1D-1 PCB ANALYSIS DATA SHEETConc. Extract Volume: Injection Volume: SDG No: Lab Sample ID: Lab File...

Pace Analytical Services, Inc.

1D-1

AP17506

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:

Conc. Extract Volume:

Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:

CAS NO COMPOUND NAMECONCENTRATION

Q

Method:

Sulfur Cleanup:

Extraction:

SL-17-071112-006

11078

12070226

Polyurethane Foam

N/A

GC20F-1324-16

07/12/2012

07/12/2012

07/13/20121

N/A

Soxhlet Method (3540C)

5000 uL

1.0 uL

EPA Method TO-4A

YES

UG

GC Column: Phenomenex, Zebron ZB-1, 30 m, 0.25 mm ID, 0.25 µm

Client ID:

LRF ID: 12070226-09

Column 1 Information:

Injection Volume:

Lab File ID: GC20B-1313-16

1.0 uL

GC Column: Phenomenex, Zebron ZB-5, 30 m, 0.25 mm ID, 0.25 µmColumn 2 Information:

NumberColumn

PCB ANALYSIS DATA SHEET

12674-11-2 Aroclor 1016 0.100 U111104-28-2 Aroclor 1221 0.547 PB111141-16-5 Aroclor 1232 0.100 U153469-21-9 Aroclor 1242 0.497 PD112672-29-6 Aroclor 1248 0.100 U111097-69-1 Aroclor 1254 0.408 AF111096-82-5 Aroclor 1260 0.100 U1

Laboratory Qualifiers:AF-Aroclor 1254 is being reported as the best Aroclor match. The sample exhibits an altered PCB pattern.PB-Aroclor 1221 is being used to report an altered PCB pattern exhibited by the sample. Actual Aroclor 1221 is not present in the sample, but is reported to more accuratelyquantify PCB present in sample that has undergone environmental alteration.PD-Aroclor 1242 is being used to report an altered PCB pattern exhibited by the sample. Actual Aroclor 1242 is not present in the sample, but is reported to more accuratelyquantify PCB present in sample that has undergone environmental alteration.Note: There were several non-target peaks.U - Denotes analyte not detected at concentration greater than or equal to the Practical Quantitation Limit (PQL). PQLs are adjusted for sample weight/volume and dilutionfactors.

Lims Version : 5.0.6.6

FORM I-CLP-PCB

Print Date: 7/17/2012


1D-1

AP17507

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

BK-5-071112-008

11078

12070226

Polyurethane Foam

N/A

GC20F-1324-17

07/12/2012

07/12/2012

07/13/20121

N/A


5000 uL

1.0 uL

EPA Method TO-4A

YES

UG


Client ID:

LRF ID: 12070226-10


Injection Volume:


1.0 uL


NumberColumn


12674-11-2 Aroclor 1016 0.100 U111104-28-2 Aroclor 1221 0.244 PB111141-16-5 Aroclor 1232 0.100 U153469-21-9 Aroclor 1242 0.100 U112672-29-6 Aroclor 1248 0.100 U111097-69-1 Aroclor 1254 0.541 AF111096-82-5 Aroclor 1260 0.100 U1

Laboratory Qualifiers:AF-Aroclor 1254 is being reported as the best Aroclor match. The sample exhibits an altered PCB pattern.PB-Aroclor 1221 is being used to report an altered PCB pattern exhibited by the sample. Actual Aroclor 1221 is not present in the sample, but is reported to more accuratelyquantify PCB present in sample that has undergone environmental alteration.Note: There were several non-target peaks.U - Denotes analyte not detected at concentration greater than or equal to the Practical Quantitation Limit (PQL). PQLs are adjusted for sample weight/volume and dilutionfactors.


FORM I-CLP-PCB



1D-1

AP17508

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

FS-071112-062312-2

11078

12070226

Polyurethane Foam

N/A

GC20F-1324-18

07/12/2012

07/12/2012

07/13/20121

N/A


5000 uL

1.0 uL

EPA Method TO-4A

YES

UG


Client ID:

LRF ID: 12070226-11


Injection Volume:


1.0 uL


NumberColumn


12674-11-2 Aroclor 1016 0.100 U111104-28-2 Aroclor 1221 0.100 U111141-16-5 Aroclor 1232 0.100 U153469-21-9 Aroclor 1242 0.100 U112672-29-6 Aroclor 1248 0.100 U111097-69-1 Aroclor 1254 1.05111096-82-5 Aroclor 1260 0.100 U1

Laboratory Qualifiers:Note: There were few non-target peaks.U - Denotes analyte not detected at concentration greater than or equal to the Practical Quantitation Limit (PQL). PQLs are adjusted for sample weight/volume and dilutionfactors.


FORM I-CLP-PCB



1D-1

AP12679B

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

METHOD BLANK

11078

12060396

Solvent

N/AGC10F-415-33

06/22/2012

06/26/20121

N/A


5000 uL

1.0 uLEPA Method TO-4A

YES

UG

GC Column:Phenomenex, Zebron ZB-1MS, 20 m, 0.18 mm ID, 0.18 µm

Client ID:

LRF ID: PBLK-66


12674-11-2 Aroclor 1016 0.100 U

11104-28-2 Aroclor 1221 0.100 U

11141-16-5 Aroclor 1232 0.100 U

53469-21-9 Aroclor 1242 0.100 U

12672-29-6 Aroclor 1248 0.100 U

11097-69-1 Aroclor 1254 0.100 U

11096-82-5 Aroclor 1260 0.100 U

Laboratory Qualifiers:U - Denotes analyte not detected at concentration greater than or equal to the Practical Quantitation Limit (PQL). PQLs are adjusted for sample weight/volume and dilutionfactors.

Media has been certified for use.


FORM I-CLP-PCB



1D-1

AP13253B

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

METHOD BLANK

11078

12060435

Solvent

N/AGC10F-415-38

06/23/2012

06/26/20121

N/A


5000 uL


YES

UG


Client ID:

LRF ID: PBLK-88


12674-11-2 Aroclor 1016 0.100 U

11104-28-2 Aroclor 1221 0.100 U

11141-16-5 Aroclor 1232 0.100 U

53469-21-9 Aroclor 1242 0.100 U

12672-29-6 Aroclor 1248 0.100 U

11097-69-1 Aroclor 1254 0.100 U

11096-82-5 Aroclor 1260 0.100 U




FORM I-CLP-PCB



1D-1

AP17498B

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

METHOD BLANK

11078

12070226

Polyurethane Foam

N/AGC20F-1324-4

07/12/2012

07/13/20121

N/A


5000 uL


YES

UG

GC Column:Phenomenex, Zebron ZB-1, 30 m, 0.25 mm ID, 0.25 µm

Client ID:

LRF ID: PBLK-57


12674-11-2 Aroclor 1016 0.100 U

11104-28-2 Aroclor 1221 0.100 U

11141-16-5 Aroclor 1232 0.100 U

53469-21-9 Aroclor 1242 0.100 U

12672-29-6 Aroclor 1248 0.100 U

11097-69-1 Aroclor 1254 0.100 U

11096-82-5 Aroclor 1260 0.100 U



FORM I-CLP-PCB



1D-1

AP17498L

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

LAB CONTROL SPIKE

11078

12070226

Polyurethane Foam

N/AGC20F-1324-5

07/12/2012

07/13/20121

N/A


5000 uL


YES

UG


Client ID:

LRF ID: LCS-57


12674-11-2 Aroclor 1016 0.100 U

11104-28-2 Aroclor 1221 0.100 U

11141-16-5 Aroclor 1232 0.100 U

53469-21-9 Aroclor 1242 0.100 U

12672-29-6 Aroclor 1248 0.100 U

11097-69-1 Aroclor 1254 1.06

11096-82-5 Aroclor 1260 0.100 U



FORM I-CLP-PCB



1D-1

AP17498S

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

LAB CONTROL SPIKE DUPLICATE

11078

12070226

Polyurethane Foam

N/AGC20F-1324-6

07/12/2012

07/13/20121

N/A


5000 uL


YES

UG


Client ID:

LRF ID: LCSD-57


12674-11-2 Aroclor 1016 0.100 U

11104-28-2 Aroclor 1221 0.100 U

11141-16-5 Aroclor 1232 0.100 U

53469-21-9 Aroclor 1242 0.100 U

12672-29-6 Aroclor 1248 0.100 U

11097-69-1 Aroclor 1254 1.05

11096-82-5 Aroclor 1260 0.100 U



FORM I-CLP-PCB


Phenomenex, Zebron ZB-1MS, 20 m, 0.18 mm ID, 0.18 µm

Phenomenex, Zebron ZB-5, 20 m, 0.18 mm ID, 0.18 µm

SURR 1 (Col 1)

LRF ID

SURR 1

Laboratory Name:Pace Analytical Services, Inc. SDG: 12060435

GC Column (1):

GC Column (2):

TOTAL

% REC # OUT

2F-1PCB SURROGATE RECOVERY

FILE ID

ELAP ID No: 11078

LABSAMPLE ID

(Col 1)SURR 2

% REC #

SURR 2 (Col 2) (Col 2)

% REC # % REC #

LAB OTHER(1)

OTHER(2)

PBLK-88 86.6 95.0 0GC10F-415-38AP13253B

PBLK-88 87.1 95.5 0GC10B-388-38AP13253B

12060435-01 99.7 104 0GC10F-415-39AP13253

12060435-01 98.4 105 0GC10B-388-39AP13253

12060435-02 94.8 102 0GC10F-415-41AP13254

12060435-02 93.9 99.3 0GC10B-388-41AP13254

12060435-03 89.1 101 0GC10F-415-42AP13255

12060435-03 89.8 103 0GC10B-388-42AP13255

Form II-CLP-PCB(PACE)Lims Version : 5.0.6.6

Advisory QC Limits.

# Column to be used to flag recovery values* Values outside of QC limitsD Surrogate diluted out

SURR1 = TETRACHLORO-META-XYLENE

SURR2 = DECACHLOROBIPHENYL (60.0-120)

(60.0-120)




SURR 1 (Col 1)

LRF ID

SURR 1


GC Column (1):

GC Column (2):

TOTAL

% REC # OUT


FILE ID

ELAP ID No: 11078

LABSAMPLE ID

(Col 1)SURR 2

% REC #


% REC # % REC #

LAB OTHER(1)

OTHER(2)

PBLK-66 86.8 94.9 0GC10F-415-33AP12679B

PBLK-66 86.0 95.7 0GC10B-388-33AP12679B

12060396-01 90.8 100 0GC10F-415-34AP12679

12060396-01 93.1 100 0GC10B-388-34AP12679

12060396-02 90.8 99.9 0GC10F-415-35AP12680

12060396-02 93.0 100 0GC10B-388-35AP12680

12060396-03 88.2 95.1 0GC10F-415-36AP12681

12060396-03 88.2 95.2 0GC10B-388-36AP12681

12060396-04 88.9 98.5 0GC10F-415-37AP12682

12060396-04 90.1 99.8 0GC10B-388-37AP12682


Advisory QC Limits.




(60.0-120)




SURR 1 (Col 1)

LRF ID

SURR 1


GC Column (1):

GC Column (2):

TOTAL

% REC # OUT


FILE ID

ELAP ID No: 11078

LABSAMPLE ID

(Col 1)SURR 2

% REC #


% REC # % REC #

LAB OTHER(1)

OTHER(2)

PBLK-72 83.9 96.9 0GC20F-1325-60AP17981B

PBLK-72 87.6 99.6 0GC20B-1314-60AP17981B

LCS-72 84.3 98.3 0GC20F-1325-61AP17981L

LCS-72 89.9 103 0GC20B-1314-61AP17981L

LCSD-72 82.3 96.3 0GC20F-1325-62AP17981S

LCSD-72 84.9 98.7 0GC20B-1314-62AP17981S

12070263-01 82.9 95.1 0GC20F-1325-63AP17981

12070263-01 87.1 98.7 0GC20B-1314-63AP17981

12070263-02 97.9 97.8 0GC20F-1325-64AP17982

12070263-02 82.5 101 0GC20B-1314-64AP17982

12070263-03 102 91.9 0GC20F-1325-65AP17983

12070263-03 82.2 95.9 0GC20B-1314-65AP17983

12070263-04RR1 71.9 D 46.2 D 0GC20F-1329-4AP17984RR1

12070263-04RR1 70.4 D 73.1 D 0GC20B-1318-4AP17984RR1

12070263-05 111 94.2 0GC20F-1325-67AP17985

12070263-05 83.3 98.4 0GC20B-1314-67AP17985

12070263-06 93.9 90.2 0GC20F-1325-68AP17986

12070263-06 81.1 94.5 0GC20B-1314-68AP17986

12070263-07 104 96.5 0GC20F-1325-70AP17987

12070263-07 85.7 98.8 0GC20B-1314-70AP17987

12070263-08 88.5 90.6 0GC20F-1325-71AP17988

12070263-08 83.7 97.2 0GC20B-1314-71AP17988

12070263-09 109 95.1 0GC20F-1325-72AP17989

12070263-09 85.6 100 0GC20B-1314-72AP17989

12070263-10 90.2 91.3 0GC20F-1325-73AP17990

12070263-10 77.3 94.1 0GC20B-1314-73AP17990

12070263-11 93.6 92.4 0GC20F-1325-74AP17991

12070263-11 79.2 98.2 0GC20B-1314-74AP17991


Advisory QC Limits.




(60.0-120)




SURR 1 (Col 1)

LRF ID

SURR 1


GC Column (1):

GC Column (2):

TOTAL

% REC # OUT


FILE ID

ELAP ID No: 11078

LABSAMPLE ID

(Col 1)SURR 2

% REC #


% REC # % REC #

LAB OTHER(1)

OTHER(2)

12070263-12 80.1 94.0 0GC20F-1325-75AP17992

12070263-12 88.0 101 0GC20B-1314-75AP17992


Advisory QC Limits.




(60.0-120)


Laboratory Name:

Method Blank File ID:

ELAP ID No: SDG No:


11078 12070263

GC20F-1325-60LCS File ID: GC20F-1325-61

3F-2 LABORATORY CONTROL SPIKE (LCS) RECOVERY

LCS Lab ID: LCS-72 Blank Sample ID: PBLK-72

07/14/2012 23:36:00

AP17981LLCS ID:

LCS Inj Date:

Method Blank ID: AP17981B

Method Blank Inj Date: 07/14/2012 23:23:26

Polyurethane FoamLCS Matrix: Polyurethane FoamMethod Blank Matrix:

COMPOUNDSPIKEADDED

LCSCONCENTRATION

LCSPERCENT

RECOVERY #

QC LIMITS

RECOVERY

PERCENT(ug) (ug)

1

Aroclor 1254 1.00 1.06 106 70.0-130

# Column to be used to flag recovery values

* Values outside of QC limits

Spike Recovery: out of outside limits.0 1

QC Limits based upon laboratory defaults.1

COMMENTS:

Form III-CLP-PCB (PACE)Lims Version : 5.0.6.6

Laboratory Name:


ELAP ID No: SDG No:


11078 12070263

GC20B-1314-60LCS File ID: GC20B-1314-61



07/14/2012 23:36:05

AP17981LLCS ID:

LCS Inj Date:




COMPOUNDSPIKEADDED

LCSCONCENTRATION

LCSPERCENT

RECOVERY #

QC LIMITS

RECOVERY

PERCENT(ug) (ug)

1

Aroclor 1254 1.00 1.08 108 70.0-130





COMMENTS:

Form III-CLP-PCB (PACE)Lims Version : 5.0.6.6

Laboratory Name:

ELAP ID No: SDG No:


11078 12070263

LCS Lab File ID: GC20F-1325-61

3F-1 PCB LAB CONTROL SAMPLE (LCS) / LAB CONTROL SAMPLE DUPLICATE (LCSD) RECOVERY

LCS LRF ID: LCS-72

07/14/2012 23:36:00

AP17981LLCS Lab Sample ID:

LCS Sample Inj Date:

LCSD Lab File ID: GC20F-1325-62

LCSD LRF ID: LCSD-72

07/14/2012 23:48:35

AP17981SLCSD Lab Sample ID:

LCSD Sample Inj Date:

COMPOUND

SPIKEADDED

LCSCONCENTRATION

LCSPERCENT

RECOVERY #

QC LIMITS

RECOVERY

PERCENT(ug) (ug)

1

Aroclor 1254 1.00 1.06 106 (70.0-130)

COMPOUNDSPIKEADDED CONCENTRATION

LCSD LCSDPERCENT RPD #

QC LIMITS

RECRPD(ug) (ug)

1

RECOVERY #

Aroclor 1254 1.00 1.07 107 0.939 20 (70.0-130)





RPD: out of outside limits.0 1

COMMENTS:

Laboratory Name:

ELAP ID No: SDG No:


11078 12070263

LCS Lab File ID: GC20B-1314-61


LCS LRF ID: LCS-72

07/14/2012 23:36:05



LCSD Lab File ID: GC20B-1314-62


07/14/2012 23:48:39



COMPOUND

SPIKEADDED

LCSCONCENTRATION

LCSPERCENT

RECOVERY #

QC LIMITS

RECOVERY

PERCENT(ug) (ug)

1

Aroclor 1254 1.00 1.08 108 (70.0-130)



QC LIMITS

RECRPD(ug) (ug)

1

RECOVERY #

Aroclor 1254 1.00 1.06 106 1.87 20 (70.0-130)






COMMENTS:

PCB METHOD BLANK SUMMARY

Laboratory Name:

ELAP ID No:

Method Blank ID:

Blank Sample ID:

SDG No:

Date Analyzed:

Time Analyzed:

Instrument ID: Lab File ID:

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES AND QC:

CLIENT

SAMPLE ID

LAB

SAMPLE ID

LAB

FILE ID

DATE / TIME

ANALYZED

PBLK-88

GC Column (1):


11078

12060435

GC10F-415-38

AP13253B

06/26/2012

06:29:25


GC10F

4C-1

Date Extracted: 06/23/2012

Matrix: Solvent

Extraction Type: Soxhlet Method (3540C)

062312-0 AP13253 GC10F-415-39 06/26/2012 06:42:01

062312-1 AP13254 GC10F-415-41 06/26/2012 07:07:14

062312-2 AP13255 GC10F-415-42 06/26/2012 07:19:50

FORM IV-CLP-PCB(PACE)

Lims Version : 5.0.6.6Print date: 7/17/2012


Laboratory Name:

ELAP ID No:

Method Blank ID:

Blank Sample ID:

SDG No:

Date Analyzed:

Time Analyzed:



CLIENT

SAMPLE ID

LAB

SAMPLE ID

LAB

FILE ID

DATE / TIME

ANALYZED

PBLK-88

GC Column (1):


11078

12060435

GC10B-388-38

AP13253B

06/26/2012

06:29:29


GC10B

4C-1


Matrix: Solvent


062312-0 AP13253 GC10B-388-39 06/26/2012 06:42:05

062312-1 AP13254 GC10B-388-41 06/26/2012 07:07:18

062312-2 AP13255 GC10B-388-42 06/26/2012 07:19:54




Laboratory Name:

ELAP ID No:

Method Blank ID:

Blank Sample ID:

SDG No:

Date Analyzed:

Time Analyzed:



CLIENT

SAMPLE ID

LAB

SAMPLE ID

LAB

FILE ID

DATE / TIME

ANALYZED

PBLK-66

GC Column (1):


11078

12060396

GC10F-415-33

AP12679B

06/26/2012

05:26:24


GC10F

4C-1


Matrix: Solvent


VER PUF LOT# 062112-0 AP12679 GC10F-415-34 06/26/2012 05:39:01

VER PUF LOT# 062112-1 AP12680 GC10F-415-35 06/26/2012 05:51:37

VER PUF LOT# 062112-2 AP12681 GC10F-415-36 06/26/2012 06:04:13

VER PUF LOT# 062112-4 AP12682 GC10F-415-37 06/26/2012 06:16:49




Laboratory Name:

ELAP ID No:

Method Blank ID:

Blank Sample ID:

SDG No:

Date Analyzed:

Time Analyzed:



CLIENT

SAMPLE ID

LAB

SAMPLE ID

LAB

FILE ID

DATE / TIME

ANALYZED

PBLK-66

GC Column (1):


11078

12060396

GC10B-388-33

AP12679B

06/26/2012

05:26:28


GC10B

4C-1


Matrix: Solvent


VER PUF LOT# 062112-0 AP12679 GC10B-388-34 06/26/2012 05:39:05

VER PUF LOT# 062112-1 AP12680 GC10B-388-35 06/26/2012 05:51:41

VER PUF LOT# 062112-2 AP12681 GC10B-388-36 06/26/2012 06:04:17

VER PUF LOT# 062112-4 AP12682 GC10B-388-37 06/26/2012 06:16:53




1D-1

AP13253

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

VER PUF LOT# 062312-0

11078

12060435

Polyurethane Foam

N/A

GC10F-415-39

06/23/2012

06/23/2012

06/26/20121

N/A


5000 uL

1.0 uL

EPA Method TO-4A

YES

UG

GC Column: Phenomenex, Zebron ZB-1MS, 20 m, 0.18 mm ID, 0.18 µm

Client ID:

LRF ID: 12060435-01


Injection Volume:


1.0 uL


NumberColumn


12674-11-2 Aroclor 1016 0.100 U111104-28-2 Aroclor 1221 0.100 U111141-16-5 Aroclor 1232 0.100 U153469-21-9 Aroclor 1242 0.100 U112672-29-6 Aroclor 1248 0.100 U111097-69-1 Aroclor 1254 0.100 U111096-82-5 Aroclor 1260 0.100 U1

Laboratory Qualifiers:Blank ID: AP13253BU - Denotes analyte not detected at concentration greater than or equal to the Practical Quantitation Limit (PQL). PQLs are adjusted for sample weight/volume and dilutionfactors.



FORM I-CLP-PCB



1D-1

AP13254

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:


11078

12060435

Polyurethane Foam

N/A

GC10F-415-41

06/23/2012

06/23/2012

06/26/20121

N/A


5000 uL

1.0 uL

EPA Method TO-4A

YES

UG


Client ID:

LRF ID: 12060435-02


Injection Volume:


1.0 uL


NumberColumn






FORM I-CLP-PCB



1D-1

AP12682

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:


11078

12060396

Filter

N/A

GC10F-415-37

06/21/2012

06/22/2012

06/26/20121

N/A


5000 uL

1.0 uL

EPA Method TO-4A

YES

UG


Client ID:

LRF ID: 12060396-04


Injection Volume:


1.0 uL


NumberColumn






FORM I-CLP-PCB



1D-1

AP17981

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

BLK-071312-100

11078

12070263

Polyurethane Foam

N/A

GC20F-1325-63

07/13/2012

07/13/2012

07/15/20121

N/A


5000 uL

1.0 uL

EPA Method TO-4A

YES

UG


Client ID:

LRF ID: 12070263-01


Injection Volume:


1.0 uL


NumberColumn





FORM I-CLP-PCB



1D-1

AP17982

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

SL-4-071312-003

11078

12070263

Polyurethane Foam

N/A

GC20F-1325-64

07/13/2012

07/13/2012

07/15/20121

N/A


5000 uL

1.0 uL

EPA Method TO-4A

YES

UG


Client ID:

LRF ID: 12070263-02


Injection Volume:


1.0 uL


NumberColumn


12674-11-2 Aroclor 1016 0.100 U111104-28-2 Aroclor 1221 0.821 PB111141-16-5 Aroclor 1232 0.100 U153469-21-9 Aroclor 1242 0.100 U112672-29-6 Aroclor 1248 2.71 PE111097-69-1 Aroclor 1254 1.77 AF111096-82-5 Aroclor 1260 0.335 AG1

Laboratory Qualifiers:AF-Aroclor 1254 is being reported as the best Aroclor match. The sample exhibits an altered PCB pattern.AG-Aroclor 1260 is being reported as the best Aroclor match. The sample exhibits an altered PCB pattern.PB-Aroclor 1221 is being used to report an altered PCB pattern exhibited by the sample. Actual Aroclor 1221 is not present in the sample, but is reported to more accuratelyquantify PCB present in sample that has undergone environmental alteration.PE-Aroclor 1248 is being used to report an altered PCB pattern exhibited by the sample. Actual Aroclor 1248 is not present in the sample, but is reported to more accuratelyquantify PCB present in sample that has undergone environmental alteration.Note: There were several non-target peaks.U - Denotes analyte not detected at concentration greater than or equal to the Practical Quantitation Limit (PQL). PQLs are adjusted for sample weight/volume and dilutionfactors.


FORM I-CLP-PCB



1D-1

AP17983

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

SL-4CO-071312-005

11078

12070263

Polyurethane Foam

N/A

GC20F-1325-65

07/13/2012

07/13/2012

07/15/20121

N/A


5000 uL

1.0 uL

EPA Method TO-4A

YES

UG


Client ID:

LRF ID: 12070263-03


Injection Volume:


1.0 uL


NumberColumn





FORM I-CLP-PCB



1D-1

AP17984RR1

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

SL-5-071312-302

11078

12070263

Polyurethane Foam

N/A

GC20F-1329-4

07/13/2012

07/13/2012

07/18/20123

N/A


5000 uL

1.0 uL

EPA Method TO-4A

YES

UG


Client ID:

LRF ID: 12070263-04RR1


Injection Volume:


1.0 uL


NumberColumn





FORM I-CLP-PCB



1D-1

AP17985

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

SL-7-071312-012

11078

12070263

Polyurethane Foam

N/A

GC20F-1325-67

07/13/2012

07/13/2012

07/15/20121

N/A


5000 uL

1.0 uL

EPA Method TO-4A

YES

UG


Client ID:

LRF ID: 12070263-05


Injection Volume:


1.0 uL


NumberColumn





FORM I-CLP-PCB



1D-1

AP17986

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

SL-11-071312-004

11078

12070263

Polyurethane Foam

N/A

GC20F-1325-68

07/13/2012

07/13/2012

07/15/20121

N/A


5000 uL

1.0 uL

EPA Method TO-4A

YES

UG


Client ID:

LRF ID: 12070263-06


Injection Volume:


1.0 uL


NumberColumn





FORM I-CLP-PCB



1D-1

AP17987

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

SL-13-071312-002

11078

12070263

Polyurethane Foam

N/A

GC20F-1325-70

07/13/2012

07/13/2012

07/15/20121

N/A


5000 uL

1.0 uL

EPA Method TO-4A

YES

UG


Client ID:

LRF ID: 12070263-07


Injection Volume:


1.0 uL


NumberColumn





FORM I-CLP-PCB



1D-1

AP17988

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

SL-15-071312-010

11078

12070263

Polyurethane Foam

N/A

GC20F-1325-71

07/13/2012

07/13/2012

07/15/20121

N/A


5000 uL

1.0 uL

EPA Method TO-4A

YES

UG


Client ID:

LRF ID: 12070263-08


Injection Volume:


1.0 uL


NumberColumn





FORM I-CLP-PCB



1D-1

AP17989

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

SL-16-071312-009

11078

12070263

Polyurethane Foam

N/A

GC20F-1325-72

07/13/2012

07/13/2012

07/15/20121

N/A


5000 uL

1.0 uL

EPA Method TO-4A

YES

UG


Client ID:

LRF ID: 12070263-09


Injection Volume:


1.0 uL


NumberColumn





FORM I-CLP-PCB



1D-1

AP17990

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

SL-17-071312-006

11078

12070263

Polyurethane Foam

N/A

GC20F-1325-73

07/13/2012

07/13/2012

07/15/20121

N/A


5000 uL

1.0 uL

EPA Method TO-4A

YES

UG


Client ID:

LRF ID: 12070263-10


Injection Volume:


1.0 uL


NumberColumn


12674-11-2 Aroclor 1016 0.100 U111104-28-2 Aroclor 1221 0.699 PB111141-16-5 Aroclor 1232 0.100 U153469-21-9 Aroclor 1242 0.100 U112672-29-6 Aroclor 1248 0.625 PE111097-69-1 Aroclor 1254 0.414 AF111096-82-5 Aroclor 1260 0.100 U1

Laboratory Qualifiers:AF-Aroclor 1254 is being reported as the best Aroclor match. The sample exhibits an altered PCB pattern.PB-Aroclor 1221 is being used to report an altered PCB pattern exhibited by the sample. Actual Aroclor 1221 is not present in the sample, but is reported to more accuratelyquantify PCB present in sample that has undergone environmental alteration.PE-Aroclor 1248 is being used to report an altered PCB pattern exhibited by the sample. Actual Aroclor 1248 is not present in the sample, but is reported to more accuratelyquantify PCB present in sample that has undergone environmental alteration.Note: There were several non-target peaks.U - Denotes analyte not detected at concentration greater than or equal to the Practical Quantitation Limit (PQL). PQLs are adjusted for sample weight/volume and dilutionfactors.


FORM I-CLP-PCB



1D-1

AP17991

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

BK-5-071312-008

11078

12070263

Polyurethane Foam

N/A

GC20F-1325-74

07/13/2012

07/13/2012

07/15/20121

N/A


5000 uL

1.0 uL

EPA Method TO-4A

YES

UG


Client ID:

LRF ID: 12070263-11


Injection Volume:


1.0 uL


NumberColumn


12674-11-2 Aroclor 1016 0.100 U111104-28-2 Aroclor 1221 0.458 PB,P111141-16-5 Aroclor 1232 0.100 U153469-21-9 Aroclor 1242 0.100 U112672-29-6 Aroclor 1248 0.350 PE,P111097-69-1 Aroclor 1254 0.708 AF111096-82-5 Aroclor 1260 0.115 AG1

Laboratory Qualifiers:AF-Aroclor 1254 is being reported as the best Aroclor match. The sample exhibits an altered PCB pattern.AG-Aroclor 1260 is being reported as the best Aroclor match. The sample exhibits an altered PCB pattern.PB-Aroclor 1221 is being used to report an altered PCB pattern exhibited by the sample. Actual Aroclor 1221 is not present in the sample, but is reported to more accuratelyquantify PCB present in sample that has undergone environmental alteration.PE-Aroclor 1248 is being used to report an altered PCB pattern exhibited by the sample. Actual Aroclor 1248 is not present in the sample, but is reported to more accuratelyquantify PCB present in sample that has undergone environmental alteration.Note: There were several non-target peaks.U - Denotes analyte not detected at concentration greater than or equal to the Practical Quantitation Limit (PQL). PQLs are adjusted for sample weight/volume and dilutionfactors.P - Indicates percent difference (PD) between primary and secondary GC column analysis exceeds 40%.


FORM I-CLP-PCB



1D-1

AP17992

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

FS-071312-062312-2

11078

12070263

Polyurethane Foam

N/A

GC20F-1325-75

07/13/2012

07/13/2012

07/15/20121

N/A


5000 uL

1.0 uL

EPA Method TO-4A

YES

UG


Client ID:

LRF ID: 12070263-12


Injection Volume:


1.0 uL


NumberColumn


12674-11-2 Aroclor 1016 0.100 U111104-28-2 Aroclor 1221 0.100 U111141-16-5 Aroclor 1232 0.100 U153469-21-9 Aroclor 1242 0.100 U112672-29-6 Aroclor 1248 0.100 U111097-69-1 Aroclor 1254 1.04111096-82-5 Aroclor 1260 0.100 U1



FORM I-CLP-PCB



1D-1

AP13253B

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

METHOD BLANK

11078

12060435

Solvent

N/AGC10B-388-38

06/23/2012

06/26/20121

N/A


5000 uL


YES

UG


Client ID:

LRF ID: PBLK-88


12674-11-2 Aroclor 1016 0.100 U

11104-28-2 Aroclor 1221 0.100 U

11141-16-5 Aroclor 1232 0.100 U

53469-21-9 Aroclor 1242 0.100 U

12672-29-6 Aroclor 1248 0.100 U

11097-69-1 Aroclor 1254 0.100 U

11096-82-5 Aroclor 1260 0.100 U




FORM I-CLP-PCB



1D-1

AP13253B

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

METHOD BLANK

11078

12060435

Solvent

N/AGC10F-415-38

06/23/2012

06/26/20121

N/A


5000 uL


YES

UG


Client ID:

LRF ID: PBLK-88


12674-11-2 Aroclor 1016 0.100 U

11104-28-2 Aroclor 1221 0.100 U

11141-16-5 Aroclor 1232 0.100 U

53469-21-9 Aroclor 1242 0.100 U

12672-29-6 Aroclor 1248 0.100 U

11097-69-1 Aroclor 1254 0.100 U

11096-82-5 Aroclor 1260 0.100 U




FORM I-CLP-PCB



1D-1

AP12679B

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

METHOD BLANK

11078

12060396

Solvent

N/AGC10B-388-33

06/22/2012

06/26/20121

N/A


5000 uL


YES

UG


Client ID:

LRF ID: PBLK-66


12674-11-2 Aroclor 1016 0.100 U

11104-28-2 Aroclor 1221 0.100 U

11141-16-5 Aroclor 1232 0.100 U

53469-21-9 Aroclor 1242 0.100 U

12672-29-6 Aroclor 1248 0.100 U

11097-69-1 Aroclor 1254 0.100 U

11096-82-5 Aroclor 1260 0.100 U




FORM I-CLP-PCB



1D-1

AP12679B

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

METHOD BLANK

11078

12060396

Solvent

N/AGC10F-415-33

06/22/2012

06/26/20121

N/A


5000 uL


YES

UG


Client ID:

LRF ID: PBLK-66


12674-11-2 Aroclor 1016 0.100 U

11104-28-2 Aroclor 1221 0.100 U

11141-16-5 Aroclor 1232 0.100 U

53469-21-9 Aroclor 1242 0.100 U

12672-29-6 Aroclor 1248 0.100 U

11097-69-1 Aroclor 1254 0.100 U

11096-82-5 Aroclor 1260 0.100 U




FORM I-CLP-PCB



1D-1

AP17981B

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

METHOD BLANK

11078

12070263

Polyurethane Foam

N/AGC20F-1325-60

07/13/2012

07/14/20121

N/A


5000 uL


YES

UG


Client ID:

LRF ID: PBLK-72


12674-11-2 Aroclor 1016 0.100 U

11104-28-2 Aroclor 1221 0.100 U

11141-16-5 Aroclor 1232 0.100 U

53469-21-9 Aroclor 1242 0.100 U

12672-29-6 Aroclor 1248 0.100 U

11097-69-1 Aroclor 1254 0.100 U

11096-82-5 Aroclor 1260 0.100 U



FORM I-CLP-PCB



1D-1

AP17981B

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

METHOD BLANK

11078

12070263

Polyurethane Foam

N/AGC20B-1314-60

07/13/2012

07/14/20121

N/A


5000 uL


YES

UG


Client ID:

LRF ID: PBLK-72


12674-11-2 Aroclor 1016 0.100 U

11104-28-2 Aroclor 1221 0.100 U

11141-16-5 Aroclor 1232 0.100 U

53469-21-9 Aroclor 1242 0.100 U

12672-29-6 Aroclor 1248 0.100 U

11097-69-1 Aroclor 1254 0.100 U

11096-82-5 Aroclor 1260 0.100 U



FORM I-CLP-PCB



1D-1

AP17981L

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

LAB CONTROL SPIKE

11078

12070263

Polyurethane Foam

N/AGC20F-1325-61

07/13/2012

07/14/20121

N/A


5000 uL


YES

UG


Client ID:

LRF ID: LCS-72


12674-11-2 Aroclor 1016 0.100 U

11104-28-2 Aroclor 1221 0.100 U

11141-16-5 Aroclor 1232 0.100 U

53469-21-9 Aroclor 1242 0.100 U

12672-29-6 Aroclor 1248 0.100 U

11097-69-1 Aroclor 1254 1.06

11096-82-5 Aroclor 1260 0.100 U



FORM I-CLP-PCB



1D-1

AP17981L

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:

LAB CONTROL SPIKE

11078

12070263

Polyurethane Foam

N/AGC20B-1314-61

07/13/2012

07/14/20121

N/A


5000 uL


YES

UG


Client ID:

LRF ID: LCS-72


12674-11-2 Aroclor 1016 0.100 U

11104-28-2 Aroclor 1221 0.100 U

11141-16-5 Aroclor 1232 0.100 U

53469-21-9 Aroclor 1242 0.100 U

12672-29-6 Aroclor 1248 0.100 U

11097-69-1 Aroclor 1254 1.08

11096-82-5 Aroclor 1260 0.100 U



FORM I-CLP-PCB



1D-1

AP17981S

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:


11078

12070263

Polyurethane Foam

N/AGC20F-1325-62

07/13/2012

07/14/20121

N/A


5000 uL


YES

UG


Client ID:

LRF ID: LCSD-72


12674-11-2 Aroclor 1016 0.100 U

11104-28-2 Aroclor 1221 0.100 U

11141-16-5 Aroclor 1232 0.100 U

53469-21-9 Aroclor 1242 0.100 U

12672-29-6 Aroclor 1248 0.100 U

11097-69-1 Aroclor 1254 1.07

11096-82-5 Aroclor 1260 0.100 U



FORM I-CLP-PCB



1D-1

AP17981S

Laboratory Name:

ELAP ID No:

Matrix:

Sample wt(Dry)/vol:

Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:

Date Extracted:

Date Analyzed:

Dilution Factor:


Q

Method:

Sulfur Cleanup:

Extraction:


11078

12070263

Polyurethane Foam

N/AGC20B-1314-62

07/13/2012

07/14/20121

N/A


5000 uL


YES

UG


Client ID:

LRF ID: LCSD-72


12674-11-2 Aroclor 1016 0.100 U

11104-28-2 Aroclor 1221 0.100 U

11141-16-5 Aroclor 1232 0.100 U

53469-21-9 Aroclor 1242 0.100 U

12672-29-6 Aroclor 1248 0.100 U

11097-69-1 Aroclor 1254 1.06

11096-82-5 Aroclor 1260 0.100 U



FORM I-CLP-PCB




SURR 1 (Col 1)

LRF ID

SURR 1


GC Column (1):

GC Column (2):

TOTAL

% REC # OUT


FILE ID

ELAP ID No: 11078

LABSAMPLE ID

(Col 1)SURR 2

% REC #


% REC # % REC #

LAB OTHER(1)

OTHER(2)

PBLK-22 77.9 89.9 0GC20F-1341-15AP21637B

PBLK-22 81.9 93.0 0GC20B-1330-15AP21637B

12070585-01 78.1 84.3 0GC20F-1341-16AP21637

12070585-01 76.7 88.3 0GC20B-1330-16AP21637

12070585-02 76.2 91.2 0GC20F-1341-17AP21638

12070585-02 81.5 94.4 0GC20B-1330-17AP21638

12070585-03 77.3 93.6 0GC20F-1341-18AP21639

12070585-03 81.8 97.8 0GC20B-1330-18AP21639


Advisory QC Limits.


SURR1 = TETRACHLORO-META-XYLENESURR2 = DECACHLOROBIPHENYL (60.0-120)

(60.0-120)

Print Date: 8/20/2012Page 3 of 33



SURR 1 (Col 1)

LRF ID

SURR 1


GC Column (1):

GC Column (2):

TOTAL

% REC # OUT


FILE ID

ELAP ID No: 11078

LABSAMPLE ID

(Col 1)SURR 2

% REC #


% REC # % REC #

LAB OTHER(1)

OTHER(2)

PBLK-85 81.5 97.2 0GC20F-1356-11AP24448B

PBLK-85 88.7 95.7 0GC20B-1345-11AP24448B

LCS-85 90.5 99.3 0GC20F-1356-12AP24448L

LCS-85 91.8 97.3 0GC20B-1345-12AP24448L

LCSD-85 85.0 99.3 0GC20F-1356-13AP24448S

LCSD-85 87.1 95.8 0GC20B-1345-13AP24448S

12080295-01 86.5 98.1 0GC20F-1356-14AP24448

12080295-01 87.5 98.6 0GC20B-1345-14AP24448

12080295-02 106 97.2 0GC20F-1356-15AP24449

12080295-02 77.4 98.6 0GC20B-1345-15AP24449

12080295-03 108 101 0GC20F-1356-16AP24450

12080295-03 84.4 99.4 0GC20B-1345-16AP24450

12080295-04 112 101 0GC20F-1356-17AP24451

12080295-04 81.0 97.5 0GC20B-1345-17AP24451

12080295-05 114 96.8 0GC20F-1356-18AP24452

12080295-05 73.7 97.6 0GC20B-1345-18AP24452

12080295-06 107 102 0GC20F-1356-20AP24453

12080295-06 89.3 96.7 0GC20B-1345-20AP24453

12080295-07 114 102 0GC20F-1356-21AP24454

12080295-07 77.1 97.9 0GC20B-1345-21AP24454

12080295-08 110 101 0GC20F-1356-22AP24455

12080295-08 86.5 97.1 0GC20B-1345-22AP24455

12080295-09 116 97.8 0GC20F-1356-23AP24456

12080295-09 82.9 97.7 0GC20B-1345-23AP24456

12080295-10 82.4 95.0 0GC20F-1356-24AP24457

12080295-10 87.5 96.2 0GC20B-1345-24AP24457


Advisory QC Limits.


SURR1 = TETRACHLORO-META-XYLENESURR2 = DECACHLOROBIPHENYL (60.0-120)

(60.0-120)


Laboratory Name:


ELAP ID No: SDG No:


11078 12080295

GC20F-1356-11LCS File ID: GC20F-1356-12



08/16/2012 14:37:20

AP24448LLCS ID:

LCS Inj Date:




COMPOUNDSPIKEADDED

LCSCONCENTRATION

LCSPERCENT

RECOVERY #

QC LIMITS

RECOVERYPERCENT

(ug) (ug)

1

Aroclor 1254 1.00 1.08 108 70.0-130

# Column to be used to flag recovery values* Values outside of QC limits

Spike Recovery: out of outside limits.0 1QC Limits based upon laboratory defaults.1

COMMENTS:

Form III-CLP-PCB (PACE) Lims Version : 5.0.6.6Page 5 of 33

Laboratory Name:


ELAP ID No: SDG No:


11078 12080295

GC20B-1345-11LCS File ID: GC20B-1345-12



08/16/2012 14:37:25

AP24448LLCS ID:

LCS Inj Date:




COMPOUNDSPIKEADDED

LCSCONCENTRATION

LCSPERCENT

RECOVERY #

QC LIMITS

RECOVERYPERCENT

(ug) (ug)

1

Aroclor 1254 1.00 1.06 106 70.0-130


Spike Recovery: out of outside limits.0 1QC Limits based upon laboratory defaults.1

COMMENTS:

Form III-CLP-PCB (PACE) Lims Version : 5.0.6.6Page 6 of 33

Laboratory Name:

ELAP ID No: SDG No:


11078 12080295

LCS Lab File ID: GC20F-1356-12


LCS LRF ID: LCS-85

08/16/2012 14:37:20



LCSD Lab File ID: GC20F-1356-13


08/16/2012 14:49:54



COMPOUNDSPIKEADDED

LCSCONCENTRATION

LCSPERCENT

RECOVERY #

QC LIMITS

RECOVERYPERCENT

(ug) (ug)

1

Aroclor 1254 1.00 1.08 108 (70.0-130)



QC LIMITSRECRPD(ug) (ug)

1

RECOVERY #

Aroclor 1254 1.00 1.10 110 1.83 20 (70.0-130)





COMMENTS:

Page 7 of 33

Laboratory Name:

ELAP ID No: SDG No:


11078 12080295

LCS Lab File ID: GC20B-1345-12


LCS LRF ID: LCS-85

08/16/2012 14:37:25



LCSD Lab File ID: GC20B-1345-13


08/16/2012 14:49:59



COMPOUNDSPIKEADDED

LCSCONCENTRATION

LCSPERCENT

RECOVERY #

QC LIMITS

RECOVERYPERCENT

(ug) (ug)

1

Aroclor 1254 1.00 1.06 106 (70.0-130)



QC LIMITSRECRPD(ug) (ug)

1

RECOVERY #

Aroclor 1254 1.00 1.13 113 6.39 20 (70.0-130)





COMMENTS:

Page 8 of 33


Laboratory Name:

ELAP ID No:

Method Blank ID:

Blank Sample ID:

SDG No:

Date Analyzed:

Time Analyzed:



CLIENT

SAMPLE ID

LAB

SAMPLE ID

LAB

FILE ID

DATE / TIME

ANALYZED

PBLK-22

GC Column (1):


11078

12070585

GC20F-1341-15

AP21637B

07/30/2012

15:43:45


GC20F

4C-1


Matrix: Solvent


VER PUF LOT #072812-2 AP21637 GC20F-1341-16 07/30/2012 15:56:18 VER PUF LOT #072812-3 AP21638 GC20F-1341-17 07/30/2012 16:08:53 VER FILTER LOT #072812-4 AP21639 GC20F-1341-18 07/30/2012 16:21:29


Lims Version : 5.0.6.6Print date: 8/20/2012Page 9 of 33


Laboratory Name:

ELAP ID No:

Method Blank ID:

Blank Sample ID:

SDG No:

Date Analyzed:

Time Analyzed:



CLIENT

SAMPLE ID

LAB

SAMPLE ID

LAB

FILE ID

DATE / TIME

ANALYZED

PBLK-22

GC Column (1):


11078

12070585

GC20B-1330-15

AP21637B

07/30/2012

15:43:48


GC20B

4C-1


Matrix: Solvent


VER PUF LOT #072812-2 AP21637 GC20B-1330-16 07/30/2012 15:56:22 VER PUF LOT #072812-3 AP21638 GC20B-1330-17 07/30/2012 16:08:57 VER FILTER LOT #072812-4 AP21639 GC20B-1330-18 07/30/2012 16:21:33




Laboratory Name:

ELAP ID No:

Method Blank ID:

Blank Sample ID:

SDG No:

Date Analyzed:

Time Analyzed:



CLIENT

SAMPLE ID

LAB

SAMPLE ID

LAB

FILE ID

DATE / TIME

ANALYZED

PBLK-85

GC Column (1):


11078

12080295

GC20F-1356-11

AP24448B

08/16/2012

14:24:45


GC20F

4C-1


Matrix: Polyurethane Foam (PF4)


LCS-85(LAB CONTROL SPIKE) AP24448L GC20F-1356-12 08/16/2012 14:37:20 LCSD-85(LAB CONTROL SPIKE DUPLICATE) AP24448S GC20F-1356-13 08/16/2012 14:49:54 BLK-081512-100 AP24448 GC20F-1356-14 08/16/2012 15:02:30 SL-1-081512-010 AP24449 GC20F-1356-15 08/16/2012 15:15:05 SL-4-081512-003 AP24450 GC20F-1356-16 08/16/2012 15:27:39 SL-4CO-081512-006 AP24451 GC20F-1356-17 08/16/2012 15:40:15 SL-5-081512-002 AP24452 GC20F-1356-18 08/16/2012 15:52:50 SL-14-081512-005 AP24453 GC20F-1356-20 08/16/2012 16:18:00 SL-16-081512-004 AP24454 GC20F-1356-21 08/16/2012 16:30:34 SL-17-081512-009 AP24455 GC20F-1356-22 08/16/2012 16:43:09 BK-5-081512-008 AP24456 GC20F-1356-23 08/16/2012 16:55:44 FS-081512-072812-2 AP24457 GC20F-1356-24 08/16/2012 17:08:18




Laboratory Name:

ELAP ID No:

Method Blank ID:

Blank Sample ID:

SDG No:

Date Analyzed:

Time Analyzed:



CLIENT

SAMPLE ID

LAB

SAMPLE ID

LAB

FILE ID

DATE / TIME

ANALYZED

PBLK-85

GC Column (1):


11078

12080295

GC20B-1345-11

AP24448B

08/16/2012

14:24:50


GC20B

4C-1


Matrix: Polyurethane Foam (PF4)


LCS-85(LAB CONTROL SPIKE) AP24448L GC20B-1345-12 08/16/2012 14:37:25 LCSD-85(LAB CONTROL SPIKE DUPLICATE) AP24448S GC20B-1345-13 08/16/2012 14:49:59 BLK-081512-100 AP24448 GC20B-1345-14 08/16/2012 15:02:35 SL-1-081512-010 AP24449 GC20B-1345-15 08/16/2012 15:15:09 SL-4-081512-003 AP24450 GC20B-1345-16 08/16/2012 15:27:44 SL-4CO-081512-006 AP24451 GC20B-1345-17 08/16/2012 15:40:19 SL-5-081512-002 AP24452 GC20B-1345-18 08/16/2012 15:52:55 SL-14-081512-005 AP24453 GC20B-1345-20 08/16/2012 16:18:04 SL-16-081512-004 AP24454 GC20B-1345-21 08/16/2012 16:30:39 SL-17-081512-009 AP24455 GC20B-1345-22 08/16/2012 16:43:13 BK-5-081512-008 AP24456 GC20B-1345-23 08/16/2012 16:55:49 FS-081512-072812-2 AP24457 GC20B-1345-24 08/16/2012 17:08:23




1D-1

AP21637

Laboratory Name:ELAP ID No:Matrix:Sample wt(Dry)/vol:Percent Moisture:


Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:

Date Received:Date Extracted:Date Analyzed:Dilution Factor:


Q

Method:Sulfur Cleanup:

Extraction:

VER PUF LOT #072812-211078

12070585

Polyurethane FoamN/A

GC20F-1341-16

07/29/201207/29/201207/30/2012

1

N/ASoxhlet Method (3540C)

5000 uL

1.0 uL

EPA Method TO-4A

YES

UG


Client ID:LRF ID: 12070585-01


Injection Volume:Lab File ID: GC20B-1330-16

1.0 uLGC Column: Phenomenex, Zebron ZB-5, 30 m, 0.25 mm ID, 0.25 µmColumn 2 Information:

NumberColumn






FORM I-CLP-PCB



1D-1

AP21638



Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:



Q


Extraction:

VER PUF LOT #072812-311078

12070585

Polyurethane FoamN/A

GC20F-1341-17

07/29/201207/29/201207/30/2012

1


5000 uL

1.0 uL

EPA Method TO-4A

YES

UG





1.0 uLGC Column: Phenomenex, Zebron ZB-5, 30 m, 0.25 mm ID, 0.25 µmColumn 2 Information:

NumberColumn






FORM I-CLP-PCB



1D-1

AP21639



Injection Volume:

SDG No:

Lab Sample ID:

Lab File ID:



Q


Extraction:

VER FILTER LOT #072812-411078

12070585

FilterN/A

GC20F-1341-18

07/29/201207/29/201207/30/2012

1


5000 uL

1.0 uL

EPA Method TO-4A

YES

UG





1.0 uLGC Colu

1D-1 PCB ANALYSIS DATA SHEETConc. Extract Volume: Injection Volume: SDG No: Lab Sample ID: Lab File...

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