyrene <0.047
0.047 0.0092 mg/Kg 05/18/12 07:14 05/20/12 21:44 1☼Naphthalene <0.047
0.047 0.020 mg/Kg 05/18/12 07:14 05/20/12 21:44 1☼Phenanthrene <0.047
0.047 0.017 mg/Kg 05/18/12 07:14 05/20/12 21:44 1☼Pyrene 0.019 J
2-Fluorobiphenyl 76 30 - 119 05/18/12 07:14 05/20/12 21:44 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 70 05/18/12 07:14 05/20/12 21:44 130 - 115
Terphenyl-d14 102 05/18/12 07:14 05/20/12 21:44 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 0.70 J B 2.9 0.38 mg/Kg ☼ 05/17/12 08:40 05/18/12 18:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.4 0.31 mg/Kg 05/17/12 08:40 05/18/12 18:49 1☼Arsenic 2.2
1.4 0.17 mg/Kg 05/17/12 08:40 05/18/12 18:49 1☼Barium 72
0.29 0.071 mg/Kg 05/17/12 08:40 05/18/12 18:49 1☼Cadmium 0.25 J
1.4 0.24 mg/Kg 05/17/12 08:40 05/18/12 18:49 1☼Chromium 15
1.4 0.39 mg/Kg 05/17/12 08:40 05/18/12 18:49 1☼Copper 18
0.71 0.25 mg/Kg 05/17/12 08:40 05/18/12 18:49 1☼Lead 69
1.4 0.41 mg/Kg 05/17/12 08:40 05/18/12 18:49 1☼Selenium <1.4
0.71 0.086 mg/Kg 05/17/12 08:40 05/18/12 18:49 1☼Silver <0.71
2.9 0.98 mg/Kg 05/17/12 08:40 05/18/12 18:49 1☼Zinc 49
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.027 0.022 0.0069 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:28 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 8.21 0.200 0.200 SU 05/16/12 16:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-11Client Sample ID: J4 (0-6")Matrix: SolidDate Collected: 05/09/12 14:40
Percent Solids: 46.0Date Received: 05/16/12 07:00
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.069 0.069 0.021 mg/Kg ☼ 05/18/12 07:14 05/20/12 22:00 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.069 0.016 mg/Kg 05/18/12 07:14 05/20/12 22:00 1☼Acenaphthylene <0.069
0.069 0.016 mg/Kg 05/18/12 07:14 05/20/12 22:00 1☼Anthracene <0.069
0.069 0.015 mg/Kg 05/18/12 07:14 05/20/12 22:00 1☼Benzo[a]anthracene 0.023 J
0.069 0.013 mg/Kg 05/18/12 07:14 05/20/12 22:00 1☼Benzo[a]pyrene 0.017 J
0.069 0.013 mg/Kg 05/18/12 07:14 05/20/12 22:00 1☼Benzo[b]fluoranthene 0.025 J
0.069 0.023 mg/Kg 05/18/12 07:14 05/20/12 22:00 1☼Benzo[g,h,i]perylene <0.069
0.069 0.017 mg/Kg 05/18/12 07:14 05/20/12 22:00 1☼Benzo[k]fluoranthene <0.069
0.069 0.016 mg/Kg 05/18/12 07:14 05/20/12 22:00 1☼Chrysene 0.032 J
0.069 0.019 mg/Kg 05/18/12 07:14 05/20/12 22:00 1☼Dibenz(a,h)anthracene <0.069
0.069 0.028 mg/Kg 05/18/12 07:14 05/20/12 22:00 1☼Fluoranthene 0.057 J
0.069 0.016 mg/Kg 05/18/12 07:14 05/20/12 22:00 1☼Fluorene <0.069
0.069 0.023 mg/Kg 05/18/12 07:14 05/20/12 22:00 1☼Indeno[1,2,3-cd]pyrene <0.069
0.069 0.013 mg/Kg 05/18/12 07:14 05/20/12 22:00 1☼Naphthalene <0.069
0.069 0.029 mg/Kg 05/18/12 07:14 05/20/12 22:00 1☼Phenanthrene 0.12
0.069 0.025 mg/Kg 05/18/12 07:14 05/20/12 22:00 1☼Pyrene 0.039 J
2-Fluorobiphenyl 69 30 - 119 05/18/12 07:14 05/20/12 22:00 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 62 05/18/12 07:14 05/20/12 22:00 130 - 115
Terphenyl-d14 97 05/18/12 07:14 05/20/12 22:00 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 1.6 J B 4.2 0.55 mg/Kg ☼ 05/17/12 08:40 05/18/12 18:55 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.1 0.45 mg/Kg 05/17/12 08:40 05/18/12 18:55 1☼Arsenic 11
2.1 0.25 mg/Kg 05/17/12 08:40 05/18/12 18:55 1☼Barium 110
0.42 0.10 mg/Kg 05/17/12 08:40 05/18/12 18:55 1☼Cadmium 0.23 J
2.1 0.35 mg/Kg 05/17/12 08:40 05/18/12 18:55 1☼Chromium 18
2.1 0.56 mg/Kg 05/17/12 08:40 05/18/12 18:55 1☼Copper 24
1.0 0.36 mg/Kg 05/17/12 08:40 05/18/12 18:55 1☼Lead 40
2.1 0.60 mg/Kg 05/17/12 08:40 05/18/12 18:55 1☼Selenium 0.70 J
1.0 0.13 mg/Kg 05/17/12 08:40 05/18/12 18:55 1☼Silver <1.0
4.2 1.4 mg/Kg 05/17/12 08:40 05/18/12 18:55 1☼Zinc 99
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.049 0.034 0.010 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.78 0.200 0.200 SU 05/16/12 16:50 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica ChicagoPage 16 of 39 5/24/2012
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Client Sample ResultsTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-13Client Sample ID: J13 (0-6")Matrix: SolidDate Collected: 05/07/12 13:40
Percent Solids: 47.7Date Received: 05/16/12 07:00
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.068 0.068 0.021 mg/Kg ☼ 05/18/12 07:14 05/20/12 22:17 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.068 0.016 mg/Kg 05/18/12 07:14 05/20/12 22:17 1☼Acenaphthylene <0.068
0.068 0.016 mg/Kg 05/18/12 07:14 05/20/12 22:17 1☼Anthracene <0.068
0.068 0.014 mg/Kg 05/18/12 07:14 05/20/12 22:17 1☼Benzo[a]anthracene 0.081
0.068 0.013 mg/Kg 05/18/12 07:14 05/20/12 22:17 1☼Benzo[a]pyrene 0.12
0.068 0.013 mg/Kg 05/18/12 07:14 05/20/12 22:17 1☼Benzo[b]fluoranthene 0.17
0.068 0.023 mg/Kg 05/18/12 07:14 05/20/12 22:17 1☼Benzo[g,h,i]perylene 0.072
0.068 0.016 mg/Kg 05/18/12 07:14 05/20/12 22:17 1☼Benzo[k]fluoranthene 0.062 J
0.068 0.016 mg/Kg 05/18/12 07:14 05/20/12 22:17 1☼Chrysene 0.12
0.068 0.019 mg/Kg 05/18/12 07:14 05/20/12 22:17 1☼Dibenz(a,h)anthracene <0.068
0.068 0.028 mg/Kg 05/18/12 07:14 05/20/12 22:17 1☼Fluoranthene 0.14
0.068 0.016 mg/Kg 05/18/12 07:14 05/20/12 22:17 1☼Fluorene <0.068
0.068 0.023 mg/Kg 05/18/12 07:14 05/20/12 22:17 1☼Indeno[1,2,3-cd]pyrene 0.064 J
0.068 0.013 mg/Kg 05/18/12 07:14 05/20/12 22:17 1☼Naphthalene <0.068
0.068 0.029 mg/Kg 05/18/12 07:14 05/20/12 22:17 1☼Phenanthrene 0.075
0.068 0.025 mg/Kg 05/18/12 07:14 05/20/12 22:17 1☼Pyrene 0.14
2-Fluorobiphenyl 60 30 - 119 05/18/12 07:14 05/20/12 22:17 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 49 05/18/12 07:14 05/20/12 22:17 130 - 115
Terphenyl-d14 86 05/18/12 07:14 05/20/12 22:17 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 46 B 3.6 0.48 mg/Kg ☼ 05/17/12 08:40 05/18/12 19:02 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.8 0.39 mg/Kg 05/17/12 08:40 05/18/12 19:02 1☼Arsenic 92
1.8 0.22 mg/Kg 05/17/12 08:40 05/18/12 19:02 1☼Barium 70
0.36 0.090 mg/Kg 05/17/12 08:40 05/18/12 19:02 1☼Cadmium 1.1
1.8 0.30 mg/Kg 05/17/12 08:40 05/18/12 19:02 1☼Chromium 510
1.8 0.49 mg/Kg 05/17/12 08:40 05/18/12 19:02 1☼Copper 580
0.91 0.31 mg/Kg 05/17/12 08:40 05/18/12 19:02 1☼Lead 6400
1.8 0.52 mg/Kg 05/17/12 08:40 05/18/12 19:02 1☼Selenium 2.3
0.91 0.11 mg/Kg 05/17/12 08:40 05/18/12 19:02 1☼Silver 0.48 J
3.6 1.2 mg/Kg 05/17/12 08:40 05/18/12 19:02 1☼Zinc 67
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.040 0.032 0.0099 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:32 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.72 0.200 0.200 SU 05/16/12 16:52 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-15Client Sample ID: J15 (0-6")Matrix: SolidDate Collected: 05/07/12 13:00
Percent Solids: 52.0Date Received: 05/16/12 07:00
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene 0.050 J 0.062 0.019 mg/Kg ☼ 05/18/12 07:14 05/20/12 22:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.062 0.014 mg/Kg 05/18/12 07:14 05/20/12 22:34 1☼Acenaphthylene <0.062
0.062 0.015 mg/Kg 05/18/12 07:14 05/20/12 22:34 1☼Anthracene 0.047 J
0.062 0.013 mg/Kg 05/18/12 07:14 05/20/12 22:34 1☼Benzo[a]anthracene 0.65
0.062 0.011 mg/Kg 05/18/12 07:14 05/20/12 22:34 1☼Benzo[a]pyrene 1.1
0.062 0.012 mg/Kg 05/18/12 07:14 05/20/12 22:34 1☼Benzo[b]fluoranthene 1.3
0.062 0.021 mg/Kg 05/18/12 07:14 05/20/12 22:34 1☼Benzo[g,h,i]perylene 0.53
0.062 0.015 mg/Kg 05/18/12 07:14 05/20/12 22:34 1☼Benzo[k]fluoranthene 0.54
0.062 0.014 mg/Kg 05/18/12 07:14 05/20/12 22:34 1☼Chrysene 0.77
0.062 0.017 mg/Kg 05/18/12 07:14 05/20/12 22:34 1☼Dibenz(a,h)anthracene 0.16
0.062 0.025 mg/Kg 05/18/12 07:14 05/20/12 22:34 1☼Fluoranthene 0.74
0.062 0.014 mg/Kg 05/18/12 07:14 05/20/12 22:34 1☼Fluorene 0.026 J
0.062 0.021 mg/Kg 05/18/12 07:14 05/20/12 22:34 1☼Indeno[1,2,3-cd]pyrene 0.50
0.062 0.012 mg/Kg 05/18/12 07:14 05/20/12 22:34 1☼Naphthalene 0.012 J
0.062 0.026 mg/Kg 05/18/12 07:14 05/20/12 22:34 1☼Phenanthrene 0.28
0.062 0.022 mg/Kg 05/18/12 07:14 05/20/12 22:34 1☼Pyrene 0.82
2-Fluorobiphenyl 59 30 - 119 05/18/12 07:14 05/20/12 22:34 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 53 05/18/12 07:14 05/20/12 22:34 130 - 115
Terphenyl-d14 89 05/18/12 07:14 05/20/12 22:34 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 15 B 3.6 0.48 mg/Kg ☼ 05/17/12 08:40 05/18/12 19:08 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.8 0.40 mg/Kg 05/17/12 08:40 05/18/12 19:08 1☼Arsenic 30
1.8 0.22 mg/Kg 05/17/12 08:40 05/18/12 19:08 1☼Barium 57
0.36 0.090 mg/Kg 05/17/12 08:40 05/18/12 19:08 1☼Cadmium 0.67
1.8 0.30 mg/Kg 05/17/12 08:40 05/18/12 19:08 1☼Chromium 27
1.8 0.49 mg/Kg 05/17/12 08:40 05/18/12 19:08 1☼Copper 27
0.91 0.31 mg/Kg 05/17/12 08:40 05/18/12 19:08 1☼Lead 3000
1.8 0.52 mg/Kg 05/17/12 08:40 05/18/12 19:08 1☼Selenium 1.3 J
0.91 0.11 mg/Kg 05/17/12 08:40 05/18/12 19:08 1☼Silver 0.31 J
3.6 1.2 mg/Kg 05/17/12 08:40 05/18/12 19:08 1☼Zinc 53
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.040 0.028 0.0084 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.76 0.200 0.200 SU 05/16/12 16:54 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-17Client Sample ID: J24 (0-6")Matrix: SolidDate Collected: 05/09/12 11:00
Percent Solids: 72.2Date Received: 05/16/12 07:00
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.044 0.044 0.013 mg/Kg ☼ 05/18/12 07:14 05/20/12 22:51 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.044 0.010 mg/Kg 05/18/12 07:14 05/20/12 22:51 1☼Acenaphthylene <0.044
0.044 0.011 mg/Kg 05/18/12 07:14 05/20/12 22:51 1☼Anthracene <0.044
0.044 0.0094 mg/Kg 05/18/12 07:14 05/20/12 22:51 1☼Benzo[a]anthracene <0.044
0.044 0.0082 mg/Kg 05/18/12 07:14 05/20/12 22:51 1☼Benzo[a]pyrene <0.044
0.044 0.0087 mg/Kg 05/18/12 07:14 05/20/12 22:51 1☼Benzo[b]fluoranthene <0.044
0.044 0.015 mg/Kg 05/18/12 07:14 05/20/12 22:51 1☼Benzo[g,h,i]perylene <0.044
0.044 0.011 mg/Kg 05/18/12 07:14 05/20/12 22:51 1☼Benzo[k]fluoranthene <0.044
0.044 0.010 mg/Kg 05/18/12 07:14 05/20/12 22:51 1☼Chrysene <0.044
0.044 0.013 mg/Kg 05/18/12 07:14 05/20/12 22:51 1☼Dibenz(a,h)anthracene <0.044
0.044 0.018 mg/Kg 05/18/12 07:14 05/20/12 22:51 1☼Fluoranthene <0.044
0.044 0.010 mg/Kg 05/18/12 07:14 05/20/12 22:51 1☼Fluorene <0.044
0.044 0.015 mg/Kg 05/18/12 07:14 05/20/12 22:51 1☼Indeno[1,2,3-cd]pyrene <0.044
0.044 0.0086 mg/Kg 05/18/12 07:14 05/20/12 22:51 1☼Naphthalene <0.044
0.044 0.019 mg/Kg 05/18/12 07:14 05/20/12 22:51 1☼Phenanthrene <0.044
0.044 0.016 mg/Kg 05/18/12 07:14 05/20/12 22:51 1☼Pyrene <0.044
2-Fluorobiphenyl 69 30 - 119 05/18/12 07:14 05/20/12 22:51 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 64 05/18/12 07:14 05/20/12 22:51 130 - 115
Terphenyl-d14 89 05/18/12 07:14 05/20/12 22:51 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 0.39 J B 2.5 0.33 mg/Kg ☼ 05/17/12 08:40 05/18/12 19:14 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.3 0.27 mg/Kg 05/17/12 08:40 05/18/12 19:14 1☼Arsenic 7.6
1.3 0.15 mg/Kg 05/17/12 08:40 05/18/12 19:14 1☼Barium 110
0.25 0.062 mg/Kg 05/17/12 08:40 05/18/12 19:14 1☼Cadmium 0.16 J
1.3 0.21 mg/Kg 05/17/12 08:40 05/18/12 19:14 1☼Chromium 24
1.3 0.34 mg/Kg 05/17/12 08:40 05/18/12 19:14 1☼Copper 29
0.63 0.22 mg/Kg 05/17/12 08:40 05/18/12 19:14 1☼Lead 20
1.3 0.36 mg/Kg 05/17/12 08:40 05/18/12 19:14 1☼Selenium 0.82 J
0.63 0.076 mg/Kg 05/17/12 08:40 05/18/12 19:14 1☼Silver <0.63
2.5 0.86 mg/Kg 05/17/12 08:40 05/18/12 19:14 1☼Zinc 63
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.063 0.021 0.0064 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:36 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.70 0.200 0.200 SU 05/16/12 16:56 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-19Client Sample ID: K7 (0-6")Matrix: SolidDate Collected: 05/07/12 16:30
Percent Solids: 43.0Date Received: 05/16/12 07:00
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.075 0.075 0.023 mg/Kg ☼ 05/18/12 07:14 05/20/12 23:07 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.075 0.017 mg/Kg 05/18/12 07:14 05/20/12 23:07 1☼Acenaphthylene <0.075
0.075 0.018 mg/Kg 05/18/12 07:14 05/20/12 23:07 1☼Anthracene <0.075
0.075 0.016 mg/Kg 05/18/12 07:14 05/20/12 23:07 1☼Benzo[a]anthracene 0.035 J
0.075 0.014 mg/Kg 05/18/12 07:14 05/20/12 23:07 1☼Benzo[a]pyrene 0.046 J
0.075 0.015 mg/Kg 05/18/12 07:14 05/20/12 23:07 1☼Benzo[b]fluoranthene 0.058 J
0.075 0.026 mg/Kg 05/18/12 07:14 05/20/12 23:07 1☼Benzo[g,h,i]perylene <0.075
0.075 0.018 mg/Kg 05/18/12 07:14 05/20/12 23:07 1☼Benzo[k]fluoranthene 0.026 J
0.075 0.017 mg/Kg 05/18/12 07:14 05/20/12 23:07 1☼Chrysene 0.050 J
0.075 0.021 mg/Kg 05/18/12 07:14 05/20/12 23:07 1☼Dibenz(a,h)anthracene <0.075
0.075 0.031 mg/Kg 05/18/12 07:14 05/20/12 23:07 1☼Fluoranthene 0.081
0.075 0.017 mg/Kg 05/18/12 07:14 05/20/12 23:07 1☼Fluorene <0.075
0.075 0.026 mg/Kg 05/18/12 07:14 05/20/12 23:07 1☼Indeno[1,2,3-cd]pyrene <0.075
0.075 0.015 mg/Kg 05/18/12 07:14 05/20/12 23:07 1☼Naphthalene <0.075
0.075 0.032 mg/Kg 05/18/12 07:14 05/20/12 23:07 1☼Phenanthrene 0.046 J
0.075 0.027 mg/Kg 05/18/12 07:14 05/20/12 23:07 1☼Pyrene 0.068 J
2-Fluorobiphenyl 60 30 - 119 05/18/12 07:14 05/20/12 23:07 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 51 05/18/12 07:14 05/20/12 23:07 130 - 115
Terphenyl-d14 98 05/18/12 07:14 05/20/12 23:07 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 2.2 J B 4.6 0.61 mg/Kg ☼ 05/17/12 08:40 05/18/12 19:35 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.3 0.50 mg/Kg 05/17/12 08:40 05/18/12 19:35 1☼Arsenic 15
2.3 0.28 mg/Kg 05/17/12 08:40 05/18/12 19:35 1☼Barium 120
0.46 0.11 mg/Kg 05/17/12 08:40 05/18/12 19:35 1☼Cadmium <0.46
2.3 0.39 mg/Kg 05/17/12 08:40 05/18/12 19:35 1☼Chromium 85
2.3 0.63 mg/Kg 05/17/12 08:40 05/18/12 19:35 1☼Copper 320
1.2 0.40 mg/Kg 05/17/12 08:40 05/18/12 19:35 1☼Lead 1900
2.3 0.66 mg/Kg 05/17/12 08:40 05/18/12 19:35 1☼Selenium 2.2 J
1.2 0.14 mg/Kg 05/17/12 08:40 05/18/12 19:35 1☼Silver <1.2
4.6 1.6 mg/Kg 05/17/12 08:40 05/18/12 19:35 1☼Zinc 73
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.052 0.038 0.011 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:41 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.77 0.200 0.200 SU 05/16/12 16:59 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-21Client Sample ID: K11 (0-6")Matrix: SolidDate Collected: 05/07/12 14:25
Percent Solids: 67.0Date Received: 05/16/12 07:00
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.047 0.047 0.014 mg/Kg ☼ 05/18/12 07:14 05/20/12 23:24 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.047 0.011 mg/Kg 05/18/12 07:14 05/20/12 23:24 1☼Acenaphthylene <0.047
0.047 0.011 mg/Kg 05/18/12 07:14 05/20/12 23:24 1☼Anthracene <0.047
0.047 0.0099 mg/Kg 05/18/12 07:14 05/20/12 23:24 1☼Benzo[a]anthracene <0.047
0.047 0.0086 mg/Kg 05/18/12 07:14 05/20/12 23:24 1☼Benzo[a]pyrene <0.047
0.047 0.0091 mg/Kg 05/18/12 07:14 05/20/12 23:24 1☼Benzo[b]fluoranthene <0.047
0.047 0.016 mg/Kg 05/18/12 07:14 05/20/12 23:24 1☼Benzo[g,h,i]perylene <0.047
0.047 0.011 mg/Kg 05/18/12 07:14 05/20/12 23:24 1☼Benzo[k]fluoranthene <0.047
0.047 0.011 mg/Kg 05/18/12 07:14 05/20/12 23:24 1☼Chrysene <0.047
0.047 0.013 mg/Kg 05/18/12 07:14 05/20/12 23:24 1☼Dibenz(a,h)anthracene <0.047
0.047 0.019 mg/Kg 05/18/12 07:14 05/20/12 23:24 1☼Fluoranthene <0.047
0.047 0.011 mg/Kg 05/18/12 07:14 05/20/12 23:24 1☼Fluorene <0.047
0.047 0.016 mg/Kg 05/18/12 07:14 05/20/12 23:24 1☼Indeno[1,2,3-cd]pyrene <0.047
0.047 0.0091 mg/Kg 05/18/12 07:14 05/20/12 23:24 1☼Naphthalene <0.047
0.047 0.020 mg/Kg 05/18/12 07:14 05/20/12 23:24 1☼Phenanthrene <0.047
0.047 0.017 mg/Kg 05/18/12 07:14 05/20/12 23:24 1☼Pyrene <0.047
2-Fluorobiphenyl 62 30 - 119 05/18/12 07:14 05/20/12 23:24 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 60 05/18/12 07:14 05/20/12 23:24 130 - 115
Terphenyl-d14 88 05/18/12 07:14 05/20/12 23:24 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 1.6 J B 2.9 0.39 mg/Kg ☼ 05/17/12 08:40 05/18/12 19:41 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.5 0.32 mg/Kg 05/17/12 08:40 05/18/12 19:41 1☼Arsenic 7.0
1.5 0.17 mg/Kg 05/17/12 08:40 05/18/12 19:41 1☼Barium 150
0.29 0.072 mg/Kg 05/17/12 08:40 05/18/12 19:41 1☼Cadmium 0.073 J
1.5 0.24 mg/Kg 05/17/12 08:40 05/18/12 19:41 1☼Chromium 23
1.5 0.39 mg/Kg 05/17/12 08:40 05/18/12 19:41 1☼Copper 21
0.73 0.25 mg/Kg 05/17/12 08:40 05/18/12 19:41 1☼Lead 38
1.5 0.42 mg/Kg 05/17/12 08:40 05/18/12 19:41 1☼Selenium 0.62 J
0.73 0.088 mg/Kg 05/17/12 08:40 05/18/12 19:41 1☼Silver <0.73
2.9 1.0 mg/Kg 05/17/12 08:40 05/18/12 19:41 1☼Zinc 59
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.060 0.024 0.0073 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:43 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.71 0.200 0.200 SU 05/16/12 17:01 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-23Client Sample ID: L5 (0-6")Matrix: SolidDate Collected: 05/09/12 15:20
Percent Solids: 61.7Date Received: 05/16/12 07:00
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.052 0.052 0.016 mg/Kg ☼ 05/18/12 07:14 05/20/12 23:41 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.052 0.012 mg/Kg 05/18/12 07:14 05/20/12 23:41 1☼Acenaphthylene <0.052
0.052 0.012 mg/Kg 05/18/12 07:14 05/20/12 23:41 1☼Anthracene <0.052
0.052 0.011 mg/Kg 05/18/12 07:14 05/20/12 23:41 1☼Benzo[a]anthracene <0.052
0.052 0.0095 mg/Kg 05/18/12 07:14 05/20/12 23:41 1☼Benzo[a]pyrene <0.052
0.052 0.010 mg/Kg 05/18/12 07:14 05/20/12 23:41 1☼Benzo[b]fluoranthene 0.013 J
0.052 0.018 mg/Kg 05/18/12 07:14 05/20/12 23:41 1☼Benzo[g,h,i]perylene <0.052
0.052 0.012 mg/Kg 05/18/12 07:14 05/20/12 23:41 1☼Benzo[k]fluoranthene <0.052
0.052 0.012 mg/Kg 05/18/12 07:14 05/20/12 23:41 1☼Chrysene 0.012 J
0.052 0.015 mg/Kg 05/18/12 07:14 05/20/12 23:41 1☼Dibenz(a,h)anthracene <0.052
0.052 0.021 mg/Kg 05/18/12 07:14 05/20/12 23:41 1☼Fluoranthene <0.052
0.052 0.012 mg/Kg 05/18/12 07:14 05/20/12 23:41 1☼Fluorene <0.052
0.052 0.018 mg/Kg 05/18/12 07:14 05/20/12 23:41 1☼Indeno[1,2,3-cd]pyrene <0.052
0.052 0.010 mg/Kg 05/18/12 07:14 05/20/12 23:41 1☼Naphthalene <0.052
0.052 0.022 mg/Kg 05/18/12 07:14 05/20/12 23:41 1☼Phenanthrene <0.052
0.052 0.019 mg/Kg 05/18/12 07:14 05/20/12 23:41 1☼Pyrene <0.052
2-Fluorobiphenyl 73 30 - 119 05/18/12 07:14 05/20/12 23:41 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 66 05/18/12 07:14 05/20/12 23:41 130 - 115
Terphenyl-d14 98 05/18/12 07:14 05/20/12 23:41 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 0.66 J B 3.0 0.40 mg/Kg ☼ 05/17/12 08:40 05/18/12 19:47 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.5 0.33 mg/Kg 05/17/12 08:40 05/18/12 19:47 1☼Arsenic 3.8
1.5 0.18 mg/Kg 05/17/12 08:40 05/18/12 19:47 1☼Barium 78
0.30 0.075 mg/Kg 05/17/12 08:40 05/18/12 19:47 1☼Cadmium 0.24 J
1.5 0.25 mg/Kg 05/17/12 08:40 05/18/12 19:47 1☼Chromium 15
1.5 0.41 mg/Kg 05/17/12 08:40 05/18/12 19:47 1☼Copper 23
0.75 0.26 mg/Kg 05/17/12 08:40 05/18/12 19:47 1☼Lead 30
1.5 0.43 mg/Kg 05/17/12 08:40 05/18/12 19:47 1☼Selenium <1.5
0.75 0.091 mg/Kg 05/17/12 08:40 05/18/12 19:47 1☼Silver <0.75
3.0 1.0 mg/Kg 05/17/12 08:40 05/18/12 19:47 1☼Zinc 49
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.045 0.025 0.0076 mg/Kg ☼ 05/16/12 14:41 05/18/12 10:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 8.27 0.200 0.200 SU 05/16/12 17:03 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Definitions/GlossaryTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Qualifiers
GC/MS Semi VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
F MS or MSD exceeds the control limits
B Compound was found in the blank and sample.
Glossary
These commonly used abbreviations may or may not be present in this report.
☼ Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CNF Contains no Free Liquid
DL, RA, RE, IN Indicates a Dilution, Reanalysis, Re-extraction, or additional Initial metals/anion analysis of the sample
EDL Estimated Detection Limit
EPA United States Environmental Protection Agency
MDL Method Detection Limit
ML Minimum Level (Dioxin)
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RL Reporting Limit
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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QC Association SummaryTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
GC/MS Semi VOA
Prep Batch: 150126
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3541500-46374-1 E24 (0-6") Total/NA
Solid 3541500-46374-3 G9 (0-6") Total/NA
Solid 3541500-46374-5 G19 (0-6") Total/NA
Solid 3541500-46374-7 I9 (0-6") Total/NA
Solid 3541500-46374-9 I18 (0-6") Total/NA
Solid 3541500-46374-11 J4 (0-6") Total/NA
Solid 3541500-46374-13 J13 (0-6") Total/NA
Solid 3541500-46374-15 J15 (0-6") Total/NA
Solid 3541500-46374-17 J24 (0-6") Total/NA
Solid 3541500-46374-19 K7 (0-6") Total/NA
Solid 3541500-46374-21 K11 (0-6") Total/NA
Solid 3541500-46374-23 L5 (0-6") Total/NA
Solid 3541LCS 500-150126/2-A Lab Control Sample Total/NA
Solid 3541MB 500-150126/1-A Method Blank Total/NA
Analysis Batch: 150266
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270C 150126500-46374-1 E24 (0-6") Total/NA
Solid 8270C 150126500-46374-3 G9 (0-6") Total/NA
Solid 8270C 150126500-46374-5 G19 (0-6") Total/NA
Solid 8270C 150126500-46374-7 I9 (0-6") Total/NA
Solid 8270C 150126500-46374-9 I18 (0-6") Total/NA
Solid 8270C 150126500-46374-11 J4 (0-6") Total/NA
Solid 8270C 150126500-46374-13 J13 (0-6") Total/NA
Solid 8270C 150126500-46374-15 J15 (0-6") Total/NA
Solid 8270C 150126500-46374-17 J24 (0-6") Total/NA
Solid 8270C 150126500-46374-19 K7 (0-6") Total/NA
Solid 8270C 150126500-46374-21 K11 (0-6") Total/NA
Solid 8270C 150126500-46374-23 L5 (0-6") Total/NA
Solid 8270C 150126LCS 500-150126/2-A Lab Control Sample Total/NA
Solid 8270C 150126MB 500-150126/1-A Method Blank Total/NA
Metals
Prep Batch: 149954
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471A500-46374-1 E24 (0-6") Total/NA
Solid 7471A500-46374-1 DU E24 (0-6") Total/NA
Solid 7471A500-46374-1 MS E24 (0-6") Total/NA
Solid 7471A500-46374-1 MSD E24 (0-6") Total/NA
Solid 7471A500-46374-3 G9 (0-6") Total/NA
Solid 7471A500-46374-5 G19 (0-6") Total/NA
Solid 7471A500-46374-7 I9 (0-6") Total/NA
Solid 7471A500-46374-9 I18 (0-6") Total/NA
Solid 7471A500-46374-11 J4 (0-6") Total/NA
Solid 7471A500-46374-13 J13 (0-6") Total/NA
Solid 7471A500-46374-15 J15 (0-6") Total/NA
Solid 7471A500-46374-17 J24 (0-6") Total/NA
Solid 7471A500-46374-19 K7 (0-6") Total/NA
Solid 7471A500-46374-21 K11 (0-6") Total/NA
Solid 7471A500-46374-23 L5 (0-6") Total/NA
Solid 7471ALCS 500-149954/8-A Lab Control Sample Total/NA
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QC Association SummaryTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Metals (Continued)
Prep Batch: 149954 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471AMB 500-149954/7-A Method Blank Total/NA
Prep Batch: 150013
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3050B500-46374-1 E24 (0-6") Total/NA
Solid 3050B500-46374-3 G9 (0-6") Total/NA
Solid 3050B500-46374-5 G19 (0-6") Total/NA
Solid 3050B500-46374-7 I9 (0-6") Total/NA
Solid 3050B500-46374-9 I18 (0-6") Total/NA
Solid 3050B500-46374-11 J4 (0-6") Total/NA
Solid 3050B500-46374-13 J13 (0-6") Total/NA
Solid 3050B500-46374-15 J15 (0-6") Total/NA
Solid 3050B500-46374-17 J24 (0-6") Total/NA
Solid 3050B500-46374-19 K7 (0-6") Total/NA
Solid 3050B500-46374-21 K11 (0-6") Total/NA
Solid 3050B500-46374-23 L5 (0-6") Total/NA
Solid 3050BLCS 500-150013/2-A Lab Control Sample Total/NA
Solid 3050BMB 500-150013/1-A Method Blank Total/NA
Analysis Batch: 150123
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010B 150013500-46374-1 E24 (0-6") Total/NA
Solid 6010B 150013500-46374-3 G9 (0-6") Total/NA
Solid 6010B 150013500-46374-5 G19 (0-6") Total/NA
Solid 6010B 150013500-46374-7 I9 (0-6") Total/NA
Solid 6010B 150013500-46374-9 I18 (0-6") Total/NA
Solid 6010B 150013500-46374-11 J4 (0-6") Total/NA
Solid 6010B 150013500-46374-13 J13 (0-6") Total/NA
Solid 6010B 150013500-46374-15 J15 (0-6") Total/NA
Solid 6010B 150013500-46374-17 J24 (0-6") Total/NA
Solid 6010B 150013500-46374-19 K7 (0-6") Total/NA
Solid 6010B 150013500-46374-21 K11 (0-6") Total/NA
Solid 6010B 150013500-46374-23 L5 (0-6") Total/NA
Solid 6010B 150013LCS 500-150013/2-A Lab Control Sample Total/NA
Solid 6010B 150013MB 500-150013/1-A Method Blank Total/NA
Analysis Batch: 150190
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471A 149954500-46374-1 E24 (0-6") Total/NA
Solid 7471A 149954500-46374-1 DU E24 (0-6") Total/NA
Solid 7471A 149954500-46374-1 MS E24 (0-6") Total/NA
Solid 7471A 149954500-46374-1 MSD E24 (0-6") Total/NA
Solid 7471A 149954500-46374-3 G9 (0-6") Total/NA
Solid 7471A 149954500-46374-5 G19 (0-6") Total/NA
Solid 7471A 149954500-46374-7 I9 (0-6") Total/NA
Solid 7471A 149954500-46374-9 I18 (0-6") Total/NA
Solid 7471A 149954500-46374-11 J4 (0-6") Total/NA
Solid 7471A 149954500-46374-13 J13 (0-6") Total/NA
Solid 7471A 149954500-46374-15 J15 (0-6") Total/NA
Solid 7471A 149954500-46374-17 J24 (0-6") Total/NA
Solid 7471A 149954500-46374-19 K7 (0-6") Total/NA
Solid 7471A 149954500-46374-21 K11 (0-6") Total/NA
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QC Association SummaryTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Metals (Continued)
Analysis Batch: 150190 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471A 149954500-46374-23 L5 (0-6") Total/NA
Solid 7471A 149954LCS 500-149954/8-A Lab Control Sample Total/NA
Solid 7471A 149954MB 500-149954/7-A Method Blank Total/NA
General Chemistry
Analysis Batch: 149849
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture500-46374-1 E24 (0-6") Total/NA
Solid Moisture500-46374-3 G9 (0-6") Total/NA
Solid Moisture500-46374-5 G19 (0-6") Total/NA
Solid Moisture500-46374-7 I9 (0-6") Total/NA
Solid Moisture500-46374-9 I18 (0-6") Total/NA
Solid Moisture500-46374-11 J4 (0-6") Total/NA
Solid Moisture500-46374-13 J13 (0-6") Total/NA
Solid Moisture500-46374-15 J15 (0-6") Total/NA
Solid Moisture500-46374-17 J24 (0-6") Total/NA
Solid Moisture500-46374-19 K7 (0-6") Total/NA
Solid Moisture500-46374-21 K11 (0-6") Total/NA
Solid Moisture500-46374-23 L5 (0-6") Total/NA
Analysis Batch: 149927
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9045C500-46374-1 E24 (0-6") Total/NA
Solid 9045C500-46374-3 G9 (0-6") Total/NA
Solid 9045C500-46374-5 G19 (0-6") Total/NA
Solid 9045C500-46374-7 I9 (0-6") Total/NA
Solid 9045C500-46374-9 I18 (0-6") Total/NA
Solid 9045C500-46374-11 J4 (0-6") Total/NA
Solid 9045C500-46374-13 J13 (0-6") Total/NA
Solid 9045C500-46374-15 J15 (0-6") Total/NA
Solid 9045C500-46374-17 J24 (0-6") Total/NA
Solid 9045C500-46374-19 K7 (0-6") Total/NA
Solid 9045C500-46374-21 K11 (0-6") Total/NA
Solid 9045C500-46374-23 L5 (0-6") Total/NA
Solid 9045C500-46374-23 DU L5 (0-6") Total/NA
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Surrogate SummaryTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Method: 8270C - Semivolatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (30-119) (30-115) (36-134)
FBP NBZ TPH
78 76 96500-46374-1
Percent Surrogate Recovery (Acceptance Limits)
E24 (0-6")
66 60 90500-46374-3 G9 (0-6")
71 60 96500-46374-5 G19 (0-6")
64 57 83500-46374-7 I9 (0-6")
76 70 102500-46374-9 I18 (0-6")
69 62 97500-46374-11 J4 (0-6")
60 49 86500-46374-13 J13 (0-6")
59 53 89500-46374-15 J15 (0-6")
69 64 89500-46374-17 J24 (0-6")
60 51 98500-46374-19 K7 (0-6")
62 60 88500-46374-21 K11 (0-6")
73 66 98500-46374-23 L5 (0-6")
83 80 88LCS 500-150126/2-A Lab Control Sample
79 76 109MB 500-150126/1-A Method Blank
Surrogate Legend
FBP = 2-Fluorobiphenyl
NBZ = Nitrobenzene-d5
TPH = Terphenyl-d14
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QC Sample ResultsTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Method: 8270C - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 500-150126/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 150266 Prep Batch: 150126
RL MDL
Acenaphthene <0.033 0.033 0.0099 mg/Kg 05/18/12 07:14 05/20/12 17:31 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.033 0.00760.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Acenaphthylene
<0.033 0.00780.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Anthracene
<0.033 0.00700.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Benzo[a]anthracene
<0.033 0.00610.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Benzo[a]pyrene
<0.033 0.00650.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Benzo[b]fluoranthene
<0.033 0.0110.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Benzo[g,h,i]perylene
<0.033 0.00790.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Benzo[k]fluoranthene
<0.033 0.00750.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Chrysene
<0.033 0.00930.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Dibenz(a,h)anthracene
<0.033 0.0140.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Fluoranthene
<0.033 0.00760.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Fluorene
<0.033 0.0110.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Indeno[1,2,3-cd]pyrene
<0.033 0.00640.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Naphthalene
<0.033 0.0140.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Phenanthrene
<0.033 0.0120.033 mg/Kg 05/18/12 07:14 05/20/12 17:31 1Pyrene
2-Fluorobiphenyl 79 30 - 119 05/20/12 17:31 1
MB MB
Surrogate
05/18/12 07:14
Dil FacPrepared AnalyzedQualifier Limits%Recovery
76 05/18/12 07:14 05/20/12 17:31 1Nitrobenzene-d5 30 - 115
109 05/18/12 07:14 05/20/12 17:31 1Terphenyl-d14 36 - 134
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-150126/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 150266 Prep Batch: 150126
Acenaphthene 1.67 1.35 mg/Kg 81 67 - 110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 1.67 1.38 mg/Kg 83 67 - 110
Anthracene 1.67 1.35 mg/Kg 81 67 - 112
Benzo[a]anthracene 1.67 1.48 mg/Kg 89 68 - 117
Benzo[a]pyrene 1.67 1.48 mg/Kg 89 64 - 118
Benzo[b]fluoranthene 1.67 1.67 mg/Kg 100 60 - 118
Benzo[g,h,i]perylene 1.67 1.17 mg/Kg 70 66 - 130
Benzo[k]fluoranthene 1.67 1.38 mg/Kg 83 56 - 129
Chrysene 1.67 1.38 mg/Kg 83 66 - 118
Dibenz(a,h)anthracene 1.67 1.30 mg/Kg 78 62 - 126
Fluoranthene 1.67 1.49 mg/Kg 89 68 - 121
Fluorene 1.67 1.41 mg/Kg 84 66 - 112
Indeno[1,2,3-cd]pyrene 1.67 1.26 mg/Kg 76 67 - 127
Naphthalene 1.67 1.32 mg/Kg 79 65 - 110
Phenanthrene 1.67 1.41 mg/Kg 84 66 - 118
Pyrene 1.67 1.40 mg/Kg 84 66 - 119
2-Fluorobiphenyl 30 - 119
Surrogate
83
LCS LCS
Qualifier Limits%Recovery
80Nitrobenzene-d5 30 - 115
88Terphenyl-d14 36 - 134
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QC Sample ResultsTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Method: 6010B - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 500-150013/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 150123 Prep Batch: 150013
RL MDL
Antimony 0.280 J 2.0 0.27 mg/Kg 05/17/12 08:40 05/18/12 17:02 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<1.0 0.221.0 mg/Kg 05/17/12 08:40 05/18/12 17:02 1Arsenic
<1.0 0.121.0 mg/Kg 05/17/12 08:40 05/18/12 17:02 1Barium
<0.20 0.0500.20 mg/Kg 05/17/12 08:40 05/18/12 17:02 1Cadmium
<1.0 0.171.0 mg/Kg 05/17/12 08:40 05/18/12 17:02 1Chromium
<1.0 0.271.0 mg/Kg 05/17/12 08:40 05/18/12 17:02 1Copper
<0.50 0.170.50 mg/Kg 05/17/12 08:40 05/18/12 17:02 1Lead
<1.0 0.291.0 mg/Kg 05/17/12 08:40 05/18/12 17:02 1Selenium
<0.50 0.0600.50 mg/Kg 05/17/12 08:40 05/18/12 17:02 1Silver
<2.0 0.692.0 mg/Kg 05/17/12 08:40 05/18/12 17:02 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-150013/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 150123 Prep Batch: 150013
Antimony 50.0 44.9 mg/Kg 90 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 10.0 8.85 mg/Kg 88 80 - 120
Barium 200 189 mg/Kg 95 80 - 120
Cadmium 5.00 4.67 mg/Kg 93 80 - 120
Chromium 20.0 19.3 mg/Kg 96 80 - 120
Copper 25.0 24.0 mg/Kg 96 80 - 120
Lead 10.0 9.89 mg/Kg 99 80 - 120
Selenium 10.0 8.10 mg/Kg 81 80 - 120
Silver 5.00 4.62 mg/Kg 92 80 - 120
Zinc 50.0 47.0 mg/Kg 94 80 - 120
Method: 7471A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 500-149954/7-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 150190 Prep Batch: 149954
RL MDL
Mercury <0.017 0.017 0.0051 mg/Kg 05/16/12 14:41 05/18/12 10:09 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-149954/8-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 150190 Prep Batch: 149954
Mercury 0.167 0.201 mg/Kg 120 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: E24 (0-6")Lab Sample ID: 500-46374-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 150190 Prep Batch: 149954
Mercury 0.035 0.0986 0.181 F mg/Kg 149 75 - 125☼
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
TestAmerica ChicagoPage 29 of 39 5/24/2012
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QC Sample ResultsTestAmerica Job ID: 500-46374-1Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Method: 7471A - Mercury (CVAA) (Continued)
Client Sample ID: E24 (0-6")Lab Sample ID: 500-46374-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 150190 Prep Batch: 149954
Mercury 0.035 0.105 0.188 F mg/Kg 146 75 - 125 3 20☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: E24 (0-6")Lab Sample ID: 500-46374-1 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 150190 Prep Batch: 149954
Mercury 0.035 0.0387 mg/Kg 10 20☼
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: 9045C - pH
Client Sample ID: L5 (0-6")Lab Sample ID: 500-46374-23 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 149927
pH 8.27 8.300 SU 0.4
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
TestAmerica ChicagoPage 30 of 39 5/24/2012
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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-46374-1
Project/Site: Naperville Sportsman Club SDG: 500-46374-1
Client Sample ID: E24 (0-6") Lab Sample ID: 500-46374-1Matrix: SolidDate Collected: 05/09/12 10:31
Percent Solids: 74.2Date Received: 05/16/12 07:00
Prep 3541 05/18/12 07:14 STW150126 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 150266 05/20/12 20:37 DA TAL CHITotal/NA
Prep 3050B 150013 05/17/12 08:40 LAH TAL CHITotal/NA
Analysis 6010B 1 150123 05/18/12 18:24 TDS TAL CHITotal/NA
Prep 7471A 149954 05/16/12 14:41 MBG TAL CHITotal/NA
Analysis 7471A 1 150190 05/18/12 10:12 PFK TAL CHITotal/NA
Analysis Moisture 1 149849 05/16/12 09:01 CMV TAL CHITotal/NA
Analysis 9045C 1 149927 TAB TAL CHITotal/NA
05/16/12 16:39
05/16/12 16:41
(Start)
(End)
Client Sample ID: G9 (0-6") Lab Sample ID: 500-46374-3Matrix: SolidDate Collected: 05/09/12 12:20
Percent Solids: 70.5Date Received: 05/16/12 07:00
Prep 3541 05/18/12 07:14 STW150126 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 150266 05/20/12 20:53 DA TAL CHITotal/NA
Prep 3050B 150013 05/17/12 08:40 LAH TAL CHITotal/NA
Analysis 6010B 1 150123 05/18/12 18:31 TDS TAL CHITotal/NA
Prep 7471A 149954 05/16/12 14:41 MBG TAL CHITotal/NA
Analysis 7471A 1 150190 05/18/12 10:23 PFK TAL CHITotal/NA
Analysis Moisture 1 149849 05/16/12 09:01 CMV TAL CHITotal/NA
Analysis 9045C 1 149927 TAB TAL CHITotal/NA
05/16/12 16:41
05/16/12 16:43
(Start)
(End)
Client Sample ID: G19 (0-6") Lab Sample ID: 500-46374-5Matrix: SolidDate Collected: 05/09/12 16:08
Percent Solids: 30.8Date Received: 05/16/12 07:00
Prep 3541 05/18/12 07:14 STW150126 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 5 150266 05/20/12 21:10 DA TAL CHITotal/NA
Prep 3050B 150013 05/17/12 08:40 LAH TAL CHITotal/NA
Analysis 6010B 1 150123 05/18/12 18:37 TDS TAL CHITotal/NA
Prep 7471A 149954 05/16/12 14:41 MBG TAL CHITotal/NA
Analysis 7471A 1 150190 05/18/12 10:25 PFK TAL CHITotal/NA
Analysis Moisture 1 149849 05/16/12 09:01 CMV TAL CHITotal/NA
Analysis 9045C 1 149927 TAB TAL CHITotal/NA
05/16/12 16:43
05/16/12 16:46
(Start)
(End)
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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-46374-1
Project/Site: Naperville Sportsman Club SDG: 500-46374-1
Client Sample ID: I9 (0-6") Lab Sample ID: 500-46374-7Matrix: SolidDate Collected: 05/09/12 13:22
Percent Solids: 59.2Date Received: 05/16/12 07:00
Prep 3541 05/18/12 07:14 STW150126 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 150266 05/20/12 21:27 DA TAL CHITotal/NA
Prep 3050B 150013 05/17/12 08:40 LAH TAL CHITotal/NA
Analysis 6010B 1 150123 05/18/12 18:43 TDS TAL CHITotal/NA
Prep 7471A 149954 05/16/12 14:41 MBG TAL CHITotal/NA
Analysis 7471A 1 150190 05/18/12 10:27 PFK TAL CHITotal/NA
Analysis Moisture 1 149849 05/16/12 09:01 CMV TAL CHITotal/NA
Analysis 9045C 1 149927 TAB TAL CHITotal/NA
05/16/12 16:46
05/16/12 16:48
(Start)
(End)
Client Sample ID: I18 (0-6") Lab Sample ID: 500-46374-9Matrix: SolidDate Collected: 05/07/12 15:45
Percent Solids: 66.7Date Received: 05/16/12 07:00
Prep 3541 05/18/12 07:14 STW150126 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 150266 05/20/12 21:44 DA TAL CHITotal/NA
Prep 3050B 150013 05/17/12 08:40 LAH TAL CHITotal/NA
Analysis 6010B 1 150123 05/18/12 18:49 TDS TAL CHITotal/NA
Prep 7471A 149954 05/16/12 14:41 MBG TAL CHITotal/NA
Analysis 7471A 1 150190 05/18/12 10:28 PFK TAL CHITotal/NA
Analysis Moisture 1 149849 05/16/12 09:01 CMV TAL CHITotal/NA
Analysis 9045C 1 149927 TAB TAL CHITotal/NA
05/16/12 16:48
05/16/12 16:50
(Start)
(End)
Client Sample ID: J4 (0-6") Lab Sample ID: 500-46374-11Matrix: SolidDate Collected: 05/09/12 14:40
Percent Solids: 46.0Date Received: 05/16/12 07:00
Prep 3541 05/18/12 07:14 STW150126 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 150266 05/20/12 22:00 DA TAL CHITotal/NA
Prep 3050B 150013 05/17/12 08:40 LAH TAL CHITotal/NA
Analysis 6010B 1 150123 05/18/12 18:55 TDS TAL CHITotal/NA
Prep 7471A 149954 05/16/12 14:41 MBG TAL CHITotal/NA
Analysis 7471A 1 150190 05/18/12 10:30 PFK TAL CHITotal/NA
Analysis Moisture 1 149849 05/16/12 09:01 CMV TAL CHITotal/NA
Analysis 9045C 1 149927 TAB TAL CHITotal/NA
05/16/12 16:50
05/16/12 16:52
(Start)
(End)
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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-46374-1
Project/Site: Naperville Sportsman Club SDG: 500-46374-1
Client Sample ID: J13 (0-6") Lab Sample ID: 500-46374-13Matrix: SolidDate Collected: 05/07/12 13:40
Percent Solids: 47.7Date Received: 05/16/12 07:00
Prep 3541 05/18/12 07:14 STW150126 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 150266 05/20/12 22:17 DA TAL CHITotal/NA
Prep 3050B 150013 05/17/12 08:40 LAH TAL CHITotal/NA
Analysis 6010B 1 150123 05/18/12 19:02 TDS TAL CHITotal/NA
Prep 7471A 149954 05/16/12 14:41 MBG TAL CHITotal/NA
Analysis 7471A 1 150190 05/18/12 10:32 PFK TAL CHITotal/NA
Analysis Moisture 1 149849 05/16/12 09:01 CMV TAL CHITotal/NA
Analysis 9045C 1 149927 TAB TAL CHITotal/NA
05/16/12 16:52
05/16/12 16:54
(Start)
(End)
Client Sample ID: J15 (0-6") Lab Sample ID: 500-46374-15Matrix: SolidDate Collected: 05/07/12 13:00
Percent Solids: 52.0Date Received: 05/16/12 07:00
Prep 3541 05/18/12 07:14 STW150126 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 150266 05/20/12 22:34 DA TAL CHITotal/NA
Prep 3050B 150013 05/17/12 08:40 LAH TAL CHITotal/NA
Analysis 6010B 1 150123 05/18/12 19:08 TDS TAL CHITotal/NA
Prep 7471A 149954 05/16/12 14:41 MBG TAL CHITotal/NA
Analysis 7471A 1 150190 05/18/12 10:34 PFK TAL CHITotal/NA
Analysis Moisture 1 149849 05/16/12 09:01 CMV TAL CHITotal/NA
Analysis 9045C 1 149927 TAB TAL CHITotal/NA
05/16/12 16:54
05/16/12 16:56
(Start)
(End)
Client Sample ID: J24 (0-6") Lab Sample ID: 500-46374-17Matrix: SolidDate Collected: 05/09/12 11:00
Percent Solids: 72.2Date Received: 05/16/12 07:00
Prep 3541 05/18/12 07:14 STW150126 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 150266 05/20/12 22:51 DA TAL CHITotal/NA
Prep 3050B 150013 05/17/12 08:40 LAH TAL CHITotal/NA
Analysis 6010B 1 150123 05/18/12 19:14 TDS TAL CHITotal/NA
Prep 7471A 149954 05/16/12 14:41 MBG TAL CHITotal/NA
Analysis 7471A 1 150190 05/18/12 10:36 PFK TAL CHITotal/NA
Analysis Moisture 1 149849 05/16/12 09:01 CMV TAL CHITotal/NA
Analysis 9045C 1 149927 TAB TAL CHITotal/NA
05/16/12 16:56
05/16/12 16:59
(Start)
(End)
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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-46374-1
Project/Site: Naperville Sportsman Club SDG: 500-46374-1
Client Sample ID: K7 (0-6") Lab Sample ID: 500-46374-19Matrix: SolidDate Collected: 05/07/12 16:30
Percent Solids: 43.0Date Received: 05/16/12 07:00
Prep 3541 05/18/12 07:14 STW150126 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 150266 05/20/12 23:07 DA TAL CHITotal/NA
Prep 3050B 150013 05/17/12 08:40 LAH TAL CHITotal/NA
Analysis 6010B 1 150123 05/18/12 19:35 TDS TAL CHITotal/NA
Prep 7471A 149954 05/16/12 14:41 MBG TAL CHITotal/NA
Analysis 7471A 1 150190 05/18/12 10:41 PFK TAL CHITotal/NA
Analysis Moisture 1 149849 05/16/12 09:01 CMV TAL CHITotal/NA
Analysis 9045C 1 149927 TAB TAL CHITotal/NA
05/16/12 16:59
05/16/12 17:01
(Start)
(End)
Client Sample ID: K11 (0-6") Lab Sample ID: 500-46374-21Matrix: SolidDate Collected: 05/07/12 14:25
Percent Solids: 67.0Date Received: 05/16/12 07:00
Prep 3541 05/18/12 07:14 STW150126 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 150266 05/20/12 23:24 DA TAL CHITotal/NA
Prep 3050B 150013 05/17/12 08:40 LAH TAL CHITotal/NA
Analysis 6010B 1 150123 05/18/12 19:41 TDS TAL CHITotal/NA
Prep 7471A 149954 05/16/12 14:41 MBG TAL CHITotal/NA
Analysis 7471A 1 150190 05/18/12 10:43 PFK TAL CHITotal/NA
Analysis Moisture 1 149849 05/16/12 09:01 CMV TAL CHITotal/NA
Analysis 9045C 1 149927 TAB TAL CHITotal/NA
05/16/12 17:01
05/16/12 17:03
(Start)
(End)
Client Sample ID: L5 (0-6") Lab Sample ID: 500-46374-23Matrix: SolidDate Collected: 05/09/12 15:20
Percent Solids: 61.7Date Received: 05/16/12 07:00
Prep 3541 05/18/12 07:14 STW150126 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 150266 05/20/12 23:41 DA TAL CHITotal/NA
Prep 3050B 150013 05/17/12 08:40 LAH TAL CHITotal/NA
Analysis 6010B 1 150123 05/18/12 19:47 TDS TAL CHITotal/NA
Prep 7471A 149954 05/16/12 14:41 MBG TAL CHITotal/NA
Analysis 7471A 1 150190 05/18/12 10:45 PFK TAL CHITotal/NA
Analysis Moisture 1 149849 05/16/12 09:01 CMV TAL CHITotal/NA
Analysis 9045C 1 149927 TAB TAL CHITotal/NA
05/16/12 17:03
05/16/12 17:05
(Start)
(End)
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200
TestAmerica ChicagoPage 34 of 39 5/24/2012
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Certification SummaryClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-46374-1
Project/Site: Naperville Sportsman Club SDG: 500-46374-1
Laboratory Authority Program EPA Region Certification ID
TestAmerica Chicago R-194A2LAA2LA
TestAmerica Chicago 40461State ProgramAlabama 4
TestAmerica Chicago 01132CANELACCalifornia 9
TestAmerica Chicago E871072NELACFlorida 4
TestAmerica Chicago 939State ProgramGeorgia 4
TestAmerica Chicago N/AState ProgramGeorgia 4
TestAmerica Chicago N/AState ProgramHawaii 9
TestAmerica Chicago 100201NELACIllinois 5
TestAmerica Chicago C-IL-02State ProgramIndiana 5
TestAmerica Chicago 82State ProgramIowa 7
TestAmerica Chicago E-10161NELACKansas 7
TestAmerica Chicago 90023State ProgramKentucky 4
TestAmerica Chicago 66State ProgramKentucky (UST) 4
TestAmerica Chicago L2304DoD ELAPL-A-B
TestAmerica Chicago L2304ISO/IEC 17025L-A-B
TestAmerica Chicago 30720NELACLouisiana 6
TestAmerica Chicago M-IL035State ProgramMassachusetts 1
TestAmerica Chicago N/AState ProgramMississippi 4
TestAmerica Chicago 291State ProgramNorth Carolina DENR 4
TestAmerica Chicago R-194State ProgramNorth Dakota 8
TestAmerica Chicago 8908State ProgramOklahoma 6
TestAmerica Chicago 77001State ProgramSouth Carolina 4
TestAmerica Chicago T104704252-09-TXNELACTexas 6
TestAmerica Chicago P330-12-00038FederalUSDA
TestAmerica Chicago 460142NELACVirginia 3
TestAmerica Chicago 999580010State ProgramWisconsin 5
TestAmerica Chicago 8TMS-QState ProgramWyoming 8
Accreditation may not be offered or required for all methods and analytes reported in this package. Please contact your project manager for the laboratory's
current list of certified methods and analytes.
TestAmerica ChicagoPage 35 of 39 5/24/2012
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Login Sample Receipt Checklist
Client: Shaw Environmental & Infrastructure, Inc Job Number: 500-46374-1
SDG Number: 500-46374-1
Login Number: 46374
Question Answer Comment
Creator: Lunt, Jeff T
List Source: TestAmerica Chicago
List Number: 1
TrueRadioactivity either was not measured or, if measured, is at or below background
N/AThe cooler's custody seal, if present, is intact.
TrueThe cooler or samples do not appear to have been compromised or tampered with.
TrueSamples were received on ice. 4.0
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the sample IDs on the containers and the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs
TrueVOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
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ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Chicago2417 Bond StreetUniversity Park, IL 60484Tel: (708)534-5200
TestAmerica Job ID: 500-46374-3TestAmerica Sample Delivery Group: 500-46374-1Client Project/Site: Naperville Sportsman Club
For:Shaw Environmental & Infrastructure, Inc1607 East Main StreetSuite ESaint Charles, Illinois 60174
Attn: Jeffrey Cademartori
Authorized for release by:6/14/2012 1:17:47 PM
Richard WrightProject Manager [email protected]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Shaw Environmental & Infrastructure, IncProject/Site: Naperville Sportsman Club
TestAmerica Job ID: 500-46374-3SDG: 500-46374-1
Page 2 of 43TestAmerica Chicago
6/14/2012
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43
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Case NarrativeClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-46374-3
Project/Site: Naperville Sportsman Club SDG: 500-46374-1
Job ID: 500-46374-3
Laboratory: TestAmerica Chicago
Narrative
Job Narrative
500-46374-3
Comments
No additional comments.
Receipt
The samples were received on 5/16/2012 7:00 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 4.0º C.
GC/MS Semi VOA
Method(s) 8270C: The following samples were prepared outside the method defined holding time because the request for the test was
made after the holding time for the sample expired. G19 (6-12") (500-46374-6), I9 (6-12") (500-46374-8), J13 (6-12") (500-46374-14), J15
(6-12") (500-46374-16), K7 (6-12") (500-46374-20)
No other analytical or quality issues were noted.
Metals
Method(s) 7471A: The following sample(s): 500-46374-6, 8, 14, 16, and 20 were prepared and/or analyzed outside the method defined
holding time for Hg because the request for the test was made after the holding time for the sample expired.
Method(s) D2974-87: A correction factor of 0.58 was applied to the calculation of FOC by Nelson and Sommers.
No other analytical or quality issues were noted.
General Chemistry
No analytical or quality issues were noted.
Organic Prep
No analytical or quality issues were noted.
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Detection SummaryTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Client Sample ID: G19 (0-6") Lab Sample ID: 500-46374-5
Barium
RL
0.50 mg/L
MDL
0.010
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B TCLP1J0.44
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0029 J
Lead 0.0075 mg/L0.0050 TCLP6010B10.66
Organic Matter at 440 Deg(C)
RL
0.10 %
RL
0.10
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
D2974-87 Total/NA13.9
FOC by Nelson and Sommers (0.58
factor)
0.058 %0.058 Total/NAD2974-8712.3
Client Sample ID: G19 (6-12") Lab Sample ID: 500-46374-6
☼Antimony
RL
2.2 mg/Kg
MDL
0.29
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B Total/NA1J0.43
☼Arsenic 1.1 mg/Kg0.24 Total/NA6010B15.7
☼Barium 1.1 mg/Kg0.13 Total/NA6010B160
☼Cadmium 0.22 mg/Kg0.054 Total/NA6010B10.48
☼Chromium 1.1 mg/Kg0.18 Total/NA6010B111
☼Copper 1.1 mg/Kg0.29 Total/NA6010B121
☼Lead 0.54 mg/Kg0.19 Total/NA6010B19.0
☼Zinc 2.2 mg/Kg0.74 Total/NA6010B135
Barium 0.50 mg/L0.010 TCLP6010B11.2
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0052
Lead 0.0075 mg/L0.0050 TCLP6010B10.0065 J
pH 0.200 SU0.200 Total/NA9045C17.60
Client Sample ID: I9 (0-6") Lab Sample ID: 500-46374-7
Arsenic
RL
0.050 mg/L
MDL
0.010
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B TCLP10.066
Barium 0.50 mg/L0.010 TCLP6010B10.70
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0036 J
Lead 0.0075 mg/L0.0050 TCLP6010B19.0
Organic Matter at 440 Deg(C)
RL
0.10 %
RL
0.10
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
D2974-87 Total/NA15.5
FOC by Nelson and Sommers (0.58
factor)
0.058 %0.058 Total/NAD2974-8713.2
Client Sample ID: I9 (6-12") Lab Sample ID: 500-46374-8
☼Benzo[a]pyrene
RL
0.050 mg/Kg
MDL
0.0092
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J H0.016
☼Benzo[b]fluoranthene 0.050 mg/Kg0.0098 Total/NA8270C10.022 J H
☼Chrysene 0.050 mg/Kg0.011 Total/NA8270C10.020 J H
☼Fluoranthene 0.050 mg/Kg0.021 Total/NA8270C10.027 J H
☼Pyrene 0.050 mg/Kg0.018 Total/NA8270C10.021 J H
☼Antimony 3.0 mg/Kg0.39 Total/NA6010B10.45 J
☼Arsenic 1.5 mg/Kg0.32 Total/NA6010B13.8
☼Barium 1.5 mg/Kg0.18 Total/NA6010B1160
☼Cadmium 0.30 mg/Kg0.073 Total/NA6010B10.47
☼Chromium 1.5 mg/Kg0.25 Total/NA6010B121
☼Copper 1.5 mg/Kg0.40 Total/NA6010B126
☼Lead 0.74 mg/Kg0.25 Total/NA6010B157
☼Selenium 1.5 mg/Kg0.42 Total/NA6010B11.0 J
☼Zinc 3.0 mg/Kg1.0 Total/NA6010B172
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Detection SummaryTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Client Sample ID: I9 (6-12") (Continued) Lab Sample ID: 500-46374-8
Barium
RL
0.50 mg/L
MDL
0.010
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B TCLP1J0.43
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0022 J
Lead 0.0075 mg/L0.0050 TCLP6010B10.022
☼Mercury 0.025 mg/Kg0.0076 Total/NA7471A10.046 H
pH 0.200 SU0.200 Total/NA9045C17.68
Client Sample ID: J13 (0-6") Lab Sample ID: 500-46374-13
Arsenic
RL
0.050 mg/L
MDL
0.010
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B TCLP10.10
Barium 0.50 mg/L0.010 TCLP6010B10.59
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0029 J
Lead 0.0075 mg/L0.0050 TCLP6010B134
Organic Matter at 440 Deg(C)
RL
0.10 %
RL
0.10
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
D2974-87 Total/NA17.0
FOC by Nelson and Sommers (0.58
factor)
0.058 %0.058 Total/NAD2974-8714.1
Client Sample ID: J13 (6-12") Lab Sample ID: 500-46374-14
☼Acenaphthene
RL
0.054 mg/Kg
MDL
0.016
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J H0.031
☼Anthracene 0.054 mg/Kg0.013 Total/NA8270C10.055 H
☼Benzo[a]anthracene 0.054 mg/Kg0.011 Total/NA8270C10.33 H
☼Benzo[a]pyrene 0.054 mg/Kg0.0098 Total/NA8270C10.46 H
☼Benzo[b]fluoranthene 0.054 mg/Kg0.011 Total/NA8270C10.63 H
☼Benzo[g,h,i]perylene 0.054 mg/Kg0.018 Total/NA8270C10.32 H
☼Benzo[k]fluoranthene 0.054 mg/Kg0.013 Total/NA8270C10.22 H
☼Chrysene 0.054 mg/Kg0.012 Total/NA8270C10.49 H
☼Dibenz(a,h)anthracene 0.054 mg/Kg0.015 Total/NA8270C10.072 H
☼Fluoranthene 0.054 mg/Kg0.022 Total/NA8270C10.75 H
☼Fluorene 0.054 mg/Kg0.012 Total/NA8270C10.038 J H
☼Indeno[1,2,3-cd]pyrene 0.054 mg/Kg0.018 Total/NA8270C10.27 H
☼Phenanthrene 0.054 mg/Kg0.023 Total/NA8270C10.11 H
☼Pyrene 0.054 mg/Kg0.020 Total/NA8270C10.57 H
☼Antimony 2.9 mg/Kg0.39 Total/NA6010B1480
☼Arsenic 1.5 mg/Kg0.32 Total/NA6010B1310
☼Barium 1.5 mg/Kg0.17 Total/NA6010B159
☼Cadmium 0.29 mg/Kg0.072 Total/NA6010B10.42
☼Chromium 1.5 mg/Kg0.24 Total/NA6010B114
☼Copper 1.5 mg/Kg0.40 Total/NA6010B129
☼Lead 73 mg/Kg25 Total/NA6010B100120000
☼Selenium 1.5 mg/Kg0.42 Total/NA6010B10.68 J
☼Silver 0.73 mg/Kg0.088 Total/NA6010B11.7
☼Zinc 2.9 mg/Kg1.0 Total/NA6010B166
Arsenic 0.050 mg/L0.010 TCLP6010B10.067
Barium 0.50 mg/L0.010 TCLP6010B10.81
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0058
Lead 0.75 mg/L0.50 TCLP6010B100120
☼Mercury 0.028 mg/Kg0.0085 Total/NA7471A10.026 J H
pH 0.200 SU0.200 Total/NA9045C17.08
Client Sample ID: J15 (0-6") Lab Sample ID: 500-46374-15
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Detection SummaryTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Client Sample ID: J15 (0-6") (Continued) Lab Sample ID: 500-46374-15
Arsenic
RL
0.050 mg/L
MDL
0.010
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B TCLP1J0.012
Barium 0.50 mg/L0.010 TCLP6010B10.57
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0024 J
Lead 0.0075 mg/L0.0050 TCLP6010B18.4
Organic Matter at 440 Deg(C)
RL
0.10 %
RL
0.10
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
D2974-87 Total/NA14.9
FOC by Nelson and Sommers (0.58
factor)
0.058 %0.058 Total/NAD2974-8712.8
Client Sample ID: J15 (6-12") Lab Sample ID: 500-46374-16
☼Acenaphthene
RL
0.053 mg/Kg
MDL
0.016
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J H0.031
☼Anthracene 0.053 mg/Kg0.013 Total/NA8270C10.027 J H
☼Benzo[a]anthracene 0.053 mg/Kg0.011 Total/NA8270C10.39 H
☼Benzo[a]pyrene 0.053 mg/Kg0.0098 Total/NA8270C10.62 H
☼Benzo[b]fluoranthene 0.053 mg/Kg0.010 Total/NA8270C10.72 H
☼Benzo[g,h,i]perylene 0.053 mg/Kg0.018 Total/NA8270C10.46 H
☼Benzo[k]fluoranthene 0.053 mg/Kg0.013 Total/NA8270C10.35 H
☼Chrysene 0.053 mg/Kg0.012 Total/NA8270C10.48 H
☼Dibenz(a,h)anthracene 0.053 mg/Kg0.015 Total/NA8270C10.11 H
☼Fluoranthene 0.053 mg/Kg0.022 Total/NA8270C10.50 H
☼Fluorene 0.053 mg/Kg0.012 Total/NA8270C10.020 J H
☼Indeno[1,2,3-cd]pyrene 0.053 mg/Kg0.018 Total/NA8270C10.40 H
☼Phenanthrene 0.053 mg/Kg0.023 Total/NA8270C10.13 H
☼Pyrene 0.053 mg/Kg0.019 Total/NA8270C10.48 H
☼Antimony 3.0 mg/Kg0.40 Total/NA6010B19.1
☼Arsenic 1.5 mg/Kg0.33 Total/NA6010B114
☼Barium 1.5 mg/Kg0.18 Total/NA6010B176
☼Cadmium 0.30 mg/Kg0.075 Total/NA6010B10.32
☼Chromium 1.5 mg/Kg0.25 Total/NA6010B115
☼Copper 1.5 mg/Kg0.41 Total/NA6010B127
☼Lead 0.76 mg/Kg0.26 Total/NA6010B12900
☼Selenium 1.5 mg/Kg0.44 Total/NA6010B10.48 J
☼Zinc 3.0 mg/Kg1.0 Total/NA6010B164
Arsenic 0.050 mg/L0.010 TCLP6010B10.023 J
Barium 0.50 mg/L0.010 TCLP6010B10.94
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0061
Lead 0.0075 mg/L0.0050 TCLP6010B123
Mercury 0.00020 mg/L0.000020 TCLP7470A10.000020 J H
☼Mercury 0.024 mg/Kg0.0073 Total/NA7471A10.034 H
pH 0.200 SU0.200 Total/NA9045C17.31
Client Sample ID: K7 (0-6") Lab Sample ID: 500-46374-19
Arsenic
RL
0.050 mg/L
MDL
0.010
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B TCLP1J0.021
Barium 0.50 mg/L0.010 TCLP6010B10.72
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0039 J
Lead 0.0075 mg/L0.0050 TCLP6010B12.7
Organic Matter at 440 Deg(C)
RL
0.10 %
RL
0.10
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
D2974-87 Total/NA14.7
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Detection SummaryTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Client Sample ID: K7 (0-6") (Continued) Lab Sample ID: 500-46374-19
FOC by Nelson and Sommers (0.58
factor)
RL
0.058 %
RL
0.058
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
D2974-87 Total/NA12.7
Client Sample ID: K7 (6-12") Lab Sample ID: 500-46374-20
☼Benzo[a]pyrene
RL
0.041 mg/Kg
MDL
0.0075
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J H0.0095
☼Benzo[b]fluoranthene 0.041 mg/Kg0.0080 Total/NA8270C10.014 J H
☼Antimony 2.3 mg/Kg0.30 Total/NA6010B10.87 J
☼Arsenic 1.1 mg/Kg0.25 Total/NA6010B12.5
☼Barium 1.1 mg/Kg0.14 Total/NA6010B163
☼Cadmium 0.23 mg/Kg0.056 Total/NA6010B10.35
☼Chromium 1.1 mg/Kg0.19 Total/NA6010B113
☼Copper 1.1 mg/Kg0.31 Total/NA6010B120
☼Lead 0.57 mg/Kg0.20 Total/NA6010B125
☼Zinc 2.3 mg/Kg0.78 Total/NA6010B144
Barium 0.50 mg/L0.010 TCLP6010B10.65
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0038 J
Lead 0.0075 mg/L0.0050 TCLP6010B10.026
☼Mercury 0.020 mg/Kg0.0060 Total/NA7471A10.014 J H
pH 0.200 SU0.200 Total/NA9045C17.64
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Method SummaryTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Method Method Description LaboratoryProtocol
SW8468270C Semivolatile Organic Compounds (GC/MS) TAL CHI
SW8466010B Metals (ICP) TAL CHI
SW8467470A Mercury (CVAA) TAL CHI
SW8467471A Mercury (CVAA) TAL CHI
SW8469045C pH TAL CHI
ASTMD2974-87 Ash Content TAL CHI
EPAMoisture Percent Moisture TAL CHI
Protocol References:
ASTM = ASTM International
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200
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Sample SummaryTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
500-46374-5 G19 (0-6") Solid 05/09/12 16:08 05/16/12 07:00
500-46374-6 G19 (6-12") Solid 05/09/12 16:08 05/16/12 07:00
500-46374-7 I9 (0-6") Solid 05/09/12 13:22 05/16/12 07:00
500-46374-8 I9 (6-12") Solid 05/09/12 13:22 05/16/12 07:00
500-46374-13 J13 (0-6") Solid 05/07/12 13:40 05/16/12 07:00
500-46374-14 J13 (6-12") Solid 05/07/12 13:40 05/16/12 07:00
500-46374-15 J15 (0-6") Solid 05/07/12 13:00 05/16/12 07:00
500-46374-16 J15 (6-12") Solid 05/07/12 13:00 05/16/12 07:00
500-46374-19 K7 (0-6") Solid 05/07/12 16:30 05/16/12 07:00
500-46374-20 K7 (6-12") Solid 05/07/12 16:30 05/16/12 07:00
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Client Sample ResultsTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-5Client Sample ID: G19 (0-6")Matrix: SolidDate Collected: 05/09/12 16:08
Date Received: 05/16/12 07:00
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic <0.050 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 08:26 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 06/13/12 12:00 06/14/12 08:26 1Barium 0.44 J
0.0050 0.0020 mg/L 06/13/12 12:00 06/14/12 08:26 1Cadmium 0.0029 J
0.025 0.010 mg/L 06/13/12 12:00 06/14/12 08:26 1Chromium <0.025
0.0075 0.0050 mg/L 06/13/12 12:00 06/14/12 08:26 1Lead 0.66
0.050 0.010 mg/L 06/13/12 12:00 06/14/12 08:26 1Selenium <0.050
0.025 0.0050 mg/L 06/13/12 12:00 06/14/12 08:26 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury <0.00020 H 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:05 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL RL
Organic Matter at 440 Deg(C) 3.9 0.10 0.10 % 06/07/12 09:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.058 0.058 % 06/07/12 09:34 1FOC by Nelson and Sommers
(0.58 factor)
2.3
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Client Sample ResultsTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-6Client Sample ID: G19 (6-12")Matrix: SolidDate Collected: 05/09/12 16:08
Percent Solids: 80.8Date Received: 05/16/12 07:00
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.039 H 0.039 0.012 mg/Kg ☼ 06/07/12 07:07 06/08/12 12:52 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.039 0.0091 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Acenaphthylene <0.039 H
0.039 0.0093 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Anthracene <0.039 H
0.039 0.0083 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Benzo[a]anthracene <0.039 H
0.039 0.0072 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Benzo[a]pyrene <0.039 H
0.039 0.0077 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Benzo[b]fluoranthene <0.039 H
0.039 0.013 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Benzo[g,h,i]perylene <0.039 H
0.039 0.0095 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Benzo[k]fluoranthene <0.039 H
0.039 0.0090 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Chrysene <0.039 H
0.039 0.011 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Dibenz(a,h)anthracene <0.039 H
0.039 0.016 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Fluoranthene <0.039 H
0.039 0.0090 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Fluorene <0.039 H
0.039 0.013 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Indeno[1,2,3-cd]pyrene <0.039 H
0.039 0.0077 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Naphthalene <0.039 H
0.039 0.017 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Phenanthrene <0.039 H
0.039 0.014 mg/Kg 06/07/12 07:07 06/08/12 12:52 1☼Pyrene <0.039 H
2-Fluorobiphenyl 53 30 - 119 06/07/12 07:07 06/08/12 12:52 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 47 06/07/12 07:07 06/08/12 12:52 130 - 115
Terphenyl-d14 71 06/07/12 07:07 06/08/12 12:52 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 0.43 J 2.2 0.29 mg/Kg ☼ 06/06/12 10:14 06/06/12 21:52 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.1 0.24 mg/Kg 06/06/12 10:14 06/06/12 21:52 1☼Arsenic 5.7
1.1 0.13 mg/Kg 06/06/12 10:14 06/06/12 21:52 1☼Barium 60
0.22 0.054 mg/Kg 06/06/12 10:14 06/06/12 21:52 1☼Cadmium 0.48
1.1 0.18 mg/Kg 06/06/12 10:14 06/06/12 21:52 1☼Chromium 11
1.1 0.29 mg/Kg 06/06/12 10:14 06/06/12 21:52 1☼Copper 21
0.54 0.19 mg/Kg 06/06/12 10:14 06/06/12 21:52 1☼Lead 9.0
1.1 0.31 mg/Kg 06/06/12 10:14 06/06/12 21:52 1☼Selenium <1.1
0.54 0.065 mg/Kg 06/06/12 10:14 06/06/12 21:52 1☼Silver <0.54
2.2 0.74 mg/Kg 06/06/12 10:14 06/06/12 21:52 1☼Zinc 35
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic <0.050 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 08:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 06/13/12 12:00 06/14/12 08:30 1Barium 1.2
0.0050 0.0020 mg/L 06/13/12 12:00 06/14/12 08:30 1Cadmium 0.0052
0.025 0.010 mg/L 06/13/12 12:00 06/14/12 08:30 1Chromium <0.025
0.0075 0.0050 mg/L 06/13/12 12:00 06/14/12 08:30 1Lead 0.0065 J
0.050 0.010 mg/L 06/13/12 12:00 06/14/12 08:30 1Selenium <0.050
0.025 0.0050 mg/L 06/13/12 12:00 06/14/12 08:30 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury <0.00020 H 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 7471A - Mercury (CVAA)RL MDL
Mercury <0.018 H 0.018 0.0054 mg/Kg ☼ 06/09/12 10:05 06/09/12 14:03 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-6Client Sample ID: G19 (6-12")Matrix: SolidDate Collected: 05/09/12 16:08
Date Received: 05/16/12 07:00
General ChemistryRL MDL
pH 7.60 0.200 0.200 SU 06/11/12 14:22 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-7Client Sample ID: I9 (0-6")Matrix: SolidDate Collected: 05/09/12 13:22
Date Received: 05/16/12 07:00
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic 0.066 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 08:50 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 06/13/12 12:00 06/14/12 08:50 1Barium 0.70
0.0050 0.0020 mg/L 06/13/12 12:00 06/14/12 08:50 1Cadmium 0.0036 J
0.025 0.010 mg/L 06/13/12 12:00 06/14/12 08:50 1Chromium <0.025
0.0075 0.0050 mg/L 06/13/12 12:00 06/14/12 08:50 1Lead 9.0
0.050 0.010 mg/L 06/13/12 12:00 06/14/12 08:50 1Selenium <0.050
0.025 0.0050 mg/L 06/13/12 12:00 06/14/12 08:50 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury <0.00020 H 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:08 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL RL
Organic Matter at 440 Deg(C) 5.5 0.10 0.10 % 06/07/12 09:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.058 0.058 % 06/07/12 09:34 1FOC by Nelson and Sommers
(0.58 factor)
3.2
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Client Sample ResultsTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-8Client Sample ID: I9 (6-12")Matrix: SolidDate Collected: 05/09/12 13:22
Percent Solids: 65.5Date Received: 05/16/12 07:00
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.050 H 0.050 0.015 mg/Kg ☼ 06/07/12 07:07 06/08/12 13:10 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.050 0.012 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Acenaphthylene <0.050 H
0.050 0.012 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Anthracene <0.050 H
0.050 0.011 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Benzo[a]anthracene <0.050 H
0.050 0.0092 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Benzo[a]pyrene 0.016 J H
0.050 0.0098 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Benzo[b]fluoranthene 0.022 J H
0.050 0.017 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Benzo[g,h,i]perylene <0.050 H
0.050 0.012 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Benzo[k]fluoranthene <0.050 H
0.050 0.011 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Chrysene 0.020 J H
0.050 0.014 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Dibenz(a,h)anthracene <0.050 H
0.050 0.021 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Fluoranthene 0.027 J H
0.050 0.011 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Fluorene <0.050 H
0.050 0.017 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Indeno[1,2,3-cd]pyrene <0.050 H
0.050 0.0097 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Naphthalene <0.050 H
0.050 0.021 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Phenanthrene <0.050 H
0.050 0.018 mg/Kg 06/07/12 07:07 06/08/12 13:10 1☼Pyrene 0.021 J H
2-Fluorobiphenyl 47 30 - 119 06/07/12 07:07 06/08/12 13:10 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 45 06/07/12 07:07 06/08/12 13:10 130 - 115
Terphenyl-d14 57 06/07/12 07:07 06/08/12 13:10 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 0.45 J 3.0 0.39 mg/Kg ☼ 06/06/12 10:14 06/06/12 21:58 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.5 0.32 mg/Kg 06/06/12 10:14 06/06/12 21:58 1☼Arsenic 3.8
1.5 0.18 mg/Kg 06/06/12 10:14 06/06/12 21:58 1☼Barium 160
0.30 0.073 mg/Kg 06/06/12 10:14 06/06/12 21:58 1☼Cadmium 0.47
1.5 0.25 mg/Kg 06/06/12 10:14 06/06/12 21:58 1☼Chromium 21
1.5 0.40 mg/Kg 06/06/12 10:14 06/06/12 21:58 1☼Copper 26
0.74 0.25 mg/Kg 06/06/12 10:14 06/06/12 21:58 1☼Lead 57
1.5 0.42 mg/Kg 06/06/12 10:14 06/06/12 21:58 1☼Selenium 1.0 J
0.74 0.089 mg/Kg 06/06/12 10:14 06/06/12 21:58 1☼Silver <0.74
3.0 1.0 mg/Kg 06/06/12 10:14 06/06/12 21:58 1☼Zinc 72
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic <0.050 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 08:54 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 06/13/12 12:00 06/14/12 08:54 1Barium 0.43 J
0.0050 0.0020 mg/L 06/13/12 12:00 06/14/12 08:54 1Cadmium 0.0022 J
0.025 0.010 mg/L 06/13/12 12:00 06/14/12 08:54 1Chromium <0.025
0.0075 0.0050 mg/L 06/13/12 12:00 06/14/12 08:54 1Lead 0.022
0.050 0.010 mg/L 06/13/12 12:00 06/14/12 08:54 1Selenium <0.050
0.025 0.0050 mg/L 06/13/12 12:00 06/14/12 08:54 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury <0.00020 H 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:10 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.046 H 0.025 0.0076 mg/Kg ☼ 06/09/12 10:05 06/09/12 14:05 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-8Client Sample ID: I9 (6-12")Matrix: SolidDate Collected: 05/09/12 13:22
Date Received: 05/16/12 07:00
General ChemistryRL MDL
pH 7.68 0.200 0.200 SU 06/11/12 14:26 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-13Client Sample ID: J13 (0-6")Matrix: SolidDate Collected: 05/07/12 13:40
Date Received: 05/16/12 07:00
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic 0.10 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:07 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 06/13/12 12:00 06/14/12 09:07 1Barium 0.59
0.0050 0.0020 mg/L 06/13/12 12:00 06/14/12 09:07 1Cadmium 0.0029 J
0.025 0.010 mg/L 06/13/12 12:00 06/14/12 09:07 1Chromium <0.025
0.0075 0.0050 mg/L 06/13/12 12:00 06/14/12 09:07 1Lead 34
0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:07 1Selenium <0.050
0.025 0.0050 mg/L 06/13/12 12:00 06/14/12 09:07 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury <0.00020 H 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:15 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL RL
Organic Matter at 440 Deg(C) 7.0 0.10 0.10 % 06/07/12 09:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.058 0.058 % 06/07/12 09:34 1FOC by Nelson and Sommers
(0.58 factor)
4.1
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Client Sample ResultsTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-14Client Sample ID: J13 (6-12")Matrix: SolidDate Collected: 05/07/12 13:40
Percent Solids: 58.9Date Received: 05/16/12 07:00
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene 0.031 J H 0.054 0.016 mg/Kg ☼ 06/07/12 07:07 06/08/12 13:27 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.054 0.012 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Acenaphthylene <0.054 H
0.054 0.013 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Anthracene 0.055 H
0.054 0.011 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Benzo[a]anthracene 0.33 H
0.054 0.0098 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Benzo[a]pyrene 0.46 H
0.054 0.011 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Benzo[b]fluoranthene 0.63 H
0.054 0.018 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Benzo[g,h,i]perylene 0.32 H
0.054 0.013 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Benzo[k]fluoranthene 0.22 H
0.054 0.012 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Chrysene 0.49 H
0.054 0.015 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Dibenz(a,h)anthracene 0.072 H
0.054 0.022 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Fluoranthene 0.75 H
0.054 0.012 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Fluorene 0.038 J H
0.054 0.018 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Indeno[1,2,3-cd]pyrene 0.27 H
0.054 0.010 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Naphthalene <0.054 H
0.054 0.023 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Phenanthrene 0.11 H
0.054 0.020 mg/Kg 06/07/12 07:07 06/08/12 13:27 1☼Pyrene 0.57 H
2-Fluorobiphenyl 53 30 - 119 06/07/12 07:07 06/08/12 13:27 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 42 06/07/12 07:07 06/08/12 13:27 130 - 115
Terphenyl-d14 58 06/07/12 07:07 06/08/12 13:27 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 480 2.9 0.39 mg/Kg ☼ 06/06/12 10:14 06/06/12 22:05 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.5 0.32 mg/Kg 06/06/12 10:14 06/06/12 22:05 1☼Arsenic 310
1.5 0.17 mg/Kg 06/06/12 10:14 06/06/12 22:05 1☼Barium 59
0.29 0.072 mg/Kg 06/06/12 10:14 06/06/12 22:05 1☼Cadmium 0.42
1.5 0.24 mg/Kg 06/06/12 10:14 06/06/12 22:05 1☼Chromium 14
1.5 0.40 mg/Kg 06/06/12 10:14 06/06/12 22:05 1☼Copper 29
73 25 mg/Kg 06/06/12 10:14 06/07/12 13:17 100☼Lead 120000
1.5 0.42 mg/Kg 06/06/12 10:14 06/06/12 22:05 1☼Selenium 0.68 J
0.73 0.088 mg/Kg 06/06/12 10:14 06/06/12 22:05 1☼Silver 1.7
2.9 1.0 mg/Kg 06/06/12 10:14 06/06/12 22:05 1☼Zinc 66
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic 0.067 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 06/13/12 12:00 06/14/12 09:11 1Barium 0.81
0.0050 0.0020 mg/L 06/13/12 12:00 06/14/12 09:11 1Cadmium 0.0058
0.025 0.010 mg/L 06/13/12 12:00 06/14/12 09:11 1Chromium <0.025
0.75 0.50 mg/L 06/13/12 12:00 06/14/12 10:23 100Lead 120
0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:11 1Selenium <0.050
0.025 0.0050 mg/L 06/13/12 12:00 06/14/12 09:11 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury <0.00020 H 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:17 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.026 J H 0.028 0.0085 mg/Kg ☼ 06/09/12 10:05 06/09/12 14:07 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-14Client Sample ID: J13 (6-12")Matrix: SolidDate Collected: 05/07/12 13:40
Date Received: 05/16/12 07:00
General ChemistryRL MDL
pH 7.08 0.200 0.200 SU 06/11/12 14:29 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-15Client Sample ID: J15 (0-6")Matrix: SolidDate Collected: 05/07/12 13:00
Date Received: 05/16/12 07:00
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic 0.012 J 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:15 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 06/13/12 12:00 06/14/12 09:15 1Barium 0.57
0.0050 0.0020 mg/L 06/13/12 12:00 06/14/12 09:15 1Cadmium 0.0024 J
0.025 0.010 mg/L 06/13/12 12:00 06/14/12 09:15 1Chromium <0.025
0.0075 0.0050 mg/L 06/13/12 12:00 06/14/12 09:15 1Lead 8.4
0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:15 1Selenium <0.050
0.025 0.0050 mg/L 06/13/12 12:00 06/14/12 09:15 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury <0.00020 H 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:19 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL RL
Organic Matter at 440 Deg(C) 4.9 0.10 0.10 % 06/07/12 09:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.058 0.058 % 06/07/12 09:34 1FOC by Nelson and Sommers
(0.58 factor)
2.8
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Client Sample ResultsTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-16Client Sample ID: J15 (6-12")Matrix: SolidDate Collected: 05/07/12 13:00
Percent Solids: 61.1Date Received: 05/16/12 07:00
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene 0.031 J H 0.053 0.016 mg/Kg ☼ 06/07/12 07:07 06/08/12 13:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.053 0.012 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Acenaphthylene <0.053 H
0.053 0.013 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Anthracene 0.027 J H
0.053 0.011 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Benzo[a]anthracene 0.39 H
0.053 0.0098 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Benzo[a]pyrene 0.62 H
0.053 0.010 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Benzo[b]fluoranthene 0.72 H
0.053 0.018 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Benzo[g,h,i]perylene 0.46 H
0.053 0.013 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Benzo[k]fluoranthene 0.35 H
0.053 0.012 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Chrysene 0.48 H
0.053 0.015 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Dibenz(a,h)anthracene 0.11 H
0.053 0.022 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Fluoranthene 0.50 H
0.053 0.012 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Fluorene 0.020 J H
0.053 0.018 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Indeno[1,2,3-cd]pyrene 0.40 H
0.053 0.010 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Naphthalene <0.053 H
0.053 0.023 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Phenanthrene 0.13 H
0.053 0.019 mg/Kg 06/07/12 07:07 06/08/12 13:44 1☼Pyrene 0.48 H
2-Fluorobiphenyl 60 30 - 119 06/07/12 07:07 06/08/12 13:44 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 50 06/07/12 07:07 06/08/12 13:44 130 - 115
Terphenyl-d14 71 06/07/12 07:07 06/08/12 13:44 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 9.1 3.0 0.40 mg/Kg ☼ 06/06/12 10:14 06/06/12 22:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.5 0.33 mg/Kg 06/06/12 10:14 06/06/12 22:11 1☼Arsenic 14
1.5 0.18 mg/Kg 06/06/12 10:14 06/06/12 22:11 1☼Barium 76
0.30 0.075 mg/Kg 06/06/12 10:14 06/06/12 22:11 1☼Cadmium 0.32
1.5 0.25 mg/Kg 06/06/12 10:14 06/06/12 22:11 1☼Chromium 15
1.5 0.41 mg/Kg 06/06/12 10:14 06/06/12 22:11 1☼Copper 27
0.76 0.26 mg/Kg 06/06/12 10:14 06/06/12 22:11 1☼Lead 2900
1.5 0.44 mg/Kg 06/06/12 10:14 06/06/12 22:11 1☼Selenium 0.48 J
0.76 0.092 mg/Kg 06/06/12 10:14 06/06/12 22:11 1☼Silver <0.76
3.0 1.0 mg/Kg 06/06/12 10:14 06/06/12 22:11 1☼Zinc 64
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic 0.023 J 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:19 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 06/13/12 12:00 06/14/12 09:19 1Barium 0.94
0.0050 0.0020 mg/L 06/13/12 12:00 06/14/12 09:19 1Cadmium 0.0061
0.025 0.010 mg/L 06/13/12 12:00 06/14/12 09:19 1Chromium <0.025
0.0075 0.0050 mg/L 06/13/12 12:00 06/14/12 09:19 1Lead 23
0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:19 1Selenium <0.050
0.025 0.0050 mg/L 06/13/12 12:00 06/14/12 09:19 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury 0.000020 J H 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:28 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.034 H 0.024 0.0073 mg/Kg ☼ 06/09/12 10:05 06/09/12 14:08 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-16Client Sample ID: J15 (6-12")Matrix: SolidDate Collected: 05/07/12 13:00
Date Received: 05/16/12 07:00
General ChemistryRL MDL
pH 7.31 0.200 0.200 SU 06/11/12 14:32 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-19Client Sample ID: K7 (0-6")Matrix: SolidDate Collected: 05/07/12 16:30
Date Received: 05/16/12 07:00
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic 0.021 J 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:23 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 06/13/12 12:00 06/14/12 09:23 1Barium 0.72
0.0050 0.0020 mg/L 06/13/12 12:00 06/14/12 09:23 1Cadmium 0.0039 J
0.025 0.010 mg/L 06/13/12 12:00 06/14/12 09:23 1Chromium <0.025
0.0075 0.0050 mg/L 06/13/12 12:00 06/14/12 09:23 1Lead 2.7
0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:23 1Selenium <0.050
0.025 0.0050 mg/L 06/13/12 12:00 06/14/12 09:23 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury <0.00020 H 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL RL
Organic Matter at 440 Deg(C) 4.7 0.10 0.10 % 06/07/12 09:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.058 0.058 % 06/07/12 09:34 1FOC by Nelson and Sommers
(0.58 factor)
2.7
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Client Sample ResultsTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-20Client Sample ID: K7 (6-12")Matrix: SolidDate Collected: 05/07/12 16:30
Percent Solids: 77.9Date Received: 05/16/12 07:00
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.041 H 0.041 0.012 mg/Kg ☼ 06/07/12 07:07 06/08/12 14:02 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.041 0.0095 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Acenaphthylene <0.041 H
0.041 0.0097 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Anthracene <0.041 H
0.041 0.0087 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Benzo[a]anthracene <0.041 H
0.041 0.0075 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Benzo[a]pyrene 0.0095 J H
0.041 0.0080 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Benzo[b]fluoranthene 0.014 J H
0.041 0.014 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Benzo[g,h,i]perylene <0.041 H
0.041 0.0099 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Benzo[k]fluoranthene <0.041 H
0.041 0.0093 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Chrysene <0.041 H
0.041 0.012 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Dibenz(a,h)anthracene <0.041 H
0.041 0.017 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Fluoranthene <0.041 H
0.041 0.0094 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Fluorene <0.041 H
0.041 0.014 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Indeno[1,2,3-cd]pyrene <0.041 H
0.041 0.0080 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Naphthalene <0.041 H
0.041 0.017 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Phenanthrene <0.041 H
0.041 0.015 mg/Kg 06/07/12 07:07 06/08/12 14:02 1☼Pyrene <0.041 H
2-Fluorobiphenyl 72 30 - 119 06/07/12 07:07 06/08/12 14:02 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 70 06/07/12 07:07 06/08/12 14:02 130 - 115
Terphenyl-d14 90 06/07/12 07:07 06/08/12 14:02 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 0.87 J 2.3 0.30 mg/Kg ☼ 06/06/12 10:14 06/06/12 22:17 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.1 0.25 mg/Kg 06/06/12 10:14 06/06/12 22:17 1☼Arsenic 2.5
1.1 0.14 mg/Kg 06/06/12 10:14 06/06/12 22:17 1☼Barium 63
0.23 0.056 mg/Kg 06/06/12 10:14 06/06/12 22:17 1☼Cadmium 0.35
1.1 0.19 mg/Kg 06/06/12 10:14 06/06/12 22:17 1☼Chromium 13
1.1 0.31 mg/Kg 06/06/12 10:14 06/06/12 22:17 1☼Copper 20
0.57 0.20 mg/Kg 06/06/12 10:14 06/06/12 22:17 1☼Lead 25
1.1 0.33 mg/Kg 06/06/12 10:14 06/06/12 22:17 1☼Selenium <1.1
0.57 0.068 mg/Kg 06/06/12 10:14 06/06/12 22:17 1☼Silver <0.57
2.3 0.78 mg/Kg 06/06/12 10:14 06/06/12 22:17 1☼Zinc 44
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic <0.050 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:27 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 06/13/12 12:00 06/14/12 09:27 1Barium 0.65
0.0050 0.0020 mg/L 06/13/12 12:00 06/14/12 09:27 1Cadmium 0.0038 J
0.025 0.010 mg/L 06/13/12 12:00 06/14/12 09:27 1Chromium <0.025
0.0075 0.0050 mg/L 06/13/12 12:00 06/14/12 09:27 1Lead 0.026
0.050 0.010 mg/L 06/13/12 12:00 06/14/12 09:27 1Selenium <0.050
0.025 0.0050 mg/L 06/13/12 12:00 06/14/12 09:27 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury <0.00020 H 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:31 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.014 J H 0.020 0.0060 mg/Kg ☼ 06/09/12 10:05 06/09/12 14:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-46374-20Client Sample ID: K7 (6-12")Matrix: SolidDate Collected: 05/07/12 16:30
Date Received: 05/16/12 07:00
General ChemistryRL MDL
pH 7.64 0.200 0.200 SU 06/11/12 14:36 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Definitions/GlossaryTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Qualifiers
GC/MS Semi VOA
Qualifier Description
H Sample was prepped or analyzed beyond the specified holding time
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Metals
Qualifier Description
H Sample was prepped or analyzed beyond the specified holding time
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
F MS or MSD exceeds the control limits
Glossary
These commonly used abbreviations may or may not be present in this report.
☼ Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CNF Contains no Free Liquid
DL, RA, RE, IN Indicates a Dilution, Reanalysis, Re-extraction, or additional Initial metals/anion analysis of the sample
EDL Estimated Detection Limit
EPA United States Environmental Protection Agency
MDL Method Detection Limit
ML Minimum Level (Dioxin)
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RL Reporting Limit
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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QC Association SummaryTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
GC/MS Semi VOA
Prep Batch: 151984
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3541500-46374-6 G19 (6-12") Total/NA
Solid 3541500-46374-8 I9 (6-12") Total/NA
Solid 3541500-46374-14 J13 (6-12") Total/NA
Solid 3541500-46374-16 J15 (6-12") Total/NA
Solid 3541500-46374-20 K7 (6-12") Total/NA
Solid 3541LCS 500-151984/2-A Lab Control Sample Total/NA
Solid 3541MB 500-151984/1-A Method Blank Total/NA
Analysis Batch: 152169
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270C 151984500-46374-6 G19 (6-12") Total/NA
Solid 8270C 151984500-46374-8 I9 (6-12") Total/NA
Solid 8270C 151984500-46374-14 J13 (6-12") Total/NA
Solid 8270C 151984500-46374-16 J15 (6-12") Total/NA
Solid 8270C 151984500-46374-20 K7 (6-12") Total/NA
Solid 8270C 151984LCS 500-151984/2-A Lab Control Sample Total/NA
Solid 8270C 151984MB 500-151984/1-A Method Blank Total/NA
Metals
Prep Batch: 151902
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3050B500-46374-6 G19 (6-12") Total/NA
Solid 3050B500-46374-8 I9 (6-12") Total/NA
Solid 3050B500-46374-14 J13 (6-12") Total/NA
Solid 3050B500-46374-16 J15 (6-12") Total/NA
Solid 3050B500-46374-20 K7 (6-12") Total/NA
Solid 3050BLCS 500-151902/2-A Lab Control Sample Total/NA
Solid 3050BMB 500-151902/1-A Method Blank Total/NA
Analysis Batch: 151982
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010B 151902500-46374-6 G19 (6-12") Total/NA
Solid 6010B 151902500-46374-8 I9 (6-12") Total/NA
Solid 6010B 151902500-46374-14 J13 (6-12") Total/NA
Solid 6010B 151902500-46374-16 J15 (6-12") Total/NA
Solid 6010B 151902500-46374-20 K7 (6-12") Total/NA
Solid 6010B 151902LCS 500-151902/2-A Lab Control Sample Total/NA
Solid 6010B 151902MB 500-151902/1-A Method Blank Total/NA
Analysis Batch: 152098
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010B 151902500-46374-14 J13 (6-12") Total/NA
Prep Batch: 152273
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471A500-46374-6 G19 (6-12") Total/NA
Solid 7471A500-46374-8 I9 (6-12") Total/NA
Solid 7471A500-46374-14 J13 (6-12") Total/NA
Solid 7471A500-46374-16 J15 (6-12") Total/NA
Solid 7471A500-46374-20 K7 (6-12") Total/NA
Solid 7471ALCS 500-152273/8-A Lab Control Sample Total/NA
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QC Association SummaryTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Metals (Continued)
Prep Batch: 152273 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471AMB 500-152273/7-A Method Blank Total/NA
Leach Batch: 152292
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 1311500-46374-5 G19 (0-6") TCLP
Solid 1311500-46374-6 G19 (6-12") TCLP
Solid 1311500-46374-7 I9 (0-6") TCLP
Solid 1311500-46374-8 I9 (6-12") TCLP
Solid 1311500-46374-8 DU I9 (6-12") TCLP
Solid 1311500-46374-8 MS I9 (6-12") TCLP
Solid 1311500-46374-13 J13 (0-6") TCLP
Solid 1311500-46374-14 J13 (6-12") TCLP
Solid 1311500-46374-15 J15 (0-6") TCLP
Solid 1311500-46374-16 J15 (6-12") TCLP
Solid 1311500-46374-19 K7 (0-6") TCLP
Solid 1311500-46374-20 K7 (6-12") TCLP
Solid 1311LB 500-152292/1-B LB Method Blank TCLP
Solid 1311LB 500-152292/1-C LB Method Blank TCLP
Analysis Batch: 152300
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471A 152273500-46374-6 G19 (6-12") Total/NA
Solid 7471A 152273500-46374-8 I9 (6-12") Total/NA
Solid 7471A 152273500-46374-14 J13 (6-12") Total/NA
Solid 7471A 152273500-46374-16 J15 (6-12") Total/NA
Solid 7471A 152273500-46374-20 K7 (6-12") Total/NA
Solid 7471A 152273LCS 500-152273/8-A Lab Control Sample Total/NA
Solid 7471A 152273MB 500-152273/7-A Method Blank Total/NA
Prep Batch: 152443
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7470A 152292500-46374-5 G19 (0-6") TCLP
Solid 7470A 152292500-46374-6 G19 (6-12") TCLP
Solid 7470A 152292500-46374-7 I9 (0-6") TCLP
Solid 7470A 152292500-46374-8 I9 (6-12") TCLP
Solid 7470A 152292500-46374-8 DU I9 (6-12") TCLP
Solid 7470A 152292500-46374-8 MS I9 (6-12") TCLP
Solid 7470A 152292500-46374-13 J13 (0-6") TCLP
Solid 7470A 152292500-46374-14 J13 (6-12") TCLP
Solid 7470A 152292500-46374-15 J15 (0-6") TCLP
Solid 7470A 152292500-46374-16 J15 (6-12") TCLP
Solid 7470A 152292500-46374-19 K7 (0-6") TCLP
Solid 7470A 152292500-46374-20 K7 (6-12") TCLP
Solid 7470A 152292LB 500-152292/1-B LB Method Blank TCLP
Solid 7470ALCS 500-152443/8-A Lab Control Sample Total/NA
Solid 7470AMB 500-152443/7-A Method Blank Total/NA
Analysis Batch: 152665
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7470A 152443500-46374-5 G19 (0-6") TCLP
Solid 7470A 152443500-46374-6 G19 (6-12") TCLP
Solid 7470A 152443500-46374-7 I9 (0-6") TCLP
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QC Association SummaryTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Metals (Continued)
Analysis Batch: 152665 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7470A 152443500-46374-8 I9 (6-12") TCLP
Solid 7470A 152443500-46374-8 DU I9 (6-12") TCLP
Solid 7470A 152443500-46374-8 MS I9 (6-12") TCLP
Solid 7470A 152443500-46374-13 J13 (0-6") TCLP
Solid 7470A 152443500-46374-14 J13 (6-12") TCLP
Solid 7470A 152443500-46374-15 J15 (0-6") TCLP
Solid 7470A 152443500-46374-16 J15 (6-12") TCLP
Solid 7470A 152443500-46374-19 K7 (0-6") TCLP
Solid 7470A 152443500-46374-20 K7 (6-12") TCLP
Solid 7470A 152443LB 500-152292/1-B LB Method Blank TCLP
Solid 7470A 152443LCS 500-152443/8-A Lab Control Sample Total/NA
Solid 7470A 152443MB 500-152443/7-A Method Blank Total/NA
Prep Batch: 152725
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3010A 152292500-46374-5 G19 (0-6") TCLP
Solid 3010A 152292500-46374-6 G19 (6-12") TCLP
Solid 3010A 152292500-46374-7 I9 (0-6") TCLP
Solid 3010A 152292500-46374-8 I9 (6-12") TCLP
Solid 3010A 152292500-46374-13 J13 (0-6") TCLP
Solid 3010A 152292500-46374-14 J13 (6-12") TCLP
Solid 3010A 152292500-46374-15 J15 (0-6") TCLP
Solid 3010A 152292500-46374-16 J15 (6-12") TCLP
Solid 3010A 152292500-46374-19 K7 (0-6") TCLP
Solid 3010A 152292500-46374-20 K7 (6-12") TCLP
Solid 3010A 152292LB 500-152292/1-C LB Method Blank TCLP
Solid 3010ALCS 500-152725/2-A Lab Control Sample Total/NA
Analysis Batch: 152812
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010B 152725500-46374-5 G19 (0-6") TCLP
Solid 6010B 152725500-46374-6 G19 (6-12") TCLP
Solid 6010B 152725500-46374-7 I9 (0-6") TCLP
Solid 6010B 152725500-46374-8 I9 (6-12") TCLP
Solid 6010B 152725500-46374-13 J13 (0-6") TCLP
Solid 6010B 152725500-46374-14 J13 (6-12") TCLP
Solid 6010B 152725500-46374-14 J13 (6-12") TCLP
Solid 6010B 152725500-46374-15 J15 (0-6") TCLP
Solid 6010B 152725500-46374-16 J15 (6-12") TCLP
Solid 6010B 152725500-46374-19 K7 (0-6") TCLP
Solid 6010B 152725500-46374-20 K7 (6-12") TCLP
Solid 6010B 152725LB 500-152292/1-C LB Method Blank TCLP
Solid 6010B 152725LCS 500-152725/2-A Lab Control Sample Total/NA
General Chemistry
Analysis Batch: 151862
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture500-46374-5 G19 (0-6") Total/NA
Solid Moisture500-46374-6 G19 (6-12") Total/NA
Solid Moisture500-46374-7 I9 (0-6") Total/NA
Solid Moisture500-46374-8 I9 (6-12") Total/NA
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QC Association SummaryTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
General Chemistry (Continued)
Analysis Batch: 151862 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture500-46374-13 J13 (0-6") Total/NA
Solid Moisture500-46374-14 J13 (6-12") Total/NA
Solid Moisture500-46374-15 J15 (0-6") Total/NA
Solid Moisture500-46374-16 J15 (6-12") Total/NA
Solid Moisture500-46374-19 K7 (0-6") Total/NA
Solid Moisture500-46374-20 K7 (6-12") Total/NA
Analysis Batch: 152028
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid D2974-87500-46374-5 G19 (0-6") Total/NA
Solid D2974-87500-46374-7 I9 (0-6") Total/NA
Solid D2974-87500-46374-13 J13 (0-6") Total/NA
Solid D2974-87500-46374-15 J15 (0-6") Total/NA
Solid D2974-87500-46374-19 K7 (0-6") Total/NA
Analysis Batch: 152439
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9045C500-46374-6 G19 (6-12") Total/NA
Solid 9045C500-46374-8 I9 (6-12") Total/NA
Solid 9045C500-46374-14 J13 (6-12") Total/NA
Solid 9045C500-46374-16 J15 (6-12") Total/NA
Solid 9045C500-46374-20 K7 (6-12") Total/NA
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Surrogate SummaryTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Method: 8270C - Semivolatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (30-119) (30-115) (36-134)
FBP NBZ TPH
53 47 71500-46374-6
Percent Surrogate Recovery (Acceptance Limits)
G19 (6-12")
47 45 57500-46374-8 I9 (6-12")
53 42 58500-46374-14 J13 (6-12")
60 50 71500-46374-16 J15 (6-12")
72 70 90500-46374-20 K7 (6-12")
89 88 81LCS 500-151984/2-A Lab Control Sample
89 89 89MB 500-151984/1-A Method Blank
Surrogate Legend
FBP = 2-Fluorobiphenyl
NBZ = Nitrobenzene-d5
TPH = Terphenyl-d14
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QC Sample ResultsTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Method: 8270C - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 500-151984/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 152169 Prep Batch: 151984
RL MDL
Acenaphthene <0.033 0.033 0.0099 mg/Kg 06/07/12 07:07 06/08/12 11:26 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.033 0.00760.033 mg/Kg 06/07/12 07:07 06/08/12 11:26 1Acenaphthylene
<0.033 0.00780.033 mg/Kg 06/07/12 07:07 06/08/12 11:26 1Anthracene
<0.033 0.00700.033 mg/Kg 06/07/12 07:07 06/08/12 11:26 1Benzo[a]anthracene
<0.033 0.00610.033 mg/Kg 06/07/12 07:07 06/08/12 11:26 1Benzo[a]pyrene
<0.033 0.00650.033 mg/Kg 06/07/12 07:07 06/08/12 11:26 1Benzo[b]fluoranthene
<0.033 0.0110.033 mg/Kg 06/07/12 07:07 06/08/12 11:26 1Benzo[g,h,i]perylene
<0.033 0.00790.033 mg/Kg 06/07/12 07:07 06/08/12 11:26 1Benzo[k]fluoranthene
<0.033 0.00750.033 mg/Kg 06/07/12 07:07 06/08/12 11:26 1Chrysene
<0.033 0.00930.033 mg/Kg 06/07/12 07:07 06/08/12 11:26 1Dibenz(a,h)anthracene
<0.033 0.0140.033 mg/Kg 06/07/12 07:07 06/08/12 11:26 1Fluoranthene
<0.033 0.00760.033 mg/Kg 06/07/12 07:07 06/08/12 11:26 1Fluorene
<0.033 0.0110.033 mg/Kg 06/07/12 07:07 06/08/12 11:26 1Indeno[1,2,3-cd]pyrene
<0.033 0.00640.033 mg/Kg 06/07/12 07:07 06/08/12 11:26 1Naphthalene
<0.033 0.0140.033 mg/Kg 06/07/12 07:07 06/08/12 11:26 1Phenanthrene
<0.033 0.0120.033 mg/Kg 06/07/12 07:07 06/08/12 11:26 1Pyrene
2-Fluorobiphenyl 89 30 - 119 06/08/12 11:26 1
MB MB
Surrogate
06/07/12 07:07
Dil FacPrepared AnalyzedQualifier Limits%Recovery
89 06/07/12 07:07 06/08/12 11:26 1Nitrobenzene-d5 30 - 115
89 06/07/12 07:07 06/08/12 11:26 1Terphenyl-d14 36 - 134
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-151984/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 152169 Prep Batch: 151984
Acenaphthene 1.67 1.46 mg/Kg 88 67 - 110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 1.67 1.51 mg/Kg 91 67 - 110
Anthracene 1.67 1.37 mg/Kg 82 67 - 112
Benzo[a]anthracene 1.67 1.44 mg/Kg 87 68 - 117
Benzo[a]pyrene 1.67 1.51 mg/Kg 91 64 - 118
Benzo[b]fluoranthene 1.67 1.71 mg/Kg 103 60 - 118
Benzo[g,h,i]perylene 1.67 1.50 mg/Kg 90 66 - 130
Benzo[k]fluoranthene 1.67 1.45 mg/Kg 87 56 - 129
Chrysene 1.67 1.57 mg/Kg 94 66 - 118
Dibenz(a,h)anthracene 1.67 1.55 mg/Kg 93 62 - 126
Fluoranthene 1.67 1.47 mg/Kg 88 68 - 121
Fluorene 1.67 1.51 mg/Kg 91 66 - 112
Indeno[1,2,3-cd]pyrene 1.67 1.53 mg/Kg 92 67 - 127
Naphthalene 1.67 1.37 mg/Kg 82 65 - 110
Phenanthrene 1.67 1.45 mg/Kg 87 66 - 118
Pyrene 1.67 1.38 mg/Kg 83 66 - 119
2-Fluorobiphenyl 30 - 119
Surrogate
89
LCS LCS
Qualifier Limits%Recovery
88Nitrobenzene-d5 30 - 115
81Terphenyl-d14 36 - 134
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QC Sample ResultsTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Method: 6010B - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 500-151902/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 151982 Prep Batch: 151902
RL MDL
Antimony <2.0 2.0 0.27 mg/Kg 06/06/12 10:14 06/06/12 20:48 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<1.0 0.221.0 mg/Kg 06/06/12 10:14 06/06/12 20:48 1Arsenic
<1.0 0.121.0 mg/Kg 06/06/12 10:14 06/06/12 20:48 1Barium
<0.20 0.0500.20 mg/Kg 06/06/12 10:14 06/06/12 20:48 1Cadmium
<1.0 0.171.0 mg/Kg 06/06/12 10:14 06/06/12 20:48 1Chromium
<1.0 0.271.0 mg/Kg 06/06/12 10:14 06/06/12 20:48 1Copper
<0.50 0.170.50 mg/Kg 06/06/12 10:14 06/06/12 20:48 1Lead
<1.0 0.291.0 mg/Kg 06/06/12 10:14 06/06/12 20:48 1Selenium
<0.50 0.0600.50 mg/Kg 06/06/12 10:14 06/06/12 20:48 1Silver
<2.0 0.692.0 mg/Kg 06/06/12 10:14 06/06/12 20:48 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-151902/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 151982 Prep Batch: 151902
Antimony 50.0 45.4 mg/Kg 91 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 10.0 8.74 mg/Kg 87 80 - 120
Barium 200 186 mg/Kg 93 80 - 120
Cadmium 5.00 4.65 mg/Kg 93 80 - 120
Chromium 20.0 19.5 mg/Kg 98 80 - 120
Copper 25.0 24.2 mg/Kg 97 80 - 120
Lead 10.0 9.60 mg/Kg 96 80 - 120
Selenium 10.0 8.22 mg/Kg 82 80 - 120
Silver 5.00 4.52 mg/Kg 90 80 - 120
Zinc 50.0 47.5 mg/Kg 95 80 - 120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-152725/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 152812 Prep Batch: 152725
Arsenic 0.100 0.0930 mg/L 93 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Barium 2.00 1.94 mg/L 97 80 - 120
Cadmium 0.0500 0.0492 mg/L 98 80 - 120
Chromium 0.200 0.197 mg/L 99 80 - 120
Lead 0.100 0.0976 mg/L 98 80 - 120
Selenium 0.100 0.0886 mg/L 89 80 - 120
Silver 0.0500 0.0504 mg/L 101 80 - 120
Client Sample ID: Method BlankLab Sample ID: LB 500-152292/1-C LB
Matrix: Solid Prep Type: TCLP
Analysis Batch: 152812 Prep Batch: 152725
RL MDL
Arsenic <0.050 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 08:18 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.50 0.0100.50 mg/L 06/13/12 12:00 06/14/12 08:18 1Barium
<0.0050 0.00200.0050 mg/L 06/13/12 12:00 06/14/12 08:18 1Cadmium
<0.025 0.0100.025 mg/L 06/13/12 12:00 06/14/12 08:18 1Chromium
<0.0075 0.00500.0075 mg/L 06/13/12 12:00 06/14/12 08:18 1Lead
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QC Sample ResultsTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Method: 6010B - Metals (ICP) (Continued)
Client Sample ID: Method BlankLab Sample ID: LB 500-152292/1-C LB
Matrix: Solid Prep Type: TCLP
Analysis Batch: 152812 Prep Batch: 152725
RL MDL
Selenium <0.050 0.050 0.010 mg/L 06/13/12 12:00 06/14/12 08:18 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.025 0.00500.025 mg/L 06/13/12 12:00 06/14/12 08:18 1Silver
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 500-152443/7-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 152665 Prep Batch: 152443
RL MDL
Mercury <0.00020 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 11:49 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-152443/8-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 152665 Prep Batch: 152443
Mercury 0.00200 0.00199 mg/L 100 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Method BlankLab Sample ID: LB 500-152292/1-B LB
Matrix: Solid Prep Type: TCLP
Analysis Batch: 152665 Prep Batch: 152443
RL MDL
Mercury 0.0000201 J 0.00020 0.000020 mg/L 06/11/12 15:20 06/12/12 12:03 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: I9 (6-12")Lab Sample ID: 500-46374-8 MS
Matrix: Solid Prep Type: TCLP
Analysis Batch: 152665 Prep Batch: 152443
Mercury <0.00020 H 0.00200 0.000968 H F mg/L 48 50 - 150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: I9 (6-12")Lab Sample ID: 500-46374-8 DU
Matrix: Solid Prep Type: TCLP
Analysis Batch: 152665 Prep Batch: 152443
Mercury <0.00020 H <0.00020 H mg/L NC 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: 7471A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 500-152273/7-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 152300 Prep Batch: 152273
RL MDL
Mercury <0.017 0.017 0.0051 mg/Kg 06/09/12 10:05 06/09/12 14:00 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
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QC Sample ResultsTestAmerica Job ID: 500-46374-3Client: Shaw Environmental & Infrastructure, Inc
SDG: 500-46374-1Project/Site: Naperville Sportsman Club
Method: 7471A - Mercury (CVAA) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-152273/8-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 152300 Prep Batch: 152273
Mercury 0.167 0.181 mg/Kg 108 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
TestAmerica ChicagoPage 34 of 43 6/14/2012
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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-46374-3
Project/Site: Naperville Sportsman Club SDG: 500-46374-1
Client Sample ID: G19 (0-6") Lab Sample ID: 500-46374-5Matrix: SolidDate Collected: 05/09/12 16:08
Date Received: 05/16/12 07:00
Leach 1311 06/09/12 13:30 PFK152292 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
TCLP
Prep 7470A 152443 06/11/12 15:20 MBG TAL CHITCLP
Analysis 7470A 1 152665 06/12/12 12:05 MBG TAL CHITCLP
Prep 3010A 152725 06/13/12 12:00 LAH TAL CHITCLP
Analysis 6010B 1 152812 06/14/12 08:26 TDS TAL CHITCLP
Analysis Moisture 1 151862 06/06/12 08:16 CMV TAL CHITotal/NA
Analysis D2974-87 1 152028 06/07/12 09:34 CMV TAL CHITotal/NA
Client Sample ID: G19 (6-12") Lab Sample ID: 500-46374-6Matrix: SolidDate Collected: 05/09/12 16:08
Percent Solids: 80.8Date Received: 05/16/12 07:00
Prep 3541 06/07/12 07:07 STW151984 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 152169 06/08/12 12:52 GES TAL CHITotal/NA
Prep 3050B 151902 06/06/12 10:14 LAH TAL CHITotal/NA
Analysis 6010B 1 151982 06/06/12 21:52 TDS TAL CHITotal/NA
Prep 7471A 152273 06/09/12 10:05 MBG TAL CHITotal/NA
Analysis 7471A 1 152300 06/09/12 14:03 MBG TAL CHITotal/NA
Leach 1311 152292 06/09/12 13:30 PFK TAL CHITCLP
Prep 7470A 152443 06/11/12 15:20 MBG TAL CHITCLP
Analysis 7470A 1 152665 06/12/12 12:06 MBG TAL CHITCLP
Prep 3010A 152725 06/13/12 12:00 LAH TAL CHITCLP
Analysis 6010B 1 152812 06/14/12 08:30 TDS TAL CHITCLP
Analysis Moisture 1 151862 06/06/12 08:16 CMV TAL CHITotal/NA
Analysis 9045C 1 152439 CLM TAL CHITotal/NA
06/11/12 14:22
06/11/12 14:26
(Start)
(End)
Client Sample ID: I9 (0-6") Lab Sample ID: 500-46374-7Matrix: SolidDate Collected: 05/09/12 13:22
Date Received: 05/16/12 07:00
Leach 1311 06/09/12 13:30 PFK152292 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
TCLP
Prep 7470A 152443 06/11/12 15:20 MBG TAL CHITCLP
Analysis 7470A 1 152665 06/12/12 12:08 MBG TAL CHITCLP
Prep 3010A 152725 06/13/12 12:00 LAH TAL CHITCLP
Analysis 6010B 1 152812 06/14/12 08:50 TDS TAL CHITCLP
Analysis Moisture 1 151862 06/06/12 08:16 CMV TAL CHITotal/NA
Analysis D2974-87 1 152028 06/07/12 09:34 CMV TAL CHITotal/NA
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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-46374-3
Project/Site: Naperville Sportsman Club SDG: 500-46374-1
Client Sample ID: I9 (6-12") Lab Sample ID: 500-46374-8Matrix: SolidDate Collected: 05/09/12 13:22
Percent Solids: 65.5Date Received: 05/16/12 07:00
Prep 3541 06/07/12 07:07 STW151984 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 152169 06/08/12 13:10 GES TAL CHITotal/NA
Prep 3050B 151902 06/06/12 10:14 LAH TAL CHITotal/NA
Analysis 6010B 1 151982 06/06/12 21:58 TDS TAL CHITotal/NA
Prep 7471A 152273 06/09/12 10:05 MBG TAL CHITotal/NA
Analysis 7471A 1 152300 06/09/12 14:05 MBG TAL CHITotal/NA
Leach 1311 152292 06/09/12 13:30 PFK TAL CHITCLP
Prep 7470A 152443 06/11/12 15:20 MBG TAL CHITCLP
Analysis 7470A 1 152665 06/12/12 12:10 MBG TAL CHITCLP
Prep 3010A 152725 06/13/12 12:00 LAH TAL CHITCLP
Analysis 6010B 1 152812 06/14/12 08:54 TDS TAL CHITCLP
Analysis Moisture 1 151862 06/06/12 08:16 CMV TAL CHITotal/NA
Analysis 9045C 1 152439 CLM TAL CHITotal/NA
06/11/12 14:26
06/11/12 14:29
(Start)
(End)
Client Sample ID: J13 (0-6") Lab Sample ID: 500-46374-13Matrix: SolidDate Collected: 05/07/12 13:40
Date Received: 05/16/12 07:00
Leach 1311 06/09/12 13:30 PFK152292 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
TCLP
Prep 7470A 152443 06/11/12 15:20 MBG TAL CHITCLP
Analysis 7470A 1 152665 06/12/12 12:15 MBG TAL CHITCLP
Prep 3010A 152725 06/13/12 12:00 LAH TAL CHITCLP
Analysis 6010B 1 152812 06/14/12 09:07 TDS TAL CHITCLP
Analysis Moisture 1 151862 06/06/12 08:16 CMV TAL CHITotal/NA
Analysis D2974-87 1 152028 06/07/12 09:34 CMV TAL CHITotal/NA
Client Sample ID: J13 (6-12") Lab Sample ID: 500-46374-14Matrix: SolidDate Collected: 05/07/12 13:40
Percent Solids: 58.9Date Received: 05/16/12 07:00
Prep 3541 06/07/12 07:07 STW151984 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 152169 06/08/12 13:27 GES TAL CHITotal/NA
Prep 3050B 151902 06/06/12 10:14 LAH TAL CHITotal/NA
Analysis 6010B 1 151982 06/06/12 22:05 TDS TAL CHITotal/NA
Analysis 6010B 100 152098 06/07/12 13:17 TDS TAL CHITotal/NA
Prep 7471A 152273 06/09/12 10:05 MBG TAL CHITotal/NA
Analysis 7471A 1 152300 06/09/12 14:07 MBG TAL CHITotal/NA
Leach 1311 152292 06/09/12 13:30 PFK TAL CHITCLP
Prep 7470A 152443 06/11/12 15:20 MBG TAL CHITCLP
Analysis 7470A 1 152665 06/12/12 12:17 MBG TAL CHITCLP
Prep 3010A 152725 06/13/12 12:00 LAH TAL CHITCLP
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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-46374-3
Project/Site: Naperville Sportsman Club SDG: 500-46374-1
Client Sample ID: J13 (6-12") Lab Sample ID: 500-46374-14Matrix: SolidDate Collected: 05/07/12 13:40
Date Received: 05/16/12 07:00
Analysis 6010B 06/14/12 09:11 TDS1 152812 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
TCLP
Analysis 6010B 100 152812 06/14/12 10:23 TDS TAL CHITCLP
Analysis Moisture 1 151862 06/06/12 08:16 CMV TAL CHITotal/NA
Analysis 9045C 1 152439 CLM TAL CHITotal/NA
06/11/12 14:29
06/11/12 14:32
(Start)
(End)
Client Sample ID: J15 (0-6") Lab Sample ID: 500-46374-15Matrix: SolidDate Collected: 05/07/12 13:00
Date Received: 05/16/12 07:00
Leach 1311 06/09/12 13:30 PFK152292 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
TCLP
Prep 7470A 152443 06/11/12 15:20 MBG TAL CHITCLP
Analysis 7470A 1 152665 06/12/12 12:19 MBG TAL CHITCLP
Prep 3010A 152725 06/13/12 12:00 LAH TAL CHITCLP
Analysis 6010B 1 152812 06/14/12 09:15 TDS TAL CHITCLP
Analysis Moisture 1 151862 06/06/12 08:16 CMV TAL CHITotal/NA
Analysis D2974-87 1 152028 06/07/12 09:34 CMV TAL CHITotal/NA
Client Sample ID: J15 (6-12") Lab Sample ID: 500-46374-16Matrix: SolidDate Collected: 05/07/12 13:00
Percent Solids: 61.1Date Received: 05/16/12 07:00
Prep 3541 06/07/12 07:07 STW151984 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 152169 06/08/12 13:44 GES TAL CHITotal/NA
Prep 3050B 151902 06/06/12 10:14 LAH TAL CHITotal/NA
Analysis 6010B 1 151982 06/06/12 22:11 TDS TAL CHITotal/NA
Prep 7471A 152273 06/09/12 10:05 MBG TAL CHITotal/NA
Analysis 7471A 1 152300 06/09/12 14:08 MBG TAL CHITotal/NA
Leach 1311 152292 06/09/12 13:30 PFK TAL CHITCLP
Prep 7470A 152443 06/11/12 15:20 MBG TAL CHITCLP
Analysis 7470A 1 152665 06/12/12 12:28 MBG TAL CHITCLP
Prep 3010A 152725 06/13/12 12:00 LAH TAL CHITCLP
Analysis 6010B 1 152812 06/14/12 09:19 TDS TAL CHITCLP
Analysis Moisture 1 151862 06/06/12 08:16 CMV TAL CHITotal/NA
Analysis 9045C 1 152439 CLM TAL CHITotal/NA
06/11/12 14:32
06/11/12 14:36
(Start)
(End)
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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-46374-3
Project/Site: Naperville Sportsman Club SDG: 500-46374-1
Client Sample ID: K7 (0-6") Lab Sample ID: 500-46374-19Matrix: SolidDate Collected: 05/07/12 16:30
Date Received: 05/16/12 07:00
Leach 1311 06/09/12 13:30 PFK152292 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
TCLP
Prep 7470A 152443 06/11/12 15:20 MBG TAL CHITCLP
Analysis 7470A 1 152665 06/12/12 12:30 MBG TAL CHITCLP
Prep 3010A 152725 06/13/12 12:00 LAH TAL CHITCLP
Analysis 6010B 1 152812 06/14/12 09:23 TDS TAL CHITCLP
Analysis Moisture 1 151862 06/06/12 08:16 CMV TAL CHITotal/NA
Analysis D2974-87 1 152028 06/07/12 09:34 CMV TAL CHITotal/NA
Client Sample ID: K7 (6-12") Lab Sample ID: 500-46374-20Matrix: SolidDate Collected: 05/07/12 16:30
Percent Solids: 77.9Date Received: 05/16/12 07:00
Prep 3541 06/07/12 07:07 STW151984 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 152169 06/08/12 14:02 GES TAL CHITotal/NA
Prep 3050B 151902 06/06/12 10:14 LAH TAL CHITotal/NA
Analysis 6010B 1 151982 06/06/12 22:17 TDS TAL CHITotal/NA
Prep 7471A 152273 06/09/12 10:05 MBG TAL CHITotal/NA
Analysis 7471A 1 152300 06/09/12 14:11 MBG TAL CHITotal/NA
Leach 1311 152292 06/09/12 13:30 PFK TAL CHITCLP
Prep 7470A 152443 06/11/12 15:20 MBG TAL CHITCLP
Analysis 7470A 1 152665 06/12/12 12:31 MBG TAL CHITCLP
Prep 3010A 152725 06/13/12 12:00 LAH TAL CHITCLP
Analysis 6010B 1 152812 06/14/12 09:27 TDS TAL CHITCLP
Analysis Moisture 1 151862 06/06/12 08:16 CMV TAL CHITotal/NA
Analysis 9045C 1 152439 CLM TAL CHITotal/NA
06/11/12 14:36
06/11/12 14:39
(Start)
(End)
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200
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Certification SummaryClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-46374-3
Project/Site: Naperville Sportsman Club SDG: 500-46374-1
Laboratory Authority Program EPA Region Certification ID
TestAmerica Chicago 40461State ProgramAlabama 4
TestAmerica Chicago 01132CANELACCalifornia 9
TestAmerica Chicago E871072NELACFlorida 4
TestAmerica Chicago 939State ProgramGeorgia 4
TestAmerica Chicago N/AState ProgramGeorgia 4
TestAmerica Chicago N/AState ProgramHawaii 9
TestAmerica Chicago 100201NELACIllinois 5
TestAmerica Chicago C-IL-02State ProgramIndiana 5
TestAmerica Chicago 82State ProgramIowa 7
TestAmerica Chicago E-10161NELACKansas 7
TestAmerica Chicago 90023State ProgramKentucky 4
TestAmerica Chicago 66State ProgramKentucky (UST) 4
TestAmerica Chicago L2304DoD ELAPL-A-B
TestAmerica Chicago L2304ISO/IEC 17025L-A-B
TestAmerica Chicago 30720NELACLouisiana 6
TestAmerica Chicago M-IL035State ProgramMassachusetts 1
TestAmerica Chicago N/AState ProgramMississippi 4
TestAmerica Chicago 291State ProgramNorth Carolina DENR 4
TestAmerica Chicago R-194State ProgramNorth Dakota 8
TestAmerica Chicago 8908State ProgramOklahoma 6
TestAmerica Chicago 77001State ProgramSouth Carolina 4
TestAmerica Chicago T104704252-09-TXNELACTexas 6
TestAmerica Chicago P330-12-00038FederalUSDA
TestAmerica Chicago 460142NELACVirginia 3
TestAmerica Chicago 999580010State ProgramWisconsin 5
TestAmerica Chicago 8TMS-QState ProgramWyoming 8
Accreditation may not be offered or required for all methods and analytes reported in this package. Please contact your project manager for the laboratory's
current list of certified methods and analytes.
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Login Sample Receipt Checklist
Client: Shaw Environmental & Infrastructure, Inc Job Number: 500-46374-3
SDG Number: 500-46374-1
Login Number: 46374
Question Answer Comment
Creator: Lunt, Jeff T
List Source: TestAmerica Chicago
List Number: 1
TrueRadioactivity either was not measured or, if measured, is at or below background
N/AThe cooler's custody seal, if present, is intact.
TrueThe cooler or samples do not appear to have been compromised or tampered with.
TrueSamples were received on ice. 4.0
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the sample IDs on the containers and the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs
TrueVOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica ChicagoPage 43 of 43 6/14/2012
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ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Chicago2417 Bond StreetUniversity Park, IL 60484Tel: (708)534-5200
TestAmerica Job ID: 500-52298-1Client Project/Site: Naperville Sportsman Club
For:Shaw Environmental & Infrastructure, Inc1607 East Main StreetSuite ESaint Charles, Illinois 60174
Attn: Jeffrey Cademartori
Authorized for release by:11/26/2012 12:00:57 PM
Richard WrightProject Manager [email protected]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Shaw Environmental & Infrastructure, IncProject/Site: Naperville Sportsman Club
TestAmerica Job ID: 500-52298-1
Page 2 of 104TestAmerica Chicago
11/26/2012
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 66
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 76
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 77
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 88
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 100
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 101
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 104
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Case NarrativeClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-52298-1
Project/Site: Naperville Sportsman Club
Job ID: 500-52298-1
Laboratory: TestAmerica Chicago
Narrative
Job Narrative
500-52298-1
Comments
No additional comments.
Receipt
The samples were received on 11/13/2012 1:30 PM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperature of the cooler at receipt was 3.2º C.
GC/MS Semi VOA
Method(s) 8270C: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for sample -10 were outside control limits for two and
nine analytes, respectively. The associated laboratory control sample (LCS) recovery met the marginal exceedence acceptance
criteria.H10 (N30') (0-6") (500-52298-10)
Method(s) 8270C: The following samples were diluted due to the abundance of non-target analytes (hydrocarbon background): H10 (N30')
(0-6") (500-52298-10), J17 (N30;W20') (0-6") (500-52298-19), K12 (W25') (12-18') (500-52298-24). Elevated reporting limits (RLs) are
provided.
No other analytical or quality issues were noted.
Metals
Method(s) 6010B: The extraction blank (LB) for preparation batch 170228 contained Pb above the reporting limit (RL). The associated
samples, 500-52298-21-24, contained detects for this analyte at concentrations greater than 10X the value found in the method blank;
therefore, re-extraction and/or re-analysis of samples was not performed.
Method(s) 6010B: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for sample 500-52298-1 were outside control limits for
Sb. The MS was also out for Cu, and the MSD was also out for Se. The associated laboratory control sample (LCS) recovery met
acceptance criteria.
Method(s) 6010B: The matrix spike / matrix spike duplicate (MS/MSD) precision for sample 500-52298-1 was outside control limits for Cu.
The associated laboratory control sample (LCS) met acceptance criteria.
Method(s) 7470A: The continuing calibration verification (CCV) at line 45 in AD batch 170438 recoverd above the upper control limit for Hg.
The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported.
Method(s) 7470A: The laboratory control sample (LCS) for batch 170438 exceeded control limits for Hg. These analytes were biased high
in the LCS and were not detected in the associated samples; therefore, the data have been reported.
Method(s) 7470A: The matrix spike (MS) recovery for sample 52298-1 was outside control limits for Hg. The associated laboratory control
sample (LCS) recovery met acceptance criteria.
No other analytical or quality issues were noted.
General Chemistry
No analytical or quality issues were noted.
Organic Prep
No analytical or quality issues were noted.
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Detection SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Client Sample ID: F20 (0-6") Lab Sample ID: 500-52298-1
☼Benzo[a]anthracene
RL
0.053 mg/Kg
MDL
0.011
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J0.045
☼Benzo[a]pyrene 0.053 mg/Kg0.0096 Total/NA8270C10.050 J
☼Benzo[b]fluoranthene 0.053 mg/Kg0.010 Total/NA8270C10.078
☼Benzo[g,h,i]perylene 0.053 mg/Kg0.018 Total/NA8270C10.046 J
☼Benzo[k]fluoranthene 0.053 mg/Kg0.013 Total/NA8270C10.044 J
☼Chrysene 0.053 mg/Kg0.012 Total/NA8270C10.082
☼Fluoranthene 0.053 mg/Kg0.022 Total/NA8270C10.11
☼Indeno[1,2,3-cd]pyrene 0.053 mg/Kg0.018 Total/NA8270C10.032 J
☼Phenanthrene 0.053 mg/Kg0.022 Total/NA8270C10.035 J
☼Pyrene 0.053 mg/Kg0.019 Total/NA8270C10.12
☼Antimony 3.3 mg/Kg0.43 Total/NA6010B10.75 J
☼Arsenic 1.6 mg/Kg0.36 Total/NA6010B15.1
☼Barium 1.6 mg/Kg0.19 Total/NA6010B155
☼Cadmium 0.33 mg/Kg0.081 Total/NA6010B10.44
☼Chromium 1.6 mg/Kg0.27 Total/NA6010B19.4
☼Copper 1.6 mg/Kg0.44 Total/NA6010B118
☼Lead 0.82 mg/Kg0.28 Total/NA6010B134
☼Selenium 1.6 mg/Kg0.47 Total/NA6010B10.79 J
☼Zinc 3.3 mg/Kg1.1 Total/NA6010B159
Barium 0.50 mg/L0.010 TCLP6010B10.45 J
Lead 0.0075 mg/L0.0050 TCLP6010B10.014
☼Mercury 0.025 mg/Kg0.0096 Total/NA7471A10.031
pH 0.200 SU0.200 Total/NA9045C17.82
Client Sample ID: F20 (6-12") Lab Sample ID: 500-52298-2
☼Chrysene
RL
0.041 mg/Kg
MDL
0.0092
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J0.012
☼Antimony 2.2 mg/Kg0.29 Total/NA6010B10.75 J
☼Arsenic 1.1 mg/Kg0.24 Total/NA6010B14.7
☼Barium 1.1 mg/Kg0.13 Total/NA6010B132
☼Cadmium 0.22 mg/Kg0.055 Total/NA6010B10.27
☼Chromium 1.1 mg/Kg0.18 Total/NA6010B17.5
☼Copper 1.1 mg/Kg0.30 Total/NA6010B113
☼Lead 0.55 mg/Kg0.19 Total/NA6010B115
☼Zinc 2.2 mg/Kg0.76 Total/NA6010B137
Barium 0.50 mg/L0.010 TCLP6010B10.64
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0024 J
Lead 0.0075 mg/L0.0050 TCLP6010B10.0077
☼Mercury 0.020 mg/Kg0.0076 Total/NA7471A10.030
pH 0.200 SU0.200 Total/NA9045C17.95
Client Sample ID: F20 (12-18") Lab Sample ID: 500-52298-3
☼Antimony
RL
2.4 mg/Kg
MDL
0.32
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B Total/NA1J0.79
☼Arsenic 1.2 mg/Kg0.26 Total/NA6010B112
☼Barium 1.2 mg/Kg0.14 Total/NA6010B144
☼Cadmium 0.24 mg/Kg0.060 Total/NA6010B10.29
☼Chromium 1.2 mg/Kg0.20 Total/NA6010B112
☼Copper 1.2 mg/Kg0.33 Total/NA6010B129
☼Lead 0.60 mg/Kg0.21 Total/NA6010B118
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Detection SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Client Sample ID: F20 (12-18") (Continued) Lab Sample ID: 500-52298-3
☼Selenium
RL
1.2 mg/Kg
MDL
0.35
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B Total/NA1J0.48
☼Zinc 2.4 mg/Kg0.83 Total/NA6010B151
Barium 0.50 mg/L0.010 TCLP6010B10.73
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0021 J
Mercury 0.00020 mg/L0.000020 TCLP7470A10.000022 J *
☼Mercury 0.019 mg/Kg0.0073 Total/NA7471A10.029
pH 0.200 SU0.200 Total/NA9045C17.84
Client Sample ID: H20 (E20') (0-6") Lab Sample ID: 500-52298-4
☼Benzo[a]anthracene
RL
0.096 mg/Kg
MDL
0.020
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J0.039
☼Benzo[a]pyrene 0.096 mg/Kg0.018 Total/NA8270C10.049 J
☼Benzo[b]fluoranthene 0.096 mg/Kg0.019 Total/NA8270C10.076 J
☼Benzo[g,h,i]perylene 0.096 mg/Kg0.032 Total/NA8270C10.058 J
☼Chrysene 0.096 mg/Kg0.022 Total/NA8270C10.052 J
☼Indeno[1,2,3-cd]pyrene 0.096 mg/Kg0.032 Total/NA8270C10.041 J
☼Pyrene 0.096 mg/Kg0.035 Total/NA8270C10.048 J
☼Antimony 5.9 mg/Kg0.78 Total/NA6010B12.8 J
☼Arsenic 2.9 mg/Kg0.64 Total/NA6010B17.1
☼Barium 2.9 mg/Kg0.35 Total/NA6010B181
☼Cadmium 0.59 mg/Kg0.15 Total/NA6010B10.62
☼Chromium 2.9 mg/Kg0.49 Total/NA6010B112
☼Copper 2.9 mg/Kg0.80 Total/NA6010B122
☼Lead 1.5 mg/Kg0.51 Total/NA6010B1110
☼Zinc 5.9 mg/Kg2.0 Total/NA6010B164
Barium 0.50 mg/L0.010 TCLP6010B10.49 J
Lead 0.0075 mg/L0.0050 TCLP6010B10.051
Mercury 0.00020 mg/L0.000020 TCLP7470A10.000025 J *
☼Mercury 0.046 mg/Kg0.017 Total/NA7471A10.034 J
pH 0.200 SU0.200 Total/NA9045C17.71
Client Sample ID: H20 (E20') (6-12") Lab Sample ID: 500-52298-5
☼Antimony
RL
2.2 mg/Kg
MDL
0.29
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B Total/NA1J0.68
☼Arsenic 1.1 mg/Kg0.24 Total/NA6010B18.6
☼Barium 1.1 mg/Kg0.13 Total/NA6010B155
☼Cadmium 0.22 mg/Kg0.054 Total/NA6010B10.23
☼Chromium 1.1 mg/Kg0.18 Total/NA6010B115
☼Copper 1.1 mg/Kg0.29 Total/NA6010B125
☼Lead 0.54 mg/Kg0.19 Total/NA6010B116
☼Zinc 2.2 mg/Kg0.74 Total/NA6010B159
Barium 0.50 mg/L0.010 TCLP6010B10.82
Mercury 0.00020 mg/L0.000020 TCLP7470A10.000041 J *
☼Mercury 0.019 mg/Kg0.0074 Total/NA7471A10.020
pH 0.200 SU0.200 Total/NA9045C17.95
Client Sample ID: H20 (E20') (12-18") Lab Sample ID: 500-52298-6
☼Antimony
RL
2.4 mg/Kg
MDL
0.32
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B Total/NA1J0.57
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Detection SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Client Sample ID: H20 (E20') (12-18") (Continued) Lab Sample ID: 500-52298-6
☼Arsenic
RL
1.2 mg/Kg
MDL
0.26
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B Total/NA117
☼Barium 1.2 mg/Kg0.14 Total/NA6010B160
☼Cadmium 0.24 mg/Kg0.059 Total/NA6010B10.19 J
☼Chromium 1.2 mg/Kg0.20 Total/NA6010B115
☼Copper 1.2 mg/Kg0.32 Total/NA6010B124
☼Lead 0.60 mg/Kg0.21 Total/NA6010B115
☼Zinc 2.4 mg/Kg0.82 Total/NA6010B152
Barium 0.50 mg/L0.010 TCLP6010B10.71
Mercury 0.00020 mg/L0.000020 TCLP7470A10.000022 J *
☼Mercury 0.020 mg/Kg0.0076 Total/NA7471A10.037
pH 0.200 SU0.200 Total/NA9045C17.96
Client Sample ID: K10 (W25') (0-6") Lab Sample ID: 500-52298-7
☼Benzo[a]anthracene
RL
0.095 mg/Kg
MDL
0.020
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA10.098
☼Benzo[a]pyrene 0.095 mg/Kg0.017 Total/NA8270C10.13
☼Benzo[b]fluoranthene 0.095 mg/Kg0.019 Total/NA8270C10.16
☼Benzo[g,h,i]perylene 0.095 mg/Kg0.032 Total/NA8270C10.12
☼Benzo[k]fluoranthene 0.095 mg/Kg0.023 Total/NA8270C10.12
☼Chrysene 0.095 mg/Kg0.022 Total/NA8270C10.13
☼Dibenz(a,h)anthracene 0.095 mg/Kg0.027 Total/NA8270C10.050 J
☼Fluoranthene 0.095 mg/Kg0.039 Total/NA8270C10.15
☼Indeno[1,2,3-cd]pyrene 0.095 mg/Kg0.032 Total/NA8270C10.10
☼Phenanthrene 0.095 mg/Kg0.040 Total/NA8270C10.053 J
☼Pyrene 0.095 mg/Kg0.035 Total/NA8270C10.12
☼Antimony 270 mg/Kg36 Total/NA6010B506900
☼Arsenic 2.7 mg/Kg0.59 Total/NA6010B12200
☼Barium 2.7 mg/Kg0.32 Total/NA6010B187
☼Cadmium 0.54 mg/Kg0.13 Total/NA6010B12.6
☼Chromium 2.7 mg/Kg0.45 Total/NA6010B18.9
☼Copper 2.7 mg/Kg0.74 Total/NA6010B123
☼Lead 68 mg/Kg23 Total/NA6010B50150000
☼Selenium 2.7 mg/Kg0.78 Total/NA6010B12.0 J
☼Silver 1.4 mg/Kg0.16 Total/NA6010B112
☼Zinc 5.4 mg/Kg1.9 Total/NA6010B160
Arsenic 0.050 mg/L0.010 TCLP6010B10.11
Barium 0.50 mg/L0.010 TCLP6010B10.54
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0041 J
Lead 0.0075 mg/L0.0050 TCLP6010B19.3
Mercury 0.00020 mg/L0.000020 TCLP7470A10.000020 J *
☼Mercury 0.045 mg/Kg0.017 Total/NA7471A10.044 J
pH 0.200 SU0.200 Total/NA9045C17.31
Client Sample ID: K10 (W25') (6-12") Lab Sample ID: 500-52298-8
☼Benzo[a]anthracene
RL
0.069 mg/Kg
MDL
0.014
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA10.072
☼Benzo[a]pyrene 0.069 mg/Kg0.013 Total/NA8270C10.084
☼Benzo[b]fluoranthene 0.069 mg/Kg0.013 Total/NA8270C10.095
☼Benzo[g,h,i]perylene 0.069 mg/Kg0.023 Total/NA8270C10.066 J
☼Benzo[k]fluoranthene 0.069 mg/Kg0.016 Total/NA8270C10.089
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Detection SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Client Sample ID: K10 (W25') (6-12") (Continued) Lab Sample ID: 500-52298-8
☼Chrysene
RL
0.069 mg/Kg
MDL
0.016
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA10.10
☼Fluoranthene 0.069 mg/Kg0.028 Total/NA8270C10.16
☼Indeno[1,2,3-cd]pyrene 0.069 mg/Kg0.023 Total/NA8270C10.061 J
☼Phenanthrene 0.069 mg/Kg0.029 Total/NA8270C10.082
☼Pyrene 0.069 mg/Kg0.025 Total/NA8270C10.14
☼Antimony 4.1 mg/Kg0.54 Total/NA6010B14.8
☼Arsenic 2.0 mg/Kg0.44 Total/NA6010B17.1
☼Barium 2.0 mg/Kg0.24 Total/NA6010B1110
☼Cadmium 0.41 mg/Kg0.10 Total/NA6010B10.52
☼Chromium 2.0 mg/Kg0.34 Total/NA6010B113
☼Copper 2.0 mg/Kg0.55 Total/NA6010B122
☼Lead 1.0 mg/Kg0.35 Total/NA6010B1950
☼Zinc 4.1 mg/Kg1.4 Total/NA6010B182
Arsenic 0.050 mg/L0.010 TCLP6010B10.42
Barium 0.50 mg/L0.010 TCLP6010B11.1
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0048 J
Lead 0.0075 mg/L0.0050 TCLP6010B143
Mercury 0.00020 mg/L0.000020 TCLP7470A10.000023 J *
☼Mercury 0.033 mg/Kg0.013 Total/NA7471A10.067
pH 0.200 SU0.200 Total/NA9045C17.34
Client Sample ID: K10 (W25') (12-18") Lab Sample ID: 500-52298-9
☼Antimony
RL
2.4 mg/Kg
MDL
0.32
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B Total/NA1J0.99
☼Arsenic 1.2 mg/Kg0.26 Total/NA6010B15.3
☼Barium 1.2 mg/Kg0.14 Total/NA6010B177
☼Cadmium 0.24 mg/Kg0.060 Total/NA6010B10.27
☼Chromium 1.2 mg/Kg0.20 Total/NA6010B110
☼Copper 1.2 mg/Kg0.33 Total/NA6010B116
☼Lead 0.61 mg/Kg0.21 Total/NA6010B115
☼Selenium 1.2 mg/Kg0.35 Total/NA6010B10.58 J
☼Zinc 2.4 mg/Kg0.83 Total/NA6010B146
Barium 0.50 mg/L0.010 TCLP6010B11.2
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0045 J
Lead 0.0075 mg/L0.0050 TCLP6010B10.74
Mercury 0.00020 mg/L0.000020 TCLP7470A10.000026 J *
☼Mercury 0.021 mg/Kg0.0078 Total/NA7471A10.010 J
pH 0.200 SU0.200 Total/NA9045C17.53
Client Sample ID: H10 (N30') (0-6") Lab Sample ID: 500-52298-10
☼Benzo[a]anthracene
RL
0.21 mg/Kg
MDL
0.045
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA5J0.20
☼Benzo[a]pyrene 0.21 mg/Kg0.039 Total/NA8270C50.34
☼Benzo[b]fluoranthene 0.21 mg/Kg0.042 Total/NA8270C50.38
☼Benzo[g,h,i]perylene 0.21 mg/Kg0.073 Total/NA8270C50.25
☼Benzo[k]fluoranthene 0.21 mg/Kg0.051 Total/NA8270C50.26
☼Chrysene 0.21 mg/Kg0.049 Total/NA8270C50.24
☼Fluoranthene 0.21 mg/Kg0.088 Total/NA8270C50.14 J
☼Indeno[1,2,3-cd]pyrene 0.21 mg/Kg0.073 Total/NA8270C50.22
☼Pyrene 0.21 mg/Kg0.078 Total/NA8270C50.15 J
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Detection SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Client Sample ID: H10 (N30') (0-6") (Continued) Lab Sample ID: 500-52298-10
☼Antimony
RL
2.4 mg/Kg
MDL
0.32
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B Total/NA1J1.5
☼Arsenic 1.2 mg/Kg0.26 Total/NA6010B17.1
☼Barium 1.2 mg/Kg0.14 Total/NA6010B181
☼Cadmium 0.24 mg/Kg0.060 Total/NA6010B10.41
☼Chromium 1.2 mg/Kg0.20 Total/NA6010B114
☼Copper 1.2 mg/Kg0.33 Total/NA6010B120
☼Lead 0.61 mg/Kg0.21 Total/NA6010B172
☼Zinc 2.4 mg/Kg0.83 Total/NA6010B187
Arsenic 0.050 mg/L0.010 TCLP6010B10.015 J
Barium 0.50 mg/L0.010 TCLP6010B10.57
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0027 J
Lead 0.0075 mg/L0.0050 TCLP6010B10.47
Mercury 0.00020 mg/L0.000020 TCLP7470A10.000025 J *
☼Mercury 0.021 mg/Kg0.0080 Total/NA7471A10.038
pH 0.200 SU0.200 Total/NA9045C17.34
Client Sample ID: H10 (N30') (6-12") Lab Sample ID: 500-52298-11
☼Arsenic
RL
1.2 mg/Kg
MDL
0.27
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B Total/NA16.0
☼Barium 1.2 mg/Kg0.14 Total/NA6010B1130
☼Cadmium 0.24 mg/Kg0.060 Total/NA6010B10.20 J
☼Chromium 1.2 mg/Kg0.20 Total/NA6010B118
☼Copper 1.2 mg/Kg0.33 Total/NA6010B122
☼Lead 0.61 mg/Kg0.21 Total/NA6010B119
☼Zinc 2.4 mg/Kg0.83 Total/NA6010B162
Barium 0.50 mg/L0.010 TCLP6010B10.72
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0020 J
Lead 0.0075 mg/L0.0050 TCLP6010B10.010
☼Mercury 0.021 mg/Kg0.0079 Total/NA7471A10.034
pH 0.200 SU0.200 Total/NA9045C17.45
Client Sample ID: H10 (N30') (12-18") Lab Sample ID: 500-52298-12
☼Antimony
RL
2.1 mg/Kg
MDL
0.28
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B Total/NA1J0.64
☼Arsenic 1.1 mg/Kg0.23 Total/NA6010B17.6
☼Barium 1.1 mg/Kg0.13 Total/NA6010B1110
☼Cadmium 0.21 mg/Kg0.052 Total/NA6010B10.21
☼Chromium 1.1 mg/Kg0.18 Total/NA6010B113
☼Copper 1.1 mg/Kg0.29 Total/NA6010B122
☼Lead 0.53 mg/Kg0.18 Total/NA6010B115
☼Zinc 2.1 mg/Kg0.72 Total/NA6010B159
Barium 0.50 mg/L0.010 TCLP6010B10.77
Lead 0.0075 mg/L0.0050 TCLP6010B10.013
Mercury 0.00020 mg/L0.000020 TCLP7470A10.000028 J *
☼Mercury 0.019 mg/Kg0.0071 Total/NA7471A10.030
pH 0.200 SU0.200 Total/NA9045C17.54
Client Sample ID: J8 (0-6") Lab Sample ID: 500-52298-13
TestAmerica Chicago
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Detection SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Client Sample ID: J8 (0-6") (Continued) Lab Sample ID: 500-52298-13
☼Benzo[a]anthracene
RL
0.044 mg/Kg
MDL
0.0093
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J0.011
☼Benzo[b]fluoranthene 0.044 mg/Kg0.0086 Total/NA8270C10.014 J
☼Chrysene 0.044 mg/Kg0.010 Total/NA8270C10.017 J
☼Naphthalene 0.044 mg/Kg0.0085 Total/NA8270C10.0087 J
☼Arsenic 1.2 mg/Kg0.25 Total/NA6010B17.8
☼Barium 1.2 mg/Kg0.14 Total/NA6010B1100
☼Cadmium 0.23 mg/Kg0.058 Total/NA6010B10.37
☼Chromium 1.2 mg/Kg0.19 Total/NA6010B115
☼Copper 1.2 mg/Kg0.32 Total/NA6010B124
☼Lead 0.58 mg/Kg0.20 Total/NA6010B125
☼Selenium 1.2 mg/Kg0.33 Total/NA6010B10.67 J
☼Zinc 2.3 mg/Kg0.80 Total/NA6010B177
Barium 0.50 mg/L0.010 TCLP6010B10.71
Lead 0.0075 mg/L0.0050 TCLP6010B10.0060 J
Mercury 0.00020 mg/L0.000020 TCLP7470A10.000020 J *
☼Mercury 0.021 mg/Kg0.0080 Total/NA7471A10.042
pH 0.200 SU0.200 Total/NA9045C17.53
Client Sample ID: J8 (6-12") Lab Sample ID: 500-52298-14
☼Arsenic
RL
1.3 mg/Kg
MDL
0.29
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B Total/NA15.4
☼Barium 1.3 mg/Kg0.16 Total/NA6010B1120
☼Cadmium 0.26 mg/Kg0.065 Total/NA6010B10.44
☼Chromium 1.3 mg/Kg0.22 Total/NA6010B118
☼Copper 1.3 mg/Kg0.36 Total/NA6010B119
☼Lead 0.66 mg/Kg0.23 Total/NA6010B127
☼Selenium 1.3 mg/Kg0.38 Total/NA6010B10.50 J
☼Zinc 2.6 mg/Kg0.90 Total/NA6010B198
Arsenic 0.050 mg/L0.010 TCLP6010B10.012 J
Barium 0.50 mg/L0.010 TCLP6010B10.40 J
Lead 0.0075 mg/L0.0050 TCLP6010B10.012
Mercury 0.00020 mg/L0.000020 TCLP7470A10.000043 J *
☼Mercury 0.022 mg/Kg0.0084 Total/NA7471A10.051
pH 0.200 SU0.200 Total/NA9045C17.68
Client Sample ID: J8 (12-18") Lab Sample ID: 500-52298-15
☼Arsenic
RL
1.2 mg/Kg
MDL
0.26
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B Total/NA15.5
☼Barium 1.2 mg/Kg0.14 Total/NA6010B1110
☼Cadmium 0.24 mg/Kg0.060 Total/NA6010B10.22 J
☼Chromium 1.2 mg/Kg0.20 Total/NA6010B118
☼Copper 1.2 mg/Kg0.33 Total/NA6010B123
☼Lead 0.60 mg/Kg0.21 Total/NA6010B123
☼Selenium 1.2 mg/Kg0.35 Total/NA6010B10.47 J
☼Zinc 2.4 mg/Kg0.83 Total/NA6010B166
Arsenic 0.050 mg/L0.010 TCLP6010B10.011 J
Barium 0.50 mg/L0.010 TCLP6010B10.43 J
Lead 0.0075 mg/L0.0050 TCLP6010B10.0073 J
Mercury 0.00020 mg/L0.000020 TCLP7470A10.000026 J *
☼Mercury 0.020 mg/Kg0.0077 Total/NA7471A10.040
TestAmerica Chicago
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Detection SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Client Sample ID: J8 (12-18") (Continued) Lab Sample ID: 500-52298-15
pH
RL
0.200 SU
MDL
0.200
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
9045C Total/NA17.43
Client Sample ID: L6 (W20') (0-6") Lab Sample ID: 500-52298-16
☼Antimony
RL
2.5 mg/Kg
MDL
0.34
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B Total/NA1J0.45
☼Arsenic 1.3 mg/Kg0.28 Total/NA6010B12.6
☼Barium 1.3 mg/Kg0.15 Total/NA6010B176
☼Cadmium 0.25 mg/Kg0.063 Total/NA6010B10.30
☼Chromium 1.3 mg/Kg0.21 Total/NA6010B113
☼Copper 1.3 mg/Kg0.35 Total/NA6010B116
☼Lead 0.64 mg/Kg0.22 Total/NA6010B112
☼Selenium 1.3 mg/Kg0.37 Total/NA6010B10.41 J
☼Zinc 2.5 mg/Kg0.87 Total/NA6010B152
Barium 0.50 mg/L0.010 TCLP6010B11.3
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0021 J
Lead 0.0075 mg/L0.0050 TCLP6010B10.0093
Mercury 0.00020 mg/L0.000020 TCLP7470A10.000032 J *
☼Mercury 0.021 mg/Kg0.0080 Total/NA7471A10.028
pH 0.200 SU0.200 Total/NA9045C17.14
Client Sample ID: L6 (W20') (6-12") Lab Sample ID: 500-52298-17
☼Antimony
RL
2.3 mg/Kg
MDL
0.31
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B Total/NA1J0.54
☼Arsenic 1.2 mg/Kg0.25 Total/NA6010B14.2
☼Barium 1.2 mg/Kg0.14 Total/NA6010B137
☼Cadmium 0.23 mg/Kg0.057 Total/NA6010B10.37
☼Chromium 1.2 mg/Kg0.19 Total/NA6010B18.0
☼Copper 1.2 mg/Kg0.31 Total/NA6010B128
☼Lead 0.58 mg/Kg0.20 Total/NA6010B115
☼Selenium 1.2 mg/Kg0.33 Total/NA6010B10.82 J
☼Silver 0.58 mg/Kg0.070 Total/NA6010B10.082 J
☼Zinc 2.3 mg/Kg0.79 Total/NA6010B158
Barium 0.50 mg/L0.010 TCLP6010B10.88
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0044 J
Lead 0.0075 mg/L0.0050 TCLP6010B10.0076
Mercury 0.00020 mg/L0.000020 TCLP7470A10.000027 J *
☼Mercury 0.018 mg/Kg0.0069 Total/NA7471A10.023
pH 0.200 SU0.200 Total/NA9045C18.09
Client Sample ID: L6 (W20') (12-18") Lab Sample ID: 500-52298-18
☼Antimony
RL
2.2 mg/Kg
MDL
0.29
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B Total/NA1J0.79
☼Arsenic 1.1 mg/Kg0.24 Total/NA6010B11.8
☼Barium 1.1 mg/Kg0.13 Total/NA6010B178
☼Cadmium 0.22 mg/Kg0.055 Total/NA6010B10.26
☼Chromium 1.1 mg/Kg0.18 Total/NA6010B114
☼Copper 1.1 mg/Kg0.30 Total/NA6010B119
☼Lead 0.55 mg/Kg0.19 Total/NA6010B115
☼Zinc 2.2 mg/Kg0.76 Total/NA6010B154
TestAmerica Chicago
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Detection SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Client Sample ID: L6 (W20') (12-18") (Continued) Lab Sample ID: 500-52298-18
Barium
RL
0.50 mg/L
MDL
0.010
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B TCLP11.1
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0022 J
Lead 0.0075 mg/L0.0050 TCLP6010B10.0066 J
Mercury 0.00020 mg/L0.000020 TCLP7470A10.000024 J *
☼Mercury 0.019 mg/Kg0.0074 Total/NA7471A10.016 J
pH 0.200 SU0.200 Total/NA9045C18.11
Client Sample ID: J17 (N30;W20') (0-6") Lab Sample ID: 500-52298-19
☼Benzo[a]anthracene
RL
0.37 mg/Kg
MDL
0.078
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA50.46
☼Benzo[a]pyrene 0.37 mg/Kg0.068 Total/NA8270C50.65
☼Benzo[b]fluoranthene 0.37 mg/Kg0.073 Total/NA8270C50.82
☼Benzo[g,h,i]perylene 0.37 mg/Kg0.13 Total/NA8270C50.61
☼Benzo[k]fluoranthene 0.37 mg/Kg0.089 Total/NA8270C50.41
☼Chrysene 0.37 mg/Kg0.084 Total/NA8270C50.63
☼Fluoranthene 0.37 mg/Kg0.15 Total/NA8270C50.60
☼Indeno[1,2,3-cd]pyrene 0.37 mg/Kg0.13 Total/NA8270C50.50
☼Pyrene 0.37 mg/Kg0.14 Total/NA8270C50.62
☼Antimony 4.3 mg/Kg0.57 Total/NA6010B111
☼Arsenic 2.2 mg/Kg0.47 Total/NA6010B115
☼Barium 2.2 mg/Kg0.26 Total/NA6010B154
☼Cadmium 0.43 mg/Kg0.11 Total/NA6010B10.47
☼Chromium 2.2 mg/Kg0.36 Total/NA6010B111
☼Copper 2.2 mg/Kg0.59 Total/NA6010B125
☼Lead 1.1 mg/Kg0.37 Total/NA6010B12600
☼Zinc 4.3 mg/Kg1.5 Total/NA6010B171
Arsenic 0.050 mg/L0.010 TCLP6010B10.026 J
Barium 0.50 mg/L0.010 TCLP6010B10.46 J
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0048 J
Lead 0.0075 mg/L0.0050 TCLP6010B10.12
Mercury 0.00020 mg/L0.000020 TCLP7470A10.000023 J *
☼Mercury 0.037 mg/Kg0.014 Total/NA7471A10.058
pH 0.200 SU0.200 Total/NA9045C17.70
Client Sample ID: J17 (N30;W20') (6-12") Lab Sample ID: 500-52298-20
☼Anthracene
RL
0.093 mg/Kg
MDL
0.022
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J0.050
☼Benzo[a]anthracene 0.093 mg/Kg0.020 Total/NA8270C10.71
☼Benzo[a]pyrene 0.093 mg/Kg0.017 Total/NA8270C10.93
☼Benzo[b]fluoranthene 0.093 mg/Kg0.018 Total/NA8270C11.2
☼Benzo[g,h,i]perylene 0.093 mg/Kg0.032 Total/NA8270C10.77
☼Benzo[k]fluoranthene 0.093 mg/Kg0.022 Total/NA8270C10.66
☼Chrysene 0.093 mg/Kg0.021 Total/NA8270C10.90
☼Dibenz(a,h)anthracene 0.093 mg/Kg0.026 Total/NA8270C10.30
☼Fluoranthene 0.093 mg/Kg0.038 Total/NA8270C11.1
☼Fluorene 0.093 mg/Kg0.021 Total/NA8270C10.031 J
☼Indeno[1,2,3-cd]pyrene 0.093 mg/Kg0.032 Total/NA8270C10.64
☼Phenanthrene 0.093 mg/Kg0.039 Total/NA8270C10.45
☼Pyrene 0.093 mg/Kg0.034 Total/NA8270C10.85
☼Antimony 260 mg/Kg35 Total/NA6010B505900
TestAmerica Chicago
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Detection SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Client Sample ID: J17 (N30;W20') (6-12") (Continued) Lab Sample ID: 500-52298-20
☼Arsenic
RL
2.6 mg/Kg
MDL
0.57
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
6010B Total/NA11900
☼Barium 2.6 mg/Kg0.31 Total/NA6010B175
☼Cadmium 0.52 mg/Kg0.13 Total/NA6010B13.0
☼Chromium 2.6 mg/Kg0.44 Total/NA6010B110
☼Copper 2.6 mg/Kg0.71 Total/NA6010B127
☼Lead 66 mg/Kg23 Total/NA6010B50110000
☼Selenium 2.6 mg/Kg0.75 Total/NA6010B11.2 J
☼Silver 1.3 mg/Kg0.16 Total/NA6010B14.2
☼Zinc 5.2 mg/Kg1.8 Total/NA6010B199
Arsenic 0.050 mg/L0.010 TCLP6010B10.047 J
Barium 0.50 mg/L0.010 TCLP6010B10.54
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0043 J
Lead 0.0075 mg/L0.0050 TCLP6010B13.0
Mercury 0.00020 mg/L0.000020 TCLP7470A10.000038 J *
☼Mercury 0.045 mg/Kg0.017 Total/NA7471A10.047
pH 0.200 SU0.200 Total/NA9045C17.30
Client Sample ID: J17 (N30;W20') (12-18") Lab Sample ID: 500-52298-21
☼Benzo[a]anthracene
RL
0.044 mg/Kg
MDL
0.0092
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA10.16
☼Benzo[a]pyrene 0.044 mg/Kg0.0080 Total/NA8270C10.20
☼Benzo[b]fluoranthene 0.044 mg/Kg0.0085 Total/NA8270C10.18
☼Benzo[g,h,i]perylene 0.044 mg/Kg0.015 Total/NA8270C10.16
☼Benzo[k]fluoranthene 0.044 mg/Kg0.010 Total/NA8270C10.23
☼Chrysene 0.044 mg/Kg0.0099 Total/NA8270C10.17
☼Dibenz(a,h)anthracene 0.044 mg/Kg0.012 Total/NA8270C10.063
☼Fluoranthene 0.044 mg/Kg0.018 Total/NA8270C10.21
☼Indeno[1,2,3-cd]pyrene 0.044 mg/Kg0.015 Total/NA8270C10.13
☼Phenanthrene 0.044 mg/Kg0.018 Total/NA8270C10.056
☼Pyrene 0.044 mg/Kg0.016 Total/NA8270C10.15
☼Antimony 2.5 mg/Kg0.34 Total/NA6010B14.9
☼Arsenic 1.3 mg/Kg0.28 Total/NA6010B19.1
☼Barium 1.3 mg/Kg0.15 Total/NA6010B150
☼Cadmium 0.25 mg/Kg0.063 Total/NA6010B10.34
☼Chromium 1.3 mg/Kg0.21 Total/NA6010B112
☼Copper 1.3 mg/Kg0.34 Total/NA6010B120
☼Lead 0.64 mg/Kg0.22 Total/NA6010B1890
☼Selenium 1.3 mg/Kg0.37 Total/NA6010B10.56 J
☼Zinc 2.5 mg/Kg0.87 Total/NA6010B158
Barium 0.50 mg/L0.010 TCLP6010B10.66
Lead 0.0075 mg/L0.0050 TCLP6010B10.66 B
Mercury 0.00020 mg/L0.000020 TCLP7470A10.000026 J B
☼Mercury 0.020 mg/Kg0.0078 Total/NA7471A10.027
pH 0.200 SU0.200 Total/NA9045C17.41
Client Sample ID: K12 (W25') (0-6') Lab Sample ID: 500-52298-22
☼Benzo[a]anthracene
RL
0.060 mg/Kg
MDL
0.013
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J0.038
☼Benzo[a]pyrene 0.060 mg/Kg0.011 Total/NA8270C10.039 J
☼Benzo[b]fluoranthene 0.060 mg/Kg0.012 Total/NA8270C10.064
TestAmerica Chicago
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Detection SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Client Sample ID: K12 (W25') (0-6') (Continued) Lab Sample ID: 500-52298-22
☼Benzo[g,h,i]perylene
RL
0.060 mg/Kg
MDL
0.020
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J0.040
☼Benzo[k]fluoranthene 0.060 mg/Kg0.014 Total/NA8270C10.025 J
☼Chrysene 0.060 mg/Kg0.014 Total/NA8270C10.053 J
☼Dibenz(a,h)anthracene 0.060 mg/Kg0.017 Total/NA8270C10.020 J
☼Fluoranthene 0.060 mg/Kg0.025 Total/NA8270C10.078
☼Indeno[1,2,3-cd]pyrene 0.060 mg/Kg0.020 Total/NA8270C10.031 J
☼Pyrene 0.060 mg/Kg0.022 Total/NA8270C10.058 J
☼Antimony 3.7 mg/Kg0.49 Total/NA6010B127
☼Arsenic 1.9 mg/Kg0.40 Total/NA6010B122
☼Barium 1.9 mg/Kg0.22 Total/NA6010B162
☼Cadmium 0.37 mg/Kg0.092 Total/NA6010B10.37
☼Chromium 1.9 mg/Kg0.31 Total/NA6010B112
☼Copper 1.9 mg/Kg0.50 Total/NA6010B122
☼Lead 0.93 mg/Kg0.32 Total/NA6010B14200
☼Zinc 3.7 mg/Kg1.3 Total/NA6010B162
Arsenic 0.050 mg/L0.010 TCLP6010B10.017 J
Barium 0.50 mg/L0.010 TCLP6010B10.40 J
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0045 J
Lead 0.0075 mg/L0.0050 TCLP6010B10.85 B
☼Mercury 0.031 mg/Kg0.012 Total/NA7471A10.046
pH 0.200 SU0.200 Total/NA9045C17.33
Client Sample ID: K12 (W25') (6-12') Lab Sample ID: 500-52298-23
☼Benzo[a]anthracene
RL
0.060 mg/Kg
MDL
0.013
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA1J0.026
☼Benzo[a]pyrene 0.060 mg/Kg0.011 Total/NA8270C10.079
☼Benzo[b]fluoranthene 0.060 mg/Kg0.012 Total/NA8270C10.027 J
☼Benzo[g,h,i]perylene 0.060 mg/Kg0.020 Total/NA8270C10.027 J
☼Benzo[k]fluoranthene 0.060 mg/Kg0.014 Total/NA8270C10.017 J
☼Chrysene 0.060 mg/Kg0.014 Total/NA8270C10.040 J
☼Fluoranthene 0.060 mg/Kg0.025 Total/NA8270C10.044 J
☼Pyrene 0.060 mg/Kg0.022 Total/NA8270C10.039 J
☼Antimony 3.2 mg/Kg0.42 Total/NA6010B143
☼Arsenic 1.6 mg/Kg0.34 Total/NA6010B132
☼Barium 1.6 mg/Kg0.19 Total/NA6010B187
☼Cadmium 0.32 mg/Kg0.078 Total/NA6010B10.59
☼Chromium 1.6 mg/Kg0.26 Total/NA6010B113
☼Copper 1.6 mg/Kg0.43 Total/NA6010B125
☼Lead 0.79 mg/Kg0.27 Total/NA6010B14600
☼Selenium 1.6 mg/Kg0.45 Total/NA6010B11.1 J
☼Zinc 3.2 mg/Kg1.1 Total/NA6010B182
Arsenic 0.050 mg/L0.010 TCLP6010B10.32
Barium 0.50 mg/L0.010 TCLP6010B10.60
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0055
Lead 0.075 mg/L0.050 TCLP6010B1073 B
Mercury 0.00020 mg/L0.000020 TCLP7470A10.000034 J B
☼Mercury 0.028 mg/Kg0.011 Total/NA7471A10.042
pH 0.200 SU0.200 Total/NA9045C17.44
Client Sample ID: K12 (W25') (12-18') Lab Sample ID: 500-52298-24
TestAmerica Chicago
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Detection SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Client Sample ID: K12 (W25') (12-18') (Continued) Lab Sample ID: 500-52298-24
☼Benzo[b]fluoranthene
RL
0.24 mg/Kg
MDL
0.048
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
8270C Total/NA5J0.088
☼Chrysene 0.24 mg/Kg0.055 Total/NA8270C50.11 J
☼Fluoranthene 0.24 mg/Kg0.10 Total/NA8270C50.19 J
☼Pyrene 0.24 mg/Kg0.089 Total/NA8270C50.16 J
☼Antimony 2.6 mg/Kg0.35 Total/NA6010B12.4 J
☼Arsenic 1.3 mg/Kg0.29 Total/NA6010B18.0
☼Barium 1.3 mg/Kg0.16 Total/NA6010B182
☼Cadmium 0.26 mg/Kg0.065 Total/NA6010B10.35
☼Chromium 1.3 mg/Kg0.22 Total/NA6010B115
☼Copper 1.3 mg/Kg0.36 Total/NA6010B121
☼Lead 0.66 mg/Kg0.23 Total/NA6010B1530
☼Selenium 1.3 mg/Kg0.38 Total/NA6010B10.57 J
☼Zinc 2.6 mg/Kg0.91 Total/NA6010B166
Arsenic 0.050 mg/L0.010 TCLP6010B10.050
Barium 0.50 mg/L0.010 TCLP6010B10.84
Cadmium 0.0050 mg/L0.0020 TCLP6010B10.0042 J
Lead 0.0075 mg/L0.0050 TCLP6010B18.6 B
☼Mercury 0.022 mg/Kg0.0086 Total/NA7471A10.037
pH 0.200 SU0.200 Total/NA9045C17.45
TestAmerica Chicago
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Method SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Method Method Description LaboratoryProtocol
SW8468270C Semivolatile Organic Compounds (GC/MS) TAL CHI
SW8466010B Metals (ICP) TAL CHI
SW8467470A Mercury (CVAA) TAL CHI
SW8467471A Mercury (CVAA) TAL CHI
SW8469045C pH TAL CHI
EPAMoisture Percent Moisture TAL CHI
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200
TestAmerica Chicago
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Sample SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
500-52298-1 F20 (0-6") Solid 11/09/12 13:15 11/13/12 13:30
500-52298-2 F20 (6-12") Solid 11/09/12 13:16 11/13/12 13:30
500-52298-3 F20 (12-18") Solid 11/09/12 13:17 11/13/12 13:30
500-52298-4 H20 (E20') (0-6") Solid 11/09/12 12:25 11/13/12 13:30
500-52298-5 H20 (E20') (6-12") Solid 11/09/12 12:26 11/13/12 13:30
500-52298-6 H20 (E20') (12-18") Solid 11/09/12 12:27 11/13/12 13:30
500-52298-7 K10 (W25') (0-6") Solid 11/09/12 11:50 11/13/12 13:30
500-52298-8 K10 (W25') (6-12") Solid 11/09/12 11:51 11/13/12 13:30
500-52298-9 K10 (W25') (12-18") Solid 11/09/12 11:52 11/13/12 13:30
500-52298-10 H10 (N30') (0-6") Solid 11/08/12 11:45 11/13/12 13:30
500-52298-11 H10 (N30') (6-12") Solid 11/08/12 11:46 11/13/12 13:30
500-52298-12 H10 (N30') (12-18") Solid 11/08/12 11:47 11/13/12 13:30
500-52298-13 J8 (0-6") Solid 11/08/12 12:00 11/13/12 13:30
500-52298-14 J8 (6-12") Solid 11/08/12 12:01 11/13/12 13:30
500-52298-15 J8 (12-18") Solid 11/08/12 12:02 11/13/12 13:30
500-52298-16 L6 (W20') (0-6") Solid 11/08/12 13:20 11/13/12 13:30
500-52298-17 L6 (W20') (6-12") Solid 11/08/12 13:21 11/13/12 13:30
500-52298-18 L6 (W20') (12-18") Solid 11/08/12 13:22 11/13/12 13:30
500-52298-19 J17 (N30;W20') (0-6") Solid 11/08/12 14:40 11/13/12 13:30
500-52298-20 J17 (N30;W20') (6-12") Solid 11/08/12 14:41 11/13/12 13:30
500-52298-21 J17 (N30;W20') (12-18") Solid 11/08/12 14:42 11/13/12 13:30
500-52298-22 K12 (W25') (0-6') Solid 11/08/12 13:55 11/13/12 13:30
500-52298-23 K12 (W25') (6-12') Solid 11/08/12 13:56 11/13/12 13:30
500-52298-24 K12 (W25') (12-18') Solid 11/08/12 13:57 11/13/12 13:30
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-1Client Sample ID: F20 (0-6")Matrix: SolidDate Collected: 11/09/12 13:15
Percent Solids: 59.3Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.053 0.053 0.016 mg/Kg ☼ 11/20/12 16:54 11/24/12 17:55 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.053 0.012 mg/Kg 11/20/12 16:54 11/24/12 17:55 1☼Acenaphthylene <0.053
0.053 0.012 mg/Kg 11/20/12 16:54 11/24/12 17:55 1☼Anthracene <0.053
0.053 0.011 mg/Kg 11/20/12 16:54 11/24/12 17:55 1☼Benzo[a]anthracene 0.045 J
0.053 0.0096 mg/Kg 11/20/12 16:54 11/24/12 17:55 1☼Benzo[a]pyrene 0.050 J
0.053 0.010 mg/Kg 11/20/12 16:54 11/24/12 17:55 1☼Benzo[b]fluoranthene 0.078
0.053 0.018 mg/Kg 11/20/12 16:54 11/24/12 17:55 1☼Benzo[g,h,i]perylene 0.046 J
0.053 0.013 mg/Kg 11/20/12 16:54 11/24/12 17:55 1☼Benzo[k]fluoranthene 0.044 J
0.053 0.012 mg/Kg 11/20/12 16:54 11/24/12 17:55 1☼Chrysene 0.082
0.053 0.015 mg/Kg 11/20/12 16:54 11/24/12 17:55 1☼Dibenz(a,h)anthracene <0.053
0.053 0.022 mg/Kg 11/20/12 16:54 11/24/12 17:55 1☼Fluoranthene 0.11
0.053 0.012 mg/Kg 11/20/12 16:54 11/24/12 17:55 1☼Fluorene <0.053
0.053 0.018 mg/Kg 11/20/12 16:54 11/24/12 17:55 1☼Indeno[1,2,3-cd]pyrene 0.032 J
0.053 0.010 mg/Kg 11/20/12 16:54 11/24/12 17:55 1☼Naphthalene <0.053
0.053 0.022 mg/Kg 11/20/12 16:54 11/24/12 17:55 1☼Phenanthrene 0.035 J
0.053 0.019 mg/Kg 11/20/12 16:54 11/24/12 17:55 1☼Pyrene 0.12
2-Fluorobiphenyl 59 30 - 119 11/20/12 16:54 11/24/12 17:55 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 47 11/20/12 16:54 11/24/12 17:55 130 - 115
Terphenyl-d14 72 11/20/12 16:54 11/24/12 17:55 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 0.75 J 3.3 0.43 mg/Kg ☼ 11/13/12 16:30 11/19/12 22:26 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.6 0.36 mg/Kg 11/13/12 16:30 11/19/12 22:26 1☼Arsenic 5.1
1.6 0.19 mg/Kg 11/13/12 16:30 11/19/12 22:26 1☼Barium 55
0.33 0.081 mg/Kg 11/13/12 16:30 11/19/12 22:26 1☼Cadmium 0.44
1.6 0.27 mg/Kg 11/13/12 16:30 11/19/12 22:26 1☼Chromium 9.4
1.6 0.44 mg/Kg 11/13/12 16:30 11/19/12 22:26 1☼Copper 18
0.82 0.28 mg/Kg 11/13/12 16:30 11/19/12 22:26 1☼Lead 34
1.6 0.47 mg/Kg 11/13/12 16:30 11/19/12 22:26 1☼Selenium 0.79 J
0.82 0.098 mg/Kg 11/13/12 16:30 11/19/12 22:26 1☼Silver <0.82
3.3 1.1 mg/Kg 11/13/12 16:30 11/19/12 22:26 1☼Zinc 59
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 21:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/19/12 21:49 1Barium 0.45 J
0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 21:49 1Cadmium <0.0050
0.025 0.010 mg/L 11/19/12 08:00 11/19/12 21:49 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 21:49 1Lead 0.014
0.050 0.010 mg/L 11/19/12 08:00 11/19/12 21:49 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 21:49 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury <0.00020 * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:37 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-1Client Sample ID: F20 (0-6")Matrix: SolidDate Collected: 11/09/12 13:15
Percent Solids: 59.3Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.031 0.025 0.0096 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:10 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.82 0.200 0.200 SU 11/15/12 09:24 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-2Client Sample ID: F20 (6-12")Matrix: SolidDate Collected: 11/09/12 13:16
Percent Solids: 78.7Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.041 0.041 0.012 mg/Kg ☼ 11/20/12 16:54 11/24/12 18:15 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.041 0.0094 mg/Kg 11/20/12 16:54 11/24/12 18:15 1☼Acenaphthylene <0.041
0.041 0.0096 mg/Kg 11/20/12 16:54 11/24/12 18:15 1☼Anthracene <0.041
0.041 0.0086 mg/Kg 11/20/12 16:54 11/24/12 18:15 1☼Benzo[a]anthracene <0.041
0.041 0.0074 mg/Kg 11/20/12 16:54 11/24/12 18:15 1☼Benzo[a]pyrene <0.041
0.041 0.0079 mg/Kg 11/20/12 16:54 11/24/12 18:15 1☼Benzo[b]fluoranthene <0.041
0.041 0.014 mg/Kg 11/20/12 16:54 11/24/12 18:15 1☼Benzo[g,h,i]perylene <0.041
0.041 0.0098 mg/Kg 11/20/12 16:54 11/24/12 18:15 1☼Benzo[k]fluoranthene <0.041
0.041 0.0092 mg/Kg 11/20/12 16:54 11/24/12 18:15 1☼Chrysene 0.012 J
0.041 0.011 mg/Kg 11/20/12 16:54 11/24/12 18:15 1☼Dibenz(a,h)anthracene <0.041
0.041 0.017 mg/Kg 11/20/12 16:54 11/24/12 18:15 1☼Fluoranthene <0.041
0.041 0.0093 mg/Kg 11/20/12 16:54 11/24/12 18:15 1☼Fluorene <0.041
0.041 0.014 mg/Kg 11/20/12 16:54 11/24/12 18:15 1☼Indeno[1,2,3-cd]pyrene <0.041
0.041 0.0079 mg/Kg 11/20/12 16:54 11/24/12 18:15 1☼Naphthalene <0.041
0.041 0.017 mg/Kg 11/20/12 16:54 11/24/12 18:15 1☼Phenanthrene <0.041
0.041 0.015 mg/Kg 11/20/12 16:54 11/24/12 18:15 1☼Pyrene <0.041
2-Fluorobiphenyl 55 30 - 119 11/20/12 16:54 11/24/12 18:15 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 48 11/20/12 16:54 11/24/12 18:15 130 - 115
Terphenyl-d14 54 11/20/12 16:54 11/24/12 18:15 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 0.75 J 2.2 0.29 mg/Kg ☼ 11/13/12 16:30 11/19/12 22:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.1 0.24 mg/Kg 11/13/12 16:30 11/19/12 22:48 1☼Arsenic 4.7
1.1 0.13 mg/Kg 11/13/12 16:30 11/19/12 22:48 1☼Barium 32
0.22 0.055 mg/Kg 11/13/12 16:30 11/19/12 22:48 1☼Cadmium 0.27
1.1 0.18 mg/Kg 11/13/12 16:30 11/19/12 22:48 1☼Chromium 7.5
1.1 0.30 mg/Kg 11/13/12 16:30 11/19/12 22:48 1☼Copper 13
0.55 0.19 mg/Kg 11/13/12 16:30 11/19/12 22:48 1☼Lead 15
1.1 0.32 mg/Kg 11/13/12 16:30 11/19/12 22:48 1☼Selenium <1.1
0.55 0.067 mg/Kg 11/13/12 16:30 11/19/12 22:48 1☼Silver <0.55
2.2 0.76 mg/Kg 11/13/12 16:30 11/19/12 22:48 1☼Zinc 37
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 21:55 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/19/12 21:55 1Barium 0.64
0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 21:55 1Cadmium 0.0024 J
0.025 0.010 mg/L 11/19/12 08:00 11/19/12 21:55 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 21:55 1Lead 0.0077
0.050 0.010 mg/L 11/19/12 08:00 11/19/12 21:55 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 21:55 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury <0.00020 * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-2Client Sample ID: F20 (6-12")Matrix: SolidDate Collected: 11/09/12 13:16
Percent Solids: 78.7Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.030 0.020 0.0076 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:12 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.95 0.200 0.200 SU 11/15/12 09:27 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-3Client Sample ID: F20 (12-18")Matrix: SolidDate Collected: 11/09/12 13:17
Percent Solids: 80.8Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.040 0.040 0.012 mg/Kg ☼ 11/20/12 16:54 11/24/12 18:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.040 0.0093 mg/Kg 11/20/12 16:54 11/24/12 18:34 1☼Acenaphthylene <0.040
0.040 0.0095 mg/Kg 11/20/12 16:54 11/24/12 18:34 1☼Anthracene <0.040
0.040 0.0085 mg/Kg 11/20/12 16:54 11/24/12 18:34 1☼Benzo[a]anthracene <0.040
0.040 0.0074 mg/Kg 11/20/12 16:54 11/24/12 18:34 1☼Benzo[a]pyrene <0.040
0.040 0.0079 mg/Kg 11/20/12 16:54 11/24/12 18:34 1☼Benzo[b]fluoranthene <0.040
0.040 0.014 mg/Kg 11/20/12 16:54 11/24/12 18:34 1☼Benzo[g,h,i]perylene <0.040
0.040 0.0096 mg/Kg 11/20/12 16:54 11/24/12 18:34 1☼Benzo[k]fluoranthene <0.040
0.040 0.0091 mg/Kg 11/20/12 16:54 11/24/12 18:34 1☼Chrysene <0.040
0.040 0.011 mg/Kg 11/20/12 16:54 11/24/12 18:34 1☼Dibenz(a,h)anthracene <0.040
0.040 0.017 mg/Kg 11/20/12 16:54 11/24/12 18:34 1☼Fluoranthene <0.040
0.040 0.0092 mg/Kg 11/20/12 16:54 11/24/12 18:34 1☼Fluorene <0.040
0.040 0.014 mg/Kg 11/20/12 16:54 11/24/12 18:34 1☼Indeno[1,2,3-cd]pyrene <0.040
0.040 0.0078 mg/Kg 11/20/12 16:54 11/24/12 18:34 1☼Naphthalene <0.040
0.040 0.017 mg/Kg 11/20/12 16:54 11/24/12 18:34 1☼Phenanthrene <0.040
0.040 0.015 mg/Kg 11/20/12 16:54 11/24/12 18:34 1☼Pyrene <0.040
2-Fluorobiphenyl 65 30 - 119 11/20/12 16:54 11/24/12 18:34 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 60 11/20/12 16:54 11/24/12 18:34 130 - 115
Terphenyl-d14 60 11/20/12 16:54 11/24/12 18:34 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 0.79 J 2.4 0.32 mg/Kg ☼ 11/13/12 16:30 11/19/12 22:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.2 0.26 mg/Kg 11/13/12 16:30 11/19/12 22:53 1☼Arsenic 12
1.2 0.14 mg/Kg 11/13/12 16:30 11/19/12 22:53 1☼Barium 44
0.24 0.060 mg/Kg 11/13/12 16:30 11/19/12 22:53 1☼Cadmium 0.29
1.2 0.20 mg/Kg 11/13/12 16:30 11/19/12 22:53 1☼Chromium 12
1.2 0.33 mg/Kg 11/13/12 16:30 11/19/12 22:53 1☼Copper 29
0.60 0.21 mg/Kg 11/13/12 16:30 11/19/12 22:53 1☼Lead 18
1.2 0.35 mg/Kg 11/13/12 16:30 11/19/12 22:53 1☼Selenium 0.48 J
0.60 0.072 mg/Kg 11/13/12 16:30 11/19/12 22:53 1☼Silver <0.60
2.4 0.83 mg/Kg 11/13/12 16:30 11/19/12 22:53 1☼Zinc 51
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 22:02 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/19/12 22:02 1Barium 0.73
0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 22:02 1Cadmium 0.0021 J
0.025 0.010 mg/L 11/19/12 08:00 11/19/12 22:02 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 22:02 1Lead <0.0075
0.050 0.010 mg/L 11/19/12 08:00 11/19/12 22:02 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 22:02 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury 0.000022 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-3Client Sample ID: F20 (12-18")Matrix: SolidDate Collected: 11/09/12 13:17
Percent Solids: 80.8Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.029 0.019 0.0073 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.84 0.200 0.200 SU 11/15/12 09:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-4Client Sample ID: H20 (E20') (0-6")Matrix: SolidDate Collected: 11/09/12 12:25
Percent Solids: 33.5Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.096 0.096 0.029 mg/Kg ☼ 11/20/12 16:54 11/24/12 18:54 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.096 0.022 mg/Kg 11/20/12 16:54 11/24/12 18:54 1☼Acenaphthylene <0.096
0.096 0.023 mg/Kg 11/20/12 16:54 11/24/12 18:54 1☼Anthracene <0.096
0.096 0.020 mg/Kg 11/20/12 16:54 11/24/12 18:54 1☼Benzo[a]anthracene 0.039 J
0.096 0.018 mg/Kg 11/20/12 16:54 11/24/12 18:54 1☼Benzo[a]pyrene 0.049 J
0.096 0.019 mg/Kg 11/20/12 16:54 11/24/12 18:54 1☼Benzo[b]fluoranthene 0.076 J
0.096 0.032 mg/Kg 11/20/12 16:54 11/24/12 18:54 1☼Benzo[g,h,i]perylene 0.058 J
0.096 0.023 mg/Kg 11/20/12 16:54 11/24/12 18:54 1☼Benzo[k]fluoranthene <0.096
0.096 0.022 mg/Kg 11/20/12 16:54 11/24/12 18:54 1☼Chrysene 0.052 J
0.096 0.027 mg/Kg 11/20/12 16:54 11/24/12 18:54 1☼Dibenz(a,h)anthracene <0.096
0.096 0.039 mg/Kg 11/20/12 16:54 11/24/12 18:54 1☼Fluoranthene <0.096
0.096 0.022 mg/Kg 11/20/12 16:54 11/24/12 18:54 1☼Fluorene <0.096
0.096 0.032 mg/Kg 11/20/12 16:54 11/24/12 18:54 1☼Indeno[1,2,3-cd]pyrene 0.041 J
0.096 0.019 mg/Kg 11/20/12 16:54 11/24/12 18:54 1☼Naphthalene <0.096
0.096 0.040 mg/Kg 11/20/12 16:54 11/24/12 18:54 1☼Phenanthrene <0.096
0.096 0.035 mg/Kg 11/20/12 16:54 11/24/12 18:54 1☼Pyrene 0.048 J
2-Fluorobiphenyl 38 30 - 119 11/20/12 16:54 11/24/12 18:54 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 30 11/20/12 16:54 11/24/12 18:54 130 - 115
Terphenyl-d14 38 11/20/12 16:54 11/24/12 18:54 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 2.8 J 5.9 0.78 mg/Kg ☼ 11/13/12 16:30 11/19/12 22:58 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.9 0.64 mg/Kg 11/13/12 16:30 11/19/12 22:58 1☼Arsenic 7.1
2.9 0.35 mg/Kg 11/13/12 16:30 11/19/12 22:58 1☼Barium 81
0.59 0.15 mg/Kg 11/13/12 16:30 11/19/12 22:58 1☼Cadmium 0.62
2.9 0.49 mg/Kg 11/13/12 16:30 11/19/12 22:58 1☼Chromium 12
2.9 0.80 mg/Kg 11/13/12 16:30 11/19/12 22:58 1☼Copper 22
1.5 0.51 mg/Kg 11/13/12 16:30 11/19/12 22:58 1☼Lead 110
2.9 0.85 mg/Kg 11/13/12 16:30 11/19/12 22:58 1☼Selenium <2.9
1.5 0.18 mg/Kg 11/13/12 16:30 11/19/12 22:58 1☼Silver <1.5
5.9 2.0 mg/Kg 11/13/12 16:30 11/19/12 22:58 1☼Zinc 64
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 22:08 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/19/12 22:08 1Barium 0.49 J
0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 22:08 1Cadmium <0.0050
0.025 0.010 mg/L 11/19/12 08:00 11/19/12 22:08 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 22:08 1Lead 0.051
0.050 0.010 mg/L 11/19/12 08:00 11/19/12 22:08 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 22:08 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury 0.000025 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:50 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-4Client Sample ID: H20 (E20') (0-6")Matrix: SolidDate Collected: 11/09/12 12:25
Percent Solids: 33.5Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.034 J 0.046 0.017 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:26 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.71 0.200 0.200 SU 11/15/12 09:32 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-5Client Sample ID: H20 (E20') (6-12")Matrix: SolidDate Collected: 11/09/12 12:26
Percent Solids: 78.9Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.040 0.040 0.012 mg/Kg ☼ 11/20/12 16:54 11/24/12 19:14 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.040 0.0093 mg/Kg 11/20/12 16:54 11/24/12 19:14 1☼Acenaphthylene <0.040
0.040 0.0096 mg/Kg 11/20/12 16:54 11/24/12 19:14 1☼Anthracene <0.040
0.040 0.0085 mg/Kg 11/20/12 16:54 11/24/12 19:14 1☼Benzo[a]anthracene <0.040
0.040 0.0074 mg/Kg 11/20/12 16:54 11/24/12 19:14 1☼Benzo[a]pyrene <0.040
0.040 0.0079 mg/Kg 11/20/12 16:54 11/24/12 19:14 1☼Benzo[b]fluoranthene <0.040
0.040 0.014 mg/Kg 11/20/12 16:54 11/24/12 19:14 1☼Benzo[g,h,i]perylene <0.040
0.040 0.0097 mg/Kg 11/20/12 16:54 11/24/12 19:14 1☼Benzo[k]fluoranthene <0.040
0.040 0.0092 mg/Kg 11/20/12 16:54 11/24/12 19:14 1☼Chrysene <0.040
0.040 0.011 mg/Kg 11/20/12 16:54 11/24/12 19:14 1☼Dibenz(a,h)anthracene <0.040
0.040 0.017 mg/Kg 11/20/12 16:54 11/24/12 19:14 1☼Fluoranthene <0.040
0.040 0.0093 mg/Kg 11/20/12 16:54 11/24/12 19:14 1☼Fluorene <0.040
0.040 0.014 mg/Kg 11/20/12 16:54 11/24/12 19:14 1☼Indeno[1,2,3-cd]pyrene <0.040
0.040 0.0078 mg/Kg 11/20/12 16:54 11/24/12 19:14 1☼Naphthalene <0.040
0.040 0.017 mg/Kg 11/20/12 16:54 11/24/12 19:14 1☼Phenanthrene <0.040
0.040 0.015 mg/Kg 11/20/12 16:54 11/24/12 19:14 1☼Pyrene <0.040
2-Fluorobiphenyl 61 30 - 119 11/20/12 16:54 11/24/12 19:14 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 56 11/20/12 16:54 11/24/12 19:14 130 - 115
Terphenyl-d14 58 11/20/12 16:54 11/24/12 19:14 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 0.68 J 2.2 0.29 mg/Kg ☼ 11/13/12 16:30 11/19/12 23:12 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.1 0.24 mg/Kg 11/13/12 16:30 11/19/12 23:12 1☼Arsenic 8.6
1.1 0.13 mg/Kg 11/13/12 16:30 11/19/12 23:12 1☼Barium 55
0.22 0.054 mg/Kg 11/13/12 16:30 11/19/12 23:12 1☼Cadmium 0.23
1.1 0.18 mg/Kg 11/13/12 16:30 11/19/12 23:12 1☼Chromium 15
1.1 0.29 mg/Kg 11/13/12 16:30 11/19/12 23:12 1☼Copper 25
0.54 0.19 mg/Kg 11/13/12 16:30 11/19/12 23:12 1☼Lead 16
1.1 0.31 mg/Kg 11/13/12 16:30 11/19/12 23:12 1☼Selenium <1.1
0.54 0.065 mg/Kg 11/13/12 16:30 11/19/12 23:12 1☼Silver <0.54
2.2 0.74 mg/Kg 11/13/12 16:30 11/19/12 23:12 1☼Zinc 59
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 22:39 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/19/12 22:39 1Barium 0.82
0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 22:39 1Cadmium <0.0050
0.025 0.010 mg/L 11/19/12 08:00 11/19/12 22:39 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 22:39 1Lead <0.0075
0.050 0.010 mg/L 11/19/12 08:00 11/19/12 22:39 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 22:39 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury 0.000041 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:51 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-5Client Sample ID: H20 (E20') (6-12")Matrix: SolidDate Collected: 11/09/12 12:26
Percent Solids: 78.9Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.020 0.019 0.0074 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:28 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.95 0.200 0.200 SU 11/15/12 09:35 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-6Client Sample ID: H20 (E20') (12-18")Matrix: SolidDate Collected: 11/09/12 12:27
Percent Solids: 78.0Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.041 0.041 0.012 mg/Kg ☼ 11/20/12 16:54 11/24/12 19:33 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.041 0.0094 mg/Kg 11/20/12 16:54 11/24/12 19:33 1☼Acenaphthylene <0.041
0.041 0.0096 mg/Kg 11/20/12 16:54 11/24/12 19:33 1☼Anthracene <0.041
0.041 0.0086 mg/Kg 11/20/12 16:54 11/24/12 19:33 1☼Benzo[a]anthracene <0.041
0.041 0.0074 mg/Kg 11/20/12 16:54 11/24/12 19:33 1☼Benzo[a]pyrene <0.041
0.041 0.0079 mg/Kg 11/20/12 16:54 11/24/12 19:33 1☼Benzo[b]fluoranthene <0.041
0.041 0.014 mg/Kg 11/20/12 16:54 11/24/12 19:33 1☼Benzo[g,h,i]perylene <0.041
0.041 0.0098 mg/Kg 11/20/12 16:54 11/24/12 19:33 1☼Benzo[k]fluoranthene <0.041
0.041 0.0092 mg/Kg 11/20/12 16:54 11/24/12 19:33 1☼Chrysene <0.041
0.041 0.011 mg/Kg 11/20/12 16:54 11/24/12 19:33 1☼Dibenz(a,h)anthracene <0.041
0.041 0.017 mg/Kg 11/20/12 16:54 11/24/12 19:33 1☼Fluoranthene <0.041
0.041 0.0093 mg/Kg 11/20/12 16:54 11/24/12 19:33 1☼Fluorene <0.041
0.041 0.014 mg/Kg 11/20/12 16:54 11/24/12 19:33 1☼Indeno[1,2,3-cd]pyrene <0.041
0.041 0.0079 mg/Kg 11/20/12 16:54 11/24/12 19:33 1☼Naphthalene <0.041
0.041 0.017 mg/Kg 11/20/12 16:54 11/24/12 19:33 1☼Phenanthrene <0.041
0.041 0.015 mg/Kg 11/20/12 16:54 11/24/12 19:33 1☼Pyrene <0.041
2-Fluorobiphenyl 65 30 - 119 11/20/12 16:54 11/24/12 19:33 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 58 11/20/12 16:54 11/24/12 19:33 130 - 115
Terphenyl-d14 67 11/20/12 16:54 11/24/12 19:33 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 0.57 J 2.4 0.32 mg/Kg ☼ 11/13/12 16:30 11/19/12 23:17 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.2 0.26 mg/Kg 11/13/12 16:30 11/19/12 23:17 1☼Arsenic 17
1.2 0.14 mg/Kg 11/13/12 16:30 11/19/12 23:17 1☼Barium 60
0.24 0.059 mg/Kg 11/13/12 16:30 11/19/12 23:17 1☼Cadmium 0.19 J
1.2 0.20 mg/Kg 11/13/12 16:30 11/19/12 23:17 1☼Chromium 15
1.2 0.32 mg/Kg 11/13/12 16:30 11/19/12 23:17 1☼Copper 24
0.60 0.21 mg/Kg 11/13/12 16:30 11/19/12 23:17 1☼Lead 15
1.2 0.34 mg/Kg 11/13/12 16:30 11/19/12 23:17 1☼Selenium <1.2
0.60 0.072 mg/Kg 11/13/12 16:30 11/19/12 23:17 1☼Silver <0.60
2.4 0.82 mg/Kg 11/13/12 16:30 11/19/12 23:17 1☼Zinc 52
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 22:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/19/12 22:45 1Barium 0.71
0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 22:45 1Cadmium <0.0050
0.025 0.010 mg/L 11/19/12 08:00 11/19/12 22:45 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 22:45 1Lead <0.0075
0.050 0.010 mg/L 11/19/12 08:00 11/19/12 22:45 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 22:45 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury 0.000022 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-6Client Sample ID: H20 (E20') (12-18")Matrix: SolidDate Collected: 11/09/12 12:27
Percent Solids: 78.0Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.037 0.020 0.0076 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.96 0.200 0.200 SU 11/15/12 09:37 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-7Client Sample ID: K10 (W25') (0-6")Matrix: SolidDate Collected: 11/09/12 11:50
Percent Solids: 33.1Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.095 0.095 0.029 mg/Kg ☼ 11/20/12 16:54 11/24/12 19:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.095 0.022 mg/Kg 11/20/12 16:54 11/24/12 19:53 1☼Acenaphthylene <0.095
0.095 0.022 mg/Kg 11/20/12 16:54 11/24/12 19:53 1☼Anthracene <0.095
0.095 0.020 mg/Kg 11/20/12 16:54 11/24/12 19:53 1☼Benzo[a]anthracene 0.098
0.095 0.017 mg/Kg 11/20/12 16:54 11/24/12 19:53 1☼Benzo[a]pyrene 0.13
0.095 0.019 mg/Kg 11/20/12 16:54 11/24/12 19:53 1☼Benzo[b]fluoranthene 0.16
0.095 0.032 mg/Kg 11/20/12 16:54 11/24/12 19:53 1☼Benzo[g,h,i]perylene 0.12
0.095 0.023 mg/Kg 11/20/12 16:54 11/24/12 19:53 1☼Benzo[k]fluoranthene 0.12
0.095 0.022 mg/Kg 11/20/12 16:54 11/24/12 19:53 1☼Chrysene 0.13
0.095 0.027 mg/Kg 11/20/12 16:54 11/24/12 19:53 1☼Dibenz(a,h)anthracene 0.050 J
0.095 0.039 mg/Kg 11/20/12 16:54 11/24/12 19:53 1☼Fluoranthene 0.15
0.095 0.022 mg/Kg 11/20/12 16:54 11/24/12 19:53 1☼Fluorene <0.095
0.095 0.032 mg/Kg 11/20/12 16:54 11/24/12 19:53 1☼Indeno[1,2,3-cd]pyrene 0.10
0.095 0.018 mg/Kg 11/20/12 16:54 11/24/12 19:53 1☼Naphthalene <0.095
0.095 0.040 mg/Kg 11/20/12 16:54 11/24/12 19:53 1☼Phenanthrene 0.053 J
0.095 0.035 mg/Kg 11/20/12 16:54 11/24/12 19:53 1☼Pyrene 0.12
2-Fluorobiphenyl 60 30 - 119 11/20/12 16:54 11/24/12 19:53 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 48 11/20/12 16:54 11/24/12 19:53 130 - 115
Terphenyl-d14 62 11/20/12 16:54 11/24/12 19:53 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 6900 270 36 mg/Kg ☼ 11/13/12 16:30 11/20/12 11:17 50
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.7 0.59 mg/Kg 11/13/12 16:30 11/19/12 23:21 1☼Arsenic 2200
2.7 0.32 mg/Kg 11/13/12 16:30 11/19/12 23:21 1☼Barium 87
0.54 0.13 mg/Kg 11/13/12 16:30 11/19/12 23:21 1☼Cadmium 2.6
2.7 0.45 mg/Kg 11/13/12 16:30 11/19/12 23:21 1☼Chromium 8.9
2.7 0.74 mg/Kg 11/13/12 16:30 11/19/12 23:21 1☼Copper 23
68 23 mg/Kg 11/13/12 16:30 11/20/12 11:17 50☼Lead 150000
2.7 0.78 mg/Kg 11/13/12 16:30 11/19/12 23:21 1☼Selenium 2.0 J
1.4 0.16 mg/Kg 11/13/12 16:30 11/19/12 23:21 1☼Silver 12
5.4 1.9 mg/Kg 11/13/12 16:30 11/19/12 23:21 1☼Zinc 60
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic 0.11 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/19/12 23:06 1Barium 0.54
0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 23:06 1Cadmium 0.0041 J
0.025 0.010 mg/L 11/19/12 08:00 11/19/12 23:06 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 23:06 1Lead 9.3
0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:06 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 23:06 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury 0.000020 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:55 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-7Client Sample ID: K10 (W25') (0-6")Matrix: SolidDate Collected: 11/09/12 11:50
Percent Solids: 33.1Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.044 J 0.045 0.017 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:32 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.31 0.200 0.200 SU 11/15/12 09:40 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-8Client Sample ID: K10 (W25') (6-12")Matrix: SolidDate Collected: 11/09/12 11:51
Percent Solids: 47.1Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.069 0.069 0.021 mg/Kg ☼ 11/20/12 16:54 11/24/12 20:12 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.069 0.016 mg/Kg 11/20/12 16:54 11/24/12 20:12 1☼Acenaphthylene <0.069
0.069 0.016 mg/Kg 11/20/12 16:54 11/24/12 20:12 1☼Anthracene <0.069
0.069 0.014 mg/Kg 11/20/12 16:54 11/24/12 20:12 1☼Benzo[a]anthracene 0.072
0.069 0.013 mg/Kg 11/20/12 16:54 11/24/12 20:12 1☼Benzo[a]pyrene 0.084
0.069 0.013 mg/Kg 11/20/12 16:54 11/24/12 20:12 1☼Benzo[b]fluoranthene 0.095
0.069 0.023 mg/Kg 11/20/12 16:54 11/24/12 20:12 1☼Benzo[g,h,i]perylene 0.066 J
0.069 0.016 mg/Kg 11/20/12 16:54 11/24/12 20:12 1☼Benzo[k]fluoranthene 0.089
0.069 0.016 mg/Kg 11/20/12 16:54 11/24/12 20:12 1☼Chrysene 0.10
0.069 0.019 mg/Kg 11/20/12 16:54 11/24/12 20:12 1☼Dibenz(a,h)anthracene <0.069
0.069 0.028 mg/Kg 11/20/12 16:54 11/24/12 20:12 1☼Fluoranthene 0.16
0.069 0.016 mg/Kg 11/20/12 16:54 11/24/12 20:12 1☼Fluorene <0.069
0.069 0.023 mg/Kg 11/20/12 16:54 11/24/12 20:12 1☼Indeno[1,2,3-cd]pyrene 0.061 J
0.069 0.013 mg/Kg 11/20/12 16:54 11/24/12 20:12 1☼Naphthalene <0.069
0.069 0.029 mg/Kg 11/20/12 16:54 11/24/12 20:12 1☼Phenanthrene 0.082
0.069 0.025 mg/Kg 11/20/12 16:54 11/24/12 20:12 1☼Pyrene 0.14
2-Fluorobiphenyl 58 30 - 119 11/20/12 16:54 11/24/12 20:12 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 45 11/20/12 16:54 11/24/12 20:12 130 - 115
Terphenyl-d14 67 11/20/12 16:54 11/24/12 20:12 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 4.8 4.1 0.54 mg/Kg ☼ 11/13/12 16:30 11/19/12 23:26 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.0 0.44 mg/Kg 11/13/12 16:30 11/19/12 23:26 1☼Arsenic 7.1
2.0 0.24 mg/Kg 11/13/12 16:30 11/19/12 23:26 1☼Barium 110
0.41 0.10 mg/Kg 11/13/12 16:30 11/19/12 23:26 1☼Cadmium 0.52
2.0 0.34 mg/Kg 11/13/12 16:30 11/19/12 23:26 1☼Chromium 13
2.0 0.55 mg/Kg 11/13/12 16:30 11/19/12 23:26 1☼Copper 22
1.0 0.35 mg/Kg 11/13/12 16:30 11/19/12 23:26 1☼Lead 950
2.0 0.58 mg/Kg 11/13/12 16:30 11/19/12 23:26 1☼Selenium <2.0
1.0 0.12 mg/Kg 11/13/12 16:30 11/19/12 23:26 1☼Silver <1.0
4.1 1.4 mg/Kg 11/13/12 16:30 11/19/12 23:26 1☼Zinc 82
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic 0.42 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:12 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/19/12 23:12 1Barium 1.1
0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 23:12 1Cadmium 0.0048 J
0.025 0.010 mg/L 11/19/12 08:00 11/19/12 23:12 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 23:12 1Lead 43
0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:12 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 23:12 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury 0.000023 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:56 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-8Client Sample ID: K10 (W25') (6-12")Matrix: SolidDate Collected: 11/09/12 11:51
Percent Solids: 47.1Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.067 0.033 0.013 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.34 0.200 0.200 SU 11/15/12 09:43 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-9Client Sample ID: K10 (W25') (12-18")Matrix: SolidDate Collected: 11/09/12 11:52
Percent Solids: 78.3Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.040 0.040 0.012 mg/Kg ☼ 11/20/12 16:54 11/24/12 20:32 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.040 0.0093 mg/Kg 11/20/12 16:54 11/24/12 20:32 1☼Acenaphthylene <0.040
0.040 0.0095 mg/Kg 11/20/12 16:54 11/24/12 20:32 1☼Anthracene <0.040
0.040 0.0085 mg/Kg 11/20/12 16:54 11/24/12 20:32 1☼Benzo[a]anthracene <0.040
0.040 0.0074 mg/Kg 11/20/12 16:54 11/24/12 20:32 1☼Benzo[a]pyrene <0.040
0.040 0.0079 mg/Kg 11/20/12 16:54 11/24/12 20:32 1☼Benzo[b]fluoranthene <0.040
0.040 0.014 mg/Kg 11/20/12 16:54 11/24/12 20:32 1☼Benzo[g,h,i]perylene <0.040
0.040 0.0097 mg/Kg 11/20/12 16:54 11/24/12 20:32 1☼Benzo[k]fluoranthene <0.040
0.040 0.0092 mg/Kg 11/20/12 16:54 11/24/12 20:32 1☼Chrysene <0.040
0.040 0.011 mg/Kg 11/20/12 16:54 11/24/12 20:32 1☼Dibenz(a,h)anthracene <0.040
0.040 0.017 mg/Kg 11/20/12 16:54 11/24/12 20:32 1☼Fluoranthene <0.040
0.040 0.0092 mg/Kg 11/20/12 16:54 11/24/12 20:32 1☼Fluorene <0.040
0.040 0.014 mg/Kg 11/20/12 16:54 11/24/12 20:32 1☼Indeno[1,2,3-cd]pyrene <0.040
0.040 0.0078 mg/Kg 11/20/12 16:54 11/24/12 20:32 1☼Naphthalene <0.040
0.040 0.017 mg/Kg 11/20/12 16:54 11/24/12 20:32 1☼Phenanthrene <0.040
0.040 0.015 mg/Kg 11/20/12 16:54 11/24/12 20:32 1☼Pyrene <0.040
2-Fluorobiphenyl 51 30 - 119 11/20/12 16:54 11/24/12 20:32 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 50 11/20/12 16:54 11/24/12 20:32 130 - 115
Terphenyl-d14 53 11/20/12 16:54 11/24/12 20:32 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 0.99 J 2.4 0.32 mg/Kg ☼ 11/13/12 16:30 11/19/12 23:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.2 0.26 mg/Kg 11/13/12 16:30 11/19/12 23:30 1☼Arsenic 5.3
1.2 0.14 mg/Kg 11/13/12 16:30 11/19/12 23:30 1☼Barium 77
0.24 0.060 mg/Kg 11/13/12 16:30 11/19/12 23:30 1☼Cadmium 0.27
1.2 0.20 mg/Kg 11/13/12 16:30 11/19/12 23:30 1☼Chromium 10
1.2 0.33 mg/Kg 11/13/12 16:30 11/19/12 23:30 1☼Copper 16
0.61 0.21 mg/Kg 11/13/12 16:30 11/19/12 23:30 1☼Lead 15
1.2 0.35 mg/Kg 11/13/12 16:30 11/19/12 23:30 1☼Selenium 0.58 J
0.61 0.073 mg/Kg 11/13/12 16:30 11/19/12 23:30 1☼Silver <0.61
2.4 0.83 mg/Kg 11/13/12 16:30 11/19/12 23:30 1☼Zinc 46
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/19/12 23:18 1Barium 1.2
0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 23:18 1Cadmium 0.0045 J
0.025 0.010 mg/L 11/19/12 08:00 11/19/12 23:18 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 23:18 1Lead 0.74
0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:18 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 23:18 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury 0.000026 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:58 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-9Client Sample ID: K10 (W25') (12-18")Matrix: SolidDate Collected: 11/09/12 11:52
Percent Solids: 78.3Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.010 J 0.021 0.0078 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:35 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.53 0.200 0.200 SU 11/15/12 09:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-10Client Sample ID: H10 (N30') (0-6")Matrix: SolidDate Collected: 11/08/12 11:45
Percent Solids: 74.5Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.21 0.21 0.065 mg/Kg ☼ 11/20/12 16:54 11/24/12 20:52 5
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.21 0.050 mg/Kg 11/20/12 16:54 11/24/12 20:52 5☼Acenaphthylene <0.21
0.21 0.051 mg/Kg 11/20/12 16:54 11/24/12 20:52 5☼Anthracene <0.21
0.21 0.045 mg/Kg 11/20/12 16:54 11/24/12 20:52 5☼Benzo[a]anthracene 0.20 J
0.21 0.039 mg/Kg 11/20/12 16:54 11/24/12 20:52 5☼Benzo[a]pyrene 0.34
0.21 0.042 mg/Kg 11/20/12 16:54 11/24/12 20:52 5☼Benzo[b]fluoranthene 0.38
0.21 0.073 mg/Kg 11/20/12 16:54 11/24/12 20:52 5☼Benzo[g,h,i]perylene 0.25
0.21 0.051 mg/Kg 11/20/12 16:54 11/24/12 20:52 5☼Benzo[k]fluoranthene 0.26
0.21 0.049 mg/Kg 11/20/12 16:54 11/24/12 20:52 5☼Chrysene 0.24
0.21 0.060 mg/Kg 11/20/12 16:54 11/24/12 20:52 5☼Dibenz(a,h)anthracene <0.21
0.21 0.088 mg/Kg 11/20/12 16:54 11/24/12 20:52 5☼Fluoranthene 0.14 J
0.21 0.049 mg/Kg 11/20/12 16:54 11/24/12 20:52 5☼Fluorene <0.21
0.21 0.073 mg/Kg 11/20/12 16:54 11/24/12 20:52 5☼Indeno[1,2,3-cd]pyrene 0.22
0.21 0.042 mg/Kg 11/20/12 16:54 11/24/12 20:52 5☼Naphthalene <0.21
0.21 0.090 mg/Kg 11/20/12 16:54 11/24/12 20:52 5☼Phenanthrene <0.21
0.21 0.078 mg/Kg 11/20/12 16:54 11/24/12 20:52 5☼Pyrene 0.15 J
2-Fluorobiphenyl 73 30 - 119 11/20/12 16:54 11/24/12 20:52 5
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 56 11/20/12 16:54 11/24/12 20:52 530 - 115
Terphenyl-d14 83 11/20/12 16:54 11/24/12 20:52 536 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 1.5 J 2.4 0.32 mg/Kg ☼ 11/13/12 16:30 11/19/12 23:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.2 0.26 mg/Kg 11/13/12 16:30 11/19/12 23:34 1☼Arsenic 7.1
1.2 0.14 mg/Kg 11/13/12 16:30 11/19/12 23:34 1☼Barium 81
0.24 0.060 mg/Kg 11/13/12 16:30 11/19/12 23:34 1☼Cadmium 0.41
1.2 0.20 mg/Kg 11/13/12 16:30 11/19/12 23:34 1☼Chromium 14
1.2 0.33 mg/Kg 11/13/12 16:30 11/19/12 23:34 1☼Copper 20
0.61 0.21 mg/Kg 11/13/12 16:30 11/19/12 23:34 1☼Lead 72
1.2 0.35 mg/Kg 11/13/12 16:30 11/19/12 23:34 1☼Selenium <1.2
0.61 0.073 mg/Kg 11/13/12 16:30 11/19/12 23:34 1☼Silver <0.61
2.4 0.83 mg/Kg 11/13/12 16:30 11/19/12 23:34 1☼Zinc 87
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic 0.015 J 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:24 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/19/12 23:24 1Barium 0.57
0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 23:24 1Cadmium 0.0027 J
0.025 0.010 mg/L 11/19/12 08:00 11/19/12 23:24 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 23:24 1Lead 0.47
0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:24 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 23:24 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury 0.000025 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:00 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-10Client Sample ID: H10 (N30') (0-6")Matrix: SolidDate Collected: 11/08/12 11:45
Percent Solids: 74.5Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.038 0.021 0.0080 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:41 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.34 0.200 0.200 SU 11/15/12 09:50 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-11Client Sample ID: H10 (N30') (6-12")Matrix: SolidDate Collected: 11/08/12 11:46
Percent Solids: 78.5Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.040 0.040 0.012 mg/Kg ☼ 11/20/12 16:54 11/24/12 21:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.040 0.0093 mg/Kg 11/20/12 16:54 11/24/12 21:11 1☼Acenaphthylene <0.040
0.040 0.0095 mg/Kg 11/20/12 16:54 11/24/12 21:11 1☼Anthracene <0.040
0.040 0.0085 mg/Kg 11/20/12 16:54 11/24/12 21:11 1☼Benzo[a]anthracene <0.040
0.040 0.0074 mg/Kg 11/20/12 16:54 11/24/12 21:11 1☼Benzo[a]pyrene <0.040
0.040 0.0079 mg/Kg 11/20/12 16:54 11/24/12 21:11 1☼Benzo[b]fluoranthene <0.040
0.040 0.014 mg/Kg 11/20/12 16:54 11/24/12 21:11 1☼Benzo[g,h,i]perylene <0.040
0.040 0.0096 mg/Kg 11/20/12 16:54 11/24/12 21:11 1☼Benzo[k]fluoranthene <0.040
0.040 0.0091 mg/Kg 11/20/12 16:54 11/24/12 21:11 1☼Chrysene <0.040
0.040 0.011 mg/Kg 11/20/12 16:54 11/24/12 21:11 1☼Dibenz(a,h)anthracene <0.040
0.040 0.017 mg/Kg 11/20/12 16:54 11/24/12 21:11 1☼Fluoranthene <0.040
0.040 0.0092 mg/Kg 11/20/12 16:54 11/24/12 21:11 1☼Fluorene <0.040
0.040 0.014 mg/Kg 11/20/12 16:54 11/24/12 21:11 1☼Indeno[1,2,3-cd]pyrene <0.040
0.040 0.0078 mg/Kg 11/20/12 16:54 11/24/12 21:11 1☼Naphthalene <0.040
0.040 0.017 mg/Kg 11/20/12 16:54 11/24/12 21:11 1☼Phenanthrene <0.040
0.040 0.015 mg/Kg 11/20/12 16:54 11/24/12 21:11 1☼Pyrene <0.040
2-Fluorobiphenyl 55 30 - 119 11/20/12 16:54 11/24/12 21:11 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 53 11/20/12 16:54 11/24/12 21:11 130 - 115
Terphenyl-d14 62 11/20/12 16:54 11/24/12 21:11 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony <2.4 2.4 0.32 mg/Kg ☼ 11/13/12 16:30 11/19/12 23:38 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.2 0.27 mg/Kg 11/13/12 16:30 11/19/12 23:38 1☼Arsenic 6.0
1.2 0.14 mg/Kg 11/13/12 16:30 11/19/12 23:38 1☼Barium 130
0.24 0.060 mg/Kg 11/13/12 16:30 11/19/12 23:38 1☼Cadmium 0.20 J
1.2 0.20 mg/Kg 11/13/12 16:30 11/19/12 23:38 1☼Chromium 18
1.2 0.33 mg/Kg 11/13/12 16:30 11/19/12 23:38 1☼Copper 22
0.61 0.21 mg/Kg 11/13/12 16:30 11/19/12 23:38 1☼Lead 19
1.2 0.35 mg/Kg 11/13/12 16:30 11/19/12 23:38 1☼Selenium <1.2
0.61 0.073 mg/Kg 11/13/12 16:30 11/19/12 23:38 1☼Silver <0.61
2.4 0.83 mg/Kg 11/13/12 16:30 11/19/12 23:38 1☼Zinc 62
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:31 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/19/12 23:31 1Barium 0.72
0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 23:31 1Cadmium 0.0020 J
0.025 0.010 mg/L 11/19/12 08:00 11/19/12 23:31 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 23:31 1Lead 0.010
0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:31 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 23:31 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury <0.00020 * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:08 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-11Client Sample ID: H10 (N30') (6-12")Matrix: SolidDate Collected: 11/08/12 11:46
Percent Solids: 78.5Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.034 0.021 0.0079 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:43 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.45 0.200 0.200 SU 11/15/12 09:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-12Client Sample ID: H10 (N30') (12-18")Matrix: SolidDate Collected: 11/08/12 11:47
Percent Solids: 81.5Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.040 0.040 0.012 mg/Kg ☼ 11/20/12 16:54 11/24/12 21:31 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.040 0.0092 mg/Kg 11/20/12 16:54 11/24/12 21:31 1☼Acenaphthylene <0.040
0.040 0.0094 mg/Kg 11/20/12 16:54 11/24/12 21:31 1☼Anthracene <0.040
0.040 0.0084 mg/Kg 11/20/12 16:54 11/24/12 21:31 1☼Benzo[a]anthracene <0.040
0.040 0.0073 mg/Kg 11/20/12 16:54 11/24/12 21:31 1☼Benzo[a]pyrene <0.040
0.040 0.0078 mg/Kg 11/20/12 16:54 11/24/12 21:31 1☼Benzo[b]fluoranthene <0.040
0.040 0.013 mg/Kg 11/20/12 16:54 11/24/12 21:31 1☼Benzo[g,h,i]perylene <0.040
0.040 0.0095 mg/Kg 11/20/12 16:54 11/24/12 21:31 1☼Benzo[k]fluoranthene <0.040
0.040 0.0090 mg/Kg 11/20/12 16:54 11/24/12 21:31 1☼Chrysene <0.040
0.040 0.011 mg/Kg 11/20/12 16:54 11/24/12 21:31 1☼Dibenz(a,h)anthracene <0.040
0.040 0.016 mg/Kg 11/20/12 16:54 11/24/12 21:31 1☼Fluoranthene <0.040
0.040 0.0091 mg/Kg 11/20/12 16:54 11/24/12 21:31 1☼Fluorene <0.040
0.040 0.013 mg/Kg 11/20/12 16:54 11/24/12 21:31 1☼Indeno[1,2,3-cd]pyrene <0.040
0.040 0.0077 mg/Kg 11/20/12 16:54 11/24/12 21:31 1☼Naphthalene <0.040
0.040 0.017 mg/Kg 11/20/12 16:54 11/24/12 21:31 1☼Phenanthrene <0.040
0.040 0.014 mg/Kg 11/20/12 16:54 11/24/12 21:31 1☼Pyrene <0.040
2-Fluorobiphenyl 54 30 - 119 11/20/12 16:54 11/24/12 21:31 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 55 11/20/12 16:54 11/24/12 21:31 130 - 115
Terphenyl-d14 61 11/20/12 16:54 11/24/12 21:31 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 0.64 J 2.1 0.28 mg/Kg ☼ 11/13/12 16:30 11/19/12 23:43 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.1 0.23 mg/Kg 11/13/12 16:30 11/19/12 23:43 1☼Arsenic 7.6
1.1 0.13 mg/Kg 11/13/12 16:30 11/19/12 23:43 1☼Barium 110
0.21 0.052 mg/Kg 11/13/12 16:30 11/19/12 23:43 1☼Cadmium 0.21
1.1 0.18 mg/Kg 11/13/12 16:30 11/19/12 23:43 1☼Chromium 13
1.1 0.29 mg/Kg 11/13/12 16:30 11/19/12 23:43 1☼Copper 22
0.53 0.18 mg/Kg 11/13/12 16:30 11/19/12 23:43 1☼Lead 15
1.1 0.30 mg/Kg 11/13/12 16:30 11/19/12 23:43 1☼Selenium <1.1
0.53 0.064 mg/Kg 11/13/12 16:30 11/19/12 23:43 1☼Silver <0.53
2.1 0.72 mg/Kg 11/13/12 16:30 11/19/12 23:43 1☼Zinc 59
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:37 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/19/12 23:37 1Barium 0.77
0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 23:37 1Cadmium <0.0050
0.025 0.010 mg/L 11/19/12 08:00 11/19/12 23:37 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 23:37 1Lead 0.013
0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:37 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 23:37 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury 0.000028 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:10 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-12Client Sample ID: H10 (N30') (12-18")Matrix: SolidDate Collected: 11/08/12 11:47
Percent Solids: 81.5Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.030 0.019 0.0071 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.54 0.200 0.200 SU 11/15/12 09:55 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-13Client Sample ID: J8 (0-6")Matrix: SolidDate Collected: 11/08/12 12:00
Percent Solids: 73.0Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.044 0.044 0.013 mg/Kg ☼ 11/20/12 16:54 11/24/12 21:51 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.044 0.010 mg/Kg 11/20/12 16:54 11/24/12 21:51 1☼Acenaphthylene <0.044
0.044 0.010 mg/Kg 11/20/12 16:54 11/24/12 21:51 1☼Anthracene <0.044
0.044 0.0093 mg/Kg 11/20/12 16:54 11/24/12 21:51 1☼Benzo[a]anthracene 0.011 J
0.044 0.0081 mg/Kg 11/20/12 16:54 11/24/12 21:51 1☼Benzo[a]pyrene <0.044
0.044 0.0086 mg/Kg 11/20/12 16:54 11/24/12 21:51 1☼Benzo[b]fluoranthene 0.014 J
0.044 0.015 mg/Kg 11/20/12 16:54 11/24/12 21:51 1☼Benzo[g,h,i]perylene <0.044
0.044 0.011 mg/Kg 11/20/12 16:54 11/24/12 21:51 1☼Benzo[k]fluoranthene <0.044
0.044 0.010 mg/Kg 11/20/12 16:54 11/24/12 21:51 1☼Chrysene 0.017 J
0.044 0.012 mg/Kg 11/20/12 16:54 11/24/12 21:51 1☼Dibenz(a,h)anthracene <0.044
0.044 0.018 mg/Kg 11/20/12 16:54 11/24/12 21:51 1☼Fluoranthene <0.044
0.044 0.010 mg/Kg 11/20/12 16:54 11/24/12 21:51 1☼Fluorene <0.044
0.044 0.015 mg/Kg 11/20/12 16:54 11/24/12 21:51 1☼Indeno[1,2,3-cd]pyrene <0.044
0.044 0.0085 mg/Kg 11/20/12 16:54 11/24/12 21:51 1☼Naphthalene 0.0087 J
0.044 0.019 mg/Kg 11/20/12 16:54 11/24/12 21:51 1☼Phenanthrene <0.044
0.044 0.016 mg/Kg 11/20/12 16:54 11/24/12 21:51 1☼Pyrene <0.044
2-Fluorobiphenyl 54 30 - 119 11/20/12 16:54 11/24/12 21:51 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 47 11/20/12 16:54 11/24/12 21:51 130 - 115
Terphenyl-d14 59 11/20/12 16:54 11/24/12 21:51 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony <2.3 2.3 0.31 mg/Kg ☼ 11/13/12 16:30 11/19/12 23:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.2 0.25 mg/Kg 11/13/12 16:30 11/19/12 23:48 1☼Arsenic 7.8
1.2 0.14 mg/Kg 11/13/12 16:30 11/19/12 23:48 1☼Barium 100
0.23 0.058 mg/Kg 11/13/12 16:30 11/19/12 23:48 1☼Cadmium 0.37
1.2 0.19 mg/Kg 11/13/12 16:30 11/19/12 23:48 1☼Chromium 15
1.2 0.32 mg/Kg 11/13/12 16:30 11/19/12 23:48 1☼Copper 24
0.58 0.20 mg/Kg 11/13/12 16:30 11/19/12 23:48 1☼Lead 25
1.2 0.33 mg/Kg 11/13/12 16:30 11/19/12 23:48 1☼Selenium 0.67 J
0.58 0.070 mg/Kg 11/13/12 16:30 11/19/12 23:48 1☼Silver <0.58
2.3 0.80 mg/Kg 11/13/12 16:30 11/19/12 23:48 1☼Zinc 77
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:43 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/19/12 23:43 1Barium 0.71
0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 23:43 1Cadmium <0.0050
0.025 0.010 mg/L 11/19/12 08:00 11/19/12 23:43 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 23:43 1Lead 0.0060 J
0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:43 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 23:43 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury 0.000020 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:12 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-13Client Sample ID: J8 (0-6")Matrix: SolidDate Collected: 11/08/12 12:00
Percent Solids: 73.0Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.042 0.021 0.0080 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.53 0.200 0.200 SU 11/15/12 09:58 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-14Client Sample ID: J8 (6-12")Matrix: SolidDate Collected: 11/08/12 12:01
Percent Solids: 69.3Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.046 0.046 0.014 mg/Kg ☼ 11/20/12 16:54 11/24/12 22:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.046 0.011 mg/Kg 11/20/12 16:54 11/24/12 22:11 1☼Acenaphthylene <0.046
0.046 0.011 mg/Kg 11/20/12 16:54 11/24/12 22:11 1☼Anthracene <0.046
0.046 0.0096 mg/Kg 11/20/12 16:54 11/24/12 22:11 1☼Benzo[a]anthracene <0.046
0.046 0.0084 mg/Kg 11/20/12 16:54 11/24/12 22:11 1☼Benzo[a]pyrene <0.046
0.046 0.0089 mg/Kg 11/20/12 16:54 11/24/12 22:11 1☼Benzo[b]fluoranthene <0.046
0.046 0.016 mg/Kg 11/20/12 16:54 11/24/12 22:11 1☼Benzo[g,h,i]perylene <0.046
0.046 0.011 mg/Kg 11/20/12 16:54 11/24/12 22:11 1☼Benzo[k]fluoranthene <0.046
0.046 0.010 mg/Kg 11/20/12 16:54 11/24/12 22:11 1☼Chrysene <0.046
0.046 0.013 mg/Kg 11/20/12 16:54 11/24/12 22:11 1☼Dibenz(a,h)anthracene <0.046
0.046 0.019 mg/Kg 11/20/12 16:54 11/24/12 22:11 1☼Fluoranthene <0.046
0.046 0.010 mg/Kg 11/20/12 16:54 11/24/12 22:11 1☼Fluorene <0.046
0.046 0.016 mg/Kg 11/20/12 16:54 11/24/12 22:11 1☼Indeno[1,2,3-cd]pyrene <0.046
0.046 0.0089 mg/Kg 11/20/12 16:54 11/24/12 22:11 1☼Naphthalene <0.046
0.046 0.019 mg/Kg 11/20/12 16:54 11/24/12 22:11 1☼Phenanthrene <0.046
0.046 0.017 mg/Kg 11/20/12 16:54 11/24/12 22:11 1☼Pyrene <0.046
2-Fluorobiphenyl 48 30 - 119 11/20/12 16:54 11/24/12 22:11 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 43 11/20/12 16:54 11/24/12 22:11 130 - 115
Terphenyl-d14 49 11/20/12 16:54 11/24/12 22:11 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony <2.6 2.6 0.35 mg/Kg ☼ 11/13/12 16:30 11/19/12 23:52 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.3 0.29 mg/Kg 11/13/12 16:30 11/19/12 23:52 1☼Arsenic 5.4
1.3 0.16 mg/Kg 11/13/12 16:30 11/19/12 23:52 1☼Barium 120
0.26 0.065 mg/Kg 11/13/12 16:30 11/19/12 23:52 1☼Cadmium 0.44
1.3 0.22 mg/Kg 11/13/12 16:30 11/19/12 23:52 1☼Chromium 18
1.3 0.36 mg/Kg 11/13/12 16:30 11/19/12 23:52 1☼Copper 19
0.66 0.23 mg/Kg 11/13/12 16:30 11/19/12 23:52 1☼Lead 27
1.3 0.38 mg/Kg 11/13/12 16:30 11/19/12 23:52 1☼Selenium 0.50 J
0.66 0.079 mg/Kg 11/13/12 16:30 11/19/12 23:52 1☼Silver <0.66
2.6 0.90 mg/Kg 11/13/12 16:30 11/19/12 23:52 1☼Zinc 98
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic 0.012 J 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/19/12 23:49 1Barium 0.40 J
0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 23:49 1Cadmium <0.0050
0.025 0.010 mg/L 11/19/12 08:00 11/19/12 23:49 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 23:49 1Lead 0.012
0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:49 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 23:49 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury 0.000043 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:13 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-14Client Sample ID: J8 (6-12")Matrix: SolidDate Collected: 11/08/12 12:01
Percent Solids: 69.3Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.051 0.022 0.0084 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.68 0.200 0.200 SU 11/15/12 10:01 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-15Client Sample ID: J8 (12-18")Matrix: SolidDate Collected: 11/08/12 12:02
Percent Solids: 72.6Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.045 0.045 0.014 mg/Kg ☼ 11/20/12 16:54 11/24/12 22:31 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.045 0.010 mg/Kg 11/20/12 16:54 11/24/12 22:31 1☼Acenaphthylene <0.045
0.045 0.011 mg/Kg 11/20/12 16:54 11/24/12 22:31 1☼Anthracene <0.045
0.045 0.0095 mg/Kg 11/20/12 16:54 11/24/12 22:31 1☼Benzo[a]anthracene <0.045
0.045 0.0083 mg/Kg 11/20/12 16:54 11/24/12 22:31 1☼Benzo[a]pyrene <0.045
0.045 0.0088 mg/Kg 11/20/12 16:54 11/24/12 22:31 1☼Benzo[b]fluoranthene <0.045
0.045 0.015 mg/Kg 11/20/12 16:54 11/24/12 22:31 1☼Benzo[g,h,i]perylene <0.045
0.045 0.011 mg/Kg 11/20/12 16:54 11/24/12 22:31 1☼Benzo[k]fluoranthene <0.045
0.045 0.010 mg/Kg 11/20/12 16:54 11/24/12 22:31 1☼Chrysene <0.045
0.045 0.013 mg/Kg 11/20/12 16:54 11/24/12 22:31 1☼Dibenz(a,h)anthracene <0.045
0.045 0.019 mg/Kg 11/20/12 16:54 11/24/12 22:31 1☼Fluoranthene <0.045
0.045 0.010 mg/Kg 11/20/12 16:54 11/24/12 22:31 1☼Fluorene <0.045
0.045 0.015 mg/Kg 11/20/12 16:54 11/24/12 22:31 1☼Indeno[1,2,3-cd]pyrene <0.045
0.045 0.0087 mg/Kg 11/20/12 16:54 11/24/12 22:31 1☼Naphthalene <0.045
0.045 0.019 mg/Kg 11/20/12 16:54 11/24/12 22:31 1☼Phenanthrene <0.045
0.045 0.016 mg/Kg 11/20/12 16:54 11/24/12 22:31 1☼Pyrene <0.045
2-Fluorobiphenyl 47 30 - 119 11/20/12 16:54 11/24/12 22:31 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 44 11/20/12 16:54 11/24/12 22:31 130 - 115
Terphenyl-d14 52 11/20/12 16:54 11/24/12 22:31 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony <2.4 2.4 0.32 mg/Kg ☼ 11/13/12 16:30 11/20/12 00:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.2 0.26 mg/Kg 11/13/12 16:30 11/20/12 00:06 1☼Arsenic 5.5
1.2 0.14 mg/Kg 11/13/12 16:30 11/20/12 00:06 1☼Barium 110
0.24 0.060 mg/Kg 11/13/12 16:30 11/20/12 00:06 1☼Cadmium 0.22 J
1.2 0.20 mg/Kg 11/13/12 16:30 11/20/12 00:06 1☼Chromium 18
1.2 0.33 mg/Kg 11/13/12 16:30 11/20/12 00:06 1☼Copper 23
0.60 0.21 mg/Kg 11/13/12 16:30 11/20/12 00:06 1☼Lead 23
1.2 0.35 mg/Kg 11/13/12 16:30 11/20/12 00:06 1☼Selenium 0.47 J
0.60 0.072 mg/Kg 11/13/12 16:30 11/20/12 00:06 1☼Silver <0.60
2.4 0.83 mg/Kg 11/13/12 16:30 11/20/12 00:06 1☼Zinc 66
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic 0.011 J 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:55 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/19/12 23:55 1Barium 0.43 J
0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 23:55 1Cadmium <0.0050
0.025 0.010 mg/L 11/19/12 08:00 11/19/12 23:55 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 23:55 1Lead 0.0073 J
0.050 0.010 mg/L 11/19/12 08:00 11/19/12 23:55 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 23:55 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury 0.000026 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:15 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-15Client Sample ID: J8 (12-18")Matrix: SolidDate Collected: 11/08/12 12:02
Percent Solids: 72.6Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.040 0.020 0.0077 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:50 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.43 0.200 0.200 SU 11/15/12 10:03 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-16Client Sample ID: L6 (W20') (0-6")Matrix: SolidDate Collected: 11/08/12 13:20
Percent Solids: 78.2Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.041 0.041 0.012 mg/Kg ☼ 11/20/12 16:54 11/24/12 22:50 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.041 0.0096 mg/Kg 11/20/12 16:54 11/24/12 22:50 1☼Acenaphthylene <0.041
0.041 0.0098 mg/Kg 11/20/12 16:54 11/24/12 22:50 1☼Anthracene <0.041
0.041 0.0087 mg/Kg 11/20/12 16:54 11/24/12 22:50 1☼Benzo[a]anthracene <0.041
0.041 0.0076 mg/Kg 11/20/12 16:54 11/24/12 22:50 1☼Benzo[a]pyrene <0.041
0.041 0.0081 mg/Kg 11/20/12 16:54 11/24/12 22:50 1☼Benzo[b]fluoranthene <0.041
0.041 0.014 mg/Kg 11/20/12 16:54 11/24/12 22:50 1☼Benzo[g,h,i]perylene <0.041
0.041 0.0099 mg/Kg 11/20/12 16:54 11/24/12 22:50 1☼Benzo[k]fluoranthene <0.041
0.041 0.0094 mg/Kg 11/20/12 16:54 11/24/12 22:50 1☼Chrysene <0.041
0.041 0.012 mg/Kg 11/20/12 16:54 11/24/12 22:50 1☼Dibenz(a,h)anthracene <0.041
0.041 0.017 mg/Kg 11/20/12 16:54 11/24/12 22:50 1☼Fluoranthene <0.041
0.041 0.0095 mg/Kg 11/20/12 16:54 11/24/12 22:50 1☼Fluorene <0.041
0.041 0.014 mg/Kg 11/20/12 16:54 11/24/12 22:50 1☼Indeno[1,2,3-cd]pyrene <0.041
0.041 0.0080 mg/Kg 11/20/12 16:54 11/24/12 22:50 1☼Naphthalene <0.041
0.041 0.017 mg/Kg 11/20/12 16:54 11/24/12 22:50 1☼Phenanthrene <0.041
0.041 0.015 mg/Kg 11/20/12 16:54 11/24/12 22:50 1☼Pyrene <0.041
2-Fluorobiphenyl 59 30 - 119 11/20/12 16:54 11/24/12 22:50 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 54 11/20/12 16:54 11/24/12 22:50 130 - 115
Terphenyl-d14 59 11/20/12 16:54 11/24/12 22:50 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 0.45 J 2.5 0.34 mg/Kg ☼ 11/13/12 16:30 11/20/12 00:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.3 0.28 mg/Kg 11/13/12 16:30 11/20/12 00:11 1☼Arsenic 2.6
1.3 0.15 mg/Kg 11/13/12 16:30 11/20/12 00:11 1☼Barium 76
0.25 0.063 mg/Kg 11/13/12 16:30 11/20/12 00:11 1☼Cadmium 0.30
1.3 0.21 mg/Kg 11/13/12 16:30 11/20/12 00:11 1☼Chromium 13
1.3 0.35 mg/Kg 11/13/12 16:30 11/20/12 00:11 1☼Copper 16
0.64 0.22 mg/Kg 11/13/12 16:30 11/20/12 00:11 1☼Lead 12
1.3 0.37 mg/Kg 11/13/12 16:30 11/20/12 00:11 1☼Selenium 0.41 J
0.64 0.077 mg/Kg 11/13/12 16:30 11/20/12 00:11 1☼Silver <0.64
2.5 0.87 mg/Kg 11/13/12 16:30 11/20/12 00:11 1☼Zinc 52
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/20/12 00:02 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/20/12 00:02 1Barium 1.3
0.0050 0.0020 mg/L 11/19/12 08:00 11/20/12 00:02 1Cadmium 0.0021 J
0.025 0.010 mg/L 11/19/12 08:00 11/20/12 00:02 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/20/12 00:02 1Lead 0.0093
0.050 0.010 mg/L 11/19/12 08:00 11/20/12 00:02 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/20/12 00:02 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury 0.000032 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:17 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-16Client Sample ID: L6 (W20') (0-6")Matrix: SolidDate Collected: 11/08/12 13:20
Percent Solids: 78.2Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.028 0.021 0.0080 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:52 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.14 0.200 0.200 SU 11/15/12 10:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
Page 48 of 104 11/26/2012
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-17Client Sample ID: L6 (W20') (6-12")Matrix: SolidDate Collected: 11/08/12 13:21
Percent Solids: 79.3Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.041 0.041 0.012 mg/Kg ☼ 11/20/12 16:54 11/24/12 23:10 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.041 0.0095 mg/Kg 11/20/12 16:54 11/24/12 23:10 1☼Acenaphthylene <0.041
0.041 0.0097 mg/Kg 11/20/12 16:54 11/24/12 23:10 1☼Anthracene <0.041
0.041 0.0086 mg/Kg 11/20/12 16:54 11/24/12 23:10 1☼Benzo[a]anthracene <0.041
0.041 0.0075 mg/Kg 11/20/12 16:54 11/24/12 23:10 1☼Benzo[a]pyrene <0.041
0.041 0.0080 mg/Kg 11/20/12 16:54 11/24/12 23:10 1☼Benzo[b]fluoranthene <0.041
0.041 0.014 mg/Kg 11/20/12 16:54 11/24/12 23:10 1☼Benzo[g,h,i]perylene <0.041
0.041 0.0098 mg/Kg 11/20/12 16:54 11/24/12 23:10 1☼Benzo[k]fluoranthene <0.041
0.041 0.0093 mg/Kg 11/20/12 16:54 11/24/12 23:10 1☼Chrysene <0.041
0.041 0.012 mg/Kg 11/20/12 16:54 11/24/12 23:10 1☼Dibenz(a,h)anthracene <0.041
0.041 0.017 mg/Kg 11/20/12 16:54 11/24/12 23:10 1☼Fluoranthene <0.041
0.041 0.0094 mg/Kg 11/20/12 16:54 11/24/12 23:10 1☼Fluorene <0.041
0.041 0.014 mg/Kg 11/20/12 16:54 11/24/12 23:10 1☼Indeno[1,2,3-cd]pyrene <0.041
0.041 0.0080 mg/Kg 11/20/12 16:54 11/24/12 23:10 1☼Naphthalene <0.041
0.041 0.017 mg/Kg 11/20/12 16:54 11/24/12 23:10 1☼Phenanthrene <0.041
0.041 0.015 mg/Kg 11/20/12 16:54 11/24/12 23:10 1☼Pyrene <0.041
2-Fluorobiphenyl 68 30 - 119 11/20/12 16:54 11/24/12 23:10 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 66 11/20/12 16:54 11/24/12 23:10 130 - 115
Terphenyl-d14 60 11/20/12 16:54 11/24/12 23:10 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 0.54 J 2.3 0.31 mg/Kg ☼ 11/13/12 16:30 11/20/12 00:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.2 0.25 mg/Kg 11/13/12 16:30 11/20/12 00:16 1☼Arsenic 4.2
1.2 0.14 mg/Kg 11/13/12 16:30 11/20/12 00:16 1☼Barium 37
0.23 0.057 mg/Kg 11/13/12 16:30 11/20/12 00:16 1☼Cadmium 0.37
1.2 0.19 mg/Kg 11/13/12 16:30 11/20/12 00:16 1☼Chromium 8.0
1.2 0.31 mg/Kg 11/13/12 16:30 11/20/12 00:16 1☼Copper 28
0.58 0.20 mg/Kg 11/13/12 16:30 11/20/12 00:16 1☼Lead 15
1.2 0.33 mg/Kg 11/13/12 16:30 11/20/12 00:16 1☼Selenium 0.82 J
0.58 0.070 mg/Kg 11/13/12 16:30 11/20/12 00:16 1☼Silver 0.082 J
2.3 0.79 mg/Kg 11/13/12 16:30 11/20/12 00:16 1☼Zinc 58
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/20/12 00:23 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/20/12 00:23 1Barium 0.88
0.0050 0.0020 mg/L 11/19/12 08:00 11/20/12 00:23 1Cadmium 0.0044 J
0.025 0.010 mg/L 11/19/12 08:00 11/20/12 00:23 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/20/12 00:23 1Lead 0.0076
0.050 0.010 mg/L 11/19/12 08:00 11/20/12 00:23 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/20/12 00:23 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury 0.000027 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-17Client Sample ID: L6 (W20') (6-12")Matrix: SolidDate Collected: 11/08/12 13:21
Percent Solids: 79.3Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.023 0.018 0.0069 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:54 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 8.09 0.200 0.200 SU 11/15/12 10:08 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
Page 50 of 104 11/26/2012
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-18Client Sample ID: L6 (W20') (12-18")Matrix: SolidDate Collected: 11/08/12 13:22
Percent Solids: 78.4Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.040 0.040 0.012 mg/Kg ☼ 11/20/12 16:54 11/24/12 23:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.040 0.0092 mg/Kg 11/20/12 16:54 11/24/12 23:30 1☼Acenaphthylene <0.040
0.040 0.0095 mg/Kg 11/20/12 16:54 11/24/12 23:30 1☼Anthracene <0.040
0.040 0.0084 mg/Kg 11/20/12 16:54 11/24/12 23:30 1☼Benzo[a]anthracene <0.040
0.040 0.0073 mg/Kg 11/20/12 16:54 11/24/12 23:30 1☼Benzo[a]pyrene <0.040
0.040 0.0078 mg/Kg 11/20/12 16:54 11/24/12 23:30 1☼Benzo[b]fluoranthene <0.040
0.040 0.014 mg/Kg 11/20/12 16:54 11/24/12 23:30 1☼Benzo[g,h,i]perylene <0.040
0.040 0.0096 mg/Kg 11/20/12 16:54 11/24/12 23:30 1☼Benzo[k]fluoranthene <0.040
0.040 0.0091 mg/Kg 11/20/12 16:54 11/24/12 23:30 1☼Chrysene <0.040
0.040 0.011 mg/Kg 11/20/12 16:54 11/24/12 23:30 1☼Dibenz(a,h)anthracene <0.040
0.040 0.016 mg/Kg 11/20/12 16:54 11/24/12 23:30 1☼Fluoranthene <0.040
0.040 0.0091 mg/Kg 11/20/12 16:54 11/24/12 23:30 1☼Fluorene <0.040
0.040 0.014 mg/Kg 11/20/12 16:54 11/24/12 23:30 1☼Indeno[1,2,3-cd]pyrene <0.040
0.040 0.0078 mg/Kg 11/20/12 16:54 11/24/12 23:30 1☼Naphthalene <0.040
0.040 0.017 mg/Kg 11/20/12 16:54 11/24/12 23:30 1☼Phenanthrene <0.040
0.040 0.015 mg/Kg 11/20/12 16:54 11/24/12 23:30 1☼Pyrene <0.040
2-Fluorobiphenyl 58 30 - 119 11/20/12 16:54 11/24/12 23:30 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 56 11/20/12 16:54 11/24/12 23:30 130 - 115
Terphenyl-d14 59 11/20/12 16:54 11/24/12 23:30 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 0.79 J 2.2 0.29 mg/Kg ☼ 11/13/12 16:30 11/20/12 00:21 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.1 0.24 mg/Kg 11/13/12 16:30 11/20/12 00:21 1☼Arsenic 1.8
1.1 0.13 mg/Kg 11/13/12 16:30 11/20/12 00:21 1☼Barium 78
0.22 0.055 mg/Kg 11/13/12 16:30 11/20/12 00:21 1☼Cadmium 0.26
1.1 0.18 mg/Kg 11/13/12 16:30 11/20/12 00:21 1☼Chromium 14
1.1 0.30 mg/Kg 11/13/12 16:30 11/20/12 00:21 1☼Copper 19
0.55 0.19 mg/Kg 11/13/12 16:30 11/20/12 00:21 1☼Lead 15
1.1 0.32 mg/Kg 11/13/12 16:30 11/20/12 00:21 1☼Selenium <1.1
0.55 0.066 mg/Kg 11/13/12 16:30 11/20/12 00:21 1☼Silver <0.55
2.2 0.76 mg/Kg 11/13/12 16:30 11/20/12 00:21 1☼Zinc 54
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/20/12 00:29 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/20/12 00:29 1Barium 1.1
0.0050 0.0020 mg/L 11/19/12 08:00 11/20/12 00:29 1Cadmium 0.0022 J
0.025 0.010 mg/L 11/19/12 08:00 11/20/12 00:29 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/20/12 00:29 1Lead 0.0066 J
0.050 0.010 mg/L 11/19/12 08:00 11/20/12 00:29 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/20/12 00:29 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury 0.000024 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:20 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-18Client Sample ID: L6 (W20') (12-18")Matrix: SolidDate Collected: 11/08/12 13:22
Percent Solids: 78.4Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.016 J 0.019 0.0074 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:56 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 8.11 0.200 0.200 SU 11/15/12 10:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-19Client Sample ID: J17 (N30;W20') (0-6")Matrix: SolidDate Collected: 11/08/12 14:40
Percent Solids: 42.0Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.37 0.37 0.11 mg/Kg ☼ 11/20/12 16:54 11/24/12 23:50 5
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.37 0.086 mg/Kg 11/20/12 16:54 11/24/12 23:50 5☼Acenaphthylene <0.37
0.37 0.088 mg/Kg 11/20/12 16:54 11/24/12 23:50 5☼Anthracene <0.37
0.37 0.078 mg/Kg 11/20/12 16:54 11/24/12 23:50 5☼Benzo[a]anthracene 0.46
0.37 0.068 mg/Kg 11/20/12 16:54 11/24/12 23:50 5☼Benzo[a]pyrene 0.65
0.37 0.073 mg/Kg 11/20/12 16:54 11/24/12 23:50 5☼Benzo[b]fluoranthene 0.82
0.37 0.13 mg/Kg 11/20/12 16:54 11/24/12 23:50 5☼Benzo[g,h,i]perylene 0.61
0.37 0.089 mg/Kg 11/20/12 16:54 11/24/12 23:50 5☼Benzo[k]fluoranthene 0.41
0.37 0.084 mg/Kg 11/20/12 16:54 11/24/12 23:50 5☼Chrysene 0.63
0.37 0.10 mg/Kg 11/20/12 16:54 11/24/12 23:50 5☼Dibenz(a,h)anthracene <0.37
0.37 0.15 mg/Kg 11/20/12 16:54 11/24/12 23:50 5☼Fluoranthene 0.60
0.37 0.085 mg/Kg 11/20/12 16:54 11/24/12 23:50 5☼Fluorene <0.37
0.37 0.13 mg/Kg 11/20/12 16:54 11/24/12 23:50 5☼Indeno[1,2,3-cd]pyrene 0.50
0.37 0.072 mg/Kg 11/20/12 16:54 11/24/12 23:50 5☼Naphthalene <0.37
0.37 0.16 mg/Kg 11/20/12 16:54 11/24/12 23:50 5☼Phenanthrene <0.37
0.37 0.14 mg/Kg 11/20/12 16:54 11/24/12 23:50 5☼Pyrene 0.62
2-Fluorobiphenyl 56 30 - 119 11/20/12 16:54 11/24/12 23:50 5
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 46 11/20/12 16:54 11/24/12 23:50 530 - 115
Terphenyl-d14 74 11/20/12 16:54 11/24/12 23:50 536 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 11 4.3 0.57 mg/Kg ☼ 11/13/12 16:30 11/20/12 00:26 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.2 0.47 mg/Kg 11/13/12 16:30 11/20/12 00:26 1☼Arsenic 15
2.2 0.26 mg/Kg 11/13/12 16:30 11/20/12 00:26 1☼Barium 54
0.43 0.11 mg/Kg 11/13/12 16:30 11/20/12 00:26 1☼Cadmium 0.47
2.2 0.36 mg/Kg 11/13/12 16:30 11/20/12 00:26 1☼Chromium 11
2.2 0.59 mg/Kg 11/13/12 16:30 11/20/12 00:26 1☼Copper 25
1.1 0.37 mg/Kg 11/13/12 16:30 11/20/12 00:26 1☼Lead 2600
2.2 0.62 mg/Kg 11/13/12 16:30 11/20/12 00:26 1☼Selenium <2.2
1.1 0.13 mg/Kg 11/13/12 16:30 11/20/12 00:26 1☼Silver <1.1
4.3 1.5 mg/Kg 11/13/12 16:30 11/20/12 00:26 1☼Zinc 71
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic 0.026 J 0.050 0.010 mg/L 11/19/12 08:00 11/20/12 00:35 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/20/12 00:35 1Barium 0.46 J
0.0050 0.0020 mg/L 11/19/12 08:00 11/20/12 00:35 1Cadmium 0.0048 J
0.025 0.010 mg/L 11/19/12 08:00 11/20/12 00:35 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/20/12 00:35 1Lead 0.12
0.050 0.010 mg/L 11/19/12 08:00 11/20/12 00:35 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/20/12 00:35 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury 0.000023 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:22 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-19Client Sample ID: J17 (N30;W20') (0-6")Matrix: SolidDate Collected: 11/08/12 14:40
Percent Solids: 42.0Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.058 0.037 0.014 mg/Kg ☼ 11/19/12 17:00 11/20/12 11:58 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.70 0.200 0.200 SU 11/15/12 10:13 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-20Client Sample ID: J17 (N30;W20') (6-12")Matrix: SolidDate Collected: 11/08/12 14:41
Percent Solids: 35.2Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.093 0.093 0.028 mg/Kg ☼ 11/20/12 16:54 11/25/12 00:09 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.093 0.021 mg/Kg 11/20/12 16:54 11/25/12 00:09 1☼Acenaphthylene <0.093
0.093 0.022 mg/Kg 11/20/12 16:54 11/25/12 00:09 1☼Anthracene 0.050 J
0.093 0.020 mg/Kg 11/20/12 16:54 11/25/12 00:09 1☼Benzo[a]anthracene 0.71
0.093 0.017 mg/Kg 11/20/12 16:54 11/25/12 00:09 1☼Benzo[a]pyrene 0.93
0.093 0.018 mg/Kg 11/20/12 16:54 11/25/12 00:09 1☼Benzo[b]fluoranthene 1.2
0.093 0.032 mg/Kg 11/20/12 16:54 11/25/12 00:09 1☼Benzo[g,h,i]perylene 0.77
0.093 0.022 mg/Kg 11/20/12 16:54 11/25/12 00:09 1☼Benzo[k]fluoranthene 0.66
0.093 0.021 mg/Kg 11/20/12 16:54 11/25/12 00:09 1☼Chrysene 0.90
0.093 0.026 mg/Kg 11/20/12 16:54 11/25/12 00:09 1☼Dibenz(a,h)anthracene 0.30
0.093 0.038 mg/Kg 11/20/12 16:54 11/25/12 00:09 1☼Fluoranthene 1.1
0.093 0.021 mg/Kg 11/20/12 16:54 11/25/12 00:09 1☼Fluorene 0.031 J
0.093 0.032 mg/Kg 11/20/12 16:54 11/25/12 00:09 1☼Indeno[1,2,3-cd]pyrene 0.64
0.093 0.018 mg/Kg 11/20/12 16:54 11/25/12 00:09 1☼Naphthalene <0.093
0.093 0.039 mg/Kg 11/20/12 16:54 11/25/12 00:09 1☼Phenanthrene 0.45
0.093 0.034 mg/Kg 11/20/12 16:54 11/25/12 00:09 1☼Pyrene 0.85
2-Fluorobiphenyl 55 30 - 119 11/20/12 16:54 11/25/12 00:09 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 47 11/20/12 16:54 11/25/12 00:09 130 - 115
Terphenyl-d14 58 11/20/12 16:54 11/25/12 00:09 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 5900 260 35 mg/Kg ☼ 11/13/12 16:30 11/20/12 11:21 50
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2.6 0.57 mg/Kg 11/13/12 16:30 11/20/12 00:30 1☼Arsenic 1900
2.6 0.31 mg/Kg 11/13/12 16:30 11/20/12 00:30 1☼Barium 75
0.52 0.13 mg/Kg 11/13/12 16:30 11/20/12 00:30 1☼Cadmium 3.0
2.6 0.44 mg/Kg 11/13/12 16:30 11/20/12 00:30 1☼Chromium 10
2.6 0.71 mg/Kg 11/13/12 16:30 11/20/12 00:30 1☼Copper 27
66 23 mg/Kg 11/13/12 16:30 11/20/12 11:21 50☼Lead 110000
2.6 0.75 mg/Kg 11/13/12 16:30 11/20/12 00:30 1☼Selenium 1.2 J
1.3 0.16 mg/Kg 11/13/12 16:30 11/20/12 00:30 1☼Silver 4.2
5.2 1.8 mg/Kg 11/13/12 16:30 11/20/12 00:30 1☼Zinc 99
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic 0.047 J 0.050 0.010 mg/L 11/19/12 08:00 11/20/12 00:41 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/20/12 00:41 1Barium 0.54
0.0050 0.0020 mg/L 11/19/12 08:00 11/20/12 00:41 1Cadmium 0.0043 J
0.025 0.010 mg/L 11/19/12 08:00 11/20/12 00:41 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/20/12 00:41 1Lead 3.0
0.050 0.010 mg/L 11/19/12 08:00 11/20/12 00:41 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/20/12 00:41 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury 0.000038 J * 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 12:24 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-20Client Sample ID: J17 (N30;W20') (6-12")Matrix: SolidDate Collected: 11/08/12 14:41
Percent Solids: 35.2Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.047 0.045 0.017 mg/Kg ☼ 11/19/12 17:00 11/20/12 12:03 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.30 0.200 0.200 SU 11/15/12 10:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-21Client Sample ID: J17 (N30;W20') (12-18")Matrix: SolidDate Collected: 11/08/12 14:42
Percent Solids: 74.5Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.044 0.044 0.013 mg/Kg ☼ 11/20/12 17:12 11/25/12 00:29 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.044 0.010 mg/Kg 11/20/12 17:12 11/25/12 00:29 1☼Acenaphthylene <0.044
0.044 0.010 mg/Kg 11/20/12 17:12 11/25/12 00:29 1☼Anthracene <0.044
0.044 0.0092 mg/Kg 11/20/12 17:12 11/25/12 00:29 1☼Benzo[a]anthracene 0.16
0.044 0.0080 mg/Kg 11/20/12 17:12 11/25/12 00:29 1☼Benzo[a]pyrene 0.20
0.044 0.0085 mg/Kg 11/20/12 17:12 11/25/12 00:29 1☼Benzo[b]fluoranthene 0.18
0.044 0.015 mg/Kg 11/20/12 17:12 11/25/12 00:29 1☼Benzo[g,h,i]perylene 0.16
0.044 0.010 mg/Kg 11/20/12 17:12 11/25/12 00:29 1☼Benzo[k]fluoranthene 0.23
0.044 0.0099 mg/Kg 11/20/12 17:12 11/25/12 00:29 1☼Chrysene 0.17
0.044 0.012 mg/Kg 11/20/12 17:12 11/25/12 00:29 1☼Dibenz(a,h)anthracene 0.063
0.044 0.018 mg/Kg 11/20/12 17:12 11/25/12 00:29 1☼Fluoranthene 0.21
0.044 0.010 mg/Kg 11/20/12 17:12 11/25/12 00:29 1☼Fluorene <0.044
0.044 0.015 mg/Kg 11/20/12 17:12 11/25/12 00:29 1☼Indeno[1,2,3-cd]pyrene 0.13
0.044 0.0085 mg/Kg 11/20/12 17:12 11/25/12 00:29 1☼Naphthalene <0.044
0.044 0.018 mg/Kg 11/20/12 17:12 11/25/12 00:29 1☼Phenanthrene 0.056
0.044 0.016 mg/Kg 11/20/12 17:12 11/25/12 00:29 1☼Pyrene 0.15
2-Fluorobiphenyl 72 30 - 119 11/20/12 17:12 11/25/12 00:29 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 63 11/20/12 17:12 11/25/12 00:29 130 - 115
Terphenyl-d14 68 11/20/12 17:12 11/25/12 00:29 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 4.9 2.5 0.34 mg/Kg ☼ 11/14/12 08:30 11/15/12 17:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.3 0.28 mg/Kg 11/14/12 08:30 11/15/12 17:53 1☼Arsenic 9.1
1.3 0.15 mg/Kg 11/14/12 08:30 11/15/12 17:53 1☼Barium 50
0.25 0.063 mg/Kg 11/14/12 08:30 11/15/12 17:53 1☼Cadmium 0.34
1.3 0.21 mg/Kg 11/14/12 08:30 11/15/12 17:53 1☼Chromium 12
1.3 0.34 mg/Kg 11/14/12 08:30 11/15/12 17:53 1☼Copper 20
0.64 0.22 mg/Kg 11/14/12 08:30 11/15/12 17:53 1☼Lead 890
1.3 0.37 mg/Kg 11/14/12 08:30 11/15/12 17:53 1☼Selenium 0.56 J
0.64 0.076 mg/Kg 11/14/12 08:30 11/15/12 17:53 1☼Silver <0.64
2.5 0.87 mg/Kg 11/14/12 08:30 11/15/12 17:53 1☼Zinc 58
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 19:42 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/19/12 19:42 1Barium 0.66
0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 19:42 1Cadmium <0.0050
0.025 0.010 mg/L 11/19/12 08:00 11/19/12 19:42 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 19:42 1Lead 0.66 B
0.050 0.010 mg/L 11/19/12 08:00 11/19/12 19:42 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 19:42 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury 0.000026 J B 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 10:07 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-21Client Sample ID: J17 (N30;W20') (12-18")Matrix: SolidDate Collected: 11/08/12 14:42
Percent Solids: 74.5Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.027 0.020 0.0078 mg/Kg ☼ 11/19/12 17:00 11/20/12 12:39 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.41 0.200 0.200 SU 11/15/12 10:19 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-22Client Sample ID: K12 (W25') (0-6')Matrix: SolidDate Collected: 11/08/12 13:55
Percent Solids: 51.8Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.060 0.060 0.018 mg/Kg ☼ 11/20/12 17:12 11/25/12 00:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.060 0.014 mg/Kg 11/20/12 17:12 11/25/12 00:49 1☼Acenaphthylene <0.060
0.060 0.014 mg/Kg 11/20/12 17:12 11/25/12 00:49 1☼Anthracene <0.060
0.060 0.013 mg/Kg 11/20/12 17:12 11/25/12 00:49 1☼Benzo[a]anthracene 0.038 J
0.060 0.011 mg/Kg 11/20/12 17:12 11/25/12 00:49 1☼Benzo[a]pyrene 0.039 J
0.060 0.012 mg/Kg 11/20/12 17:12 11/25/12 00:49 1☼Benzo[b]fluoranthene 0.064
0.060 0.020 mg/Kg 11/20/12 17:12 11/25/12 00:49 1☼Benzo[g,h,i]perylene 0.040 J
0.060 0.014 mg/Kg 11/20/12 17:12 11/25/12 00:49 1☼Benzo[k]fluoranthene 0.025 J
0.060 0.014 mg/Kg 11/20/12 17:12 11/25/12 00:49 1☼Chrysene 0.053 J
0.060 0.017 mg/Kg 11/20/12 17:12 11/25/12 00:49 1☼Dibenz(a,h)anthracene 0.020 J
0.060 0.025 mg/Kg 11/20/12 17:12 11/25/12 00:49 1☼Fluoranthene 0.078
0.060 0.014 mg/Kg 11/20/12 17:12 11/25/12 00:49 1☼Fluorene <0.060
0.060 0.020 mg/Kg 11/20/12 17:12 11/25/12 00:49 1☼Indeno[1,2,3-cd]pyrene 0.031 J
0.060 0.012 mg/Kg 11/20/12 17:12 11/25/12 00:49 1☼Naphthalene <0.060
0.060 0.025 mg/Kg 11/20/12 17:12 11/25/12 00:49 1☼Phenanthrene <0.060
0.060 0.022 mg/Kg 11/20/12 17:12 11/25/12 00:49 1☼Pyrene 0.058 J
2-Fluorobiphenyl 62 30 - 119 11/20/12 17:12 11/25/12 00:49 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 51 11/20/12 17:12 11/25/12 00:49 130 - 115
Terphenyl-d14 61 11/20/12 17:12 11/25/12 00:49 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 27 3.7 0.49 mg/Kg ☼ 11/14/12 08:30 11/15/12 17:57 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.9 0.40 mg/Kg 11/14/12 08:30 11/15/12 17:57 1☼Arsenic 22
1.9 0.22 mg/Kg 11/14/12 08:30 11/15/12 17:57 1☼Barium 62
0.37 0.092 mg/Kg 11/14/12 08:30 11/15/12 17:57 1☼Cadmium 0.37
1.9 0.31 mg/Kg 11/14/12 08:30 11/15/12 17:57 1☼Chromium 12
1.9 0.50 mg/Kg 11/14/12 08:30 11/15/12 17:57 1☼Copper 22
0.93 0.32 mg/Kg 11/14/12 08:30 11/15/12 17:57 1☼Lead 4200
1.9 0.53 mg/Kg 11/14/12 08:30 11/15/12 17:57 1☼Selenium <1.9
0.93 0.11 mg/Kg 11/14/12 08:30 11/15/12 17:57 1☼Silver <0.93
3.7 1.3 mg/Kg 11/14/12 08:30 11/15/12 17:57 1☼Zinc 62
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic 0.017 J 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 19:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/19/12 19:48 1Barium 0.40 J
0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 19:48 1Cadmium 0.0045 J
0.025 0.010 mg/L 11/19/12 08:00 11/19/12 19:48 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 19:48 1Lead 0.85 B
0.050 0.010 mg/L 11/19/12 08:00 11/19/12 19:48 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 19:48 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury <0.00020 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 10:12 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-22Client Sample ID: K12 (W25') (0-6')Matrix: SolidDate Collected: 11/08/12 13:55
Percent Solids: 51.8Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.046 0.031 0.012 mg/Kg ☼ 11/19/12 17:00 11/20/12 12:41 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.33 0.200 0.200 SU 11/15/12 10:21 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-23Client Sample ID: K12 (W25') (6-12')Matrix: SolidDate Collected: 11/08/12 13:56
Percent Solids: 54.3Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.060 0.060 0.018 mg/Kg ☼ 11/20/12 17:12 11/25/12 01:08 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.060 0.014 mg/Kg 11/20/12 17:12 11/25/12 01:08 1☼Acenaphthylene <0.060
0.060 0.014 mg/Kg 11/20/12 17:12 11/25/12 01:08 1☼Anthracene <0.060
0.060 0.013 mg/Kg 11/20/12 17:12 11/25/12 01:08 1☼Benzo[a]anthracene 0.026 J
0.060 0.011 mg/Kg 11/20/12 17:12 11/25/12 01:08 1☼Benzo[a]pyrene 0.079
0.060 0.012 mg/Kg 11/20/12 17:12 11/25/12 01:08 1☼Benzo[b]fluoranthene 0.027 J
0.060 0.020 mg/Kg 11/20/12 17:12 11/25/12 01:08 1☼Benzo[g,h,i]perylene 0.027 J
0.060 0.014 mg/Kg 11/20/12 17:12 11/25/12 01:08 1☼Benzo[k]fluoranthene 0.017 J
0.060 0.014 mg/Kg 11/20/12 17:12 11/25/12 01:08 1☼Chrysene 0.040 J
0.060 0.017 mg/Kg 11/20/12 17:12 11/25/12 01:08 1☼Dibenz(a,h)anthracene <0.060
0.060 0.025 mg/Kg 11/20/12 17:12 11/25/12 01:08 1☼Fluoranthene 0.044 J
0.060 0.014 mg/Kg 11/20/12 17:12 11/25/12 01:08 1☼Fluorene <0.060
0.060 0.020 mg/Kg 11/20/12 17:12 11/25/12 01:08 1☼Indeno[1,2,3-cd]pyrene <0.060
0.060 0.012 mg/Kg 11/20/12 17:12 11/25/12 01:08 1☼Naphthalene <0.060
0.060 0.025 mg/Kg 11/20/12 17:12 11/25/12 01:08 1☼Phenanthrene <0.060
0.060 0.022 mg/Kg 11/20/12 17:12 11/25/12 01:08 1☼Pyrene 0.039 J
2-Fluorobiphenyl 44 30 - 119 11/20/12 17:12 11/25/12 01:08 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 35 11/20/12 17:12 11/25/12 01:08 130 - 115
Terphenyl-d14 44 11/20/12 17:12 11/25/12 01:08 136 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 43 3.2 0.42 mg/Kg ☼ 11/14/12 08:30 11/15/12 18:01 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.6 0.34 mg/Kg 11/14/12 08:30 11/15/12 18:01 1☼Arsenic 32
1.6 0.19 mg/Kg 11/14/12 08:30 11/15/12 18:01 1☼Barium 87
0.32 0.078 mg/Kg 11/14/12 08:30 11/15/12 18:01 1☼Cadmium 0.59
1.6 0.26 mg/Kg 11/14/12 08:30 11/15/12 18:01 1☼Chromium 13
1.6 0.43 mg/Kg 11/14/12 08:30 11/15/12 18:01 1☼Copper 25
0.79 0.27 mg/Kg 11/14/12 08:30 11/15/12 18:01 1☼Lead 4600
1.6 0.45 mg/Kg 11/14/12 08:30 11/15/12 18:01 1☼Selenium 1.1 J
0.79 0.095 mg/Kg 11/14/12 08:30 11/15/12 18:01 1☼Silver <0.79
3.2 1.1 mg/Kg 11/14/12 08:30 11/15/12 18:01 1☼Zinc 82
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic 0.32 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 19:55 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/19/12 19:55 1Barium 0.60
0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 19:55 1Cadmium 0.0055
0.025 0.010 mg/L 11/19/12 08:00 11/19/12 19:55 1Chromium <0.025
0.075 0.050 mg/L 11/19/12 08:00 11/20/12 11:25 10Lead 73 B
0.050 0.010 mg/L 11/19/12 08:00 11/19/12 19:55 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 19:55 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury 0.000034 J B 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 10:14 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-23Client Sample ID: K12 (W25') (6-12')Matrix: SolidDate Collected: 11/08/12 13:56
Percent Solids: 54.3Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.042 0.028 0.011 mg/Kg ☼ 11/19/12 17:00 11/20/12 12:42 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.44 0.200 0.200 SU 11/15/12 10:24 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-24Client Sample ID: K12 (W25') (12-18')Matrix: SolidDate Collected: 11/08/12 13:57
Percent Solids: 64.3Date Received: 11/13/12 13:30
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
Acenaphthene <0.24 0.24 0.073 mg/Kg ☼ 11/20/12 17:12 11/25/12 01:28 5
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.24 0.056 mg/Kg 11/20/12 17:12 11/25/12 01:28 5☼Acenaphthylene <0.24
0.24 0.058 mg/Kg 11/20/12 17:12 11/25/12 01:28 5☼Anthracene <0.24
0.24 0.051 mg/Kg 11/20/12 17:12 11/25/12 01:28 5☼Benzo[a]anthracene <0.24
0.24 0.045 mg/Kg 11/20/12 17:12 11/25/12 01:28 5☼Benzo[a]pyrene <0.24
0.24 0.048 mg/Kg 11/20/12 17:12 11/25/12 01:28 5☼Benzo[b]fluoranthene 0.088 J
0.24 0.083 mg/Kg 11/20/12 17:12 11/25/12 01:28 5☼Benzo[g,h,i]perylene <0.24
0.24 0.059 mg/Kg 11/20/12 17:12 11/25/12 01:28 5☼Benzo[k]fluoranthene <0.24
0.24 0.055 mg/Kg 11/20/12 17:12 11/25/12 01:28 5☼Chrysene 0.11 J
0.24 0.069 mg/Kg 11/20/12 17:12 11/25/12 01:28 5☼Dibenz(a,h)anthracene <0.24
0.24 0.10 mg/Kg 11/20/12 17:12 11/25/12 01:28 5☼Fluoranthene 0.19 J
0.24 0.056 mg/Kg 11/20/12 17:12 11/25/12 01:28 5☼Fluorene <0.24
0.24 0.083 mg/Kg 11/20/12 17:12 11/25/12 01:28 5☼Indeno[1,2,3-cd]pyrene <0.24
0.24 0.047 mg/Kg 11/20/12 17:12 11/25/12 01:28 5☼Naphthalene <0.24
0.24 0.10 mg/Kg 11/20/12 17:12 11/25/12 01:28 5☼Phenanthrene <0.24
0.24 0.089 mg/Kg 11/20/12 17:12 11/25/12 01:28 5☼Pyrene 0.16 J
2-Fluorobiphenyl 62 30 - 119 11/20/12 17:12 11/25/12 01:28 5
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Nitrobenzene-d5 50 11/20/12 17:12 11/25/12 01:28 530 - 115
Terphenyl-d14 69 11/20/12 17:12 11/25/12 01:28 536 - 134
Method: 6010B - Metals (ICP)RL MDL
Antimony 2.4 J 2.6 0.35 mg/Kg ☼ 11/14/12 08:30 11/15/12 18:05 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.3 0.29 mg/Kg 11/14/12 08:30 11/15/12 18:05 1☼Arsenic 8.0
1.3 0.16 mg/Kg 11/14/12 08:30 11/15/12 18:05 1☼Barium 82
0.26 0.065 mg/Kg 11/14/12 08:30 11/15/12 18:05 1☼Cadmium 0.35
1.3 0.22 mg/Kg 11/14/12 08:30 11/15/12 18:05 1☼Chromium 15
1.3 0.36 mg/Kg 11/14/12 08:30 11/15/12 18:05 1☼Copper 21
0.66 0.23 mg/Kg 11/14/12 08:30 11/15/12 18:05 1☼Lead 530
1.3 0.38 mg/Kg 11/14/12 08:30 11/15/12 18:05 1☼Selenium 0.57 J
0.66 0.079 mg/Kg 11/14/12 08:30 11/15/12 18:05 1☼Silver <0.66
2.6 0.91 mg/Kg 11/14/12 08:30 11/15/12 18:05 1☼Zinc 66
Method: 6010B - Metals (ICP) - TCLPRL MDL
Arsenic 0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 20:40 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.50 0.010 mg/L 11/19/12 08:00 11/19/12 20:40 1Barium 0.84
0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 20:40 1Cadmium 0.0042 J
0.025 0.010 mg/L 11/19/12 08:00 11/19/12 20:40 1Chromium <0.025
0.0075 0.0050 mg/L 11/19/12 08:00 11/19/12 20:40 1Lead 8.6 B
0.050 0.010 mg/L 11/19/12 08:00 11/19/12 20:40 1Selenium <0.050
0.025 0.0050 mg/L 11/19/12 08:00 11/19/12 20:40 1Silver <0.025
Method: 7470A - Mercury (CVAA) - TCLPRL MDL
Mercury <0.00020 ^ 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 10:19 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Client Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Lab Sample ID: 500-52298-24Client Sample ID: K12 (W25') (12-18')Matrix: SolidDate Collected: 11/08/12 13:57
Percent Solids: 64.3Date Received: 11/13/12 13:30
Method: 7471A - Mercury (CVAA)RL MDL
Mercury 0.037 0.022 0.0086 mg/Kg ☼ 11/19/12 17:00 11/20/12 12:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
pH 7.45 0.200 0.200 SU 11/15/12 10:26 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Chicago
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Definitions/GlossaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Qualifiers
GC/MS Semi VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
F MS or MSD exceeds the control limits
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
* LCS or LCSD exceeds the control limits
F MS or MSD exceeds the control limits
F RPD of the MS and MSD exceeds the control limits
B Compound was found in the blank and sample.
4 MS, MSD: The analyte present in the original sample is 4 times greater than the matrix spike concentration; therefore, control limits are not
applicable.
^ ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard: Instrument related QC exceeds the control limits.
Glossary
These commonly used abbreviations may or may not be present in this report.
☼ Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
DL, RA, RE, IN Indicates a Dilution, Reanalysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
EDL Estimated Detection Limit
EPA United States Environmental Protection Agency
MDA Minimum detectable activity
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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QC Association SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
GC/MS Semi VOA
Prep Batch: 170477
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3541500-52298-1 F20 (0-6") Total/NA
Solid 3541500-52298-2 F20 (6-12") Total/NA
Solid 3541500-52298-3 F20 (12-18") Total/NA
Solid 3541500-52298-4 H20 (E20') (0-6") Total/NA
Solid 3541500-52298-5 H20 (E20') (6-12") Total/NA
Solid 3541500-52298-6 H20 (E20') (12-18") Total/NA
Solid 3541500-52298-7 K10 (W25') (0-6") Total/NA
Solid 3541500-52298-8 K10 (W25') (6-12") Total/NA
Solid 3541500-52298-9 K10 (W25') (12-18") Total/NA
Solid 3541500-52298-10 H10 (N30') (0-6") Total/NA
Solid 3541500-52298-10 MS H10 (N30') (0-6") Total/NA
Solid 3541500-52298-10 MSD H10 (N30') (0-6") Total/NA
Solid 3541500-52298-11 H10 (N30') (6-12") Total/NA
Solid 3541500-52298-12 H10 (N30') (12-18") Total/NA
Solid 3541500-52298-13 J8 (0-6") Total/NA
Solid 3541500-52298-14 J8 (6-12") Total/NA
Solid 3541500-52298-15 J8 (12-18") Total/NA
Solid 3541500-52298-16 L6 (W20') (0-6") Total/NA
Solid 3541500-52298-17 L6 (W20') (6-12") Total/NA
Solid 3541500-52298-18 L6 (W20') (12-18") Total/NA
Solid 3541500-52298-19 J17 (N30;W20') (0-6") Total/NA
Solid 3541500-52298-20 J17 (N30;W20') (6-12") Total/NA
Solid 3541LCS 500-170477/2-A Lab Control Sample Total/NA
Solid 3541MB 500-170477/1-A Method Blank Total/NA
Prep Batch: 170478
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3541500-52298-21 J17 (N30;W20') (12-18") Total/NA
Solid 3541500-52298-22 K12 (W25') (0-6') Total/NA
Solid 3541500-52298-23 K12 (W25') (6-12') Total/NA
Solid 3541500-52298-24 K12 (W25') (12-18') Total/NA
Solid 3541LCS 500-170478/2-A Lab Control Sample Total/NA
Solid 3541MB 500-170478/1-A Method Blank Total/NA
Analysis Batch: 170527
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270C 170478LCS 500-170478/2-A Lab Control Sample Total/NA
Analysis Batch: 170539
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270C 170478MB 500-170478/1-A Method Blank Total/NA
Analysis Batch: 170779
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270C 170477LCS 500-170477/2-A Lab Control Sample Total/NA
Solid 8270C 170477MB 500-170477/1-A Method Blank Total/NA
Analysis Batch: 170783
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270C 170477500-52298-1 F20 (0-6") Total/NA
Solid 8270C 170477500-52298-2 F20 (6-12") Total/NA
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QC Association SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
GC/MS Semi VOA (Continued)
Analysis Batch: 170783 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270C 170477500-52298-3 F20 (12-18") Total/NA
Solid 8270C 170477500-52298-4 H20 (E20') (0-6") Total/NA
Solid 8270C 170477500-52298-5 H20 (E20') (6-12") Total/NA
Solid 8270C 170477500-52298-6 H20 (E20') (12-18") Total/NA
Solid 8270C 170477500-52298-7 K10 (W25') (0-6") Total/NA
Solid 8270C 170477500-52298-8 K10 (W25') (6-12") Total/NA
Solid 8270C 170477500-52298-9 K10 (W25') (12-18") Total/NA
Solid 8270C 170477500-52298-10 H10 (N30') (0-6") Total/NA
Solid 8270C 170477500-52298-10 MS H10 (N30') (0-6") Total/NA
Solid 8270C 170477500-52298-10 MSD H10 (N30') (0-6") Total/NA
Solid 8270C 170477500-52298-11 H10 (N30') (6-12") Total/NA
Solid 8270C 170477500-52298-12 H10 (N30') (12-18") Total/NA
Solid 8270C 170477500-52298-13 J8 (0-6") Total/NA
Solid 8270C 170477500-52298-14 J8 (6-12") Total/NA
Solid 8270C 170477500-52298-15 J8 (12-18") Total/NA
Solid 8270C 170477500-52298-16 L6 (W20') (0-6") Total/NA
Solid 8270C 170477500-52298-17 L6 (W20') (6-12") Total/NA
Solid 8270C 170477500-52298-18 L6 (W20') (12-18") Total/NA
Solid 8270C 170477500-52298-19 J17 (N30;W20') (0-6") Total/NA
Solid 8270C 170477500-52298-20 J17 (N30;W20') (6-12") Total/NA
Solid 8270C 170478500-52298-21 J17 (N30;W20') (12-18") Total/NA
Solid 8270C 170478500-52298-22 K12 (W25') (0-6') Total/NA
Solid 8270C 170478500-52298-23 K12 (W25') (6-12') Total/NA
Solid 8270C 170478500-52298-24 K12 (W25') (12-18') Total/NA
Metals
Prep Batch: 169568
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3050B500-52298-1 F20 (0-6") Total/NA
Solid 3050B500-52298-1 DU F20 (0-6") Total/NA
Solid 3050B500-52298-1 MS F20 (0-6") Total/NA
Solid 3050B500-52298-1 MSD F20 (0-6") Total/NA
Solid 3050B500-52298-2 F20 (6-12") Total/NA
Solid 3050B500-52298-3 F20 (12-18") Total/NA
Solid 3050B500-52298-4 H20 (E20') (0-6") Total/NA
Solid 3050B500-52298-5 H20 (E20') (6-12") Total/NA
Solid 3050B500-52298-6 H20 (E20') (12-18") Total/NA
Solid 3050B500-52298-7 K10 (W25') (0-6") Total/NA
Solid 3050B500-52298-8 K10 (W25') (6-12") Total/NA
Solid 3050B500-52298-9 K10 (W25') (12-18") Total/NA
Solid 3050B500-52298-10 H10 (N30') (0-6") Total/NA
Solid 3050B500-52298-11 H10 (N30') (6-12") Total/NA
Solid 3050B500-52298-12 H10 (N30') (12-18") Total/NA
Solid 3050B500-52298-13 J8 (0-6") Total/NA
Solid 3050B500-52298-14 J8 (6-12") Total/NA
Solid 3050B500-52298-15 J8 (12-18") Total/NA
Solid 3050B500-52298-16 L6 (W20') (0-6") Total/NA
Solid 3050B500-52298-17 L6 (W20') (6-12") Total/NA
Solid 3050B500-52298-18 L6 (W20') (12-18") Total/NA
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QC Association SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Metals (Continued)
Prep Batch: 169568 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3050B500-52298-19 J17 (N30;W20') (0-6") Total/NA
Solid 3050B500-52298-20 J17 (N30;W20') (6-12") Total/NA
Solid 3050BLCS 500-169568/2-A Lab Control Sample Total/NA
Solid 3050BMB 500-169568/1-A Method Blank Total/NA
Prep Batch: 169626
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3050B500-52298-21 J17 (N30;W20') (12-18") Total/NA
Solid 3050B500-52298-22 K12 (W25') (0-6') Total/NA
Solid 3050B500-52298-23 K12 (W25') (6-12') Total/NA
Solid 3050B500-52298-24 K12 (W25') (12-18') Total/NA
Solid 3050BLCS 500-169626/2-A Lab Control Sample Total/NA
Solid 3050BMB 500-169626/1-A Method Blank Total/NA
Analysis Batch: 169928
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010B 169626500-52298-21 J17 (N30;W20') (12-18") Total/NA
Solid 6010B 169626500-52298-22 K12 (W25') (0-6') Total/NA
Solid 6010B 169626500-52298-23 K12 (W25') (6-12') Total/NA
Solid 6010B 169626500-52298-24 K12 (W25') (12-18') Total/NA
Solid 6010B 169626LCS 500-169626/2-A Lab Control Sample Total/NA
Solid 6010B 169626MB 500-169626/1-A Method Blank Total/NA
Leach Batch: 170018
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 1311500-52298-1 F20 (0-6") TCLP
Solid 1311500-52298-1 DU F20 (0-6") TCLP
Solid 1311500-52298-1 MS F20 (0-6") TCLP
Solid 1311500-52298-2 F20 (6-12") TCLP
Solid 1311500-52298-3 F20 (12-18") TCLP
Solid 1311500-52298-4 H20 (E20') (0-6") TCLP
Solid 1311500-52298-4 DU H20 (E20') (0-6") TCLP
Solid 1311500-52298-4 MS H20 (E20') (0-6") TCLP
Solid 1311500-52298-5 H20 (E20') (6-12") TCLP
Solid 1311500-52298-6 H20 (E20') (12-18") TCLP
Solid 1311500-52298-7 K10 (W25') (0-6") TCLP
Solid 1311500-52298-8 K10 (W25') (6-12") TCLP
Solid 1311500-52298-9 K10 (W25') (12-18") TCLP
Solid 1311500-52298-10 H10 (N30') (0-6") TCLP
Solid 1311500-52298-11 H10 (N30') (6-12") TCLP
Solid 1311500-52298-12 H10 (N30') (12-18") TCLP
Solid 1311500-52298-13 J8 (0-6") TCLP
Solid 1311500-52298-14 J8 (6-12") TCLP
Solid 1311500-52298-15 J8 (12-18") TCLP
Solid 1311500-52298-16 L6 (W20') (0-6") TCLP
Solid 1311500-52298-17 L6 (W20') (6-12") TCLP
Solid 1311500-52298-18 L6 (W20') (12-18") TCLP
Solid 1311500-52298-19 J17 (N30;W20') (0-6") TCLP
Solid 1311500-52298-20 J17 (N30;W20') (6-12") TCLP
Solid 1311LB 500-170018/1-B LB Method Blank TCLP
Solid 1311LB 500-170018/1-C LB Method Blank TCLP
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QC Association SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Metals (Continued)
Leach Batch: 170019
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 1311500-52298-21 J17 (N30;W20') (12-18") TCLP
Solid 1311500-52298-21 DU J17 (N30;W20') (12-18") TCLP
Solid 1311500-52298-21 MS J17 (N30;W20') (12-18") TCLP
Solid 1311500-52298-22 K12 (W25') (0-6') TCLP
Solid 1311500-52298-23 K12 (W25') (6-12') TCLP
Solid 1311500-52298-23 DU K12 (W25') (6-12') TCLP
Solid 1311500-52298-23 MS K12 (W25') (6-12') TCLP
Solid 1311500-52298-24 K12 (W25') (12-18') TCLP
Solid 1311LB 500-170019/1-B LB Method Blank TCLP
Solid 1311LB 500-170019/1-E LB Method Blank TCLP
Prep Batch: 170225
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3010A 170018500-52298-1 F20 (0-6") TCLP
Solid 3010A 170018500-52298-2 F20 (6-12") TCLP
Solid 3010A 170018500-52298-3 F20 (12-18") TCLP
Solid 3010A 170018500-52298-4 H20 (E20') (0-6") TCLP
Solid 3010A 170018500-52298-4 DU H20 (E20') (0-6") TCLP
Solid 3010A 170018500-52298-4 MS H20 (E20') (0-6") TCLP
Solid 3010A 170018500-52298-5 H20 (E20') (6-12") TCLP
Solid 3010A 170018500-52298-6 H20 (E20') (12-18") TCLP
Solid 3010A 170018500-52298-7 K10 (W25') (0-6") TCLP
Solid 3010A 170018500-52298-8 K10 (W25') (6-12") TCLP
Solid 3010A 170018500-52298-9 K10 (W25') (12-18") TCLP
Solid 3010A 170018500-52298-10 H10 (N30') (0-6") TCLP
Solid 3010A 170018500-52298-11 H10 (N30') (6-12") TCLP
Solid 3010A 170018500-52298-12 H10 (N30') (12-18") TCLP
Solid 3010A 170018500-52298-13 J8 (0-6") TCLP
Solid 3010A 170018500-52298-14 J8 (6-12") TCLP
Solid 3010A 170018500-52298-15 J8 (12-18") TCLP
Solid 3010A 170018500-52298-16 L6 (W20') (0-6") TCLP
Solid 3010A 170018500-52298-17 L6 (W20') (6-12") TCLP
Solid 3010A 170018500-52298-18 L6 (W20') (12-18") TCLP
Solid 3010A 170018500-52298-19 J17 (N30;W20') (0-6") TCLP
Solid 3010A 170018500-52298-20 J17 (N30;W20') (6-12") TCLP
Solid 3010A 170018LB 500-170018/1-B LB Method Blank TCLP
Solid 3010ALCS 500-170225/2-A Lab Control Sample Total/NA
Prep Batch: 170228
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3010A 170019500-52298-21 J17 (N30;W20') (12-18") TCLP
Solid 3010A 170019500-52298-22 K12 (W25') (0-6') TCLP
Solid 3010A 170019500-52298-23 K12 (W25') (6-12') TCLP
Solid 3010A 170019500-52298-23 DU K12 (W25') (6-12') TCLP
Solid 3010A 170019500-52298-23 MS K12 (W25') (6-12') TCLP
Solid 3010A 170019500-52298-24 K12 (W25') (12-18') TCLP
Solid 3010A 170019LB 500-170019/1-B LB Method Blank TCLP
Solid 3010ALCS 500-170228/3-A Lab Control Sample Total/NA
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QC Association SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Metals (Continued)
Prep Batch: 170250
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471A500-52298-1 F20 (0-6") Total/NA
Solid 7471A500-52298-2 F20 (6-12") Total/NA
Solid 7471A500-52298-3 F20 (12-18") Total/NA
Solid 7471A500-52298-3 DU F20 (12-18") Total/NA
Solid 7471A500-52298-3 MS F20 (12-18") Total/NA
Solid 7471A500-52298-3 MSD F20 (12-18") Total/NA
Solid 7471A500-52298-4 H20 (E20') (0-6") Total/NA
Solid 7471A500-52298-5 H20 (E20') (6-12") Total/NA
Solid 7471A500-52298-6 H20 (E20') (12-18") Total/NA
Solid 7471A500-52298-7 K10 (W25') (0-6") Total/NA
Solid 7471A500-52298-8 K10 (W25') (6-12") Total/NA
Solid 7471A500-52298-9 K10 (W25') (12-18") Total/NA
Solid 7471A500-52298-10 H10 (N30') (0-6") Total/NA
Solid 7471A500-52298-11 H10 (N30') (6-12") Total/NA
Solid 7471A500-52298-12 H10 (N30') (12-18") Total/NA
Solid 7471A500-52298-13 J8 (0-6") Total/NA
Solid 7471A500-52298-14 J8 (6-12") Total/NA
Solid 7471A500-52298-15 J8 (12-18") Total/NA
Solid 7471A500-52298-16 L6 (W20') (0-6") Total/NA
Solid 7471A500-52298-17 L6 (W20') (6-12") Total/NA
Solid 7471A500-52298-18 L6 (W20') (12-18") Total/NA
Solid 7471A500-52298-19 J17 (N30;W20') (0-6") Total/NA
Solid 7471A500-52298-20 J17 (N30;W20') (6-12") Total/NA
Solid 7471ALCS 500-170250/8-A Lab Control Sample Total/NA
Solid 7471AMB 500-170250/7-A Method Blank Total/NA
Prep Batch: 170259
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471A500-52298-21 J17 (N30;W20') (12-18") Total/NA
Solid 7471A500-52298-22 K12 (W25') (0-6') Total/NA
Solid 7471A500-52298-23 K12 (W25') (6-12') Total/NA
Solid 7471A500-52298-24 K12 (W25') (12-18') Total/NA
Solid 7471ALCS 500-170259/8-A Lab Control Sample Total/NA
Solid 7471AMB 500-170259/7-A Method Blank Total/NA
Prep Batch: 170293
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7470A 170019500-52298-21 J17 (N30;W20') (12-18") TCLP
Solid 7470A 170019500-52298-21 DU J17 (N30;W20') (12-18") TCLP
Solid 7470A 170019500-52298-21 MS J17 (N30;W20') (12-18") TCLP
Solid 7470A 170019500-52298-22 K12 (W25') (0-6') TCLP
Solid 7470A 170019500-52298-23 K12 (W25') (6-12') TCLP
Solid 7470A 170019500-52298-24 K12 (W25') (12-18') TCLP
Solid 7470A 170019LB 500-170019/1-E LB Method Blank TCLP
Solid 7470ALCS 500-170293/8-A Lab Control Sample Total/NA
Solid 7470AMB 500-170293/7-A Method Blank Total/NA
Prep Batch: 170296
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7470A 170018500-52298-1 F20 (0-6") TCLP
Solid 7470A 170018500-52298-1 DU F20 (0-6") TCLP
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QC Association SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Metals (Continued)
Prep Batch: 170296 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7470A 170018500-52298-1 MS F20 (0-6") TCLP
Solid 7470A 170018500-52298-2 F20 (6-12") TCLP
Solid 7470A 170018500-52298-3 F20 (12-18") TCLP
Solid 7470A 170018500-52298-4 H20 (E20') (0-6") TCLP
Solid 7470A 170018500-52298-5 H20 (E20') (6-12") TCLP
Solid 7470A 170018500-52298-6 H20 (E20') (12-18") TCLP
Solid 7470A 170018500-52298-7 K10 (W25') (0-6") TCLP
Solid 7470A 170018500-52298-8 K10 (W25') (6-12") TCLP
Solid 7470A 170018500-52298-9 K10 (W25') (12-18") TCLP
Solid 7470A 170018500-52298-10 H10 (N30') (0-6") TCLP
Solid 7470A 170018500-52298-11 H10 (N30') (6-12") TCLP
Solid 7470A 170018500-52298-12 H10 (N30') (12-18") TCLP
Solid 7470A 170018500-52298-13 J8 (0-6") TCLP
Solid 7470A 170018500-52298-14 J8 (6-12") TCLP
Solid 7470A 170018500-52298-15 J8 (12-18") TCLP
Solid 7470A 170018500-52298-16 L6 (W20') (0-6") TCLP
Solid 7470A 170018500-52298-17 L6 (W20') (6-12") TCLP
Solid 7470A 170018500-52298-18 L6 (W20') (12-18") TCLP
Solid 7470A 170018500-52298-19 J17 (N30;W20') (0-6") TCLP
Solid 7470A 170018500-52298-20 J17 (N30;W20') (6-12") TCLP
Solid 7470A 170018LB 500-170018/1-C LB Method Blank TCLP
Solid 7470ALCS 500-170296/8-A Lab Control Sample Total/NA
Solid 7470AMB 500-170296/7-A Method Blank Total/NA
Analysis Batch: 170334
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010B 170225500-52298-1 F20 (0-6") TCLP
Solid 6010B 170225500-52298-2 F20 (6-12") TCLP
Solid 6010B 170225500-52298-3 F20 (12-18") TCLP
Solid 6010B 170225500-52298-4 H20 (E20') (0-6") TCLP
Solid 6010B 170225500-52298-4 DU H20 (E20') (0-6") TCLP
Solid 6010B 170225500-52298-4 MS H20 (E20') (0-6") TCLP
Solid 6010B 170225500-52298-5 H20 (E20') (6-12") TCLP
Solid 6010B 170225500-52298-6 H20 (E20') (12-18") TCLP
Solid 6010B 170225500-52298-7 K10 (W25') (0-6") TCLP
Solid 6010B 170225500-52298-8 K10 (W25') (6-12") TCLP
Solid 6010B 170225500-52298-9 K10 (W25') (12-18") TCLP
Solid 6010B 170225500-52298-10 H10 (N30') (0-6") TCLP
Solid 6010B 170225500-52298-11 H10 (N30') (6-12") TCLP
Solid 6010B 170225500-52298-12 H10 (N30') (12-18") TCLP
Solid 6010B 170225500-52298-13 J8 (0-6") TCLP
Solid 6010B 170225500-52298-14 J8 (6-12") TCLP
Solid 6010B 170225500-52298-15 J8 (12-18") TCLP
Solid 6010B 170225500-52298-16 L6 (W20') (0-6") TCLP
Solid 6010B 170225500-52298-17 L6 (W20') (6-12") TCLP
Solid 6010B 170225500-52298-18 L6 (W20') (12-18") TCLP
Solid 6010B 170225500-52298-19 J17 (N30;W20') (0-6") TCLP
Solid 6010B 170225500-52298-20 J17 (N30;W20') (6-12") TCLP
Solid 6010B 170228500-52298-21 J17 (N30;W20') (12-18") TCLP
Solid 6010B 170228500-52298-22 K12 (W25') (0-6') TCLP
Solid 6010B 170228500-52298-23 K12 (W25') (6-12') TCLP
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QC Association SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Metals (Continued)
Analysis Batch: 170334 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010B 170228500-52298-23 DU K12 (W25') (6-12') TCLP
Solid 6010B 170228500-52298-23 MS K12 (W25') (6-12') TCLP
Solid 6010B 170228500-52298-24 K12 (W25') (12-18') TCLP
Solid 6010B 170225LB 500-170018/1-B LB Method Blank TCLP
Solid 6010B 170228LB 500-170019/1-B LB Method Blank TCLP
Solid 6010B 170225LCS 500-170225/2-A Lab Control Sample Total/NA
Solid 6010B 170228LCS 500-170228/3-A Lab Control Sample Total/NA
Analysis Batch: 170336
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010B 169568500-52298-1 F20 (0-6") Total/NA
Solid 6010B 169568500-52298-1 DU F20 (0-6") Total/NA
Solid 6010B 169568500-52298-1 MS F20 (0-6") Total/NA
Solid 6010B 169568500-52298-1 MSD F20 (0-6") Total/NA
Solid 6010B 169568500-52298-2 F20 (6-12") Total/NA
Solid 6010B 169568500-52298-3 F20 (12-18") Total/NA
Solid 6010B 169568500-52298-4 H20 (E20') (0-6") Total/NA
Solid 6010B 169568500-52298-5 H20 (E20') (6-12") Total/NA
Solid 6010B 169568500-52298-6 H20 (E20') (12-18") Total/NA
Solid 6010B 169568500-52298-7 K10 (W25') (0-6") Total/NA
Solid 6010B 169568500-52298-8 K10 (W25') (6-12") Total/NA
Solid 6010B 169568500-52298-9 K10 (W25') (12-18") Total/NA
Solid 6010B 169568500-52298-10 H10 (N30') (0-6") Total/NA
Solid 6010B 169568500-52298-11 H10 (N30') (6-12") Total/NA
Solid 6010B 169568500-52298-12 H10 (N30') (12-18") Total/NA
Solid 6010B 169568500-52298-13 J8 (0-6") Total/NA
Solid 6010B 169568500-52298-14 J8 (6-12") Total/NA
Solid 6010B 169568500-52298-15 J8 (12-18") Total/NA
Solid 6010B 169568500-52298-16 L6 (W20') (0-6") Total/NA
Solid 6010B 169568500-52298-17 L6 (W20') (6-12") Total/NA
Solid 6010B 169568500-52298-18 L6 (W20') (12-18") Total/NA
Solid 6010B 169568500-52298-19 J17 (N30;W20') (0-6") Total/NA
Solid 6010B 169568500-52298-20 J17 (N30;W20') (6-12") Total/NA
Solid 6010B 169568LCS 500-169568/2-A Lab Control Sample Total/NA
Solid 6010B 169568MB 500-169568/1-A Method Blank Total/NA
Analysis Batch: 170422
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010B 169568500-52298-7 K10 (W25') (0-6") Total/NA
Solid 6010B 169568500-52298-20 J17 (N30;W20') (6-12") Total/NA
Solid 6010B 170228500-52298-23 K12 (W25') (6-12') TCLP
Solid 6010B 170228500-52298-23 DU K12 (W25') (6-12') TCLP
Solid 6010B 170228500-52298-23 MS K12 (W25') (6-12') TCLP
Analysis Batch: 170438
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7470A 170296500-52298-1 F20 (0-6") TCLP
Solid 7470A 170296500-52298-1 DU F20 (0-6") TCLP
Solid 7470A 170296500-52298-1 MS F20 (0-6") TCLP
Solid 7470A 170296500-52298-2 F20 (6-12") TCLP
Solid 7470A 170296500-52298-3 F20 (12-18") TCLP
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QC Association SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Metals (Continued)
Analysis Batch: 170438 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7470A 170296500-52298-4 H20 (E20') (0-6") TCLP
Solid 7470A 170296500-52298-5 H20 (E20') (6-12") TCLP
Solid 7470A 170296500-52298-6 H20 (E20') (12-18") TCLP
Solid 7470A 170296500-52298-7 K10 (W25') (0-6") TCLP
Solid 7470A 170296500-52298-8 K10 (W25') (6-12") TCLP
Solid 7470A 170296500-52298-9 K10 (W25') (12-18") TCLP
Solid 7470A 170296500-52298-10 H10 (N30') (0-6") TCLP
Solid 7470A 170296500-52298-11 H10 (N30') (6-12") TCLP
Solid 7470A 170296500-52298-12 H10 (N30') (12-18") TCLP
Solid 7470A 170296500-52298-13 J8 (0-6") TCLP
Solid 7470A 170296500-52298-14 J8 (6-12") TCLP
Solid 7470A 170296500-52298-15 J8 (12-18") TCLP
Solid 7470A 170296500-52298-16 L6 (W20') (0-6") TCLP
Solid 7470A 170296500-52298-17 L6 (W20') (6-12") TCLP
Solid 7470A 170296500-52298-18 L6 (W20') (12-18") TCLP
Solid 7470A 170296500-52298-19 J17 (N30;W20') (0-6") TCLP
Solid 7470A 170296500-52298-20 J17 (N30;W20') (6-12") TCLP
Solid 7470A 170293500-52298-21 J17 (N30;W20') (12-18") TCLP
Solid 7470A 170293500-52298-21 DU J17 (N30;W20') (12-18") TCLP
Solid 7470A 170293500-52298-21 MS J17 (N30;W20') (12-18") TCLP
Solid 7470A 170293500-52298-22 K12 (W25') (0-6') TCLP
Solid 7470A 170293500-52298-23 K12 (W25') (6-12') TCLP
Solid 7470A 170293500-52298-24 K12 (W25') (12-18') TCLP
Solid 7470A 170296LB 500-170018/1-C LB Method Blank TCLP
Solid 7470A 170293LB 500-170019/1-E LB Method Blank TCLP
Solid 7470A 170293LCS 500-170293/8-A Lab Control Sample Total/NA
Solid 7470A 170296LCS 500-170296/8-A Lab Control Sample Total/NA
Solid 7470A 170293MB 500-170293/7-A Method Blank Total/NA
Solid 7470A 170296MB 500-170296/7-A Method Blank Total/NA
Analysis Batch: 170439
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471A 170250500-52298-1 F20 (0-6") Total/NA
Solid 7471A 170250500-52298-2 F20 (6-12") Total/NA
Solid 7471A 170250500-52298-3 F20 (12-18") Total/NA
Solid 7471A 170250500-52298-3 DU F20 (12-18") Total/NA
Solid 7471A 170250500-52298-3 MS F20 (12-18") Total/NA
Solid 7471A 170250500-52298-3 MSD F20 (12-18") Total/NA
Solid 7471A 170250500-52298-4 H20 (E20') (0-6") Total/NA
Solid 7471A 170250500-52298-5 H20 (E20') (6-12") Total/NA
Solid 7471A 170250500-52298-6 H20 (E20') (12-18") Total/NA
Solid 7471A 170250500-52298-7 K10 (W25') (0-6") Total/NA
Solid 7471A 170250500-52298-8 K10 (W25') (6-12") Total/NA
Solid 7471A 170250500-52298-9 K10 (W25') (12-18") Total/NA
Solid 7471A 170250500-52298-10 H10 (N30') (0-6") Total/NA
Solid 7471A 170250500-52298-11 H10 (N30') (6-12") Total/NA
Solid 7471A 170250500-52298-12 H10 (N30') (12-18") Total/NA
Solid 7471A 170250500-52298-13 J8 (0-6") Total/NA
Solid 7471A 170250500-52298-14 J8 (6-12") Total/NA
Solid 7471A 170250500-52298-15 J8 (12-18") Total/NA
Solid 7471A 170250500-52298-16 L6 (W20') (0-6") Total/NA
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QC Association SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Metals (Continued)
Analysis Batch: 170439 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471A 170250500-52298-17 L6 (W20') (6-12") Total/NA
Solid 7471A 170250500-52298-18 L6 (W20') (12-18") Total/NA
Solid 7471A 170250500-52298-19 J17 (N30;W20') (0-6") Total/NA
Solid 7471A 170250500-52298-20 J17 (N30;W20') (6-12") Total/NA
Solid 7471A 170259500-52298-21 J17 (N30;W20') (12-18") Total/NA
Solid 7471A 170259500-52298-22 K12 (W25') (0-6') Total/NA
Solid 7471A 170259500-52298-23 K12 (W25') (6-12') Total/NA
Solid 7471A 170259500-52298-24 K12 (W25') (12-18') Total/NA
Solid 7471A 170250LCS 500-170250/8-A Lab Control Sample Total/NA
Solid 7471A 170259LCS 500-170259/8-A Lab Control Sample Total/NA
Solid 7471A 170250MB 500-170250/7-A Method Blank Total/NA
Solid 7471A 170259MB 500-170259/7-A Method Blank Total/NA
General Chemistry
Analysis Batch: 169544
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture500-52298-1 F20 (0-6") Total/NA
Solid Moisture500-52298-1 DU F20 (0-6") Total/NA
Solid Moisture500-52298-2 F20 (6-12") Total/NA
Solid Moisture500-52298-3 F20 (12-18") Total/NA
Solid Moisture500-52298-4 H20 (E20') (0-6") Total/NA
Solid Moisture500-52298-5 H20 (E20') (6-12") Total/NA
Solid Moisture500-52298-6 H20 (E20') (12-18") Total/NA
Solid Moisture500-52298-7 K10 (W25') (0-6") Total/NA
Solid Moisture500-52298-8 K10 (W25') (6-12") Total/NA
Solid Moisture500-52298-9 K10 (W25') (12-18") Total/NA
Solid Moisture500-52298-10 H10 (N30') (0-6") Total/NA
Solid Moisture500-52298-11 H10 (N30') (6-12") Total/NA
Solid Moisture500-52298-12 H10 (N30') (12-18") Total/NA
Solid Moisture500-52298-13 J8 (0-6") Total/NA
Solid Moisture500-52298-14 J8 (6-12") Total/NA
Solid Moisture500-52298-15 J8 (12-18") Total/NA
Solid Moisture500-52298-16 L6 (W20') (0-6") Total/NA
Solid Moisture500-52298-17 L6 (W20') (6-12") Total/NA
Solid Moisture500-52298-18 L6 (W20') (12-18") Total/NA
Solid Moisture500-52298-19 J17 (N30;W20') (0-6") Total/NA
Solid Moisture500-52298-20 J17 (N30;W20') (6-12") Total/NA
Solid Moisture500-52298-21 J17 (N30;W20') (12-18") Total/NA
Solid Moisture500-52298-22 K12 (W25') (0-6') Total/NA
Solid Moisture500-52298-23 K12 (W25') (6-12') Total/NA
Solid Moisture500-52298-24 K12 (W25') (12-18') Total/NA
Analysis Batch: 169904
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9045C500-52298-1 F20 (0-6") Total/NA
Solid 9045C500-52298-2 F20 (6-12") Total/NA
Solid 9045C500-52298-3 F20 (12-18") Total/NA
Solid 9045C500-52298-4 H20 (E20') (0-6") Total/NA
Solid 9045C500-52298-5 H20 (E20') (6-12") Total/NA
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QC Association SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
General Chemistry (Continued)
Analysis Batch: 169904 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9045C500-52298-6 H20 (E20') (12-18") Total/NA
Solid 9045C500-52298-7 K10 (W25') (0-6") Total/NA
Solid 9045C500-52298-8 K10 (W25') (6-12") Total/NA
Solid 9045C500-52298-8 DU K10 (W25') (6-12") Total/NA
Solid 9045C500-52298-9 K10 (W25') (12-18") Total/NA
Solid 9045C500-52298-10 H10 (N30') (0-6") Total/NA
Solid 9045C500-52298-11 H10 (N30') (6-12") Total/NA
Solid 9045C500-52298-12 H10 (N30') (12-18") Total/NA
Solid 9045C500-52298-13 J8 (0-6") Total/NA
Solid 9045C500-52298-14 J8 (6-12") Total/NA
Solid 9045C500-52298-15 J8 (12-18") Total/NA
Solid 9045C500-52298-16 L6 (W20') (0-6") Total/NA
Solid 9045C500-52298-17 L6 (W20') (6-12") Total/NA
Solid 9045C500-52298-18 L6 (W20') (12-18") Total/NA
Solid 9045C500-52298-19 J17 (N30;W20') (0-6") Total/NA
Solid 9045C500-52298-20 J17 (N30;W20') (6-12") Total/NA
Solid 9045C500-52298-21 J17 (N30;W20') (12-18") Total/NA
Solid 9045C500-52298-22 K12 (W25') (0-6') Total/NA
Solid 9045C500-52298-23 K12 (W25') (6-12') Total/NA
Solid 9045C500-52298-24 K12 (W25') (12-18') Total/NA
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Surrogate SummaryTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Method: 8270C - Semivolatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (30-119) (30-115) (36-134)
FBP NBZ TPH
59 47 72500-52298-1
Percent Surrogate Recovery (Acceptance Limits)
F20 (0-6")
55 48 54500-52298-2 F20 (6-12")
65 60 60500-52298-3 F20 (12-18")
38 30 38500-52298-4 H20 (E20') (0-6")
61 56 58500-52298-5 H20 (E20') (6-12")
65 58 67500-52298-6 H20 (E20') (12-18")
60 48 62500-52298-7 K10 (W25') (0-6")
58 45 67500-52298-8 K10 (W25') (6-12")
51 50 53500-52298-9 K10 (W25') (12-18")
73 56 83500-52298-10 H10 (N30') (0-6")
66 57 66500-52298-10 MS H10 (N30') (0-6")
57 49 56500-52298-10 MSD H10 (N30') (0-6")
55 53 62500-52298-11 H10 (N30') (6-12")
54 55 61500-52298-12 H10 (N30') (12-18")
54 47 59500-52298-13 J8 (0-6")
48 43 49500-52298-14 J8 (6-12")
47 44 52500-52298-15 J8 (12-18")
59 54 59500-52298-16 L6 (W20') (0-6")
68 66 60500-52298-17 L6 (W20') (6-12")
58 56 59500-52298-18 L6 (W20') (12-18")
56 46 74500-52298-19 J17 (N30;W20') (0-6")
55 47 58500-52298-20 J17 (N30;W20') (6-12")
72 63 68500-52298-21 J17 (N30;W20') (12-18")
62 51 61500-52298-22 K12 (W25') (0-6')
44 35 44500-52298-23 K12 (W25') (6-12')
62 50 69500-52298-24 K12 (W25') (12-18')
80 71 85LCS 500-170477/2-A Lab Control Sample
78 68 74LCS 500-170478/2-A Lab Control Sample
78 72 85MB 500-170477/1-A Method Blank
89 79 119MB 500-170478/1-A Method Blank
Surrogate Legend
FBP = 2-Fluorobiphenyl
NBZ = Nitrobenzene-d5
TPH = Terphenyl-d14
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QC Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Method: 8270C - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 500-170477/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170779 Prep Batch: 170477
RL MDL
Acenaphthene <0.033 0.033 0.0099 mg/Kg 11/20/12 16:54 11/24/12 12:22 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.033 0.00760.033 mg/Kg 11/20/12 16:54 11/24/12 12:22 1Acenaphthylene
<0.033 0.00780.033 mg/Kg 11/20/12 16:54 11/24/12 12:22 1Anthracene
<0.033 0.00700.033 mg/Kg 11/20/12 16:54 11/24/12 12:22 1Benzo[a]anthracene
<0.033 0.00610.033 mg/Kg 11/20/12 16:54 11/24/12 12:22 1Benzo[a]pyrene
<0.033 0.00650.033 mg/Kg 11/20/12 16:54 11/24/12 12:22 1Benzo[b]fluoranthene
<0.033 0.0110.033 mg/Kg 11/20/12 16:54 11/24/12 12:22 1Benzo[g,h,i]perylene
<0.033 0.00790.033 mg/Kg 11/20/12 16:54 11/24/12 12:22 1Benzo[k]fluoranthene
<0.033 0.00750.033 mg/Kg 11/20/12 16:54 11/24/12 12:22 1Chrysene
<0.033 0.00930.033 mg/Kg 11/20/12 16:54 11/24/12 12:22 1Dibenz(a,h)anthracene
<0.033 0.0140.033 mg/Kg 11/20/12 16:54 11/24/12 12:22 1Fluoranthene
<0.033 0.00760.033 mg/Kg 11/20/12 16:54 11/24/12 12:22 1Fluorene
<0.033 0.0110.033 mg/Kg 11/20/12 16:54 11/24/12 12:22 1Indeno[1,2,3-cd]pyrene
<0.033 0.00640.033 mg/Kg 11/20/12 16:54 11/24/12 12:22 1Naphthalene
<0.033 0.0140.033 mg/Kg 11/20/12 16:54 11/24/12 12:22 1Phenanthrene
<0.033 0.0120.033 mg/Kg 11/20/12 16:54 11/24/12 12:22 1Pyrene
2-Fluorobiphenyl 78 30 - 119 11/24/12 12:22 1
MB MB
Surrogate
11/20/12 16:54
Dil FacPrepared AnalyzedQualifier Limits%Recovery
72 11/20/12 16:54 11/24/12 12:22 1Nitrobenzene-d5 30 - 115
85 11/20/12 16:54 11/24/12 12:22 1Terphenyl-d14 36 - 134
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-170477/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170779 Prep Batch: 170477
Acenaphthene 1.67 1.10 mg/Kg 66 53 - 110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 1.67 1.16 mg/Kg 69 51 - 110
Anthracene 1.67 1.12 mg/Kg 67 52 - 110
Benzo[a]anthracene 1.67 1.26 mg/Kg 75 57 - 110
Benzo[a]pyrene 1.67 1.33 mg/Kg 80 56 - 110
Benzo[b]fluoranthene 1.67 1.32 mg/Kg 79 50 - 110
Benzo[g,h,i]perylene 1.67 1.30 mg/Kg 78 54 - 117
Benzo[k]fluoranthene 1.67 1.36 mg/Kg 82 43 - 121
Chrysene 1.67 1.27 mg/Kg 76 54 - 110
Dibenz(a,h)anthracene 1.67 1.32 mg/Kg 79 52 - 118
Fluoranthene 1.67 1.21 mg/Kg 73 55 - 113
Fluorene 1.67 1.17 mg/Kg 70 52 - 112
Indeno[1,2,3-cd]pyrene 1.67 1.32 mg/Kg 79 53 - 116
Naphthalene 1.67 1.08 mg/Kg 65 48 - 110
Phenanthrene 1.67 1.12 mg/Kg 67 51 - 116
Pyrene 1.67 1.30 mg/Kg 78 50 - 112
2-Fluorobiphenyl 30 - 119
Surrogate
80
LCS LCS
Qualifier Limits%Recovery
71Nitrobenzene-d5 30 - 115
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QC Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-170477/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170779 Prep Batch: 170477
Terphenyl-d14 36 - 134
Surrogate
85
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: H10 (N30') (0-6")Lab Sample ID: 500-52298-10 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170783 Prep Batch: 170477
Acenaphthene <0.21 2.20 1.46 mg/Kg 66 53 - 110☼
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acenaphthylene <0.21 2.20 1.31 mg/Kg 59 51 - 110☼
Anthracene <0.21 2.20 1.50 mg/Kg 68 52 - 110☼
Benzo[a]anthracene 0.20 J 2.20 1.50 mg/Kg 59 57 - 110☼
Benzo[a]pyrene 0.34 2.20 1.39 F mg/Kg 47 56 - 110☼
Benzo[b]fluoranthene 0.38 2.20 1.32 F mg/Kg 43 50 - 110☼
Benzo[g,h,i]perylene 0.25 2.20 1.59 mg/Kg 61 54 - 117☼
Benzo[k]fluoranthene 0.26 2.20 2.09 mg/Kg 83 43 - 121☼
Chrysene 0.24 2.20 1.53 mg/Kg 59 54 - 110☼
Dibenz(a,h)anthracene <0.21 2.20 1.44 mg/Kg 65 52 - 118☼
Fluoranthene 0.14 J 2.20 1.75 mg/Kg 73 55 - 113☼
Fluorene <0.21 2.20 1.46 mg/Kg 66 52 - 112☼
Indeno[1,2,3-cd]pyrene 0.22 2.20 1.46 mg/Kg 56 53 - 116☼
Naphthalene <0.21 2.20 1.09 mg/Kg 50 48 - 110☼
Phenanthrene <0.21 2.20 1.69 mg/Kg 77 51 - 116☼
Pyrene 0.15 J 2.20 1.36 mg/Kg 55 50 - 112☼
2-Fluorobiphenyl 30 - 119
Surrogate
66
MS MS
Qualifier Limits%Recovery
57Nitrobenzene-d5 30 - 115
66Terphenyl-d14 36 - 134
Client Sample ID: H10 (N30') (0-6")Lab Sample ID: 500-52298-10 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170783 Prep Batch: 170477
Acenaphthene <0.21 2.18 1.23 mg/Kg 56 53 - 110 17 30☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acenaphthylene <0.21 2.18 1.07 F mg/Kg 49 51 - 110 20 30☼
Anthracene <0.21 2.18 1.29 mg/Kg 59 52 - 110 15 30☼
Benzo[a]anthracene 0.20 J 2.18 1.25 F mg/Kg 48 57 - 110 18 30☼
Benzo[a]pyrene 0.34 2.18 1.17 F mg/Kg 38 56 - 110 17 30☼
Benzo[b]fluoranthene 0.38 2.18 1.33 F mg/Kg 44 50 - 110 1 30☼
Benzo[g,h,i]perylene 0.25 2.18 1.25 F mg/Kg 46 54 - 117 24 30☼
Benzo[k]fluoranthene 0.26 2.18 1.66 mg/Kg 64 43 - 121 23 30☼
Chrysene 0.24 2.18 1.27 F mg/Kg 48 54 - 110 18 30☼
Dibenz(a,h)anthracene <0.21 2.18 1.13 mg/Kg 52 52 - 118 24 30☼
Fluoranthene 0.14 J 2.18 1.49 mg/Kg 62 55 - 113 16 30☼
Fluorene <0.21 2.18 1.20 mg/Kg 55 52 - 112 19 30☼
Indeno[1,2,3-cd]pyrene 0.22 2.18 1.19 F mg/Kg 44 53 - 116 21 30☼
Naphthalene <0.21 2.18 0.966 F mg/Kg 44 48 - 110 12 30☼
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QC Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: H10 (N30') (0-6")Lab Sample ID: 500-52298-10 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170783 Prep Batch: 170477
Phenanthrene <0.21 2.18 1.28 mg/Kg 59 51 - 116 28 30☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Pyrene 0.15 J 2.18 1.17 F mg/Kg 47 50 - 112 16 30☼
2-Fluorobiphenyl 30 - 119
Surrogate
57
MSD MSD
Qualifier Limits%Recovery
49Nitrobenzene-d5 30 - 115
56Terphenyl-d14 36 - 134
Client Sample ID: Method BlankLab Sample ID: MB 500-170478/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170539 Prep Batch: 170478
RL MDL
Acenaphthene <0.033 0.033 0.0099 mg/Kg 11/20/12 17:12 11/21/12 13:21 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.033 0.00760.033 mg/Kg 11/20/12 17:12 11/21/12 13:21 1Acenaphthylene
<0.033 0.00780.033 mg/Kg 11/20/12 17:12 11/21/12 13:21 1Anthracene
<0.033 0.00700.033 mg/Kg 11/20/12 17:12 11/21/12 13:21 1Benzo[a]anthracene
<0.033 0.00610.033 mg/Kg 11/20/12 17:12 11/21/12 13:21 1Benzo[a]pyrene
<0.033 0.00650.033 mg/Kg 11/20/12 17:12 11/21/12 13:21 1Benzo[b]fluoranthene
<0.033 0.0110.033 mg/Kg 11/20/12 17:12 11/21/12 13:21 1Benzo[g,h,i]perylene
<0.033 0.00790.033 mg/Kg 11/20/12 17:12 11/21/12 13:21 1Benzo[k]fluoranthene
<0.033 0.00750.033 mg/Kg 11/20/12 17:12 11/21/12 13:21 1Chrysene
<0.033 0.00930.033 mg/Kg 11/20/12 17:12 11/21/12 13:21 1Dibenz(a,h)anthracene
<0.033 0.0140.033 mg/Kg 11/20/12 17:12 11/21/12 13:21 1Fluoranthene
<0.033 0.00760.033 mg/Kg 11/20/12 17:12 11/21/12 13:21 1Fluorene
<0.033 0.0110.033 mg/Kg 11/20/12 17:12 11/21/12 13:21 1Indeno[1,2,3-cd]pyrene
<0.033 0.00640.033 mg/Kg 11/20/12 17:12 11/21/12 13:21 1Naphthalene
<0.033 0.0140.033 mg/Kg 11/20/12 17:12 11/21/12 13:21 1Phenanthrene
<0.033 0.0120.033 mg/Kg 11/20/12 17:12 11/21/12 13:21 1Pyrene
2-Fluorobiphenyl 89 30 - 119 11/21/12 13:21 1
MB MB
Surrogate
11/20/12 17:12
Dil FacPrepared AnalyzedQualifier Limits%Recovery
79 11/20/12 17:12 11/21/12 13:21 1Nitrobenzene-d5 30 - 115
119 11/20/12 17:12 11/21/12 13:21 1Terphenyl-d14 36 - 134
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-170478/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170527 Prep Batch: 170478
Acenaphthene 1.67 1.13 mg/Kg 68 53 - 110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 1.67 1.19 mg/Kg 71 51 - 110
Anthracene 1.67 1.18 mg/Kg 71 52 - 110
Benzo[a]anthracene 1.67 1.29 mg/Kg 78 57 - 110
Benzo[a]pyrene 1.67 1.47 mg/Kg 88 56 - 110
Benzo[b]fluoranthene 1.67 1.37 mg/Kg 82 50 - 110
Benzo[g,h,i]perylene 1.67 1.29 mg/Kg 78 54 - 117
Benzo[k]fluoranthene 1.67 1.60 mg/Kg 96 43 - 121
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QC Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-170478/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170527 Prep Batch: 170478
Chrysene 1.67 1.26 mg/Kg 76 54 - 110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Dibenz(a,h)anthracene 1.67 1.44 mg/Kg 86 52 - 118
Fluoranthene 1.67 1.31 mg/Kg 79 55 - 113
Fluorene 1.67 1.23 mg/Kg 74 52 - 112
Indeno[1,2,3-cd]pyrene 1.67 1.39 mg/Kg 83 53 - 116
Naphthalene 1.67 1.07 mg/Kg 64 48 - 110
Phenanthrene 1.67 1.25 mg/Kg 75 51 - 116
Pyrene 1.67 1.18 mg/Kg 71 50 - 112
2-Fluorobiphenyl 30 - 119
Surrogate
78
LCS LCS
Qualifier Limits%Recovery
68Nitrobenzene-d5 30 - 115
74Terphenyl-d14 36 - 134
Method: 6010B - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 500-169568/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170336 Prep Batch: 169568
RL MDL
Antimony <2.0 2.0 0.27 mg/Kg 11/13/12 16:30 11/19/12 22:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<1.0 0.221.0 mg/Kg 11/13/12 16:30 11/19/12 22:17 1Arsenic
<1.0 0.121.0 mg/Kg 11/13/12 16:30 11/19/12 22:17 1Barium
<0.20 0.0500.20 mg/Kg 11/13/12 16:30 11/19/12 22:17 1Cadmium
<1.0 0.171.0 mg/Kg 11/13/12 16:30 11/19/12 22:17 1Chromium
<1.0 0.271.0 mg/Kg 11/13/12 16:30 11/19/12 22:17 1Copper
<0.50 0.170.50 mg/Kg 11/13/12 16:30 11/19/12 22:17 1Lead
<1.0 0.291.0 mg/Kg 11/13/12 16:30 11/19/12 22:17 1Selenium
<0.50 0.0600.50 mg/Kg 11/13/12 16:30 11/19/12 22:17 1Silver
<2.0 0.692.0 mg/Kg 11/13/12 16:30 11/19/12 22:17 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-169568/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170336 Prep Batch: 169568
Antimony 50.0 46.8 mg/Kg 94 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 10.0 9.37 mg/Kg 94 80 - 120
Barium 200 191 mg/Kg 96 80 - 120
Cadmium 5.00 4.76 mg/Kg 95 80 - 120
Chromium 20.0 18.8 mg/Kg 94 80 - 120
Copper 25.0 24.1 mg/Kg 96 80 - 120
Lead 10.0 9.76 mg/Kg 98 80 - 120
Selenium 10.0 9.48 mg/Kg 95 80 - 120
Silver 5.00 4.26 mg/Kg 85 80 - 120
Zinc 50.0 47.7 mg/Kg 95 80 - 120
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QC Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Method: 6010B - Metals (ICP) (Continued)
Client Sample ID: F20 (0-6")Lab Sample ID: 500-52298-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170336 Prep Batch: 169568
Antimony 0.75 J 78.0 39.8 F mg/Kg 50 75 - 125☼
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic 5.1 15.6 19.6 mg/Kg 93 75 - 125☼
Barium 55 312 327 mg/Kg 87 75 - 125☼
Cadmium 0.44 7.80 7.33 mg/Kg 88 75 - 125☼
Chromium 9.4 31.2 37.8 mg/Kg 91 75 - 125☼
Copper 18 39.0 78.5 F mg/Kg 154 75 - 125☼
Lead 34 15.6 49.7 mg/Kg 102 75 - 125☼
Selenium 0.79 J 15.6 13.1 mg/Kg 79 75 - 125☼
Silver <0.82 7.80 6.31 mg/Kg 81 75 - 125☼
Zinc 59 78.0 132 mg/Kg 92 75 - 125☼
Client Sample ID: F20 (0-6")Lab Sample ID: 500-52298-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170336 Prep Batch: 169568
Antimony 0.75 J 74.8 39.0 F mg/Kg 51 75 - 125 2 20☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Arsenic 5.1 15.0 17.9 mg/Kg 85 75 - 125 9 20☼
Barium 55 299 307 mg/Kg 84 75 - 125 6 20☼
Cadmium 0.44 7.48 6.86 mg/Kg 86 75 - 125 7 20☼
Chromium 9.4 29.9 34.9 mg/Kg 85 75 - 125 8 20☼
Copper 18 37.4 51.3 F mg/Kg 88 75 - 125 42 20☼
Lead 34 15.0 46.6 mg/Kg 86 75 - 125 7 20☼
Selenium 0.79 J 15.0 11.2 F mg/Kg 70 75 - 125 15 20☼
Silver <0.82 7.48 5.97 mg/Kg 80 75 - 125 6 20☼
Zinc 59 74.8 118 mg/Kg 79 75 - 125 11 20☼
Client Sample ID: F20 (0-6")Lab Sample ID: 500-52298-1 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170336 Prep Batch: 169568
Antimony 0.75 J 0.839 J mg/Kg 11 20☼
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Arsenic 5.1 5.08 mg/Kg 0.9 20☼
Barium 55 51.3 mg/Kg 7 20☼
Cadmium 0.44 0.410 mg/Kg 6 20☼
Chromium 9.4 9.25 mg/Kg 1 20☼
Copper 18 17.6 mg/Kg 5 20☼
Lead 34 30.0 mg/Kg 12 20☼
Selenium 0.79 J <1.6 mg/Kg NC 20☼
Silver <0.82 <0.79 mg/Kg NC 20☼
Zinc 59 56.0 mg/Kg 6 20☼
Client Sample ID: Method BlankLab Sample ID: MB 500-169626/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 169928 Prep Batch: 169626
RL MDL
Antimony <2.0 2.0 0.27 mg/Kg 11/14/12 08:30 11/15/12 16:53 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
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QC Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Method: 6010B - Metals (ICP) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 500-169626/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 169928 Prep Batch: 169626
RL MDL
Arsenic <1.0 1.0 0.22 mg/Kg 11/14/12 08:30 11/15/12 16:53 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<1.0 0.121.0 mg/Kg 11/14/12 08:30 11/15/12 16:53 1Barium
<0.20 0.0500.20 mg/Kg 11/14/12 08:30 11/15/12 16:53 1Cadmium
<1.0 0.171.0 mg/Kg 11/14/12 08:30 11/15/12 16:53 1Chromium
<1.0 0.271.0 mg/Kg 11/14/12 08:30 11/15/12 16:53 1Copper
<0.50 0.170.50 mg/Kg 11/14/12 08:30 11/15/12 16:53 1Lead
<1.0 0.291.0 mg/Kg 11/14/12 08:30 11/15/12 16:53 1Selenium
<0.50 0.0600.50 mg/Kg 11/14/12 08:30 11/15/12 16:53 1Silver
<2.0 0.692.0 mg/Kg 11/14/12 08:30 11/15/12 16:53 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-169626/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 169928 Prep Batch: 169626
Antimony 50.0 47.6 mg/Kg 95 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 10.0 9.75 mg/Kg 97 80 - 120
Barium 200 199 mg/Kg 99 80 - 120
Cadmium 5.00 4.81 mg/Kg 96 80 - 120
Chromium 20.0 19.3 mg/Kg 96 80 - 120
Copper 25.0 24.8 mg/Kg 99 80 - 120
Lead 10.0 10.0 mg/Kg 100 80 - 120
Selenium 10.0 9.52 mg/Kg 95 80 - 120
Silver 5.00 4.38 mg/Kg 88 80 - 120
Zinc 50.0 47.9 mg/Kg 96 80 - 120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-170225/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170334 Prep Batch: 170225
Arsenic 0.100 0.0908 mg/L 91 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Barium 0.500 0.490 J mg/L 98 80 - 120
Cadmium 0.0500 0.0476 mg/L 95 80 - 120
Chromium 0.200 0.195 mg/L 97 80 - 120
Lead 0.100 0.0969 mg/L 97 80 - 120
Selenium 0.100 0.0885 mg/L 89 80 - 120
Silver 0.0500 0.0472 mg/L 94 80 - 120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-170228/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170334 Prep Batch: 170228
Arsenic 0.100 0.0937 mg/L 94 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Barium 0.500 0.501 mg/L 100 80 - 120
Cadmium 0.0500 0.0486 mg/L 97 80 - 120
Chromium 0.200 0.198 mg/L 99 80 - 120
Lead 0.100 0.0986 mg/L 99 80 - 120
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QC Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Method: 6010B - Metals (ICP) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-170228/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170334 Prep Batch: 170228
Selenium 0.100 0.0899 mg/L 90 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Silver 0.0500 0.0483 mg/L 97 80 - 120
Client Sample ID: Method BlankLab Sample ID: LB 500-170018/1-B LB
Matrix: Solid Prep Type: TCLP
Analysis Batch: 170334 Prep Batch: 170225
RL MDL
Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 21:22 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.50 0.0100.50 mg/L 11/19/12 08:00 11/19/12 21:22 1Barium
<0.0050 0.00200.0050 mg/L 11/19/12 08:00 11/19/12 21:22 1Cadmium
<0.025 0.0100.025 mg/L 11/19/12 08:00 11/19/12 21:22 1Chromium
<0.0075 0.00500.0075 mg/L 11/19/12 08:00 11/19/12 21:22 1Lead
<0.050 0.0100.050 mg/L 11/19/12 08:00 11/19/12 21:22 1Selenium
<0.025 0.00500.025 mg/L 11/19/12 08:00 11/19/12 21:22 1Silver
Client Sample ID: H20 (E20') (0-6")Lab Sample ID: 500-52298-4 MS
Matrix: Solid Prep Type: TCLP
Analysis Batch: 170334 Prep Batch: 170225
Arsenic <0.050 0.100 0.113 mg/L 113 50 - 150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Barium 0.49 J 0.500 1.01 mg/L 103 50 - 150
Cadmium <0.0050 0.0500 0.0503 mg/L 101 50 - 150
Chromium <0.025 0.200 0.202 mg/L 101 50 - 150
Lead 0.051 0.100 0.155 mg/L 104 50 - 150
Selenium <0.050 0.100 0.107 mg/L 107 50 - 150
Silver <0.025 0.0500 0.0530 mg/L 106 50 - 150
Client Sample ID: H20 (E20') (0-6")Lab Sample ID: 500-52298-4 DU
Matrix: Solid Prep Type: TCLP
Analysis Batch: 170334 Prep Batch: 170225
Arsenic <0.050 <0.050 mg/L NC 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Barium 0.49 J 0.502 mg/L 2 20
Cadmium <0.0050 <0.0050 mg/L NC 20
Chromium <0.025 <0.025 mg/L NC 20
Lead 0.051 0.0523 mg/L 2 20
Selenium <0.050 <0.050 mg/L NC 20
Silver <0.025 <0.025 mg/L NC 20
Client Sample ID: Method BlankLab Sample ID: LB 500-170019/1-B LB
Matrix: Solid Prep Type: TCLP
Analysis Batch: 170334 Prep Batch: 170228
RL MDL
Arsenic <0.050 0.050 0.010 mg/L 11/19/12 08:00 11/19/12 19:24 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.50 0.0100.50 mg/L 11/19/12 08:00 11/19/12 19:24 1Barium
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QC Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Method: 6010B - Metals (ICP) (Continued)
Client Sample ID: Method BlankLab Sample ID: LB 500-170019/1-B LB
Matrix: Solid Prep Type: TCLP
Analysis Batch: 170334 Prep Batch: 170228
RL MDL
Cadmium <0.0050 0.0050 0.0020 mg/L 11/19/12 08:00 11/19/12 19:24 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
<0.025 0.0100.025 mg/L 11/19/12 08:00 11/19/12 19:24 1Chromium
0.0149 0.00500.0075 mg/L 11/19/12 08:00 11/19/12 19:24 1Lead
<0.050 0.0100.050 mg/L 11/19/12 08:00 11/19/12 19:24 1Selenium
<0.025 0.00500.025 mg/L 11/19/12 08:00 11/19/12 19:24 1Silver
Client Sample ID: K12 (W25') (6-12')Lab Sample ID: 500-52298-23 MS
Matrix: Solid Prep Type: TCLP
Analysis Batch: 170334 Prep Batch: 170228
Arsenic 0.32 0.100 0.421 mg/L 100 50 - 150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Barium 0.60 0.500 1.07 mg/L 94 50 - 150
Cadmium 0.0055 0.0500 0.0536 mg/L 96 50 - 150
Chromium <0.025 0.200 0.196 mg/L 98 50 - 150
Selenium <0.050 0.100 0.103 mg/L 103 50 - 150
Silver <0.025 0.0500 0.0504 mg/L 101 50 - 150
Client Sample ID: K12 (W25') (6-12')Lab Sample ID: 500-52298-23 MS
Matrix: Solid Prep Type: TCLP
Analysis Batch: 170422 Prep Batch: 170228
Arsenic 0.32 0.100 0.397 J mg/L 73 50 - 150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Barium 0.62 0.500 1.12 J mg/L 99 50 - 150
Cadmium <0.050 0.0500 0.0566 mg/L 113 50 - 150
Chromium <0.25 0.200 0.188 J mg/L 94 50 - 150
Lead 73 B 0.100 72.6 4 mg/L -438 50 - 150
Selenium <0.50 0.100 0.104 J mg/L 104 50 - 150
Silver <0.25 0.0500 0.0543 J mg/L 109 50 - 150
Client Sample ID: K12 (W25') (6-12')Lab Sample ID: 500-52298-23 DU
Matrix: Solid Prep Type: TCLP
Analysis Batch: 170334 Prep Batch: 170228
Arsenic 0.32 0.333 mg/L 4 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Barium 0.60 0.628 mg/L 4 20
Cadmium 0.0055 0.00550 mg/L 0.7 20
Chromium <0.025 <0.025 mg/L NC 20
Selenium <0.050 <0.050 mg/L NC 20
Silver <0.025 <0.025 mg/L NC 20
Client Sample ID: K12 (W25') (6-12')Lab Sample ID: 500-52298-23 DU
Matrix: Solid Prep Type: TCLP
Analysis Batch: 170422 Prep Batch: 170228
Arsenic 0.32 0.322 J mg/L 0.6 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
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QC Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Method: 6010B - Metals (ICP) (Continued)
Client Sample ID: K12 (W25') (6-12')Lab Sample ID: 500-52298-23 DU
Matrix: Solid Prep Type: TCLP
Analysis Batch: 170422 Prep Batch: 170228
Barium 0.62 0.626 J mg/L 0.7 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Cadmium <0.050 <0.050 mg/L NC 20
Chromium <0.25 <0.25 mg/L NC 20
Lead 73 B 73.2 mg/L 0.3 20
Selenium <0.50 <0.50 mg/L NC 20
Silver <0.25 <0.25 mg/L NC 20
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 500-170293/7-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170438 Prep Batch: 170293
RL MDL
Mercury <0.00020 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 09:39 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-170293/8-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170438 Prep Batch: 170293
Mercury 0.00200 0.00200 mg/L 100 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Method BlankLab Sample ID: MB 500-170296/7-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170438 Prep Batch: 170296
RL MDL
Mercury <0.00020 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:31 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-170296/8-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170438 Prep Batch: 170296
Mercury 0.00200 0.00268 * mg/L 134 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Method BlankLab Sample ID: LB 500-170019/1-E LB
Matrix: Solid Prep Type: TCLP
Analysis Batch: 170438 Prep Batch: 170293
RL MDL
Mercury 0.0000279 J 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 10:03 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
TestAmerica Chicago
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QC Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Method: 7470A - Mercury (CVAA) (Continued)
Client Sample ID: J17 (N30;W20') (12-18")Lab Sample ID: 500-52298-21 MS
Matrix: Solid Prep Type: TCLP
Analysis Batch: 170438 Prep Batch: 170293
Mercury 0.000026 J B 0.00100 0.000940 mg/L 91 50 - 150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: J17 (N30;W20') (12-18")Lab Sample ID: 500-52298-21 DU
Matrix: Solid Prep Type: TCLP
Analysis Batch: 170438 Prep Batch: 170293
Mercury 0.000026 J B 0.0000273 J mg/L 5 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Client Sample ID: Method BlankLab Sample ID: LB 500-170018/1-C LB
Matrix: Solid Prep Type: TCLP
Analysis Batch: 170438 Prep Batch: 170296
RL MDL
Mercury <0.00020 0.00020 0.000020 mg/L 11/19/12 16:00 11/20/12 11:35 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: F20 (0-6")Lab Sample ID: 500-52298-1 MS
Matrix: Solid Prep Type: TCLP
Analysis Batch: 170438 Prep Batch: 170296
Mercury <0.00020 * 0.00100 0.000393 F mg/L 39 50 - 150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: F20 (0-6")Lab Sample ID: 500-52298-1 DU
Matrix: Solid Prep Type: TCLP
Analysis Batch: 170438 Prep Batch: 170296
Mercury <0.00020 * 0.0000237 J * mg/L NC 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: 7471A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 500-170250/7-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170439 Prep Batch: 170250
RL MDL
Mercury <0.017 0.017 0.0064 mg/Kg 11/19/12 17:00 11/20/12 11:07 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-170250/8-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170439 Prep Batch: 170250
Mercury 0.167 0.157 mg/Kg 94 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
TestAmerica Chicago
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QC Sample ResultsTestAmerica Job ID: 500-52298-1Client: Shaw Environmental & Infrastructure, Inc
Project/Site: Naperville Sportsman Club
Method: 7471A - Mercury (CVAA) (Continued)
Client Sample ID: F20 (12-18")Lab Sample ID: 500-52298-3 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170439 Prep Batch: 170250
Mercury 0.029 0.101 0.120 mg/Kg 90 75 - 125☼
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: F20 (12-18")Lab Sample ID: 500-52298-3 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170439 Prep Batch: 170250
Mercury 0.029 0.102 0.121 mg/Kg 90 75 - 125 1 20☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: F20 (12-18")Lab Sample ID: 500-52298-3 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170439 Prep Batch: 170250
Mercury 0.029 0.0226 mg/Kg 26 20☼
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Client Sample ID: Method BlankLab Sample ID: MB 500-170259/7-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170439 Prep Batch: 170259
RL MDL
Mercury <0.017 0.017 0.0064 mg/Kg 11/19/12 17:00 11/20/12 12:05 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 500-170259/8-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 170439 Prep Batch: 170259
Mercury 0.167 0.161 mg/Kg 96 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Method: 9045C - pH
Client Sample ID: K10 (W25') (6-12")Lab Sample ID: 500-52298-8 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 169904
pH 7.34 7.330 SU 0.1
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
TestAmerica Chicago
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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-52298-1
Project/Site: Naperville Sportsman Club
Client Sample ID: F20 (0-6") Lab Sample ID: 500-52298-1Matrix: SolidDate Collected: 11/09/12 13:15
Percent Solids: 59.3Date Received: 11/13/12 13:30
Prep 3541 11/20/12 16:54 DEA170477 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 170783 11/24/12 17:55 DA TAL CHITotal/NA
Leach 1311 170018 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170225 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/19/12 21:49 TDS TAL CHITCLP
Prep 3050B 169568 11/13/12 16:30 RL TAL CHITotal/NA
Analysis 6010B 1 170336 11/19/12 22:26 TDS TAL CHITotal/NA
Prep 7470A 170296 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 11:37 BJB TAL CHITCLP
Prep 7471A 170250 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 11:10 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 09:24
11/15/12 09:27
(Start)
(End)
Client Sample ID: F20 (6-12") Lab Sample ID: 500-52298-2Matrix: SolidDate Collected: 11/09/12 13:16
Percent Solids: 78.7Date Received: 11/13/12 13:30
Prep 3541 11/20/12 16:54 DEA170477 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 170783 11/24/12 18:15 DA TAL CHITotal/NA
Leach 1311 170018 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170225 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/19/12 21:55 TDS TAL CHITCLP
Prep 3050B 169568 11/13/12 16:30 RL TAL CHITotal/NA
Analysis 6010B 1 170336 11/19/12 22:48 TDS TAL CHITotal/NA
Prep 7470A 170296 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 11:46 BJB TAL CHITCLP
Prep 7471A 170250 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 11:12 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 09:27
11/15/12 09:30
(Start)
(End)
Client Sample ID: F20 (12-18") Lab Sample ID: 500-52298-3Matrix: SolidDate Collected: 11/09/12 13:17
Percent Solids: 80.8Date Received: 11/13/12 13:30
Prep 3541 11/20/12 16:54 DEA170477 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
TestAmerica Chicago
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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-52298-1
Project/Site: Naperville Sportsman Club
Client Sample ID: F20 (12-18") Lab Sample ID: 500-52298-3Matrix: SolidDate Collected: 11/09/12 13:17
Percent Solids: 80.8Date Received: 11/13/12 13:30
Analysis 8270C 11/24/12 18:34 DA1 170783 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Leach 1311 170018 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170225 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/19/12 22:02 TDS TAL CHITCLP
Prep 3050B 169568 11/13/12 16:30 RL TAL CHITotal/NA
Analysis 6010B 1 170336 11/19/12 22:53 TDS TAL CHITotal/NA
Prep 7470A 170296 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 11:48 BJB TAL CHITCLP
Prep 7471A 170250 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 11:18 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 09:30
11/15/12 09:32
(Start)
(End)
Client Sample ID: H20 (E20') (0-6") Lab Sample ID: 500-52298-4Matrix: SolidDate Collected: 11/09/12 12:25
Percent Solids: 33.5Date Received: 11/13/12 13:30
Prep 3541 11/20/12 16:54 DEA170477 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 170783 11/24/12 18:54 DA TAL CHITotal/NA
Leach 1311 170018 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170225 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/19/12 22:08 TDS TAL CHITCLP
Prep 3050B 169568 11/13/12 16:30 RL TAL CHITotal/NA
Analysis 6010B 1 170336 11/19/12 22:58 TDS TAL CHITotal/NA
Prep 7470A 170296 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 11:50 BJB TAL CHITCLP
Prep 7471A 170250 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 11:26 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 09:32
11/15/12 09:35
(Start)
(End)
Client Sample ID: H20 (E20') (6-12") Lab Sample ID: 500-52298-5Matrix: SolidDate Collected: 11/09/12 12:26
Percent Solids: 78.9Date Received: 11/13/12 13:30
Prep 3541 11/20/12 16:54 DEA170477 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 170783 11/24/12 19:14 DA TAL CHITotal/NA
TestAmerica Chicago
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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-52298-1
Project/Site: Naperville Sportsman Club
Client Sample ID: H20 (E20') (6-12") Lab Sample ID: 500-52298-5Matrix: SolidDate Collected: 11/09/12 12:26
Date Received: 11/13/12 13:30
Leach 1311 11/16/12 12:00 MP170018 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
TCLP
Prep 3010A 170225 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/19/12 22:39 TDS TAL CHITCLP
Prep 3050B 169568 11/13/12 16:30 RL TAL CHITotal/NA
Analysis 6010B 1 170336 11/19/12 23:12 TDS TAL CHITotal/NA
Prep 7470A 170296 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 11:51 BJB TAL CHITCLP
Prep 7471A 170250 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 11:28 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 09:35
11/15/12 09:37
(Start)
(End)
Client Sample ID: H20 (E20') (12-18") Lab Sample ID: 500-52298-6Matrix: SolidDate Collected: 11/09/12 12:27
Percent Solids: 78.0Date Received: 11/13/12 13:30
Prep 3541 11/20/12 16:54 DEA170477 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 170783 11/24/12 19:33 DA TAL CHITotal/NA
Leach 1311 170018 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170225 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/19/12 22:45 TDS TAL CHITCLP
Prep 3050B 169568 11/13/12 16:30 RL TAL CHITotal/NA
Analysis 6010B 1 170336 11/19/12 23:17 TDS TAL CHITotal/NA
Prep 7470A 170296 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 11:53 BJB TAL CHITCLP
Prep 7471A 170250 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 11:30 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 09:37
11/15/12 09:40
(Start)
(End)
Client Sample ID: K10 (W25') (0-6") Lab Sample ID: 500-52298-7Matrix: SolidDate Collected: 11/09/12 11:50
Percent Solids: 33.1Date Received: 11/13/12 13:30
Prep 3541 11/20/12 16:54 DEA170477 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 170783 11/24/12 19:53 DA TAL CHITotal/NA
Leach 1311 170018 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170225 11/19/12 08:00 LAH TAL CHITCLP
TestAmerica Chicago
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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-52298-1
Project/Site: Naperville Sportsman Club
Client Sample ID: K10 (W25') (0-6") Lab Sample ID: 500-52298-7Matrix: SolidDate Collected: 11/09/12 11:50
Date Received: 11/13/12 13:30
Analysis 6010B 11/19/12 23:06 TDS1 170334 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
TCLP
Prep 3050B 169568 11/13/12 16:30 RL TAL CHITotal/NA
Analysis 6010B 1 170336 11/19/12 23:21 TDS TAL CHITotal/NA
Analysis 6010B 50 170422 11/20/12 11:17 TDS TAL CHITotal/NA
Prep 7470A 170296 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 11:55 BJB TAL CHITCLP
Prep 7471A 170250 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 11:32 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 09:40
11/15/12 09:43
(Start)
(End)
Client Sample ID: K10 (W25') (6-12") Lab Sample ID: 500-52298-8Matrix: SolidDate Collected: 11/09/12 11:51
Percent Solids: 47.1Date Received: 11/13/12 13:30
Prep 3541 11/20/12 16:54 DEA170477 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 170783 11/24/12 20:12 DA TAL CHITotal/NA
Leach 1311 170018 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170225 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/19/12 23:12 TDS TAL CHITCLP
Prep 3050B 169568 11/13/12 16:30 RL TAL CHITotal/NA
Analysis 6010B 1 170336 11/19/12 23:26 TDS TAL CHITotal/NA
Prep 7470A 170296 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 11:56 BJB TAL CHITCLP
Prep 7471A 170250 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 11:34 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 09:43
11/15/12 09:45
(Start)
(End)
Client Sample ID: K10 (W25') (12-18") Lab Sample ID: 500-52298-9Matrix: SolidDate Collected: 11/09/12 11:52
Percent Solids: 78.3Date Received: 11/13/12 13:30
Prep 3541 11/20/12 16:54 DEA170477 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 170783 11/24/12 20:32 DA TAL CHITotal/NA
Leach 1311 170018 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170225 11/19/12 08:00 LAH TAL CHITCLP
TestAmerica Chicago
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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-52298-1
Project/Site: Naperville Sportsman Club
Client Sample ID: K10 (W25') (12-18") Lab Sample ID: 500-52298-9Matrix: SolidDate Collected: 11/09/12 11:52
Date Received: 11/13/12 13:30
Analysis 6010B 11/19/12 23:18 TDS1 170334 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
TCLP
Prep 3050B 169568 11/13/12 16:30 RL TAL CHITotal/NA
Analysis 6010B 1 170336 11/19/12 23:30 TDS TAL CHITotal/NA
Prep 7470A 170296 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 11:58 BJB TAL CHITCLP
Prep 7471A 170250 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 11:35 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 09:48
11/15/12 09:50
(Start)
(End)
Client Sample ID: H10 (N30') (0-6") Lab Sample ID: 500-52298-10Matrix: SolidDate Collected: 11/08/12 11:45
Percent Solids: 74.5Date Received: 11/13/12 13:30
Prep 3541 11/20/12 16:54 DEA170477 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 5 170783 11/24/12 20:52 DA TAL CHITotal/NA
Leach 1311 170018 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170225 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/19/12 23:24 TDS TAL CHITCLP
Prep 3050B 169568 11/13/12 16:30 RL TAL CHITotal/NA
Analysis 6010B 1 170336 11/19/12 23:34 TDS TAL CHITotal/NA
Prep 7470A 170296 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 12:00 BJB TAL CHITCLP
Prep 7471A 170250 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 11:41 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 09:50
11/15/12 09:53
(Start)
(End)
Client Sample ID: H10 (N30') (6-12") Lab Sample ID: 500-52298-11Matrix: SolidDate Collected: 11/08/12 11:46
Percent Solids: 78.5Date Received: 11/13/12 13:30
Prep 3541 11/20/12 16:54 DEA170477 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 170783 11/24/12 21:11 DA TAL CHITotal/NA
Leach 1311 170018 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170225 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/19/12 23:31 TDS TAL CHITCLP
TestAmerica Chicago
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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-52298-1
Project/Site: Naperville Sportsman Club
Client Sample ID: H10 (N30') (6-12") Lab Sample ID: 500-52298-11Matrix: SolidDate Collected: 11/08/12 11:46
Percent Solids: 78.5Date Received: 11/13/12 13:30
Prep 3050B 11/13/12 16:30 RL169568 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 6010B 1 170336 11/19/12 23:38 TDS TAL CHITotal/NA
Prep 7470A 170296 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 12:08 BJB TAL CHITCLP
Prep 7471A 170250 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 11:43 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 09:53
11/15/12 09:55
(Start)
(End)
Client Sample ID: H10 (N30') (12-18") Lab Sample ID: 500-52298-12Matrix: SolidDate Collected: 11/08/12 11:47
Percent Solids: 81.5Date Received: 11/13/12 13:30
Prep 3541 11/20/12 16:54 DEA170477 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 170783 11/24/12 21:31 DA TAL CHITotal/NA
Leach 1311 170018 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170225 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/19/12 23:37 TDS TAL CHITCLP
Prep 3050B 169568 11/13/12 16:30 RL TAL CHITotal/NA
Analysis 6010B 1 170336 11/19/12 23:43 TDS TAL CHITotal/NA
Prep 7470A 170296 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 12:10 BJB TAL CHITCLP
Prep 7471A 170250 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 11:44 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 09:55
11/15/12 09:58
(Start)
(End)
Client Sample ID: J8 (0-6") Lab Sample ID: 500-52298-13Matrix: SolidDate Collected: 11/08/12 12:00
Percent Solids: 73.0Date Received: 11/13/12 13:30
Prep 3541 11/20/12 16:54 DEA170477 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 170783 11/24/12 21:51 DA TAL CHITotal/NA
Leach 1311 170018 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170225 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/19/12 23:43 TDS TAL CHITCLP
Prep 3050B 169568 11/13/12 16:30 RL TAL CHITotal/NA
Analysis 6010B 1 170336 11/19/12 23:48 TDS TAL CHITotal/NA
TestAmerica Chicago
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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-52298-1
Project/Site: Naperville Sportsman Club
Client Sample ID: J8 (0-6") Lab Sample ID: 500-52298-13Matrix: SolidDate Collected: 11/08/12 12:00
Date Received: 11/13/12 13:30
Prep 7470A 11/19/12 16:00 BJB170296 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
TCLP
Analysis 7470A 1 170438 11/20/12 12:12 BJB TAL CHITCLP
Prep 7471A 170250 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 11:46 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 09:58
11/15/12 10:01
(Start)
(End)
Client Sample ID: J8 (6-12") Lab Sample ID: 500-52298-14Matrix: SolidDate Collected: 11/08/12 12:01
Percent Solids: 69.3Date Received: 11/13/12 13:30
Prep 3541 11/20/12 16:54 DEA170477 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 170783 11/24/12 22:11 DA TAL CHITotal/NA
Leach 1311 170018 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170225 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/19/12 23:49 TDS TAL CHITCLP
Prep 3050B 169568 11/13/12 16:30 RL TAL CHITotal/NA
Analysis 6010B 1 170336 11/19/12 23:52 TDS TAL CHITotal/NA
Prep 7470A 170296 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 12:13 BJB TAL CHITCLP
Prep 7471A 170250 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 11:48 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 10:01
11/15/12 10:03
(Start)
(End)
Client Sample ID: J8 (12-18") Lab Sample ID: 500-52298-15Matrix: SolidDate Collected: 11/08/12 12:02
Percent Solids: 72.6Date Received: 11/13/12 13:30
Prep 3541 11/20/12 16:54 DEA170477 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 170783 11/24/12 22:31 DA TAL CHITotal/NA
Leach 1311 170018 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170225 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/19/12 23:55 TDS TAL CHITCLP
Prep 3050B 169568 11/13/12 16:30 RL TAL CHITotal/NA
Analysis 6010B 1 170336 11/20/12 00:06 TDS TAL CHITotal/NA
Prep 7470A 170296 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 12:15 BJB TAL CHITCLP
TestAmerica Chicago
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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-52298-1
Project/Site: Naperville Sportsman Club
Client Sample ID: J8 (12-18") Lab Sample ID: 500-52298-15Matrix: SolidDate Collected: 11/08/12 12:02
Percent Solids: 72.6Date Received: 11/13/12 13:30
Prep 7471A 11/19/12 17:00 BJB170250 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 7471A 1 170439 11/20/12 11:50 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 10:03
11/15/12 10:06
(Start)
(End)
Client Sample ID: L6 (W20') (0-6") Lab Sample ID: 500-52298-16Matrix: SolidDate Collected: 11/08/12 13:20
Percent Solids: 78.2Date Received: 11/13/12 13:30
Prep 3541 11/20/12 16:54 DEA170477 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 170783 11/24/12 22:50 DA TAL CHITotal/NA
Leach 1311 170018 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170225 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/20/12 00:02 TDS TAL CHITCLP
Prep 3050B 169568 11/13/12 16:30 RL TAL CHITotal/NA
Analysis 6010B 1 170336 11/20/12 00:11 TDS TAL CHITotal/NA
Prep 7470A 170296 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 12:17 BJB TAL CHITCLP
Prep 7471A 170250 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 11:52 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 10:06
11/15/12 10:08
(Start)
(End)
Client Sample ID: L6 (W20') (6-12") Lab Sample ID: 500-52298-17Matrix: SolidDate Collected: 11/08/12 13:21
Percent Solids: 79.3Date Received: 11/13/12 13:30
Prep 3541 11/20/12 16:54 DEA170477 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 170783 11/24/12 23:10 DA TAL CHITotal/NA
Leach 1311 170018 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170225 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/20/12 00:23 TDS TAL CHITCLP
Prep 3050B 169568 11/13/12 16:30 RL TAL CHITotal/NA
Analysis 6010B 1 170336 11/20/12 00:16 TDS TAL CHITotal/NA
Prep 7470A 170296 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 12:18 BJB TAL CHITCLP
Prep 7471A 170250 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 11:54 BJB TAL CHITotal/NA
TestAmerica Chicago
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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-52298-1
Project/Site: Naperville Sportsman Club
Client Sample ID: L6 (W20') (6-12") Lab Sample ID: 500-52298-17Matrix: SolidDate Collected: 11/08/12 13:21
Date Received: 11/13/12 13:30
Analysis Moisture 11/13/12 14:51 CMV1 169544 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 10:08
11/15/12 10:11
(Start)
(End)
Client Sample ID: L6 (W20') (12-18") Lab Sample ID: 500-52298-18Matrix: SolidDate Collected: 11/08/12 13:22
Percent Solids: 78.4Date Received: 11/13/12 13:30
Prep 3541 11/20/12 16:54 DEA170477 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 170783 11/24/12 23:30 DA TAL CHITotal/NA
Leach 1311 170018 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170225 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/20/12 00:29 TDS TAL CHITCLP
Prep 3050B 169568 11/13/12 16:30 RL TAL CHITotal/NA
Analysis 6010B 1 170336 11/20/12 00:21 TDS TAL CHITotal/NA
Prep 7470A 170296 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 12:20 BJB TAL CHITCLP
Prep 7471A 170250 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 11:56 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 10:11
11/15/12 10:13
(Start)
(End)
Client Sample ID: J17 (N30;W20') (0-6") Lab Sample ID: 500-52298-19Matrix: SolidDate Collected: 11/08/12 14:40
Percent Solids: 42.0Date Received: 11/13/12 13:30
Prep 3541 11/20/12 16:54 DEA170477 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 5 170783 11/24/12 23:50 DA TAL CHITotal/NA
Leach 1311 170018 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170225 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/20/12 00:35 TDS TAL CHITCLP
Prep 3050B 169568 11/13/12 16:30 RL TAL CHITotal/NA
Analysis 6010B 1 170336 11/20/12 00:26 TDS TAL CHITotal/NA
Prep 7470A 170296 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 12:22 BJB TAL CHITCLP
Prep 7471A 170250 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 11:58 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
TestAmerica Chicago
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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-52298-1
Project/Site: Naperville Sportsman Club
Client Sample ID: J17 (N30;W20') (0-6") Lab Sample ID: 500-52298-19Matrix: SolidDate Collected: 11/08/12 14:40
Date Received: 11/13/12 13:30
Analysis 9045C EAT1 169904 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
11/15/12 10:13
11/15/12 10:16
(Start)
(End)
Client Sample ID: J17 (N30;W20') (6-12") Lab Sample ID: 500-52298-20Matrix: SolidDate Collected: 11/08/12 14:41
Percent Solids: 35.2Date Received: 11/13/12 13:30
Prep 3541 11/20/12 16:54 DEA170477 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 170783 11/25/12 00:09 DA TAL CHITotal/NA
Leach 1311 170018 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170225 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/20/12 00:41 TDS TAL CHITCLP
Prep 3050B 169568 11/13/12 16:30 RL TAL CHITotal/NA
Analysis 6010B 1 170336 11/20/12 00:30 TDS TAL CHITotal/NA
Analysis 6010B 50 170422 11/20/12 11:21 TDS TAL CHITotal/NA
Prep 7470A 170296 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 12:24 BJB TAL CHITCLP
Prep 7471A 170250 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 12:03 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 10:16
11/15/12 10:19
(Start)
(End)
Client Sample ID: J17 (N30;W20') (12-18") Lab Sample ID: 500-52298-21Matrix: SolidDate Collected: 11/08/12 14:42
Percent Solids: 74.5Date Received: 11/13/12 13:30
Prep 3541 11/20/12 17:12 DEA170478 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 170783 11/25/12 00:29 DA TAL CHITotal/NA
Prep 3050B 169626 11/14/12 08:30 LAH TAL CHITotal/NA
Analysis 6010B 1 169928 11/15/12 17:53 TDS TAL CHITotal/NA
Leach 1311 170019 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170228 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/19/12 19:42 TDS TAL CHITCLP
Prep 7470A 170293 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 10:07 BJB TAL CHITCLP
Prep 7471A 170259 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 12:39 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
TestAmerica Chicago
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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-52298-1
Project/Site: Naperville Sportsman Club
Client Sample ID: J17 (N30;W20') (12-18") Lab Sample ID: 500-52298-21Matrix: SolidDate Collected: 11/08/12 14:42
Date Received: 11/13/12 13:30
Analysis 9045C EAT1 169904 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
11/15/12 10:19
11/15/12 10:21
(Start)
(End)
Client Sample ID: K12 (W25') (0-6') Lab Sample ID: 500-52298-22Matrix: SolidDate Collected: 11/08/12 13:55
Percent Solids: 51.8Date Received: 11/13/12 13:30
Prep 3541 11/20/12 17:12 DEA170478 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 170783 11/25/12 00:49 DA TAL CHITotal/NA
Prep 3050B 169626 11/14/12 08:30 LAH TAL CHITotal/NA
Analysis 6010B 1 169928 11/15/12 17:57 TDS TAL CHITotal/NA
Leach 1311 170019 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170228 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/19/12 19:48 TDS TAL CHITCLP
Prep 7470A 170293 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 10:12 BJB TAL CHITCLP
Prep 7471A 170259 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 12:41 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 10:21
11/15/12 10:24
(Start)
(End)
Client Sample ID: K12 (W25') (6-12') Lab Sample ID: 500-52298-23Matrix: SolidDate Collected: 11/08/12 13:56
Percent Solids: 54.3Date Received: 11/13/12 13:30
Prep 3541 11/20/12 17:12 DEA170478 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 1 170783 11/25/12 01:08 DA TAL CHITotal/NA
Prep 3050B 169626 11/14/12 08:30 LAH TAL CHITotal/NA
Analysis 6010B 1 169928 11/15/12 18:01 TDS TAL CHITotal/NA
Leach 1311 170019 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170228 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/19/12 19:55 TDS TAL CHITCLP
Analysis 6010B 10 170422 11/20/12 11:25 TDS TAL CHITCLP
Prep 7470A 170293 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 10:14 BJB TAL CHITCLP
Prep 7471A 170259 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 12:42 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
TestAmerica Chicago
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Lab ChronicleClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-52298-1
Project/Site: Naperville Sportsman Club
Client Sample ID: K12 (W25') (6-12') Lab Sample ID: 500-52298-23Matrix: SolidDate Collected: 11/08/12 13:56
Date Received: 11/13/12 13:30
Analysis 9045C EAT1 169904 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
11/15/12 10:24
11/15/12 10:26
(Start)
(End)
Client Sample ID: K12 (W25') (12-18') Lab Sample ID: 500-52298-24Matrix: SolidDate Collected: 11/08/12 13:57
Percent Solids: 64.3Date Received: 11/13/12 13:30
Prep 3541 11/20/12 17:12 DEA170478 TAL CHI
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8270C 5 170783 11/25/12 01:28 DA TAL CHITotal/NA
Prep 3050B 169626 11/14/12 08:30 LAH TAL CHITotal/NA
Analysis 6010B 1 169928 11/15/12 18:05 TDS TAL CHITotal/NA
Leach 1311 170019 11/16/12 12:00 MP TAL CHITCLP
Prep 3010A 170228 11/19/12 08:00 LAH TAL CHITCLP
Analysis 6010B 1 170334 11/19/12 20:40 TDS TAL CHITCLP
Prep 7470A 170293 11/19/12 16:00 BJB TAL CHITCLP
Analysis 7470A 1 170438 11/20/12 10:19 BJB TAL CHITCLP
Prep 7471A 170259 11/19/12 17:00 BJB TAL CHITotal/NA
Analysis 7471A 1 170439 11/20/12 12:48 BJB TAL CHITotal/NA
Analysis Moisture 1 169544 11/13/12 14:51 CMV TAL CHITotal/NA
Analysis 9045C 1 169904 EAT TAL CHITotal/NA
11/15/12 10:26
11/15/12 10:29
(Start)
(End)
Laboratory References:
TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200
TestAmerica Chicago
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Certification SummaryClient: Shaw Environmental & Infrastructure, Inc TestAmerica Job ID: 500-52298-1
Project/Site: Naperville Sportsman Club
Laboratory: TestAmerica ChicagoAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
Alabama 04-30-13404614State Program
California NELAC 9 01132CA 04-30-13
Georgia State Program 4 N/A 04-30-13
Georgia State Program 4 939 04-30-13
Hawaii State Program 9 N/A 04-30-13
Illinois NELAC 5 100201 04-30-13
Indiana State Program 5 C-IL-02 04-30-13
Iowa State Program 7 82 05-01-14
Kansas NELAC 7 E-10161 10-31-13
Kentucky State Program 4 90023 12-31-12
Kentucky (UST) State Program 4 66 04-11-13
L-A-B DoD ELAP L2304 01-06-13
L-A-B ISO/IEC 17025 L2304 01-06-13
Louisiana NELAC 6 30720 06-30-13
Massachusetts State Program 1 M-IL035 06-30-13
Mississippi State Program 4 N/A 04-30-13
North Carolina DENR State Program 4 291 12-31-12
North Dakota State Program 8 R-194 04-30-13
Oklahoma State Program 6 8908 08-31-13
South Carolina State Program 4 77001 04-30-13
Texas NELAC 6 T104704252-09-TX 02-28-13
USDA Federal P330-12-00038 02-06-15
Virginia NELAC 3 460142 06-14-13
Wisconsin State Program 5 999580010 08-31-13
Wyoming State Program 8 8TMS-Q 04-30-13
TestAmerica Chicago
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Page 101 of 104 11/26/2012
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Login Sample Receipt Checklist
Client: Shaw Environmental & Infrastructure, Inc Job Number: 500-52298-1
Login Number: 52298
Question Answer Comment
Creator: Lunt, Jeff T
List Source: TestAmerica Chicago
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice. 3.2
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica ChicagoPage 104 of 104 11/26/2012
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