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AMX/ARX - AVANCE
2H Lockswitch 500MHzTechnical Manual
BRUKER
Version
004
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The information in this manual may be altered without notice.
BRUKER accepts no responsibility for actions taken as a resultof use of this manual. BRUKER accepts no liability for any mis-takes contained in the manual, leading to coincidental damage,whether during installation or operation of the instrument. Un-authorised reproduction of manual contents, without writtenpermission from the publishers, or translation into another lan-guage, either in full or in part, is forbidden.
This manual was written by
BARTHELEMY Philippe
© December 15, 1998: Bruker SA
Wissembourg, France
Manual P/N: Z31455DWG-Nr: 1165004
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Contents
Contents ............................................................... 3
Index ..................................................................... 5
1 General description ................................................ 71.1 Description .......................................................................... 71.2 Specifications ...................................................................... 81.3 Spectrometer environment ................................................... 91.4 Wiring ................................................................................. 9
2 Control signal & RF signal route...........................112.1 About polarity selection ..................................................... 112.2 Internal polarity selection ................................................... 112.3 Output signal polarities function of selected jumpers .......... 122.4 RF signal of DEC 2H IN route ............................................ 13
3 Applications.......................................................... 153.1 Applications spectra .......................................................... 15
Composit pulse program spectra ....................................163.2 Pulse program ................................................................... 18
Sequence for AMX, ASX and ARX spectrometer ............18Sequence for Avance spectrometer DMX, DRX ..............19
4 2H Lockswitch 500MHZ ........................................ 21
5 Control Board ....................................................... 23
6 Blanking Switch BLMK 32-160MHZ ...................... 29
7 HP Coupler 3dB 62,5-125MHZ .............................. 33
8 Specifications ....................................................... 378.1 2H Lockswitch 500 MHz specifications ............................... 37
Figures ................................................................ 39
Tables .................................................................. 41
Technical Manual Version 004 BRUKER 3 (43)
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Contents
4 (43) BRUKER Technical Manual Version 004
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Index
Numerics
13C chloroform line ............................................................................................. 152H TX OUT from LOCK TRANSMITER................................................................ 9
A
AMX/ARX polarity ............................................................................................... 11Auxiliary BLK OUT ................................................................................................ 9AVANCE polarity................................................................................................. 11
B
BLK from X Amplifier............................................................................................. 9
F
Frequency range................................................................................................. 37
O
Observation 13C decoupling 2H and 1H............................................................. 15
P
Power requirements ............................................................................................ 37Pulse program for AMX....................................................................................... 18Pulse program for ARX ....................................................................................... 18Pulse program for ASX ....................................................................................... 18Pulse program for DMX....................................................................................... 19Pulse program for DRX....................................................................................... 19
R
RF POWER from X Amplifier ................................................................................ 9RF to 2H Probe ..................................................................................................... 9
S
Software control .................................................................................................. 37Spectra................................................................................................................ 15Spectra with 1H WALTS-16 & 2H GARP............................................................ 16Spectra with 1H WALTS-16 & 2H WALTS-16..................................................... 17
Technical Manual Version 004 BRUKER 5 (43)
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Index
T
TCU OBS 2H selection ......................................................................................... 9TCU programed BLK............................................................................................. 9
W
W4B132147 C..................................................................................................... 22W4D132510 A..................................................................................................... 28W4L132122 G ..................................................................................................... 25W4L132146......................................................................................................... 35W4S132122 G..................................................................................................... 24W4S132144 A ..................................................................................................... 30W4S132146 ........................................................................................................ 34
X
X out...................................................................................................................... 9
6 (43) BRUKER Technical Manual Version 004
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1General description 1Description 1.1
The 2H Lockswitch system allows to perform experiments with Lock and Deuteri-um decoupling or just Deuterium observation. It is possible to switch from the Xobservation to Deuterium observation by using only one X amplifier without doingany cable changes. This manipulation is possible because of the internal «rout-ing» that dispatches the source [channel 1 = 13C (2H)] either on the «Deuterium»output (Dec / Lock 2H to HPPR) or on the «X» output (BB Preamplifier).
The commutation for «Lock» and «1H or X» observation is possible with this ac-cessory (automatic).
This system allows also to perform 1 axis «Deuterium Gradient Shiming».
Figure 1.1. Synoptic of 2H Lockswitch
2H LOCKSWITCH
Sel Obs-2H
Lockswitch andHPPR 2H BLKelaboration
TP-FO in
Sel 2H/Dec
TP-FO out
2H TR inTR Switch
Relay SwitchDec 2H in
BB Preamp.
RX-BLNK out
TX-BLNK out
Coupler
Dec/Lock 2Hto HPPR
Technical Manual Version 004 BRUKER 7 (43)
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General description
Specifications 1.2
- Power supply: 200 V to 240 V AC (rear socket)- Range: 62,5 to 125 MHz- Insertion loss: 4 dB ±1 dB in the range (X channel and 2H channel both)- 2H TR IN Input to DEC 2H IN Input Isolation (when BLKM on RF active state) :
20 dB to 30 dB (DEC/LOCK 2H Output 50 Ohms loaded )
- 2H TR IN Input to DEC 2H IN Input Isolation (when BLKM desactivated state):greater as 75 dB
- 2H TR IN Input to DEC 2H IN Input Isolation (when BLKM desactivated state) :greater as 75 dB
- 2H TR IN Input to DEC/LOCK 2H Output Isolation (when BLKM desactivatedstate) : greater as 60 dB
- Total switching time : less than 15µs for ’’SEL 2H/DEC & SEL OBS-2H’’ andless than 0,5 µs for TP-FO
- Universal Polarity capability on all logical outputs and TP-FO INSelection (See more details below )
- SEL 2H/DEC & SEL OBS-2H INPUTS OPTO-ISOLATED :Input current > 0,5 mA (1,5 V In) => active levelInput current < 0,3 mA (1,0 V In) => unactive level
- High speed TP-FO INPUT OPTO-ISOLATED :Input current > 5 mA (2,8 V In) => active levelInput current < 2 mA (1,2 V In) => unactive level
➪ Don’t exceed TTL Level; it could cause damage to the Input isolation opto-couplers
8 (43) BRUKER Technical Manual Version 004
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Spectrometer environment
Spectrometer environment 1.3
Figure 1.2. Synoptic of 2H Lockswitch in the Spectrometer
Wiring 1.4
Figure 1.3. Front panel wiring
HPPR
1st channel
BB
2nd channel
1H
3rd channel
2H
BSMS-lock
BLKy
2H TR
TP-FOTX-BLNK
RX-BLNK
RX-BLNK outTX-BLNK out
TP-FO in
2H TR in
Sel 2H/Dec
Sel Obs 2H
Sel 2H/Dec
Sel Obs 2H
BB Preamp
Dec 2H in
13C pass
2H LOCKSWITCH
Lockswitch andHPPR 2H BLKelaboration
13C
1H
2H
2H stopBB 1H
Receiver
2HReceiver
Dec/Lock 2HHPPR
TP-FO out
Probe
13C
2H
1H
Lock and 2H decouplingfor AMX and AVANCEequiped with BSMS and HPPRusing T-LX with RF blanking
(13C)
TP-FO OUT
2H LOCKSWITCH 500 MHZ
2H TR IN SEL. OBS-2HBB PREAMP. TP-FO INSEL.2H/DEC DEC/LOCK 2Hto HPPRTX-BLNK OUTRX-BLNK OUT DEC 2H IN
2H TX OUT fromLOCK TRANSMITER
X out TCU programedBLK
TCU OBS 2Hselection
BLK fromX Amplifier
(paralle conected)
General
AuxiliaryBLK OUT
(to BSMS L-TX)
RF POWER from X Amplifier
RF to 2H Probe
Technical Manual Version 004 BRUKER 9 (43)
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General description
10 (43) BRUKER Technical Manual Version 004
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2Control signal & RF signal route 2About polarity selection 2.1
The 3 switches located on the control board (inside the device) allow to solveproblems about input and output standard polarity.
• AMX/ARX polarity or shows that the validation is done at level 1 to outputand at a current flow in the used optocouplers (from BLK inputs).
• AVANCE polarity or shows that the validation is done at level 0 to out-put and with no current flow in the used optocouplers (from BLK inputs).
Internal polarity selection 2.2
Figure 2.1. AVANCE and AMX/ARX Configurations
➪ For the delivery, the jumpers are setted for «AVANCE» configuration
AM
X/A
RX
AV
AN
CE
J10 J9 J7 J8 J13
OB
S-2
H
SE
L2H
/DE
C
TP
-FO
IN
TP
-FO
OU
T
RX
-TX
AVANCEConfiguration
AMX/ARXConfiguration
AM
X/A
RX
AV
AN
CE
J10 J9 J7 J8 J13
OB
S-2
H
SE
L2H
/DE
C
TP
-FO
IN
TP
-FO
OU
T
RX
-TX
Technical Manual Version 004 BRUKER 11 (43)
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Control signal & RF signal route
Output signal polarities function of selected jumpers 2.3
Table 2.1. For RX-TX Blanking in AVANCE configuration
TP-FO OUTPOL SELECT
SEL 2H/DECPOL IN
TP-FOPOL IN
SEL2H/DEC TP-FO INBLMKState
RX & TXBLNK OUT
TP-FO OUTState for
AMX/ARX
TP-FO OUTState forAVANCE
AMX/ARX AMX/ARX
No SignalCurrent
No SignalCurrent
No SignalNo SignalCurrentCurrent
ThroughIsolatedThroughIsolated
1010
0111
1000
AMX/ARX AVANCE
No SignalCurrent
No SignalCurrent
No SignalNo SignalCurrentCurrent
ThroughIsolatedThroughIsolated
1010
1101
0010
AVANCE AMX/ARX
No SignalCurrent
No SignalCurrent
No SignalNo SignalCurrentCurrent
IsolatedThroughIsolatedThrough
0101
1011
0100
AVANCE AVANCE
No SignalCurrent
No SignalCurrent
No SignalNo SignalCurrentCurrent
IsolatedThroughIsolatedThrough
0101
1110
0001
Table 2.2. For RX-TX Blanking in AMX/ARX configuration
TP-FO OUTPOL SELECT
SEL 2H/DECPOL IN
TP-FOPOL IN
SEL2H/DEC TP-FO INBLMKState
RX & TXBLNK OUT
TP-FO OUTState for
AMX/ARX
TP-FO OUTState forAVANCE
AMX/ARX AMX/ARX
No SignalCurrent
No SignalCurrent
No SignalNo SignalCurrentCurrent
ThroughIsolatedThroughIsolated
0101
0111
1000
AMX/ARX AVANCE
No SignalCurrent
No SignalCurrent
No SignalNo SignalCurrentCurrent
ThroughIsolatedThroughIsolated
0101
1101
0010
AVANCE AMX/ARX
No SignalCurrent
No SignalCurrent
No SignalNo SignalCurrentCurrent
IsolatedThroughIsolatedThrough
1010
1011
0100
AVANCE AVANCE
No SignalCurrent
No SignalCurrent
No SignalNo SignalCurrentCurrent
IsolatedThroughIsolatedThrough
1010
1110
0001
12 (43) BRUKER Technical Manual Version 004
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RF signal of DEC 2H IN route
RF signal of DEC 2H IN route 2.4
Table 2.3. For BB PREAMP output device only
SEL OBS 2HPOL IN
SEL OBS 2H Signal from DEC 2H IN routed on
AMX/ARXNo SignalCurrent
BB PREAMP outputDEC/LOCK 2H to HPPR output
AVANCENo SignalCurrent
DEC/LOCK 2H to HPPR outputBB PREAMP output
Technical Manual Version 004 BRUKER 13 (43)
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Control signal & RF signal route
14 (43) BRUKER Technical Manual Version 004
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3Applications 3Applications spectra 3.1
Effect on 13C chloroform line of ± n x 1500Hz 2H decoupling offset switchingagainst on resonance frequency.
Figure 3.1. Resonnance spectum
Observation 13C decoupling 2H and 1H, lock 2HSample 10% EB in CDC13Using «2H LOCK-SWITCH» accessoryDecoupling sequences:- On 1H composit pulse program = WALTZ-16- On 2H composit pulse program = GARP(2H irradiation frequenzy ±1500Hz around on-resonance)
+4500 +3000 +1500 Resonnance -1500 -3000 -4500
Technical Manual Version 004 BRUKER 15 (43)
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Applications
Composit pulse program spectra 3.1.1
Figure 3.2. 1H WALTZ-16 and 2H GARP
Obsevation 13C decoupling 1H, lock 2HSample 10% EB in CDC13Using 2H LOCK-SWITCH accessoryDecoupling sequence :
- On 1H composit pulse program = WALTZ-16
Obsevation 13C decoupling 2H and 1H, lock 2HSample 10% EB in CDC13Using 2H LOCK-SWITCH accessoryDecoupling sequences :
- On 1H composit pulse program = WALT-16- On 2H composit pulse program = GARP
(2H irridaition frequency on resonnance)
Obsevation 13C decoupling 2H and 1H, lock 2HSample 10% EB in CDC13Using 2H LOCK-SWITCH accessoryDecoupling sequences :
- On 1H composit pulse program = WALT-16- On 2H composit pulse program = GARP
(2H irridaition frequency +1500Hz off resonnance)
Obsevation 13C decoupling 2H and 1H, lock 2HSample 10% EB in CDC13Using 2H LOCK-SWITCH accessoryDecoupling sequences :
- On 1H composit pulse program = WALT-16- On 2H composit pulse program = GARP
(2H irridaition frequency -1500Hz off resonnance)
16 (43) BRUKER Technical Manual Version 004
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Applications spectra
Figure 3.3. 1H WALTZ-16 and 2H WALTZ-16
Obsevation 13C decoupling 1H, lock 2HSample 10% EB in CDC13Using 2H LOCK-SWITCH accessoryDecoupling sequence :
- On 1H composit pulse program = WALTZ-16
Obsevation 13C decoupling 2H and 1H, lock 2HSample 10% EB in CDC13Using 2H LOCK-SWITCH accessoryDecoupling sequences :
- On 1H composit pulse program = WALT-16- On 2H composit pulse program = WALT-16
(2H irridaition frequency on resonnance)
Obsevation 13C decoupling 2H and 1H, lock 2HSample 10% EB in CDC13Using 2H LOCK-SWITCH accessoryDecoupling sequences :
- On 1H composit pulse program = WALT-16- On 2H composit pulse program = WALT-16
(2H irridaition frequency +1500Hz off resonnance)
Obsevation 13C decoupling 2H and 1H, lock 2HSample 10% EB in CDC13Using 2H LOCK-SWITCH accessoryDecoupling sequences :
- On 1H composit pulse program = WALT-16- On 2H composit pulse program = WALT-16
(2H irridaition frequency -1500Hz off resonnance)
Technical Manual Version 004 BRUKER 17 (43)
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Applications
Pulse program 3.2
Sequence for AMX, ASX and ARX spectrometer 3.2.1
;zgdc_2h_A;1D sequence for X-nucleus with 1H and 2H decoupling;AMX,ASX and ARX version
d11=30m#define lo_hold_on 45u setf2|9#define lo_hold_off 45u setf2^9#define sel_2h_dec_on 45u setf1^7#define sel_2h_dec_off 45u setf1|7
d11 hl1 cpd dbl0 dbo sel_2h_dec_off1 ze2 d1 dbo lo_hold_off sel_2h_dec_offlo_hold_on sel_2h_dec_ond11 cpdbp1 ph1go=2 ph31lo_hold_off sel_2h_dec_offwr#0d11 do dbo
exit
ph1=0 2 2 0 1 3 3 1ph31=0 2 2 0 1 3 3 1
;hl1: ecoupler power level for CPD decoupling;dbl0: ecoupler power level for CPDB decoupling;p1 : 90 degree transmitter high power pulse;p31: 90 degree pulse for salve timer (cpd-sequence);p30: 90 degree pulse for salve timer (cpdb-sequence);d1 : relaxation delay; 1-5 * T1;d11: delay for disk I/O................[30msec];cpd: cpd-decoupling according to sequence defined by cpdbprg;cpdb: cpdb-decoupling according to sequence defined by cpdbprg
18 (43) BRUKER Technical Manual Version 004
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Pulse program
Sequence for Avance spectrometer DMX, DRX 3.2.2
;zgdc_2h_D1D sequence for X-nucleus with H-1 and H-2 decoupling;Avance spectrometer DMX,DRX;jmt SADIS wissembourg
#include
d11=30m
1 zeH2_LOCK.................;define in Avance.incl setnmr8|4d12 setnmr0|8...........;gating 1H HPPR in case of using 5 preamp. units
2 d11 pl13:f2 do:f3d11 cpds2:f2d1 pl14:f3 H2_LOCK......;define in Avance.incl setnmr8|4d11 cpds3:f3 H2_PULSE...;define in Avance.incl setnmr8|4p1 ph1go=2 ph31 cpds2:f2wr#0d11 do:f2d11 do:f3d12 setnmr0^8
exit
ph1=0 2 2 0 1 3 3 1ph11=0 2 2 0 1 3 3 1
;pl13: decoupler power level for decoupling in CDP mode on H-1;pl14: decoupler power level for decoupling in CDP mode on H-2;p1 : 90 degree transmitter high power pulse;p31: 90 degree pulse for salve timer (cpd2:f2-sequence);p30: 90 degree pulse for salve timer (cpd3:f3-sequence);d1 : relaxation delay; 1-5 * T1;d11: delay for disk I/O................[30msec]
;cpd2:f2: f2-decoupling according to sequence defined by cpdprg2:WALTZ16;cpd3:f3: f3-decoupling according to sequence defined by cpdprg3:WALTZ16f3
Technical Manual Version 004 BRUKER 19 (43)
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Applications
20 (43) BRUKER Technical Manual Version 004
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42H Lockswitch 500MHZ 4
Technical Manual Version 004 BRUKER 21 (43)
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12
Te
345678
J8
2 1
A
B
C
D
P/N:W1342102
REAR PANELFROM FRAME
N
LINE IN
J3
P
DRAWN:DATE:
APPROV:DATE:
DWG:
VISA:
VISA:
SHEET:
DW
W4B132147
03/12/98
PHB
C
15/12/98
1/1
Figure 4.1.
2H Locksw
itch 500MH
Z B
lock Diagram
chn
ical Man
ual V
ersion
004B
RU
KE
R22 (43)
8 7 6 5 4 3
D
C
B
A
P3
J7
DEC 2H IN
DEC/LOCK 2Hto HPPR
J9
BB PREAMP
J1
J3
P1 J2 P2
RELAY SWITCHP/N:73705
COUPLER HP 3dBP/N:W1345141
P2 J2
J3 P3
P1 J1
J2 P2
F1
BLANKING SWITCHBLMK
P/N:W1345135
P1 J1
CP1
J10
2H TR IN
P/N:W1341016FRONT PANEL
J11SEL OBS-2H
TP5 TP6 J3
F1
+15V
220V
POWERSUPPLY
TP1
J1SEL 2H/DEC
J2TP-FO IN
J4TP-FO OUT
J6TX-BLNK OUT
J5RX-BLNK OUT
CONTROL BOARDP/N:W1346044
TP20V
P/N:O56541
F2
TP3
LD1POWERSTATUS
TP4
NOTE :
J8 = 59053 : SMA CONNECTORJ7 = 14848 : N CONNECTOR
LD1 = 32510 : POWER STATUS LED
J3 = 52666 : LINE IN CONNECTOR
J9 = 14848 : N CONNECTORJ10 = 59053 : SMA CONNECTOR
BLOCK DIAGRAM
ART: W1345010
2H LOCKSWITCH UNIT500MHZ
EC: 04
-
5Control Board 5
Technical Manual Version 004 BRUKER 23 (43)
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12
24 (4
345678
2 1
A
B
C
D
2
A04
J3BLKM BLK
OUT
J4TP-FO OUT
R26100
R947.5
J5RX-BLNK OUT
R27100
R5100
4
B04
6
C04
8
D04
10
E04
J6TX-BLNK OUT
R6100
R28100
D21N4007
+15V
TP5+REL
R29100
12
F04
D31N4007
TP6-REL
J12PIN DIODE
SWITCHR2147.5
R1933.2
+5V +5V
C6100NF
U5
CE322UF35V
U3
5V
C5100NF
DRAWN:DATE:
APPROV:DATE:
DWG:
VISA:
VISA:
SHEET:
DW
W4S132122
PHB
12/11/97
13/11/97
G 1/1
S.a.d.i.s
SPECTROSPIN
Figure 5.1.
Control B
oard Schem
atic
3)B
RU
KE
RT
echn
ical Man
ual V
ersion
004
8 7 6 5 4 3
D
C
B
A
+5V
23456
1
RS14.7K
+5V
23456789
1
RS24.7K
J11SEL OBS-2H
R1470
R23.32K
J1SEL 2H/DEC
1
2
8
7
3
4 6
5
U1HCPL-2731
R3470
R43.32K
+5V R22100
R23100
R24100
+5V
IN1 1
IN2 2
IN3 3
IN4 4
IN5 5
IN6 6
IN7 7
IN8 8
IN9 9
GND 10
VCC 20
I/O8 19
I/O7 18
I/O6 17
I/O5 16
I/O4 15
I/O3 14
I/O2 13
I/O1 12
IN10 11
U2EP330
HLS04/01
1
U374HC
R1047.5
3
U374HC
5
U374HC
R1147.5
R25100
R17100
+5V+5V
R201K
1
27
5
8U5A
HCPL-2630J2
TP-FO IN
R161K
R15332
R14100
9
U374HC
11
U374HC
R1247.5
13
U374HC
1 2 3
J8OUT
R13100
RX-TX
R30100
1 2 3
J13SEL
123
J7IN
123
J9SEL
2H/DEC TP-FO
123
J10SEL
OBS-2H
1-2 : AVANCE2-3 : AMX / ARX
T1BS170
R18100
+5V+5V +
C2100NF
U2 U3
C1100NF
U1
+5V
CE222UF35V
C4100NF
C3100NF
R7121
CE122UF35V
R31121
R32121
VI1 VO 2GND
3
U4MC7805CT
TP2DGND
D11N4007
TP3LED K
TP1+15V
+15V
L110UH
TP4LED A +5V
R8470
VCC
ART: W1346044
2H LOCKSWITCHCONTROL BOARD
EC: 09
-
12
Te
345678
+15V
DGND
P2P1
J6
2 1
A
B
C
D
VISA:
VISA:
G SHEET: 1/1
S.a.d.i.s
SPECTROSPIN
Figure 5.2.
Control B
oard Location
chn
ical Man
ual V
ersion
004B
RU
KE
R25 (43)
W4P132122GLED
A
K
AV
AN
CE
AM
X/A
RX
TP
-FO
IN
TP
-FO
OU
T
SE
L2H
/DE
C
OB
S-2
H
-REL+
RX
-TX
J3 J12TP4
TP3
TT
TP6 TP5
U1 U5
U2
J8J7J9J10 J13
R1
R2
R3
R4 R
5
R7
R8
R11
R10
R9
R6
R13
R19
R16
R18
R17R14
R15
R21
R20
R25
R24R23R22
R12
R29
R28R
27
R26
R30
R32
R31C1
C2
C3
C4
C5
C6
D1D3 D2
L1
CE1
CE2
CE3
RS
1
T1
U3
RS
2
J1 J2 J4 J5J11
U4
8 7 6 5 4 3
D
C
B
A ART:
2H LOCKSWITCH
W1346044 DRAWN:DATE:
APPROV:DATE:
DWG:
EC: RC05/01/98
W4L132122
05/01/98PhBCONTROL BOARD
CI : W4P132122G
-
Control Board
Value Table
+------------------------------------------------------------------------------+¦ Part:W1346044 Drawing:W4S132122G Copy In Part: Draw: ¦¦ Desc:2H LOCKSWITCH CIRCUIT CONTROL ECL:9 Modified:03/12/98 By:DW ¦+-- Value Tab ---------------------------------------------------------------+¦ Pos. Component Local Description ¦¦ C01 37167 COND CERM 100N 100V 10% X7R ¦¦ C02 37167 COND CERM 100N 100V 10% X7R ¦¦ C03 37167 COND CERM 100N 100V 10% X7R ¦¦ C04 37167 COND CERM 100N 100V 10% X7R ¦¦ C05 37167 COND CERM 100N 100V 10% X7R ¦¦ C06 37167 COND CERM 100N 100V 10% X7R ¦¦ CE01 10017 COND CHIMI RAD 22U 35V 6.3X7 ¦¦ CE02 10017 COND CHIMI RAD 22U 35V 6.3X7 ¦¦ CE03 10017 COND CHIMI RAD 22U 35V 6.3X7 ¦¦ CI01 W1356617 CI CONTROL 2H LOCKSWITCH ¦¦ D01 355 DIODE 1N4007 ¦¦ D02 355 DIODE 1N4007 ¦¦ D03 355 DIODE 1N4007 ¦¦ ICSU01 4285 IC SUPPORT DIL8 TULIPE ¦¦ ICSU02 9276 IC SUPPORT DIL20 TULIPE ¦¦ ICSU03 4284 IC SUPPORT DIL14 TULIPE ¦¦ ICSU05 4285 IC SUPPORT DIL8 TULIPE ¦¦ J01 22656 CN COAX SMA F C PRT L=29.5MM ¦¦ J02 22656 CN COAX SMA F C PRT L=29.5MM ¦¦ J03 8747 ACCBL PICOT FOURCHE D1.3MM ¦¦ J03' 59995 ACCBL PICOT FOURCHE D1.1MM ¦¦ J04 22656 CN COAX SMA F C PRT L=29.5MM ¦¦ J05 22656 CN COAX SMA F C PRT L=29.5MM ¦¦ J06 22656 CN COAX SMA F C PRT L=29.5MM ¦¦ J07 W1204337 CN M 3 D PRT BARSIL R2.54 H8 ¦¦ J07' 3033 ACCBL CAVALIER F 2.54MM ¦¦ J08 W1204337 CN M 3 D PRT BARSIL R2.54 H8 ¦¦ J08' 3033 ACCBL CAVALIER F 2.54MM ¦¦ J09 W1204337 CN M 3 D PRT BARSIL R2.54 H8 ¦¦ J09' 3033 ACCBL CAVALIER F 2.54MM ¦¦ J10 W1204337 CN M 3 D PRT BARSIL R2.54 H8 ¦¦ J10' 3033 ACCBL CAVALIER F 2.54MM ¦¦ J11 22656 CN COAX SMA F C PRT L=29.5MM ¦¦ J12 8747 ACCBL PICOT FOURCHE D1.3MM ¦¦ J12' 59995 ACCBL PICOT FOURCHE D1.1MM ¦¦ J13 W1204337 CN M 3 D PRT BARSIL R2.54 H8 ¦¦ J13' 3033 ACCBL CAVALIER F 2.54MM ¦¦ L01 30609 SELF 10UH 0.33A ¦¦ R01 2741 RES MET 470 1% 0.6W 50PPM ¦¦ R02 1016 RES MET 3.32K 1% 0.6W 50PPM ¦¦ R03 2741 RES MET 470 1% 0.6W 50PPM ¦¦ R04 1016 RES MET 3.32K 1% 0.6W 50PPM ¦¦ R05 998 RES MET 100 1% 0.6W 50PPM ¦¦ R06 998 RES MET 100 1% 0.6W 50PPM ¦¦ R07 999 RES MET 121 1% 0.6W 50PPM ¦¦ R08 2741 RES MET 470 1% 0.6W 50PPM ¦¦ R09 994 RES MET 47.5 1% 0.6W 50PPM ¦¦ R10 994 RES MET 47.5 1% 0.6W 50PPM ¦¦ R11 994 RES MET 47.5 1% 0.6W 50PPM ¦¦ R12 994 RES MET 47.5 1% 0.6W 50PPM ¦¦ R13 998 RES MET 100 1% 0.6W 50PPM ¦¦ R14 998 RES MET 100 1% 0.6W 50PPM ¦¦ R15 1004 RES MET 332 1% 0.6W 50PPM ¦¦ R16 1010 RES MET 1K 1% 0.6W 50PPM ¦
26 (43) BRUKER Technical Manual Version 004
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+------------------------------------------------------------------------------+¦ Part:W1346044 Drawing:W4S132122G Copy In Part: Draw: ¦¦ Desc:2H LOCKSWITCH CIRCUIT CONTROL ECL:9 Modified:03/12/98 By:DW ¦+-- Value Tab ---------------------------------------------------------------+¦ Pos. Component Local Description ¦¦ R17 998 RES MET 100 1% 0.6W 50PPM ¦¦ R18 998 RES MET 100 1% 0.6W 50PPM ¦¦ R19 992 RES MET 33.2 1% 0.6W 50PPM ¦¦ R20 1010 RES MET 1K 1% 0.6W 50PPM ¦¦ R21 994 RES MET 47.5 1% 0.6W 50PPM ¦¦ R22 998 RES MET 100 1% 0.6W 50PPM ¦¦ R23 998 RES MET 100 1% 0.6W 50PPM ¦¦ R24 998 RES MET 100 1% 0.6W 50PPM ¦¦ R25 998 RES MET 100 1% 0.6W 50PPM ¦¦ R26 998 RES MET 100 1% 0.6W 50PPM ¦¦ R27 998 RES MET 100 1% 0.6W 50PPM ¦¦ R28 998 RES MET 100 1% 0.6W 50PPM ¦¦ R29 998 RES MET 100 1% 0.6W 50PPM ¦¦ R30 998 RES MET 100 1% 0.6W 50PPM ¦¦ R31 999 RES MET 121 1% 0.6W 50PPM ¦¦ R32 999 RES MET 121 1% 0.6W 50PPM ¦¦ RS01 9818 RES RES 4.7KX5 2% SIL6 ¦¦ RS02 7223 RES RES 4.7KX8 2% SIL9 ¦¦ T01 34607 TRANS BS170 N VMOS TO92 ¦¦ TP01 59995 ACCBL PICOT FOURCHE D1.1MM ¦¦ TP02 59995 ACCBL PICOT FOURCHE D1.1MM ¦¦ TP03 59995 ACCBL PICOT FOURCHE D1.1MM ¦¦ TP04 59995 ACCBL PICOT FOURCHE D1.1MM ¦¦ TP05 59995 ACCBL PICOT FOURCHE D1.1MM ¦¦ TP06 59995 ACCBL PICOT FOURCHE D1.1MM ¦¦ U01 14820 OPTO COUP HCPL-2731 DIL8 2-FOI ¦¦ U02 W1356676 IC 220/2H LOCKSWITCH CONTROL ¦¦ U03 10812 IC 7404/MM74HC04N PDIP 14 ¦¦ U04 446 IC 7805/VREG MC7805CT TO220 ¦¦ U05 5941 IC HCPL 2630 ¦+------------------------------------------------------------------------------+
Technical Manual Version 004 BRUKER 27 (43)
-
Figure 5.3. Pal HLS01/01 Schematic
8 7 6 5 4 3 2 1
A
B
C
D
12345678
D
C
B
A
VCC
TPFOOUT
TXBLNKRXBLNK
BLKMOUTIN1 1
IN2 2
IN3 3
IN4 4
IN5 5
IN6 6
IN7 7
IN8 8
IN9 9
GND 10
VCC 20
I/O8 19
I/O7 18
I/O6 17
I/O5 16
I/O4 15
I/O3 14
I/O2 13
I/O1 12
IN10 11
EP330PC-12
SEL2HDEC
GND
TPINPOLTPOUTPOL
SELOBS2H
HLS04/0111/09/96
GND
TPFOINSELPOL
OBS2HPOLRXTXSEL
GND
RESERVEDRESERVEDRESERVED
RELAYOUT
SEL2HDEC 3
9 RXTXSEL
NOT
XOR
NOT
XOR
NOT
NOT
BLKMOUT
RXBLNK
TXBLNK 16
17
19
NOT
NOT
TPFOOUT 18
NOTXOROR2
XOR
NOT
NOT
SELPOL
TPFOIN
TPINPOL
TPOUTPOL
6
7
4
5
SELOBS2H
OBS2HPOL
2
8
XOR NOT
15 RELAYOUT
ART:
HLS04/01PAL 2H LOCKSWITCH
W1356676 EC: DRAWN:DATE:
APPROV:DATE:
DWG:
DW11/09/96
W4D132510
11/09/96PHB
VISA:
VISA:
SHEET: 1/1A
S.a.d.i.s
SPECTROSPIN
28 (43) BRUKER Technical Manual Version 004
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6Blanking Switch BLMK 32-160MHZ 6
Technical Manual Version 004 BRUKER 29 (43)
-
12345678
30 (4
2 1
A
B
C
D
J2RF OUT
8F
C72PF
CI1
VISA:
VISA:
SHEET: 1/1A
Figure 6.1.
Blanking S
witch B
LMK
32-160MH
Z S
chematic
3)B
RU
KE
RT
echn
ical Man
ual V
ersion
004
8 7 6 5 4 3
D
C
B
A
R250
TT40C3
6.8NFC4
6.8NF
R551.1
C64.7PF
1
3
2
4
SW2DH80050
C1N
L41.5UH
1.
R4392
L31.5UH
C51NFL2
1.5UHR3392
L11.5UH
1
3
2
4SW1
DH80050
C21NF
CL150R
J1RF IN
C11NF
R11K
R9470
L51.5UH
R7392
C10390PF
R61K
C96.8NF
R8470
CE122UF
50V
NC1
IA2
GND3
IB4
NC 8
OA 7
V+ 6
OB 5
U1TSC428CPA
R104.7K
CP1BLK1\
F1+15V
ART:
2H LOCKSWITCHBLANKING SWITH BLKMSWITCH 10W / 32-160MHZ
W1345135 DRAWN:DATE:
APPROV:DATE:
DWG:
EC: 01 DW06/11/98
W4S132144
15/12/98PHB
-
Value Table
+------------------------------------------------------------------------------+¦ Part:W1345135 Drawing:W4S132144A Copy In Part: Draw: ¦¦ Desc:COMMUTATEUR BLKM 32-160MHZ ECL:1 Modified:09/11/98 By:DW ¦+-- Value Tab ---------------------------------------------------------------+¦ Pos. Component Local Description ¦¦ C1 30424 COND CMS CDR14 1N 50V 20% ¦¦ C2 30424 COND CMS CDR14 1N 50V 20% ¦¦ C3 56276 COND CERM 6.8N 500V 5% X7R ¦¦ C4 56276 COND CERM 6.8N 500V 5% X7R ¦¦ C5 30424 COND CMS CDR14 1N 50V 20% ¦¦ C6 30396 COND CMS CDR14 4.7P 500V 0.25P ¦¦ C7 30389 COND CMS CDR14 1.2P 500V 0.25P ¦¦ C8 30424 COND CMS CDR14 1N 50V 20% ¦¦ C9 56276 COND CERM 6.8N 500V 5% X7R ¦¦ C10 30419 COND CMS CDR14 390P 200V 20% ¦¦ CE1 1983 COND CHIMI RAD 22U 50V 7X7 ¦¦ CI1 W1356240 CI B-LKM BLANKING SWITCH 10W ¦¦ CP1 56154 COND PAS FILTRE 100P 100V 10A ¦¦ ICSU1 4285 IC SUPPORT DIL8 TULIPE ¦¦ J1 33011 CN COAX SMA F D EMB PLATINE ¦¦ J2 33011 CN COAX SMA F D EMB PLATINE ¦¦ L1 51528 SELF 1.5UH 0.56A ¦¦ L2 51528 SELF 1.5UH 0.56A ¦¦ L3 51528 SELF 1.5UH 0.56A ¦¦ L4 51528 SELF 1.5UH 0.56A ¦¦ L5 51528 SELF 1.5UH 0.56A ¦¦ R1 20737 RES CMS 1K 1% 0.25W 1206 ¦¦ R2 30863 RES HF 50 40W ¦¦ R3 20731 RES CMS 392 1% 0.25W 1206 ¦¦ R4 20731 RES CMS 392 1% 0.25W 1206 ¦¦ R5 20765 RES CMS 51.1 1% 0.25W 1206 ¦¦ R6 20737 RES CMS 1K 1% 0.25W 1206 ¦¦ R7 20731 RES CMS 392 1% 0.25W 1206 ¦¦ R8 51288 RES CMS 475 1% 0.25W 1206 ¦¦ R9 51288 RES CMS 475 1% 0.25W 1206 ¦¦ R10 20745 RES CMS 4.7K 1% 0.25W 1206 ¦¦ RAD1 W1305665 BLAH RADIAT BLANKING SWITCH ¦¦ SW1 30636 DIODE PIN SW 10W ¦¦ SW2 30636 DIODE PIN SW 10W ¦¦ U1 56292 IC 428/DRV TSC428CPA DIP8 ¦+------------------------------------------------------------------------------+
Technical Manual Version 004 BRUKER 31 (43)
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Blanking Switch BLMK 32-160MHZ
32 (43) BRUKER Technical Manual Version 004
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7HP Coupler 3dB 62,5-125MHZ 7
Technical Manual Version 004 BRUKER 33 (43)
-
Figure 7.1. HP Coupler 3dB 62,5-125MHZ Schematic
8 7 6 5 4 3 2 1
A
B
C
D
12345678
D
C
B
A
IN 1
0
2
ISO3
90
4
AN110261-3
J1RF IN 1
J2RF IN 2
R150
150W
CI1
J3RF OUT
HP COUPLER 3dB62.5-125MHZ
2H LOCKSWITCH
ART: W1345141 EC: 01 DRAWN:DATE:
APPROV:DATE:
DWG:
DW31/05/95
W4S132146
31/05/95PHB
VISA:
VISA:
SHEET: 1/1
S.a.d.i.s
SPECTROSPIN
34 (43) BRUKER Technical Manual Version 004
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12345678
Te
2 1
A
B
C
D
VISA:
VISA:
- SHEET: 1/1
S.a.d.i.s
SPECTROSPIN
Figure 7.2.
HP
Coupler 3dB
62,5-125MH
Z Location
chn
ical Man
ual V
ersion
004B
RU
KE
R35 (43)
J1
J3
J2
8 7 6 5 4 3
D
C
B
A ART: W1345141 DRAWN:DATE:
APPROV:DATE:
DWG:
EC: DW10/11/98
W4L132146
10/11/98PhBCOUPLEUR HP 3dB 62.5-125MHz
CI : W4P132448
W4P132448
INIS
O
R1
90°
AN1
0°
-
HP Coupler 3dB 62,5-125MHZ
Value Table
+------------------------------------------------------------------------------+¦ Part:W1345141 Drawing:W4S132146 Copy In Part: Draw: ¦¦ Desc:COUPLEUR HP 3DB / 62.5-125MHZ ECL:1 Modified:22/04/96 By:DW ¦+-- Value Tab ---------------------------------------------------------------+¦ Pos. Component Local Description ¦¦ AN01 56522 IC 10261/COUPL.HF 62.5-125MHZ ¦¦ CI01 W1340016 CI 3DB HP COUPLEUR 62.5-125MHZ ¦¦ J01 6194 CN COAX N F D EMB PLATINE ¦¦ J02 6194 CN COAX N F D EMB PLATINE ¦¦ J03 6194 CN COAX N F D EMB PLATINE ¦¦ R01 20138 RES HF CHARGE 50 OHMS 5% 150W ¦+------------------------------------------------------------------------------+
36 (43) BRUKER Technical Manual Version 004
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8Specifications 82H Lockswitch 500 MHz specifications 8.1
Table 8.1. General requirements
Power requirements 220 V ±10%, 50/60 Hz
Power consumption 15 W
Weight 4 Kg
Dimensions445 / 484 mm width (cabinet / front panel)1 Unit height280 mm depth
Software control XWINNMR or UXNMR
Table 8.2. Insertion loss
Decoupling channel 4 dB ±1dB
Lock channel 4 dB ±1dB
BB channel 1dB maximum
BLK 2H isolation 50 dB Typical
DEC 2H IN / 2H TR IN directivity 20 dB Typical
Table 8.3. Switching time
SEL 2H/DEC 15 µs typical (minimum current for level 1 INPUT : 0,5 mA)
SEL OBS 2H 15 µs typical (minimum current for level 1 INPUT : 0,5 mA)
TP-FO IN 300 ns typical (minimum current for level 1 INPUT : 5 mA)
Polarity selection DMX and AMX for all IN and OUT logical compatible
Table 8.4. Logic fan out
TP-FO OUT & RX BLNK / TX BLNKLevel 0 : 5 mA sink for 0,7 V outLevel 1 : 10 mA source for 1,5 V out
’’2H’’ Frequency range 70 to 80 MHz
DEC 2H IN power capability 600 W
Technical Manual Version 004 BRUKER 37 (43)
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Specifications
38 (43) BRUKER Technical Manual Version 004
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Figures
1 General description 7Figure 1.1. Synoptic of 2H Lockswitch .....................................................7Figure 1.2. Synoptic of 2H Lockswitch in the Spectrometer ......................9Figure 1.3. Front panel wiring ..................................................................9
2 Control signal & RF signal route 11Figure 2.1. AVANCE and AMX/ARX Configurations ............................... 11
3 Applications 15Figure 3.1. Resonnance spectum ..........................................................15Figure 3.2. 1H WALTZ-16 and 2H GARP ...............................................16Figure 3.3. 1H WALTZ-16 and 2H WALTZ-16 .........................................17
4 2H Lockswitch 500MHZ 21Figure 4.1. 2H Lockswitch 500MHZ Block Diagram ................................22
5 Control Board 23Figure 5.1. Control Board Schematic .....................................................24Figure 5.2. Control Board Location ........................................................25Figure 5.3. Pal HLS01/01 Schematic .....................................................28
6 Blanking Switch BLMK 32-160MHZ 29Figure 6.1. Blanking Switch BLMK 32-160MHZ Schematic ....................30
7 HP Coupler 3dB 62,5-125MHZ 33Figure 7.1. HP Coupler 3dB 62,5-125MHZ Schematic ...........................34Figure 7.2. HP Coupler 3dB 62,5-125MHZ Location ..............................35
8 Specifications 37
Technical Manual Version 004 BRUKER 39 (43)
-
Figures
40 (43) BRUKER Technical Manual Version 004
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Tables
1 General description 7
2 Control signal & RF signal route 11Table 2.1. For RX-TX Blanking in AVANCE configuration ................ 12Table 2.2. For RX-TX Blanking in AMX/ARX configuration .............. 12Table 2.3. For BB PREAMP output device only ............................... 13
3 Applications 15
4 2H Lockswitch 500MHZ 21
5 Control Board 23
6 Blanking Switch BLMK 32-160MHZ 29
7 HP Coupler 3dB 62,5-125MHZ 33
8 Specifications 37Table 8.1. General requirements .................................................... 37Table 8.2. Insertion loss ................................................................. 37Table 8.3. Switching time ............................................................... 37Table 8.4. Logic fan out .................................................................. 37
Technical Manual Version 004 BRUKER 41 (43)
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Tables
42 (43) BRUKER Technical Manual Version 004
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Technical Manual Version 004 BRUKER 43 (43)
Lastpage
ContentsIndexGeneral descriptionDescription 1.1Figure 1.1. Synoptic of 2H Lockswitch
Specifications 1.2Spectrometer environment 1.3Figure 1.2. Synoptic of 2H Lockswitch in the Spectrometer
Wiring 1.4Figure 1.3. Front panel wiring
Control signal & RF signal routeAbout polarity selection 2.1Internal polarity selection 2.2Figure 2.1. AVANCE and AMX/ARX Configurations
Output signal polarities function of selected jumpers 2.3Table 2.1. For RX-TX Blanking in AVANCE configurationTable 2.2. For RX-TX Blanking in AMX/ARX configuration
RF signal of DEC 2H IN route 2.4Table 2.3. For BB PREAMP output device only
ApplicationsApplications spectra 3.1Figure 3.1. Resonnance spectumComposit pulse program spectra 3.1.1Figure 3.2. 1H WALTZ-16 and 2H GARPFigure 3.3. 1H WALTZ-16 and 2H WALTZ-16
Pulse program 3.2Sequence for AMX, ASX and ARX spectrometer 3.2.1Sequence for Avance spectrometer DMX, DRX 3.2.2
2H Lockswitch 500MHZFigure 4.1. 2H Lockswitch 500MHZ Block Diagram
Control BoardFigure 5.1. Control Board SchematicFigure 5.2. Control Board LocationFigure 5.3. Pal HLS01/01 Schematic
Blanking Switch BLMK 32-160MHZFigure 6.1. Blanking Switch BLMK 32-160MHZ Schematic
HP Coupler 3dB 62,5- 125MHZFigure 7.1. HP Coupler 3dB 62,5-125MHZ SchematicFigure 7.2. HP Coupler 3dB 62,5-125MHZ Location
Specifications2H Lockswitch 500 MHz specifications 8.1Table 8.1. General requirementsTable 8.2. Insertion lossTable 8.3. Switching timeTable 8.4. Logic fan out
FiguresTables