Ahmad Aqel Abdelfattah IFSEISI - KSU

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Ahmad Aqel Abdelfattah IFSEISI Academician and Researcher… Associate Professor of Analytical Chemistry Department of Chemistry Researcher Advanced Materials Research Chair College of Science King Saud University Riyadh, KSA Work Tel.: +966 11 4676009 Fax: +966 11 4675992 P.O. Box 2455 Riyadh 11451 Saudi Arabia Mobile: +966 505284007 (SA)

+962 795972995 (JOR) Email: [email protected]

[email protected] Web Site: https://fac.ksu.edu.sa/aifseisi Youtube Channel: https://www.youtube.com/user/MrAhmadaqel Author identifiers Orcid iD: 0000-0001-7895-6895 Web of Science: U-5756-2017 Scopus: 36503609900 Place & Date of Birth: Kuwait, Dec. 21, 1982 Nationality: Jordanian

mailto:[email protected]


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EDUCATION

Graduate …

PhD: Analytical Chemistry Rated as Excellent grade (4.74/5) Thesis Title: "Preparation and characterization of novel capillary monolithic columns and application on a modified liquid chromatograph". Advisor: Prof. Abdulrahman A. Alwarthan. Co-Advisor: Prof. Ahmed-Yacine Badjah-Hadj-Ahmed. Courses covered in this program: advanced inorganic chemistry, applied physical chemistry, advanced organic chemistry, different topics in analytical chemistry, advanced studies in instrumental analysis, applied analytical chemistry, selected topics in analytical chemistry, and six comprehensive exams and a personal meeting.

King Saud University, Oct/2008–Nov/2012 Riyadh, Saudi Arabia

MSc: Chemistry, Analytical Chemistry Emphasis Rated as Excellent grade (3.72/4) Thesis Title: "Development of preconcentration method for some pesticides in water samples using carbon nanotubes prior to high performance liquid chromatographic analysis". Advisor: Prof. Amjad H. El-Sheikh. Co-Advisor: Prof. Jamal A. Sweileh. Courses covered in this program: quantum chemistry, mechanistic of organic compounds, advanced analytical analysis, advanced inorganic chemistry, laser and its chemical applications, inorganic reaction mechanisms and applications of complexes, research methods in chemistry and chemical kinetics and dynamics.

The Hashemite University, Oct/2005–Jan/2008 Zarqa, Jordan

College …

BSc: Chemistry Rated as Very Good grade (3.26/4) Graduation Project: "Nicotine: Chemistry, properties and facts", (office, literature and seminar project). Advisor: Prof. Ahmad S. Abu-Shamleh. The Hashemite University, Oct/2001–Jun/2005 Zarqa, Jordan

High School …

The General Secondary Education Certificate (Scientific Stream) Percentage Average: 81.3% Mu'awiyah ibn Abi-Sufyan Secondary School, Sep/2000–Aug/2001 Zarqa, Jordan


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EMPLOYMENT HISTORY

Feb/2020 – Present …

Associate Professor, Chemistry Department, College of Science, King Saud University, Riyadh, Kingdom of Saudi Arabia.

Aug/2013 – Dec/2019 …

Assistant Professor, Chemistry Department, College of Science, King Saud University, Riyadh, Kingdom of Saudi Arabia.

Dec/2012 – Present …

Researcher, Advanced Materials Research Chair, College of Science, King Saud University, Riyadh, Kingdom of Saudi Arabia.

Oct/2008 – Jul/2013 …

Researcher, King Abdullah Institute for Nanotechnology, King Saud University, Riyadh, Kingdom of Saudi Arabia.

Mar/2008 – Aug/2008 …

Researcher, Laboratory of Analytical Chemistry, Chemistry Department, The Hashemite University, Zarqa, Jordan.

Oct/2005 – Oct/2007 …

Teaching Assistant, Chemistry Department, The Hashemite University, Zarqa, Jordan (as a part of a Master student teaching assistantship employment program).

Feb/2004 – Jun/2004 …

Laboratory Demonstrator, Chemistry Department, The Hashemite University, Zarqa, Jordan (as a part of Bachelor student employment program).

EXPERIENCE

• Proposal and supervision of yearly theoretical and practical training courses on different chromatography techniques in cooperation with the Chemistry Department, Saudi Chemical Society, and Advanced Materials Research Chair Laboratories at King Saud University, since 2013–now.

• A member of a committee of preparation and approval of the Applied Chemistry Program and the Environmental Sciences Program (interdisciplinary programs between the Chemistry Department and other Departments at the College of Science), King Saud University, Oct 2018–now.


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• Academic consultant for Chemistry curriculums, students activities designer, and exams reviewer and corrector for MAWHIBA program for gifted and creative students, King Abdulaziz and his Companions Foundation for Giftedness and Creativity, Riyadh, Kingdom of Saudi Arabia. Link: www.mawhiba.org.sa, Apr 2018–now.

• A member of a committee of assessment and development of the experimental sections of the Analytical Chemistry courses, Chemistry Department, King Saud University, Sep 2020–now.

• Scientific and administrative committees: -Promotion of scientific research, College of Science, KSU, Nov 2015–Nov 2016. -Academic accreditation & assessment, Chemistry Department, KSU, Feb 2016–now. -Development and quality, Chemistry Department, KSU, Nov 2016–now. -Statistics, Chemistry Department, KSU, Jan 2018–now.

• Participant in the Organization committees of the following events: -The 7th international chemistry conference, Chemistry beyond borders (Nov 12–14, 2018) Riyadh, Saudi Arabia. Organized by Chemistry Department and Saudi Chemical Society, King Saud University. -The 6th international chemistry conference, New trends in chemistry (Nov 08–10, 2016) Riyadh, Saudi Arabia. Organized by Chemistry Department and Saudi Chemical Society, King Saud University. -The 4th international chemistry conference, Chemistry and its role and application in development (Nov 19–21, 2011) Riyadh, Saudi Arabia. Organized by Chemistry Department, King Saud University.

• A number of theoretical and practical trainings as follows: -Practical training on Waters AcquityTM Ultra Performance LC-Tandem Quadrapole Detector TQD, with MassLynx software, Advanced Materials research Chair Laboratories, Department of Chemistry, College of Science, King Saud University (4–6 Apr 2010). -Theoretical and practical training on Thermo Scientific Trace GC Ultra / FID and TCD, with ChromCard software, Advanced Materials research Chair Laboratories, Department of Chemistry, College of Science, King Saud University (20–24 Mar 2010). -Theoretical and practical training on Thermo Scientific Finnigan Surveyor HPLC, with ChromQuest software, Advanced Materials research Chair Laboratories, Department of Chemistry, College of Science, King Saud University (6–10 Mar 2010).

• A number of training courses in different topics of teaching and active learning provided by Deanship of Skills Development and College of Science at King Saud University and Saudi Digital Library, Riyadh, KSA. Examples: developing university teaching philosophy, strategies for student encouragement, course design and construction, learning theories, learning management system (blackboard), virtual classrooms, critical thinking and active learning, competencies of professional teaching, using Google tools in education, effective college teaching…

• A number of training courses in different topics of scientific research, publishing and databases provided by Deanship of Skills Development at King Saud University and Saudi Digital Library, Riyadh, KSA.


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Examples: web of science certification program, patent constituents and determinants, academic misconduct detection techniques (plagiarism), publication in international journals (ISI), projects and research proposals writing, scientific thesis supervision and discussion skills, international standards and skills in the arbitration of scientific research, searching skills in various e-libraries and scientific platforms…

• A number of training courses and workshops in the quality and academic accreditation provided by the National Center for Academic Accreditation and Assessment, Deanship of Skills Development and College of Science at King Saud University, Riyadh, KSA. Examples: academic programs outcomes evaluation, course specification and report, academic program specification and report, methods of learning outcomes assessment, education evaluation commission standards, program accreditation standards, ISO standards…

• A number of training courses and workshops in the academic leadership, educational guidance, management and skills development provided by Deanship of Skills Development and College of Science at King Saud University, Riyadh, KSA. Examples: project management professional (PMP), designing interactive presentation by Prezi, fast reading skills, multiple intelligences, fundamentals of information security, basics of academic leadership, work stress management, academic advising skills, skills of effective communication…

• The major chromatographic instruments, samples and materials preparation, and characterization techniques used during the course of research work are as follows: HPLC systems … - Waters AcquityTM Ultra Performance LC (with MassLynx 4.1 software). - Dionex UltiMate 3000 nanoLC-Thermo (with Chromeleon 7 software). - Shimadzu semi-preparative LC system, LC-6AD (with LabSolutions software). - Thermo Scientific Finnigan Surveyor LC (with ChromQuest 5.0 software). - Shimadzu UFLC Prominence LC-20AD (with LCsolution software). - Shimadzu LC-2010AHT (with LCsolution software). - Shimadzu LC-6A (Chart Recorder). - Perkin Elmer 785A LC Plus system (Chart Recorder).

GC systems … - Thermo Scientific TSQ Quantum GC-MS (with Xcalibur 2.1 software). - Thermo Scientific Trace GC Ultra / FID and TCD (with ChromCard software). - Shimadzu GC-2025 / FID (with GCsolution software). - Shimadzu GC-2010 Plus for MS-QP2010 SE (with GCsolution software). - Hewlett Packard HP 5890 Series II GC (Chart Recorder).

Other analysis and characterization techniques … - Direct analysis in real time-time of flight-mass spectrometer (DART-ToF-MS); Jeol. - Atomic absorption spectrometer (AAS); Perkin Elmer & Thermo Scientific. - Inductive coupled plasma (ICP); Perkin Elmer & Thermo Scientific. - Scanning electron microscope (SEM); Jeol. - Transmission electron microscope (TEM); Jeol.


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- Spectrophotometer, UV/VIS spectrometer; Thermo Scientific. - FT-IR spectrometer; Thermo Scientific. - X-ray diffraction (XRD); Bruker. - Optical microscope with digital camera; Micromaster Fisher Scientific. - Elemental analyzer; PerkinElmer. - Surface area and pore size analyzer; Nova Quantachrome & Gemini Micromeritics. - Thermal gravimetric analyzer (TGA & DSC); Mettler Toledo. - Packing station system; Restek. - Sonic sifter; Advantech. - Solid phase processor (SPE & SPME); Supelco. - Rotary evaporator; BUCHI.

TEACHING EXPERIENCE

Theoretical Courses …

• General Chemistry Textbooks: (1) Raymond Chang, Jason Overby, Chemistry, 13th ed., 2019, McGraw-Hill, USA. (2) Theodore E. Brown, H. Eugene LeMay, Bruce E. Bursten, Catherine Murphy, Chemistry, The Central Science, 11th ed., 2009, Pearson Education, Inc., USA.

• Fundamentals of Analytical Chemistry Textbooks: (1) Gary D. Christian, Purnendu K. Dasgupta, Kevin A. Schug, Analytical Chemistry, 7th ed., 2013, Wiley, USA. (2) Douglas A. Skoog, Donald M. West, F. James Holler, Stanley R. Crouch, Fundamentals of Analytical Chemistry, 9th ed., 2014, Cengage Learning, USA.

• Spectroscopic Analytical Methods Textbook: Douglas A. Skoog, F. James Holler, Stanley R. Crouch, Principles of Instrumental Analysis, 7th ed., 2018, Cengage Learning, USA.

• Instrumental Methods of Analysis Textbook: Douglas A. Skoog, F. James Holler, Stanley R. Crouch, Principles of Instrumental Analysis, 7th ed., 2018, Cengage Learning, USA.

• Chemical Separation & Chromatographic Methods Textbooks: (1) Douglas A. Skoog, F. James Holler, Stanley R. Crouch, Principles of Instrumental Analysis, 7th ed., 2018, Cengage Learning, USA. (2) Kevin Robards, Paul R. Haddad, Peter E. Jackson, Principles and Practice of Modern Chromatographic Methods, 2012, Elsevier Academic Press, Netherlands.

• Computer Applications in Chemistry Topics include; applications of computer in data analysis and statistics (e.g., Microsoft excel and OriginLab), applications of computer in chemical structure drawing and molecular modeling (e.g., ChemOffice, HyperChem, and ISIS Draw), and applications of computer in literature searching and chemical databases (e.g., Chemical Abstracts Service).

• Research Methods Topics include; developing the hypothesis and the research problem, the scientific thinking, research methodology, literature searching and the chemical databases, academic writing and references management, presenting data, and research ethics and academic integrity.

Laboratory Courses …

• General chemistry.

• Engineering chemistry.

• Basic analytical chemistry.

• Instrumental analysis.


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• Chemical separation & chromatographic methods.

• Spectroscopic analytical methods.

• Industrial analysis.

• Physical chemistry.

• Training on the chemistry instruments. Note: The materials of courses along with their specifications and tutorials are available by the following link: http://fac.ksu.edu.sa/aifseisi/courses

RESEARCH WORK STATUS

Author of more than 70 scientific contributions; 33 original papers, 2 review

articles, 2 patents, 3 book chapters, and 37 presentations in conference

proceedings, symposiums, and workshops. Orcid iD… 0000-0001-7895-6895 Web of Science… Researcher ID: U-5756-2017 h-index: 11, total citations: 689 (Jan 13, 2021) https://publons.com/researcher/3088481/ahmad-aqel/ Scopus… Author ID: 36503609900 h-index: 11, total citations: 728 (Jan 13, 2021) https://www.scopus.com/authid/detail.uri?authorId=36503609900 Google Scholar… h-index: 14, i10-index: 19, total citations: 1018 (Jan 13, 2021) https://scholar.google.com/citations?user=ImJJeVEAAAAJ&hl=en Document and citation trends:

Scopus: Nov 06, 2020.

AREAS OF RESEARCH INTERESTS


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General Research Areas …

• Analytical chemistry.

• Separation and chromatography research.

• Food, pharmaceutical, environmental and natural products analysis.

• Development and validation of analytical methods.

Specific Research Areas …

• Miniaturization in liquid chromatography; towards cheap and green chromatographic techniques.

• Preparation and development of chromatographic columns for HPLC and GC applications (conventional and capillary scales).

• Synthesis and characterization of polymer-based and composite stationary phases for chromatographic applications.

• Solid-phase extraction/microextraction and preconcentration of trace organic and inorganic samples using new adsorbents.

• Sample treatment, separation, purification and characterization of organic and inorganic species.

• Selective preconcentration of environmental and other samples using carbon nanotubes, activated carbon and modified adsorbents. Note: My main research interests in 90 s are available by the following link: https://www.youtube.com/watch?v=RjzV31T-d74

AWARDS & PRIZES

• King Saud University award for scientific excellence, 2014, Riyadh, Saudi Arabia.

• Almarai prize for the Best Research Unit - Advanced Materials Research Chair (Team Award), 2014, Almarai Company, Riyadh, Saudi Arabia.

• A fully-funded award for IUPAC conference (POC2012), Qatar Petroleum Company QAPCO, 2012, Doha, Qatar.

• Vice-rectorate for graduate studies and research prize for the excellence scientific research, 2012, King Saud University, Riyadh, Saudi Arabia.

• A fully-funded PhD. scholarship, 2008, King Abdullah Institute for Nanotechnology, King Saud University, Riyadh, Saudi Arabia.

• The distinct and creator students prize, 2008, Hashemite University, Zarqa, Jordan.

• A fully-funded MSc. scholarship, 2005, Hashemite University, Zarqa, Jordan.

PROJECT GRANTS

• Apr/2020–Now, Co-investigator (CO-I) of the Research group no. RG-1441-433, Vice-rectorate for Graduate Studies and Scientific Research, Deanship of Scientific Research, King Saud University (Budget: 150,000 SR – 40,000 USD).


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Group title: Organic-inorganic composite materials development and related applications.

• Mar/2020–Now, Principle Investigator (PI), Project ID: 2-17-01-001-0053, National Science, Technology and Innovation Plan, King Abdulaziz City for Science and Technology, Riyadh, Saudi Arabia (Budget: 590,000 SR – 157,333 USD). Project title: Preparation of hybrid organic-inorganic monolithic columns for capillary liquid chromatography and gas chromatography applications. This project was recommended by the American Association for the Advancement of Science (AAAS).

• Feb/2020–Now, Co-investigator (CO-I) of the Research group no. RG-1441-358, Vice-rectorate for Graduate Studies and Scientific Research, Deanship of Scientific Research, King Saud University (Budget: 150,000 SR – 40,000 USD). Group title: Advanced materials in environmental analysis and separation techniques.

• Jul/2017–Jun/2018, Co-investigator (CO-I), Project ID: 222-S-38, Deanship of Scientific Research, Princess Nourah bint Abdulrahman University, Riyadh, Saudi Arabia (Budget: 86,200 SR – 22,986 USD). Project title: Determination of some bioactive coumarin compounds in two Convolvulaceae plants using UPLC/MS.

• Jun/2017–Aug/2018, Co-investigator (CO-I), Project ID: DSR-NFG R-17-02-27, Ra’ed Program, Deanship of Scientific Research, King Saud University, Riyadh, Saudi Arabia (Budget: 70,000 SR – 18,666 USD). Project title: Preparation of methacrylate based monolithic capillary columns for pharmaceutical analysis.

• Apr/2017–Mar/2020, Co-investigator (CO-I) of the Research group no. RG-1438-0007, Deanship of Scientific Research, Princess Nourah bint Abdulrahman University, Riyadh, Saudi Arabia (Budget: 200,000 SR – 53,333 USD). Group title: Natural products chemistry and its analysis methods.

• May/2017, Project ID: ST/2017/014, Dae'em program, Research center, King Saud University, Riyadh, Saudi Arabia (Budget: 20,000 SR – 5,333 USD). Project title: Determination of free fatty acids in olive oils by UHPLC-MS.

• Aug/2016–Jul/2017, Co-investigator (CO-I), Project ID: 178-H-37, Deanship of Scientific Research, Princess Nourah bint Abdulrahman University, Riyadh, Saudi Arabia (Budget: 109,400 SR – 29,173 USD). Project title: Preparation of methacrylate based monolithic capillary columns for analysis of aromatic hydrocarbon compounds in some natural samples.


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• Nov/2015–Now, Principle Investigator (PI) of the Research group no. RG-1437-011, Vice-rectorate for Graduate Studies and Scientific Research, Deanship of Scientific Research, King Saud University (Budget: 150,000 SR – 40,000 USD / per 12 months). Group title: Chemical separation and chromatographic methods.

• Sep/2015–Aug/2017, Principle Investigator (PI), Project ID: 14-ADV2447-02, National Science, Technology and Innovation Plan, King Abdulaziz City for Science and Technology, Riyadh, Saudi Arabia (Budget: 1,934,560 SR – 515,882 USD). Project title: Development of metal-organic framework-based materials as a composite stationary phase for chromatographic applications. This project was recommended by AAAS with a total score 10.0/15.0.

• Mar/2014–Feb/2016, Principle Investigator (PI), Project ID: 14-ADV931-02, National Science, Technology and Innovation Plan, King Abdulaziz City for Science and Technology, Riyadh, Saudi Arabia (Budget: 1,608,700 SR – 428,986 USD). Project title: Preparation and characterization of organic polymer based monolithic columns for capillary chromatography applications. This project was highly recommended by AAAS with a total score 12.2/15.0.

• Sep/2013, Project ID: ST/2013/20, Dae'em program, Research center, King Saud University, Riyadh, Saudi Arabia (Budget: 20,000 SR – 5,333 USD). Project title: Preparation and characterization of capillary monolithic columns for liquid chromatographic applications.

• Dec/2010, Project ID: 3/2/163933, Vice Rectorate for Graduate Studies and Scientific Research, King Saud University, Riyadh, Saudi Arabia (Budget: 25,000 SR – 6,666 USD). Project title: Development and application of novel capillary monolithic columns for capillary chromatography.

SUPERVISION OF THESIS (MSc & PhD students) [11] MSc student Mansour Saud Alharbi (Student no. 441100125) Thesis title: “Removal of hazardous pollutants from water using naturally occurring montmorillonite” (current student). [10] MSc student Khaleda Mosaed Alrashidi (Student no. 437204361) Thesis title: “Chromatographic fingerprint and the direct analysis of the major bioactive components of some medicinal plants growing in Saudi Arabia” (current student). [9] MSc student Amjad Abdullah Altwaim (Student no. 436203547) Thesis title: “Fractionation, characterization and analysis of phenolic compounds in some medicinal plants growing in Saudi Arabia” (current student).


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[8] MSc student Raed Mansour Alafra’a (Student no. 437106628) Thesis title: “Chromatographic evaluation of some narcotic drugs illegally produced or seized in Saudi Arabia” (current student). [7] PhD student Rabab Ali Hakami (Student no. 435203508) Thesis title: “Determination of pesticides residues in cereals using gas chromatography and mass spectrometry techniques”, Dissertation defense date: 01 Jun 2020. [6] PhD student Ahmad Muiid Alammari (Student no. 437105913) Thesis title: “Development of high-throughput chromatographic methods for analysis of bisphenolic compounds in food using UPLC-MS/MS and monolithic stationary phases”, Dissertation defense date: 13 May 2020. [5] MSc student Norah Mohammed Alkatheri (Student no. 436204034) Thesis title: “Application of metal-organic frameworks as stationary phase in high-performance liquid chromatography”, Dissertation defense date: 14 Mar 2019. [4] MSc student Tariq Aziz Alomari (Student no. 437105789) Thesis title: “Assessment of trace metal contamination in three marine fishes, seagrass and macro algae from the Saudi Arabian coast of the Arabian Gulf”, Dissertation defense date: 23 Apr 2018. [3] MSc student Soad Saad Al-Zahrani (Student no. 434203177) Thesis title: “Preparation of methacrylate-based monolithic capillary columns for determination of some aromatic hydrocarbons in water”, Dissertation defense date: 31 May 2017. [2] MSc student Mohammad Ibrahim Al-Turki (Student no. 435107952) Thesis title: “Determination of BTX pollutants in water samples using capillary liquid chromatography”, Dissertation defense date: 05 May 2016. [1] MSc student Abdullah German Al-Enezi (Student no. 434107056) Thesis title: “Separation and characterization of some constituents of Arabian crude oil by gas chromatography-tandem mass spectrometry and time-of-flight mass spectrometry”, Dissertation defense date: 02 Mar 2016.

THESIS EXAMINATION COMMITTEES MEMBER [2] MSc student Ahmed Abdulrahman Almulla (Student no. 431105513) Thesis title: “Fast determination of xanthine compounds in tea samples by liquid chromatography techniques with spectrophotometry and mass spectrometry methods”, Dissertation defense date: 27 Dec 2017. King Saud University, Riyadh, Saudi Arabia. [1] MSc student Raja Saad Al-Otaibi (Student no. 432202541)


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Thesis title: “Separation and characterization of chiral constituents in essential oil extracted from mint (Mentha spicata L.) by GC-MS and DART-TOF-MS”, Dissertation defense date: 19 May 2016. King Saud University, Riyadh, Saudi Arabia.

SUPERVISION OF GRADUATION PROJECTS (BSc students) [7] Wafaa Jar-Allah Alghamdi (Student no. 435201708) Project title: “Preparation of metal-organic framework MIL-53 (Al) as stationary phase for HPLC analysis of caffeine in food”, second semester 2018/2019. [6] Abdullah Abdelkareem Alshawmar (Student no. 435106493) Project title: “Identification and determination of some phenolic compounds in Calendula tripterocarpa plant”, second semester 2017/2018. [5] Nasser Musfir Alqhtani (Student no. 434103152) Project title: “Montmorillonite based liquid chromatography stationary phase for drugs analysis”, first semester 2017/2018. [4] Abdulaziz Muniir Almutairi (Student no. 434101812) Project title: “Preparation of hexylmethacrylate monolithic column for gas chromatography applications”, first semester 2017/2018. [3] Abdullah Khalaf Al-Lohian (Student no. 433105716) Project title: “Preparation of polymer-based capillary monolithic column for analysis of PAHs in water”, second semester 2016/2017. [2] Faisal Gedaii Al-Enezi (Student no. 431106079) Project title: “Development and validation of HPLC method for analysis of paracetamol and chlorzoxazone using home-made phenyl-hexyl methacrylate packed column”, first semester 2016/2017. [1] Ahmad Mohammad Alqahtani (Student no. 432101970) Project title: “Determination of aromatic hydrocarbon pollutants in water samples using capillary liquid chromatography”, second semester 2015/2016.

LIST OF PUBLICATIONS

I. Original Articles …

[33] Ahmad Aqel, Asma A. Alothman, Wafa J. Alghamdi, Norah Alkatheri, Amal M. Al-Mohaimeed, Ayman Ghafer, Zeid A. ALOthman, Ahmed-Yacine Badjah-Hadj-Ahmed, Synthesis of value-added MIL-53(Cr) from waste polyethylene terephthalate bottles for the high-performance liquid chromatographic determination of methylxanthines in tea, Microchemical Journal (Accepted).


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[32] Mohammad R. Khan, Ahmad M. AlAmmari, Ahmad Aqel, Mohammad Azam, Trace analysis of environmental endocrine disrupting contaminant bisphenol A in canned, bottled glass and polyethylene terephthalate plastic carbonated beverages of diverse flavors and country of origins, Food Science and Technology (doi: 10.1590/fst.03420). [31] Rabab A. Hakami, Ahmad Aqel, Ayman A. Ghafr, Zeid A. ALOthman, Ahmed-Yacine Badjah-Hadj-Ahmed, Development of QuEChERS extraction method for the determination of pesticide residues in cereals using DART-ToF-MS and GC-MS techniques. Correlation and quantification study, Journal of Food Composition and Analysis (2021) 103822 (IF: 3.712, 2020). [30] Ahmad Aqel, Norah Alkatheri, Ayman Ghafer, Ameen M. Alsubhi, Zeid A. ALOthman, Ahmed-Yacine Badjah-Hadj-Ahmed, Preparation of value-added metal-organic frameworks for high-performance liquid chromatography. Towards green chromatographic columns, Journal of Chromatography A 1638 (2021) 461857 (IF: 4.512, 2020). [29] Mutaz E. Salih, Ahmad Aqel, Babiker Y. Abdulkhair, Munir S. Obbed, Zeid A. ALOthman, Ahmed-Yacine Badjah-Hadj-Ahmed, Mohamad A. Abdulaziz, Preparation and characterization of glycidyl polymethacrylate monolith column and its application for simultaneous determination of paracetamol and chlorzoxazone in their combined pharmaceutical formulations, Journal of Analytical Chemistry 75 (2020) 1435–1442 (IF: 0.840, 2019). [28] Asma’a Al-Rifai, Ahmad Aqel, Muneera Al-Saleem, Development and validation of a rapid and efficient method for simultaneous determination of scopolin and scopoletin in Convolvulus species by ultra-high-performance liquid chromatography-tandem mass spectrometry, Current Pharmaceutical Analysis 16 (2020) 494–503 (IF: 0.923, 2019). [27] Ahmad Aqel, Soad S. Alzahrani, Asma’a Al-Rifai, Mohammed Alturkey, Kareem Yusuf, Zeid A. ALOthman, Ahmed-Yacine Badjah-Hadj-Ahmed, Determination of monoaromatic hydrocarbons in water samples by nano-liquid chromatography using a composite carbon nanotubes-lauryl polymethacrylate capillary monolithic column, Current Analytical Chemistry 16 (2020) 223–233 (IF: 1.365, 2019). [26] Ahmad M. AlAmmari, Mohammad R. Khan, Ahmad Aqel, Trace identification of endocrine-disrupting bisphenol A in drinking water by solid-phase extraction and ultra-performance liquid chromatography-tandem mass spectrometry, Journal of King Saud University - Science 32 (2020) 1634–1640 (IF: 3.819, 2019). [25] Ahmad Aqel, Ahmed Almulla, Asma’a Al-Rifai, Saikh M. Wabaidur, Zeid A. ALOthman, Ahmed-Yacine Badjah-Hadj-Ahmed, Rapid and sensitive


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determination of methylxanthines in commercial brands of tea using ultra-high performance liquid chromatography-mass spectrometry, International Journal of Analytical Chemistry 2019 (2019) 2926580 (IF: 1.682, 2018). [24] Norah Albekairi, Ahmad Aqel, Zeid A. ALOthman, Simultaneous capillary liquid chromatography determination of drugs in pharmaceutical preparations using tunable platforms of polymethacrylate monolithic columns modified with octadecylamine, Chromatographia 82 (2019) 1003–1015 (IF: 1.552, 2018). [23] Mutaz E. Salih, Ahmad Aqel, Babiker Y. Abdulkhair, Zeid A. ALOthman, Mohamad A. Abdulaziz, Ahmed-Yacine Badjah-Hadj-Ahmed, Simultaneous determination of paracetamol and chlorzoxazone in their combined pharmaceutical formulations by reversed-phase capillary liquid chromatography using a polymethacrylate monolithic column, Journal of Chromatographic Science 56 (2018) 819–827 (IF: 1.037, 2017). [22] Munir S. Obbed, Ahmad Aqel, Zeid A. ALOthman, Ahmed-Yacine Badjah-Hadj-Ahmed, Preparation, characterization and application of polymethacrylate-based monolithic columns for fast and efficient separation of alkanes, alcohols, alkylbenzenes and isomeric mixtures by gas chromatography, Journal of Chromatography A 1555 (2018) 89–99 (IF: 3.716, 2017). [21] Asma’a Al-Rifai, Ahmad Aqel, Lamya Al Wahibi, Zeid A. ALOthman, Ahmed-Yacine Badjah-Hadj-Ahmed, Carbon nanotube-based benzyl polymethacrylate composite monolith as a solid phase extraction adsorbent and a stationary phase material for simultaneous extraction and analysis of polycyclic aromatic hydrocarbon in water, Journal of Chromatography A 1535 (2018) 17–26 (IF: 3.716, 2017). [20] Asma’a Al-Rifai, Ahmad Aqel, Tarfah Al-Warhi, Saikh M. Wabaidur, Zeid A. Al-Othman, Ahmed-Yacine Badjah-Hadj-Ahmed, Antibacterial, antioxidant activity of ethanolic plant extracts of some Convolvulus species and their DART-ToF-MS profiling, Evidence-Based Complementary and Alternative Medicine 2017 (2017) 5694305 (IF: 1.740, 2016). [19] Ahmad Aqel, Zeid A. ALOthman, Ahmed-Yacine Badjah-Hadj-Ahmed, Incorporation of micro and nanoparticles in porous polymer monolithic columns for capillary liquid chromatography application, Journal of Chromatography and Separation Techniques 8 (2017) 43 (IF: 1.010, 2016). [18] Kareem Yusuf, Ahmad Aqel, Amro Dyab, Zeid A. ALOthman, Ahmed-Yacine Badjah-Hadj-Ahmed, Effect of sporopollenin microparticle incorporation into the hexyl methacrylate-based monolithic columns for capillary liquid chromatography, Journal of Liquid Chromatography and Related Technologies 39 (2016) 752–761 (IF: 0.630, 2015).


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[17] Saikh M. Wabaidur, Ahmad M. AlAmmari, Ahmad Aqel, Saad A. AL-Tamarah, Zeid A. Alothman, Ahmed-Yacine Badjah-Hadj-Ahmed, Determination of free fatty acids in olive oils by UHPLC-MS, Journal of Chromatography B 1031 (2016) 109–115 (IF: 2.687, 2015). [16] Ahmad Aqel, Abdulrhman M. Dhabbah, Kareem Yusuf, Nasser M. AL-Harbi, Zeid A. ALOthman, Ahmed-Yacine Badjah-Hadj-Ahmed, Determination of gasoline and diesel residues on wool, silk, polyester and cotton materials by SPME-GC-MS, Journal of Analytical Chemistry 71 (2016) 730–736 (IF: 0.694, 2015). [15] Kareem Yusuf, Ahmed-Yacine Badjah-Hadj-Ahmed, Ahmad Aqel, Taieb Aouak, Zeid A. Al-Othman, Zeolitic imidazolate framework-methacrylate composite monolith characterization by inverse gas chromatography, Journal of Chromatography A 1443 (2016) 233–240 (IF: 3.926, 2015). [14] Kareem Yusuf, Ahmed-Yacine Badjah-Hadj-Ahmed, Ahmad Aqel, Zeid A. Al-Othman, Monolithic metal-organic framework MIL-53(Al)-polymethacrylate composite column for the reverse phase capillary liquid chromatography separation of small aromatics, Journal of Separation Science 39 (2016) 880–888 (IF: 2.741, 2015). [13] Kareem Yusuf, Ahmed-Yacine Badjah-Hadj-Ahmed, Ahmad Aqel, Zeid A. Al-Othman, Fabrication of zeolitic imidazolate framework-8-methacrylate monolith composite capillary columns for fast gas chromatographic separation of small molecules, Journal of Chromatography A 1406 (2015) 299–306 (IF: 4.169, 2014). [12] Asma’a Al-Rifai, Ahmad Aqel, Amani Awad, Zeid A. ALOthman, Analysis of quercetin and kaempferol in alcoholic extract of Convolvulus pilosellifolius using HPLC, Communications in Soil Science and Plant Analysis 46 (2015) 1411–1418 (IF: 0.390, 2014). [11] Ahmad Aqel, Kareem Yusuf, Zeid A. ALOthman, Ahmed-Yacine Badjah-Hadj-Ahmed, Sporopollenin microparticle-based monolithic capillary columns for liquid chromatography, Chromatographia 78 (2015) 481–486 (IF: 1.411, 2014). [10] Hessa Alshemari, Ahmad Aqel, Zeid A. ALOthman, Preparation of high porous poly(2-ethylhexyl methacrylate-co-ethylene glycol dimethacrylate) monolithic columns for fast separation of small molecules, Asian Journal of Chemistry 26 (2014) 8223–8228 (IF: 0.355, 2013). [9] Asma’a Al-Rifai, Amani Awad, Ahmad Aqel, Bioguded fractionation and isolation of natural anti-ulcergenic compounds and anti-Heliobactor pylori from Concolvuus austroaegptaus, Natural Products Chemistry and Research 2 (2014) 160 (IF: 1.70, 2016).


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[8] Abdulrhman M. Dhabbah, Sultan N. Al-Jaber, Ahmad H. Al-Ghamdi, Ahmad Aqel, Determination of gasoline residues on carpets by SPME-GC-MS technique, Arabian Journal for Science and Engineering 39 (2014) 6749–6756 (IF: 0.367, 2013). [7] Ahmad Aqel, Zeid A. ALOthman, Ahmed-Yacine Badjah-Hadj-Ahmed, Kareem Yusuf, Abdulrahman A. Alwarthan, Preparation and evaluation of benzyl methacrylate monoliths for capillary chromatography, Journal of Chromatographic Science 52 (2014) 201–210 (IF: 1.026, 2013). [6] Kareem Yusuf, Ahmad Aqel, Zeid A. Al-Othman, Ahmed-Yacine Badjah-Hadj-Ahmed, Preparation and characterization of alkyl methacrylate-based monolithic columns for capillary gas chromatography applications, Journal of Chromatography A 1301 (2013) 200–208 (IF: 4.612, 2012). [5] Ahmad Aqel, Kareem Yusuf, Zeid A. Al-Othman, Ahmed-Yacine Badjah-Hadj-Ahmed, Abdulrahman A. Alwarthan, Effect of multi-wall carbon nanotubes incorporation to benzyl methacrylate monolithic columns in capillary liquid chromatography, Analyst 137 (2012) 4309–4317 (IF: 4.230, 2011). [4] Zeid A. Al-Othman, Ahmad Aqel, Muteb K.E. Al Badrani, Ahmed-Yacine Badjah-Hadj-Ahmed, Abdulrahman A. Alwarthan, Fast chromatographic determination of caffeine in food using a capillary hexyl methacrylate monolithic column, Food Chemistry 132 (2012) 2217–2223 (IF: 3.655, 2011). [3] Zeid A. Al-Othman, Ahmad Aqel, Hadeel A. Al Abdelmoneim, Ahmed-Yacine Badjah-Hadj-Ahmed, Abdulrahman A. Alwarthan, Preparation and evaluation of long chain alkyl methacrylate monoliths for capillary chromatography, Chromatographia 74 (2011) 1–8 (IF: 1.075, 2010). [2] Amjad H. El-Sheikh, Jamal A. Sweileh, Yahya S. Al-Degs, Ahmad A. Insisi, Nancy Al-Rabady, Critical evaluation and comparison of enrichment efficiency of multi-walled carbon nanotubes, C18 silica and activated carbon towards some pesticides from environmental waters, Talanta 74 (2008) 1675–1680 (IF: 3.374, 2007). [1] Amjad H. El-Sheikh, Ahmad A. Insisi, Jamal A. Sweileh, Effect of oxidation and dimensions of multi-walled carbon nanotubes on solid phase extraction and enrichment of some pesticides from environmental waters prior to their simultaneous determination by high performance liquid chromatography, Journal of Chromatography A 1164 (2007) 25–32 (IF: 3.096, 2006).

II. Review Articles …


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[2] Kareem Yusuf, Ahmad Aqel, Zeid A. ALOthman, Metal organic frameworks in chromatography, Journal of Chromatography A 1348 (2014) 1–16 (IF: 4.612, 2013). [1] Ahmad Aqel, Kholoud M. M. Abou El-Nour, Reda A. A. Ammar, Abdulrahman Alwarthan, Carbon nanotubes, science and technology part (I): structure, synthesis and characterization, Arabian Journal of Chemistry 5 (2012) 1–23 (IF: 1.367, 2011).

III. Patents …

[2] Ahmad Aqel, Ayman A. Ahmed, Ahmed-Yacine Badjah-Hadj-Ahmed, Zeid A. Al-Othman, Montmorillonite-Based Liquid Chromatography Column, Application number: 16/267,348 (United States Patent and Trademark Office, International Protection), Attorney Docket no. 33007.48, Date of filing: Feb. 04, 2019, Publication number: US 2020/0246777 A1, Publication date: Aug. 6, 2020. [1] Abdulrahman Alwarthan, Ahmed-Yacine Badjah-Hadj-Ahmed, Zeid A. Al-Othman, Ahmad Aqel, Liquid Chromatography Device, Application number: EP12154228.6, Grant number: EP2626697B1 (European Patent Office, International Protection), EPO FB26211, File number: 102011-00387, Date of filing: Feb. 07, 2012, Date of publication of application: Aug. 14, 2013, Date of publication and mention of the grant of the patent: Oct. 31, 2018.

IV. Chapters in Books …

[3] Ahmad Aqel, Title of the chapter: Using of nanomaterials to enhance the separation efficiency of monolithic columns, Title of the book: Nanomaterials in Chromatography: Current Trends in Chromatographic Research Technology and Techniques (edited by: Chaudhery M. Hussain), Elsevier Inc., Amsterdam, Netherlands, 2018, Chapter 10, pp. 299–322. [2] Ahmad Aqel, Kareem Yusuf, Asma’a Al-Rifai, Zeid A. ALOthman, Title of the chapter: Vitamin analysis in food by UPLC-MS, Title of the book: Ultra Performance Liquid Chromatography Mass Spectrometry: Evaluation and Applications in Food Analysis (edited by: Mu. Naushad, M. R. Khan), CRC Press, Taylor & Francis Group, New York, USA, 2014, Chapter 10, pp. 243–278. [1] Kareem Yusuf, Ahmad Aqel, Ayman Abdel Ghfar, Zeid A. ALOthman, Title of the chapter: UPLC-MS as an analytical tool for the determination of aflatoxins in food, Title of the book: Ultra Performance Liquid Chromatography Mass Spectrometry: Evaluation and Applications in Food Analysis (edited by: Mu. Naushad, M. R. Khan), CRC Press, Taylor & Francis Group, New York, USA, 2014, Chapter 11, pp. 279–306.

V. Conferences, Symposiums, & Workshops …


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[37] Ahmad Aqel, General Webinar Lecture entitled: “Fundamentals of Separation and Chromatographic Analysis”, (Nov 23, 2020). Link: https://bit.ly/2KN07QG [36] Ahmad Aqel, General Webinar Lecture entitled: “High-performance liquid chromatography, fundamentals and applications”, (Aug 07, 2019). Link: https://register.gotowebinar.com/recording/3858686980343432194. [35] Ahmad Aqel, General Webinar Lecture entitled: “Gas chromatography, fundamentals and applications”, (Feb 27, 2019). Link: https://register.gotowebinar.com/recording/7921513283297966850. [34] Ahmad Aqel, General Webinar Lecture entitled: “An introduction to chromatographic separations”, (Feb 27, 2019). Link: https://register.gotowebinar.com/recording/7921513283297966850. [33] Ameen M. Alsubhi, Ahmad Aqel, Zeid A. ALOthman, Ahmed-Yacine Badjah-Hadj-Ahmed, Mohamed R. Siddiqi, Developing of capillary column using functionalized graphene and graphene oxide nanosheets as stationary phase for gas chromatography, The 7th international chemistry conference, Chemistry beyond borders (Nov 12–14, 2018) Riyadh, Saudi Arabia. [32] Ahmad M. AlAmmari, Mohammad R. Khan, Ahmad Aqel, Zeid A. ALOthman, Development of chromatographic methods for analysis of bisphenolic compounds in food using UPLC-MS/MS and monolithic stationary phases, The 7th international chemistry conference, Chemistry beyond borders (Nov 12–14, 2018) Riyadh, Saudi Arabia. [31] Asma’a Al-Rifai, Ahmad Aqel, Zeid ALOthman, High-throughput quantification of scopolin and scopoletin in Convolvulus species by ultra-high performance liquid chromatography-tandem mass spectrometry, The 7th international chemistry conference, Chemistry beyond borders (Nov 12–14, 2018) Riyadh, Saudi Arabia. [30] Asma’a Al-Rifai, Ahmad Aqel, Amani Awad, Zeid A. ALOthman, Analysis of quercetin and kaempferol in alcoholic extract of Convolvulus pilosellifolius using HPLC, Scientific research forum, Deanship of Scientific Research, King Saud University (Feb 18–22, 2018) Riyadh, Saudi Arabia. [29] Ahmad Aqel, Incorporation of micro and nanoparticles in porous polymer monolithic columns for capillary liquid chromatography application, The 3rd international conference and exhibition on advances in chromatography & HPLC techniques (Jul 13–14, 2017) Berlin, Germany.


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[28] Ahmad Aqel, Chromatographic methods: mechanisms and applications, Advanced chromatographic applications - Workshop (Mar 29, 2017) King Saud University, Riyadh, KSA. [27] Ahmad Aqel, Preparation and evaluation of polymethacrylate monolithic columns for capillary liquid chromatography application, The 6th international chemistry conference, New trends in chemistry (Nov 08–10, 2016) Riyadh, Saudi Arabia. [26] Ahmad Aqel, Kareem Yusuf, Zeid A. ALOthman, Ahmed-Yacine Badjah-Hadj-Ahmed, Modification of a conventional liquid chromatograph for capillary scale columns applications, The 42th international symposium on high performance liquid phase separations and related techniques, PSA-MICRO-04 (Jun 21–25, 2015) Geneva, Switzerland. [25] Kareem Yusuf, Ahmad Aqel, Ahmed-Yacine Badjah-Hadj-Ahmed, Zeid A. ALOthman, Incorporation of sporopollenin microparticles to hexyl methacrylate monolithic columns in capillary liquid chromatography, The 42th international symposium on high performance liquid phase separations and related techniques, PSB-COL-26 (Jun 21–25, 2015) Geneva, Switzerland. [24] Ahmad Alammari, Ahmad Aqel, Siaikh Wabaidur, Zeid A. ALOthman, Ahmed-Yacine Badjah-Hadj-Ahmed, Determination of some free fatty acids in plant oils using ultra-performance LC-ESI-MS, The 42th international symposium on high performance liquid phase separations and related techniques, PSA-FOOD-28 (Jun 21–25, 2015) Geneva, Switzerland. [23] Ahmad Aqel, Application of some micro and nanoparticles for monolithic capillary columns preparation, Environmental applications of nanotechnology - Workshop (Mar 29 – Apr 1, 2015) King Saud University, Riyadh, KSA. [22] Asma’a A. Al-Rifai, Amani S. Awad, Ahmad Aqel, Bioguided fractionation and isolation of natural anti-ulcerogenic compounds and anti-Helicobacter pylori from Convolvulus austroaegyptiacus, The 2nd international conference and exhibition on pharmacognosy, phytochemistry & natural products (Aug 25–27, 2014) Beijing, China. [21] Ahmad Aqel, Kareem Yusuf, Zeid A. ALOthman, Amro Dyab, Ahmed-Yacine Badjah-Hadj-Ahmed, Using of sporopollenin microparticles to enhance the liquid chromatographic separation of ketonic molecules, The 41th international symposium on high performance liquid phase separations and related techniques, P-M-0505 (May 11–15, 2014) New Orleans, Louisiana, USA. [20] Kareem Yusuf, Ahmad Aqel, Ahmed-Yacine Badjah-Hadj-Ahmed, Zeid A. ALOthman, Preparation of novel functional polymeric monoliths for specific capillary liquid chromatographic separations, The 41th international symposium


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on high performance liquid phase separations and related techniques, P-M-0504 (May 11–15, 2014) New Orleans, Louisiana, USA. [19] Zeid A. ALOthman, Ahmad Aqel, Kareem Yusuf, Ahmed-Yacine Badjah-Hadj-Ahmed, Abdulrahman A. Alwarthan, Effect of polymeric mixture composition on porous and chromatographic properties of monolithic benzyl methacrylate-based capillary columns, The 5th international chemistry conference, Chemistry for durable globe and society welfare (Apr 26–29, 2014) King Khalid University, Abha, Saudi Arabia. [18] Ahmad Aqel, Kareem Yusuf, Zeid A. ALOthman, Ahmed-Yacine Badjah-Hadj-Ahmed, Preparation, characterization and application of methacrylate monolithic columns for capillary liquid chromatography, The 39th international symposium on high performance liquid phase separations and related techniques, PO-MONO-02-TU (Jun 16–20, 2013) Amsterdam, The Netherlands. [17] Kareem Yusuf, Ahmad Aqel, Amro Dyab, Zeid A. ALOthman, Ahmed-Yacine Badjah-Hadj-Ahmed, Incorporation of sporopollenin particles into polymethacrylate based monolithic capillary columns to be use as templates for HPLC separations, The 39th international symposium on high performance liquid phase separations and related techniques, PO-MONO-23-TU (Jun 16–20, 2013) Amsterdam, The Netherlands. [16] Hessa K. Al-Shammari, Ahmad Aqel, Zeid A. ALOthman, Stearyl methacrylate monolithic capillary columns, preparation, characterization and qualitative analysis of drugs, The 1st chemistry students meeting (Apr 30 – May 1, 2013) King Saud University, Riyadh, Saudi Arabia. [15] Hadeel A. Al-Abdelmoneim, Zeid A. ALOthman, Ahmad Aqel, Long chain alkyl methacrylate monolithic columns for capillary liquid chromatography, The 1st chemistry students meeting (Apr 30 – May 1, 2013) King Saud University, Riyadh, Saudi Arabia. [14] Eman Al-Damegh, Zeid A. ALOthman, Ahmad Aqel, Functionalization of silica gel with aminoazole derivatives for determination of copper and cadmium by flame atomic absorption spectrometry, The 1st chemistry students meeting (Apr 30 – May 1, 2013) King Saud University, Riyadh, Saudi Arabia. [13] Ahmad Aqel, Development and application of methacrylate monolithic columns for capillary liquid chromatography, The 7th Singapore international chemical conference and 12th Asia-Pacific international symposium on capillary electrophoresis and microscale separation and analysis, SICC7 (Dec 16–19, 2012) National University of Singapore, Singapore. [12] Abdulrahman A. Alwarthan, Ahmad Aqel, Incorporation of carbon nanotube into organic polymer monolithic columns for capillary liquid chromatography,


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Hybrid and organic photovoltaics conference, nanoGe - HOPV2012, PO-79 (May 6–9, 2012) Uppsala, Sweden. [11] Ahmad Aqel, Kareem Yusuf, Zeid A. Al-Othman, Ahmed-Yacine Badjah-Hadj-Ahmed, Abdulrahman A. Alwarthan, Incorporation of multi-walled carbon nanotube into organic polymer monolithic columns for capillary liquid chromatography, The 14th international union of pure and applied chemistry (IUPAC) conference on polymers and organic chemistry, POC2012, PO-123 (Jan 6–9, 2012) Doha, Qatar. [10] Ahmad Aqel, Development and application of capillary monolithic columns for liquid chromatography, The 4th international chemistry conference, Chemistry and its role and application in development (Nov 19–21, 2011) King Saud University, Riyadh, Saudi Arabia. [9] Ahmad Aqel, Kareem Yusuf, Zeid A. Al-Othman, Ahmed-Yacine Badjah-Hadj-Ahmed, Abdulrahman A. Alwarthan, Preparation, characterization and application of benzyl methacrylate capillary monolithic columns, The 4th international chemistry conference, Chemistry and its role and application in development, POA-19 (Nov 19–21, 2011) King Saud University, Riyadh, Saudi Arabia. [8] Kareem Yusuf, Ahmad Aqel, Ahmed-Yacine Badjah-Hadj-Ahmed, Zeid A. Al-Othman, Preparation, characterization and application of polyalkyl methacrylate monolithic columns in gas chromatography, The 4th international chemistry conference, Chemistry and its role and application in development, POA-29 (Nov 19–21, 2011) King Saud University, Riyadh, Saudi Arabia. [7] Ahmad Aqel, Hadeel A. Al Abdelmoneim, Ahmed-Yacine Badjah-Hadj-Ahmed, Zeid A. Al-Othman, Abdulrahman A. Alwarthan, Preparation, characterization and application of alkyl methacrylate monolithic columns for capillary chromatography, The 1st United Arab Emirates conference on pure and applied chemistry, ECPAC11, PO-020 (Mar 1–3, 2011) American University of Sharjah, Sharjah, United Arab Emirates. [6] Kareem Yusuf, Ahmad Aqel, Zeid A. Al-Othman, Ahmed-Yacine Badjah-Hadj-Ahmed, Abdulrahman A. Alwarthan, Stearyl methacrylate monolithic capillary column preparation, characterization and qualitative analysis of drugs, The 1st United Arab Emirates conference on pure and applied chemistry, ECPAC11, PO-199 (Mar 1–3, 2011) American University of Sharjah, Sharjah, United Arab Emirates. [5] Ahmad Aqel, Preparation and characterization of capillary hexyl methacrylate monolithic column and application in rapid determination of caffeine in food samples, King Saud University 2nd students scientific symposium (Dec 15–16, 2010) King Saud University, Riyadh, Saudi Arabia.


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[4] Zeid A. Al-Othman, Hadeel A. Al Abdelmoneim, Ahmad Aqel, Ahmed-Yacine Badjah-Hadj-Ahmed, Abdulrahman Alwarthan, Alkyl polymethacrylate monolithic columns for capillary liquid chromatography, The 34th international symposium on capillary chromatography (ISCC) and 7th GCxGC symposium, PO-F-08 (May 30 – Jun 4, 2010) Research Institute for Chromatography, Riva Del Garda, Italy. [3] Ahmed-Yacine Badjah-Hadj-Ahmed, Zeid A. Al-Othman, Ahmad Aqel, Metaab Al-Badrani, Abdulrahman A. Alwarthan, Rapid analysis and determination of caffeine in some food samples using capillary hexyl methacrylate monolithic column, The 34th international symposium on capillary chromatography (ISCC) and 7th GCxGC symposium, PO-F-07 (May 30 – Jun 4, 2010) Research Institute for Chromatography, Riva Del Garda, Italy. [2] Ahmad Aqel, Development and application of nanoscale chromatographic techniques, King Saud University students research conference, KSUSRC (Dec 9–10, 2009) King Saud University, Riyadh, Saudi Arabia. [1] Ahmad A. Insisi, Amjad H. El-Sheikh, Jamal A. Sweileh, Solid phase extraction of pesticides from water samples using oxidized carbon nanotubes, The 8th Jordanian chemical conference, JCC, PO-05 (Apr 21, 2008) Petra University, Amman, Jordan.

VI. Reviewing Articles & Grants …

[19] Journal: Microchemical Journal. Manuscript ID: MICROC-D-21-00120. Manuscript title: Eco-friendly chiral HPLC method for determination of alfuzosin enantiomers and solifenacin in their newly pharmaceutical combination: Method optimization via central composite design. Publisher: Elsevier. Date: 31 Jan 2021. [18] Journal: LWT - Food Science and Technology. Manuscript ID: LWT-D-20-07286. Manuscript title: Simultaneous determination of N-methyl carbamates residues in pork tissues based on ultrasound assisted QuEChERS-dSPE extraction followed by reversed phase LC-FLD analysis. Publisher: Elsevier. Date: 10 Jan 2021. [17] Journal: Talanta. Manuscript ID: TAL-D-20-04055. Manuscript title: Amphipathic carbon quantum dots-functionalized silica stationary phase for reversed phase/hydrophilic interaction chromatography. Publisher: Elsevier. Date: 17 Nov 2020. [16] Journal: Journal of Micromechanics and Microengineering. Manuscript ID: JMM-105129. Manuscript title: A microcolumn coated with polydimethylsiloxane functionalized by graphene oxide quantum dots for the gas chromatographic


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separation of characteristic markers of advanced fibrosis. Publisher: IOPscience. Date: 14 Nov 2020. [15] Journal: Talanta. Manuscript ID: TAL-D-20-03644. Manuscript title: Multi-templates surface molecularly imprinted polymer for simultaneously and rapid separation of sulfonamides and quinolones in water: effect of carbon-carbon double bond. Publisher: Elsevier. Date: 13 Oct 2020. [14] Journal: Talanta. Manuscript ID: TAL-D-20-02800. Manuscript title: Facile synthesis of tubular magnetic fluorinated covalent organic frameworks for efficient enrichment of ultratrace polybrominated diphenyl ethers from environmental samples. Publisher: Elsevier. Date: 19 Aug 2020. [13] Journal: Talanta. Manuscript ID: TAL-D-20-01328. Manuscript title: Analytical methods for determination of multi-targeted tyrosine kinase inhibitor; Sunitinib: Critical Review. Publisher: Elsevier. Date: 24 Apr 2020. [12] Journal: RSC Advances. Manuscript ID: RA-ART-10-2019-008717R1. Manuscript title: Core-shell particles and monolithic columns; tools for simultaneous LC analysis of avanafil, sildenafil, apomorphine, trazodone, yohimbine, tramadol and dapoxetine in pharmaceutical dosage forms, counterfeit products and human plasma. Publisher: Royal Society of Chemistry. Date: 15 Dec 2019. [11] Journal: RSC Advances. Manuscript ID: RA-ART-10-2019-008717. Manuscript title: Core-shell particles and monolithic columns; tools for simultaneous LC analysis of avanafil, sildenafil, apomorphine, trazodone, yohimbine, tramadol and dapoxetine in pharmaceutical dosage forms, counterfeit products and human plasma. Publisher: Royal Society of Chemistry. Date: 02 Dec 2019. [10] Journal: Analytical Letters. Manuscript ID: LANL-2019-0907. Manuscript title: Development of HS-PTV-GC/MS method to analyse volatile components in tea infusions and discriminate different types of tea with the aid of chemometrics. Publisher: Taylor & Francis. Date: 30 Oct 2019. [9] Journal: Analytical and Bioanalytical Chemistry. Manuscript ID: ABC-01480-2019. Manuscript title: Porous silica monolithic polymers for micromachined gas chromatography columns: A featured phase for fast and efficient separations of light compounds mixtures. Publisher: Springer. Date: 23 Aug 2019. [8] Journal: Analytical and Bioanalytical Chemistry. Manuscript ID: ABC-01022-2019. Manuscript title: Fast screening and quantitative mass spectral imaging of thin-layer chromatography plates with flowing atmospheric-pressure afterglow high-resolution mass spectrometry. Publisher: Springer. Date: 10 Jun 2019.


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[7] Journal: Journal of Saudi Chemical Society. Manuscript ID: JSCS-D-18-00713R1. Manuscript title: Determination of chlorinated hydrocarbons in milk samples using sol-gel based polymer coated silica sorbent for stir-bar supported micro-solid-phase extraction coupled with gas chromatography mass-spectrometry. Publisher: Elsevier. Date: 29 Nov 2018. [6] Journal: Journal of Saudi Chemical Society. Manuscript ID: JSCS-D-18-00713. Manuscript title: Determination of chlorinated hydrocarbons in milk samples using sol-gel based polymer coated silica sorbent for stir-bar supported micro-solid-phase extraction coupled with gas chromatography mass-spectrometry. Publisher: Elsevier. Date: 12 Oct 2018. [5] Journal: Food Chemistry. Manuscript ID: FOODCHEM-D-18-01919R3. Manuscript title: Mass spectrometry-based metabolomics and chemometric analysis of Pu-erh teas of various origins. Publisher: Elsevier. Date: 09 Jun 2018. [4] Journal: Food Chemistry. Manuscript ID: FOODCHEM-D-18-01919. Manuscript title: Analysis of Pu-erh teas using high resolution mass spectrometry-based metabolomics. Publisher: Elsevier. Date: 22 May 2018. [3] Journal: Analytical Methods. Manuscript ID: AY-ART-03-2018-000474. Manuscript title: Supercritical CO2 extraction for the determination of tetrachloroethylene residues in dry-cleaned apparel. Publisher: Royal Society of Chemistry. Date: 21 Mar 2018. [2] Journal: Analytical Methods. Manuscript ID: AY-ART-11-2017-002632. Manuscript title: Supercritical CO2 extraction for the determination of tetrachloroethylene residues in dry-cleaned apparels. Publisher: Royal Society of Chemistry. Date: 13 Jan 2018. [1] Research proposal applied for the Ministry of Higher Education, Shaqra University, Saudi Arabia Kingdom. Project title: Environmental studies: studying the effect of chemical fertilizers on groundwater in the Sajir area - Saudi Arabia. Date: 07 Jan 2017.

VII. Online Lectures …

Main research interests [14] https://www.youtube.com/watch?v=RjzV31T-d74 High performance liquid chromatography: fundamentals & applications [13] https://www.youtube.com/watch?v=vjGIAS0hPa0&t=31s [12] https://www.youtube.com/watch?v=f4eizS2Nrhk&t=126s [11] https://www.youtube.com/watch?v=lCVPk6s6jpI [10] https://www.youtube.com/watch?v=ZETDxmZSAsw&t=24s [9] https://www.youtube.com/watch?v=xjPVqCR1MZQ [8] https://www.youtube.com/watch?v=wR4dEehrjyE


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[7] https://www.youtube.com/watch?v=5YFJt42CXes&t=89s Gas chromatography: fundamentals & applications [6] https://www.youtube.com/watch?v=-QKYloVw0l0 [5] https://www.youtube.com/watch?v=gxSIhnQvq1g [4] https://www.youtube.com/watch?v=RRj2UNaOEIA [3] https://www.youtube.com/watch?v=dq6j9_pLblY An introduction to chromatographic separations [2] https://www.youtube.com/watch?v=8hNzrmBConc [1] https://www.youtube.com/watch?v=iSx5Ji5mku8

VIII. Submitted Manuscripts …

[6] Ahmad Aqel, Mohammad Khan, Ibrahim Alsohaimi, Ameen Alsubhi, Ahmed Alammari, Monitoring of probable carcinogen bisphenol A in polyethylene terephthalate and glass bottled drinking water using improved solid-phase extraction and UHPLC-MS. [5] Soad Alzahrani, Ahmad Aqel, Zeid A. ALOthman, Fast and sensitive determination of BTX and PAHs in water samples by nano-liquid chromatography using benzyl polymethacrylate monolithic column. [4] Ahmad Aqel, Asma’a Al-Rifai, Zeid A. ALOthman, Determination of scopolin and scopoletin in alcoholic extract of Convolvulus pilosellifolius using HPLC. [3] Asma’a Al-Rifai, Ahmad Aqel, Phytochemical screening, total phenol and flavonoids contents of different extracts from some Convolvulaceae plants. [2] Eman Al-Damegh, Ahmad Aqel, Zeid A. ALOthman, Chemically modified silica gel with aminohydrazinopyrazole for preconcentration and determination of Cu(II), Cd(II) and Hg(II). [1] Ahmad Aqel, Eman Al-Damegh, Zeid A. ALOthman, Functionalization of silica gel with aminoazole derivatives for determination of copper and cadmium by flame atomic absorption spectrometry.

REFERENCES & CONTACT PERSONS

• Prof. Ahmed-Yacine Badjah-Hadj-Ahmed (King Saud University) E-mail: [email protected], [email protected]

• Prof. Abdulrahman A. Alwarthan (King Saud University) E-mail: [email protected]

• Prof. Amjad H. El-Sheikh (Hashemite University)

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of 26 A. AQEL

E-mail: [email protected]

• Prof. Zeid A. ALOthman (King Saud University) E-mail: [email protected]

• Prof. Ismail I. Fasfous (Hashemite University) E-mail: [email protected]



Ahmad Aqel Abdelfattah IFSEISI - KSU

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