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Transcript of newtowncreek.infonewtowncreek.info/docs2/2 Remedial Investigation/Phase 1...
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ANALYTICAL REPORT
Job Number: 180-15932-1
Job Description: 120782-01.01 Newtown Creek
For:Anchor QEA LLC
720 Olive WaySuite 1900
Seattle, WA 98101
Attention: Delaney Peterson
_____________________________________________
Approved for release.Carrie L GamberCustomer Service Manager12/4/2012 9:14 AM
Carrie L GamberCustomer Service Manager
[email protected]/04/2012Revision: 1
The test results in this report meet all NELAP requirements for parameters for which accreditation is required oravailable. Any exceptions to the NELAP requirements are noted in this report. Pursuant to NELAP, this report may notbe reproduced, except in full, without the written approval of the laboratory. This report is confidential and is intendedfor the sole use of TestAmerica and its client. All questions regarding this report should be directed to the TestAmericaProject Manager or designee who has signed this report.
TestAmerica Laboratories, Inc.
TestAmerica Pittsburgh 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238
Tel (412) 963-7058 Fax (412) 963-2468 www.testamericainc.com
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mailto:[email protected]://www.testamericainc.comhttp://
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Table of ContentsCover Title Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Data Summaries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Report Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Manual Integration Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
Executive Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
Method / Analyst Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
Sample Datasheets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
QC Data Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
Data Qualifiers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26
Reagent Traceability . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
COAs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 85
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 117
Organic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 118
GC/MS Semi VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 118
Method 8270C . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 118Method 8270C QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 119Method 8270C Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 131Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 181
Method 8270C ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 181Method 8270C CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 243
Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 267
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Table of ContentsMethod 8270C Tune Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 267Method 8270C Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 279Method 8270C LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 288
Method 8270C Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 306Method 8270C Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 308
Inorganic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 325
General Chemistry Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 325
Gen Chem Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 326
Gen Chem MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 327
Gen Chem Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 329
Gen Chem Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 330
Shipping and Receiving Documents . . . . . . . . . . . . . . . . . . . . . . . . . . . 331
Client Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 332
Sample Receipt Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 334
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CASE NARRATIVE
Client: Anchor QEA LLC
Project: 120782-01.01 Newtown Creek
Report Number: 180-15932-1 Revised
NOTE: This report has been revised to include the corrected dilution factor for the semivolatile sample.
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The sample was received on 10/31/2012; the samples arrived in good condition, properly preserved and on ice. The temperature of the
cooler at receipt was 19.8º C.
SEMIVOLATILE ORGANIC COMPOUNDS (GC-MS)
As per client request, sample SED-20121017-1 was extracted and analyzed outside of holding time for 8270C semivolatile organic
compounds. The data are qualified and reported with this narrative.
Surrogate compounds were inadvertently omitted during the extraction process for sample SED-20121017-1 (180-15932-1). There was
insufficient sample remaining to perform re-extraction and/or re-analysis; therefore, the data have been reported and qualified. All QC
surrogate compounds recovered within acceptable limits.
GENERAL CHEMISTRY
Sample SED-20121017-1 (180-15932-1) was analyzed for percent solids in accordance with EPA SW846 3550C. The sample was
analyzed on 10/30/2012 and originally reported in job 180-15569-1.
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Lab Name: Job No.:
SDG No.:
GC/MS SEMI VOA MANUAL INTEGRATION SUMMARY
TestAmerica Pittsburgh 180-15932-1
Instrument ID: Analysis Batch Number:722 54021
Lab Sample ID: Client Sample ID:
Date Analyzed: Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
ICIS 180-54021/21
F11010C1.D11/01/12 09:09 GC Column: Rxi-5SilMS ID: 0.32(mm)
1,4-Dioxane Poor Chromatography PGH_BNA 11/02/12 08:510.98
Benzoic acid Poor Chromatography PGH_BNA 11/02/12 08:525.03
Lab Sample ID: Client Sample ID:
Date Analyzed: Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
IC 180-54021/22
F11010C3.D11/01/12 09:54 GC Column: Rxi-5SilMS ID: 0.32(mm)
Pyridine Poor Chromatography PGH_BNA 11/02/12 08:571.43
Methyl methanesulfonate Peak Not Found PGH_BNA 11/02/12 08:573.02
Isophorone Poor Chromatography PGH_BNA 11/02/12 08:574.87
Dimethyl phthalate Peak Integrated Incorrectly bungardf 11/01/12 23:516.38
2-Naphthylamine Peak Integrated Incorrectly bungardf 11/01/12 23:516.86
2,4,6-Tribromophenol Peak Integrated Incorrectly bungardf 11/01/12 23:527.19
Atrazine Peak Integrated Incorrectly bungardf 11/01/12 23:527.51
Benzidine Peak Integrated Incorrectly bungardf 11/01/12 23:518.81
3,3'-Dichlorobenzidine Peak Integrated Incorrectly bungardf 11/01/12 23:519.91
Bis(2-ethylhexyl) phthalate Peak Integrated Incorrectly bungardf 11/01/12 23:529.97
Di-n-octyl phthalate Peak Integrated Incorrectly bungardf 11/01/12 23:5210.59
Indeno[1,2,3-cd]pyrene Peak Integrated Incorrectly bungardf 11/01/12 23:5212.76
Lab Sample ID: Client Sample ID:
Date Analyzed: Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
IC 180-54021/24
F11010C5.D11/01/12 10:37 GC Column: Rxi-5SilMS ID: 0.32(mm)
Benzoic acid Poor Chromatography PGH_BNA 11/02/12 09:015.05
8270C LL
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Lab Name: Job No.:
SDG No.:
GC/MS SEMI VOA MANUAL INTEGRATION SUMMARY
TestAmerica Pittsburgh 180-15932-1
Instrument ID: Analysis Batch Number:722 54021
Lab Sample ID: Client Sample ID:
Date Analyzed: Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
IC 180-54021/25
F11010C6.D11/01/12 10:58 GC Column: Rxi-5SilMS ID: 0.32(mm)
Benzoic acid Peak Integrated Incorrectly bungardf 11/01/12 23:585.07
Lab Sample ID: Client Sample ID:
Date Analyzed: Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
IC 180-54021/26
F11010C7.D11/01/12 11:19 GC Column: Rxi-5SilMS ID: 0.32(mm)
Benzoic acid Peak Integrated Incorrectly bungardf 11/01/12 23:595.08
Lab Sample ID: Client Sample ID:
Date Analyzed: Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
IC 180-54021/27
F11010C8.D11/01/12 11:40 GC Column: Rxi-5SilMS ID: 0.32(mm)
Benzoic acid Peak Integrated Incorrectly bungardf 11/02/12 00:005.09
Lab Sample ID: Client Sample ID:
Date Analyzed: Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
IC 180-54021/28
F11010C9.D11/01/12 12:01 GC Column: Rxi-5SilMS ID: 0.32(mm)
Benzoic acid Peak Integrated Incorrectly bungardf 11/02/12 00:085.10
Benzo[b]fluoranthene Peak Integrated Incorrectly bungardf 11/02/12 00:0810.91
Lab Sample ID: Client Sample ID:
Date Analyzed: Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
ICV 180-54021/29
F11010V1.D11/01/12 12:22 GC Column: Rxi-5SilMS ID: 0.32(mm)
Benzoic acid Peak Integrated Incorrectly bungardf 11/02/12 00:105.06
8270C LL
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Lab Name: Job No.:
SDG No.:
GC/MS SEMI VOA MANUAL INTEGRATION SUMMARY
TestAmerica Pittsburgh 180-15932-1
Instrument ID: Analysis Batch Number:722 54476
Lab Sample ID: Client Sample ID:
Date Analyzed: Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
CCVIS 180-54476/2
F11070C2.D11/07/12 05:52 GC Column: Rxi-5SilMS ID: 0.32(mm)
1,4-Dioxane Peak Integrated Incorrectly bachas 11/07/12 08:240.93
Pyridine Peak Integrated Incorrectly bungardf 11/07/12 06:561.34
Benzyl alcohol Peak Integrated Incorrectly bungardf 11/07/12 06:564.33
Benzoic acid Peak Integrated Incorrectly bungardf 11/07/12 06:565.01
Pentachlorophenol Peak Integrated Incorrectly bungardf 11/07/12 06:577.53
Benzidine Peak Integrated Incorrectly bungardf 11/07/12 06:578.73
Lab Sample ID: Client Sample ID:
Date Analyzed: Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
LCS 180-54209/2-B
F1107003.D11/07/12 08:43 GC Column: Rxi-5SilMS ID: 0.32(mm)
1,4-Dioxane Peak Integrated Incorrectly bungardf 11/08/12 09:000.93
Pentachlorophenol Peak Integrated Incorrectly bachas 11/08/12 10:467.54
Lab Sample ID: Client Sample ID:
Date Analyzed: Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
LCSD 180-54209/3-B
F1107004.D11/07/12 09:04 GC Column: Rxi-5SilMS ID: 0.32(mm)
1,4-Dioxane Peak Integrated Incorrectly bungardf 11/08/12 09:020.93
Pentachlorophenol Peak Integrated Incorrectly bachas 11/08/12 10:477.55
8270C LL
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SAMPLE SUMMARY
Client: Anchor QEA LLC Job Number: 180-15932-1
Client Sample IDLab Sample ID Client Matrix Sampled Received
Date/Time Date/Time
180-15932-1 SED-20121017-1 Sediment 10/17/2012 1510 10/31/2012 0900
TestAmerica Pittsburgh Page 8 of 334
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EXECUTIVE SUMMARY - Detections
Client: Anchor QEA LLC Job Number: 180-15932-1
Analyte Result
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
Qualifier
180-15932-1 SED-20121017-1
260 ug/Kg 8270C LL74 J H1,1'-Biphenyl
260 ug/Kg 8270C LL170 J HAcetophenone
260 ug/Kg 8270C LL330 HBenzaldehyde
53 ug/Kg 8270C LL110 HAcenaphthene
53 ug/Kg 8270C LL490 HAcenaphthylene
53 ug/Kg 8270C LL490 HAnthracene
53 ug/Kg 8270C LL2500 HBenzo[a]anthracene
53 ug/Kg 8270C LL1900 HBenzo[a]pyrene
53 ug/Kg 8270C LL2900 HBenzo[b]fluoranthene
53 ug/Kg 8270C LL1500 HBenzo[g,h,i]perylene
530 ug/Kg 8270C LL10000 HBis(2-ethylhexyl) phthalate
260 ug/Kg 8270C LL280 HButyl benzyl phthalate
53 ug/Kg 8270C LL100 HCarbazole
260 ug/Kg 8270C LL170 J H4-Chloroaniline
53 ug/Kg 8270C LL2700 HChrysene
53 ug/Kg 8270C LL470 HDibenz(a,h)anthracene
260 ug/Kg 8270C LL150 J HDibenzofuran
260 ug/Kg 8270C LL220 J HDi-n-butyl phthalate
260 ug/Kg 8270C LL74 J HDiethyl phthalate
260 ug/Kg 8270C LL120 J HDi-n-octyl phthalate
53 ug/Kg 8270C LL4700 HFluoranthene
53 ug/Kg 8270C LL180 HFluorene
53 ug/Kg 8270C LL1400 HIndeno[1,2,3-cd]pyrene
260 ug/Kg 8270C LL26 J HIsophorone
53 ug/Kg 8270C LL230 H2-Methylnaphthalene
53 ug/Kg 8270C LL370 HNaphthalene
53 ug/Kg 8270C LL2300 HPhenanthrene
53 ug/Kg 8270C LL3400 HPyrene
260 ug/Kg 8270C LL46 J HMethylphenol, 3 & 4
53 ug/Kg 8270C LL73 HPhenol
0.10 % Moisture1.1Percent Moisture
TestAmerica Pittsburgh Page 9 of 334
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METHOD SUMMARY
Client: Anchor QEA LLC Job Number: 180-15932-1
Preparation MethodMethodLab LocationDescription
Matrix: Sediment
Semivolatile Organic Compounds by GCMS - Low Levels TAL PIT SW846 8270C LL
Automated Soxhlet Extraction (Low Level) TAL PIT SW846 3541
Gel-Permeation Cleanup TAL PIT SW846 3640A
Percent Moisture TAL PIT EPA Moisture
Lab References:
TAL PIT = TestAmerica Pittsburgh
Method References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
TestAmerica Pittsburgh Page 10 of 334
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METHOD / ANALYST SUMMARY
Client: Anchor QEA LLC Job Number: 180-15932-1
Method Analyst Analyst ID
Bacha, Sharon A SABSW846 8270C LL
Kunkle, Sarah SKEPA Moisture
TestAmerica Pittsburgh
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Analytical Data
Client: Anchor QEA LLC Job Number: 180-15932-1
Client Sample ID:
Lab Sample ID:
SED-20121017-1
Client Matrix: % Moisture: 1.1
180-15932-1
Sediment
Date Sampled: 10/17/2012 1510
Date Received: 10/31/2012 0900
8270C LL Semivolatile Organic Compounds by GCMS - Low Levels
Dilution:
11/05/2012 0739
11/07/2012 0925
5.0
8270C LL
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
F1107005.D
19.2 g
10.0 mL
2 uL
3541
722
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
180-54476
180-54209
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
74 J H 260241,1'-Biphenyl
170 J H 26022Acetophenone
260 U H 26026Atrazine
330 H 26040Benzaldehyde
1300 U H 1300200Caprolactam
110 H 535.1Acenaphthene
490 H 536.0Acenaphthylene
490 H 535.2Anthracene
2500 H 536.6Benzo[a]anthracene
1900 H 535.3Benzo[a]pyrene
2900 H 538.3Benzo[b]fluoranthene
1500 H 535.2Benzo[g,h,i]perylene
53 U H 5311Benzo[k]fluoranthene
53 U H 537.1Bis(2-chloroethyl)ether
260 U H 26017Bis(2-chloroethoxy)methane
10000 H 53043Bis(2-ethylhexyl) phthalate
260 U H 260234-Bromophenyl phenyl ether
280 H 26036Butyl benzyl phthalate
100 H 534.9Carbazole
170 J H 260214-Chloroaniline
53 U H 535.52-Chloronaphthalene
260 U H 260294-Chlorophenyl phenyl ether
2700 H 536.3Chrysene
470 H 535.9Dibenz(a,h)anthracene
150 J H 26026Dibenzofuran
220 J H 26033Di-n-butyl phthalate
260 U H 260283,3'-Dichlorobenzidine
74 J H 26029Diethyl phthalate
260 U H 26029Dimethyl phthalate
260 U H 260212,4-Dinitrotoluene
260 U H 260272,6-Dinitrotoluene
120 J H 26028Di-n-octyl phthalate
4700 H 535.6Fluoranthene
180 H 536.9Fluorene
53 U H 535.6Hexachlorobenzene
53 U H 535.9Hexachlorobutadiene
260 U H 26028Hexachlorocyclopentadiene
260 U H 26019Hexachloroethane
1400 H 535.4Indeno[1,2,3-cd]pyrene
26 J H 26020Isophorone
230 H 534.72-Methylnaphthalene
370 H 534.5Naphthalene
1300 U H 13001202-Nitroaniline
1300 U H 13001103-Nitroaniline
1300 U H 13001104-Nitroaniline
530 U H 53022Nitrobenzene
TestAmerica Pittsburgh Page 12 of 334
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Analytical Data
Client: Anchor QEA LLC Job Number: 180-15932-1
Client Sample ID:
Lab Sample ID:
SED-20121017-1
Client Matrix: % Moisture: 1.1
180-15932-1
Sediment
Date Sampled: 10/17/2012 1510
Date Received: 10/31/2012 0900
8270C LL Semivolatile Organic Compounds by GCMS - Low Levels
Dilution:
11/05/2012 0739
11/07/2012 0925
5.0
8270C LL
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
F1107005.D
19.2 g
10.0 mL
2 uL
3541
722
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
180-54476
180-54209
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
53 U H 536.2N-Nitrosodi-n-propylamine
260 U H 26024N-Nitrosodiphenylamine
2300 H 538.4Phenanthrene
3400 H 535.3Pyrene
260 U H 260244-Chloro-3-methylphenol
260 U H 260222-Chlorophenol
260 U H 260182-Methylphenol
46 J H 26026Methylphenol, 3 & 4
53 U H 535.32,4-Dichlorophenol
260 U H 260412,4-Dimethylphenol
1300 U H 13003102,4-Dinitrophenol
1300 U H 13001104,6-Dinitro-2-methylphenol
1300 U H 1300964-Nitrophenol
260 U H 260292-Nitrophenol
260 U H 26024Pentachlorophenol
73 H 536.2Phenol
260 U H 260282,4,5-Trichlorophenol
260 U H 260392,4,6-Trichlorophenol
53 U H 535.72,2'-oxybis[1-chloropropane]
260 U H 260172,3,4,6-Tetrachlorophenol
260 U H 260201,2,4,5-Tetrachlorobenzene
530 U H 530301,4-Dioxane
Surrogate %Rec Acceptance LimitsQualifier
0 21 - 116X2,4,6-Tribromophenol
0 28 - 108X2-Fluorobiphenyl
0 28 - 107X2-Fluorophenol
0 27 - 110XNitrobenzene-d5
0 30 - 112XPhenol-d5
0 21 - 130XTerphenyl-d14
TestAmerica Pittsburgh Page 13 of 334
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Analytical Data
Client: Anchor QEA LLC Job Number: 180-15932-1
Client Sample ID:
Lab Sample ID:
SED-20121017-1
Client Matrix: % Moisture: 1.1
180-15932-1
Sediment
Date Sampled: 10/17/2012 1510
Date Received: 10/31/2012 0900
8270C LL Semivolatile Organic Compounds by GCMS - Low Levels
Dilution:
11/05/2012 0739
11/07/2012 0925
5.0
8270C LL
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
F1107005.D
19.2 g
10.0 mL
2 uL
3541
722
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
180-54476
180-54209
Analysis Method:
Prep Method:
Tentatively Identified Compounds
QualifierEst. Result (ug/Kg)RTAnalyteCas Number
10Number TIC's Found:
2.29 2900 H JUnknown
2.69 2900 H JUnknown
106-46-7 4.23 51 J H1,4-Dichlorobenzene
120-82-1 5.15 27 J H1,2,4-Trichlorobenzene
949-41-7 8.08 1600 H J N1H-Cyclopropa[l]phenanthrene,1a,9b-dihyd
8.31 1400 H JUnknown
10.19 150 H JUnknown Hydrocarbon
10.33 120 H JUnknown
11.11 1200 H JUnknown
11.73 910 H JUnknown
TestAmerica Pittsburgh Page 14 of 334
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Analytical Data
Client: Anchor QEA LLC Job Number: 180-15932-1
General Chemistry
Client Sample ID:
Lab Sample ID:
SED-20121017-1
Client Matrix:
180-15932-1
Sediment
Date Sampled: 10/17/2012 1510
Date Received: 10/31/2012 0900
Analyte Result Qual Units MDL RL Dil Method
Percent Moisture 1.1 % 0.10 0.10 1.0 Moisture
DryWt Corrected: NAnalysis Date: 10/30/2012 1538Analysis Batch: 180-54503
TestAmerica Pittsburgh Page 15 of 334
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Quality Control Results
Job Number: 180-15932-1Client: Anchor QEA LLC
Surrogate Recovery Report
8270C LL Semivolatile Organic Compounds by GCMS - Low Levels
Client Matrix: Sediment
Lab Sample ID Client Sample ID
2FP PHL NBZ FBP TBP TPH
%Rec %Rec %Rec %Rec %Rec %Rec
180-15932-1 SED-20121017-1 0X 0X 0X 0X 0X 0X
MB 180-54209/1-B 84 84 74 68 78 83
LCS 180-54209/2-B 87 83 80 74 84 78
LCSD 180-54209/3-B 88 88 78 73 83 79
Surrogate Acceptance Limits
2FP = 2-Fluorophenol 28-107
PHL = Phenol-d5 30-112
NBZ = Nitrobenzene-d5 27-110
FBP = 2-Fluorobiphenyl 28-108
TBP = 2,4,6-Tribromophenol 21-116
TPH = Terphenyl-d14 21-130
TestAmerica Pittsburgh
Page 16 of 334
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Quality Control Results
Job Number: 180-15932-1Client: Anchor QEA LLC
SedimentClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 180-54209
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
F1107001.D
30.0 g
10.0 mLUnits: ug/Kg
Method: 8270C LL
Preparation: 3541
722MB 180-54209/1-B
Analysis Date: 11/07/2012 0634
Analysis Batch:
Prep Batch:
Leach Batch: N/A
180-54476
180-54209
Prep Date: Injection Volume: 2 uL
Leach Date:
11/05/2012 0739
N/A
Analyte RLMDLQualResult
33 U 333.01,1'-Biphenyl
33 U 332.7Acetophenone
33 U 333.2Atrazine
33 U 335.0Benzaldehyde
170 U 17025Caprolactam
6.7 U 6.70.64Acenaphthene
6.7 U 6.70.76Acenaphthylene
6.7 U 6.70.65Anthracene
6.7 U 6.70.84Benzo[a]anthracene
6.7 U 6.70.67Benzo[a]pyrene
6.7 U 6.71.0Benzo[b]fluoranthene
6.7 U 6.70.66Benzo[g,h,i]perylene
6.7 U 6.71.3Benzo[k]fluoranthene
6.7 U 6.70.90Bis(2-chloroethyl)ether
33 U 332.2Bis(2-chloroethoxy)methane
67 U 675.4Bis(2-ethylhexyl) phthalate
33 U 332.94-Bromophenyl phenyl ether
33 U 334.6Butyl benzyl phthalate
6.7 U 6.70.61Carbazole
33 U 332.74-Chloroaniline
6.7 U 6.70.702-Chloronaphthalene
33 U 333.74-Chlorophenyl phenyl ether
6.7 U 6.70.79Chrysene
6.7 U 6.70.74Dibenz(a,h)anthracene
33 U 333.3Dibenzofuran
33 U 334.2Di-n-butyl phthalate
33 U 333.53,3'-Dichlorobenzidine
33 U 333.6Diethyl phthalate
33 U 333.6Dimethyl phthalate
33 U 332.72,4-Dinitrotoluene
33 U 333.42,6-Dinitrotoluene
33 U 333.5Di-n-octyl phthalate
6.7 U 6.70.71Fluoranthene
6.7 U 6.70.88Fluorene
6.7 U 6.70.71Hexachlorobenzene
6.7 U 6.70.75Hexachlorobutadiene
33 U 333.6Hexachlorocyclopentadiene
33 U 332.4Hexachloroethane
6.7 U 6.70.69Indeno[1,2,3-cd]pyrene
33 U 332.5Isophorone
6.7 U 6.70.602-Methylnaphthalene
6.7 U 6.70.58Naphthalene
170 U 170152-Nitroaniline
170 U 170143-Nitroaniline
170 U 170144-Nitroaniline
TestAmerica Pittsburgh Page 17 of 334
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Quality Control Results
Job Number: 180-15932-1Client: Anchor QEA LLC
SedimentClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 180-54209
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
F1107001.D
30.0 g
10.0 mLUnits: ug/Kg
Method: 8270C LL
Preparation: 3541
722MB 180-54209/1-B
Analysis Date: 11/07/2012 0634
Analysis Batch:
Prep Batch:
Leach Batch: N/A
180-54476
180-54209
Prep Date: Injection Volume: 2 uL
Leach Date:
11/05/2012 0739
N/A
Analyte RLMDLQualResult
67 U 672.8Nitrobenzene
6.7 U 6.70.78N-Nitrosodi-n-propylamine
33 U 333.1N-Nitrosodiphenylamine
6.7 U 6.71.1Phenanthrene
6.7 U 6.70.67Pyrene
33 U 333.14-Chloro-3-methylphenol
33 U 332.72-Chlorophenol
33 U 332.32-Methylphenol
33 U 333.3Methylphenol, 3 & 4
6.7 U 6.70.672,4-Dichlorophenol
33 U 335.22,4-Dimethylphenol
170 U 170402,4-Dinitrophenol
170 U 170134,6-Dinitro-2-methylphenol
170 U 170124-Nitrophenol
33 U 333.72-Nitrophenol
33 U 333.0Pentachlorophenol
6.7 U 6.70.79Phenol
33 U 333.62,4,5-Trichlorophenol
33 U 335.02,4,6-Trichlorophenol
6.7 U 6.70.722,2'-oxybis[1-chloropropane]
33 U 332.12,3,4,6-Tetrachlorophenol
33 U 332.51,2,4,5-Tetrachlorobenzene
67 U 673.81,4-Dioxane
Surrogate % Rec Acceptance Limits
2,4,6-Tribromophenol 78 21 - 116
2-Fluorobiphenyl 68 28 - 108
2-Fluorophenol 84 28 - 107
Nitrobenzene-d5 74 27 - 110
Phenol-d5 84 30 - 112
Terphenyl-d14 83 21 - 130
Method Blank TICs- Batch: 180-54209
Cas Number Analyte RT Est. Result Qual
Tentatively Identified Compound None
TestAmerica Pittsburgh Page 18 of 334
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Quality Control Results
Job Number: 180-15932-1Client: Anchor QEA LLC
Dilution:
Dilution:
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 180-54209
1.0
1.0
Sediment
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Client Matrix: Sediment
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
ug/Kg
F1107003.D
30.0 g
10.0 mL
2 uL
F1107004.D
30.0 g
10.0 mL
2 uL
ug/Kg
Method: 8270C LL
Preparation: 3541
722
722
LCS 180-54209/2-B
LCSD 180-54209/3-B
Analysis Date:
Prep Date:
Leach Date:
11/07/2012 0843
11/05/2012 0739
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
180-54476
180-54209
N/A
Analysis Date:
Prep Date:
Leach Date:
11/07/2012 0904
11/05/2012 0739
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
180-54476
180-54209
N/A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
7474 30 - 150 0 401,1'-Biphenyl
7973 30 - 150 8 40Acetophenone
112115 30 - 150 3 40Atrazine
3735 30 - 150 6 40Benzaldehyde
9395 30 - 150 2 40Caprolactam
7475 42 - 104 2 34Acenaphthene
7980 43 - 117 0 36Acenaphthylene
7774 43 - 111 3 35Anthracene
7876 45 - 110 3 31Benzo[a]anthracene
7676 42 - 114 0 31Benzo[a]pyrene
6766 37 - 108 2 28Benzo[b]fluoranthene
7474 35 - 127 1 21Benzo[g,h,i]perylene
6971 39 - 115 3 42Benzo[k]fluoranthene
7975 40 - 100 5 33Bis(2-chloroethyl)ether
7575 42 - 103 0 35Bis(2-chloroethoxy)methane
7773 41 - 121 5 31Bis(2-ethylhexyl) phthalate
7172 43 - 111 1 204-Bromophenyl phenyl ether
7473 40 - 117 1 34Butyl benzyl phthalate
8383 42 - 114 0 35Carbazole
7979 33 - 102 0 284-Chloroaniline
7069 40 - 104 2 342-Chloronaphthalene
8273 42 - 111 12 374-Chlorophenyl phenyl ether
7979 44 - 108 0 31Chrysene
6868 34 - 131 0 32Dibenz(a,h)anthracene
7371 42 - 106 2 33Dibenzofuran
8281 44 - 120 2 34Di-n-butyl phthalate
8886 24 - 113 2 303,3'-Dichlorobenzidine
8876 44 - 113 14 32Diethyl phthalate
7373 44 - 111 0 34Dimethyl phthalate
8380 48 - 118 3 332,4-Dinitrotoluene
8079 47 - 119 2 302,6-Dinitrotoluene
7067 35 - 129 4 33Di-n-octyl phthalate
8784 40 - 118 3 23Fluoranthene
8476 43 - 110 10 37Fluorene
7169 42 - 110 3 29Hexachlorobenzene
7275 40 - 114 4 25Hexachlorobutadiene
TestAmerica Pittsburgh Page 19 of 334
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Quality Control Results
Job Number: 180-15932-1Client: Anchor QEA LLC
Dilution:
Dilution:
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 180-54209
1.0
1.0
Sediment
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Client Matrix: Sediment
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
ug/Kg
F1107003.D
30.0 g
10.0 mL
2 uL
F1107004.D
30.0 g
10.0 mL
2 uL
ug/Kg
Method: 8270C LL
Preparation: 3541
722
722
LCS 180-54209/2-B
LCSD 180-54209/3-B
Analysis Date:
Prep Date:
Leach Date:
11/07/2012 0843
11/05/2012 0739
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
180-54476
180-54209
N/A
Analysis Date:
Prep Date:
Leach Date:
11/07/2012 0904
11/05/2012 0739
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
180-54476
180-54209
N/A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
8181 10 - 150 0 33Hexachlorocyclopentadiene
8076 40 - 102 5 34Hexachloroethane
6970 34 - 130 1 30Indeno[1,2,3-cd]pyrene
7677 39 - 114 1 33Isophorone
7779 43 - 105 2 342-Methylnaphthalene
7979 42 - 104 0 25Naphthalene
7471 41 - 118 3 332-Nitroaniline
8281 38 - 116 2 273-Nitroaniline
9687 37 - 120 10 314-Nitroaniline
7273 40 - 109 2 31Nitrobenzene
7872 42 - 108 8 32N-Nitrosodi-n-propylamine
7676 41 - 110 1 32N-Nitrosodiphenylamine
7471 41 - 107 4 20Phenanthrene
7067 39 - 113 3 28Pyrene
8283 43 - 110 2 314-Chloro-3-methylphenol
8076 40 - 105 5 372-Chlorophenol
8077 41 - 104 4 372-Methylphenol
8581 43 - 107 5 36Methylphenol, 3 & 4
7779 44 - 110 2 272,4-Dichlorophenol
7072 39 - 106 3 422,4-Dimethylphenol
7180 19 - 140 12 432,4-Dinitrophenol
7880 28 - 130 2 354,6-Dinitro-2-methylphenol
8279 27 - 131 4 334-Nitrophenol
7980 45 - 112 1 302-Nitrophenol
8283 18 - 125 1 34Pentachlorophenol
7874 39 - 105 5 40Phenol
7474 42 - 110 0 352,4,5-Trichlorophenol
7168 43 - 111 4 362,4,6-Trichlorophenol
7670 37 - 105 8 312,2'-oxybis[1-chloropropane]
8186 43 - 108 7 362,3,4,6-Tetrachlorophenol
7371 30 - 125 2 251,2,4,5-Tetrachlorobenzene
6562 41 - 102 5 351,4-Dioxane
Surrogate LCS % Rec LCSD % Rec Acceptance Limits
2,4,6-Tribromophenol 84 83 21 - 116
2-Fluorobiphenyl 74 73 28 - 108
TestAmerica Pittsburgh Page 20 of 334
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Quality Control Results
Job Number: 180-15932-1Client: Anchor QEA LLC
Surrogate LCS % Rec LCSD % Rec Acceptance Limits
2-Fluorophenol 87 88 28 - 107
Nitrobenzene-d5 80 78 27 - 110
Phenol-d5 83 88 30 - 112
Terphenyl-d14 78 79 21 - 130
TestAmerica Pittsburgh Page 21 of 334
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Quality Control Results
Job Number: 180-15932-1Client: Anchor QEA LLC
Sediment
11/07/2012 0843
Dilution: Dilution:1.0 1.0
Client Matrix:
LCSD Lab Sample ID:
Client Matrix: Sediment
Laboratory Control/
Laboratory Duplicate Data Report - Batch: 180-54209
Method: 8270C LL
Preparation: 3541
Units: ug/KgLCS 180-54209/2-B LCSD 180-54209/3-BLCS Lab Sample ID:
Analysis Date:
Prep Date:
Leach Date:
11/05/2012 0739
Analysis Date:
Prep Date:
Leach Date:
11/07/2012 0904
11/05/2012 0739
N/AN/A
LCSD
Result/Qual
LCS
Result/Qual
LCSD Spike
Amount
LCS Spike
AmountAnalyte
246247333 3331,1'-Biphenyl
264243333 333Acetophenone
373383333 333Atrazine
124116333 333Benzaldehyde
308316333 333Caprolactam
246250333 333Acenaphthene
265266333 333Acenaphthylene
255248333 333Anthracene
259252333 333Benzo[a]anthracene
254254333 333Benzo[a]pyrene
223220333 333Benzo[b]fluoranthene
245247333 333Benzo[g,h,i]perylene
231238333 333Benzo[k]fluoranthene
262248333 333Bis(2-chloroethyl)ether
249250333 333Bis(2-chloroethoxy)methane
258245333 333Bis(2-ethylhexyl) phthalate
237239333 3334-Bromophenyl phenyl ether
246243333 333Butyl benzyl phthalate
277276333 333Carbazole
263263333 3334-Chloroaniline
235230333 3332-Chloronaphthalene
273244333 3334-Chlorophenyl phenyl ether
262263333 333Chrysene
227228333 333Dibenz(a,h)anthracene
242238333 333Dibenzofuran
273269333 333Di-n-butyl phthalate
293287333 3333,3'-Dichlorobenzidine
292253333 333Diethyl phthalate
243242333 333Dimethyl phthalate
276268333 3332,4-Dinitrotoluene
268262333 3332,6-Dinitrotoluene
232224333 333Di-n-octyl phthalate
290280333 333Fluoranthene
281253333 333Fluorene
237229333 333Hexachlorobenzene
239249333 333Hexachlorobutadiene
271271333 333Hexachlorocyclopentadiene
267253333 333Hexachloroethane
229232333 333Indeno[1,2,3-cd]pyrene
TestAmerica Pittsburgh Page 22 of 334
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Quality Control Results
Job Number: 180-15932-1Client: Anchor QEA LLC
Sediment
11/07/2012 0843
Dilution: Dilution:1.0 1.0
Client Matrix:
LCSD Lab Sample ID:
Client Matrix: Sediment
Laboratory Control/
Laboratory Duplicate Data Report - Batch: 180-54209
Method: 8270C LL
Preparation: 3541
Units: ug/KgLCS 180-54209/2-B LCSD 180-54209/3-BLCS Lab Sample ID:
Analysis Date:
Prep Date:
Leach Date:
11/05/2012 0739
Analysis Date:
Prep Date:
Leach Date:
11/07/2012 0904
11/05/2012 0739
N/AN/A
LCSD
Result/Qual
LCS
Result/Qual
LCSD Spike
Amount
LCS Spike
AmountAnalyte
255258333 333Isophorone
258263333 3332-Methylnaphthalene
262263333 333Naphthalene
245237333 3332-Nitroaniline
274269333 3333-Nitroaniline
321292333 3334-Nitroaniline
240244333 333Nitrobenzene
259240333 333N-Nitrosodi-n-propylamine
252254333 333N-Nitrosodiphenylamine
246235333 333Phenanthrene
232225333 333Pyrene
273277333 3334-Chloro-3-methylphenol
265253333 3332-Chlorophenol
267256333 3332-Methylphenol
568540667 667Methylphenol, 3 & 4
257262333 3332,4-Dichlorophenol
233239333 3332,4-Dimethylphenol
237267333 3332,4-Dinitrophenol
261266333 3334,6-Dinitro-2-methylphenol
274264333 3334-Nitrophenol
264266333 3332-Nitrophenol
274277333 333Pentachlorophenol
259247333 333Phenol
246247333 3332,4,5-Trichlorophenol
237228333 3332,4,6-Trichlorophenol
253234333 3332,2'-oxybis[1-chloropropane]
269287333 3332,3,4,6-Tetrachlorophenol
242238333 3331,2,4,5-Tetrachlorobenzene
217207333 3331,4-Dioxane
TestAmerica Pittsburgh Page 23 of 334
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DATA REPORTING QUALIFIERS
Client: Anchor QEA LLC Job Number: 180-15932-1
Lab Section Qualifier Description
GC/MS Semi VOA
Indicates an Estimated Value for TICsJ
Indicates the analyte was analyzed for but not detected.U
Result is less than the RL but greater than or equal to the MDL and the
concentration is an approximate value.
J
Sample was prepped or analyzed beyond the specified holding timeH
Surrogate is outside control limitsX
This flag indicates the presumptive evidence of a compound.N
TestAmerica Pittsburgh Page 24 of 334
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Quality Control Results
Client: Anchor QEA LLC Job Number: 180-15932-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
GC/MS Semi VOA
Prep Batch: 180-54209
Lab Control Sample Sediment 3541LCS 180-54209/2-B T
Lab Control Sample Duplicate Sediment 3541LCSD 180-54209/3-B T
Method Blank Sediment 3541MB 180-54209/1-B T
SedimentSED-20121017-1 3541180-15932-1 T
Analysis Batch:180-54476
Lab Control Sample Sediment 180-542098270C LLLCS 180-54209/2-B T
Lab Control Sample Duplicate Sediment 180-542098270C LLLCSD 180-54209/3-B T
Method Blank Sediment 180-542098270C LLMB 180-54209/1-B T
Sediment 180-54209SED-20121017-1 8270C LL180-15932-1 T
Report Basis
T = Total
General Chemistry
Analysis Batch:180-54503
SedimentSED-20121017-1 Moisture180-15932-1 T
Report Basis
T = Total
TestAmerica Pittsburgh
Page 25 of 334
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Quality Control Results
Client: Anchor QEA LLC Job Number: 180-15932-1
Laboratory Chronicle
10/31/2012 09:00
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: Received Date/Time:10/17/2012 15:10
180-15932-1 SED-20121017-1
P:3541 180-15932-A-1-B 180-54476 180-54209 11/05/2012 07:39 KGTAL PIT5
A:8270C LL 180-15932-A-1-B 180-54476 180-54209 11/07/2012 09:25 SABTAL PIT5
A:Moisture 180-15932-A-1 180-54503 10/30/2012 15:38 SKTAL PIT1
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: N/A Received Date/Time: N/A
MB N/A
P:3541 MB 180-54209/1-B 180-54476 180-54209 11/05/2012 07:39 KGTAL PIT1
A:8270C LL MB 180-54209/1-B 180-54476 180-54209 11/07/2012 06:34 SABTAL PIT1
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: N/A Received Date/Time: N/A
LCS N/A
P:3541 LCS 180-54209/2-B 180-54476 180-54209 11/05/2012 07:39 KGTAL PIT1
A:8270C LL LCS 180-54209/2-B 180-54476 180-54209 11/07/2012 08:43 SABTAL PIT1
Lab ID:
Method Bottle ID Run
Analysis
Batch Prep Batch
Date Prepared /
Analyzed Dil Lab Analyst
Client ID:
Sample Date/Time: N/A Received Date/Time: N/A
LCSD N/A
P:3541 LCSD 180-54209/3-B 180-54476 180-54209 11/05/2012 07:39 KGTAL PIT1
A:8270C LL LCSD 180-54209/3-B 180-54476 180-54209 11/07/2012 09:04 SABTAL PIT1
Lab References:TAL PIT = TestAmerica Pittsburgh
A = Analytical Method P = Prep Method TestAmerica Pittsburgh
Page 26 of 334
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
03/31/13 (Purchased Reagent) 1,1'-Biphenyl 200 ug/mLRestek, Lot A090885OPDODADNLSPKs_000041,2,4,5-Tetrachlorobenzene 200 ug/mL1,4-Dioxane 200 ug/mL2,6-Dichlorophenol 200 ug/mL2-Naphthylamine 200 ug/mL7,12-Dimethylbenz(a)anthracene 200 ug/mLAcetophenone 200 ug/mLBenzaldehyde 200 ug/mLBenzidine 200 ug/mLCaprolactam 200 ug/mLIndene 200 ug/mLMethyl methanesulfonate 200 ug/mLN-Nitrosopyrrolidine 200 ug/mL
07/31/13 (Purchased Reagent) 1,2,4-Trichlorobenzene 200 ug/mLSupelco, Lot LB93750OPHC8270SPKs_000271,2-Dichlorobenzene 200 ug/mL1,2-Dinitrobenzene 200 ug/mL1,2-Diphenylhydrazine 200 ug/mL1,3-Dichlorobenzene 200 ug/mL1,4-Dichlorobenzene 200 ug/mL1,4-Dinitrobenzene 200 ug/mL1-Methylnaphthalene 200 ug/mL2,2'-oxybis[1-chloropropane] 200 ug/mL2,3,4,6-Tetrachlorophenol 200 ug/mL2,3,5,6-Tetrachlorophenol 200 ug/mL2,4,5-Trichlorophenol 200 ug/mL2,4,6-Trichlorophenol 200 ug/mL2,4-Dichlorophenol 200 ug/mL2,4-Dimethylphenol 200 ug/mL2,4-Dinitrophenol 200 ug/mL2,4-Dinitrotoluene 200 ug/mL2,6-Dinitrotoluene 200 ug/mL2-Chloronaphthalene 200 ug/mL2-Chlorophenol 200 ug/mL2-Methylnaphthalene 200 ug/mL2-Methylphenol 200 ug/mL2-Nitroaniline 200 ug/mL2-Nitrophenol 200 ug/mL3 & 4 Methylphenol 400 ug/mL3,3'-Dichlorobenzidine 200 ug/mL3-Methylphenol 200 ug/mL3-Nitroaniline 200 ug/mL4,6-Dinitro-2-methylphenol 200 ug/mL4-Bromophenyl phenyl ether 200 ug/mL4-Chloro-3-methylphenol 200 ug/mL4-Chloroaniline 200 ug/mL4-Chlorophenyl phenyl ether 200 ug/mL4-Nitroaniline 200 ug/mL
Page 27 of 334
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
4-Nitrophenol 200 ug/mLAcenaphthene 200 ug/mLAcenaphthylene 200 ug/mLAniline 200 ug/mLAnthracene 200 ug/mLBenzo[a]anthracene 200 ug/mLBenzo[a]pyrene 200 ug/mLBenzo[b]fluoranthene 200 ug/mLBenzo[g,h,i]perylene 200 ug/mLBenzo[k]fluoranthene 200 ug/mLBenzoic acid 200 ug/mLBenzyl alcohol 200 ug/mLBis(2-chloroethoxy)methane 200 ug/mLBis(2-chloroethyl)ether 200 ug/mLBis(2-ethylhexyl) phthalate 200 ug/mLBis-2-ethylhexyl adipate 200 ug/mLButyl benzyl phthalate 200 ug/mLCarbazole 200 ug/mLChrysene 200 ug/mLDi-n-butyl phthalate 200 ug/mLDi-n-octyl phthalate 200 ug/mLDibenz(a,h)anthracene 200 ug/mLDibenzofuran 200 ug/mLDiethyl phthalate 200 ug/mLDimethyl phthalate 200 ug/mLFluoranthene 200 ug/mLFluorene 200 ug/mLHexachlorobenzene 200 ug/mLHexachlorobutadiene 200 ug/mLHexachlorocyclopentadiene 200 ug/mLHexachloroethane 200 ug/mLIndeno[1,2,3-cd]pyrene 200 ug/mLIsophorone 200 ug/mLMethyl Phenols,Total 600 ug/mLMethylphenol, 3 & 4 400 ug/mLN-Nitrosodi-n-propylamine 200 ug/mLN-Nitrosodimethylamine 200 ug/mLN-Nitrosodiphenylamine 200 ug/mLNaphthalene 200 ug/mLNitrobenzene 200 ug/mLPentachlorophenol 200 ug/mLPhenanthrene 200 ug/mLPhenol 200 ug/mLPyrene 200 ug/mLPyridine 200 ug/mLTotal Cresols 600 ug/mL
OPABSURRSPKs_00013 1,2-Dichlorobenzene-d4 200 ug/mL500 mL 100 mL06/19/13 10/19/12OPQL-8270SURi_00040 Methanol, Lot DG596
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
2,4,6-Tribromophenol 300 ug/mL2-Chlorophenol-d4 300 ug/mL2-Fluorobiphenyl 200 ug/mL2-Fluorophenol 300 ug/mLNitrobenzene-d5 200 ug/mLPhenol-d5 300 ug/mLTerphenyl-d14 200 ug/mL
05/31/15 (Purchased Reagent) 1,2-Dichlorobenzene-d4 1000 ug/mLSupelco, Lot LB92759.OPABSURRSPKs_000132,4,6-Tribromophenol 1500 ug/mL2-Chlorophenol-d4 1500 ug/mL2-Fluorobiphenyl 1000 ug/mL2-Fluorophenol 1500 ug/mLNitrobenzene-d5 1000 ug/mLPhenol-d5 1500 ug/mLTerphenyl-d14 1000 ug/mL
SVSS1245TCBs_00003 1,2,4,5-Tetrachlorobenzene 10 ug/mL1 mL 0.01 mL10/31/12 09/07/12SV2NDSOURCEi_00009 mecl2, Lot 4954471,4-Dioxane 10 ug/mLSVSS14DIOXANs_00001 0.01 mL2,6-Dichlorophenol 10 ug/mLSVSS26DCPs_00003 0.01 mL1-Methylnaphthalene 10 ug/mLSVSSADDONs_00001 0.005 mL2,3,4,6-Tetrachlorophenol 10 ug/mL2,3,5,6-Tetrachlorophenol 10 ug/mLMethyl methanesulfonate 10 ug/mL3,3'-Dichlorobenzidine 10 ug/mLSVSSBENZIDNs_00002 0.005 mL1,2,4-Trichlorobenzene 10 ug/mLSVSSCALIBMX1s_00003 0.01 mL1,2-Diphenylhydrazine 10 ug/mL2,2'-oxybis[1-chloropropane] 10 ug/mL2,4,5-Trichlorophenol 10 ug/mL2,4,6-Trichlorophenol 10 ug/mL2,4-Dichlorophenol 10 ug/mL2,4-Dimethylphenol 10 ug/mL2,4-Dinitrophenol 10 ug/mL2,4-Dinitrotoluene 10 ug/mL2,6-Dinitrotoluene 10 ug/mL2-Chloronaphthalene 10 ug/mL2-Chlorophenol 10 ug/mL2-Methylnaphthalene 10 ug/mL2-Methylphenol 10 ug/mL2-Nitroaniline 10 ug/mL2-Nitrophenol 10 ug/mL3-Nitroaniline 10 ug/mL4,6-Dinitro-2-methylphenol 10 ug/mL4-Bromophenyl phenyl ether 10 ug/mL4-Chloro-3-methylphenol 10 ug/mL4-Chloroaniline 10 ug/mL4-Chlorophenyl phenyl ether 10 ug/mL4-Nitroaniline 10 ug/mL4-Nitrophenol 10 ug/mL
Page 29 of 334
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
Acenaphthene 10 ug/mLAcenaphthylene 10 ug/mLAnthracene 10 ug/mLBenzo[a]anthracene 10 ug/mLBenzo[a]pyrene 10 ug/mLBenzo[b]fluoranthene 10 ug/mLBenzo[g,h,i]perylene 10 ug/mLBenzo[k]fluoranthene 10 ug/mLBis(2-chloroethoxy)methane 10 ug/mLBis(2-chloroethyl)ether 10 ug/mLBis(2-ethylhexyl) phthalate 10 ug/mLButyl benzyl phthalate 10 ug/mLCarbazole 10 ug/mLChrysene 10 ug/mLDi-n-butyl phthalate 10 ug/mLDi-n-octyl phthalate 10 ug/mLDibenz(a,h)anthracene 10 ug/mLDibenzofuran 10 ug/mLDiethyl phthalate 10 ug/mLDimethyl phthalate 10 ug/mLFluoranthene 10 ug/mLFluorene 10 ug/mLHexachlorobenzene 10 ug/mLHexachlorobutadiene 10 ug/mLHexachlorocyclopentadiene 10 ug/mLHexachloroethane 10 ug/mLIndeno[1,2,3-cd]pyrene 10 ug/mLIsophorone 10 ug/mLMethylphenol, 3 & 4 10 ug/mLN-Nitrosodi-n-propylamine 10 ug/mLN-Nitrosodimethylamine 10 ug/mLNaphthalene 10 ug/mLNitrobenzene 10 ug/mLPentachlorophenol 10 ug/mLPhenanthrene 10 ug/mLPhenol 10 ug/mLPyrene 10 ug/mLAniline 10 ug/mLSVSSCALIBMX4s_00003 0.005 mLBenzyl alcohol 10 ug/mLPyridine 10 ug/mLN-Nitrosodiphenylamine 10 ug/mLSVSSNNITRDPAs_00007 0.002 mL1,1'-Biphenyl 10 ug/mLSVSSOLMO42s_00003 0.005 mLAcetophenone 10 ug/mLCaprolactam 10 ug/mL
02/22/15 (Purchased Reagent) 1,2,4,5-Tetrachlorobenzene 1000 ug/mLSpex Certiprep, Lot T1090123013.SVSS1245TCBs_0000308/09/15 (Purchased Reagent) 1,4-Dioxane 1000 ug/mLAbsolute, Lot 080910.SVSS14DIOXANs_0000106/04/13 (Purchased Reagent) 2,6-Dichlorophenol 1000 ug/mLSpex Certiprep, Lot N1060606003.SVSS26DCPs_0000309/30/14 (Purchased Reagent) 1-Methylnaphthalene 2000 ug/mLSupelco, Lot LB66202.SVSSADDONs_00001
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
2,3,4,6-Tetrachlorophenol 2000 ug/mL2,3,5,6-Tetrachlorophenol 2000 ug/mLMethyl methanesulfonate 2000 ug/mL
06/30/14 (Purchased Reagent) 3,3'-Dichlorobenzidine 2000 ug/mLSupelco, Lot LB85259.SVSSBENZIDNs_0000204/30/13 (Purchased Reagent) 1,2,4-Trichlorobenzene 1000 ug/mLSupelco, Lot LB75037.SVSSCALIBMX1s_00003
1,2-Diphenylhydrazine 1000 ug/mL2,2'-oxybis[1-chloropropane] 1000 ug/mL2,4,5-Trichlorophenol 1000 ug/mL2,4,6-Trichlorophenol 1000 ug/mL2,4-Dichlorophenol 1000 ug/mL2,4-Dimethylphenol 1000 ug/mL2,4-Dinitrophenol 1000 ug/mL2,4-Dinitrotoluene 1000 ug/mL2,6-Dinitrotoluene 1000 ug/mL2-Chloronaphthalene 1000 ug/mL2-Chlorophenol 1000 ug/mL2-Methylnaphthalene 1000 ug/mL2-Methylphenol 1000 ug/mL2-Nitroaniline 1000 ug/mL2-Nitrophenol 1000 ug/mL3-Nitroaniline 1000 ug/mL4,6-Dinitro-2-methylphenol 1000 ug/mL4-Bromophenyl phenyl ether 1000 ug/mL4-Chloro-3-methylphenol 1000 ug/mL4-Chloroaniline 1000 ug/mL4-Chlorophenyl phenyl ether 1000 ug/mL4-Nitroaniline 1000 ug/mL4-Nitrophenol 1000 ug/mLAcenaphthene 1000 ug/mLAcenaphthylene 1000 ug/mLAnthracene 1000 ug/mLBenzo[a]anthracene 1000 ug/mLBenzo[a]pyrene 1000 ug/mLBenzo[b]fluoranthene 1000 ug/mLBenzo[g,h,i]perylene 1000 ug/mLBenzo[k]fluoranthene 1000 ug/mLBis(2-chloroethoxy)methane 1000 ug/mLBis(2-chloroethyl)ether 1000 ug/mLBis(2-ethylhexyl) phthalate 1000 ug/mLButyl benzyl phthalate 1000 ug/mLCarbazole 1000 ug/mLChrysene 1000 ug/mLDi-n-butyl phthalate 1000 ug/mLDi-n-octyl phthalate 1000 ug/mLDibenz(a,h)anthracene 1000 ug/mLDibenzofuran 1000 ug/mLDiethyl phthalate 1000 ug/mLDimethyl phthalate 1000 ug/mL
Page 31 of 334
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
Fluoranthene 1000 ug/mLFluorene 1000 ug/mLHexachlorobenzene 1000 ug/mLHexachlorobutadiene 1000 ug/mLHexachlorocyclopentadiene 1000 ug/mLHexachloroethane 1000 ug/mLIndeno[1,2,3-cd]pyrene 1000 ug/mLIsophorone 1000 ug/mLMethylphenol, 3 & 4 1000 ug/mLN-Nitrosodi-n-propylamine 1000 ug/mLN-Nitrosodimethylamine 1000 ug/mLNaphthalene 1000 ug/mLNitrobenzene 1000 ug/mLPentachlorophenol 1000 ug/mLPhenanthrene 1000 ug/mLPhenol 1000 ug/mLPyrene 1000 ug/mL
05/31/14 (Purchased Reagent) Aniline 2000 ug/mLSupelco, Lot LB86775.SVSSCALIBMX4s_00003Benzyl alcohol 2000 ug/mLPyridine 2000 ug/mL
02/28/14 (Purchased Reagent) N-Nitrosodiphenylamine 5000 ug/mLSupelco, Lot LB82298.SVSSNNITRDPAs_0000710/31/12 (Purchased Reagent) 1,1'-Biphenyl 2000 ug/mLSupelco, Lot LB70627.SVSSOLMO42s_00003
Acetophenone 2000 ug/mLCaprolactam 2000 ug/mL
09/30/14 (Purchased Reagent) Atrazine 200 ug/mLRestek, Lot A030933SVATRAZINEs_00034
SV2NAPAMINEs_00001 2-Naphthylamine 10 ug/mL1 mL 0.01 mL10/31/12 09/07/12SVDOD2NDSORi_00004 MeCl2, Lot 495447Benzidine 10 ug/mLSVBENZIDINEDs_00001 0.01 mLAtrazine 10 ug/mLSVSSOLMO42s_00002 0.005 mLBenzaldehyde 10 ug/mL
04/30/14 (Purchased Reagent) 2-Naphthylamine 1000 ug/mLUltra Scientific, Lot CG-1087.SV2NAPAMINEs_0000110/11/13 (Purchased Reagent) Benzidine 1000 ug/mLAbsolute, Lot 101110.SVBENZIDINEDs_0000110/31/12 (Purchased Reagent) Atrazine 2000 ug/mLSupelco, Lot LB70627.SVSSOLMO42s_00002
Benzaldehyde 2000 ug/mL
SV24DINITPOHi_00004 2,4-Dinitrophenol 1 ug/mL1 mL 0.008 mL12/12/12 07/30/12SVLLSSTD0.4i_00010 MeCl2, Lot 4800194,6-Dinitro-2-methylphenol 1 ug/mLSV46DN2MPHOHi_00004 0.008 mL4-Nitrophenol 1 ug/mLSV4NITPHOHi_00004 0.008 mLBenzoic acid 1 ug/mLSVBENZOICACi_00005 0.008 mL1-Methylnaphthalene 0.2 ug/mLSVLLSTOCKi_00008 0.005 mL2,3,4,6-Tetrachlorophenol 0.2 ug/mL2,3,5,6-Tetrachlorophenol 0.2 ug/mL2-Naphthylamine 0.2 ug/mL7,12-Dimethylbenz(a)anthracene 0.2 ug/mLMethyl methanesulfonate 0.2 ug/mL1,2,4,5-Tetrachlorobenzene 0.2 ug/mL1,4-Dioxane 0.2 ug/mL2,6-Dichlorophenol 0.2 ug/mL2,4,6-Tribromophenol 0.2 ug/mL
Page 32 of 334
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
2-Fluorophenol 0.2 ug/mLPhenol-d5 0.2 ug/mL3,3'-Dichlorobenzidine 0.2 ug/mLBenzidine 0.2 ug/mL2-Fluorobiphenyl 0.2 ug/mLNitrobenzene-d5 0.2 ug/mLTerphenyl-d14 0.2 ug/mLAniline 0.2 ug/mLBenzoic acid 1 ug/mLBenzyl alcohol 0.2 ug/mLPyridine 0.2 ug/mL1,1'-Biphenyl 0.2 ug/mLAcetophenone 0.2 ug/mLAtrazine 0.2 ug/mLBenzaldehyde 0.2 ug/mLCaprolactam 0.2 ug/mL1,2,4-Trichlorobenzene 0.2 ug/mL1,2-Dichlorobenzene 0.2 ug/mL1,2-Diphenylhydrazine 0.2 ug/mL1,3-Dichlorobenzene 0.2 ug/mL1,4-Dichlorobenzene 0.2 ug/mL2,2'-oxybis[1-chloropropane] 0.2 ug/mL2,4,5-Trichlorophenol 0.2 ug/mL2,4,6-Trichlorophenol 0.2 ug/mL2,4-Dichlorophenol 0.2 ug/mL2,4-Dimethylphenol 0.2 ug/mL2,4-Dinitrophenol 1 ug/mL2,4-Dinitrotoluene 0.2 ug/mL2,6-Dinitrotoluene 0.2 ug/mL2-Chloronaphthalene 0.2 ug/mL2-Chlorophenol 0.2 ug/mL2-Methylnaphthalene 0.2 ug/mL2-Methylphenol 0.2 ug/mL2-Nitroaniline 0.2 ug/mL2-Nitrophenol 0.2 ug/mL3-Nitroaniline 0.2 ug/mL4,6-Dinitro-2-methylphenol 1 ug/mL4-Bromophenyl phenyl ether 0.2 ug/mL4-Chloro-3-methylphenol 0.2 ug/mL4-Chloroaniline 0.2 ug/mL4-Chlorophenyl phenyl ether 0.2 ug/mL4-Nitroaniline 0.2 ug/mL4-Nitrophenol 1 ug/mLAcenaphthene 0.2 ug/mLAcenaphthylene 0.2 ug/mLAnthracene 0.2 ug/mLBenzo[a]anthracene 0.2 ug/mLBenzo[a]pyrene 0.2 ug/mL
Page 33 of 334
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
Benzo[b]fluoranthene 0.2 ug/mLBenzo[g,h,i]perylene 0.2 ug/mLBenzo[k]fluoranthene 0.2 ug/mLBis(2-chloroethoxy)methane 0.2 ug/mLBis(2-chloroethyl)ether 0.2 ug/mLBis(2-ethylhexyl) phthalate 0.2 ug/mLButyl benzyl phthalate 0.2 ug/mLCarbazole 0.2 ug/mLChrysene 0.2 ug/mLDi-n-butyl phthalate 0.2 ug/mLDi-n-octyl phthalate 0.2 ug/mLDibenz(a,h)anthracene 0.2 ug/mLDibenzofuran 0.2 ug/mLDiethyl phthalate 0.2 ug/mLDimethyl phthalate 0.2 ug/mLFluoranthene 0.2 ug/mLFluorene 0.2 ug/mLHexachlorobenzene 0.2 ug/mLHexachlorobutadiene 0.2 ug/mLHexachlorocyclopentadiene 0.2 ug/mLHexachloroethane 0.2 ug/mLIndeno[1,2,3-cd]pyrene 0.2 ug/mLIsophorone 0.2 ug/mLMethylphenol, 3 & 4 0.2 ug/mLN-Nitrosodi-n-propylamine 0.2 ug/mLN-Nitrosodimethylamine 0.2 ug/mLNaphthalene 0.2 ug/mLNitrobenzene 0.2 ug/mLPentachlorophenol 1 ug/mLPhenanthrene 0.2 ug/mLPhenol 0.2 ug/mLPyrene 0.2 ug/mLIndene 0.2 ug/mLN-Nitrosodiphenylamine 0.2 ug/mLN-Nitrosopyrrolidine 0.2 ug/mLPentachlorophenol 1 ug/mLSVPENTACHLPHi_00005 0.008 mL1,4-Dichlorobenzene-d4 4 ug/mLSVSIMINTERNi_00009 0.01 mLAcenaphthene-d10 4 ug/mLChrysene-d12 4 ug/mLNaphthalene-d8 4 ug/mLPerylene-d12 4 ug/mLPhenanthrene-d10 4 ug/mL
12/12/12 07/30/12 1 mL SV24DINITPHNs_00001 0.1 mL 2,4-Dinitrophenol 100 ug/mL.SV24DINITPOHi_00004 MeCl2, Lot 48001912/12/12 (Purchased Reagent) 2,4-Dinitrophenol 1000 ug/mLAbsolute Standards, Lot 121207..SV24DINITPHNs_0000101/30/13 07/30/12 1 mL SV46DN2MPHOHs_00001 0.1 mL 4,6-Dinitro-2-methylphenol 100 ug/mL.SV46DN2MPHOHi_00004 MeCl2, Lot 48001901/27/15 (Purchased Reagent) 4,6-Dinitro-2-methylphenol 1000 ug/mLAbsolute Standards, Lot 012710..SV46DN2MPHOHs_0000101/31/13 07/30/12 1 mL SV4NITROPHOHs_00001 0.1 mL 4-Nitrophenol 100 ug/mL.SV4NITPHOHi_00004 MeCl2, Lot 48001903/08/15 (Purchased Reagent) 4-Nitrophenol 1000 ug/mLAbsolute Standards, Lot 030810..SV4NITROPHOHs_00001
Page 34 of 334
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
01/31/13 07/30/12 1 mL SVBENZOICACDs_00001 0.1 mL Benzoic acid 100 ug/mL.SVBENZOICACi_00005 MeCl2, Lot 48001910/21/14 (Purchased Reagent) Benzoic acid 1000 ug/mLAbsolute Standards, Lot 102109..SVBENZOICACDs_00001
SV ADDON MIXs_00003 1-Methylnaphthalene 40 ug/mL10 mL 0.2 mL01/27/13 07/30/12.SVLLSTOCKi_00008 MeCl2, Lot 2997512,3,4,6-Tetrachlorophenol 40 ug/mL2,3,5,6-Tetrachlorophenol 40 ug/mL2-Naphthylamine 40 ug/mL7,12-Dimethylbenz(a)anthracene 40 ug/mLMethyl methanesulfonate 40 ug/mL1,2,4,5-Tetrachlorobenzene 40 ug/mLSV1245TCBENZs_00001 0.4 mL1,4-Dioxane 40 ug/mLSV14DIOXANEs_00002 0.2 mL2,6-Dichlorophenol 40 ug/mLSV26DCPHENOLs_00001 0.08 mL2,4,6-Tribromophenol 40 ug/mLSVACIDSURMIXs_00001 0.2 mL2-Fluorophenol 40 ug/mLPhenol-d5 40 ug/mL3,3'-Dichlorobenzidine 40 ug/mLSVBENZIDINEs_00008 0.2 mLBenzidine 40 ug/mL2-Fluorobiphenyl 40 ug/mLSVBNSURMIXs_00003 0.4 mLNitrobenzene-d5 40 ug/mLTerphenyl-d14 40 ug/mLAniline 40 ug/mLSVCALIBMIX4s_00002 0.2 mLBenzoic acid 40 ug/mLBenzyl alcohol 40 ug/mLPyridine 40 ug/mL1,1'-Biphenyl 40 ug/mLSVCLPOLM4MIXs_00003 0.2 mLAcetophenone 40 ug/mLAtrazine 40 ug/mLBenzaldehyde 40 ug/mLCaprolactam 40 ug/mL1,2,4-Trichlorobenzene 40 ug/mLSVCLPSVMIXs_00005 0.4 mL1,2-Dichlorobenzene 40 ug/mL1,2-Diphenylhydrazine 40 ug/mL1,3-Dichlorobenzene 40 ug/mL1,4-Dichlorobenzene 40 ug/mL2,2'-oxybis[1-chloropropane] 40 ug/mL2,4,5-Trichlorophenol 40 ug/mL2,4,6-Trichlorophenol 40 ug/mL2,4-Dichlorophenol 40 ug/mL2,4-Dimethylphenol 40 ug/mL2,4-Dinitrophenol 40 ug/mL2,4-Dinitrotoluene 40 ug/mL2,6-Dinitrotoluene 40 ug/mL2-Chloronaphthalene 40 ug/mL2-Chlorophenol 40 ug/mL2-Methylnaphthalene 40 ug/mL2-Methylphenol 40 ug/mL2-Nitroaniline 40 ug/mL2-Nitrophenol 40 ug/mL3-Nitroaniline 40 ug/mL
Page 35 of 334
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
4,6-Dinitro-2-methylphenol 40 ug/mL4-Bromophenyl phenyl ether 40 ug/mL4-Chloro-3-methylphenol 40 ug/mL4-Chloroaniline 40 ug/mL4-Chlorophenyl phenyl ether 40 ug/mL4-Nitroaniline 40 ug/mL4-Nitrophenol 40 ug/mLAcenaphthene 40 ug/mLAcenaphthylene 40 ug/mLAnthracene 40 ug/mLBenzo[a]anthracene 40 ug/mLBenzo[a]pyrene 40 ug/mLBenzo[b]fluoranthene 40 ug/mLBenzo[g,h,i]perylene 40 ug/mLBenzo[k]fluoranthene 40 ug/mLBis(2-chloroethoxy)methane 40 ug/mLBis(2-chloroethyl)ether 40 ug/mLBis(2-ethylhexyl) phthalate 40 ug/mLButyl benzyl phthalate 40 ug/mLCarbazole 40 ug/mLChrysene 40 ug/mLDi-n-butyl phthalate 40 ug/mLDi-n-octyl phthalate 40 ug/mLDibenz(a,h)anthracene 40 ug/mLDibenzofuran 40 ug/mLDiethyl phthalate 40 ug/mLDimethyl phthalate 40 ug/mLFluoranthene 40 ug/mLFluorene 40 ug/mLHexachlorobenzene 40 ug/mLHexachlorobutadiene 40 ug/mLHexachlorocyclopentadiene 40 ug/mLHexachloroethane 40 ug/mLIndeno[1,2,3-cd]pyrene 40 ug/mLIsophorone 40 ug/mLMethylphenol, 3 & 4 40 ug/mLN-Nitrosodi-n-propylamine 40 ug/mLN-Nitrosodimethylamine 40 ug/mLNaphthalene 40 ug/mLNitrobenzene 40 ug/mLPentachlorophenol 40 ug/mLPhenanthrene 40 ug/mLPhenol 40 ug/mLPyrene 40 ug/mLIndene 40 ug/mLSVINDENEs_00010 0.4 mLN-Nitrosodiphenylamine 40 ug/mLSVNNDIPHENAMs_00002 0.08 mL
SVNNITROPYROs_00001 0.4 mL N-Nitrosopyrrolidine 40 ug/mL01/31/13 (Purchased Reagent) 1-Methylnaphthalene 2000 ug/mLSupelco, Lot LB 879735..SV ADDON MIXs_00003
Page 36 of 334
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
2,3,4,6-Tetrachlorophenol 2000 ug/mL2,3,5,6-Tetrachlorophenol 2000 ug/mL2-Naphthylamine 2000 ug/mL7,12-Dimethylbenz(a)anthracene 2000 ug/mLMethyl methanesulfonate 2000 ug/mL
09/09/13 (Purchased Reagent) 1,2,4,5-Tetrachlorobenzene 1000 ug/mLAbsolute Standards, Lot 090908..SV1245TCBENZs_0000110/31/16 (Purchased Reagent) 1,4-Dioxane 2000 ug/mLRestek, Lot A077490..SV14DIOXANEs_0000208/31/13 (Purchased Reagent) 2,6-Dichlorophenol 5000 ug/mLSupelco, Lot LB78166..SV26DCPHENOLs_0000101/31/13 (Purchased Reagent) 2,4,6-Tribromophenol 2000 ug/mLUltra Scientific, Lot CF-5141..SVACIDSURMIXs_00001
2-Fluorophenol 2000 ug/mLPhenol-d5 2000 ug/mL
01/27/13 (Purchased Reagent) 3,3'-Dichlorobenzidine 2000 ug/mLSupelco, Lot LB79050..SVBENZIDINEs_00008Benzidine 2000 ug/mL
08/30/13 (Purchased Reagent) 2-Fluorobiphenyl 1000 ug/mLUltra Scientific, Lot CG-2463..SVBNSURMIXs_00003Nitrobenzene-d5 1000 ug/mLTerphenyl-d14 1000 ug/mL
11/30/14 (Purchased Reagent) Aniline 2000 ug/mLSupelco, Lot LB88725..SVCALIBMIX4s_00002Benzoic acid 2000 ug/mLBenzyl alcohol 2000 ug/mLPyridine 2000 ug/mL
04/30/13 (Purchased Reagent) 1,1'-Biphenyl 2000 ug/mLSupelco, Lot LB73726..SVCLPOLM4MIXs_00003Acetophenone 2000 ug/mLAtrazine 2000 ug/mLBenzaldehyde 2000 ug/mLCaprolactam 2000 ug/mL
09/30/13 (Purchased Reagent) 1,2,4-Trichlorobenzene 1000 ug/mLSupelco, Lot lb78428..SVCLPSVMIXs_000051,2-Dichlorobenzene 1000 ug/mL1,2-Diphenylhydrazine 1000 ug/mL1,3-Dichlorobenzene 1000 ug/mL1,4-Dichlorobenzene 1000 ug/mL2,2'-oxybis[1-chloropropane] 1000 ug/mL2,4,5-Trichlorophenol 1000 ug/mL2,4,6-Trichlorophenol 1000 ug/mL2,4-Dichlorophenol 1000 ug/mL2,4-Dimethylphenol 1000 ug/mL2,4-Dinitrophenol 1000 ug/mL2,4-Dinitrotoluene 1000 ug/mL2,6-Dinitrotoluene 1000 ug/mL2-Chloronaphthalene 1000 ug/mL2-Chlorophenol 1000 ug/mL2-Methylnaphthalene 1000 ug/mL2-Methylphenol 1000 ug/mL2-Nitroaniline 1000 ug/mL2-Nitrophenol 1000 ug/mL3-Nitroaniline 1000 ug/mL4,6-Dinitro-2-methylphenol 1000 ug/mL4-Bromophenyl phenyl ether 1000 ug/mL4-Chloro-3-methylphenol 1000 ug/mL
Page 37 of 334
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
4-Chloroaniline 1000 ug/mL4-Chlorophenyl phenyl ether 1000 ug/mL4-Nitroaniline 1000 ug/mL4-Nitrophenol 1000 ug/mLAcenaphthene 1000 ug/mLAcenaphthylene 1000 ug/mLAnthracene 1000 ug/mLBenzo[a]anthracene 1000 ug/mLBenzo[a]pyrene 1000 ug/mLBenzo[b]fluoranthene 1000 ug/mLBenzo[g,h,i]perylene 1000 ug/mLBenzo[k]fluoranthene 1000 ug/mLBis(2-chloroethoxy)methane 1000 ug/mLBis(2-chloroethyl)ether 1000 ug/mLBis(2-ethylhexyl) phthalate 1000 ug/mLButyl benzyl phthalate 1000 ug/mLCarbazole 1000 ug/mLChrysene 1000 ug/mLDi-n-butyl phthalate 1000 ug/mLDi-n-octyl phthalate 1000 ug/mLDibenz(a,h)anthracene 1000 ug/mLDibenzofuran 1000 ug/mLDiethyl phthalate 1000 ug/mLDimethyl phthalate 1000 ug/mLFluoranthene 1000 ug/mLFluorene 1000 ug/mLHexachlorobenzene 1000 ug/mLHexachlorobutadiene 1000 ug/mLHexachlorocyclopentadiene 1000 ug/mLHexachloroethane 1000 ug/mLIndeno[1,2,3-cd]pyrene 1000 ug/mLIsophorone 1000 ug/mLMethylphenol, 3 & 4 1000 ug/mLN-Nitrosodi-n-propylamine 1000 ug/mLN-Nitrosodimethylamine 1000 ug/mLNaphthalene 1000 ug/mLNitrobenzene 1000 ug/mLPentachlorophenol 1000 ug/mLPhenanthrene 1000 ug/mLPhenol 1000 ug/mLPyrene 1000 ug/mL
10/10/13 (Purchased Reagent) Indene 1000 ug/mLAbsolute Standards, Lot 101011..SVINDENEs_0001006/30/13 (Purchased Reagent) N-Nitrosodiphenylamine 5000 ug/mLSupelco, Lot LB76738..SVNNDIPHENAMs_0000212/09/14 (Purchased Reagent) N-Nitrosopyrrolidine 1000 ug/mLAbsolute Standards, Lot 120909..SVNNITROPYROs_0000101/31/13 07/30/12 1 mL SVPENTCLPHENs_00001 0.1 mL Pentachlorophenol 100 ug/mL.SVPENTACHLPHi_00005 MeCl2, Lot 48001909/17/14 (Purchased Reagent) Pentachlorophenol 1000 ug/mLAbsolute Standards, Lot 091709..SVPENTCLPHENs_00001
SVINTSTDMIXs_00002 1,4-Dichlorobenzene-d4 400 ug/mL10 mL 2 mL12/17/12 12/17/11.SVSIMINTERNi_00009 MeCl2, Lot 222635Acenaphthene-d10 400 ug/mL
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
Chrysene-d12 400 ug/mLNaphthalene-d8 400 ug/mLPerylene-d12 400 ug/mLPhenanthrene-d10 400 ug/mL
07/31/13 (Purchased Reagent) 1,4-Dichlorobenzene-d4 2000 ug/mLSupelco, Lot LB77211..SVINTSTDMIXs_00002Acenaphthene-d10 2000 ug/mLChrysene-d12 2000 ug/mLNaphthalene-d8 2000 ug/mLPerylene-d12 2000 ug/mLPhenanthrene-d10 2000 ug/mL
SV24DINITPOHi_00004 2,4-Dinitrophenol 10 ug/mL1 mL 0.05 mL12/12/12 07/30/12SVLLSSTD10i_00006 MeCl2, Lot 4800194,6-Dinitro-2-methylphenol 10 ug/mLSV46DN2MPHOHi_00004 0.05 mL4-Nitrophenol 10 ug/mLSV4NITPHOHi_00004 0.05 mLBenzoic acid 10 ug/mLSVBENZOICACi_00005 0.05 mL1-Methylnaphthalene 5 ug/mLSVLLSTOCKi_00008 0.125 mL2,3,4,6-Tetrachlorophenol 5 ug/mL2,3,5,6-Tetrachlorophenol 5 ug/mL2-Naphthylamine 5 ug/mL7,12-Dimethylbenz(a)anthracene 5 ug/mLMethyl methanesulfonate 5 ug/mL1,2,4,5-Tetrachlorobenzene 5 ug/mL1,4-Dioxane 5 ug/mL2,6-Dichlorophenol 5 ug/mL2,4,6-Tribromophenol 5 ug/mL2-Fluorophenol 5 ug/mLPhenol-d5 5 ug/mL3,3'-Dichlorobenzidine 5 ug/mLBenzidine 5 ug/mL2-Fluorobiphenyl 5 ug/mLNitrobenzene-d5 5 ug/mLTerphenyl-d14 5 ug/mLAniline 5 ug/mLBenzoic acid 10 ug/mLBenzyl alcohol 5 ug/mLPyridine 5 ug/mL1,1'-Biphenyl 5 ug/mLAcetophenone 5 ug/mLAtrazine 5 ug/mLBenzaldehyde 5 ug/mLCaprolactam 5 ug/mL1,2,4-Trichlorobenzene 5 ug/mL1,2-Dichlorobenzene 5 ug/mL1,2-Diphenylhydrazine 5 ug/mL1,3-Dichlorobenzene 5 ug/mL1,4-Dichlorobenzene 5 ug/mL2,2'-oxybis[1-chloropropane] 5 ug/mL2,4,5-Trichlorophenol 5 ug/mL
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
2,4,6-Trichlorophenol 5 ug/mL2,4-Dichlorophenol 5 ug/mL2,4-Dimethylphenol 5 ug/mL2,4-Dinitrophenol 10 ug/mL2,4-Dinitrotoluene 5 ug/mL2,6-Dinitrotoluene 5 ug/mL2-Chloronaphthalene 5 ug/mL2-Chlorophenol 5 ug/mL2-Methylnaphthalene 5 ug/mL2-Methylphenol 5 ug/mL2-Nitroaniline 5 ug/mL2-Nitrophenol 5 ug/mL3-Nitroaniline 5 ug/mL4,6-Dinitro-2-methylphenol 10 ug/mL4-Bromophenyl phenyl ether 5 ug/mL4-Chloro-3-methylphenol 5 ug/mL4-Chloroaniline 5 ug/mL4-Chlorophenyl phenyl ether 5 ug/mL4-Nitroaniline 5 ug/mL4-Nitrophenol 10 ug/mLAcenaphthene 5 ug/mLAcenaphthylene 5 ug/mLAnthracene 5 ug/mLBenzo[a]anthracene 5 ug/mLBenzo[a]pyrene 5 ug/mLBenzo[b]fluoranthene 5 ug/mLBenzo[g,h,i]perylene 5 ug/mLBenzo[k]fluoranthene 5 ug/mLBis(2-chloroethoxy)methane 5 ug/mLBis(2-chloroethyl)ether 5 ug/mLBis(2-ethylhexyl) phthalate 5 ug/mLButyl benzyl phthalate 5 ug/mLCarbazole 5 ug/mLChrysene 5 ug/mLDi-n-butyl phthalate 5 ug/mLDi-n-octyl phthalate 5 ug/mLDibenz(a,h)anthracene 5 ug/mLDibenzofuran 5 ug/mLDiethyl phthalate 5 ug/mLDimethyl phthalate 5 ug/mLFluoranthene 5 ug/mLFluorene 5 ug/mLHexachlorobenzene 5 ug/mLHexachlorobutadiene 5 ug/mLHexachlorocyclopentadiene 5 ug/mLHexachloroethane 5 ug/mLIndeno[1,2,3-cd]pyrene 5 ug/mLIsophorone 5 ug/mL
Page 40 of 334
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
Methylphenol, 3 & 4 5 ug/mLN-Nitrosodi-n-propylamine 5 ug/mLN-Nitrosodimethylamine 5 ug/mLNaphthalene 5 ug/mLNitrobenzene 5 ug/mLPentachlorophenol 10 ug/mLPhenanthrene 5 ug/mLPhenol 5 ug/mLPyrene 5 ug/mLIndene 5 ug/mLN-Nitrosodiphenylamine 5 ug/mLN-Nitrosopyrrolidine 5 ug/mLPentachlorophenol 10 ug/mLSVPENTACHLPHi_00005 0.05 mL1,4-Dichlorobenzene-d4 4 ug/mLSVSIMINTERNi_00009 0.01 mLAcenaphthene-d10 4 ug/mLChrysene-d12 4 ug/mLNaphthalene-d8 4 ug/mLPerylene-d12 4 ug/mLPhenanthrene-d10 4 ug/mL
12/12/12 07/30/12 1 mL SV24DINITPHNs_00001 0.1 mL 2,4-Dinitrophenol 100 ug/mL.SV24DINITPOHi_00004 MeCl2, Lot 48001912/12/12 (Purchased Reagent) 2,4-Dinitrophenol 1000 ug/mLAbsolute Standards, Lot 121207..SV24DINITPHNs_0000101/30/13 07/30/12 1 mL SV46DN2MPHOHs_00001 0.1 mL 4,6-Dinitro-2-methylphenol 100 ug/mL.SV46DN2MPHOHi_00004 MeCl2, Lot 48001901/27/15 (Purchased Reagent) 4,6-Dinitro-2-methylphenol 1000 ug/mLAbsolute Standards, Lot 012710..SV46DN2MPHOHs_0000101/31/13 07/30/12 1 mL SV4NITROPHOHs_00001 0.1 mL 4-Nitrophenol 100 ug/mL.SV4NITPHOHi_00004 MeCl2, Lot 48001903/08/15 (Purchased Reagent) 4-Nitrophenol 1000 ug/mLAbsolute Standards, Lot 030810..SV4NITROPHOHs_0000101/31/13 07/30/12 1 mL SVBENZOICACDs_00001 0.1 mL Benzoic acid 100 ug/mL.SVBENZOICACi_00005 MeCl2, Lot 48001910/21/14 (Purchased Reagent) Benzoic acid 1000 ug/mLAbsolute Standards, Lot 102109..SVBENZOICACDs_00001
SV ADDON MIXs_00003 1-Methylnaphthalene 40 ug/mL10 mL 0.2 mL01/27/13 07/30/12.SVLLSTOCKi_00008 MeCl2, Lot 2997512,3,4,6-Tetrachlorophenol 40 ug/mL2,3,5,6-Tetrachlorophenol 40 ug/mL2-Naphthylamine 40 ug/mL7,12-Dimethylbenz(a)anthracene 40 ug/mLMethyl methanesulfonate 40 ug/mL1,2,4,5-Tetrachlorobenzene 40 ug/mLSV1245TCBENZs_00001 0.4 mL1,4-Dioxane 40 ug/mLSV14DIOXANEs_00002 0.2 mL2,6-Dichlorophenol 40 ug/mLSV26DCPHENOLs_00001 0.08 mL2,4,6-Tribromophenol 40 ug/mLSVACIDSURMIXs_00001 0.2 mL2-Fluorophenol 40 ug/mLPhenol-d5 40 ug/mL3,3'-Dichlorobenzidine 40 ug/mLSVBENZIDINEs_00008 0.2 mLBenzidine 40 ug/mL2-Fluorobiphenyl 40 ug/mLSVBNSURMIXs_00003 0.4 mLNitrobenzene-d5 40 ug/mLTerphenyl-d14 40 ug/mLAniline 40 ug/mLSVCALIBMIX4s_00002 0.2 mLBenzoic acid 40 ug/mLBenzyl alcohol 40 ug/mLPyridine 40 ug/mL
Page 41 of 334
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
1,1'-Biphenyl 40 ug/mLSVCLPOLM4MIXs_00003 0.2 mLAcetophenone 40 ug/mLAtrazine 40 ug/mLBenzaldehyde 40 ug/mLCaprolactam 40 ug/mL1,2,4-Trichlorobenzene 40 ug/mLSVCLPSVMIXs_00005 0.4 mL1,2-Dichlorobenzene 40 ug/mL1,2-Diphenylhydrazine 40 ug/mL1,3-Dichlorobenzene 40 ug/mL1,4-Dichlorobenzene 40 ug/mL2,2'-oxybis[1-chloropropane] 40 ug/mL2,4,5-Trichlorophenol 40 ug/mL2,4,6-Trichlorophenol 40 ug/mL2,4-Dichlorophenol 40 ug/mL2,4-Dimethylphenol 40 ug/mL2,4-Dinitrophenol 40 ug/mL2,4-Dinitrotoluene 40 ug/mL2,6-Dinitrotoluene 40 ug/mL2-Chloronaphthalene 40 ug/mL2-Chlorophenol 40 ug/mL2-Methylnaphthalene 40 ug/mL2-Methylphenol 40 ug/mL2-Nitroaniline 40 ug/mL2-Nitrophenol 40 ug/mL3-Nitroaniline 40 ug/mL4,6-Dinitro-2-methylphenol 40 ug/mL4-Bromophenyl phenyl ether 40 ug/mL4-Chloro-3-methylphenol 40 ug/mL4-Chloroaniline 40 ug/mL4-Chlorophenyl phenyl ether 40 ug/mL4-Nitroaniline 40 ug/mL4-Nitrophenol 40 ug/mLAcenaphthene 40 ug/mLAcenaphthylene 40 ug/mLAnthracene 40 ug/mLBenzo[a]anthracene 40 ug/mLBenzo[a]pyrene 40 ug/mLBenzo[b]fluoranthene 40 ug/mLBenzo[g,h,i]perylene 40 ug/mLBenzo[k]fluoranthene 40 ug/mLBis(2-chloroethoxy)methane 40 ug/mLBis(2-chloroethyl)ether 40 ug/mLBis(2-ethylhexyl) phthalate 40 ug/mLButyl benzyl phthalate 40 ug/mLCarbazole 40 ug/mLChrysene 40 ug/mLDi-n-butyl phthalate 40 ug/mLDi-n-octyl phthalate 40 ug/mL
Page 42 of 334
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
Dibenz(a,h)anthracene 40 ug/mLDibenzofuran 40 ug/mLDiethyl phthalate 40 ug/mLDimethyl phthalate 40 ug/mLFluoranthene 40 ug/mLFluorene 40 ug/mLHexachlorobenzene 40 ug/mLHexachlorobutadiene 40 ug/mLHexachlorocyclopentadiene 40 ug/mLHexachloroethane 40 ug/mLIndeno[1,2,3-cd]pyrene 40 ug/mLIsophorone 40 ug/mLMethylphenol, 3 & 4 40 ug/mLN-Nitrosodi-n-propylamine 40 ug/mLN-Nitrosodimethylamine 40 ug/mLNaphthalene 40 ug/mLNitrobenzene 40 ug/mLPentachlorophenol 40 ug/mLPhenanthrene 40 ug/mLPhenol 40 ug/mLPyrene 40 ug/mLIndene 40 ug/mLSVINDENEs_00010 0.4 mLN-Nitrosodiphenylamine 40 ug/mLSVNNDIPHENAMs_00002 0.08 mL
SVNNITROPYROs_00001 0.4 mL N-Nitrosopyrrolidine 40 ug/mL01/31/13 (Purchased Reagent) 1-Methylnaphthalene 2000 ug/mLSupelco, Lot LB 879735..SV ADDON MIXs_00003
2,3,4,6-Tetrachlorophenol 2000 ug/mL2,3,5,6-Tetrachlorophenol 2000 ug/mL2-Naphthylamine 2000 ug/mL7,12-Dimethylbenz(a)anthracene 2000 ug/mLMethyl methanesulfonate 2000 ug/mL
09/09/13 (Purchased Reagent) 1,2,4,5-Tetrachlorobenzene 1000 ug/mLAbsolute Standards, Lot 090908..SV1245TCBENZs_0000110/31/16 (Purchased Reagent) 1,4-Dioxane 2000 ug/mLRestek, Lot A077490..SV14DIOXANEs_0000208/31/13 (Purchased Reagent) 2,6-Dichlorophenol 5000 ug/mLSupelco, Lot LB78166..SV26DCPHENOLs_0000101/31/13 (Purchased Reagent) 2,4,6-Tribromophenol 2000 ug/mLUltra Scientific, Lot CF-5141..SVACIDSURMIXs_00001
2-Fluorophenol 2000 ug/mLPhenol-d5 2000 ug/mL
01/27/13 (Purchased Reagent) 3,3'-Dichlorobenzidine 2000 ug/mLSupelco, Lot LB79050..SVBENZIDINEs_00008Benzidine 2000 ug/mL
08/30/13 (Purchased Reagent) 2-Fluorobiphenyl 1000 ug/mLUltra Scientific, Lot CG-2463..SVBNSURMIXs_00003Nitrobenzene-d5 1000 ug/mLTerphenyl-d14 1000 ug/mL
11/30/14 (Purchased Reagent) Aniline 2000 ug/mLSupelco, Lot LB88725..SVCALIBMIX4s_00002Benzoic acid 2000 ug/mLBenzyl alcohol 2000 ug/mLPyridine 2000 ug/mL
04/30/13 (Purchased Reagent) 1,1'-Biphenyl 2000 ug/mLSupelco, Lot LB73726..SVCLPOLM4MIXs_00003Acetophenone 2000 ug/mLAtrazine 2000 ug/mL
Page 43 of 334
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
Benzaldehyde 2000 ug/mLCaprolactam 2000 ug/mL
09/30/13 (Purchased Reagent) 1,2,4-Trichlorobenzene 1000 ug/mLSupelco, Lot lb78428..SVCLPSVMIXs_000051,2-Dichlorobenzene 1000 ug/mL1,2-Diphenylhydrazine 1000 ug/mL1,3-Dichlorobenzene 1000 ug/mL1,4-Dichlorobenzene 1000 ug/mL2,2'-oxybis[1-chloropropane] 1000 ug/mL2,4,5-Trichlorophenol 1000 ug/mL2,4,6-Trichlorophenol 1000 ug/mL2,4-Dichlorophenol 1000 ug/mL2,4-Dimethylphenol 1000 ug/mL2,4-Dinitrophenol 1000 ug/mL2,4-Dinitrotoluene 1000 ug/mL2,6-Dinitrotoluene 1000 ug/mL2-Chloronaphthalene 1000 ug/mL2-Chlorophenol 1000 ug/mL2-Methylnaphthalene 1000 ug/mL2-Methylphenol 1000 ug/mL2-Nitroaniline 1000 ug/mL2-Nitrophenol 1000 ug/mL3-Nitroaniline 1000 ug/mL4,6-Dinitro-2-methylphenol 1000 ug/mL4-Bromophenyl phenyl ether 1000 ug/mL4-Chloro-3-methylphenol 1000 ug/mL4-Chloroaniline 1000 ug/mL4-Chlorophenyl phenyl ether 1000 ug/mL4-Nitroaniline 1000 ug/mL4-Nitrophenol 1000 ug/mLAcenaphthene 1000 ug/mLAcenaphthylene 1000 ug/mLAnthracene 1000 ug/mLBenzo[a]anthracene 1000 ug/mLBenzo[a]pyrene 1000 ug/mLBenzo[b]fluoranthene 1000 ug/mLBenzo[g,h,i]perylene 1000 ug/mLBenzo[k]fluoranthene 1000 ug/mLBis(2-chloroethoxy)methane 1000 ug/mLBis(2-chloroethyl)ether 1000 ug/mLBis(2-ethylhexyl) phthalate 1000 ug/mLButyl benzyl phthalate 1000 ug/mLCarbazole 1000 ug/mLChrysene 1000 ug/mLDi-n-butyl phthalate 1000 ug/mLDi-n-octyl phthalate 1000 ug/mLDibenz(a,h)anthracene 1000 ug/mLDibenzofuran 1000 ug/mLDiethyl phthalate 1000 ug/mL
Page 44 of 334
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
Dimethyl phthalate 1000 ug/mLFluoranthene 1000 ug/mLFluorene 1000 ug/mLHexachlorobenzene 1000 ug/mLHexachlorobutadiene 1000 ug/mLHexachlorocyclopentadiene 1000 ug/mLHexachloroethane 1000 ug/mLIndeno[1,2,3-cd]pyrene 1000 ug/mLIsophorone 1000 ug/mLMethylphenol, 3 & 4 1000 ug/mLN-Nitrosodi-n-propylamine 1000 ug/mLN-Nitrosodimethylamine 1000 ug/mLNaphthalene 1000 ug/mLNitrobenzene 1000 ug/mLPentachlorophenol 1000 ug/mLPhenanthrene 1000 ug/mLPhenol 1000 ug/mLPyrene 1000 ug/mL
10/10/13 (Purchased Reagent) Indene 1000 ug/mLAbsolute Standards, Lot 101011..SVINDENEs_0001006/30/13 (Purchased Reagent) N-Nitrosodiphenylamine 5000 ug/mLSupelco, Lot LB76738..SVNNDIPHENAMs_0000212/09/14 (Purchased Reagent) N-Nitrosopyrrolidine 1000 ug/mLAbsolute Standards, Lot 120909..SVNNITROPYROs_0000101/31/13 07/30/12 1 mL SVPENTCLPHENs_00001 0.1 mL Pentachlorophenol 100 ug/mL.SVPENTACHLPHi_00005 MeCl2, Lot 48001909/17/14 (Purchased Reagent) Pentachlorophenol 1000 ug/mLAbsolute Standards, Lot 091709..SVPENTCLPHENs_00001
SVINTSTDMIXs_00002 1,4-Dichlorobenzene-d4 400 ug/mL10 mL 2 mL12/17/12 12/17/11.SVSIMINTERNi_00009 MeCl2, Lot 222635Acenaphthene-d10 400 ug/mLChrysene-d12 400 ug/mLNaphthalene-d8 400 ug/mLPerylene-d12 400 ug/mLPhenanthrene-d10 400 ug/mL
07/31/13 (Purchased Reagent) 1,4-Dichlorobenzene-d4 2000 ug/mLSupelco, Lot LB77211..SVINTSTDMIXs_00002Acenaphthene-d10 2000 ug/mLChrysene-d12 2000 ug/mLNaphthalene-d8 2000 ug/mLPerylene-d12 2000 ug/mLPhenanthrene-d10 2000 ug/mL
SV24DINITPOHi_00004 2,4-Dinitrophenol 2 ug/mL1 mL 0.01 mL12/12/12 07/30/12SVLLSSTD2.0i_00006 MeCl2, Lot 4800194,6-Dinitro-2-methylphenol 2 ug/mLSV46DN2MPHOHi_00004 0.01 mL4-Nitrophenol 2 ug/mLSV4NITPHOHi_00004 0.01 mLBenzoic acid 2 ug/mLSVBENZOICACi_00005 0.01 mL1-Methylnaphthalene 1 ug/mLSVLLSTOCKi_00008 0.025 mL2,3,4,6-Tetrachlorophenol 1 ug/mL2,3,5,6-Tetrachlorophenol 1 ug/mL2-Naphthylamine 1 ug/mL7,12-Dimethylbenz(a)anthracene 1 ug/mLMethyl methanesulfonate 1 ug/mL1,2,4,5-Tetrachlorobenzene 1 ug/mL1,4-Dioxane 1 ug/mL
Page 45 of 334
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
2,6-Dichlorophenol 1 ug/mL2,4,6-Tribromophenol 1 ug/mL2-Fluorophenol 1 ug/mLPhenol-d5 1 ug/mL3,3'-Dichlorobenzidine 1 ug/mLBenzidine 1 ug/mL2-Fluorobiphenyl 1 ug/mLNitrobenzene-d5 1 ug/mLTerphenyl-d14 1 ug/mLAniline 1 ug/mLBenzoic acid 2 ug/mLBenzyl alcohol 1 ug/mLPyridine 1 ug/mL1,1'-Biphenyl 1 ug/mLAcetophenone 1 ug/mLAtrazine 1 ug/mLBenzaldehyde 1 ug/mLCaprolactam 1 ug/mL1,2,4-Trichlorobenzene 1 ug/mL1,2-Dichlorobenzene 1 ug/mL1,2-Diphenylhydrazine 1 ug/mL1,3-Dichlorobenzene 1 ug/mL1,4-Dichlorobenzene 1 ug/mL2,2'-oxybis[1-chloropropane] 1 ug/mL2,4,5-Trichlorophenol 1 ug/mL2,4,6-Trichlorophenol 1 ug/mL2,4-Dichlorophenol 1 ug/mL2,4-Dimethylphenol 1 ug/mL2,4-Dinitrophenol 2 ug/mL2,4-Dinitrotoluene 1 ug/mL2,6-Dinitrotoluene 1 ug/mL2-Chloronaphthalene 1 ug/mL2-Chlorophenol 1 ug/mL2-Methylnaphthalene 1 ug/mL2-Methylphenol 1 ug/mL2-Nitroaniline 1 ug/mL2-Nitrophenol 1 ug/mL3-Nitroaniline 1 ug/mL4,6-Dinitro-2-methylphenol 2 ug/mL4-Bromophenyl phenyl ether 1 ug/mL4-Chloro-3-methylphenol 1 ug/mL4-Chloroaniline 1 ug/mL4-Chlorophenyl phenyl ether 1 ug/mL4-Nitroaniline 1 ug/mL4-Nitrophenol 2 ug/mLAcenaphthene 1 ug/mLAcenaphthylene 1 ug/mLAnthracene 1 ug/mL
Page 46 of 334
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
Benzo[a]anthracene 1 ug/mLBenzo[a]pyrene 1 ug/mLBenzo[b]fluoranthene 1 ug/mLBenzo[g,h,i]perylene 1 ug/mLBenzo[k]fluoranthene 1 ug/mLBis(2-chloroethoxy)methane 1 ug/mLBis(2-chloroethyl)ether 1 ug/mLBis(2-ethylhexyl) phthalate 1 ug/mLButyl benzyl phthalate 1 ug/mLCarbazole 1 ug/mLChrysene 1 ug/mLDi-n-butyl phthalate 1 ug/mLDi-n-octyl phthalate 1 ug/mLDibenz(a,h)anthracene 1 ug/mLDibenzofuran 1 ug/mLDiethyl phthalate 1 ug/mLDimethyl phthalate 1 ug/mLFluoranthene 1 ug/mLFluorene 1 ug/mLHexachlorobenzene 1 ug/mLHexachlorobutadiene 1 ug/mLHexachlorocyclopentadiene 1 ug/mLHexachloroethane 1 ug/mLIndeno[1,2,3-cd]pyrene 1 ug/mLIsophorone 1 ug/mLMethylphenol, 3 & 4 1 ug/mLN-Nitrosodi-n-propylamine 1 ug/mLN-Nitrosodimethylamine 1 ug/mLNaphthalene 1 ug/mLNitrobenzene 1 ug/mLPentachlorophenol 2 ug/mLPhenanthrene 1 ug/mLPhenol 1 ug/mLPyrene 1 ug/mLIndene 1 ug/mLN-Nitrosodiphenylamine 1 ug/mLN-Nitrosopyrrolidine 1 ug/mLPentachlorophenol 2 ug/mLSVPENTACHLPHi_00005 0.01 mL1,4-Dichlorobenzene-d4 4 ug/mLSVSIMINTERNi_00009 0.01 mLAcenaphthene-d10 4 ug/mLChrysene-d12 4 ug/mLNaphthalene-d8 4 ug/mLPerylene-d12 4 ug/mLPhenanthrene-d10 4 ug/mL
12/12/12 07/30/12 1 mL SV24DINITPHNs_00001 0.1 mL 2,4-Dinitrophenol 100 ug/mL.SV24DINITPOHi_00004 MeCl2, Lot 48001912/12/12 (Purchased Reagent) 2,4-Dinitrophenol 1000 ug/mLAbsolute Standards, Lot 121207..SV24DINITPHNs_0000101/30/13 07/30/12 1 mL SV46DN2MPHOHs_00001 0.1 mL 4,6-Dinitro-2-methylphenol 100 ug/mL.SV46DN2MPHOHi_00004 MeCl2, Lot 48001901/27/15 (Purchased Reagent) 4,6-Dinitro-2-methylphenol 1000 ug/mLAbsolute Standards, Lot 012710..SV46DN2MPHOHs_00001
Page 47 of 334
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
01/31/13 07/30/12 1 mL SV4NITROPHOHs_00001 0.1 mL 4-Nitrophenol 100 ug/mL.SV4NITPHOHi_00004 MeCl2, Lot 48001903/08/15 (Purchased Reagent) 4-Nitrophenol 1000 ug/mLAbsolute Standards, Lot 030810..SV4NITROPHOHs_0000101/31/13 07/30/12 1 mL SVBENZOICACDs_00001 0.1 mL Benzoic acid 100 ug/mL.SVBENZOICACi_00005 MeCl2, Lot 48001910/21/14 (Purchased Reagent) Benzoic acid 1000 ug/mLAbsolute Standards, Lot 102109..SVBENZOICACDs_00001
SV ADDON MIXs_00003 1-Methylnaphthalene 40 ug/mL10 mL 0.2 mL01/27/13 07/30/12.SVLLSTOCKi_00008 MeCl2, Lot 2997512,3,4,6-Tetrachlorophenol 40 ug/mL2,3,5,6-Tetrachlorophenol 40 ug/mL2-Naphthylamine 40 ug/mL7,12-Dimethylbenz(a)anthracene 40 ug/mLMethyl methanesulfonate 40 ug/mL1,2,4,5-Tetrachlorobenzene 40 ug/mLSV1245TCBENZs_00001 0.4 mL1,4-Dioxane 40 ug/mLSV14DIOXANEs_00002 0.2 mL2,6-Dichlorophenol 40 ug/mLSV26DCPHENOLs_00001 0.08 mL2,4,6-Tribromophenol 40 ug/mLSVACIDSURMIXs_00001 0.2 mL2-Fluorophenol 40 ug/mLPhenol-d5 40 ug/mL3,3'-Dichlorobenzidine 40 ug/mLSVBENZIDINEs_00008 0.2 mLBenzidine 40 ug/mL2-Fluorobiphenyl 40 ug/mLSVBNSURMIXs_00003 0.4 mLNitrobenzene-d5 40 ug/mLTerphenyl-d14 40 ug/mLAniline 40 ug/mLSVCALIBMIX4s_00002 0.2 mLBenzoic acid 40 ug/mLBenzyl alcohol 40 ug/mLPyridine 40 ug/mL1,1'-Biphenyl 40 ug/mLSVCLPOLM4MIXs_00003 0.2 mLAcetophenone 40 ug/mLAtrazine 40 ug/mLBenzaldehyde 40 ug/mLCaprolactam 40 ug/mL1,2,4-Trichlorobenzene 40 ug/mLSVCLPSVMIXs_00005 0.4 mL1,2-Dichlorobenzene 40 ug/mL1,2-Diphenylhydrazine 40 ug/mL1,3-Dichlorobenzene 40 ug/mL1,4-Dichlorobenzene 40 ug/mL2,2'-oxybis[1-chloropropane] 40 ug/mL2,4,5-Trichlorophenol 40 ug/mL2,4,6-Trichlorophenol 40 ug/mL2,4-Dichlorophenol 40 ug/mL2,4-Dimethylphenol 40 ug/mL2,4-Dinitrophenol 40 ug/mL2,4-Dinitrotoluene 40 ug/mL2,6-Dinitrotoluene 40 ug/mL2-Chloronaphthalene 40 ug/mL2-Chlorophenol 40 ug/mL2-Methylnaphthalene 40 ug/mL2-Methylphenol 40 ug/mL2-Nitroaniline 40 ug/mL
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
2-Nitrophenol 40 ug/mL3-Nitroaniline 40 ug/mL4,6-Dinitro-2-methylphenol 40 ug/mL4-Bromophenyl phenyl ether 40 ug/mL4-Chloro-3-methylphenol 40 ug/mL4-Chloroaniline 40 ug/mL4-Chlorophenyl phenyl ether 40 ug/mL4-Nitroaniline 40 ug/mL4-Nitrophenol 40 ug/mLAcenaphthene 40 ug/mLAcenaphthylene 40 ug/mLAnthracene 40 ug/mLBenzo[a]anthracene 40 ug/mLBenzo[a]pyrene 40 ug/mLBenzo[b]fluoranthene 40 ug/mLBenzo[g,h,i]perylene 40 ug/mLBenzo[k]fluoranthene 40 ug/mLBis(2-chloroethoxy)methane 40 ug/mLBis(2-chloroethyl)ether 40 ug/mLBis(2-ethylhexyl) phthalate 40 ug/mLButyl benzyl phthalate 40 ug/mLCarbazole 40 ug/mLChrysene 40 ug/mLDi-n-butyl phthalate 40 ug/mLDi-n-octyl phthalate 40 ug/mLDibenz(a,h)anthracene 40 ug/mLDibenzofuran 40 ug/mLDiethyl phthalate 40 ug/mLDimethyl phthalate 40 ug/mLFluoranthene 40 ug/mLFluorene 40 ug/mLHexachlorobenzene 40 ug/mLHexachlorobutadiene 40 ug/mLHexachlorocyclopentadiene 40 ug/mLHexachloroethane 40 ug/mLIndeno[1,2,3-cd]pyrene 40 ug/mLIsophorone 40 ug/mLMethylphenol, 3 & 4 40 ug/mLN-Nitrosodi-n-propylamine 40 ug/mLN-Nitrosodimethylamine 40 ug/mLNaphthalene 40 ug/mLNitrobenzene 40 ug/mLPentachlorophenol 40 ug/mLPhenanthrene 40 ug/mLPhenol 40 ug/mLPyrene 40 ug/mLIndene 40 ug/mLSVINDENEs_00010 0.4 mLN-Nitrosodiphenylamine 40 ug/mLSVNNDIPHENAMs_00002 0.08 mL
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REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.: 180-15932-1TestAmerica Pittsburgh
Reagent IDExpDate Date
Prep DilutantUsed
ReagentFinalVolume
Parent Reagent
Reagent IDVolumeAdded ConcentrationAnalyte
SVNNITROPYROs_00001 0.4 mL N-Nitrosopyrrolidine 40 ug/mL01/31/13 (Purchased Reagent) 1-Methylnaphthalene 2000 ug/mLSupelco, Lot LB 879735..SV ADDON MIXs_00003
2,3,4,6-Tetrachlorophenol 2000 ug/mL2,3,5,6-Tetrachlorophenol 2000 ug/mL2-Naphthylamine 2000 ug/mL7,12-Dimethylbenz(a)anthracene 2000 ug/mLMethyl methanesulfonate 2000 ug/mL
09/09/13 (Purchased Reagent) 1,2,4,5-Tetrachlorobenzene 1000 ug/mLAbsolute Standards, Lot 090908..SV1245TCBENZs_0000110/31/16 (Purchased Reagent) 1,4-Dioxane 2000 ug/mLRestek, Lot A077490..SV14DIOXANEs_0000208/31/13 (Purchased Reagent) 2,6-Dichlorophenol 5000 ug/mLSupelco, Lot LB78166..SV26DCPHENOLs_0000101/31/13 (Purchased Reagent) 2,4,6-Tribromophenol 2000 ug/mLUltra Scientific, Lot CF-5141..SVACIDSURMIXs_00001
2-Fluorophenol 2000 ug/mLPhenol-d5 2000 ug/mL
01/27/13 (Purchased Reagent) 3,3'-Dichlorobenzidine 2000 ug/mLSupelco, Lot LB79050..SVBENZIDINEs_00008Benzidine 2000 ug/mL
08/30/13 (Purchased Reagent) 2-Fluorobiphenyl 1000 ug/mLUltra Scientific, Lot CG-2463..SVBNSURMIXs_00003Nitrobenzene-d5 1000 ug/mLTerphenyl-d14 1000 ug/mL
11/30/14 (Purchased Reagent) Aniline 2000 ug/mLSupelco, Lot LB88725..SVCALIBMIX4s_00002Benzoic acid 2000 ug/mLBenzyl alcohol 2000 ug/mLPyridine 2000 ug/mL
04/30/13 (Purchased Reagent) 1,1'-Biphenyl 2000 ug/mLSupelco, Lot LB73726..SVCLPOLM4MIXs_00003Acetophenone 2000 ug/mLAtrazine 2000 ug/mLBenzaldehyde 2000 ug/mLCaprolactam 2000 ug/mL
09/30/13 (Purchased Reagent) 1,2,4-Trichlorobenzene 1000 ug/mLSupelco, Lot lb78428..SVCLPSVMIXs_000051,2-Dichlorobenzene 1000 ug/mL1,2-Diphenylhydrazine 1000 ug/mL1,3-Dichlorobenzene 1000 ug/mL1,4-Dichlorobenzene 1000 ug/mL2,2'-oxybis[1-chloropropane] 1000 ug/mL2,4,5-Trichlorophenol 1000 ug/mL2,4,6-Trichlorophenol 1000 ug/mL2,4-Dichlorophenol 1000 ug/mL2,4-Dimethylphenol 1000 ug/mL2,4-Dinitrophenol 1000 ug/mL2,4-Dinitrotoluene 1000 ug/mL2,6-Dinitrotoluene 1000 ug/mL2-Chloronaphthalene 1000 ug/mL2-Chlorophenol 1000 ug/mL2-Methylnaphthalene 1000 ug/mL2-Methylphenol 1000 ug/mL2-Nitroaniline 1000 ug/mL2-Nitrophenol 1000 ug/mL3-Nitroaniline 1000 ug/mL4,6-Dinitro-2-methylphenol 1000 ug/mL
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