2003 European Winter Conferenceon Plasma Spectrochemistry

1 2 - 17 January 2003Garmisch-Partenkirchen

Programme

and

Abstracts of the Scientific Contributions

TIB/UB Hannover 89126 153 507

ISBN 3-936028-06-0

Monday, 13 January 2003

Opening ceremony and opening lecture Festsaal Werdenfels

08.30-09.30 Opening by the conference chairman and welcome by the Lord Major ofGarmisch-PartenkirchenEuropean Award for Plasma Spectrochemistry:Laudatio by F. Adams, University of AntwerpPresentation of the award to D. Guenther by the chairman of the jury,K.G. Heumann, and the representative of Agilent Technologies, D. PotterAward lecture by D. Guenther, ETH Zurich:Laser ablation ICP-MS: a mature and exciting analytical tool 45

09.30-10.15 Atmospheric ultra trace substances: influence on environment and climateArnold. F.. Heidelberg/D

46

10.15-10.45 Coffee Break

ICP-MS and ICP-AES: Instrumentation and fundamentals

Chair: Hieftje, G.M., Bloomington/USA

Festsaal Werdenfels

10.45-11.15 New directions for ICP-MS 47IL 01 Houk. R.S., Ames/USA, Aeschliman, D. B. Ames/USA, Baldwin, D.,

Ames /USA, Bajic, S., Ames/USA

11.15-11.45 ICP-AES: do we need further instrument development or more efficient 48IL 02 data processing?

Mermet. J.M.. Villeurbanne/F

11.45-12.05 Determining the most appropriate mass bias correction expression for an 49O 01 ICP-MS system

Sharp. B. L.. Loughborouqh/GB. Ingle, C. P., Loughborough/GB,Horstwood, M. S. A., Nottingham/GB and Parrish, R. R., Nottingham/GB

12.05-12.25 Figures of Merit for a New Focal Plane Camera Fitted to an Inductively 50O 02 Coupled Plasma Mattauch-Herzog Geometry Mass Spectrograph

Barnes. IV. J.H.. Bloominaton. IN/USA, Schilling, G.D., Bloomington,IN/USA, Sperline, R.P., Tucson, AZ/USA, Young, E.T., Tucson, AZ/USA,Denton, M.B., Tucson, AZ/USA, Barinaga, C.J., Richland, WA/USA,Koppenaal, D.W., Richland, WA/USA, Hieftje, G.M., Bloomington, IN/USA

12.25-14.00 Lunch

Sample introduction and preparation

Chain Barnes, R.M., Hadley/USA

Festsaal Werdenfels

14.00-14.30 Recent Developments in On-line Sample Introduction for ICP-Sectrometry 51IL04 Barndt. H.. Dortmund/D. Jacob, P., Dortmund/D, Razilov, I., Dortmund/D,

Schaldach, G., Dortmund/D

14.30-14.50 Determination of Platinum Group Metals in Clinical and Environmental 52O 51 Samples by Flow Injection combined with ICP-TOF-MS detection

Benkhedda. K.. Beloium/B. Goenaga, H, Antwerp/B, Dimitrova, B,Sofia/BG,Ivanova, E, Sofia/BG, Adams, F, Antwerp/B

14.50-15.10 The use of slurry nebulization with inductively coupled plasma 53O 03 spectroscopy

McCrindle. R.I.. Pretoria/ZA. Botha, B.M., Pretoria/ZA, Marjanovic, L.,Pretoria/ZA Schwarzer S., Pretoria/ZA

15.10-15.30 Influence of Digestion Procedures on the Determination of Selected Trace 54O 04 Elements in Peat and Plant Materials by USN-ICP-MS

Krachler. M.. Heidelberq/D. Emons, H., Juelich/D, Shotyk, W.,Heidelberg/D

15.30-15.50 An Iminodiacetate based sample pretreatment system for the determination 55O 05 of trace elements in marine samples by ICP-MS

Casev. N.. Slioo/IRL. McGowan T., Sligo/IRL

15.50-16.20 Coffee Break

Collision and reaction cells

Chair: Becker, J.S., Jiilich/D

Festsaal Werdenfels

16.20-16.50 Collision and Reaction Cell Dynamics in Multipole Cells for ICP-MS 56IL 05 Tanner. S. P.. Concord. Ontario/CDN. Baranov, V.I., Concord,

Ontario/CDN Bandura, D.R., Concord, Ontario/CDN

16.50-17.20 Collision-Induced Dissociation Reactions of Glow-Discharge-Generated 57IL 06 Polyatomic Ions in Quadrupole Ion Trap Mass Spectrometry

Duckworth. D.C.. Oak Ridge/USA. Jackson, G.P., Oak Ridge/USA,Goeringer, D.E., Oak Ridge/USA

17.20-17.40 Method Development for Ion-Molecule Reactions in Inductively Coupled 58O 06 Plasma Mass Spectrometry

Hattendorf. B.. Zurich/CH. Gunther, D., Zurich/CH

17.40-18.00 A Study of Gases and their Properties in an ICP Mass Spectrometer with 59O 07 Reaction Cell

Thomsen, M.. Seer Green/GB. Green D., Seer Green/GB

18.00-20.00 Poster session and exhibition(including wine presented by the poster authors and exhibitors and Brezeinfrom the conference organizers)

Tuesday, 14 January 2003

Elemental speciation

Chair: Lobinski, R., Pau/FFestsaal Werdenfels

08.30-09.00 New developments in elemental speciation studies 60IL 07 Caruso. J. A.. Cincinnati/USA. Meija, J., Cincinnati/USA, Montes Bayon,

M., Cincinnati/USA, Vonderheide, A., Cincinnati/USA, Wrobel, K.,Cincinnati/USA, Wrobel, K., Cincinnati/USA, Kannamkumarath, S.,Cincinnati/USA

09.00-09.30 High Resolution and Multicollector Sector Field ICP-MS for Speciation 61IL 08 Studies

Evans. E. H.. Plvmouth/GB. Clough, R., Plymouth/GB, Cartwright, A.,Plymouth/GB, Belt, S., Plymouth/GB, Fairman, B., Teddington/GB, Wolff,J.-C, Stevenage/GB

09.30-09.50 Determination of labile/free aluminium and other trace metals in fresh water 62O 08 using different fractionation procedures

Lund. W..Oslo/N

09.50-10.10 Application of LC-ICP-SFMS to cisplatin speciation in the aquatic 63O 09 environment

Hann. S.. Vienna/A. Kollensperger, G., Vienna/A, Stingeder, G., Vienna/A,Fuerhacker, M., Vienna/A, Mader, R.M., Vienna/A, Buchberger, W., Linz/A

10.10-10.30 Speciation of Arsenic, Mercury and Tin in Mussels from Sardinia Island 64O 10 (Italy) and the Limits of Speciation as Routine Analytical Tool

Fodor, Peter. Budapest/H. Bodo, E.T., Budapest/H, Soros, Cs., Budapest/H,Ipolyi, I., Budapest/H, Sposato, S., Rome/I, Di Rosa, F., Rome/I,Massanisso, P., Rome/I, Morabito, R., Rome/I

10.30-11.00 Coffee Break

Chair: Adams, F., Antwerp/B

11.00-11.30 From sheep to earthworms: limitations of ICP-MS for arsenic speciation 65IL 09 analysis in environmental studies

Feldmann, J., Old Aberdeen/GB. Raab, A.,Old Aberdeen/UK Meharg, A.,Old Aberdeen/UK

11.30-11.50 High resolution separation of 17 arsenic species in food by IC-ICP-MS - 66O 11 results and benefits

Kohlmever, U.. Geesthacht/D. Kuballa, J., Geesthacht / D, Jantzen E.,Geesthacht / D

11.50-12.10 The use of HPLC-ICP-MS and HPLC-electrospray-MS to characterise Se 67O 12 and As species in environmental samples

Ebdon. L.C.. Plvmouth/GB. Fitzpatrick, S., Plymouth/GB, Foulkes, M.,Plymouth/GB

12.10-12.30 Determination of inorganic selenium species in rain and sea waters by ion 68O 13 chromatography-hydride generation-inductively-coupled plasma-dynamic

reaction cell-mass spectrometry (IC-HG-ICP-DRC-MS)Wallschlaqer. P.. Peterborough/CDN. London, J., Seattle/USA

10 11

12.30-14.00 Lunch

14.00-15.30 Poster session (odd numbers), exhibition and coffee

Chair: Ebdon, U, Plymouth/UK

15.30-16.00 Multidimensional analytical approaches for elemental speciation in life 69IL 10 sciences

Szpunar. J.. Pau/F. Ruiz Encinar, J., Pau/F

16.00-16.30 Speciation of metalloproteins using hyphenated techniques 70JL 11 Pranae. A.. Geesthacht/D

16.30-16.50 Characterization of metal complexes with metailothioneins in the Cyprinus 71O 14 carpio tissue by reversed-phase HPLC with ICP-time-of-flight-mass

spectrometry and electrospray (ES)-mass spectrometryGoenaoa Infante. H., Antwerp/B. Van Campenhout, K., Antwerp/B,Cuyckens, F., Antwerp/B, Claeys M., Antwerp/B, Blust R., Antwerp/B,Adams F. C, Antwerp/B

16.50-17.10 Induced Biomolecules in the Phytoremediation of Toxic Elements (Se, Cd, 72O 15 As and Ag) by Mass Spectrometric Techniques (ICP-MS/ES-MS).

Montes-Bavon. M.. Oviedo/E. Meija, J., Cincinnati/USA, Caruso, J.A.,Cincinnati/USA, Sanz-Medel, A., Oviedo/E

17.10-17.30 Characterization of Manganese species in human milk 73O 16 Michalke. B.. Neuherberg/D

17.30-17.50 Speciation analysis of nickel in the latex of a hyperaccumulating tree 74O 17 Sebertia acuminata by HPLC with ICP MS and electrospray MS/MS

detectionSchaumloffel. P.. Pau/F, Ouerdane, L, Pau/F, Lobinski, R., Pau/F

19.00-19.15 Enhanced Elemental and Isotopic Analysis Capabilities Using ICP-TOFMS 79V 05 Lehmkamper. H.. Monchenqladbach/D

19.15-19.30 Status and Outlook and of High Resolution Sector Field ICP-MS 80V 06 Hamester. M.. Bremen/P. Rottmann, L, Bremen/P, Schwieters, H.,

Bremen/D

19.30-19.45 Latest Pevelopments in NP-YAG and Excimer Laser Ablation Systems for 81V 07 ICP-MS and ICP-OES

Neufeld. L. M.. Fremont/CPN. Mao, X., Berkeley/CPN, Mao, S.,Berkely/CPN, Russo, R. E., Berkely/CDN

EVISA Information and Short Course Olympiasaal

18.00-18.10 Out of the Research Laboratories into the REAL WORLP of IndustrialApplications - The Next Step for Establishing Speciation Analysis inEurope: The European Virtual Institute for Speciation Analysis (EVISA)Sperling. M.. Sipplingen/P. Buscher, W. Munster/D, Ponard, O. F. X.,Pau/F

18.10-20.00 Short course on Biological Speciation(organized by J. Caruso)

82

Meetings

20.00 Young Scientists' Evening

Gasthaus Braustuberl

Vendors Workshop

Chair: Brenner, I.B., Jerusalem/IL

Festsaal Werdenfels

18.00-18.15 Introduction. Setting the Scene - Challenges for Plasma Based 75V 01 Instrumentation

Brenner. I.B.. Jerusalem/IL

18.15-18.30 Pevelopment of the innovative new high sensitivity 90 degree reflecting ion 76V 02 optics Varian ICP-MS

Elliott. S.. Mulorave/AUS. Anderson, S.E., Mulgrave/AUS Kalinitchenko, I.,Mulgrave/AUS

18.30-18.45 New Developments in Collision and Reaction Cell ICP-MS for Multi- 77V 03 Element Analysis in Unknown Samples and for Coupled Chromatography

ICP-MSTve, C. Sinoapore/SGP. McCurdy, E, Manchester/GB, Woods, G,Manchester/GB, Potter, D, Manchester/GB

18.45-19.00 Multi-elemental Analysis of Samples by DRC-ICP-MS - Can it be done with 78V 04 one gas?

Wolf. R. E.. Shelton/USA. Neubauer, K. R., Shelton/USA

20.00 User Meeting of CETAC Technologies

12 13

Wednesday, 15 January 2003

New instrumentation and alternative plasma sources

Chair: Houk, R.S., Ames/USA

Festsaal Werdenfels

08.30-09.00 New Combinations, Configurations, and Capabilities in Plasma-Source 83IL 12 Mass Spectrometry

Hieftie. G.M.. Bloominqton/USA, Barinaga, C.J., Richland/USA, Barnes,J.H, IV, Bloomington/USA, Penton, MB., Tucson/USA, Koppenaal, P.W.,Richland/USA, McClenathan, P.M., Bloomington/USA, Ray, S.J.,Bloomington/USA, Rosen, A.L., Bloomington/USA, Schilling, G.D.,Bloomington/USA, Sperline, R., Tucson/USA, Wetzel, W.C.,Bloomington/USA

09.00-09.20 A miniaturized plasma as a detector for gas chromatography 84O 18 Franzke. J.. Portmund/P, Kunze.K., Dortmund/P, Miclea, M., Portmund/P,

Niemax, K., Portmund/P

09.20-09.40 Characterisation of a microchip-size radio frequency plasma in optical 85O 19 emission spectrometry

Siemens. V.. Esproo/FIN

09.40-10.00 A capacitively coupled microplasma on a fused silica capillary 86O 20 Hauser. P. C. Basel/CH. Guchardi, R., Basel/CH

10.00-10.20 A new low flow ICP torch 87O 21 Klostermeier. A.. Muenster/P, Buscher.W., Muenster/D

10.20-10.40 New ICP-MS system 880 22 Kalinitchenko. I.. Mularave/AUS

10.40-11.10 Coffee Break

Applications by ICP spectrometry

Chair: Mermet, J.M., Villeurbanne/F

Festsaal Werdenfels

11.10-11.40 Selenium determination and lead isotopic measurements by ICP ion trap 89IL 13 mass spectrometry

Furuta. N.. Tokvo/J

11.40-12.00 ICP-OES On-Line Continuous Emission Monitoring for the Control of 90O 23 Industrial Thermal Processes: Interface Design and Choice of Operating

ConditionsTrassv. C. Saint Martin d'Heres/F, Alemany, C, St-Martin d'Heres/F,Ardelt, P., Kleve/D, Falk, H., Kleve/P, Hassaine, S., Villeurbanne/F

12.00-12.20 Analysis of alternative fuels by argon-oxygen mixed-gas inductively 91O 24 coupled plasma optical emission spectrometry

Ardelt. P.. Kleve/D. Heitland, P., Kleve/P, Visser, H., Kleve/D, Vogt, T.,Kleve/P

12.20-12.40 Petermination of Trace Elements in Difficult Matrices by Inductively 92O 25 Coupled Plasma - Dynamic Reaction Cell - Mass Spectrometry

Gurleviik. H.. Seattle/USA. Scanlan, K. Seattle/USA

12.40-14.00 Lunch

14.00-15.30 Poster session (even numbers), exhibition and coffee

Chair: Broekaert, J.A.C., Hamburg/D

15.30-16.00 Field-Flow Fractionation and Inductively Coupled Plasma Mass 93IL 14 Spectrometry

Barnes, R.. Amherst/USA. Siripinyanond, A., Amherst/USA, Danku, J.,Amherst/USA, Amarasiriwardena, P., Amherst/USA

16.00-16.20 Determination of trace levels of arsenic in small volumes of mouse blood 94O 26 using ICPMS - a comparison between Hydride generation, High resolution

and octapole reaction cell ICPMS.Sturup. S.. Hanover/USA

16.20-16.40 Platinum group elements determination in environmental matrices by ICP- 95O 27 SFMS with a low-flow micronebulization/desolvation system

Barbante, C. Venice/I. Varga, A., Venice/I, Cozzi, G., Venice/I.Turetta, C,Venice/I, Cescon, P., Venice/I

16.40-17.00 A simple procedure for the determination of platinum group elements and 96O 28 rhenium (Ru, Rh, Pd, Re, Ir and Pt) with an inexpensive LC-ICP-MS

coupling in geological and environmental reference materialsMeisel. T.. Leoben/A. Fellner N., Leoben/A

17.00-17.20 Heavy Metals in Arctic Snow -Distribution between particulate and soluble 97O29 phase-

Kriews. M., Bremerhaven/D, Stolting I, Bremerhaven, P

17.20-17.40 Compound Independent Calibration of Pesticides and Herbicides by GC- 98O 30 ICP-MS

Wilbur. S.M.. Bellevue/USA. Cummings, R., Manchester/USA

17.40-18.00 Clinical sample analysis using ICP-MS. 99O 31 Nelms. S. M.. Winsford/GB. Spence, B., Winsford/UK, Nash, M.,

Winsford/UK

Meetings

18.30 User Meetings

14 15

Thursday, 16 January 2003

Isotopes used for elemental speciation and other applications

Chair: Vanhaecke, F., Gent/B

Festsaal Werdenfels

08.30-0900 Application of multiple-spiking mode in IPMS for elemental speciation 100IL 15 Garcia Alonso. J. lonacio. Oviedo/E. Rodriguez Gonzalez, P., Oviedo/E,

Ruiz Encinar, J. Oviedo/E Sanz-Medel, A. Oviedo/E

09.00-09.30 Potentials and limits of speciated isotopic approaches in environmental 101IL 16 research

Ponard. O.F.X.. Pau/F

09.30-09.50 Speciation of selenium in human serum by FPLC-IPA-ORS-ICP-MS 102O 32 Marchante-Gavon. J. M.. Oviedo/E, Sanz-Medel, A., Oviedo/E, Hinojosa

Reyes, L., Oviedo/E, Garcia Alonso, J.I., Oviedo/E

09.50-10.10 Is there fractionation after 34? Isotope fractionation of antimony through 103O 33 biovolatilization

Wehmeier. S.. Aberdeen/GB, Feldmann, J., Aberdeen/GB

10.10-10.30 Investigation on the Mercury Isotope Distribution of Mercury Species 704O 34 (MMHg and Hg2+) in different Fish Tissue Samples

Krupp. E.M.. Pau/F. Pecheyran, C, Pau/F, Donard, O.F.X., Pau/F

10.30-11.00 Coffee Break

Isotope ratio measurements

Chair: Prohaska, T., Vienna/A

Festsaal Werdenfels

11.00-11.30 A new large-geometry high-resolution multiple collector ICP-MS for precise 105IL 17 interference-free isotope ratio measurement

Hallidav. A.N.. Zurich/CH, Freedman, P. A., North Wales/UK, Oberli, F.,Zurich/CH, Baur, S., Zurich/CH, Hollins, S., North Wales/UK, Levasseur,S., Zurich/CH, Leya, I., Zurich/CH, Quitte, G., Zurich/CH, Teutsch, N.,Zurich/CH, Wiechert, U., Zurich/CH, Williams, H., North Wales/UK,Williams, J., North Wales/UK

11.30-12.00 Recent developments and applications of precise isotope ratio 106(L18 measurements

Moens. L.. Ghent/B. Vanhaecke, F., Ghent/B

12.00-12.20 High-precision multi-element isotope dilution by HR-ICP-MS 107O 35 Willbold. M.. Mainz/D, Amini, M., Mainz/D, Jochum, KP., Mainz/D, Stoll, B.,

Mainz/D, Hofmann, AW., Mainz/D

12.20-12.40 Silicon isotope ratio measurements with high resolution, collision cell, multi- 108O 36 collector ICPMS

Goldsmith. S. L.. Manchester/GB, Palacz, Z., Manchester, GB, Meffan-Main, S., Manchester, GB, Turner, P.J.T., Manchester, GB

12.40-14.00 Lunch

Chair: Prohaska, T., Vienna/A

14.00-14.20 Isotope Ratio Measurements of Selected REE by MC-ICP-Ms 109O 37 Platzner. I.T.. Jerusalem/IL. Segal I., Jerusalem/IL, Halicz L, Jerusalem/IL

14.20-14.40 Measurement of Isotopic Ratios on Transient Signals by MC-ICP-MS 110O 38 Gunther-Leopold. I.. Villioen/CH. Wernli, B., Villigen/CH, Kopajtic, Z.,

Villigen/CH

14.40-15.00 Mass discrimination in isotope ratio measurements with DRC-ICP-MS 111O 39 Vanhaecke. F.. Ghent/B. Balcaen, L, Ghent/B, Deconinck, I., Ghent/B,

Moens, L., Ghent/B

15.00-15.30 Coffee Break

New developments in GDMS and GDAES

Chair: Marcus, R.K., Clemson/USAFestsaal Werdenfels

15.30-16.00 New roles for the glow discharge plasma 112IL 19 Harrison. W.W.. Gainesville/USA. Oxley, E.S., Gainesville/USA,

Coon, J.J., Gainesville/USA

16.00-16.30 Modern developments in glow discharge spectrometry and their application 113IL 20 in material science

Hoffmann. V.. Presden/P

16.30-16.50 Modeling of a millisecond pulsed glow discharge: New insights in the 114O 40 afterpeak behavior

Boqaerts. A.. Antwerpen/B. Gijbels, R., Antwerpen/B

16.50-17.10 The Effect of Small Quantities of Hydrogen or Nitrogen on the Spectrum of 115O 41 the Plasma Gas in Glow Pischarge Spectrometry

Steers. E.B.M.. London/GB. Smid, P., Plzen/CZ, Pickering, J.C.,London/GB

17.15-19.30 Poster session and exhibition

Vendors Workshop

Chair: Brenner, I.B., Jerusalem/ILFestsaal Werdenfels

17.15-17.30 Pifferent solid sampling techniques in combination with Spectros Ciros 116V 08 CCP ICP-OES

Voot. T.. Kleve/P. Ardelt, P., Kleve/P, Heitland, P., Kleve/P, Visser, H.,Kleve/P

17.30-17.45 Designing an Echelle Optical System for an Inductively Coupled Plasma 117V 09 Emission Spectrometer (ICP-OES) to Improve the Qulaity of Results

Sotera. John J., Hudson/USA. Pfeil, D. L, Hudson/USA, Brown, P.,Hudson/USA

16 17

17.45-18.00 New ICP-AES developments and applications in Jobin Yvon 118V 10 Tyler, G.. Lonoiumeau/F. Cosnier, A., Longjumeau/F, Le Corre, N.,

Longjumeau/F, Velasquez, S., Longjumeau/F, Nehm, R., Grasbrunn/D

18.00-18.15 Improvement of UV On/Off Ratios of a Gated ICCD by Simultaneously 119V11 Gating the MCP

Hamilton. S.. Belfast/IRL. Conroy, E., Belfast/IRL

18.15-18.30 Nebulization of ICP Samples at Low Uptakes 1P0V12 Eastgate, A.. Vevev/CH

18.30-18.45 Performance criteria in wet chemical sample preparation 121V 13 Lafer. M., Graz/A, Kettisch, P., Graz/A, Kainrath, P., Ueberlingen/D

18.45-19.00 Enviro-PT Performance Evaluation Program - Nuts and Bolts 122V 14 Kocherlakota, N., Metuchen/USA. Obenauf, R., Metuchen/USA

19.00-19.10 Variable Cleanroom Units to Be Applied to Procedures of Analytical 123V15 Chemistry

Ohls, K.. Erdinq/P. Rickert, F., Erding/P

19.10-19.20 History of ICP-MS and ICP-OES Spectrometer Glove-Box-Adaptions as 124V16 Turn-Key-Projects

Wiesmann. H.. Meinhard/P

Friday, 17 January 2003

Applications by GDMS and GDAES

ghair: Jakubowski, N., Dortmund/D

Festsaal Werdenfels

08.30-09.00 New developments for the exploitation of GPMS in nuclear and 125IL 21 environmental samples

Betti. M.. Karlsruhe/P

09.00-09.20 Application of Radio Frequency Glow Discharge Optical Emission 126O 42 Spectroscopy (rf-GD-OES) for Monitoring of Trace Elements On and In

Silicon WafersMarcus. R. K.. Clemson/USA. Luesaiwong, W, Clemson/USA

09.20-09.40 Radio-Frequency Glow Pischarge Emission Source Boosted by Bias- 127O 43 Current Introduction and Its Application to Petermination of Minor Elements

in SteelWaqatsuma. K.. Sendai/J

09.40-10.00 Pepth Profiling of Organic Coatings with GD-OES Investigation of line 128O 44 interference corrections

Benotson, A., Stockholm/S

10.00-10.20 Depth profiling of lithium and boron isotopes by GDMS and SIMS 1290 45 Aldave de Las Heras. L.. Karlsruhe/P. Toscano, E. H., Karlsruhe/P, Betti,

M., Karlsruhe/P

10.20-10.50 Coffee Break

LA-ICP-MS: Instrumentation and fundamentals

Chair: Giinther, D., Zurich/CH

Festsaal Werdenfels

10.50-11.20 So how accurate is laser ablation ICP-MS? New solutions for spectral 130IL 23 interferences with collision and reaction cells

Mason. P.R.D.. Utrecht/NL

11.20-11.40 Femtosecond Laser Ablation ' 131O 52 Heroenroder. R.. Portmund/D. Niemax, K., Portmund/D, Margetic, V.,

Dortmund/D

11.40-12.00 Wavelength, particles, and ICP: A comparison of effects influencing 132O 46 elemental fractionation in Laser Ablation.

Guillonq. M.. Zurich/CH. Horn, I., Zurich/CH, Kuhn, H.-R., Zurich/CH,Gunther, D., Zurich/CH

12.00-12.20 New developments in laser ICP-MS with 157 nm excimer laser 133O 47 Telouk. P.. Lvon/F. Rose-Koga, E.F., Lyon/F, Albarede, F., Lyon/F

12.20-14.00 Lunch

18 19

Applications by LA-ICP-MS

Chair: Gunther, D., Zurich/CH

Festsaal Werdenfels

14.00-14.30 High resolution depth and surface compositional profiling using laser 134IL 24 ablation ICPMS

Eaoins. S.M.. Canberra/AUS. McCulloch, MX, Canberra/AUS Shelley,J.M.G., Canberra/AUS

14.30-14.50 Determination of REE in geological samples by ICP-TOFMS -A 135O 48 comparison between Laser Ablation with RVAC and Ultrasonic

NebulizationEmteboro. H., Tres Cantos, Madrid/E, Castillo Carrion, M., Madrid/E,Reyes Andres, J., Madrid/E, Martin Rubi, J. A., Madrid/E

14.50-15.10 Measurement of Isotope ratios with Laser Ablation 136O 49 ICP-OTOF-MS.

Kozlov. B.. Melbourne/AUS. Saint, A., Melbourne/AUS

15.10-15.30 Application of the Isotope Dilution Technique to the Analysis of Powdered 137O 50 Samples by Laser Ablation ICP-MS

Tibi. M.. Mainz/P. Heumann. K. G., Mainz/P

Closing session Festsaal Werdenfels

15.30-16.00 Presentation of poster awardsAnnouncement of next Winter Conference on Plasma Spectrochemistry

16.00-16.15 Closing remarksAnnouncement of 2004 and 2005 Winter Conferences on PlasmaSpectrochemistry

List of Posters

Plasma sources for atomic and mass spectrometry Konzertsaal Richard Strauss

P-PI-001 Thermodynamical simulation of the thermochemical processes for ICP-AES 138and ICP-MSPupyshev. A. A., Ekaterinburg/RUS

P-PI-002 Investigation of non-spectroscopic interference and internal standardization 139method in axially and radially viewed inductively coupled plasma opticalemission spectrometry using cross-flow and ultrasonic nebulizersSun. Y.C.. Hsinchu/T. Wu, S.H., Hsinchu/RC, Lee,C.C.,Hsinchu/RC

P-PI-003 The effects of matrix induced mass bias effects for high accuracy elemental 140analysis by Isotope dilution ICP-MSEvans. P.J., London/GB. Hearn, R., London/GB, Fairman, B., London/GBCatterick, T., London/ GB

P-PI-004 Gas-Phase Ion Chemistry of Uranium Species upon ICP Conditions 141Vais. V.. Ottawa/CPN. Cornett, J., Ottawa/CPN, Li, C , Ottawa/CPN

P-PI-005 Intellectual Analytical Machines 142Prudnikov. E.P., St. Petersburg/RUS. Prudnikov, E. E., St. Petersburg/RUS

P-PI-006 Universal Theory for Analytical Sciences 143Prudnikov. E. P., St. Petersburg/RUS. Prudnikov, E.E., St. Petersburg/RUS

P-PI-007 Theoretical Study of Cool Plasma in ICP-MS 144Prudnikov. E.P.. St. Petersburg/RUS. Prudnikov, E.E., St. Petersburg/RUS,McLeod C.W., Sheffield/GB

P-PI-008 Thermodynamic simulation of applicability of negative ions in ICP-MS 145Pupyshev. A. A., Ekaterinburg/RUS. Surikov, V.T., Ekaterinburg/RUS

P-PI-009 Analysis of the superconductor materials using the microwave plasma 146optical emission spectrometerKoutchoumov, V.A., Moscow/RUS

P-PI-010 Low pressure ICP as excitation source for optical emission spectrometry 747when aqueous samples analyzing t

Kartasheva. M.A., St Petersburq/RUS. Gerasimov, G. N., St.Petersburg/RUS, Golubev, E. M., St. Petersburg/RUS, Kononova, O. N, St.Petersburg/RUS, Maleshin, M. N., St. Petersburg/RUS

P-PI-011 Short pulsed capillary discharge as excitation and ion source for spectral 148analysis.Golubev. E. M.. St. Petersburo/RUS. Kartasheva, M. A., St.Petersburg/RUS, Levina, O. V., St. Petersburg/RUS

P-PI-012 New Developments in the Static High Sensitivity ICP (SHIP) 149Evers. S.. Muenster/P. Buscher, W., Muenster/P, Berndt, H., Portmund/P

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P-PI-013 Micro-structured electrode arrays: An alternative plasma source for 150generating uniform glow discharges over a wide pressure range up toatmospheric pressureBaars-Hibbe. L.. Braunschweiq/D. Schrader C, Braunschweig / D, Sichler,P., Braunhschweig / D, Gericke, K.-H., Braunschweig / P, Biittgenbach, S.,Braunschweig/ P, Penache, M. C, Frankfurt/ D, Schmidt-Bocking, H.,Frankfurt / D

P-PI-014 Mercury capillary plasma sources for Hg atomic analyzer 757Revalde. G.. Rioa/LV. Skudra, J., Riga/LV, Skudra, A., Riga/LV,Sholupov,A., St. Petersburg/RUS

P-PI-015 Development of a VUV-LIPS system 152Radivoievic. I.. Munchen/P. Panne, U., Munchen/P, Haisch, C,Munchen/D, Niessner, R., Munchen/D, Becker-Ross, H., Berlin/D,Florek, S., Berlin/D

P-PI-016 Characterization of the Liquid Sampling Atmospheric Pressure Glow 753Discharge (LS-APGD) Plasma for Capillary HPLC DetectionMarcus. R. K.. Clemson/USA, Pavis, W.C., Clemson/USA

P-PI-017 Development and scaling of microwave induced plasma sources at 754atmospheric pressureSeelio. M.. Portmund/P. Stonies, R., Dortmund/D , Voges, E., Dortmund/D

Instrumentation (ICP-MS, ICP-AES, MIP-AES etc.) Konzertsaal Richard Strauss

P-ln-001 Robust ICP operating conditions and interfaces reduce Na and Ca induced 755matrix effects - evaluation of a new compact inductively coupled plasma-mass spectrometer for geo-environmental analysisBrenner. I. B.. Jerusalem/IL, Spence, B., Winsford/UK, Sigsworth, P.,Winsford/UK, Walder, A., Winsford/UK

P-ln-002 Tunable diode laser spectroscopy at the 324.75-nm Cu line in a direct 756current plasma jetLaurila. T.. Tampere/FIN, Oikari R., Tampere/FIN, Hernberg R.,Tampere/FIN

P-ln-003 Practical Implementation of a 10 GHz Ion Counting Detector using 757Conventional ElectronicsHunter. K. L. Erminoton/AUS, Sheils, W.L., Ermington/AUS, Stresau,R.W., Ermington/AUS

P-ln-004 Performance Characteristics of a Micro-uptake Glass Concentric Nebulizer 75Sfor Inductively Coupled Plasma SpectrometryFasch. E.. Leoben/A. Unterweger, G., Leoben/A., Wegscheider, W.,Leoben/A

P-ln-005 Going Local: ICP-OES Online Process Monitoring and Control. 159Instrumentation, Calibration Strategies and Selected Applications forLiquids and GasesArdelt. P.. Kleve/D. Falk, H., Kleve/D, Swithenbank, J., Sheffield/UK,Trassy, C, St-Martin d'Heres/F

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Elemental Analysis in Hostile and Extreme Environments by Means of a 760Remote Open-Path Stand-Off Laser Induced Plasma SpectrometerLaserna. J. J., Malaoa/E, Vadillo, J. M, Malaga/E, Garcia-Aguilera, P.,Malaga/E, Palanco, S., Malaga/E, Baena, J. M., Cadiz/E

Lights and shadows in the in-depth characterization of solid samples by 767laser atomization/ionization time-of-flight mass spectrometry (LI-TOFMS)Vadillo. J. M.. Malaqa/E. Garcia, C. C. Malaga/E, Ruiz, J. Malaga/E,Laserna, J. J. Malaga/E

ICP-AES with Flow Sorption Preconcentration for Trace Element Analysis 762of Sea WatersStarshinova. N.. Moscow/RUS. Sedykh, E., Moscow/RUS, Stepanets, O.,Moscow/RUS, Solovjeva, G., Moscow/RUS

Determination of Fe in complex matrices with DRC-ICP-ID-MS. 763Balcaen. L.. Ghent/B. Moens, L, Ghent/B, Vanhaecke, F., Ghent/B

Ion Energy Effects in Hexapole Collision/reaction Cell ICP-MS: Reactivity 764and the Control of Input Ion EnergyDexter. M. A.. Louohborouoh/GB. Sharp, B. L., Loughborough/GB, Reid, H.J., Loughborough/GB

Practical Approach for On-line Analysis of Various Chemicals by Dynamic 765Reaction Cell ICP-MSKishi. Y.. Concord/CDN, Kawabata, K., Concord/CDN, Wiederin, D.,Omaha/USA

Overcoming the problems of interferences in the determination of sulphur 766and phosphorus by ICP-MS with an Octopole Reaction SystemLeonhard. P.. Geesthacht/P. Proefrock, P., Geesthacht/P, Prange, A.,Geesthacht/P

On-line measurement of essential plant nutrients in the root medium using 767ICP-MS with an octopole reaction systemHusted. S.. Copenhaaen/PK. Holm, P.E., Copenhagen/PK, Hansen,H.C.B., Copenhagen/PK, Schjoerring, J.K., Copenhagen/PK

Petermination of Radioisotopes in Environmental Samples by Collision Cell 768ICP-MS with a Pesolvating NebulizerEpov. V. N.. Peterborouoh/CDN. Taylor, V.,'Peterborough/CPN, Lariviere,P., Peterborough/CPN, Evans, R.P., Peterborough/CPN, Comett, R.J.,Ottawa/CPN

Multi-element Analysis of Complex Samples Using Collision/Reaction Cell 769ICP-MS, Without Element-specific Conditions, Cluster Ions or Analyte Loss.Tve, C. Sinqaoore/SGP. McCurdy, E., Manchester/GB., Yamada, N.,Tokyo/J, Woods, G., Manchester/GB.

A Rapid Method for the Analysis of Environmental Samples with a Reaction 7 70Cell InstrumentThomsen. M.. Seer Green/GB

Characterisation of Elbe river colloids with FIFFF and ICP-MS with an 777Octopole Reaction SystemSaal. C . Hamburo/P. Leonhard, P., Geesthacht/P, von der Kammer, F.,Hamburg/P, Prange, A., Geesthacht/P

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P-ln-018 The Use of the Collision Cell ICP-MS for the Determination of Platinum 7 72Group elementsMoldovan. M.. Pau/F. Pecheyran, C, Pau/F, Brenner, I.B., Jerusalem/IL,Donard, O. F. X., Pau/F

P-ln-019 Determination of 129 Iodine by DRC-ICP-MS with Axial Field Technology 7 73Kawabata, K.. Concord/CDN. Takaku, Y., Rokkasho/J, Kishi, Y.,Concord/CDN

P-ln-020 Improvement of selenium speciation in environmental samples by HPLC- 774CCT-ICP-MS. Optimisation of collision cell parameters and applicationsSimon. S.. Pau/F, Aguerre, S., Pau/F, Potin-Gautier, M., Pau/F

P-ln-021 Decoking of a Coked Zeolite Catalyst in a Glow Discharge 775Khan. M. A.. Dhahran/KSA. Al-Jalal, A. A., Dhahran/KSA, Bakhtiari, I. A.,Dhahran/KSA

P-ln-022 Arsenic determination in aqua regia by the method of inductively coupled 776palsma mass spectrometry;possible elimination of spectral intreferenciesChrastnv. V.. Ceske Budeiovice/CZ. Svehla, J., Ceske Budejovice/CZ

P-ln-023 Optimization of Capillary Electrophoresis hyphenated to Inductively 777Coupled Plasma - Sector Field - Mass Spectrometry for the detection of Sand Zn in Aeromonas hydrophila Zn-beta-lactamaseVan Lierde. V.. Ghent/B. Galleni, M., Liege/B, Van Beeumen, J., Ghent/B,Vanhaecke, F., Ghent/B, Moens, L, Ghent/B

P-ln-024 Element Determination in Petroleum Products by High-Resolution ICP-MS 778Prevfus, S., Pau/F, Pecheyran, C, Pau/F, Garraud, H. Pau/F, Magnier, C,Rueil/F, Prinzhofer, A., Rueil/F, Lynch, J., Rueil/F, Donard, O.F.X., Pau/F

P-ln-025 Analysis of semiconductor grade mineral acids by sector-field HR-ICPMS 7 79Wills. J.P.. Bremen/P. Settembre, G., Hopewell Junction/USA

P-ln-026 Application of a high performance ion detection system to the analysis of 780geological samples by HR-ICP-MSRottmann. L.. Bremen/D. Kliigel, A., Bremen/D, Anders, H., Bremen/D

P-ln-027 Using Interference Corrections for the Petermination of REEs in Geological 787Materials by Quadrupole ICP-MSGreen. P.A.. Beaconsfield/GB

P-ln-028 Petermination of Mo and Mn in human brain samples by different 782techniquesCsaszma. I.. Budapest/H. Andrasi, E., Budapest/H, Lasztity, A.,Budapest/H, Bertalan, E., Budapest/H, Gawlik, P., Berlin/P

P-ln-029 Comparison of NAA, ICP-AES and ICP-MS analysis for alkali metals in 783normal human brainBelavari, C. Budapest/H. Andrasi, E. Budapest/H, Bratter, P., Berlin/P,Agoston, Cs. Budapest/H, Molnar, Zs. Budapest/H

P-ln-030 Extending the scope of multi-element analysis of waters and wastes by 784ICP-AES - Determination of major, minor and trace elements including Cland Br using low UV spectral linesBrenner. I. B.. Jerusalem/IL. Dubuisson, C, Longjumeau/F, Cosnier, A.,Longjumeau/F, Tyler, G., Longjumeau/F, Le Marchand, A., Longjumeau/F

p-ln-031 Advanced transient ICP-OES diagnostics of flue gases to minimise toxicheavy metal emission from waste incineration plantsSwithenbank. J.. Sheffield/GB. Sharifi, V.N., Sheffield/UK, Clarkson, P.J.,Sheffield/UK, Yang, Y.B., Sheffield/UK, Ardelt, D., Kleve/D, Falk, H.,Kleve/D, Trassy, C, St-Martin d'Heres/F

P-ln-032 Improving the reproducibility and detection limits for the component 786analysis of the Cu-Sn and Fe-Nb-Ti alloys using the microwave plasmaoptical emission spectrometer with CCD detector.Agrafenin. A.V.. Moscow/RUS

P-ln-033 Laser Ablation-lnductively Coupled Plasma-Mass Spectrometric Analyte 187Concentration Calculation using Multiple Calibration Materials and MultipleInternal StandardsLongerich. H.. St. Johns/CDN. Jackson, S. E., Ryde/AUS, Gunther, D.,Zurich/CH

P-ln-034 Analysis of Trace Elements in Juvenile Fish Otoliths By ICP-MS 788Hu, Y.. Townsville/AUS. Patterson, H., Townsville/AUS, Kingsford, M.,Townsville/AUS

P-ln-035 Analysis of Lead, Cadmium and other Trace Metals in Chocolate by 789ICP/ICPMSKocherlakota. N. K.. Metuchen/USA. Obenauf, R.H., Metuchen/USA

P-ln-036 ICPAES abilities for analysis of plants within the Wageningen evaluating 790programmes for international analytical exchangeVuchkova. L. Sofia/BG

P-ln-037 Petermination of Selenium in Sediment by Isotope Pilution Inductively 797Coupled Plasma Mass Spectrometry with an Octopole Reaction CellInaoaki. K.. Tsukuba/J. Takatsu, A., Tsukuba/J, Nakama, A., Tsukuba/J,Chiba, K., Tsukuba/J, Okamoto, K., Tsukuba/J, Yabutani, T., Tokusima/J

P-ln-038 Comparison of ICP-MS with an Octopole Reaction Cell and Sector-field 792ICP-MS: Petermination of As and Se in SedimentInaoaki. K.. Tsukuba/J. Takatsu, A., Tsukuba/J, Nakama, A., Tsukuba/J,Chiba, K., Tsukuba/J, Okamoto, K., Tsukuba/J, Yabutani, T., Tokusima/J

P-ln-039 Algorithm for application of internal standard, on ICP-MS transient signals 793Kmetov. V.. Plovdiv/BG. Stefanova, V., Plovdiv/BG

P-ln-040 Characterisation of an Ombrotrophic Peat Bog Candidate Reference 794Material By High-Resolution and Quadrupole ICP-MSCairns. W.R.L.. Venice/I. Barbante, C, Venice/1, Cozzi, G., Venice/1,Moret, I., Venice/1, Cescon, P. Venice/1

P-ln-041 Flow Injection ICP Time-of-Fligth Mass Spectrometry Coupled to Hydraulic 795High Pressure Nebulizer for the Analysis of Low Volume BiologicalSamplesStefanka. Z.. Budapest/H

P-ln-042 Advanced ICP-AFS applications for the analysis of the composition of 796modern inorganic materialsMazo. G. N.. Moscow/RUS

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P-ln-043 Re-defining the limits of Quadrupole ICP-MS - innovative new high 797sensitivity 90 degree reflecting ion optics ICP-MS for routine sampleanalysis.Elliott. S.. Mulorave/AUS. Hoss, T., Parmstadt/D, Kalinitchenko, I.,Mulgrave/AUS

P-ln-044 Better ICP-MS Stability for Difficult Samples 798Plantz. M.. Wood Dale/USA. Anderson, S.E., Mulgrave/AUS, Elliott, S.,Mulgrave/AUS, Kalinitchenko, I., Mulgrave/AUS

P-ln-045 Direct determination of silicon in environmental water by ICP-MS with an 799Octopole Reaction CellYabutani. T.. Tokushima/J. Motonaka, J., Tokushima/J, Inagaki.K.,Tsukuba/J, Takatsu A., Tsukuba/J, Chiba K., Tsukuba/J

P-ln-046 Comparison of chemical and different electrochemical hydride generation 200systems coupled to microwave plasma torch optical emission spectrometry(MPT-OES) for the determination of arsenicOzmen. B., Leipzio/D. Bings, N. H., Hamburg/D, Broekaert, J. A. C.Hamburg/D

P-ln-047 Trace Element Determination in Natural Waters using Orthogonal Time of 207Flight ICP- MSSkroce. A.. Melbourne/AUS. Saint, A., Melbourne/AUS, McCrum, M.,Melbourne/AUS

P-ln-048 Drinking Water and Environmental Analysis: All Elements by a Single 202TechniqueSpence. B., Winsford/GB. Nelms, S. M, Winsford/GB

P-ln-049 Distribution of platinum group elements in urban aerosol 203Kanitsar. K.. Vienna/A. Koellensperger, G., Vienna/A, Hann, S., Vienna/A,Stingeder, G., Vienna/A, Limbeck, A., Vienna/A, Puxbaum, H., Vienna/A

P-ln-050 Comparison of isotope dilution analyses of geological materials using HR- 204ICPMS, conventional SSMS, MIC-SSMS and TIMSJochum. K. P.. Mainz/D. Willbold, M., Mainz/D, Stoll, B., Mainz/D, Amini,M., Mainz/P, Raczek, I., Mainz/D, Hofmann, A. W., Mainz/D

P-ln-051 Analysis of metals in plant material by supercritical fluid extraction 205and ICP-MSMcCrindle. R. I.. Pretoria/ZA, Botha, B.M., Pretoria/ZA, Marjanovic, B.,Pretoria/ZA, Voin, N., Pretoria/ZA

P-ln-052 Direct Trace Analysis of Ca and S in Oleochemicals by ICP-MS 206Abbes. H.. Gouda/NL. Wiedemann, S., Gouda / NL

P-ln-053 Analysis of additive metals in fuel and emission aerosols of diesel vehicles 207 jwith and without particle traps jUlrich. A.. Dubendorf/CH I

P-ln-054 Alternate solvents for the direct analysis of organic samples by ICP-OES 208 jNolte. J.. Owingen/P |

P-ln-055 Zinc concentrations during pregnancy 209 fSaldivar. L.. Mexico/MEX. Lastra, M. P., Mexico/MEX, Munguia, N.,Mexico/MEX, Martinez, K., Mexico/MEX, Aguilar, A. E., Mexico/MEX

p-ln-056 Comparison of Pifferent Analytical Procedures for the Reliable 270Petermination of Arsenic in Peat and Plant MaterialsFrank. J.. Heidelbero/P, Krachler, M., Heidelberg/D, Shotyk, W.,Heidelberg/P

p-ln-057 Petermination of As, Co, Cr, Cu, Mn, Ni, Se, V and Zn in biological 27 7materials by inductively coupled plasma dynamic reaction cell massspectrometry (ICP-PRCMS)Zischka. M.. Graz/A. Maichin, B., Graz/A, Motter, H., Graz/A, Knapp.G.,Graz/A

P-ln-058 "Routine" ICP-SFMS analyses at ultratrace levels (pg/g and fg/g) 272Cozzi. G.. Venezia/I. Barbante, C, Venezia/I, Cescon, P., Venezia/I

p-ln-059 Trace elements determination in seawater by ICP-SFMS coupled with a 273micro-flow nebulization/desolvation systemTuretta. C. Venice/I. Barbante, C, Venice/I, Cozzi, G., Venice/I,Capodaglio, G., Venice/I

P-ln-060 Analysis of Organophosphorus Pesticides by GC-ICP-MS 274Vonderheide. A. P.. Cincinnati/USA. Montes-BayOn, M., Cincinnati/USA,Caruso, J., A., Cincinnati/USA

P-ln-061 Microwave Pigestion Procedures for Bio-Monitoring of Neurotoxic Elements 275in HumanBocca, B.. Rome/I. Forte, G., Rome/I, Petrucci, F.,Rome/l, Senofonte, 0.,Rome/I, Violante, N., Rome/I, Alimonti, A., Rome/I

P-ln-062 Petermination of 90Sr by ICP-MS 276Taylor. V. F., Peterborouqh/CPN. Epov, V., Peterborough/CDN, Evans, R.D., Peterborough/CDN, Cornett, R. J., Ottawa/CPN

P-ln-063 On line polyatomic interference removal for Fe determination by ICP-MS 277(shield torch) using a desferal-solgel microcolumnSequra. M.. Madrid/E. Madrid, Y., Madrid/E, Camara, C., Madrid/E

P-ln-064 Applications of a New Inductively Coupled Plasma Spectrometer with a 278Classic Vertical TorchHoult. P. W.. Seer Green/GB. Yates, D., Shelton/USA

P-ln-065 Development of a method for the determination of Co, Ni, Ti, Cr and Mo in 279biological fluids by means of Inductively Coupled Plasma MassSpectrometry (ICP-MS)Sarmiento Gonzalez. A., Oviedo/E. Sariego Muniz C, Oviedo/E,Marchante-Gayon J. M., Oviedo/E, Sanz-Medel, A. Oviedo/E

P-ln-066 Determination of phosphorus concentration in small protein samples by 220ICP-MS and LA-ICP-MS in combination with 2D gel electrophoresisBecker. J. S.. Julich/P. Boulyga, S. F., Julich/P, Pickhardt, C, Julich/P,Becker, J. S., Konstanz/D, Przybylski, M., Konstanz/D

P-ln-067 Liquid Chromatography Coupled to High Resolution SF-ICP-MS and 227Electrospray Mass Spectrometry for the Determination of PhosphorylationSites in Tryptic Digests of Peptides.Cartwriqht, A. J.. Plvmouth/GB. Evans, E. H., Plymouth/GB, Jones, P.,Plymouth/GB, Wolff, J. C, Stevenage/GB, Eckers, C, Stevenage/GB,Schneider, K., Harlow/GB

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P-ln-068 Environmental Impact of Road Transport Pollutants in the Aspe Valley 222(Pyrenees, France)Veschambre. S., Pau/F. Moldovan, M., Pau/F, Amouroux, D., Pau/F,Pinaly, H., Pau/F, Ponard, O. F. X., Pau/F

P-ln-069 Sampling and Analysis of Mercury Species in Combustion Flue Gas 223Pavaoeau. M. P.. Pau/F, Pecheyran, C, Pau/F, Krupp, E., Pau/F, Morin,A., Verneuil-en Halatte/F, Ponard, O. F. X., Pau/F

P-ln-070 Petermination of Al in Foodstufs by ICP-AES and ITS Leachability from Al- 224CookwareMilacic. R.. Liubliana/SLO. Scancar, J., Ljubljana/SLO

P-ln-071 Geochemical Samples Analysis Using Atomic Spectrometric Methods 225Safronova, N. S.. Moscow/RUS, Mazo, G. N., Moscow/RUS, Shepeleva, E.S., Moscow/RUS

P-ln-072 Fast and sensitive multi-element quantification in clinical samples with high- 226resolution sector-field ICP-MSHinrichs. J.. Bremen/P. Aubry, J.-C, Bruxelles/B, Boeynaems, J.-M.,Bruxelles/B

P-ln-073 Simultaneous Measurement of Cu.Zn and Se in Physiological Fluids 227Roberts. E.A, Liverpool/GB. Roberts, N.B., Liverpool/GB, Nelmes, S.M,Winsford/GB

P-ln-074 Changes of the metal concentration in white German wines during different 228wine-making processesCastineira. M.. Portmund/P, Brandt, R. Portmund/P, Jakubowski, N.Portmund/P, Andersson, J. Munster/P.

P-ln-075 The application of ICP-TOF-MS technique to the determination of toxic 229elements in food-packaging materialsSkrzvdlewska. E., Warsaw/PL, Balcerzak, M., Warsaw/PL

P-ln-076 Trace analysis of hydride forming elements and "normal" by ICP-OES in 230complex samplesTyler. G.. Lonqiumeau/F. Cosnier, A., Longjumeau/F, Velasquez, S.,Longjumeau/F, Bartha, A., Budapest/H, Ballok, M., Budapest/H, Nehm, R.,Grasbrunn/P

P-ln-077 Speciation analysis of arsenic with HPLC coupled to Element Sector Field 237ICPMSZheno. J.. Peterborough/CPN. Dimock, B., Peterborough/CDN, Dzsuko,M.S., Peterborough/CDN, Hintelmann, H., Peterborough/CDN

P-ln-078 Direct Seawater Analysis by Inductively Coupled Plasma Mass 232Spectrometry Using a Mixed-Gas Plasma, Flow Injection and ExternalCalibrationHollidav. A.E.. Kinqston/CDN. Beauchemin, D. Kingston/CDN

P-ln-079 A possible steady state kinetic model for the effects of easily ionized 233elements on analyte ion lines in the ICP: Application to interference effectsof excess Li on the Ca ion lineZaranvika. M.F.. Harare/ZW. Chirenje A.T., Harare/ZW

p-ln-080 The use of glow discharge graphite hollow cathode as an excitation source 234for atomic emission trace level analysisShuvaeva. O.V.. Novosibirsk/RUS. Galdina N.V.,Novosibirsk/RUS,Saprykin A.I.,Novosibirsk/RUS

p-ln-081 Analysis of ultra high purity (UHP) chemicals by ICP-MS: Tasks, 235possibilities and limitationsBlodorn, W.. Seelze/D. Potter, D., Cheshire/GB

P-ln-082 A new time of flight mass spectrometer combined with an ICP 236Ludke. C. Berlin/D. Hoffmann, E., Berlin/D, Skole, J., Berlin/D,Wollbrandt, J., Berlin/D

P-ln-083 Determination of Uranium and Thorium Concentration and 235U/238U 237Isotope Ratios at Trace and Ultratrace Level in Urine by ICP-MS and LA-ICP-MSBurow. M.. Julich/D. Boulyga, S.F., Juelich/P, Pickhardt, C, Juelich/P,Ostapczuk ,P., Juelich/P, Becker, J. S,Juelich/P

Sample introduction and pretreatment Konzertsaal Richard Strauss

P-Sa-001 Matching purified water quality to experimental detection limits 238Mabic. S.. St. Quentin en Yvelines/F. Kano, I., St. Quentin en Yvelines/F ,Parbouret, P., St. Quentin en Yvelines/F

P-Sa-002 Petermination of refractory elements in used lubricating oil by ICP-OES 239employing emulsified sample introduction and calibration with inorganicstandardsPorto da Silveira. C.L.. Rio de Janeiro/BR, Souza, R.M., Rio de Janeiro/BR,Aucelio, R.Q.A., Rio de Janeiro/BR

P-Sa-003 Evaluation of Electrochemically Modulated Separations Coupled On-line 240with Time-Of-Flight ICP-MSPuckworth. D.C., Oak Ridoe/USA. Park, S.H., Oak Ridge/USA, Van Berkel,G.J., Oak Ridge/USA

P-Sa-004 Inorganic multielemental speciation by SECjCOupled-ICP-MS 247Castillo. J.R.. Zaraqoza/E. Laborda, F., Zaragoza/E, Medrano, J.,Zaragoza/E

P-Sa-005 Use of a Single Extractant Sequential Extraction Procedure with 242Chemometric Pata Treatment and ICP-AES Analysis to Asses the MetalPistribution within the Physico-Chemical Components in SedimentsHill. S. J.. Plvmouth/GB. Santamaria-Fernandez, R., Plymouth/GB Cave,M.R., Nottingham/GB

P-Sa-006 The Effect of Humic Acids on the Sequential Extraction of Metals from Soils 243Hill. S. J.. Plvmouth/GB. Santamaria-Fernandez, R., Plymouth/GB, Cave,M.R., Nottingham/GB

P-Sa-007 An Application of Computational Fluid Pynamics (CFP) to the 244Characterisation and Optimisation of a Cyclonic Spray Chamber for ICP-AES and ICP-MS.Berndt. H.. Portmund/P. Schaldach.G., Dortmund/D, Razilov.l.,Dortmund/D, Sharp, B.L. Loughborough/GB

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P-Sa-008 Enhanced Detection of Platinum Group Elements with ICP-AES usingUltrasonic NebulizationSmith. F.. Omaha/USA

P-Sa-009 Micro-Suction ICP-MS for small volume sample analysisKomoda. M.. Yamaquchi/J, Mori, Y., Yamaguchi/J, Uemura, K.,Yamaguchi/J

P-Sa-010 Determination of Low Concentrations of Stable and Radiogenic CesiumUsing Cation Exchange and Inductively Coupled Plasma MassSpectrometryEpov. V.N.. Peterborouqh/CDN. Lariviere, D., Peterborough/CDN, Taylor,V., Peterborough/CDN, Evans, R.D., Peterborough/CDN, Cornett, R.J.,Ottawa/CDN

P-Sa-011 Petermination of Ra-226 in soils and sediments by EC-ICP-MSEPOV. V.N.. Peterborough/CPN. Lariviere, P., Peterborough/CPN, Evans,R.P., Peterborough/CPN, Cornett, R.J., Ottawa/CPN

P-Sa-014 Petermination of Butyltin compounds in harbour sediments using closed-vessel microwave extractionMonperrus, M.. Pau/F. Benoit, C, Pau/F, Krupp, E.M., Pau/F, Ketisch, P.,Graz/A, Ponard, O.F.X., Pau/F

P-Sa-015 An offline methode for matrix stripping and preconcentration of seawaterand brines using a chelating resinVan Os. B.J.H.. Utrecht/NL. Klaver, G.Th. Utrecht/NL, Van Vilsteren, E.Utrecht/NL, Pe Lange G.J. Utrecht/NL, Corrales E. Utrecht/NL

P-Sa-016 Petermination of Cationic Trace Impurities in Ultrapure Salts usingChelation Ion Chromatography/lnductively Coupled Argon PlasmaSpectroscopyPfluqer. M.. Buchs/CH. Armbruster, J., Buchs/CH, Gerth, R., Buchs/CH

P-Sa-017 A Comparison Between the North American Soils Pigestion Procedure andthe German PIN S7 Soil Digestion on a Temperature Controlled GraphiteBlock Digester Using a CRMRoss. A., Montreal/CDN. Kainrath, P., Ueberlingen/D

P-Sa-018 Ultrapure Water for Elemental AnalysisMabic. S.. St. Quentin en Yvelines/F. Kano, I., St. Quentin en Yvelines/F,Darbouret, D., St. Quentin en Yvelines/F

P-Sa-019 Microwave induced plasmas in atmospheric pressure for the modification ofsurfacesSeelio. M.. Dortmund/D. Stonies, R., Dortmund/D, Voges, E., Dortmund/D

P-Sa-020 Sample preparation of electronic-chemicals and analysis by ICP-MSBlodorn. W., Seelze/D

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Speciation of Non-Pesticidal Organotin Compounds Using Gas 256Chromatography with Inductively Coupled Plasma-Mass SpectrometryGallagher. P.A., Cincinnati/USA. Even, O., Cincinnati/USA, Parks, A.N.,Cincinnati/USA, Schwegel, C.A., Cincinnati/USA, Ackerman, A.H.,Cincinnati/USA, Creed, J.T., Cincinnati/USA, Wilbur, S., Seattle/USA

Considerations for the coupling of HPLC to ICP-MS systems: More than 257just joining a tubelWalker. H. J., Manchester/GB. Abou-Shakra, F.R., Manchester/GB ,Eaton, A.N., Manchester/GB

LC - high-efficiency photooxidation - hydride generation - ICP-MS for 258determination of ultra-trace levels of highly methylated arsenicals inenvironmental watersNakazato. T.. Tsukuba/J. Tao, H., Tsukuba/J

Elemental Proteomics I: Application of Particle Beam/Hollow Cathode- 259Optical Emission Spectroscopy (PB/HC-OES) for Total ProteinDeterminations based on Atomic Carbon ResponsesMarcus. R. K.. Clemson/USA. Jin, F., Clemson/USA, Lenghaus, K.Clemson/USA, Hickman, J.J., Clemson/USA

Speciation Analysis of Arsenic by IC-ICP-DRC-MS 260Gurlevuk. H.. Seattle/USA

Direct volatile organo-selenium speciation using SPME 267Dietz. C. Madrid/E. Perez-Corona, T., Madrid/E, Madrid-Albarran, Y.,Madrid/E, Camara, C, Madrid/E

A Comparison of Hydride Generation Atomic Fluorescence and Inductively 262Coupled Plasma-Mass Spectrometry Detectors for the LiquidChromatographic Determination of Arsenic Species in FoodsDeNicola. K.. Cincinnati/USA. Grant, T.D., Cincinnati/USA, Caruso, J.A.,Cincinnati/USA, Heitkemper, D.T., Cincinnati/USA

Improving detection limits for speciation analysis using sector field ICP-MS 263Lindemann. T.. Bremen/D. Hamester, M. Bremen/D, Wills, J. Bremen/D,Hinrichs, J. Bremen/D

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Speciation of organonotins: comparison of GC-LRMS, GC-HRMS and GC- 264ICP-MSTirez. K.. Mol/B. Vanermen, G., Mol/B, Brusten, W., Mol/B, Borburgh, A.,Mol/B, Debaene, L., Mechelen/B

A Commercial Interface for the coupling of GC with ICP/MS 265Krupp. E.M.. Pau/F. Pecheyran, C, Pau/F, Vindel, A., Madrid/E, Brenner,I.B., Jerusalem/IL, Donard, O.F.X., Pau/F

Multi-Element Determination and Fractionation Using a Sequential Hydride 266Generation / Pneumatic Nebulisation (HG/PN) ICP-MS SystemPerqantis. S. A.. London/GB. Anderson, S., London/GB

Ion Chromatography and ICP-MS Detection of Phosphonates 267Kovacevic. M.. Liubliana/SLO. Novic, M., Ljubljana/SLO

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P-EI-013 A quantitative approach for the determination of Se-methionine in yeast 268and nuts using methanesulfonic acid for protein hydrolysis.Kannamkumarath. S. S.. Cincinnati/USA, Wrobel, K., Cincinnati/USA,Wrobel, K., Cincinnati/USA, Caruso, J. A., Cincinnati/USA

P-EI-014 Extraction and characterization of metal proteins from liver samples: 269aspects of sample pretreatment and cell fractionationNischwitz, V.. Neuherbero/D, Michalke, B., Neuherberg/P, Kettrup, A.,Neuherberg/D

P-EI-015 Use of the dynamic reaction cell (PRC) technology for the detection of Se 270and V in biological samplesCherv. C. C. Ghent/B. De Cremer, K., Ghent/B, Gunther, D., Zurich/CH,Vanhaecke, F., Ghent/B, Cornells, R., Ghent/B, Moens, L, Ghent/B

P-EI-016 Advantages of narrow bore anion exchange chromatography coupled to 277ICP-MS for metal speciation in environmental samplesAmmann. A. A.. Pubendorf/CH

P-EI-017 Direct Determination of Arsenic Species in Urine by Ion Chromatography 272Coupled with Inductively Coupled Plasma Mass SpectrometryNam, S., Chonnam/SK. Kim, J., Chonnam/SK, Han, S., Chonnam/SK

P-EI-018 Speciation of Elements in Industrial Sludge by Ion Chromatography 273Coupled with Inductively Coupled Plasma Mass SpectrometryLee. J.. Taeion/ROK, Nam, S., Chonnam/SK, Kim, J., Chonnam/SK, Han,S., Chonnam/SK

P-EI-019 Speciation of germanium compounds and multi-element screening with 274HR-ICPMS for the analysis of commerical medicineKrvstek, P.. Bilthoven/NL. Ritsema, R., Bilthoven/NL

P-EI-020 Arsenic Speciation in infected human hair and nail samples 275Patel. K. S.. Raipur/IND. Raab, A., Aberdeen/UK, Feldmann, J.,Abberdeen/UK, Shrivas, K., Raipur/IND

P-EI-021 Exploration of arsenic species in drinking water of central India 276Patel. K. S.. Raipur/IND. Shriva, K., Raipur/IND, Brandt, R., Dortmund/D,Jakubowski, N., Dortmund/D, Corns, W. London/UK

P-EI-022 Hyphenation of different separation techniques with octopole reaction cell 277ICP-MS for species analysis of biologically relevant moleculesProefrock. P.. Geesthacht/D. Leonhard, P., Geesthacht/D, Prange, A.,Geesthacht/D

P-EI-023 The Liberation of Arsenosugars from Matrix Components in Difficult to 278Extract Seafood Samples Utilizing TMAOH / Acetic Acid Sequentially in aTwo-Stage Extraction ProcessParks, A. N., Cincinnati/USA. Gallagher, P. A., Cincinnati/USA, Schwegel,C. A., Cincinnati/USA, Ackerman, A. H., Cincinnati/USA, Creed, J. T.,Cincinnati/USA

P-EI-024 A Mass Balance Approach to Determine Arsenic Absorption Rates from 279Contaminated Water by Rice During the Food Preparation ProcessAckerman. A. H.. Cincinnati/USA. Gallagher, P. A., Cincinnati/USA, Parks,A. N., Cincinnati/USA, Schwegel, C. A., Cincinnati/USA, Creed, J. T.,Cincinnati/USA, Heitkemper, D. T., Cincinnati/USA, Vela, N. P.,Cincinnati/USA

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Investigation of Volatile Selenium Species in Coffee by GC-ICP-MS 280Meiia. J.. Cincinnati/USA. Bryson, J. M., Cincinnati/USA, Vonderheide, A.P., Cincinnati/USA, Montes-Bayon, M., Oviedo/E, Caruso, J. A.,Cincinnati/USA

HPSEC-ICP-MS Studies for Elements Bound to Humic Substances in 287Compost Obtained from Urban Solid WasteSadi, B. B. M. Cincinnati/USA. Wrobel, K., Guanajuato/MEX, Wrobel, K.,Guanajuato/MEX, Castillo, J. R., Zaragoza/E, Caruso, J. A., Cincinnati/USA

Nickel species analysis of cytosols of malignant and healthy tissues of 282human colon using CE and SEC coupled to ICP-MSKnispel. T.. Geesthacht/D. Bonsack, S., Geesthacht/D, Prange, A.,Geesthacht/D, Denkhaus, E., Puisburg/P

Biogenically produced halocarbons determined by two-dimensional 283detection with ECD and ICP-MS after GC-separationSchwarz, A., Mainz/D. Heumann, K. G., Mainz/D

Continuous Differentiation of Arsenic Species by on-line Microdialysis- 284Microbore-HPLC-CollisionCell-ICP-MSLee. P. L. Hsinchu/RC. Yang, M. H., Hsinchu/RC, Sun, Y. C ,Hsinchu/RC, Chung, Y. T., Hsinchu/RC

Speciation of carbon containing compounds using Hot Water 285Chromatography Coupled to an Inductively Coupled Mass SpectrometerAbou-Shakra. F. R.. Manchester/GB. Smith, C. J., Macclesfield/GB, Wilson,I. D., Macclesfield/GB, Payne, R., Macclesfield/GB, Walker, H. J.,Manchester/GB, Eaton, A. N., Manchester/GB

Separation of Plutonium and Neptunium Species by CE - ICP - MS and 286Application of this Method to Natural Groundwater SamplesKuczewski. B.. Mainz/D. Geckeis, H., Karlsruhe/D, Kratz, J. V., Mainz/D,Marquardt, C, Karlsruhe/P, Seibert, A., Karlsruhe/P, Trautmann, N.,Mainz/P

Quantification strategies in CE-ICP-MS 287Koellensperger. G.. Vienna/A. Nurmi, J., Vienna/A, Hann, S., Vienna/A,Prohaska, T., Vienna/A, Stingeder, G., Vienna/A

Investigation of metal - ligand complexatiorf relevant in the industrial 288production process of viscose fibersNurmi. J.. Vienna/A. Koellensperger, G., Vienna/A, Stingeder, G.,Vienna/A, Potthast, A., Vienna/A, Rosenau, T., Vienna/A

New sample preparation schemes for characterisation of high molecular Se 289species in yeastRuiz-Encinar. J.. Pau/F. Sliwka-Kaszynska, M., Pau/F, Pernovics, M.,Pau/F, Ruzik, R., Pau/F, Szpunar, J., Pau/F

HPLC-IP-ICP-MS for Speciation of Antimony: a Contribution 290Kahr, E.. Leoben/A. Matos J., Lissabon/P, Wegscheider W., Leoben/A

Comparison of extraction procedures for the determination of butyltin 297compounds in CRM 477 (mussel tissue) by multiple-spike isotope dilutionGC-ICP-MSRodriguez-Gonzalez. P.. Oviedo/E. Ruiz Encinar, J., Oviedo/E,Garcia Alonso, J. I., Oviedo/E, Sanz-Medel, A., Oviedo/E

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Comparison of microwave extraction and accelerated solvent extraction 292(ASE) for arsenic speciation in environmental samples and herbal medicinefollowed by HPLC-ICP-MS analysis.Wahlen. R.. Teddinoton/GB, Catterick, T. Teddington/GB

Selenium Incorporation into Brassica juncea for Contaminated Soil 293PeNicola. K.. Cincinnati/USA. Shann, J. R., Cincinnati/USA, Caruso, J. A.,Cincinnati/USA

The Investigation of Arsenosugar Interactions with Matrix Components in 294Difficult to Extract Seafood Matrices using an On-Column Mass BalanceApproachCreed. J. T.. Cincinnati/USA. Gallagher, P. A., Cincinnati/USA, Schwegel,C. A., Cincinnati/USA, Parks, A. N., Cincinnati/USA, Ackerman, A. H.,Cincinnati/USA, Shoemaker, J. A., Cincinnati/USA

Comparative parameter study about hydride generation of arsenic, tin, 295antimony and mercury species: effect of pH, amount of NaBH4, L-cysteineand metal(oid) interferencesFelix. J.. Essen/D. Diaz-Bone, R. A., Essen/D, Hirner, A.V., Essen/D

Multi-element organometal(oid) analysis by pH-gradient hydride generation 296Diaz-Bone. R. A.. Essen/D. Felix, J., Essen/D, Hirner, A. V., Essen/D

Synthesis Characterization and Determination Of Selenonium Species in 297Plant TissueGrant. T.. Cincinnati/USA. Fricke, M. W., Cincinnati/USA, Montes-BayOn,M., Cincinnati/USA, Caruso, J. A., Cincinnati/USA

Passive sampling of metal ions in water by DGT technology 298Rovset. P.. Oslo/N

Rapid Determination of Mercury Species in Environmental Samples by 299MCGC-ICP-TOFMS Following in situ Ethylation and Purge-and-TrapInjectionJitaru. P.. Antwerp/B. Goenaga Infante, H., Antwerp/B, Adams, F. C,Antwerp/B

A Novel Microwave Assisted Method for the Sample Preparation of the 300Determination of Organotin Compounds by GC-ICP-MSFruhmann, H.. Graz/A. Knapp, G., Graz/A , Zischka, M., Graz/A

Applications of ICP-MS to the Speciation of "Biometals" 307Bettmer. J.. Mainz/D. Bruchert, W., Mainz/D

Characterisation of metailothioneins using HPLC-ICP-MS coupling 302techniquesBruchert. W.. Mainz/D. Bettmer, J., Mainz/D

Speciation Analysis of Cyanide by IC-ICP-DRC-MS 303Gurlevuk. H.. Seattle/USA. Kilner, P., Seattle/USA, Mitchell, S.,Seattle/USA

Extraction and Determination of Hexavalent Chromium in Fish Tissue 304Gurlevuk. H.. Seattle/USA. Mitchell, S., Seattle/USA

p-EI-052 Particle Beam/Glow Discharge Mass Spectrometry (PB/GDMS): A NewTool in Identification and Sequencing of Nucleosides, Nucleotides, andMixed-Base Sequence ss-DNA OligonucleotidesMarcus, R. K., Clemson/USA. Davis, W. C , Clemson/USA, Venzie, J. L,Clemson/USA

|. p-EI-053 Determination of total thorium and REE in soil water and its humic fractionby ICP-MS and on-line coupled size exclusion chromatographyMiekelev. N., Rio de Janeiro/BR. Casartelli, E. A., Rio de Janeiro/BR

P-EI-055 Sequential extractions of selenium soils: total selenium and speciationmeasurements with ICP-MS detectionPonce de Leon. C. Cincinnati/USA. DeNicola, K., Cincinnati/USA, MontesBayon, M., Cincinnati/USA, Caruso, J. A., Cincinnati/USA

P-EI-056 Speciation of Arsenic in Crop, Vegetable and Soil Samples from an AreaIrrigated with Arsenic Contaminated Groundwater in West Bengal, IndiaGrant. T. P., Cincinnati/USA. Vela, N. P., Cincinnati/USA, Heitkemper, P.T., Cincinnati/USA, Chowdhury, U. K., Kolkata/INP, Rahman, M. M.,Kolkata/INP, Samanta, G., Kolkata/IND, Chakraborti, D., Kolkata/IND,Sekaran, N. C , Tokyo/J, Tokunaga, H., Tokyo/J

•'•»' P-EI-057 Comparison between Capillary Electrophoresis with UV detection andAnion Chromatography Inductively Coupled Plasma Mass Spectrometry forAntimony SpeciationCosta Casado, R.. Hannover/D. Ulrich, N., Hannover/P

P-EI-058 Arsenic stability in riceCamara, C , Madrid/E. Pizarro, I., Madrid/E, Gimez, M., Madrid/E, PalaciosM. A., Madrid/E

P-EI-059 Simultaneous determination of mono-, di- and tributyltin in environmentalsamples using isotope dilution gas chromato-graphy with massspectrometric detection: comparison of electron impact ionisation-massselective detection and inductively coupled plasma-mass spectrometryCentineo, G.. Oviedo/E. Rodriguez-Gonzalez, P., Oviedo/E, BlancoGonzalez, E., Oviedo/E, Garcia Alonso, J. I., Oviedo/E and Sanz-Medel,

' A., Oviedo/E

P-EI-060 Speciated Isotope Pilution for the simultaneous Petermination of MercuryCompounds and Tributyltin in the EnvironmentMonperrus. M.. Pau/F. Tessier, E., Pau/F, Rodriguez, R., Toledo/E,Amouroux, P., Pau/F, Donard, O. F. X., Pau/F

P-EI-061 Sensitive species-specific determination of a new metallodrug and itsmetabolites in blood by cation exchange HPLC - ICP MSVacchina. V.. Pau/F. Torti, L., Bresso/I, Allievi, C., Bresso/I, Lobinski, R.,Pau/F

P-EI-062 Temporal variations in the composition and size distribution of natural watercolloids and associated elements in the Kalix River by FIFFF - HR ICPMSAndersson. K., G6teborq/S. Larsson, T., G6teborg/S, Stolpe, B.,G6teborg/S, Turner, P., G6teborg/S

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P-EI-063 Speciation analysis of Ni in a hyperaccumulating plant by multidimensionalhyphenated techniques assisted by molecular biologyVacchina. V.. Pau/F. Mari, S., Montpellier/F, Lebrun, M., Montpellier/F,Lobinski, R., Pau/F

P-EI-064 Sensitive determination of selenomethionine by anion exchange HPLC -ICPMSVacchina. V.. Pau/F, Lobinski, R., Pau/F

P-EI-065 Using HPLC - ICP-MS to Study the Non-Enzymatic Methylation of Arseniteby MethylcobalaminPeraantis. S. A.. London/GB. Miguens-Rodriguez, M., London/GB,Heitkemper, P. T., Cincinnati/USA, Vela, N. P., Cincinnati/USA

P-EI-066 Size fractionation of non volatile dissolved organic carbon and metalspecies in German white winesCastineira. M.. Portmund/P. Burba, P. Portmund/P, Jakubowski, N.Portmund/P, Andersson, J. Munster/D.

P-EI-067 Exploration of Arsenic Species in Drinking Water of Central IndiaPatel. K. S.. Raipur/IND. Shrivas, K., Raipur/IND, Brandt, R., Dortmund/P,Jakubowski, N., Dortmund/D, Corns, W., London/GB

P-EI-068 Mercury speciation in environmental samples using GC-ICP-MS and GC-Py-AFS couplingsGomez-Ariza. J. L. Huelva/E. Lorenzo, F., Huelva/E, Sanchez-Rodas, D.,Huelva/E

P-EI-069 Comparative study of ICP-MS and AFS detectors for selenium chiralspeciation in breast and formula milkGomez-Ariza. J. L. Huelva/E. Bernal-Daza, V., Huelva/E, Sanchez-Rodas,D., Huelva/E

P-EI-070 Determination of arsenic species in marine CRMs by ion-exchange HPLC-ICPMS - emphasis on minor constituentsSloth. J. J.. Berqen/N. Julshamn, K., Bergen/N, Larsen, E. H., Soborg/DK

P-EI-071 Speciation of Aluminium complexes relevant in plant physiology by meansof Ion Chromatography-ICP-AESSeubert. A.. Marburo/D, Borrmann, D., Hannover/P, Busch, M.,Hannover/D

P-EI-072 Synthesis of Y-glutamyl-Se-methionine: A Standard for Chemical Speciationof Selenium Enriched GarlicFricke. M.. Cincinnati/USA. Grant, T. D., Cincinnati/USA, Caruso, J. A.,Cincinnati/USA

P-EI-073 Speciation of lodinated Phenols in Water Samples by GC-ICP-MSCaruso. J. A.. Cincinnati/USA. Wuilloud, R. G., Cincinnati/USA, deWuilloud, J. C. A., Cincinnati/USA, Vonderheide, A. P. Cincinnati/USA

P-EI-074 Determination of Iodine in Coastal Atmospheric Particles using InductivelyCoupled Plasma Mass Spectrometry (ICP-MS)Chen. H.. Dortmund/D. Brand, R., Dortmund/D, Jakubowski, N.,Dortmund/D, Hoffmann, T., Dortmund/D

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I75 New Evidence on Refractory Arsenicals in estuarine waters obtained by 327HPLC-MW-HG-QFAAS, Ultrafiltration and LC-ESI-Msnde Bettencourt. A.. Evora/P. Capelo, S. G., Evora/P, Carapeto, C. M.,Lisboa/P, Florencio, M. H., Lisboa/P, Gomes, M. L. R., Oeiras/P, VilasBoas, L. F., Oeiras/P, Larsen, B. R., Ispra/I

Phosphorus-31 ICP-MS - a New Tool in Analysis of Protein 328PhosphorylationLehmann. W.D., Heidelberg/D. Wind, M. Dortmund/D, Jakubowski, N.,Dortmund/D

pe analyses Raum Alpspitze

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Overcoming present limitations in ICP-MS for iron measurements 329Voql. J.. Berlin/D. Klingbeil, P., Berlin/D, Pritzkow, W., Berlin/D, Riebe, G.,Berlin/D, Wermann, G., Berlin/D

Accurate measurement of Selenium Isotopes in Difficult Matrices by MC- 330ICP-MS.Goldsmith. S. L. Manchester/GB. Palacz, Z., Manchester/GB

Uranium isotope ratio measurements using a collision cell interfaced multi- 337collector mass spectrometerGoldsmith. S. L.. Manchester/GB. Palacz, Z., Manchester/GB, Meffan-Main, S., Manchester/GB, Turner P. J., Manchester/GB

Uranium isotope ratio measurements using multiple ion counting on a multi- 332collector ICPMSPalacz. Z.. Manchester/GB. Goldsmith, S. L., Manchester/GB, Meffan-Main, S., Manchester/GB, Turner, P. J., Manchester/GB

Laser Ablation Multi-lon-Counting-ICPMS 333Schwieters. J.B.. Bremen/D. Bouman, C, Bremen/D, Tuttas, D., Bremen/D

Application of ICP-MS for environment monitoring of long-lived 334radionuclides in contaminated areas in BelarusBoulvqa. S.F.. Julich/D. Becker, J.S. Julich/D

Sample clean-up by HPLC-ICP-MS for Am determination by alpha 335spectrometryPema. L.. Karlsruhe/P. Jernstrom, J.,Karlsruhe/P, de Pablo, J.,Barcelona/E, Betti, M., Karlsruhe/P

Certification of trace element amount contents in food matrices using 336Isotope dilution Inductively coupled plasma mass spectrometry: Importantanalytical challengesVassileva. E.. Geel/B. Quetel, C. R., Geel/B, Taylor, P. P. P., Geel/B

Uncertainty Contributions to Isotope Pilution Analysis ICP MS for Mercury 337SpeciationClouqh. Robert. Plvmouth/GB. Evans, E. H., Plymouth/GB, Belt, S.,Plymouth/GB, Fairman, B., Teddington/GB

Isotopic composition of zinc 338Tanimizu. M., Tokvo/J. Asada, Y., Tokyo/J, Hirata, T., Tokyo/J

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P-ls-011 High Precision Measurement of Lead Isotopes In Natural Waters by MC- 339ICP-MSMotelica-Heino. M.. Orleans/F. Robert, M., Orleans/F, Cocherie, A.,Orleans/F

P-ls-012 Study of elemental mobility wihtin a soil profile using isotopic fingerprints 340measured by ICP-SFMSProhaska. T.. Vienna/A. Schultheis, G., Vienna/A, Wenzel, W., Vienna/A,Stingeder, G., Vienna/A

P-ls-013 Analysis of biogenic Sr in archaeological samples by ICP-MS 347Schultheis. G.. Vienna/A, Prohaska, T., Vienna/A, Teschler-Nicola, M.,Vienna/A, Stingeder, G., Vienna/A

P-ls-014 Comparison of ICP-MS and alpha-spectroscopy for the evaluation of 342environmental contamination with depleted uranium in the post conflictenvironment.Campbell, M. J. Vienna/A, Moreno J., Vienna/A, Burns K.I., Vienna/A

P-ls-015 The use of Cd icotope dilution ICP-MS in the study of metal - bacterial 343community relationshipScancar. J.. Liubliana/SLO. Amouroux, D., Pau/F Point, D. Pau/FMonperrus, M., Pau/F, Ponard, O.F.X., Pau/F

P-ls-016 Evaluation of EDTA as mobile phase for the separation of transition and 344rare earth elements using Ion Chromatography with ICP-MS detection.Garcia. R.. Oviedo/E. Garcia Alonso, J.I., Oviedo/E, Sanz-Medel, A.,Oviedo/E

P-ls-017 Isotopic analysis of nanogram Li samples by quadrupole ICPMS 345Kosler. J.. Praque/CZ. Horka, M., Prague/CZ, Libertinova, J., Prague/CZ

P-ls-018 21 OPb: can it be determined by ICPMS? 346Ketterer. M. E.. Flagstaff/USA, Matisoff, G., Cleveland/USA, Wilson, C.G.,Cleveland/USA

P-ls-019 236U as a tracer of anthropogenic U: three case studies by sector ICPMS 347Ketterer. M. E.. Flaostaff/USA. Hafer, K., Flagstaff/USA, Royden, C,Flagstaff/USA, Link, C, Flagstaff/USA, Hartsock, W., Flagstaff/USA

P-ls-020 Resolving global vs. local/regional Pu sources in the environment by sector 348ICPMSKetterer. M. E.. Flaastaff/USA. Hafer, K., Flagstaff/USA, Royden, C,Flagstaff/USA, Link, C, Flagstaff/USA, Hartsock, W., Flagstaff/USA

P-ls-021 Uranium Isotope Ratio Measurements in Saline Solutions by MC-ICP-MS: 349A Comparative Study Between On- and Offline Matrix SeparationKopaitic. Z.. Villiqen/CH, Giinther-Leopold, I., Villigen/CH, Wernli, B.,Villigen/CH

P-ls-022 A short comparison of quadrupole and multicollector ICP-MS for the 350measurement of Ca absorption in nutritional studies using the dual tracertechniqueKastenmaver. P.. Lausanne/CH. Hoogewerff, J., Norwich/GB

P-ls-023 Elemental Fingerprinting and lostope Ratio Determinations of Coins by LA- 357DRC-ICP-MS using a non-destructive Sampling TechniqueTalib. P.. Sheffield/GB, Green, P., Beaconsfield/GB

p-ls-024 Certification of the n(235U)/n(238U) isotope ratio in human urine samples 352within ~ 2% uncertainty using sector field ICP-MSTresl. I.. Geel/B. De Wannemacker, G., Gent/B, Quetel, C. R., Geel/B,Petrov, I., Geel/B, Moens, L, Gent/B, Taylor, P. P. P., Geel/B

p-ls-025 On-line Determination of Cadmium in Waters Using Isotope Dilution 353Combined with Preconcentration and Matrix Elimination TechniquesPoint. P.. Pau/F. Krupp, E., Pau/F Moldovan, M., Pau/F Scancar, J., Pau/F,Amouroux, P., Pau/F, Bareille, G., Pau/F, Ponard, O.F.X., Pau/F

P-ls-026 Advantages of Sector Field ICP-MS for Nuclear Applications 354Hamester. M., Bremen/P. Wills, J., Bremen/P, Hinrichs, J., Bremen/D,Lindemann, T., Bremen/D

P-ls-027 Improvement of Measurement Precision of SPME-GC/MS Petermination of 355Tributyltin Using Isotope Pilution CalibrationBancon-Montionv, C. Ottawa/CPN. Maxwell, P., Ottawa/CPN, Yang, L,Ottawa/CPN, Mester, Z., Ottawa/CDN, Sturgeon, R. E. Ottawa/CDN

P-ls-028 Lead isotope ratios as tracers of lead pollution in a soil from a coal 356carbonization plantDiaz Somoano. M.. Oviedo/E. Suarez, S., Oviedo/E, Moinelo, S.R.,Oviedo/E, Garcia, R., Oviedo/E, Martinez-Tarazona, M.R., Oviedo/E

P-ls-029 Laser Mass-Spectrometric Isotope Analysis of Isotope Inriched Sabstances 357Kovalev. I.P.. Nizhnv Novgorod/RUS. Potapov A.M., NizhnyNovgorod/RUS, Suchkov A.I., Nizhny Novgorod/RUS

P-ls-030 Isotopic studies of Pb exposure at Valkenburg (100 AD): a comparative 358study using single collector and multiple collector sector field ICPMSKetterer, M.. Flaostaff/USA. Fischer, J., Johannesburg/ZA, Vanhaecke, F.,Ghent/B, Moens, L, Ghent/B, de Wolff, F., Leiden/NL, Smits, E.,Amsterdam/NL

P-ls-031 Monitoring the in vivo Methylation of Selenium using stable isotopes - 359Determination of Dimethylselenide in human breathKremer. P.. Bavreuth/D. Feldmann, J., Aberdeen/Scotland GB

P-ls-032 Determination of Ru, Pd, Re, Os, Ir, Pt, (Rh) concentrations in soils along 360Aus-trian motorways by isotope dilution ICP;MSFritsche. J.. Leoben/A. Meisel, T. Leoben/A

P-ls-033 Combined measurement uncertainty in isotope dilution MC-ICP-MS 367Fortunate G.. St.Gallen/CH. Wunderli, S., St.Gallen/CH

P-ls-034 Isotope ratio measurement of uranium in isotope standard reference 362materials and environmental samples by ICP-MSZoriv. M.. Juelich/D, Boulyga, S.F., Juelich/D, Izmer, A., Juelich/D,Ostapczuk, P., Juelich/D, Ketterer, M., Flagstaff/USA, Becker, J.S.,Juelich/D

P-ls-035 Determination of 1-129 in environmental samples by ISP-MS 363Izmer, A.V.. Juelich/D. Boulyga S.F., Juelich/P, Zoriy M. Juelich/D,Becker J.S., Juelich/D

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GDMS and GDAES Raum Zugspitze

P-GD-001 He - Ar Pulse Discharge in Thin-Walled Metallic Hollow Cathode for 364Effective Sputtering of Residue and Ions Transportation with TOF MSPetectionGaneev. A.. St. Petersburg/RUS. Potapov S., St.Petersburg/RUS, IsrailovE., St.Petersburg/RUS, Tverjanovich I., St.Petersburg/RUS, Voronov M.,St.Petersburg/RUS, Vergizova V. St.Petersburg/RUS

P-GP-002 Role of Thin-Walled Hollow Cathode Temperature for Residual and Solid- 365State Analysis in GP-TOF MS.Potapov. S.V.. St. Petersburq/RUS. Ganeev A.A., St.Petersburg/RUS,Voronov M.V., St.Petersburg/RUS, Tverjanovich I.A.,St.Petersburg/RUS,Israilov E.K., St.Petersburg/RUS, Vergizova V.S., St.Petersburg/RUS

P-GP-003 Erosion rate, and in-situ depth measurements for GP-OES 366Wilken. L. Presden/P. Hoffmann, V., Presden/P, Wetzig, K., Presden/P

P-GP-004 Development of a 6.78 MHz RF system for analytical glow discharges 367Dorka. R.. Dresden/D, Wilken, L, Dresden/D, Hoffmann, V., Dresden/D,Uhlemann, H.-J., Dresden/D, Wetzig, K., Dresden/D

P-GD-005 Development of a versatile GD ion source coupled to an on-axis TOF mass 368spectrometer for direct solid analysis.Pisonero. J.. Oviedo/E. Vazquez, M., Oviedo/E, Costa, J., Oviedo/E,Pereiro, R., Oviedo/E, Bordel, N., Oviedo/E, Sanz-Medel, A., Oviedo/E

P-GD-006 Effect of added hydrogen, nitrogen or oxygen on bulk and thin-film analysis 369using radiofrequency argon glow discharge optical emission spectrometry.Fernandez. B.. Oviedo/E. Bordel, N., Oviedo/E, Pereiro, R., Oviedo/E,Sanz-Medel, A., Oviedo/E

P-GD-007 GD-OES with the CCD detection: new results and new challenges 370Weiss, Z.. Plzen/CZ

P-GD-008 Characterization of Water and Water Resources in Israel by Long-Lived 377Radionuclides using ICP-MS in the frame of a bilateral cooperation projectPickhardt. C. Julich/P, Halicz, L. , Jerusalem/IL, Boulyga, S., Julich/P,Platzner, T., Jerusalem/IL, Gavrieli, I., Jerusalem/IL, Geyer, S., Leipzig/P,Becker, J.S., Julich/P

LA-ICP-MS and ETV-ICP-MS

P-LA-001

P-LA-002

Effects of laser defocusing and He gas on laser ablation inductivelycoupled plasma mass spectrometer (LA-ICP-MS) using emission signalsfrom a laser-induced plasma (LIP)Ohata, M.. Tokvo/J. Furuta N., Tokyo/J

Matrix-independent Quantification of Minerals (fluorite, apatite, rutile) withLA-ICP-MSLatkoczv. C. Zurich/CH, Gunther, P., Zurich/CH, Odegard, M.,Trondheim/N

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373

J^p-LA-003 Feasibility of LA-ICP-MS for forensic multi-element glass analysis: Round 374Robin Results within the NITE-CRIME European NetworkLatkoczv. C. Zurich/CH. Gunther, P., Zurich/CH, Almirall, J., Miami/USA,Becker, S., Wiesbaden/P, Pobney, A., Rijswijk/NL, Koons, R.,Quantico/USA, Watling, J., Perth/AUS, Zdanowicz, V., Springfield/USA

jpP-LA-004 Elemental fractionation studies on laser induced brass aerosols 375Kuhn. H.-R.. Zurich/CH. Gunther, P., Zurich/CH

[P-LA-005 A solid state 193 nm Nd:YAG for LA-ICP-MS 376Horn. I.. Zurich/CH. Gunther, P., Zurich/CH

IP-LA-006 Consideration of Geometry of Laser Beam and Crater Development for 377Refining of True Concentration Profile from Transient Data in LaserAblation ICP MSPlotnikov. A.. Dresden/D. Vogt, C, Hannover/D, Wetzig, K., Dresden/D

i P-LA-007 Optimisation of ICP-Parameters for Quantitative Analysis by LA-ICP-MS 378Ramseier. M.. Zurich/CH. Hattendorf, B., Zurich/CH, Gunther, D.,Zurich/CH

P-LA-008 Determination of trace elements in high-purity metals using laser ablation 379ICP-MS and instrumental neutron activation analysisBoulyqa. S.F.. Julich/P. Pickhardt C, Julich/P, Tsekhanovich, I.A.,Grenoble/F, Zhuk, I.V., Minsk/BY, Zauner, S., Mainz/P, Becker, J.S.Julich/P

P-LA-009 Analysis of whole blood and serum samples by tungsten coil electrothermal 380vaporization in combination with inductively coupled plasma time-of-flightmass spectrometryBinqs. N.H.. Leipzig/P. Stefanka, Zs., Budapest/H

P-LA-010 Elemental analysis of material in hard to sample places 387Aarts. S.. Eindhoven/NL. Smulders, J., Eindhoven/NL, Mank, A.J.G.,Eindhoven/NL

; P-LA-011 New matrix matched standards for forensic float glass analysis by LA-ICP- 382MSBecker. S.. Wiesbaden/D. Ducking, M., Wiesbaden/D, Stoecklein, W.,Wiesbaden/D »

f P-LA-012 Laser ablation ICP-MS in forensic glass analysis: Wavelength dependent 383changes of refractive index of glass fragments after laser ablationBecker. S., Wiesbaden/D. Ducking, M., Wiesbaden/D, Schmid, C,Wiesbaden/D, Stoecklein, W., Wiesbaden/D, Gunther, D., Zurich/CH,Latkoczy, Ch., Zurich/CH

|,P-LA-013 Manganese Distribution in Polystyrene Beads Prepared by 384Copolymerization with Cross-Linking Dentritic Salens Using Laser Ablation-Inductively Coupled Plasma-Mass Spectrometry.Hametner. K.. Zurich/CH. Sellner, H., Zurich/CH, Seebach, D., Zurich/CH,Gunther, D., Zurich/CH

LP-LA-014 Application of LA-ICP-MS in polar ice core studies 385Reinhardt. H.. Bremerhaven/D. Kriews, M., Bremerhaven/D, Miller, H.,Bremerhaven/D, Ludke, C,Berlin/D, Hoffmann, E., Berlin/D, Skole, J.,Berlin/D

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P-LA-015 Application of solid sampling-electrothermal vaporization-inductively 386coupled plasma-isotope dilution-mass spectrometry for the speciation ofmercury in biological and environmental samplesGelaude. I.. Ghent/B. Resano, M., Ghent/B, Vanhaecke, F., Ghent/B,Dams, R., Ghent/B, Moens, L, Ghent/B

P-LA-016 Analysis of size classified aerosol particles from an urban site in Berlin and 387from an remoete area in the high ArcticKriews. M.. Bremerhaven/D, Ludke C, Berlin/D, Hoffmann E, Berlin/D,Skole J, Berlin/D, Taubner K, Berlin/D

P-LA-017 Characterisation of functionally graded elements in Solid Oxide Fuel Cells 388using Laser Ablation Inductively Coupled Plasma Mass SpectrometryBleiner. P.. Pubendorf/CH, Ulrich, A., Pubendorf/CH, Holtappels, P.,Dubendorf/CH, Graule, T., Dubendorf/CH, Vonmont, H., Dubendorf/CH

P-LA-018 Investigation on the Factors Affecting In Situ Major and Trace Elements 389Analysis For Glass and Garnet by LA-ICPMSLuo. Y.. Hong Konq/PRC, Gao, S., Xian/PRC, Sun, M., Hong Kong/PRC

P-LA-019 Laser Ablation ICP-MS Analyses of Geological Materials 390Koenio. A.E.. Omaha/USA

P-LA-020 2-D-Mapping of trace elements in scrapie-infected and non-infected mice 397brain by laser ablation-ICP-MSFeldmann. J.. Old Aberdeen/GB, Lyon, D., Glasgow/UK Sekaran, C.N. OldAberdeen/UK

P-LA-021 Determonation of Rhenium and Osmium Concentrations in Molybdenite 392Using Laser Ablation Double Focusing Sector Field ICP-MSMalinovskiv. P.. Lulea/S, Rodishkin, I., Lulea/S, Axelsson, M., Lulea/S,Baxter, P. C , Lulea/S

P-LA-022 High Resolution Pistribution of Trace Elements in Scallop Shell by Laser 393Ablation Inductively Coupled Plasma Mass SpectrometryPechevran. C. Pau/F. Krupp, E., Pau/F, Amouroux, P., Pau/F, Chauvaud,L, Plouzane/F, Lorrain, A., Plouzane/F, Paulet, Y.M., Plouzane/F, Ponard,O.F.X., Pau/F

P-LA-023 Trace element analysis of synthetic mono-and polycrystalline CaF2 by 394ultraviolet laser ablation ICP-MS at 266 nm and 193 nmBolshov. M.. Troitzk/RUS. Koch, J., Portmund/P, Jakuboswki, N.,Portmund/P, Hergenroder, R., Portmund/P, Niemax, K., Dortmund/D,Gunther, D., Zurich/CH

Quality assurance, standards

P-Qu-002

P-Qu-003

An Unusual Systematic Behaviour of Detection Limits for Elements from55Cs to 73TaVerma. S.P.. Temixco/MEX. Santoyo, E., Temixco/MEX

An uncertainty budget for a combined analytical procedure by isotope-dilution ICP-MSMoser. J., Leoben/A. Meisel, T., Leoben/A, Wegscheider, W., Leoben/A

Raum Zugspitze

395

p-Qu-004 Reverse isotope dilution ICP-MS procedure applied to the certification of an 397isotopically enriched Cd candidate reference material: a case studyTresl. I.. Geel/B. Quetel, C. R., Geel/B, Taylor, P. D. P., Geel/B

'. p-Qu-005 Comparison of different procedures for metallic element determination in 398drying agents of paints:proposal of a reference method by ICP-OESCastillo, J.R.. Zaragoza/E. Lopez, A., Zaragoza/E, Cebrian, M.A.,Zaragoza/E

* P-Qu-006 On-line emulsions of organic samples and ICP-MS multielemental 399determinationCastillo. J.R.. Zaragoza/E. Jimenez, M.S.,Zaragoza/E, Velarte, R.,Zaragoza/E

P-Qu-007 Limits of Detection: Effect of Low Backgrounds and Short Data Integration 400TimesLonqerich, H.. St. Johns/CDN. Wegscheider, W., Leoben/A

p-Qu-008 Preparation of a Laboratory Reference Material (LRM) for Selenium 407SpeciationBodo, T.E., Budapest/H. Dernovics, M., Budapest/H, Stefanka, Z.,Budapest/H, Fodor, P., Budapest/H

P-Qu-009 An assessment of high accuracy methods for elemental analysis in a 402complex matrixWolff-Briche. C.S.J.. London/GB. Merson, S, London/GB

P-Qu-010 A new international measurement evaluation programme comparison, 403IMEP®-20, for heavy metals in tuna. Certification of Hg and Pb contents.Snell, J.P., Geel/B. Quetel, C. R., Geel/B, Aregbe, Y., Geel/B

P-Qu-011 Traceability of the Boron Determination of Isotopically Enriched Boron- 404Alloyed Steels by ICP-OESPrattes, K., Kapfenbero/A. Fauler, G., Graz/A , Moser, C, Graz/A ,Zischka, M., Graz/A

; P-Qu-012 Toward a common European measurement system: an EU funded 405information platform (www.trainmic.org) for training in Metrology inChemistryTaylor. P.D.P., Geel/B. Vassileva, E, Geel/B, Bulska, E, Warsaw/PL,Quetel, C.R., Geel/B

| P-Qu-013 Multi-Element Analysis by ICP-AES of Mineral Premixes Used in Food 406FortificationHammer. P.. Lausanne/CH. Perring, L., Lausanne/CH, Basic-Pvorzak, M.,Lausanne/CH

|P-Qu-014 Uncertainty budget for mass values determined by electronic balances 407New method for air buoyancy correctionWunderli. S.. St.Gallen/CH. Fortunato, G., St.Gallen/CH, Reichmuth, A.,Greifensee/CH, Richard, Ph., Wabern/CH

396

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