newtowncreek.infonewtowncreek.info/docs2/2 Remedial Investigation... · L1218042 Anchor QEA, LLC...

L1218042

Anchor QEA, LLC

120782-01.01

NEWTOWN CREEK RI

Client:

Project Name:

Project Number:

11/05/12

320 Forbes Boulevard, Mansfield, MA 02048-1806

Lab Number:

Report Date:

508-822-9300 (Fax) 508-822-3288 800-624-9220 - www.alphalab.com

720 Olive Way

Suite 1900

Delaney PetersonATTN:

ANALYTICAL REPORT

Seattle, WA 98101

Certifications & Approvals: NY (11627), CT (PH-0141), NH (2206), NJ NELAP (MA015), RI (LAO00299), PA (68-02089), LA NELAP (03090),FL (E87814), TX (T104704419), WA (C954), DOD (L2217.01), USDA (Permit #P330-11-00109), US Army Corps of Engineers.

(206) 287-9130Phone:

The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in itsentirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.

Serial_No:11051209:46

of 279

L1218042-01

L1218042-02

L1218042-03

L1218042-04

L1218042-05

L1218042-06

L1218042-07

L1218042-08

L1218042-09

L1218042-10

L1218042-11

L1218042-12

L1218042-13

L1218042-14

L1218042-15

L1218042-16

L1218042-17

L1218042-18

L1218042-19

L1218042-20

L1218042-21

L1218042-22

L1218042-23

L1218042-24

L1218042-25

L1218042-26

L1218042-27

L1218042-28

L1218042-29

L1218042-30

L1218042-31

Alpha Sample ID

TN005SG-000014-20121005

TN005SG-000014-20121005

TN002SG-000011-20121005

TN002SG-000011-20121005

TN003SG-000015-20121005

TN003SG-000015-20121005

TN004SG-000015-20121005

TN004SG-000015-20121005

TN006SG-000015-20121005

TN006SG-000015-20121005

SG-RB-20121006

SG-RB-20121006

HB008SG-000015-20121006

HB008SG-000015-20121006

HB007SG-000015-20121006

HB007SG-000015-20121006

HB006SG-000015-20121006

HB006SG-000015-20121006

HB005SG-000015-20121006

HB005SG-000015-20121006

HB1005SG-000015-20121006

HB1005SG-000015-20121006

HB004SG-000015-20121006

HB004SG-000015-20121006

HB003SG-000015-20121006

HB003SG-000015-20121006

HB002SG-000015-20121006

HB002SG-000015-20121006

HB001SG-000015-20121006

HB001SG-000015-20121006

SG-TB-20121006

Client ID

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Not Specified

Sample Location

NEWTOWN CREEK RI

120782-01.01

Project Name:Project Number:

Lab Number: Report Date:

L121804211/05/12

10/05/12 09:32

10/05/12 09:32

10/05/12 10:41

10/05/12 10:41

10/05/12 11:24

10/05/12 11:24

10/05/12 11:46

10/05/12 11:46

10/05/12 13:16

10/05/12 13:16

10/06/12 09:05

10/06/12 09:05

10/06/12 09:55

10/06/12 09:55

10/06/12 10:45

10/06/12 10:45

10/06/12 11:30

10/06/12 11:30

10/06/12 12:19

10/06/12 12:19

10/06/12 12:19

10/06/12 12:19

10/06/12 13:27

10/06/12 13:27

10/06/12 14:21

10/06/12 14:21

10/06/12 15:05

10/06/12 15:05

10/06/12 15:54

10/06/12 15:54

10/06/12 16:23

Collection Date/Time

Serial_No:11051209:46

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L1218042-32

Alpha Sample ID

SRM 1650B

Client ID

Not Specified

Sample Location

10/06/12 12:00

Collection Date/Time

Serial_No:11051209:46

of 279

NEWTOWN CREEK RI

120782-01.01

Project Name:

Project Number:

Lab Number:

Report Date:L1218042

11/05/12

Case Narrative

The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation

or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report.

Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet all of the requirements of

NELAC, for all NELAC accredited parameters. The data presented in this report is organized by parameter (i.e. VOC, SVOC, etc.). Sample

specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list for each individual sample,

followed by the Laboratory Batch Quality Control at the end of each parameter. If a sample was re-analyzed or re-extracted due to a

required quality control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is

designated with an "R" or "RE", respectively. When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the

associated samples for each element are noted in the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific %

recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report. Performance criteria for CAM and RCP methods

allow for some LCS compound failures to occur and still be within method compliance. In these instances, the specific failures are not

narrated but are noted in the associated QC table. This information is also incorporated in the Data Usability format for our Data Merger tool

where it can be reviewed along with any associated usability implications. Soil/sediments, solids and tissues are reported on a dry weight

basis unless otherwise noted. Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary located at the

back of the report.

In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria for CAM and RCP methods allow for some

quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the

associated QC table. The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed

along with any associated usability implications.

Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical

Standards requested on the Chain of Custody.

HOLD POLICY

For samples submitted on hold, Alpha's policy is to hold samples free of charge for 30 days from the date the project is completed. After 30

days, we will dispose of all samples submitted including those put on hold unless you have contacted your Client Service Representative and

made arrangements for Alpha to continue to hold the samples.

Please contact Client Services at 800-624-9220 with any questions.

Serial_No:11051209:46

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Case Narrative (continued)

NEWTOWN CREEK RI

120782-01.01

Project Name:

Project Number:

Lab Number:


11/05/12

Volatile Organics

The WG566791-3/4 LCS/LCSD recoveries, associated with L1218042-01, -03, -05, -07, -09, -13, -15, -17,

-19, -21, -23, -25, -27 and -29, are above the individual acceptance criteria for Methylene Chloride (MSD @

153%), Vinyl chloride (MSD @ 134%) and Dichlorodifluoromethane (149%/161%), but within the overall method

allowances. Since all associated samples are non-detect for the affected compounds, no further action was

taken.

Alkylated PAHs

Concentrations for compounds flagged with "G" qualifiers may be biased high due to matrix interference

included in the quantitation.

L1218042-11 was re-analyzed due to quality control failures on the original analysis. The results of the re-

analysis have been reported.

The continuing calibration standard, WG568203-1, had %Ds above the acceptance criteria for Retene at

(29%D) and Benzo(b)fluorene at (29%D); however, they are within the method allowances, therefore no further

action was required.

Saturated Hydrocarbons

The results for n-Octadecane (C18) and n-Nonacosane (C29) are "C" qualified on all detectable results in all

samples, as well as the WG566066-1 Method Blank, due to the positive bias determined to be present in the

samples caused by the co-elution with laboratory standards (i.e. PAH surrogates and/or internal standards).

Concentrations for compounds flagged with "G" qualifiers may be biased high due to matrix interference

included in the quantitation.

Serial_No:11051209:46

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NEWTOWN CREEK RI

120782-01.01

Project Name:

Project Number:

Lab Number:


11/05/12

Total Metals

All sediment samples have elevated detection limits for all analytes due to the additional dilutions (10x/50x)

required by the elevated concentrations of target analytes in the samples.

All sediment samples were re-analyzed for Total Tin. In addition, L1218042-11 was re-analyzed for Total

Cobalt.

The WG568940-1 Method Blank, associated with all sediment samples, has a concentration above the

reporting limit for Total Vanadium. Since the associated sample concentrations are greater than 5x the blank

concentration for this analyte, no qualification of the results was performed.

The WG568938-4 MS recovery, performed on L1218042-01, is below the acceptance criteria for Total

Antimony (25%); however, the associated LCS/LCSD recoveries were within criteria.

The WG568940-4 MS recoveries, performed on L1218042-01, are above the acceptance criteria for Total

Aluminum (179%), Calcium (752%) and Iron (384%); however, the spikes do not apply because the sample

concentrations are greater than four times the spike amounts added.

The WG568940-3 Laboratory Duplicate RPDs, performed on L1218042-01, are outside the acceptance

criteria for Total Barium (112%), Cadmium (97%), Calcium (66%), Lead (93%), Selenium (129%) and Thallium

(138%). The elevated RPDs have been attributed to the non-homogeneous nature of the sample utilized for

the laboratory duplicate. In addition, the RPDs are above the acceptance criteria for Total Beryllium (54%) and

Zinc (26%); however, the sample and duplicate results are less than five times the reporting limit. Therefore,

the RPDs are valid.

Total Organic Carbon

All sediment samples were analyzed beyond the QAPP-defined holding time due to a lab oversight; however,

the analysis was performed within the internal laboratory 28-day holding time. In addition, all samples were in

Serial_No:11051209:46

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NEWTOWN CREEK RI

120782-01.01

Project Name:

Project Number:

Lab Number:


11/05/12

frozen storage until analysis. The data is released without further action.

The WG566725-3 Laboratory Duplicate RPD, performed on L1218042-01, is outside the acceptance criteria

for Total Organic Carbon-Rep 2 (26%). The elevated RPD has been attributed to the non-homogeneous

nature of the sample utilized for the laboratory duplicate.

Nitrate/Nitrite Nitrogen


for Nitrate/Nitrite Nitrogen (30%); however, the sample and duplicate results are less than five times the

reporting limit. Therefore, the RPD is valid.

Total Phosphorus

All samples have elevated detection limits due to the dilutions required to quantitate the results within the

calibration range.

The WG567984-3 MS recovery, performed on L1218042-29, is below the acceptance criteria for Total

Phosphorus (14%); however, the associated LCS is within criteria. The low recovery has been attributed to

sample matrix interference.

Sulfide

All samples have elevated detection limits due to the dilutions required to quantitate the results within the

calibration range.

The WG566113-4 MS recovery, performed on L1218042-07, is above the acceptance criteria for Sulfide

(390%); however, the spike does not apply because the sample concentration is greater than four times the

spike amount added.

Serial_No:11051209:46

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NEWTOWN CREEK RI

120782-01.01

Project Name:

Project Number:

Lab Number:


11/05/12


for Sulfide (33%). The elevated RPD has been attributed to the non-homogeneous nature of the sample

utilized for the laboratory duplicate.

Percent Soot

All sediment samples were analyzed beyond the QAPP-defined holding time due to a lab oversight; however,

the analysis was performed within the internal laboratory 28-day holding time. In addition, all samples were in

frozen storage until analysis. The data is released without further action.


for Percent Soot-Rep 1 (79%). The elevated RPD has been attributed to the non-homogeneous nature of the

sample utilized for the laboratory duplicate.

I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report.

Authorized Signature:

Title: Technical Director/Representative Date: 11/05/12

Serial_No:11051209:46

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ORGANICS

Serial_No:11051209:46

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VOLATILES

Serial_No:11051209:46

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FF

Methylene chloride

1,1-Dichloroethane

Chloroform

Carbon tetrachloride

1,2-Dichloropropane

Dibromochloromethane

1,1,2-Trichloroethane

Tetrachloroethene

Chlorobenzene

Trichlorofluoromethane

1,2-Dichloroethane


Bromodichloromethane

trans-1,3-Dichloropropene

cis-1,3-Dichloropropene

Bromoform

1,1,2,2-Tetrachloroethane

Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene

trans-1,2-Dichloroethene

Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

Methyl tert butyl ether

Parameter Result Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

Volatile Organics by GC/MS-5035 - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

14

2.1

2.1

1.4

4.9

1.4

2.1

1.4

1.4

7.0

1.4

1.4

1.4

1.4

1.4

5.6

1.4

1.4

2.1

1.4

7.0

2.8

2.8

2.8

1.4

2.1

1.4

7.0

7.0

7.0

2.8

11/05/12

TN005SG-000014-20121005Client ID:10/05/12 09:32Date Collected:10/08/12Date Received:

Not SpecifiedSample Location:

L1218042-01Lab ID:

Field Prep: Not SpecifiedMatrix: SedimentAnalytical Method:Analytical Date:Analyst:

1,8260C10/11/12 20:22BN 72%Percent Solids:

MDL

2.8

0.33

0.45

0.39

0.35

0.44

0.57

0.40

0.34

0.60

0.41

0.28

0.54

0.47

0.37

1.6

0.40

0.27

0.26

0.53

1.1

0.81

0.77

0.61

0.46

0.42

0.39

0.51

0.52

0.42

0.92

Serial_No:11051209:46

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p/m-Xylene

o-Xylene

cis-1,2-Dichloroethene

Styrene

Dichlorodifluoromethane

Acetone

Carbon disulfide

2-Butanone

Vinyl acetate

4-Methyl-2-pentanone

2-Hexanone

Bromochloromethane

1,2-Dibromoethane

1,2-Dibromo-3-chloropropane

Isopropylbenzene

1,2,3-Trichlorobenzene


Methyl Acetate

Cyclohexane

Methyl cyclohexane

Freon-113

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

ND

7.9

3.6

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

2.8

2.8

1.4

2.8

14

50

14

14

14

14

14

7.0

5.6

7.0

1.4

7.0

7.0

28

28

5.6

28

1,2-Dichloroethane-d4

Toluene-d8

4-Bromofluorobenzene

Dibromofluoromethane

105

97

99

103

70-130

70-130

70-130

70-130

Acceptance CriteriaSurrogate % Recovery Qualifier

11/05/12



L1218042-01Lab ID:

Field Prep: Not Specified

No Tentatively Identified Compounds ND ug/kg 1

Tentatively Identified Compounds

MDL

0.64

0.79

0.36

0.85

2.4

4.5

0.36

5.4

1.9

2.4

1.8

0.50

0.30

2.1

0.27

1.3

1.2

28.

28.

5.6

1.3

Serial_No:11051209:46

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Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

16

2.4

2.4

1.6

5.6

1.6

2.4

1.6

1.6

8.0

1.6

1.6

1.6

1.6

1.6

6.4

1.6

1.6

2.4

1.6

8.0

3.2

3.2

3.2

1.6

2.4

1.6

8.0

8.0

8.0

3.2

11/05/12



L1218042-03Lab ID:



MDL

3.2

0.38

0.52

0.45

0.40

0.52

0.66

0.47

0.40

0.70

0.47

0.33

0.62

0.54

0.43

1.8

0.47

0.31

0.30

0.61

1.3

0.94

0.89

0.71

0.53

0.48

0.45

0.59

0.61

0.49

1.1

Serial_No:11051209:46

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p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

Methyl cyclohexane

Freon-113

Parameter Result

J

J

J

Dilution Factor

ND

ND

ND

ND

ND

33

9.5

6.6

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

3.2

3.2

1.6

3.2

16

58

16

16

16

16

16

8.0

6.4

8.0

1.6

8.0

8.0

32

32

6.4

32


Toluene-d8



105

96

101

103

70-130

70-130

70-130

70-130


11/05/12



L1218042-03Lab ID:


Dimethyl sulfide NJ9.1 ug/kg 1


MDL

0.74

0.92

0.41

0.99

2.8

5.2

0.41

6.2

2.2

2.8

2.0

0.58

0.34

2.4

0.31

1.5

1.4

32.

32.

6.4

1.5

Serial_No:11051209:46

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Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

22

3.3

3.3

2.2

7.7

2.2

3.3

2.2

2.2

11

2.2

2.2

2.2

2.2

2.2

8.8

2.2

2.2

3.3

2.2

11

4.4

4.4

4.4

2.2

3.3

2.2

11

11

11

4.4

11/05/12



L1218042-05Lab ID:



MDL

4.4

0.52

0.71

0.61

0.55

0.70

0.90

0.64

0.54

0.96

0.64

0.44

0.84

0.74

0.59

2.4

0.63

0.42

0.42

0.83

1.7

1.3

1.2

0.96

0.73

0.66

0.62

0.80

0.83

0.67

1.4

Serial_No:11051209:46

of 279

p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

Methyl cyclohexane

Freon-113

Parameter Result

J

J

J

Dilution Factor

ND

ND

ND

ND

ND

70

11

14

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

4.4

4.4

2.2

4.4

22

79

22

22

22

22

22

11

8.8

11

2.2

11

11

44

44

8.8

44


Toluene-d8



104

96

103

104

70-130

70-130

70-130

70-130


11/05/12



L1218042-05Lab ID:


Dimethyl sulfide NJ12 ug/kg 1


MDL

1.0

1.2

0.56

1.3

3.8

7.1

0.56

8.5

3.0

3.9

2.8

0.78

0.47

3.2

0.42

2.0

1.9

44.

44.

8.8

2.0

Serial_No:11051209:46

of 279

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

19

2.8

2.8

1.9

6.7

1.9

2.8

1.9

1.9

9.5

1.9

1.9

1.9

1.9

1.9

7.6

1.9

1.9

2.8

1.9

9.5

3.8

3.8

3.8

1.9

2.8

1.9

9.5

9.5

9.5

3.8

11/05/12



L1218042-07Lab ID:



MDL

3.8

0.45

0.62

0.53

0.48

0.61

0.78

0.55

0.47

0.83

0.56

0.39

0.73

0.64

0.51

2.1

0.55

0.37

0.36

0.72

1.5

1.1

1.0

0.84

0.63

0.57

0.54

0.69

0.72

0.58

1.2

Serial_No:11051209:46

of 279

p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

Methyl cyclohexane

Freon-113

Parameter Result

J

J

J

Dilution Factor

ND

ND

ND

ND

ND

57

14

11

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

3.8

3.8

1.9

3.8

19

68

19

19

19

19

19

9.5

7.6

9.5

1.9

9.5

9.5

38

38

7.6

38


Toluene-d8



105

96

102

104

70-130

70-130

70-130

70-130


11/05/12



L1218042-07Lab ID:




MDL

0.87

1.1

0.49

1.2

3.3

6.2

0.49

7.4

2.6

3.4

2.4

0.68

0.41

2.8

0.37

1.8

1.6

38.

38.

7.6

1.8

Serial_No:11051209:46

of 279

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

12

1.8

1.8

1.2

4.1

1.2

1.8

1.2

1.2

5.8

1.2

1.2

1.2

1.2

1.2

4.7

1.2

1.2

1.8

1.2

5.8

2.3

2.3

2.3

1.2

1.8

1.2

5.8

5.8

5.8

2.3

11/05/12



L1218042-09Lab ID:



MDL

2.3

0.28

0.38

0.32

0.29

0.37

0.48

0.34

0.29

0.51

0.34

0.24

0.45

0.39

0.31

1.3

0.34

0.22

0.22

0.44

0.92

0.68

0.65

0.51

0.39

0.35

0.33

0.42

0.44

0.36

0.77

Serial_No:11051209:46

of 279

p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

Methyl cyclohexane

Freon-113

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

0.88

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

2.3

2.3

1.2

2.3

12

42

12

12

12

12

12

5.8

4.7

5.8

1.2

5.8

5.8

23

23

4.7

23


Toluene-d8



104

96

99

104

70-130

70-130

70-130

70-130


11/05/12



L1218042-09Lab ID:




MDL

0.53

0.66

0.30

0.72

2.0

3.8

0.30

4.5

1.6

2.1

1.5

0.42

0.25

1.7

0.22

1.1

1.0

23.

23.

4.7

1.1

Serial_No:11051209:46

of 279

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

Volatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

3.0

0.75

0.75

0.50

1.8

0.50

0.75

0.50

0.50

2.5

0.50

0.50

0.50

0.50

0.50

2.0

0.50

0.50

0.75

0.50

2.5

1.0

1.0

1.0

0.50

0.75

0.50

2.5

2.5

2.5

1.0

11/05/12

SG-RB-20121006Client ID:10/06/12 09:05Date Collected:10/08/12Date Received:


L1218042-11Lab ID:

Field Prep: Not SpecifiedMatrix: WaterAnalytical Method:Analytical Date:Analyst:

1,8260C10/17/12 10:01PD

MDL

0.54

0.22

0.20

0.16

0.30

0.19

0.26

0.18

0.19

0.27

0.16

0.16

0.19

0.16

0.14

0.25

0.19

0.19

0.23

0.26

0.28

0.26

0.22

0.23

0.18

0.21

0.17

0.18

0.19

0.22

0.16

Serial_No:11051209:46

of 279

p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

Freon-113

Methyl cyclohexane

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

2.2

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

1.0

1.0

0.50

1.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

2.5

2.0

2.5

0.50

2.5

2.5

10

10

10

10


Toluene-d8



106

100

123

98

70-130

70-130

70-130

70-130


11/05/12



L1218042-11Lab ID:


Unknown1 J1.1 ug/l 1


MDL

0.35

0.33

0.19

0.36

0.30

1.6

0.30

1.9

0.31

0.42

0.58

0.33

0.32

0.33

0.19

0.23

0.22

10.

0.24

0.23

0.29

Serial_No:11051209:46

of 279

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

35

5.3

5.3

3.5

12

3.5

5.3

3.5

3.5

18

3.5

3.5

3.5

3.5

3.5

14

3.5

3.5

5.3

3.5

18

7.1

7.1

7.1

3.5

5.3

3.5

18

18

18

7.1

11/05/12

HB008SG-000015-20121006Client ID:10/06/12 09:55Date Collected:10/08/12Date Received:


L1218042-13Lab ID:



MDL

7.1

0.83

1.1

0.98

0.89

1.1

1.4

1.0

0.87

1.5

1.0

0.72

1.4

1.2

0.94

3.9

1.0

0.68

0.67

1.3

2.8

2.0

2.0

1.6

1.2

1.1

0.99

1.3

1.3

1.1

2.3

Serial_No:11051209:46

of 279

p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

Methyl cyclohexane

Freon-113

Parameter Result

J

J

Dilution Factor

ND

ND

ND

ND

ND

130

22

32

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

7.1

7.1

3.5

7.1

35

130

35

35

35

35

35

18

14

18

3.5

18

18

71

71

14

71


Toluene-d8



108

99

107

106

70-130

70-130

70-130

70-130


11/05/12



L1218042-13Lab ID:




MDL

1.6

2.0

0.90

2.2

6.1

11.

0.91

14.

4.8

6.2

4.4

1.3

0.76

5.2

0.68

3.3

3.1

71.

71.

14.

3.3

Serial_No:11051209:46

of 279

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

37

5.6

5.6

3.7

13

3.7

5.6

3.7

3.7

18

3.7

3.7

3.7

3.7

3.7

15

3.7

3.7

5.6

3.7

18

7.4

7.4

7.4

3.7

5.6

3.7

18

18

18

7.4

11/05/12



L1218042-15Lab ID:



MDL

7.4

0.87

1.2

1.0

0.93

1.2

1.5

1.1

0.92

1.6

1.1

0.75

1.4

1.2

0.99

4.1

1.1

0.71

0.70

1.4

2.9

2.2

2.1

1.6

1.2

1.1

1.0

1.4

1.4

1.1

2.4

Serial_No:11051209:46

of 279

p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

Methyl cyclohexane

Freon-113

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

240

20

54

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

7.4

7.4

3.7

7.4

37

130

37

37

37

37

37

18

15

18

3.7

18

18

74

74

15

74


Toluene-d8



107

100

111

104

70-130

70-130

70-130

70-130


11/05/12



L1218042-15Lab ID:




MDL

1.7

2.1

0.95

2.3

6.4

12.

0.95

14.

5.1

6.6

4.7

1.3

0.80

5.5

0.72

3.4

3.2

74.

74.

15.

3.5

Serial_No:11051209:46

of 279

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

28

4.2

4.2

2.8

9.8

2.8

4.2

2.8

2.8

14

2.8

2.8

2.8

2.8

2.8

11

2.8

2.8

4.2

2.8

14

5.6

5.6

5.6

2.8

4.2

2.8

14

14

14

5.6

11/05/12



L1218042-17Lab ID:



MDL

5.6

0.66

0.91

0.78

0.70

0.90

1.2

0.81

0.69

1.2

0.82

0.57

1.1

0.94

0.75

3.1

0.81

0.54

0.53

1.1

2.2

1.6

1.6

1.2

0.93

0.84

0.79

1.0

1.0

0.86

1.8

Serial_No:11051209:46

of 279

p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

Methyl cyclohexane

Freon-113

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

270

6.8

60

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

5.6

5.6

2.8

5.6

28

100

28

28

28

28

28

14

11

14

2.8

14

14

56

56

11

56


Toluene-d8



103

99

106

104

70-130

70-130

70-130

70-130


11/05/12



L1218042-17Lab ID:




MDL

1.3

1.6

0.72

1.7

4.8

9.1

0.72

11.

3.8

5.0

3.5

1.0

0.60

4.2

0.54

2.6

2.4

56.

56.

11.

2.6

Serial_No:11051209:46

of 279

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

38

5.6

5.6

3.8

13

3.8

5.6

3.8

3.8

19

3.8

3.8

3.8

3.8

3.8

15

3.8

3.8

5.6

3.8

19

7.5

7.5

7.5

3.8

5.6

3.8

19

19

19

7.5

11/05/12



L1218042-19Lab ID:



MDL

7.5

0.89

1.2

1.0

0.95

1.2

1.5

1.1

0.93

1.6

1.1

0.76

1.4

1.3

1.0

4.2

1.1

0.72

0.72

1.4

3.0

2.2

2.1

1.6

1.2

1.1

1.1

1.4

1.4

1.2

2.5

Serial_No:11051209:46

of 279

p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

Methyl cyclohexane

Freon-113

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

580

16

120

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

7.5

7.5

3.8

7.5

38

140

38

38

38

38

38

19

15

19

3.8

19

19

75

75

15

75


Toluene-d8



104

98

106

105

70-130

70-130

70-130

70-130


11/05/12



L1218042-19Lab ID:




MDL

1.7

2.1

0.96

2.3

6.5

12.

0.97

15.

5.1

6.7

4.7

1.3

0.81

5.6

0.73

3.5

3.3

75.

75.

15.

3.5

Serial_No:11051209:46

of 279

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

36

5.4

5.4

3.6

13

3.6

5.4

3.6

3.6

18

3.6

3.6

3.6

3.6

3.6

14

3.6

3.6

5.4

3.6

18

7.2

7.2

7.2

3.6

5.4

3.6

18

18

18

7.2

11/05/12



L1218042-21Lab ID:



MDL

7.2

0.85

1.2

1.0

0.91

1.2

1.5

1.0

0.89

1.6

1.0

0.73

1.4

1.2

0.96

4.0

1.0

0.69

0.68

1.4

2.8

2.1

2.0

1.6

1.2

1.1

1.0

1.3

1.4

1.1

2.4

Serial_No:11051209:46

of 279

p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

Methyl cyclohexane

Freon-113


ND

ND

ND

ND

ND

370

38

81

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

7.2

7.2

3.6

7.2

36

130

36

36

36

36

36

18

14

18

3.6

18

18

72

72

14

72


Toluene-d8



104

99

106

105

70-130

70-130

70-130

70-130


11/05/12



L1218042-21Lab ID:




MDL

1.6

2.0

0.92

2.2

6.2

12.

0.93

14.

4.9

6.4

4.5

1.3

0.77

5.3

0.70

3.3

3.1

72.

72.

14.

3.4

Serial_No:11051209:46

of 279

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

26

3.9

3.9

2.6

9.0

2.6

3.9

2.6

2.6

13

2.6

2.6

2.6

2.6

2.6

10

2.6

2.6

3.9

2.6

13

5.2

5.2

5.2

2.6

3.9

2.6

13

13

13

5.2

11/05/12



L1218042-23Lab ID:



MDL

5.2

0.61

0.84

0.72

0.65

0.82

1.0

0.75

0.63

1.1

0.76

0.52

0.99

0.87

0.69

2.9

0.74

0.50

0.49

0.98

2.0

1.5

1.4

1.1

0.85

0.77

0.72

0.94

0.97

0.79

1.7

Serial_No:11051209:46

of 279

p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

Methyl cyclohexane

Freon-113

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

160

16

36

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

5.2

5.2

2.6

5.2

26

93

26

26

26

26

26

13

10

13

2.6

13

13

52

52

10

52


Toluene-d8



106

98

106

103

70-130

70-130

70-130

70-130


11/05/12



L1218042-23Lab ID:




MDL

1.2

1.5

0.66

1.6

4.5

8.3

0.66

10.

3.5

4.6

3.2

0.92

0.55

3.8

0.50

2.4

2.2

52.

52.

10.

2.4

Serial_No:11051209:46

of 279

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

33

5.0

5.0

3.3

12

3.3

5.0

3.3

3.3

17

3.3

3.3

3.3

3.3

3.3

13

3.3

3.3

5.0

3.3

17

6.7

6.7

6.7

3.3

5.0

3.3

17

17

17

6.7

11/05/12



L1218042-25Lab ID:



MDL

6.7

0.78

1.1

0.93

0.84

1.1

1.4

0.97

0.82

1.4

0.98

0.68

1.3

1.1

0.89

3.7

0.96

0.64

0.63

1.3

2.6

1.9

1.8

1.5

1.1

1.0

0.94

1.2

1.2

1.0

2.2

Serial_No:11051209:46

of 279

p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

Methyl cyclohexane

Freon-113

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

420

14

91

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

6.7

6.7

3.3

6.7

33

120

33

33

33

33

33

17

13

17

3.3

17

17

67

67

13

67


Toluene-d8



106

99

109

105

70-130

70-130

70-130

70-130


11/05/12



L1218042-25Lab ID:




MDL

1.5

1.9

0.85

2.0

5.8

11.

0.86

13.

4.5

5.9

4.2

1.2

0.71

4.9

0.64

3.1

2.9

67.

67.

13.

3.1

Serial_No:11051209:46

of 279

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

28

4.2

4.2

2.8

9.8

2.8

4.2

2.8

2.8

14

2.8

2.8

2.8

2.8

2.8

11

2.8

2.8

4.2

2.8

14

5.6

5.6

5.6

2.8

4.2

2.8

14

14

14

5.6

11/05/12



L1218042-27Lab ID:



MDL

5.6

0.66

0.91

0.78

0.71

0.90

1.2

0.82

0.69

1.2

0.83

0.57

1.1

0.95

0.75

3.1

0.81

0.54

0.53

1.1

2.2

1.6

1.6

1.2

0.93

0.84

0.79

1.0

1.0

0.86

1.9

Serial_No:11051209:46

of 279

p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

Methyl cyclohexane

Freon-113

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

320

9.5

72

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

5.6

5.6

2.8

5.6

28

100

28

28

28

28

28

14

11

14

2.8

14

14

56

56

11

56


Toluene-d8



104

97

105

103

70-130

70-130

70-130

70-130


11/05/12



L1218042-27Lab ID:




MDL

1.3

1.6

0.72

1.7

4.9

9.1

0.72

11.

3.8

5.0

3.5

1.0

0.60

4.2

0.54

2.6

2.4

56.

56.

11.

2.6

Serial_No:11051209:46

of 279

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

33

4.9

4.9

3.3

12

3.3

4.9

3.3

3.3

16

3.3

3.3

3.3

3.3

3.3

13

3.3

3.3

4.9

3.3

16

6.6

6.6

6.6

3.3

4.9

3.3

16

16

16

6.6

11/05/12



L1218042-29Lab ID:



MDL

6.6

0.77

1.1

0.92

0.83

1.0

1.4

0.95

0.81

1.4

0.96

0.67

1.3

1.1

0.88

3.7

0.95

0.63

0.62

1.2

2.6

1.9

1.8

1.4

1.1

0.99

0.92

1.2

1.2

1.0

2.2

Serial_No:11051209:46

of 279

p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

Methyl cyclohexane

Freon-113

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

410

7.8

97

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

6.6

6.6

3.3

6.6

33

120

33

33

33

33

33

16

13

16

3.3

16

16

66

66

13

66


Toluene-d8



103

97

105

104

70-130

70-130

70-130

70-130


11/05/12



L1218042-29Lab ID:




MDL

1.5

1.9

0.84

2.0

5.7

11.

0.84

13.

4.5

5.8

4.1

1.2

0.70

4.9

0.64

3.0

2.8

66.

66.

13.

3.1

Serial_No:11051209:46

of 279

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene



ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

3.0

0.75

0.75

0.50

1.8

0.50

0.75

0.50

0.50

2.5

0.50

0.50

0.50

0.50

0.50

2.0

0.50

0.50

0.75

0.50

2.5

1.0

1.0

1.0

0.50

0.75

0.50

2.5

2.5

2.5

1.0

11/05/12

SG-TB-20121006Client ID:10/06/12 16:23Date Collected:10/08/12Date Received:


L1218042-31Lab ID:

Field Prep: Not SpecifiedMatrix: WaterAnalytical Method:Analytical Date:Analyst:

1,8260C10/17/12 10:36PD

MDL

0.54

0.22

0.20

0.16

0.30

0.19

0.26

0.18

0.19

0.27

0.16

0.16

0.19

0.16

0.14

0.25

0.19

0.19

0.23

0.26

0.28

0.26

0.22

0.23

0.18

0.21

0.17

0.18

0.19

0.22

0.16

Serial_No:11051209:46

of 279

p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

Freon-113

Methyl cyclohexane

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

2.4

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

1.0

1.0

0.50

1.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

2.5

2.0

2.5

0.50

2.5

2.5

10

10

10

10


Toluene-d8



107

101

123

98

70-130

70-130

70-130

70-130


11/05/12

SG-TB-20121006Client ID:10/06/12 16:23Date Collected:10/08/12Date Received:


L1218042-31Lab ID:


No Tentatively Identified Compounds ND ug/l 1


MDL

0.35

0.33

0.19

0.36

0.30

1.6

0.30

1.9

0.31

0.42

0.58

0.33

0.32

0.33

0.19

0.23

0.22

10.

0.24

0.23

0.29

Serial_No:11051209:46

of 279

Method Blank AnalysisBatch Quality Control

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

10/11/12 18:171,8260CAnalytical Method:

Analytical Date:

11/05/12

Analyst: BN

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

Parameter Result

4.2

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

10

1.5

1.5

1.0

3.5

1.0

1.5

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

4.0

1.0

1.0

1.5

1.0

5.0

2.0

2.0

2.0

1.0

1.5

1.0

5.0

5.0

5.0

J ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

Volatile Organics by GC/MS-5035 - Westborough Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566791-5

MDL

2.0

0.24

0.32

0.28

0.25

0.32

0.41

0.29

0.25

0.44

0.29

0.20

0.38

0.34

0.27

1.1

0.29

0.19

0.19

0.38

0.78

0.58

0.55

0.44

0.33

0.30

0.28

0.36

0.38

0.30

Serial_No:11051209:46

of 279


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042


Analytical Date:

11/05/12

Analyst: BN


p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

Methyl cyclohexane

Freon-113

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

2.0

2.0

2.0

1.0

2.0

10

36

10

10

10

10

10

5.0

4.0

5.0

1.0

5.0

5.0

20

20

4.0

20

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier


No Tentatively Identified Compounds ND ug/kg


MDL

0.66

0.46

0.57

0.26

0.61

1.7

3.2

0.26

3.9

1.4

1.8

1.2

0.36

0.21

1.5

0.19

0.92

0.87

20.

20.

4.0

0.93

Serial_No:11051209:46

of 279


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042


Analytical Date:

11/05/12

Analyst: BN

Parameter Result RLUnitsQualifier



Toluene-d8



104

96

100

103

70-130

70-130

70-130

70-130

Surrogate %Recovery QualifierAcceptance

Criteria

MDL

Serial_No:11051209:46

of 279


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042


Analytical Date:

11/05/12

Analyst: PD

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

3.0

0.75

0.75

0.50

1.8

0.50

0.75

0.50

0.50

2.5

0.50

0.50

0.50

0.50

0.50

2.0

0.50

0.50

0.75

0.50

2.5

1.0

1.0

1.0

0.50

0.75

0.50

2.5

2.5

2.5

1.0

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier

Volatile Organics by GC/MS - Westborough Lab for sample(s): 11,31 Batch: WG567640-5

MDL

0.54

0.22

0.20

0.16

0.30

0.19

0.26

0.18

0.19

0.27

0.16

0.16

0.19

0.16

0.14

0.25

0.19

0.19

0.23

0.26

0.28

0.26

0.22

0.23

0.18

0.21

0.17

0.18

0.19

0.22

0.16

Serial_No:11051209:46

of 279


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042


Analytical Date:

11/05/12

Analyst: PD

p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

Freon-113

Methyl cyclohexane

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

1.0

1.0

0.50

1.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

2.5

2.0

2.5

0.50

2.5

2.5

10

10

10

10

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

ug/l

UnitsQualifier


No Tentatively Identified Compounds ND ug/l


MDL

0.35

0.33

0.19

0.36

0.30

1.6

0.30

1.9

0.31

0.42

0.58

0.33

0.32

0.33

0.19

0.23

0.22

10.

0.24

0.23

0.29

Serial_No:11051209:46

of 279


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042


Analytical Date:

11/05/12

Analyst: PD

Parameter Result RLUnitsQualifier



Toluene-d8



105

102

123

98

70-130

70-130

70-130

70-130


Criteria

MDL

Serial_No:11051209:46

of 279

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

123

105

106

106

103

96

99

95

96

111

110

107

103

96

102

92

96

102

94

95

153

112

114

115

108

101

104

104

102

125

113

115

109

100

107

94

96

110

100

102

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-139

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

22

6

7

8

5

5

5

9

6

12

3

7

6

4

5

2

0

8

6

7

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery

Limits RPD RPD Limits

Volatile Organics by GC/MS-5035 - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566791-3 WG566791-4

Lab Control Sample AnalysisBatch Quality Control

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

Qual Qual

Q

Qual

Serial_No:11051209:46

of 279

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate

118

97

124

128

109

105

105

94

92

94

107

94

96

105

95

149

126

105

110

104

127

102

134

138

119

115

113

96

97

97

110

101

101

111

100

161

126

115

111

106

52-130

57-147

67-130

50-151

65-135

70-130

70-130

70-130

70-130

70-130

66-130

70-130

70-130

70-130

70-130

30-146

54-140

59-130

70-130

70-130

7

5

8

8

9

9

7

2

5

3

3

7

5

6

5

8

0

9

1

2

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

Qual Qual

Q

Q

Q

Qual

Serial_No:11051209:46

of 279


2-Hexanone

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

Methyl cyclohexane

1,1,2-Trichloro-1,2,2-Trifluoroethane

103

98

113

100

93

91

91

91

105

102

102

112

104

97

120

103

100

98

94

94

104

111

111

123

70-130

70-130

70-130

70-130

68-130

70-130

70-130

70-130

65-130

70-130

70-130

70-130

1

1

6

3

7

7

3

3

1

8

8

9

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042


Toluene-d8



104

96

97

106

70-130

70-130

70-130

70-130

105

97

96

104

Surrogate Qual%Recovery Qual%RecoveryLCS LCSD

11/05/12

AcceptanceCriteria

Qual Qual Qual

Serial_No:11051209:46

of 279

Methylene chloride

1,1-Dichloroethane

Chloroform


1,2-Dichloropropane



Tetrachloroethene

Chlorobenzene


1,2-Dichloroethane





Bromoform


Benzene

Toluene

Ethylbenzene

Chloromethane

100

99

98

68

97

78

97

100

98

101

99

80

91

75

76

86

104

98

98

99

93

96

95

95

74

96

82

98

95

94

93

97

84

94

81

81

92

103

93

94

95

109

70-130

70-130

70-130

63-132

70-130

63-130

70-130

70-130

75-130

62-150

70-130

67-130

67-130

70-130

70-130

54-136

67-130

70-130

70-130

70-130

64-130

4

4

3

8

1

5

1

5

4

8

2

5

3

8

6

7

1

5

4

4

16

20

20

20

20

20

20

20

20

25

20

20

20

20

20

20

20

20

25

25

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 11,31 Batch: WG567640-3 WG567640-4


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

Qual Qual Qual

Serial_No:11051209:46

of 279

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene


Trichloroethene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


p/m-Xylene

o-Xylene


Styrene


Acetone

Carbon disulfide

2-Butanone

Vinyl acetate


2-Hexanone

112

94

94

97

97

97

98

100

96

83

97

98

97

87

91

105

101

99

77

86

99

132

92

92

93

90

93

95

96

93

89

94

97

88

87

86

107

88

100

86

92

105

39-139

55-140

55-138

61-145

70-130

70-130

70-130

70-130

70-130

63-130

70-130

70-130

70-130

70-130

36-147

58-148

51-130

63-138

70-130

59-130

57-130

16

2

2

4

7

4

3

4

3

7

3

1

10

0

6

2

14

1

11

7

6

20

20

20

25

20

25

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

Qual Qual Qual

Serial_No:11051209:46

of 279

Bromochloromethane

1,2-Dibromoethane


Isopropylbenzene



Methyl Acetate

Cyclohexane

1,1,2-Trichloro-1,2,2-Trifluoroethane

Methyl cyclohexane

96

100

80

90

87

85

94

104

101

106

93

102

88

87

90

89

100

98

94

96

70-130

70-130

41-144

70-130

70-130

70-130

70-130

70-130

70-130

70-130

3

2

10

3

3

5

6

6

7

10

20

20

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042


Toluene-d8



102

100

107

99

70-130

70-130

70-130

70-130

101

100

103

99


11/05/12

AcceptanceCriteria

Qual Qual Qual

Serial_No:11051209:46

of 279

SEMIVOLATILES

Serial_No:11051209:46

of 279

FF

cis/trans-Decalin

C1-Decalin

C2-Decalin

C3-Decalin

C4-Decalin

Naphthalene

C1-Naphthalenes

C2-Naphthalenes

C3-Naphthalenes

C4-Naphthalenes

2-Methylnaphthalene

1-Methylnaphthalene

Benzothiophene

C1-Benzo(b)thiophene




2,6-Dimethylnaphthalene

Acenaphthylene

Acenaphthene

2,3,5-Trimethylnaphthalene

Fluorene

C1-Fluorenes

C2-Fluorenes

C3-Fluorenes

Dibenzothiophene

4-Methyldibenzothiophene

2,3-Methyldibenzothiophene


C1-Dibenzothiophenes


Parameter Result

J

J

Dilution Factor

ND

3.59

13.6

19.6

36.1

76.5

48.2

53.0

41.8

31.8

55.7

26.0

3.58

6.15

8.53

13.6

9.20

28.7

209

26.9

6.78

34.4

44.3

66.8

82.8

27.4

19.4

27.6

6.30

61.3

95.6

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

PAHs - Mansfield Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

2.59

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

11/05/12



L1218042-01Lab ID:

Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:

Cleanup Method1:Analytical Method:Analytical Date:Analyst:

1,8270D-SIM(M)10/17/12 14:00MT

ALPHA OP-013

EPA 3611BExtraction Date: 10/12/12 12:37

Cleanup Date1: 10/16/12 72%Percent Solids:

MDL

1.30

1.30

1.30

1.30

1.30

1.49

1.49

1.49

1.49

1.49

1.34

1.63

1.62

1.62

1.62

1.62

1.62

1.23

0.989

0.914

0.848

1.38

1.38

1.38

1.38

1.43

1.43

1.43

1.43

1.43

1.43

Serial_No:11051209:46

of 279



Phenanthrene

2-Methylphenanthrene

2-Methylanthracene

9,4-Methylphenanthrene

C1-Phenanthrenes/anthracenes




Retene

Anthracene

Carbazole


Fluoranthene

Pyrene

C1-Pyrene/fluoranthenes

Benzonaphthothiophene

Benz(a)anthracene

Chrysene

C1-Benzanthracene/chrysenes




Benzo(b)fluoranthene

Benzo(j)+(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene

Perylene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)+(a,c)anthracene

Benzo(g,h,i)perylene


94.7

46.3

270

50.6

60.3

85.9

295

325

170

81.4

ND

161

17.6

56.4

526

1230

1360

190

506

534

713

396

174

75.8

460

555

513

891

146

400

132

414

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

5.18

Naphthalene-d8

Phenanthrene-d10

Benzo(a)pyrene-d12

76

95

88

50-130

50-130

50-130


11/05/12



L1218042-01Lab ID:


MDL

1.43

1.43

1.72

1.72

1.72

1.72

1.72

1.72

1.72

1.72

1.27

1.07

1.70

1.37

1.65

1.36

1.36

1.45

1.06

1.05

1.05

1.05

1.05

1.05

1.35

1.03

1.07

1.48

1.00

1.41

1.40

1.38

Serial_No:11051209:46

of 279

cis/trans-Decalin

C1-Decalin

C2-Decalin

C3-Decalin

C4-Decalin

Naphthalene

C1-Naphthalenes

C2-Naphthalenes

C3-Naphthalenes

C4-Naphthalenes

2-Methylnaphthalene

1-Methylnaphthalene

Benzothiophene






Acenaphthylene

Acenaphthene


Fluorene

C1-Fluorenes

C2-Fluorenes

C3-Fluorenes

Dibenzothiophene







5.24

8.83

30.8

47.0

79.4

183

134

168

136

98.7

157

72.5

8.62

14.1

19.6

29.4

24.7

89.8

633

92.9

20.8

89.5

152

228

217

75.7

70.4

66.9

20.0

184

329

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

2.23

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

11/05/12



L1218042-03Lab ID:



1,8270D-SIM(M)10/17/12 15:28MT

ALPHA OP-013



MDL

1.12

1.12

1.12

1.12

1.12

1.28

1.28

1.28

1.28

1.28

1.15

1.41

1.40

1.40

1.40

1.40

1.40

1.06

0.852

0.788

0.731

1.19

1.19

1.19

1.19

1.23

1.23

1.23

1.23

1.23

1.23

Serial_No:11051209:46

of 279



Phenanthrene


2-Methylanthracene






Retene

Anthracene

Carbazole


Fluoranthene

Pyrene



Benz(a)anthracene

Chrysene







Benzo(e)pyrene

Benzo(a)pyrene

Perylene





268

122

591

155

226

295

1010

1020

474

179

67.8

524

33.8

196

1410

2430

3430

507

1640

1730

2040

1110

496

207

1430

1470

1380

2540

441

1250

420

1270

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

4.47

Naphthalene-d8

Phenanthrene-d10

Benzo(a)pyrene-d12

69

89

91

50-130

50-130

50-130


11/05/12



L1218042-03Lab ID:


MDL

1.23

1.23

1.48

1.48

1.48

1.48

1.48

1.48

1.48

1.48

1.10

0.921

1.46

1.18

1.42

1.18

1.18

1.25

0.911

0.903

0.903

0.903

0.903

0.903

1.16

0.887

0.922

1.28

0.862

1.21

1.21

1.19

Serial_No:11051209:46

of 279

cis/trans-Decalin

C1-Decalin

C2-Decalin

C3-Decalin

C4-Decalin

Naphthalene

C1-Naphthalenes

C2-Naphthalenes

C3-Naphthalenes

C4-Naphthalenes

2-Methylnaphthalene

1-Methylnaphthalene

Benzothiophene






Acenaphthylene

Acenaphthene


Fluorene

C1-Fluorenes

C2-Fluorenes

C3-Fluorenes

Dibenzothiophene







9.65

17.8

59.3

93.3

167

338

241

323

253

172

272

138

15.6

27.1

38.4

54.3

38.6

176

1100

183

39.4

150

272

388

371

144

130

114

36.2

331

535

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

4.28

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

11/05/12



L1218042-05Lab ID:



1,8270D-SIM(M)10/17/12 16:58MT

ALPHA OP-013



MDL

2.15

2.15

2.15

2.15

2.15

2.46

2.46

2.46

2.46

2.46

2.21

2.70

2.68

2.68

2.68

2.68

2.68

2.03

1.63

1.51

1.40

2.28

2.28

2.28

2.28

2.36

2.36

2.36

2.36

2.36

2.36

Serial_No:11051209:46

of 279



Phenanthrene


2-Methylanthracene






Retene

Anthracene

Carbazole


Fluoranthene

Pyrene



Benz(a)anthracene

Chrysene







Benzo(e)pyrene

Benzo(a)pyrene

Perylene





433

214

1030

248

373

506

1720

1640

767

324

129

910

50.1

345

2380

3720

5360

811

2620

2790

3130

1680

789

324

2080

2330

2180

3970

743

2080

703

2060

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

8.56

Naphthalene-d8

Phenanthrene-d10

Benzo(a)pyrene-d12

65

87

90

50-130

50-130

50-130


11/05/12



L1218042-05Lab ID:


MDL

2.36

2.36

2.83

2.83

2.83

2.83

2.83

2.83

2.83

2.83

2.10

1.76

2.80

2.26

2.72

2.25

2.25

2.39

1.74

1.73

1.73

1.73

1.73

1.73

2.22

1.70

1.76

2.44

1.65

2.32

2.31

2.27

Serial_No:11051209:46

of 279

cis/trans-Decalin

C1-Decalin

C2-Decalin

C3-Decalin

C4-Decalin

Naphthalene

C1-Naphthalenes

C2-Naphthalenes

C3-Naphthalenes

C4-Naphthalenes

2-Methylnaphthalene

1-Methylnaphthalene

Benzothiophene






Acenaphthylene

Acenaphthene


Fluorene

C1-Fluorenes

C2-Fluorenes

C3-Fluorenes

Dibenzothiophene






Parameter Result

J

Dilution Factor

3.39

5.30

16.2

23.5

38.2

123

83.9

101

74.8

50.0

94.3

49.9

5.76

9.32

12.0

17.0

13.8

55.9

238

76.0

10.8

67.8

80.7

105

109

49.2

34.9

37.5

10.4

99.4

141

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

2.83

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

11/05/12



L1218042-07Lab ID:



1,8270D-SIM(M)10/17/12 18:26MT

ALPHA OP-013



MDL

1.42

1.42

1.42

1.42

1.42

1.62

1.62

1.62

1.62

1.62

1.46

1.78

1.77

1.77

1.77

1.77

1.77

1.34

1.08

0.996

0.924

1.51

1.51

1.51

1.51

1.56

1.56

1.56

1.56

1.56

1.56

Serial_No:11051209:46

of 279



Phenanthrene


2-Methylanthracene






Retene

Anthracene

Carbazole


Fluoranthene

Pyrene



Benz(a)anthracene

Chrysene







Benzo(e)pyrene

Benzo(a)pyrene

Perylene





123

61.5

465

83.7

97.3

142

505

459

243

94.5

53.1

267

40.8

104

827

1250

1490

240

772

822

876

468

213

104

624

700

611

1080

246

548

191

555

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

5.65

Naphthalene-d8

Phenanthrene-d10

Benzo(a)pyrene-d12

65

87

88

50-130

50-130

50-130


11/05/12



L1218042-07Lab ID:


MDL

1.56

1.56

1.87

1.87

1.87

1.87

1.87

1.87

1.87

1.87

1.39

1.16

1.85

1.49

1.80

1.49

1.49

1.58

1.15

1.14

1.14

1.14

1.14

1.14

1.47

1.12

1.17

1.61

1.09

1.53

1.53

1.50

Serial_No:11051209:46

of 279

cis/trans-Decalin

C1-Decalin

C2-Decalin

C3-Decalin

C4-Decalin

Naphthalene

C1-Naphthalenes

C2-Naphthalenes

C3-Naphthalenes

C4-Naphthalenes

2-Methylnaphthalene

1-Methylnaphthalene

Benzothiophene






Acenaphthylene

Acenaphthene


Fluorene

C1-Fluorenes

C2-Fluorenes

C3-Fluorenes

Dibenzothiophene






Parameter Result

J

J

J

J

J

J

G

Dilution Factor

ND

2.16

5.31

8.02

14.2

50.1

29.1

29.8

23.0

16.0

31.7

17.6

2.04

3.57

4.00

7.42

4.18

16.3

106

24.8

4.16

37.0

26.9

35.3

64.3

28.1

13.7

21.1

4.64

45.1

52.0

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

2.11

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

11/05/12



L1218042-09Lab ID:



1,8270D-SIM(M)10/17/12 21:22MT

ALPHA OP-013



MDL

1.06

1.06

1.06

1.06

1.06

1.21

1.21

1.21

1.21

1.21

1.09

1.33

1.32

1.32

1.32

1.32

1.32

1.00

0.805

0.744

0.690

1.12

1.12

1.12

1.12

1.16

1.16

1.16

1.16

1.16

1.16

Serial_No:11051209:46

of 279



Phenanthrene


2-Methylanthracene






Retene

Anthracene

Carbazole


Fluoranthene

Pyrene



Benz(a)anthracene

Chrysene







Benzo(e)pyrene

Benzo(a)pyrene

Perylene





40.8

18.9

427

66.6

26.8

59.3

250

172

81.3

35.3

ND

127

50.7

58.0

973

915

572

141

560

568

349

173

95.2

60.8

497

491

385

594

144

392

124

357

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

4.22

Naphthalene-d8

Phenanthrene-d10

Benzo(a)pyrene-d12

75

93

86

50-130

50-130

50-130


11/05/12



L1218042-09Lab ID:


MDL

1.16

1.16

1.40

1.40

1.40

1.40

1.40

1.40

1.40

1.40

1.04

0.870

1.38

1.11

1.34

1.11

1.11

1.18

0.860

0.853

0.853

0.853

0.853

0.853

1.10

0.837

0.870

1.20

0.814

1.14

1.14

1.12

Serial_No:11051209:46

of 279

cis/trans-Decalin

C1-Decalin

C2-Decalin

C3-Decalin

C4-Decalin

Naphthalene

C1-Naphthalenes

C2-Naphthalenes

C3-Naphthalenes

C4-Naphthalenes

2-Methylnaphthalene

1-Methylnaphthalene

Benzothiophene






Acenaphthylene

Acenaphthene


Fluorene

C1-Fluorenes

C2-Fluorenes

C3-Fluorenes

Dibenzothiophene






Parameter Result

J

J

J

J

J

J

J

Dilution Factor

3.02

ND

ND

ND

ND

70.8

17.9

6.65

4.58

ND

18.4

11.1

ND

ND

ND

ND

ND

ND

2.52

3.00

ND

7.38

ND

ND

ND

ND

ND

ND

ND

ND

ND

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

5.81

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11/05/12



L1218042-11Lab ID:

Field Prep: Not SpecifiedMatrix: Water Extraction Method:Analytical Method:Analytical Date:Analyst:

1,8270D-SIM(M)10/17/12 02:12MT

EPA 3510CExtraction Date: 10/10/12 07:46

MDL

2.51

2.51

2.51

2.51

2.51

2.73

2.73

2.73

2.73

2.73

1.55

1.88

2.89

2.89

2.89

2.89

2.89

3.25

2.44

1.56

2.21

2.53

2.53

2.53

2.53

1.66

1.66

1.66

1.66

1.66

1.66

Serial_No:11051209:46

of 279



Phenanthrene


2-Methylanthracene






Retene

Anthracene

Carbazole


Fluoranthene

Pyrene



Benz(a)anthracene

Chrysene







Benzo(e)pyrene

Benzo(a)pyrene

Perylene




Parameter Result

J

J

J

J

Dilution Factor

ND

ND

4.54

ND

ND

ND

ND

4.15

ND

ND

4.18

ND

ND

ND

ND

1.69

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

Naphthalene-d8

Phenanthrene-d10

Benzo(a)pyrene-d12

85

100

85

50-130

50-130

50-130


11/05/12



L1218042-11Lab ID:


MDL

1.66

1.66

2.76

2.76

2.76

2.76

2.76

2.76

2.76

2.76

2.63

2.17

5.33

4.04

3.05

1.05

1.05

1.37

3.08

1.88

1.88

1.88

1.88

1.88

1.30

2.98

1.91

4.94

3.39

2.11

2.53

1.90

Serial_No:11051209:46

of 279

cis/trans-Decalin

C1-Decalin

C2-Decalin

C3-Decalin

C4-Decalin

Naphthalene

C1-Naphthalenes

C2-Naphthalenes

C3-Naphthalenes

C4-Naphthalenes

2-Methylnaphthalene

1-Methylnaphthalene

Benzothiophene






Acenaphthylene

Acenaphthene


Fluorene

C1-Fluorenes

C2-Fluorenes

C3-Fluorenes

Dibenzothiophene






Parameter Result

J

J

G

J

Dilution Factor

25.3

17.6

62.4

70.3

126

47.2

35.7

95.8

40.8

46.9

37.7

18.3

ND

ND

11.2

24.0

ND

119

90.0

29.0

4.64

36.5

25.4

66.5

178

26.2

13.2

55.0

ND

78.3

89.8

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

7.30

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

11/05/12



L1218042-13Lab ID:



1,8270D-SIM(M)10/17/12 22:50MT

ALPHA OP-013



MDL

3.67

3.67

3.67

3.67

3.67

4.20

4.20

4.20

4.20

4.20

3.77

4.60

4.58

4.58

4.58

4.58

4.58

3.47

2.79

2.58

2.39

3.90

3.90

3.90

3.90

4.03

4.03

4.03

4.03

4.03

4.03

Serial_No:11051209:46

of 279



Phenanthrene


2-Methylanthracene






Retene

Anthracene

Carbazole


Fluoranthene

Pyrene



Benz(a)anthracene

Chrysene







Benzo(e)pyrene

Benzo(a)pyrene

Perylene





158

124

273

42.0

26.4

49.1

204

298

262

188

ND

139

41.4

40.1

1160

1290

700

208

559

798

513

485

449

326

1030

881

774

858

284

817

196

792

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

14.6

Naphthalene-d8

Phenanthrene-d10

Benzo(a)pyrene-d12

73

96

97

50-130

50-130

50-130


11/05/12



L1218042-13Lab ID:


MDL

4.03

4.03

4.84

4.84

4.84

4.84

4.84

4.84

4.84

4.84

3.58

3.01

4.78

3.86

4.64

3.84

3.84

4.09

2.98

2.95

2.95

2.95

2.95

2.95

3.80

2.90

3.01

4.17

2.82

3.96

3.95

3.88

Serial_No:11051209:46

of 279

cis/trans-Decalin

C1-Decalin

C2-Decalin

C3-Decalin

C4-Decalin

Naphthalene

C1-Naphthalenes

C2-Naphthalenes

C3-Naphthalenes

C4-Naphthalenes

2-Methylnaphthalene

1-Methylnaphthalene

Benzothiophene






Acenaphthylene

Acenaphthene


Fluorene

C1-Fluorenes

C2-Fluorenes

C3-Fluorenes

Dibenzothiophene






Parameter Result

J

J

G

J

Dilution Factor

29.2

20.7

72.6

79.0

150

54.6

40.2

130

50.6

55.9

42.8

20.5

ND

ND

15.0

29.8

ND

172

122

33.7

6.83

50.0

28.4

81.8

213

37.1

18.6

77.6

5.52

107

82.8

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

8.71

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

11/05/12



L1218042-15Lab ID:



1,8270D-SIM(M)10/18/12 00:18MT

ALPHA OP-013



MDL

4.37

4.37

4.37

4.37

4.37

5.01

5.01

5.01

5.01

5.01

4.49

5.49

5.46

5.46

5.46

5.46

5.46

4.14

3.32

3.07

2.85

4.65

4.65

4.65

4.65

4.80

4.80

4.80

4.80

4.80

4.80

Serial_No:11051209:46

of 279



Phenanthrene


2-Methylanthracene






Retene

Anthracene

Carbazole


Fluoranthene

Pyrene



Benz(a)anthracene

Chrysene







Benzo(e)pyrene

Benzo(a)pyrene

Perylene





136

110

366

55.6

32.0

60.4

259

347

255

177

ND

195

59.9

57.4

1900

1860

876

282

764

1070

553

430

473

393

1560

1190

1190

1290

384

1140

274

1130

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

17.4

Naphthalene-d8

Phenanthrene-d10

Benzo(a)pyrene-d12

70

91

98

50-130

50-130

50-130


11/05/12



L1218042-15Lab ID:


MDL

4.80

4.80

5.77

5.77

5.77

5.77

5.77

5.77

5.77

5.77

4.27

3.59

5.70

4.60

5.54

4.58

4.58

4.87

3.55

3.52

3.52

3.52

3.52

3.52

4.53

3.46

3.59

4.97

3.36

4.73

4.70

4.63

Serial_No:11051209:46

of 279

cis/trans-Decalin

C1-Decalin

C2-Decalin

C3-Decalin

C4-Decalin

Naphthalene

C1-Naphthalenes

C2-Naphthalenes

C3-Naphthalenes

C4-Naphthalenes

2-Methylnaphthalene

1-Methylnaphthalene

Benzothiophene






Acenaphthylene

Acenaphthene


Fluorene

C1-Fluorenes

C2-Fluorenes

C3-Fluorenes

Dibenzothiophene






Parameter Result

J

J

J

J

J

J

J

G

J

J

Dilution Factor

13.2

5.55

17.7

ND

ND

15.0

12.2

33.5

16.8

16.8

11.7

6.18

ND

ND

5.93

13.7

ND

40.8

26.1

9.33

ND

14.8

8.50

22.7

56.4

8.38

4.17

30.2

ND

39.5

18.0

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

6.16

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

11/05/12



L1218042-17Lab ID:



1,8270D-SIM(M)10/18/12 01:45MT

ALPHA OP-013



MDL

3.09

3.09

3.09

3.09

3.09

3.54

3.54

3.54

3.54

3.54

3.18

3.88

3.86

3.86

3.86

3.86

3.86

2.93

2.35

2.17

2.01

3.28

3.28

3.28

3.28

3.40

3.40

3.40

3.40

3.40

3.40

Serial_No:11051209:46

of 279



Phenanthrene


2-Methylanthracene






Retene

Anthracene

Carbazole


Fluoranthene

Pyrene



Benz(a)anthracene

Chrysene







Benzo(e)pyrene

Benzo(a)pyrene

Perylene




Parameter Result

J

J

J

Dilution Factor

25.5

21.1

86.1

13.2

6.75

13.0

59.4

53.3

45.2

35.8

8.32

40.4

11.9

13.5

337

328

164

54.2

136

205

99.6

72.7

89.3

98.5

262

204

187

209

161

194

48.9

198

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

12.3

Naphthalene-d8

Phenanthrene-d10

Benzo(a)pyrene-d12

71

99

92

50-130

50-130

50-130


11/05/12



L1218042-17Lab ID:


MDL

3.40

3.40

4.08

4.08

4.08

4.08

4.08

4.08

4.08

4.08

3.02

2.54

4.03

3.25

3.91

3.24

3.24

3.45

2.51

2.49

2.49

2.49

2.49

2.49

3.20

2.44

2.54

3.52

2.38

3.34

3.33

3.27

Serial_No:11051209:46

of 279

cis/trans-Decalin

C1-Decalin

C2-Decalin

C3-Decalin

C4-Decalin

Naphthalene

C1-Naphthalenes

C2-Naphthalenes

C3-Naphthalenes

C4-Naphthalenes

2-Methylnaphthalene

1-Methylnaphthalene

Benzothiophene






Acenaphthylene

Acenaphthene


Fluorene

C1-Fluorenes

C2-Fluorenes

C3-Fluorenes

Dibenzothiophene






Parameter Result

J

J

G

J

Dilution Factor

31.0

18.8

60.3

72.4

124

50.7

40.8

119

47.0

49.0

42.5

20.8

ND

ND

14.8

28.6

ND

152

102

27.2

6.05

45.2

24.8

66.7

205

30.4

14.6

56.0

ND

80.2

70.5

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

8.37

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

11/05/12



L1218042-19Lab ID:



1,8270D-SIM(M)10/18/12 03:12MT

ALPHA OP-013



MDL

4.20

4.20

4.20

4.20

4.20

4.81

4.81

4.81

4.81

4.81

4.32

5.27

5.24

5.24

5.24

5.24

5.24

3.98

3.19

2.95

2.74

4.46

4.46

4.46

4.46

4.61

4.61

4.61

4.61

4.61

4.61

Serial_No:11051209:46

of 279



Phenanthrene


2-Methylanthracene






Retene

Anthracene

Carbazole


Fluoranthene

Pyrene



Benz(a)anthracene

Chrysene







Benzo(e)pyrene

Benzo(a)pyrene

Perylene





108

93.6

302

45.1

24.9

50.2

219

282

213

143

ND

156

47.8

52.1

1420

1510

722

231

618

901

445

338

371

338

1250

1010

978

1070

324

974

236

950

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

16.7

Naphthalene-d8

Phenanthrene-d10

Benzo(a)pyrene-d12

71

92

102

50-130

50-130

50-130


11/05/12



L1218042-19Lab ID:


MDL

4.61

4.61

5.54

5.54

5.54

5.54

5.54

5.54

5.54

5.54

4.10

3.45

5.47

4.42

5.32

4.40

4.40

4.68

3.41

3.38

3.38

3.38

3.38

3.38

4.35

3.32

3.45

4.78

3.23

4.54

4.52

4.44

Serial_No:11051209:46

of 279

cis/trans-Decalin

C1-Decalin

C2-Decalin

C3-Decalin

C4-Decalin

Naphthalene

C1-Naphthalenes

C2-Naphthalenes

C3-Naphthalenes

C4-Naphthalenes

2-Methylnaphthalene

1-Methylnaphthalene

Benzothiophene






Acenaphthylene

Acenaphthene


Fluorene

C1-Fluorenes

C2-Fluorenes

C3-Fluorenes

Dibenzothiophene






Parameter Result

J

J

G

J

Dilution Factor

27.4

18.9

62.6

81.2

122

52.1

40.4

130

45.6

52.4

42.4

20.4

ND

ND

13.4

24.8

ND

177

100

27.3

4.00

43.2

26.9

71.5

189

31.4

15.3

66.6

4.72

89.4

68.7

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

7.55

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

11/05/12



L1218042-21Lab ID:



1,8270D-SIM(M)10/18/12 04:38MT

ALPHA OP-013



MDL

3.79

3.79

3.79

3.79

3.79

4.34

4.34

4.34

4.34

4.34

3.90

4.76

4.73

4.73

4.73

4.73

4.73

3.59

2.88

2.66

2.47

4.03

4.03

4.03

4.03

4.16

4.16

4.16

4.16

4.16

4.16

Serial_No:11051209:46

of 279



Phenanthrene


2-Methylanthracene






Retene

Anthracene

Carbazole


Fluoranthene

Pyrene



Benz(a)anthracene

Chrysene







Benzo(e)pyrene

Benzo(a)pyrene

Perylene





104

85.8

291

46.0

26.7

55.4

222

269

201

136

ND

159

49.1

47.2

1350

1430

680

222

585

817

429

329

322

265

1200

920

860

936

279

918

236

885

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

15.1

Naphthalene-d8

Phenanthrene-d10

Benzo(a)pyrene-d12

74

96

92

50-130

50-130

50-130


11/05/12



L1218042-21Lab ID:


MDL

4.16

4.16

5.00

5.00

5.00

5.00

5.00

5.00

5.00

5.00

3.71

3.11

4.94

3.99

4.80

3.97

3.97

4.23

3.08

3.05

3.05

3.05

3.05

3.05

3.93

3.00

3.12

4.31

2.92

4.10

4.08

4.01

Serial_No:11051209:46

of 279

cis/trans-Decalin

C1-Decalin

C2-Decalin

C3-Decalin

C4-Decalin

Naphthalene

C1-Naphthalenes

C2-Naphthalenes

C3-Naphthalenes

C4-Naphthalenes

2-Methylnaphthalene

1-Methylnaphthalene

Benzothiophene






Acenaphthylene

Acenaphthene


Fluorene

C1-Fluorenes

C2-Fluorenes

C3-Fluorenes

Dibenzothiophene






Parameter Result

J

J

G

J

J

Dilution Factor

19.1

11.7

34.4

36.6

66.3

29.6

23.6

82.5

28.2

26.2

24.9

12.2

ND

ND

8.88

16.8

ND

111

59.4

14.7

1.83

20.3

15.2

37.7

107

13.7

7.74

24.9

3.16

39.7

38.7

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

5.36

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

11/05/12



L1218042-23Lab ID:



1,8270D-SIM(M)10/18/12 06:04MT

ALPHA OP-013



MDL

2.69

2.69

2.69

2.69

2.69

3.08

3.08

3.08

3.08

3.08

2.76

3.38

3.36

3.36

3.36

3.36

3.36

2.55

2.04

1.89

1.75

2.86

2.86

2.86

2.86

2.96

2.96

2.96

2.96

2.96

2.96

Serial_No:11051209:46

of 279



Phenanthrene


2-Methylanthracene






Retene

Anthracene

Carbazole


Fluoranthene

Pyrene



Benz(a)anthracene

Chrysene







Benzo(e)pyrene

Benzo(a)pyrene

Perylene





51.8

47.7

163

25.8

14.0

28.5

125

143

110

83.7

ND

80.5

22.2

27.4

546

709

351

98.2

275

384

234

174

192

166

596

514

454

499

150

455

110

443

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

10.7

Naphthalene-d8

Phenanthrene-d10

Benzo(a)pyrene-d12

73

97

102

50-130

50-130

50-130


11/05/12



L1218042-23Lab ID:


MDL

2.96

2.96

3.55

3.55

3.55

3.55

3.55

3.55

3.55

3.55

2.63

2.21

3.50

2.83

3.40

2.82

2.82

3.00

2.18

2.17

2.17

2.17

2.17

2.17

2.79

2.13

2.21

3.06

2.07

2.91

2.90

2.85

Serial_No:11051209:46

of 279

cis/trans-Decalin

C1-Decalin

C2-Decalin

C3-Decalin

C4-Decalin

Naphthalene

C1-Naphthalenes

C2-Naphthalenes

C3-Naphthalenes

C4-Naphthalenes

2-Methylnaphthalene

1-Methylnaphthalene

Benzothiophene






Acenaphthylene

Acenaphthene


Fluorene

C1-Fluorenes

C2-Fluorenes

C3-Fluorenes

Dibenzothiophene






Parameter Result

J

J

J

G

J

Dilution Factor

30.6

11.9

40.0

34.4

72.6

46.1

36.4

102

39.9

34.9

38.5

18.9

ND

ND

9.70

22.8

ND

124

80.1

28.6

4.33

41.6

22.7

55.8

156

27.9

12.2

48.3

ND

69.1

52.7

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

7.43

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

11/05/12



L1218042-25Lab ID:



1,8270D-SIM(M)10/18/12 07:31MT

ALPHA OP-013



MDL

3.73

3.73

3.73

3.73

3.73

4.27

4.27

4.27

4.27

4.27

3.83

4.68

4.66

4.66

4.66

4.66

4.66

3.53

2.84

2.62

2.43

3.96

3.96

3.96

3.96

4.10

4.10

4.10

4.10

4.10

4.10

Serial_No:11051209:46

of 279



Phenanthrene


2-Methylanthracene






Retene

Anthracene

Carbazole


Fluoranthene

Pyrene



Benz(a)anthracene

Chrysene







Benzo(e)pyrene

Benzo(a)pyrene

Perylene





70.6

63.4

344

43.6

19.5

44.6

194

220

146

98.3

ND

125

48.6

43.7

1050

1140

543

169

475

666

345

247

283

269

890

782

737

826

245

708

177

704

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

14.9

Naphthalene-d8

Phenanthrene-d10

Benzo(a)pyrene-d12

71

93

102

50-130

50-130

50-130


11/05/12



L1218042-25Lab ID:


MDL

4.10

4.10

4.92

4.92

4.92

4.92

4.92

4.92

4.92

4.92

3.65

3.06

4.86

3.92

4.72

3.91

3.91

4.16

3.03

3.00

3.00

3.00

3.00

3.00

3.86

2.95

3.07

4.24

2.87

4.03

4.02

3.95

Serial_No:11051209:46

of 279

cis/trans-Decalin

C1-Decalin

C2-Decalin

C3-Decalin

C4-Decalin

Naphthalene

C1-Naphthalenes

C2-Naphthalenes

C3-Naphthalenes

C4-Naphthalenes

2-Methylnaphthalene

1-Methylnaphthalene

Benzothiophene






Acenaphthylene

Acenaphthene


Fluorene

C1-Fluorenes

C2-Fluorenes

C3-Fluorenes

Dibenzothiophene






Parameter Result

J

J

J

G

J

Dilution Factor

23.2

8.53

24.4

30.1

52.5

31.6

25.9

62.6

27.9

25.2

27.9

12.6

ND

ND

8.64

18.1

ND

74.1

50.9

13.1

2.99

20.8

15.3

37.7

98.7

14.2

7.86

26.4

ND

41.3

33.9

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

5.78

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11/05/12



L1218042-27Lab ID:



1,8270D-SIM(M)10/18/12 08:59MT

ALPHA OP-013



MDL

2.90

2.90

2.90

2.90

2.90

3.32

3.32

3.32

3.32

3.32

2.98

3.64

3.62

3.62

3.62

3.62

3.62

2.75

2.20

2.04

1.89

3.08

3.08

3.08

3.08

3.19

3.19

3.19

3.19

3.19

3.19

Serial_No:11051209:46

of 279



Phenanthrene


2-Methylanthracene






Retene

Anthracene

Carbazole


Fluoranthene

Pyrene



Benz(a)anthracene

Chrysene







Benzo(e)pyrene

Benzo(a)pyrene

Perylene





45.4

36.6

130

21.2

12.6

26.3

111

139

89.1

68.4

ND

71.6

18.6

25.2

475

571

289

87.5

232

313

188

137

149

150

447

372

336

370

124

358

89.8

349

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

11.6

Naphthalene-d8

Phenanthrene-d10

Benzo(a)pyrene-d12

65

93

87

50-130

50-130

50-130


11/05/12



L1218042-27Lab ID:


MDL

3.19

3.19

3.83

3.83

3.83

3.83

3.83

3.83

3.83

3.83

2.83

2.38

3.78

3.05

3.67

3.04

3.04

3.23

2.36

2.34

2.34

2.34

2.34

2.34

3.00

2.29

2.38

3.30

2.23

3.14

3.12

3.07

Serial_No:11051209:46

of 279

cis/trans-Decalin

C1-Decalin

C2-Decalin

C3-Decalin

C4-Decalin

Naphthalene

C1-Naphthalenes

C2-Naphthalenes

C3-Naphthalenes

C4-Naphthalenes

2-Methylnaphthalene

1-Methylnaphthalene

Benzothiophene






Acenaphthylene

Acenaphthene


Fluorene

C1-Fluorenes

C2-Fluorenes

C3-Fluorenes

Dibenzothiophene






Parameter Result

J

J

J

G

J

Dilution Factor

26.7

10.2

29.6

32.5

52.5

37.9

29.7

83.5

32.5

28.0

30.7

15.3

ND

ND

10.1

18.7

ND

105

60.6

16.6

4.42

27.8

19.4

41.3

112

17.3

9.69

40.0

ND

57.2

40.6

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

6.24

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

11/05/12



L1218042-29Lab ID:



1,8270D-SIM(M)10/18/12 10:26MT

ALPHA OP-013



MDL

3.14

3.14

3.14

3.14

3.14

3.59

3.59

3.59

3.59

3.59

3.22

3.94

3.91

3.91

3.91

3.91

3.91

2.97

2.38

2.20

2.04

3.33

3.33

3.33

3.33

3.44

3.44

3.44

3.44

3.44

3.44

Serial_No:11051209:46

of 279



Phenanthrene


2-Methylanthracene






Retene

Anthracene

Carbazole


Fluoranthene

Pyrene



Benz(a)anthracene

Chrysene







Benzo(e)pyrene

Benzo(a)pyrene

Perylene





52.7

43.7

160

27.8

15.6

32.5

137

167

112

70.0

27.0

98.8

22.7

31.8

622

692

374

108

292

389

223

156

179

199

548

472

417

458

153

435

114

430

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

12.5

Naphthalene-d8

Phenanthrene-d10

Benzo(a)pyrene-d12

71

97

93

50-130

50-130

50-130


11/05/12



L1218042-29Lab ID:


MDL

3.44

3.44

4.14

4.14

4.14

4.14

4.14

4.14

4.14

4.14

3.06

2.57

4.08

3.30

3.97

3.28

3.28

3.49

2.55

2.52

2.52

2.52

2.52

2.52

3.25

2.48

2.58

3.56

2.41

3.39

3.37

3.32

Serial_No:11051209:46

of 279


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

10/12/12 18:291,8270D-SIM(M)Analytical Method:

Analytical Date:Extraction Method: EPA 3510CExtraction Date: 10/10/12 07:35

11/05/12

Analyst: MT

cis/trans-Decalin

C1-Decalin

C2-Decalin

C3-Decalin

C4-Decalin

Naphthalene

C1-Naphthalenes

C2-Naphthalenes

C3-Naphthalenes

C4-Naphthalenes

2-Methylnaphthalene

1-Methylnaphthalene

Benzothiophene






Acenaphthylene

Acenaphthene


Fluorene

C1-Fluorenes

C2-Fluorenes

C3-Fluorenes

Dibenzothiophene






Parameter Result

2.30

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

5.00

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

J ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

UnitsQualifier

PAHs - Mansfield Lab for sample(s): 11 Batch: WG566066-1

MDL

2.16

2.16

2.16

2.16

2.16

2.35

2.35

2.35

2.35

2.35

1.33

1.62

2.48

2.48

2.48

2.48

2.48

2.80

2.10

1.34

1.90

2.18

2.18

2.18

2.18

1.42

1.42

1.42

1.42

1.42

1.42

Serial_No:11051209:46

of 279


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042



11/05/12

Analyst: MT



Phenanthrene


2-Methylanthracene






Retene

Anthracene

Carbazole


Fluoranthene

Pyrene



Benz(a)anthracene

Chrysene







Benzo(e)pyrene

Benzo(a)pyrene

Perylene



Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

10.0

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

ng/l

UnitsQualifier


MDL

1.42

1.42

2.38

2.38

2.38

2.38

2.38

2.38

2.38

2.38

2.26

1.87

4.58

3.47

2.62

0.900

0.900

1.18

2.65

1.62

1.62

1.62

1.62

1.62

1.12

2.56

1.64

4.25

2.91

1.81

2.18

Serial_No:11051209:46

of 279


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042



11/05/12

Analyst: MT


Parameter Result

ND

RL

10.0ng/l

UnitsQualifier


Naphthalene-d8

Phenanthrene-d10

Benzo(a)pyrene-d12

94

89

94

50-130

50-130

50-130


Criteria

MDL

1.64

Serial_No:11051209:46

of 279


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042


Analytical Date:Extraction Method:

Cleanup Method1:

ALPHA OP-013


11/05/12

Analyst: MT

cis/trans-Decalin

C1-Decalin

C2-Decalin

C3-Decalin

C4-Decalin

Naphthalene

C1-Naphthalenes

C2-Naphthalenes

C3-Naphthalenes

C4-Naphthalenes

2-Methylnaphthalene

1-Methylnaphthalene

Benzothiophene






Acenaphthylene

Acenaphthene


Fluorene

C1-Fluorenes

C2-Fluorenes

C3-Fluorenes

Dibenzothiophene





Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

0.500

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier

PAHs - Mansfield Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566754-1

Cleanup Date1: 10/16/12

MDL

0.251

0.251

0.251

0.251

0.251

0.287

0.287

0.287

0.287

0.287

0.258

0.315

0.313

0.313

0.313

0.313

0.313

0.238

0.191

0.176

0.164

0.267

0.267

0.267

0.267

0.276

0.276

0.276

0.276

0.276

Serial_No:11051209:46

of 279


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042



Cleanup Method1:

ALPHA OP-013


11/05/12

Analyst: MT




Phenanthrene


2-Methylanthracene






Retene

Anthracene

Carbazole


Fluoranthene

Pyrene



Benz(a)anthracene

Chrysene







Benzo(e)pyrene

Benzo(a)pyrene

Perylene

Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

ug/kg

UnitsQualifier



MDL

0.276

0.276

0.276

0.331

0.331

0.331

0.331

0.331

0.331

0.331

0.331

0.245

0.206

0.327

0.264

0.318

0.263

0.263

0.280

0.204

0.202

0.202

0.202

0.202

0.202

0.260

0.198

0.206

0.285

0.193

Serial_No:11051209:46

of 279


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042



Cleanup Method1:

ALPHA OP-013


11/05/12

Analyst: MT




Parameter Result

ND

ND

ND

RL

1.00

1.00

1.00

ug/kg

ug/kg

ug/kg

UnitsQualifier


Naphthalene-d8

Phenanthrene-d10

Benzo(a)pyrene-d12

79

94

80

50-130

50-130

50-130


Criteria


MDL

0.271

0.270

0.266

Serial_No:11051209:46

of 279

Naphthalene

2-Methylnaphthalene

Acenaphthylene

Acenaphthene

Fluorene

Phenanthrene

Anthracene

Fluoranthene

Pyrene

Benz(a)anthracene

Chrysene


Benzo(j)+(k)Fluoranthene

Benzo(a)pyrene

Indeno(1,2,3-cd)Pyrene


Benzo(ghi)perylene

93

104

97

100

92

95

112

113

118

96

99

94

103

106

104

108

98

90

98

97

101

95

95

112

123

129

96

99

95

103

106

98

100

91

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

3

6

0

1

3

0

0

8

9

0

0

1

0

0

6

8

7

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


PAHs - Mansfield Lab Associated sample(s): 11 Batch: WG566066-2 WG566066-3


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

Qual Qual Qual

Serial_No:11051209:46

of 279

Naphthalene

2-Methylnaphthalene

Acenaphthylene

Acenaphthene

Fluorene

Phenanthrene

Anthracene

Fluoranthene

Pyrene

84

83

74

86

90

93

86

92

95

90

89

82

91

90

97

91

96

100

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

7

7

10

6

0

4

6

4

5

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


PAHs - Mansfield Lab Associated sample(s): 11 Batch: WG566066-2 WG566066-3

PAHs - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566754-2 WG566754-3


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Naphthalene-d8

Phenanthrene-d10

Benzo(a)pyrene-d12

89

90

91

50-130

50-130

50-130

85

90

91


11/05/12

AcceptanceCriteria

Qual Qual Qual

Serial_No:11051209:46

of 279

Benz(a)anthracene

Chrysene



Benzo(a)pyrene



Benzo(ghi)perylene

69

85

73

86

68

58

52

60

79

90

85

101

86

71

69

74

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

14

6

15

16

23

20

28

21

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


PAHs - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566754-2 WG566754-3


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Naphthalene-d8

Phenanthrene-d10

Benzo(a)pyrene-d12

77

94

64

50-130

50-130

50-130

89

98

79


11/05/12

AcceptanceCriteria

Qual Qual Qual

Serial_No:11051209:46

of 279

S.R.M. Standard Quality Control

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Parameter

11/05/12

% Recovery QC CriteriaPhenanthrene

Fluoranthene

Pyrene

Benz(a)anthracene

Chrysene/Triphenylene



Benzo(e)Pyrene

Benzo(a)pyrene

Perylene



Benzo(ghi)perylene

Naphthalene-d8 (Surrogate)

Phenanthrene-d10 (Surrogate)

Benzo(a)pyrene-d12 (Surrogate)

98

91

88

81

89

81

86

93

87

79

101

116

106

73

96

87

67-135

67-135

67-136

68-133

66-138

62-144

60-149

68-134

68-134

56-157

67-135

62-144

68-135

50-130

50-130

50-130

Standard Reference Material (SRM): WG566754-4

Qual

Serial_No:11051209:46

of 279

PETROLEUM HYDROCARBONS

Serial_No:11051209:46

of 279

FF

n-Nonane (C9)

n-Decane (C10)

n-Undecane (C11)

n-Dodecane (C12)

n-Tridecane (C13)

2,6,10-Trimethyldodecane (1380)

n-Tetradecane (C14)

2,6,10-Trimethyltridecane (1470)

n-Pentadecane (C15)

n-Hexadecane (C16)

Norpristane (1650)

n-Heptadecane (C17)

Pristane

n-Octadecane (C18)

Phytane

n-Nonadecane (C19)

n-Eicosane (C20)

n-Heneicosane (C21)

n-Docosane (C22)

n-Tricosane (C23)

n-Tetracosane (C24)

n-Pentacosane (C25)

n-Hexacosane (C26)

n-Heptacosane (C27)

n-Octacosane (C28)

n-Nonacosane (C29)

n-Triacontane (C30)

n-Hentriacontane (C31)

n-Dotriacontane (C32)

n-Tritriacontane (C33)

n-Tetratriacontane (C34)

Parameter Result

JG

G

JG

J

G

J

C

J

J

J

J

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

0.211

ND

ND

ND

ND

ND

0.351

0.155

ND

ND

ND

ND

0.326

ND

0.734

ND

0.197

ND

0.798

0.071

0.242

0.064

0.296

0.113

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL

Saturated Hydrocarbons by GC-FID - Mansfield Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

0.346

11/05/12



L1218042-01Lab ID:



1,8015D(M)10/20/12 00:35DP

ALPHA OP-013



MDL

0.102

0.110

0.103

0.075

0.095

0.052

0.052

0.041

0.041

0.052

0.114

0.114

0.074

0.069

0.043

0.089

0.049

0.041

0.036

0.044

0.058

0.183

0.051

0.042

0.074

0.230

0.040

0.049

0.044

0.049

0.055

Serial_No:11051209:46

of 279

n-Pentatriacontane (C35)

n-Hexatriacontane (C36)

n-Heptatriacontane (C37)

n-Octatriacontane (C38)

n-Nonatriacontane (C39)

n-Tetracontane (C40)

Total Petroleum Hydrocarbons (C9-C40)

DRO (C10-C28)

Parameter Result

J

Dilution Factor

ND

ND

ND

0.088

ND

ND

245

132

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.346

0.346

0.346

0.346

0.346

0.346

11.4

7.26

ortho-terphenyl

d50-Tetracosane

92

91

50-130

50-130


11/05/12



L1218042-01Lab ID:


MDL

0.060

0.069

0.077

0.081

0.112

0.112

2.51

1.50

Serial_No:11051209:46

of 279

n-Nonane (C9)

n-Decane (C10)

n-Undecane (C11)

n-Dodecane (C12)

n-Tridecane (C13)


n-Tetradecane (C14)


n-Pentadecane (C15)

n-Hexadecane (C16)

Norpristane (1650)

n-Heptadecane (C17)

Pristane

n-Octadecane (C18)

Phytane

n-Nonadecane (C19)

n-Eicosane (C20)

n-Heneicosane (C21)

n-Docosane (C22)

n-Tricosane (C23)

n-Tetracosane (C24)

n-Pentacosane (C25)

n-Hexacosane (C26)

n-Heptacosane (C27)

n-Octacosane (C28)

n-Nonacosane (C29)

n-Triacontane (C30)





Parameter Result

J

G

J

J

J

J

G

G

G

J

C

J

Dilution Factor

ND

ND

ND

ND

ND

ND

0.048

0.678

0.040

0.121

ND

0.231

0.118

0.735

0.531

ND

ND

ND

ND

0.868

ND

2.37

0.269

0.649

ND

0.769

ND

0.674

0.138

0.357

0.460

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

0.298

11/05/12



L1218042-03Lab ID:



1,8015D(M)10/20/12 02:06DP

ALPHA OP-013



MDL

0.088

0.095

0.089

0.065

0.082

0.045

0.045

0.036

0.036

0.045

0.098

0.098

0.064

0.060

0.037

0.077

0.042

0.036

0.031

0.038

0.050

0.158

0.044

0.036

0.064

0.198

0.034

0.042

0.038

0.042

0.047

Serial_No:11051209:46

of 279








DRO (C10-C28)

Parameter Result

J

J

Dilution Factor

0.150

ND

ND

0.264

ND

ND

675

354

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.298

0.298

0.298

0.298

0.298

0.298

9.83

6.26

ortho-terphenyl

d50-Tetracosane

90

89

50-130

50-130


11/05/12



L1218042-03Lab ID:


MDL

0.052

0.059

0.066

0.069

0.097

0.097

2.16

1.29

Serial_No:11051209:46

of 279

n-Nonane (C9)

n-Decane (C10)

n-Undecane (C11)

n-Dodecane (C12)

n-Tridecane (C13)


n-Tetradecane (C14)


n-Pentadecane (C15)

n-Hexadecane (C16)

Norpristane (1650)

n-Heptadecane (C17)

Pristane

n-Octadecane (C18)

Phytane

n-Nonadecane (C19)

n-Eicosane (C20)

n-Heneicosane (C21)

n-Docosane (C22)

n-Tricosane (C23)

n-Tetracosane (C24)

n-Pentacosane (C25)

n-Hexacosane (C26)

n-Heptacosane (C27)

n-Octacosane (C28)

n-Nonacosane (C29)

n-Triacontane (C30)





Parameter Result

G

J

J

J

J

G

G

J

G

J

C

J

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

1.20

0.096

0.189

ND

0.409

0.217

1.24

0.906

0.146

ND

ND

ND

1.10

ND

3.73

0.462

1.16

ND

1.41

0.316

1.30

0.292

0.789

0.756

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

0.570

11/05/12



L1218042-05Lab ID:



1,8015D(M)10/20/12 03:36DP

ALPHA OP-013



MDL

0.169

0.182

0.170

0.124

0.156

0.086

0.086

0.068

0.068

0.086

0.188

0.188

0.122

0.114

0.072

0.146

0.081

0.068

0.060

0.073

0.095

0.302

0.084

0.069

0.122

0.380

0.065

0.081

0.072

0.080

0.091

Serial_No:11051209:46

of 279








DRO (C10-C28)

Parameter Result

J

J

J

J

J

Dilution Factor

0.259

0.359

0.127

0.516

0.246

ND

1260

645

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.570

0.570

0.570

0.570

0.570

0.570

18.8

12.0

ortho-terphenyl

d50-Tetracosane

88

87

50-130

50-130


11/05/12



L1218042-05Lab ID:


MDL

0.100

0.113

0.127

0.133

0.185

0.185

4.14

2.47

Serial_No:11051209:46

of 279

n-Nonane (C9)

n-Decane (C10)

n-Undecane (C11)

n-Dodecane (C12)

n-Tridecane (C13)


n-Tetradecane (C14)


n-Pentadecane (C15)

n-Hexadecane (C16)

Norpristane (1650)

n-Heptadecane (C17)

Pristane

n-Octadecane (C18)

Phytane

n-Nonadecane (C19)

n-Eicosane (C20)

n-Heneicosane (C21)

n-Docosane (C22)

n-Tricosane (C23)

n-Tetracosane (C24)

n-Pentacosane (C25)

n-Hexacosane (C26)

n-Heptacosane (C27)

n-Octacosane (C28)

n-Nonacosane (C29)

n-Triacontane (C30)





Parameter Result

JG

J

J

G

JG

J

G

J

C

J

J

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

0.264

ND

0.061

ND

0.136

ND

0.554

0.283

ND

ND

ND

ND

0.312

ND

1.38

0.173

0.702

ND

1.15

0.142

0.518

0.096

0.564

0.273

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

0.377

11/05/12



L1218042-07Lab ID:



1,8015D(M)10/20/12 05:07DP

ALPHA OP-013



MDL

0.112

0.120

0.112

0.082

0.103

0.057

0.057

0.045

0.045

0.057

0.124

0.124

0.081

0.076

0.047

0.097

0.053

0.045

0.039

0.048

0.063

0.199

0.055

0.045

0.081

0.251

0.043

0.053

0.048

0.053

0.060

Serial_No:11051209:46

of 279








DRO (C10-C28)

Parameter Result

J

Dilution Factor

0.083

ND

ND

ND

ND

ND

383

178

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.377

0.377

0.377

0.377

0.377

0.377

12.4

7.91

ortho-terphenyl

d50-Tetracosane

88

86

50-130

50-130


11/05/12



L1218042-07Lab ID:


MDL

0.066

0.075

0.084

0.088

0.122

0.122

2.74

1.63

Serial_No:11051209:46

of 279

n-Nonane (C9)

n-Decane (C10)

n-Undecane (C11)

n-Dodecane (C12)

n-Tridecane (C13)


n-Tetradecane (C14)


n-Pentadecane (C15)

n-Hexadecane (C16)

Norpristane (1650)

n-Heptadecane (C17)

Pristane

n-Octadecane (C18)

Phytane

n-Nonadecane (C19)

n-Eicosane (C20)

n-Heneicosane (C21)

n-Docosane (C22)

n-Tricosane (C23)

n-Tetracosane (C24)

n-Pentacosane (C25)

n-Hexacosane (C26)

n-Heptacosane (C27)

n-Octacosane (C28)

n-Nonacosane (C29)

n-Triacontane (C30)





Parameter Result

JG

G

JG

J

G

J

J

C

J

J

J

J

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

0.105

ND

ND

ND

ND

ND

0.511

0.137

ND

ND

ND

ND

0.111

ND

0.730

0.068

0.121

ND

0.620

0.052

0.157

0.038

0.255

0.075

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

0.281

11/05/12



L1218042-09Lab ID:



1,8015D(M)10/20/12 06:37DP

ALPHA OP-013



MDL

0.083

0.090

0.084

0.061

0.077

0.042

0.042

0.034

0.034

0.042

0.093

0.093

0.060

0.056

0.035

0.072

0.040

0.034

0.029

0.036

0.047

0.149

0.041

0.034

0.060

0.187

0.032

0.040

0.035

0.040

0.045

Serial_No:11051209:46

of 279








DRO (C10-C28)


ND

ND

ND

ND

ND

ND

165

71.3

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.281

0.281

0.281

0.281

0.281

0.281

9.28

5.91

ortho-terphenyl

d50-Tetracosane

94

93

50-130

50-130


11/05/12



L1218042-09Lab ID:


MDL

0.049

0.056

0.063

0.066

0.091

0.091

2.04

1.22

Serial_No:11051209:46

of 279

n-Nonane (C9)

n-Decane (C10)

n-Undecane (C11)

n-Dodecane (C12)

n-Tridecane (C13)


n-Tetradecane (C14)


n-Pentadecane (C15)

n-Hexadecane (C16)

Norpristane (1650)

n-Heptadecane (C17)

Pristane

n-Octadecane (C18)

Phytane

n-Nonadecane (C19)

n-Eicosane (C20)

n-Heneicosane (C21)

n-Docosane (C22)

n-Tricosane (C23)

n-Tetracosane (C24)

n-Pentacosane (C25)

n-Hexacosane (C26)

n-Heptacosane (C27)

n-Octacosane (C28)

n-Nonacosane (C29)

n-Triacontane (C30)





Parameter Result

JC

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.001

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.001

0.001

0.001

0.001

0.006

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.006

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

11/05/12



L1218042-11Lab ID:

Field Prep: Not SpecifiedMatrix: Water Extraction Method:Analytical Method:Analytical Date:Analyst:

1,8015D(M)10/12/12 23:51DP

EPA 3510CExtraction Date: 10/10/12 07:46

MDL

0.0004

0.0001

0.0001

0.0002

0.001

0.0001

0.0001

0.0002

0.0002

0.0002

0.0002

0.0002

0.0002

0.0001

0.0001

0.0002

0.0001

0.0001

0.00005

0.0001

0.0001

0.001

0.0001

0.0001

0.0002

0.0001

0.0001

0.0002

0.0001

0.0002

0.0002

Serial_No:11051209:46

of 279








DRO (C10-C28)

Parameter Result

J

Dilution Factor

ND

ND

ND

ND

ND

ND

0.035

0.028

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.001

0.001

0.001

0.001

0.001

0.001

0.038

0.024

ortho-terphenyl

d50-Tetracosane

91

87

50-130

50-130


11/05/12



L1218042-11Lab ID:


MDL

0.0002

0.0002

0.0002

0.0002

0.0002

0.0002

0.006

0.004

Serial_No:11051209:46

of 279

n-Nonane (C9)

n-Decane (C10)

n-Undecane (C11)

n-Dodecane (C12)

n-Tridecane (C13)


n-Tetradecane (C14)


n-Pentadecane (C15)

n-Hexadecane (C16)

Norpristane (1650)

n-Heptadecane (C17)

Pristane

n-Octadecane (C18)

Phytane

n-Nonadecane (C19)

n-Eicosane (C20)

n-Heneicosane (C21)

n-Docosane (C22)

n-Tricosane (C23)

n-Tetracosane (C24)

n-Pentacosane (C25)

n-Hexacosane (C26)

n-Heptacosane (C27)

n-Octacosane (C28)

n-Nonacosane (C29)

n-Triacontane (C30)





Parameter Result

JG

J

J

JG

JG

J

G

J

J

C

J

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

0.287

0.251

ND

ND

0.960

ND

0.430

0.409

ND

ND

ND

ND

0.388

ND

3.97

0.747

4.20

0.514

5.34

0.784

4.85

0.592

4.50

5.20

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

0.974

11/05/12



L1218042-13Lab ID:



1,8015D(M)10/20/12 08:08DP

ALPHA OP-013



MDL

0.289

0.311

0.291

0.212

0.267

0.146

0.146

0.116

0.116

0.147

0.321

0.321

0.208

0.195

0.122

0.250

0.138

0.116

0.102

0.124

0.163

0.516

0.143

0.117

0.209

0.649

0.112

0.138

0.123

0.137

0.155

Serial_No:11051209:46

of 279








DRO (C10-C28)

Parameter Result

J

J

J

J

J

J

Dilution Factor

0.820

0.736

0.658

0.733

0.758

0.484

2390

1010

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.974

0.974

0.974

0.974

0.974

0.974

32.1

20.4

ortho-terphenyl

d50-Tetracosane

94

90

50-130

50-130


11/05/12



L1218042-13Lab ID:


MDL

0.170

0.194

0.216

0.227

0.316

0.316

7.07

4.22

Serial_No:11051209:46

of 279

n-Nonane (C9)

n-Decane (C10)

n-Undecane (C11)

n-Dodecane (C12)

n-Tridecane (C13)


n-Tetradecane (C14)


n-Pentadecane (C15)

n-Hexadecane (C16)

Norpristane (1650)

n-Heptadecane (C17)

Pristane

n-Octadecane (C18)

Phytane

n-Nonadecane (C19)

n-Eicosane (C20)

n-Heneicosane (C21)

n-Docosane (C22)

n-Tricosane (C23)

n-Tetracosane (C24)

n-Pentacosane (C25)

n-Hexacosane (C26)

n-Heptacosane (C27)

n-Octacosane (C28)

n-Nonacosane (C29)

n-Triacontane (C30)





Parameter Result

JG

J

J

JG

JG

J

J

G

J

C

J

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

0.382

0.153

ND

ND

1.22

0.298

0.563

0.622

0.358

ND

ND

ND

0.535

ND

4.26

1.21

5.41

0.586

8.05

1.11

6.90

0.893

6.18

6.72

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

1.16

11/05/12



L1218042-15Lab ID:



1,8015D(M)10/20/12 14:10DP

ALPHA OP-013



MDL

0.344

0.370

0.347

0.253

0.319

0.175

0.175

0.138

0.138

0.175

0.383

0.383

0.248

0.233

0.146

0.298

0.164

0.139

0.121

0.148

0.194

0.615

0.171

0.140

0.249

0.774

0.133

0.164

0.146

0.163

0.185

Serial_No:11051209:46

of 279








DRO (C10-C28)

Parameter Result

J

J

J

J

Dilution Factor

1.28

1.17

0.871

0.920

1.04

0.618

3210

1360

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

1.16

1.16

1.16

1.16

1.16

1.16

38.3

24.4

ortho-terphenyl

d50-Tetracosane

95

90

50-130

50-130


11/05/12



L1218042-15Lab ID:


MDL

0.203

0.231

0.258

0.271

0.377

0.377

8.43

5.03

Serial_No:11051209:46

of 279

n-Nonane (C9)

n-Decane (C10)

n-Undecane (C11)

n-Dodecane (C12)

n-Tridecane (C13)


n-Tetradecane (C14)


n-Pentadecane (C15)

n-Hexadecane (C16)

Norpristane (1650)

n-Heptadecane (C17)

Pristane

n-Octadecane (C18)

Phytane

n-Nonadecane (C19)

n-Eicosane (C20)

n-Heneicosane (C21)

n-Docosane (C22)

n-Tricosane (C23)

n-Tetracosane (C24)

n-Pentacosane (C25)

n-Hexacosane (C26)

n-Heptacosane (C27)

n-Octacosane (C28)

n-Nonacosane (C29)

n-Triacontane (C30)





Parameter Result

J

J

JG

JG

J

J

JG

J

J

C

J

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

ND

0.100

ND

ND

0.386

ND

0.211

0.134

ND

ND

0.111

ND

0.222

ND

0.714

0.430

3.07

0.317

6.06

0.392

2.02

0.303

1.78

2.11

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

0.821

11/05/12



L1218042-17Lab ID:



1,8015D(M)10/20/12 15:40DP

ALPHA OP-013



MDL

0.244

0.262

0.245

0.179

0.225

0.124

0.124

0.098

0.098

0.124

0.271

0.271

0.175

0.165

0.103

0.211

0.116

0.098

0.086

0.104

0.137

0.435

0.121

0.099

0.176

0.547

0.094

0.116

0.103

0.116

0.131

Serial_No:11051209:46

of 279








DRO (C10-C28)

Parameter Result

J

J

J

J

J

J

Dilution Factor

0.280

0.377

0.257

0.487

0.505

0.310

743

266

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.821

0.821

0.821

0.821

0.821

0.821

27.1

17.2

ortho-terphenyl

d50-Tetracosane

95

92

50-130

50-130


11/05/12



L1218042-17Lab ID:


MDL

0.143

0.163

0.182

0.191

0.267

0.267

5.96

3.55

Serial_No:11051209:46

of 279

n-Nonane (C9)

n-Decane (C10)

n-Undecane (C11)

n-Dodecane (C12)

n-Tridecane (C13)


n-Tetradecane (C14)


n-Pentadecane (C15)

n-Hexadecane (C16)

Norpristane (1650)

n-Heptadecane (C17)

Pristane

n-Octadecane (C18)

Phytane

n-Nonadecane (C19)

n-Eicosane (C20)

n-Heneicosane (C21)

n-Docosane (C22)

n-Tricosane (C23)

n-Tetracosane (C24)

n-Pentacosane (C25)

n-Hexacosane (C26)

n-Heptacosane (C27)

n-Octacosane (C28)

n-Nonacosane (C29)

n-Triacontane (C30)





Parameter Result

JG

J

J

J

JG

JG

J

J

J

J

G

J

J

C

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

0.357

0.147

ND

ND

1.10

0.249

0.547

0.595

0.315

ND

ND

0.184

0.520

0.260

4.80

0.792

5.14

0.851

14.0

1.21

6.82

0.806

5.84

6.85

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

1.12

11/05/12



L1218042-19Lab ID:



1,8015D(M)10/20/12 17:11DP

ALPHA OP-013



MDL

0.331

0.356

0.333

0.243

0.306

0.168

0.168

0.133

0.133

0.168

0.368

0.368

0.238

0.224

0.140

0.287

0.158

0.134

0.116

0.142

0.187

0.590

0.164

0.134

0.239

0.743

0.128

0.158

0.140

0.157

0.178

Serial_No:11051209:46

of 279








DRO (C10-C28)

Parameter Result

J

J

J

J

Dilution Factor

1.37

1.17

1.10

1.00

1.05

0.676

2980

1220

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

1.12

1.12

1.12

1.12

1.12

1.12

36.8

23.4

ortho-terphenyl

d50-Tetracosane

95

95

50-130

50-130


11/05/12



L1218042-19Lab ID:


MDL

0.195

0.222

0.248

0.260

0.362

0.362

8.10

4.83

Serial_No:11051209:46

of 279

n-Nonane (C9)

n-Decane (C10)

n-Undecane (C11)

n-Dodecane (C12)

n-Tridecane (C13)


n-Tetradecane (C14)


n-Pentadecane (C15)

n-Hexadecane (C16)

Norpristane (1650)

n-Heptadecane (C17)

Pristane

n-Octadecane (C18)

Phytane

n-Nonadecane (C19)

n-Eicosane (C20)

n-Heneicosane (C21)

n-Docosane (C22)

n-Tricosane (C23)

n-Tetracosane (C24)

n-Pentacosane (C25)

n-Hexacosane (C26)

n-Heptacosane (C27)

n-Octacosane (C28)

n-Nonacosane (C29)

n-Triacontane (C30)





Parameter Result

JG

J

J

JG

JG

J

G

J

C

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

0.350

0.133

ND

ND

1.11

0.266

0.513

0.576

0.283

ND

ND

ND

ND

ND

4.09

1.22

4.95

0.657

12.5

1.08

6.39

0.946

4.13

6.58

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

11/05/12



L1218042-21Lab ID:



1,8015D(M)10/20/12 18:41DP

ALPHA OP-013



MDL

0.299

0.321

0.301

0.219

0.276

0.151

0.151

0.120

0.120

0.152

0.332

0.332

0.215

0.202

0.126

0.259

0.142

0.120

0.105

0.128

0.168

0.533

0.148

0.121

0.216

0.671

0.116

0.143

0.127

0.142

0.160

Serial_No:11051209:46

of 279








DRO (C10-C28)

Parameter Result

J

J

J

J

Dilution Factor

1.20

0.965

0.886

0.879

1.17

0.528

2920

1170

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

1.01

1.01

1.01

1.01

1.01

1.01

33.2

21.2

ortho-terphenyl

d50-Tetracosane

96

94

50-130

50-130


11/05/12



L1218042-21Lab ID:


MDL

0.176

0.200

0.224

0.235

0.327

0.327

7.31

4.36

Serial_No:11051209:46

of 279

n-Nonane (C9)

n-Decane (C10)

n-Undecane (C11)

n-Dodecane (C12)

n-Tridecane (C13)


n-Tetradecane (C14)


n-Pentadecane (C15)

n-Hexadecane (C16)

Norpristane (1650)

n-Heptadecane (C17)

Pristane

n-Octadecane (C18)

Phytane

n-Nonadecane (C19)

n-Eicosane (C20)

n-Heneicosane (C21)

n-Docosane (C22)

n-Tricosane (C23)

n-Tetracosane (C24)

n-Pentacosane (C25)

n-Hexacosane (C26)

n-Heptacosane (C27)

n-Octacosane (C28)

n-Nonacosane (C29)

n-Triacontane (C30)





Parameter Result

JG

J

JG

JG

J

J

G

J

C

J

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

0.121

ND

ND

ND

0.624

ND

0.249

0.229

ND

ND

ND

0.091

0.236

ND

2.42

0.516

3.55

ND

7.28

0.606

3.67

0.502

2.21

4.99

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

0.714

11/05/12



L1218042-23Lab ID:



1,8015D(M)10/20/12 20:11DP

ALPHA OP-013



MDL

0.212

0.228

0.213

0.156

0.196

0.107

0.107

0.085

0.085

0.108

0.236

0.236

0.153

0.143

0.090

0.184

0.101

0.086

0.075

0.091

0.120

0.378

0.105

0.086

0.153

0.476

0.082

0.101

0.090

0.100

0.114

Serial_No:11051209:46

of 279








DRO (C10-C28)

Parameter Result

J

J

J

J

Dilution Factor

0.954

0.725

0.426

0.464

0.589

0.423

1780

724

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.714

0.714

0.714

0.714

0.714

0.714

23.6

15.0

ortho-terphenyl

d50-Tetracosane

96

95

50-130

50-130


11/05/12



L1218042-23Lab ID:


MDL

0.125

0.142

0.159

0.166

0.232

0.232

5.19

3.09

Serial_No:11051209:46

of 279

n-Nonane (C9)

n-Decane (C10)

n-Undecane (C11)

n-Dodecane (C12)

n-Tridecane (C13)


n-Tetradecane (C14)


n-Pentadecane (C15)

n-Hexadecane (C16)

Norpristane (1650)

n-Heptadecane (C17)

Pristane

n-Octadecane (C18)

Phytane

n-Nonadecane (C19)

n-Eicosane (C20)

n-Heneicosane (C21)

n-Docosane (C22)

n-Tricosane (C23)

n-Tetracosane (C24)

n-Pentacosane (C25)

n-Hexacosane (C26)

n-Heptacosane (C27)

n-Octacosane (C28)

n-Nonacosane (C29)

n-Triacontane (C30)





Parameter Result

JG

J

J

JG

JG

J

J

G

J

J

C

J

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

0.158

0.148

ND

ND

0.846

ND

0.540

0.300

ND

ND

ND

0.134

0.294

ND

2.92

0.561

3.69

0.563

10.4

0.889

4.91

0.777

3.67

4.80

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

0.991

11/05/12



L1218042-25Lab ID:



1,8015D(M)10/20/12 21:41DP

ALPHA OP-013



MDL

0.294

0.316

0.296

0.216

0.272

0.149

0.149

0.118

0.118

0.149

0.327

0.327

0.212

0.199

0.124

0.255

0.140

0.119

0.103

0.126

0.166

0.524

0.146

0.119

0.212

0.660

0.114

0.140

0.125

0.139

0.158

Serial_No:11051209:46

of 279








DRO (C10-C28)

Parameter Result

J

J

J

J

J

J

Dilution Factor

0.788

0.878

0.607

0.688

0.924

0.653

2190

845

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.991

0.991

0.991

0.991

0.991

0.991

32.7

20.8

ortho-terphenyl

d50-Tetracosane

95

94

50-130

50-130


11/05/12



L1218042-25Lab ID:


MDL

0.173

0.197

0.220

0.231

0.322

0.322

7.20

4.29

Serial_No:11051209:46

of 279

n-Nonane (C9)

n-Decane (C10)

n-Undecane (C11)

n-Dodecane (C12)

n-Tridecane (C13)


n-Tetradecane (C14)


n-Pentadecane (C15)

n-Hexadecane (C16)

Norpristane (1650)

n-Heptadecane (C17)

Pristane

n-Octadecane (C18)

Phytane

n-Nonadecane (C19)

n-Eicosane (C20)

n-Heneicosane (C21)

n-Docosane (C22)

n-Tricosane (C23)

n-Tetracosane (C24)

n-Pentacosane (C25)

n-Hexacosane (C26)

n-Heptacosane (C27)

n-Octacosane (C28)

n-Nonacosane (C29)

n-Triacontane (C30)





Parameter Result

JG

J

JG

JG

J

J

JG

J

J

C

J

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

0.096

ND

ND

ND

0.611

ND

0.227

0.172

ND

ND

ND

0.089

0.200

ND

0.639

0.615

2.73

0.382

6.98

0.539

3.16

0.482

2.38

3.13

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

0.770

11/05/12



L1218042-27Lab ID:



1,8015D(M)10/20/12 23:11DP

ALPHA OP-013



MDL

0.228

0.246

0.230

0.168

0.211

0.116

0.116

0.092

0.092

0.116

0.254

0.254

0.164

0.155

0.097

0.198

0.109

0.092

0.080

0.098

0.129

0.408

0.113

0.093

0.165

0.513

0.088

0.109

0.097

0.108

0.122

Serial_No:11051209:46

of 279








DRO (C10-C28)

Parameter Result

J

J

J

J

J

J

Dilution Factor

0.555

0.535

0.401

0.590

0.618

0.416

1420

550

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.770

0.770

0.770

0.770

0.770

0.770

25.4

16.2

ortho-terphenyl

d50-Tetracosane

91

89

50-130

50-130


11/05/12



L1218042-27Lab ID:


MDL

0.134

0.153

0.171

0.180

0.250

0.250

5.59

3.33

Serial_No:11051209:46

of 279

n-Nonane (C9)

n-Decane (C10)

n-Undecane (C11)

n-Dodecane (C12)

n-Tridecane (C13)


n-Tetradecane (C14)


n-Pentadecane (C15)

n-Hexadecane (C16)

Norpristane (1650)

n-Heptadecane (C17)

Pristane

n-Octadecane (C18)

Phytane

n-Nonadecane (C19)

n-Eicosane (C20)

n-Heneicosane (C21)

n-Docosane (C22)

n-Tricosane (C23)

n-Tetracosane (C24)

n-Pentacosane (C25)

n-Hexacosane (C26)

n-Heptacosane (C27)

n-Octacosane (C28)

n-Nonacosane (C29)

n-Triacontane (C30)





Parameter Result

JG

J

J

JG

JG

J

J

G

J

J

C

J

J

Dilution Factor

ND

ND

ND

ND

ND

ND

ND

0.121

0.101

ND

ND

0.778

ND

0.292

0.230

ND

ND

ND

0.102

0.271

ND

2.22

0.692

3.32

0.457

9.24

0.723

4.10

0.693

3.40

3.96

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

0.833

11/05/12



L1218042-29Lab ID:



1,8015D(M)10/21/12 00:41DP

ALPHA OP-013



MDL

0.247

0.266

0.249

0.181

0.228

0.125

0.125

0.099

0.099

0.125

0.275

0.275

0.178

0.167

0.104

0.214

0.118

0.100

0.087

0.106

0.139

0.441

0.122

0.100

0.179

0.555

0.096

0.118

0.105

0.117

0.132

Serial_No:11051209:46

of 279








DRO (C10-C28)

Parameter Result

J

J

J

J

J

Dilution Factor

0.792

0.655

0.570

0.697

0.931

0.570

1680

623

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

Qualifier Units RL


SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

0.833

0.833

0.833

0.833

0.833

0.833

27.5

17.5

ortho-terphenyl

d50-Tetracosane

96

95

50-130

50-130


11/05/12



L1218042-29Lab ID:


MDL

0.145

0.166

0.185

0.194

0.270

0.270

6.05

3.60

Serial_No:11051209:46

of 279


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

10/11/12 14:191,8015D(M)Analytical Method:


11/05/12

Analyst: DP

n-Nonane (C9)

n-Decane (C10)

n-Undecane (C11)

n-Dodecane (C12)

n-Tridecane (C13)


n-Tetradecane (C14)


n-Pentadecane (C15)

n-Hexadecane (C16)

Norpristane (1650)

n-Heptadecane (C17)

Pristane

n-Octadecane (C18)

Phytane

n-Nonadecane (C19)

n-Eicosane (C20)

n-Heneicosane (C21)

n-Docosane (C22)

n-Tricosane (C23)

n-Tetracosane (C24)

n-Pentacosane (C25)

n-Hexacosane (C26)

n-Heptacosane (C27)

n-Octacosane (C28)

n-Nonacosane (C29)

n-Triacontane (C30)





Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

0.001

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

0.001

0.001

0.001

0.001

0.005

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.005

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

0.001

JC

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

UnitsQualifier

Saturated Hydrocarbons by GC-FID - Mansfield Lab for sample(s): 11 Batch: WG566066-1

MDL

0.0003

0.0001

0.0001

0.0001

0.001

0.0001

0.0001

0.0001

0.0001

0.0001

0.0001

0.0001

0.0002

0.0001

0.0001

0.0002

0.0001

0.0001

0.00004

0.0001

0.0001

0.001

0.0001

0.0001

0.0002

0.0001

0.0001

0.0001

0.0001

0.0001

0.0002

Serial_No:11051209:46

of 279


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042



11/05/12

Analyst: DP







Total Petroleum Hydrocarbons (C9-C40)DRO (C10-C28)

Parameter Result

ND

ND

ND

ND

ND

ND

ND

0.010

RL

0.001

0.001

0.001

0.001

0.001

0.001

0.033

0.021J

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

UnitsQualifier

Saturated Hydrocarbons by GC-FID - Mansfield Lab for sample(s): 11 Batch: WG566066-1

ortho-terphenyl

d50-Tetracosane

95

92

50-130

50-130


Criteria

MDL

0.0002

0.0001

0.0002

0.0002

0.0002

0.0002

0.006

0.004

Serial_No:11051209:46

of 279


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042



Cleanup Method1:

ALPHA OP-013


11/05/12

Analyst: DP

n-Nonane (C9)

n-Decane (C10)

n-Undecane (C11)

n-Dodecane (C12)

n-Tridecane (C13)


n-Tetradecane (C14)


n-Pentadecane (C15)

n-Hexadecane (C16)

Norpristane (1650)

n-Heptadecane (C17)

Pristane

n-Octadecane (C18)

Phytane

n-Nonadecane (C19)

n-Eicosane (C20)

n-Heneicosane (C21)

n-Docosane (C22)

n-Tricosane (C23)

n-Tetracosane (C24)

n-Pentacosane (C25)

n-Hexacosane (C26)

n-Heptacosane (C27)

n-Octacosane (C28)

n-Nonacosane (C29)

n-Triacontane (C30)




Parameter Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

RL

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

0.067

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

UnitsQualifier

Saturated Hydrocarbons by GC-FID - Mansfield Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566754-1


MDL

0.020

0.021

0.020

0.015

0.018

0.010

0.010

0.008

0.008

0.010

0.022

0.022

0.014

0.013

0.008

0.017

0.009

0.008

0.007

0.008

0.011

0.035

0.010

0.008

0.014

0.044

0.008

0.009

0.008

0.009

Serial_No:11051209:46

of 279


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042



Cleanup Method1:

ALPHA OP-013


11/05/12

Analyst: DP








Total Petroleum Hydrocarbons (C9-C40)DRO (C10-C28)

Parameter Result

ND

ND

ND

ND

ND

ND

ND

0.525

0.338

RL

0.067

0.067

0.067

0.067

0.067

0.067

0.067

2.20

1.40

J

J

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

UnitsQualifier

Saturated Hydrocarbons by GC-FID - Mansfield Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566754-1

ortho-terphenyl

d50-Tetracosane

95

97

50-130

50-130


Criteria


MDL

0.011

0.012

0.013

0.015

0.016

0.022

0.022

0.484

0.288

Serial_No:11051209:46

of 279

Nonane (C9)

Decane (C10)

Dodecane (C12)

Tetradecane (C14)

Hexadecane (C16)

Octadecane (C18)

Nonadecane (C19)

Eicosane (C20)

Docosane (C22)

Tetracosane (C24)

Hexacosane (C26)

Octacosane (C28)

Triacontane (C30)

Hexatriacontane (C36)

76

85

90

96

103

107

96

99

99

99

98

98

99

96

60

71

80

94

104

108

97

100

100

100

100

99

100

97

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

24

18

12

2

1

1

1

1

1

1

2

1

1

1

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


Saturated Hydrocarbons by GC-FID - Mansfield Lab Associated sample(s): 11 Batch: WG566066-2 WG566066-3


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

o-Terphenyl

d50-Tetracosane

93

89

50-130

50-130

94

90


11/05/12

AcceptanceCriteria

Qual Qual Qual

Serial_No:11051209:46

of 279

Nonane (C9)

Decane (C10)

Dodecane (C12)

Tetradecane (C14)

Hexadecane (C16)

Octadecane (C18)

Nonadecane (C19)

Eicosane (C20)

Docosane (C22)

Tetracosane (C24)

Hexacosane (C26)

Octacosane (C28)

Triacontane (C30)

Hexatriacontane (C36)

67

77

75

83

94

96

90

92

92

93

93

93

94

90

77

87

82

89

99

100

94

96

97

98

98

98

99

96

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

50-130

14

12

9

7

5

4

4

4

5

5

5

5

5

6

30

30

30

30

30

30

30

30

30

30

30

30

30

30

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


Saturated Hydrocarbons by GC-FID - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566754-2 WG566754-3


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

o-Terphenyl

d50-Tetracosane

91

90

50-130

50-130

94

94


11/05/12

AcceptanceCriteria

Qual Qual Qual

Serial_No:11051209:46

of 279

METALS

Serial_No:11051209:46

of 279

FF

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS


Matrix: SedimentNot SpecifiedSample Location:

L1218042-01Lab ID:


Parameter ResultDilution FactorQualifier Units RL

DateAnalyzed

AnalyticalMethod Analyst

Date Prepared

Total Metals - Mansfield Lab

Antimony, Total

Silver, Total

0.062

0.682

mg/kg

mg/kg

2

2

0.033

0.033

10/24/12 19:26

10/24/12 19:26

1,6020A

1,6020A

PD

PD

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 72%

MDL

0.006

0.002

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-01Lab ID:



DateAnalyzed


Date Prepared


Tin, Total 5.14 mg/kg 23.25 10/31/12 15:25 1,6020A PD10/30/12 15:23 EPA 3050B

PrepMethod

Percent Solids: 72%

R

MDL

0.328

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-01Lab ID:



DateAnalyzed


Date Prepared


Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Thallium, Total

Vanadium, Total

5.18

14.8

0.288

1.06

18.6

3.68

27.8

34.7

161

9.90

1.98

0.509

9.88

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

10

10

10

10

10

10

10

10

10

10

10

10

10

0.162

0.975

0.098

0.065

0.650

0.162

0.650

0.195

0.650

0.325

0.325

0.065

0.325

10/24/12 17:29

10/24/12 17:29

10/24/12 17:29

10/24/12 17:29

10/24/12 17:29

10/24/12 17:29

10/24/12 17:29

10/24/12 17:29

10/24/12 17:29

10/24/12 17:29

10/24/12 17:29

10/24/12 17:29

10/24/12 17:29

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 72%

D2

MDL

0.020

0.250

0.028

0.009

0.152

0.017

0.037

0.063

0.145

0.049

0.081

0.009

0.015

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-01Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Calcium, Total

Iron, Total

Magnesium, Total

Potassium, Total

Sodium, Total

Zinc, Total

2960

15800

6940

2660

896

3760

54.2

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

50

50

50

50

50

50

50

162

812

325

162

162

162

16.2

10/24/12 16:24

10/24/12 16:24

10/24/12 16:24

10/24/12 16:24

10/24/12 16:24

10/24/12 16:24

10/24/12 16:24

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 72%

D

MDL

24.1

98.8

33.5

20.0

24.6

14.0

4.22

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-03Lab ID:



DateAnalyzed


Date Prepared


Antimony, Total

Silver, Total

0.190

1.83

mg/kg

mg/kg

2

2

0.046

0.046

10/24/12 19:31

10/24/12 19:31

1,6020A

1,6020A

PD

PD

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 55%

MDL

0.008

0.002

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-03Lab ID:



DateAnalyzed


Date Prepared



PrepMethod

Percent Solids: 55%

R

MDL

0.424

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-03Lab ID:



DateAnalyzed


Date Prepared


Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Thallium, Total

Vanadium, Total

7.94

41.2

0.308

1.04

40.7

5.10

70.1

69.9

305

16.2

0.960

0.180

18.7

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

10

10

10

10

10

10

10

10

10

10

10

10

10

0.223

1.34

0.134

0.089

0.894

0.223

0.894

0.268

0.894

0.447

0.447

0.089

0.447

10/24/12 17:40

10/24/12 17:40

10/24/12 17:40

10/24/12 17:40

10/24/12 17:40

10/24/12 17:40

10/24/12 17:40

10/24/12 17:40

10/24/12 17:40

10/24/12 17:40

10/24/12 17:40

10/24/12 17:40

10/24/12 17:40

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 55%

D2

MDL

0.028

0.343

0.039

0.012

0.210

0.023

0.051

0.086

0.199

0.067

0.111

0.012

0.021

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-03Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Calcium, Total

Iron, Total

Magnesium, Total

Potassium, Total

Sodium, Total

Zinc, Total

5680

89800

14700

4590

1850

8690

142

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

50

50

50

50

50

50

50

223

1120

447

223

223

223

22.3

10/24/12 16:31

10/24/12 16:31

10/24/12 16:31

10/24/12 16:31

10/24/12 16:31

10/24/12 16:31

10/24/12 16:31

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 55%

D

MDL

33.1

136.

46.0

27.6

33.8

19.2

5.80

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-05Lab ID:



DateAnalyzed


Date Prepared


Antimony, Total

Silver, Total

0.180

3.08

mg/kg

mg/kg

2

2

0.060

0.060

10/24/12 19:32

10/24/12 19:32

1,6020A

1,6020A

PD

PD

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 41%

MDL

0.011

0.003

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-05Lab ID:



DateAnalyzed


Date Prepared



PrepMethod

Percent Solids: 41%

R

MDL

0.662

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-05Lab ID:



DateAnalyzed


Date Prepared


Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Thallium, Total

Vanadium, Total

10.2

68.5

0.555

1.46

69.8

8.65

122

118

459

26.3

1.53

0.245

32.3

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

10

10

10

10

10

10

10

10

10

10

10

10

10

0.316

1.90

0.190

0.126

1.26

0.316

1.26

0.379

1.26

0.632

0.632

0.126

0.632

10/24/12 17:41

10/24/12 17:41

10/24/12 17:41

10/24/12 17:41

10/24/12 17:41

10/24/12 17:41

10/24/12 17:41

10/24/12 17:41

10/24/12 17:41

10/24/12 17:41

10/24/12 17:41

10/24/12 17:41

10/24/12 17:41

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 41%

D2

MDL

0.039

0.486

0.055

0.017

0.296

0.033

0.071

0.122

0.281

0.095

0.157

0.017

0.029

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-05Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Calcium, Total

Iron, Total

Magnesium, Total

Potassium, Total

Sodium, Total

Zinc, Total

10000

47500

23800

7410

3000

12600

205

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

50

50

50

50

50

50

50

316

1580

632

316

316

316

31.6

10/24/12 16:32

10/24/12 16:32

10/24/12 16:32

10/24/12 16:32

10/24/12 16:32

10/24/12 16:32

10/24/12 16:32

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 41%

D

MDL

46.9

192.

65.2

39.0

47.8

27.2

8.21

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-07Lab ID:



DateAnalyzed


Date Prepared


Antimony, Total

Silver, Total

0.089

1.13

mg/kg

mg/kg

2

2

0.050

0.050

10/24/12 19:32

10/24/12 19:32

1,6020A

1,6020A

PD

PD

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 51%

MDL

0.009

0.002

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-07Lab ID:



DateAnalyzed


Date Prepared



PrepMethod

Percent Solids: 51%

R

MDL

0.465

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-07Lab ID:



DateAnalyzed


Date Prepared


Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Thallium, Total

Vanadium, Total

8.17

35.0

0.511

0.583

34.7

7.46

43.8

45.8

424

19.2

0.929

0.152

25.8

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

10

10

10

10

10

10

10

10

10

10

10

10

10

0.225

1.35

0.135

0.090

0.900

0.225

0.900

0.270

0.900

0.450

0.450

0.090

0.450

10/24/12 17:43

10/24/12 17:43

10/24/12 17:43

10/24/12 17:43

10/24/12 17:43

10/24/12 17:43

10/24/12 17:43

10/24/12 17:43

10/24/12 17:43

10/24/12 17:43

10/24/12 17:43

10/24/12 17:43

10/24/12 17:43

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 51%

D2

MDL

0.028

0.346

0.039

0.012

0.211

0.024

0.051

0.087

0.200

0.068

0.112

0.012

0.021

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-07Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Calcium, Total

Iron, Total

Magnesium, Total

Potassium, Total

Sodium, Total

Zinc, Total

8270

26100

19900

6080

2510

9030

104

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

50

50

50

50

50

50

50

225

1120

450

225

225

225

22.5

10/24/12 16:33

10/24/12 16:33

10/24/12 16:33

10/24/12 16:33

10/24/12 16:33

10/24/12 16:33

10/24/12 16:33

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 51%

D

MDL

33.4

137.

46.4

27.8

34.0

19.3

5.85

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-09Lab ID:



DateAnalyzed


Date Prepared


Antimony, Total

Silver, Total

0.044

0.324

mg/kg

mg/kg

2

2

0.031

0.031

10/24/12 19:33

10/24/12 19:33

1,6020A

1,6020A

PD

PD

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 78%

MDL

0.005

0.001

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-09Lab ID:



DateAnalyzed


Date Prepared


Tin, Total J2.16 mg/kg 23.57 10/31/12 15:32 1,6020A PD10/30/12 15:23 EPA 3050B

PrepMethod

Percent Solids: 78%

R

MDL

0.360

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-09Lab ID:



DateAnalyzed


Date Prepared


Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Thallium, Total

Vanadium, Total

J

2.97

9.21

0.137

0.206

11.8

2.85

16.9

19.0

108

7.89

0.268

0.077

7.58

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

10

10

10

10

10

10

10

10

10

10

10

10

10

0.167

1.00

0.100

0.067

0.669

0.167

0.669

0.201

0.669

0.335

0.335

0.067

0.335

10/24/12 17:45

10/24/12 17:45

10/24/12 17:45

10/24/12 17:45

10/24/12 17:45

10/24/12 17:45

10/24/12 17:45

10/24/12 17:45

10/24/12 17:45

10/24/12 17:45

10/24/12 17:45

10/24/12 17:45

10/24/12 17:45

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 78%

D2

MDL

0.021

0.257

0.029

0.009

0.157

0.018

0.038

0.065

0.149

0.050

0.083

0.009

0.015

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-09Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Calcium, Total

Iron, Total

Magnesium, Total

Potassium, Total

Sodium, Total

Zinc, Total

2190

11900

5170

2070

631

2890

37.1

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

50

50

50

50

50

50

50

167

837

335

167

167

167

16.7

10/24/12 16:34

10/24/12 16:34

10/24/12 16:34

10/24/12 16:34

10/24/12 16:34

10/24/12 16:34

10/24/12 16:34

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 78%

D

MDL

24.8

102.

34.5

20.6

25.3

14.4

4.35

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS


Matrix: WaterNot SpecifiedSample Location:

L1218042-11Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Tin, Total

Vanadium, Total

Zinc, Total

J

J

J

J

J

J

J

J

J

J

ND

ND

ND

0.0002

ND

ND

0.069

0.001

0.001

0.013

0.0002

0.134

0.0008

0.0007

0.068

ND

ND

1.11

0.00001

0.0002

ND

0.005

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

0.100

0.0005

0.0005

0.0005

0.0005

0.0005

0.100

0.001

0.001

0.050

0.0010

0.070

0.0005

0.0005

0.100

0.005

0.0003

0.100

0.00020

0.0005

0.005

0.010

10/23/12 18:19

10/23/12 18:19

10/23/12 18:19

10/23/12 18:19

10/23/12 18:19

10/23/12 18:19

10/23/12 18:19

10/23/12 18:19

10/23/12 18:19

10/23/12 18:19

10/23/12 18:19

10/23/12 18:19

10/23/12 18:19

10/23/12 18:19

10/23/12 18:19

10/23/12 18:19

10/23/12 18:19

10/23/12 18:19

10/23/12 18:19

10/23/12 18:19

10/23/12 18:19

10/23/12 18:19

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

EPA 3020A

EPA 3020A

EPA 3020A

EPA 3020A

EPA 3020A

EPA 3020A

EPA 3020A

EPA 3020A

EPA 3020A

EPA 3020A

EPA 3020A

EPA 3020A

EPA 3020A

EPA 3020A

EPA 3020A

EPA 3020A

EPA 3020A

EPA 3020A

EPA 3020A

EPA 3020A

EPA 3020A

EPA 3020A

PrepMethodMDL

0.023

0.00003

0.0001

0.0001

0.0001

0.0001

0.019

0.0003

0.0003

0.008

0.0001

0.002

0.0001

0.0002

0.006

0.0003

0.00002

0.006

0.00001

0.0001

0.0001

0.001

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS


Matrix: WaterNot SpecifiedSample Location:

L1218042-11Lab ID:



DateAnalyzed


Date Prepared


Cobalt, Total J0.00005 mg/l 10.00020 10/23/12 18:49 1,6020A PD10/17/12 12:00 EPA 3020A

PrepMethod

R

MDL

0.00002

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-13Lab ID:



DateAnalyzed


Date Prepared


Antimony, Total

Silver, Total

0.431

1.89

mg/kg

mg/kg

2

2

0.096

0.096

10/24/12 19:34

10/24/12 19:34

1,6020A

1,6020A

PD

PD

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 27%

MDL

0.017

0.004

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-13Lab ID:



DateAnalyzed


Date Prepared



PrepMethod

Percent Solids: 27%

R

MDL

1.00

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-13Lab ID:



DateAnalyzed


Date Prepared


Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Thallium, Total

Vanadium, Total

16.4

36.6

0.667

1.68

47.8

8.60

115

128

232

26.5

2.62

0.372

50.7

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

10

10

10

10

10

10

10

10

10

10

10

10

10

0.473

2.84

0.284

0.189

1.89

0.473

1.89

0.567

1.89

0.946

0.946

0.189

0.946

10/24/12 17:47

10/24/12 17:47

10/24/12 17:47

10/24/12 17:47

10/24/12 17:47

10/24/12 17:47

10/24/12 17:47

10/24/12 17:47

10/24/12 17:47

10/24/12 17:47

10/24/12 17:47

10/24/12 17:47

10/24/12 17:47

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 27%

D2

MDL

0.058

0.726

0.082

0.025

0.444

0.050

0.107

0.182

0.421

0.142

0.236

0.026

0.043

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-13Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Calcium, Total

Iron, Total

Magnesium, Total

Potassium, Total

Sodium, Total

Zinc, Total

11300

5580

34500

8430

3290

24500

312

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

50

50

50

50

50

50

50

473

2360

946

473

473

473

47.3

10/24/12 16:35

10/24/12 16:35

10/24/12 16:35

10/24/12 16:35

10/24/12 16:35

10/24/12 16:35

10/24/12 16:35

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 27%

D

MDL

70.1

288.

97.5

58.3

71.5

40.6

12.3

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-15Lab ID:



DateAnalyzed


Date Prepared


Antimony, Total

Silver, Total

0.635

1.87

mg/kg

mg/kg

2

2

0.099

0.099

10/24/12 19:35

10/24/12 19:35

1,6020A

1,6020A

PD

PD

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 25%

MDL

0.018

0.005

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-15Lab ID:



DateAnalyzed


Date Prepared



PrepMethod

Percent Solids: 25%

R

MDL

1.10

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-15Lab ID:



DateAnalyzed


Date Prepared


Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Thallium, Total

Vanadium, Total

16.1

40.8

0.715

1.93

52.8

9.32

136

147

215

28.6

3.00

0.442

63.3

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

10

10

10

10

10

10

10

10

10

10

10

10

10

0.478

2.87

0.287

0.191

1.91

0.478

1.91

0.573

1.91

0.956

0.956

0.191

0.956

10/24/12 17:48

10/24/12 17:48

10/24/12 17:48

10/24/12 17:48

10/24/12 17:48

10/24/12 17:48

10/24/12 17:48

10/24/12 17:48

10/24/12 17:48

10/24/12 17:48

10/24/12 17:48

10/24/12 17:48

10/24/12 17:48

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 25%

D2

MDL

0.059

0.734

0.083

0.025

0.448

0.050

0.108

0.184

0.425

0.143

0.238

0.026

0.044

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-15Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Calcium, Total

Iron, Total

Magnesium, Total

Potassium, Total

Sodium, Total

Zinc, Total

12600

5900

34200

9620

3750

27200

373

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

50

50

50

50

50

50

50

478

2390

956

478

478

478

47.8

10/24/12 16:36

10/24/12 16:36

10/24/12 16:36

10/24/12 16:36

10/24/12 16:36

10/24/12 16:36

10/24/12 16:36

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 25%

D

MDL

70.8

291.

98.5

58.9

72.2

41.1

12.4

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-17Lab ID:



DateAnalyzed


Date Prepared


Antimony, Total

Silver, Total

0.166

0.459

mg/kg

mg/kg

2

2

0.074

0.074

10/24/12 19:36

10/24/12 19:36

1,6020A

1,6020A

PD

PD

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 34%

MDL

0.013

0.003

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-17Lab ID:



DateAnalyzed


Date Prepared


Tin, Total J4.47 mg/kg 26.69 10/31/12 15:35 1,6020A PD10/30/12 15:23 EPA 3050B

PrepMethod

Percent Solids: 34%

R

MDL

0.675

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-17Lab ID:



DateAnalyzed


Date Prepared


Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Thallium, Total

Vanadium, Total

14.2

24.8

0.671

0.516

37.5

8.55

39.5

38.8

234

21.8

1.60

0.213

44.2

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

10

10

10

10

10

10

10

10

10

10

10

10

10

0.352

2.11

0.211

0.141

1.41

0.352

1.41

0.422

1.41

0.704

0.704

0.141

0.704

10/24/12 17:50

10/24/12 17:50

10/24/12 17:50

10/24/12 17:50

10/24/12 17:50

10/24/12 17:50

10/24/12 17:50

10/24/12 17:50

10/24/12 17:50

10/24/12 17:50

10/24/12 17:50

10/24/12 17:50

10/24/12 17:50

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 34%

D2

MDL

0.044

0.541

0.061

0.019

0.330

0.037

0.080

0.136

0.313

0.106

0.175

0.019

0.032

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-17Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Calcium, Total

Iron, Total

Magnesium, Total

Potassium, Total

Sodium, Total

Zinc, Total

11100

2710

32400

6660

2940

16500

116

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

50

50

50

50

50

50

50

352

1760

704

352

352

352

35.2

10/24/12 16:37

10/24/12 16:37

10/24/12 16:37

10/24/12 16:37

10/24/12 16:37

10/24/12 16:37

10/24/12 16:37

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 34%

D

MDL

52.2

214.

72.6

43.4

53.2

30.3

9.15

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-19Lab ID:



DateAnalyzed


Date Prepared


Antimony, Total

Silver, Total

0.531

1.93

mg/kg

mg/kg

2

2

0.095

0.095

10/24/12 19:37

10/24/12 19:37

1,6020A

1,6020A

PD

PD

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 26%

MDL

0.017

0.004

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-19Lab ID:



DateAnalyzed


Date Prepared



PrepMethod

Percent Solids: 26%

R

MDL

0.965

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-19Lab ID:



DateAnalyzed


Date Prepared


Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Thallium, Total

Vanadium, Total

15.2

37.7

0.673

1.62

48.7

8.37

121

127

212

25.8

2.91

0.392

62.5

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

10

10

10

10

10

10

10

10

10

10

10

10

10

0.454

2.72

0.272

0.182

1.82

0.454

1.82

0.545

1.82

0.908

0.908

0.182

0.908

10/24/12 17:52

10/24/12 17:52

10/24/12 17:52

10/24/12 17:52

10/24/12 17:52

10/24/12 17:52

10/24/12 17:52

10/24/12 17:52

10/24/12 17:52

10/24/12 17:52

10/24/12 17:52

10/24/12 17:52

10/24/12 17:52

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 26%

D2

MDL

0.056

0.697

0.079

0.024

0.426

0.048

0.102

0.175

0.404

0.136

0.226

0.025

0.042

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-19Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Calcium, Total

Iron, Total

Magnesium, Total

Potassium, Total

Sodium, Total

Zinc, Total

11500

4330

34500

7960

3390

22700

328

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

50

50

50

50

50

50

50

454

2270

908

454

454

454

45.4

10/24/12 16:38

10/24/12 16:38

10/24/12 16:38

10/24/12 16:38

10/24/12 16:38

10/24/12 16:38

10/24/12 16:38

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 26%

D

MDL

67.3

276.

93.6

56.0

68.6

39.0

11.8

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-21Lab ID:



DateAnalyzed


Date Prepared


Antimony, Total

Silver, Total

0.563

2.00

mg/kg

mg/kg

2

2

0.094

0.094

10/24/12 19:38

10/24/12 19:38

1,6020A

1,6020A

PD

PD

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 25%

MDL

0.017

0.004

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-21Lab ID:



DateAnalyzed


Date Prepared



PrepMethod

Percent Solids: 25%

R

MDL

2.00

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-21Lab ID:



DateAnalyzed


Date Prepared


Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Thallium, Total

Vanadium, Total

15.4

38.1

0.597

1.66

48.5

8.75

123

134

217

27.3

2.78

0.399

61.9

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

10

10

10

10

10

10

10

10

10

10

10

10

10

0.494

2.96

0.296

0.197

1.97

0.494

1.97

0.592

1.97

0.987

0.987

0.197

0.987

10/24/12 17:54

10/24/12 17:54

10/24/12 17:54

10/24/12 17:54

10/24/12 17:54

10/24/12 17:54

10/24/12 17:54

10/24/12 17:54

10/24/12 17:54

10/24/12 17:54

10/24/12 17:54

10/24/12 17:54

10/24/12 17:54

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 25%

D2

MDL

0.061

0.758

0.086

0.026

0.463

0.052

0.112

0.190

0.439

0.148

0.246

0.027

0.045

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-21Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Calcium, Total

Iron, Total

Magnesium, Total

Potassium, Total

Sodium, Total

Zinc, Total

11200

4250

33700

8140

3490

23200

328

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

50

50

50

50

50

50

50

494

2470

987

494

494

494

49.4

10/24/12 16:39

10/24/12 16:39

10/24/12 16:39

10/24/12 16:39

10/24/12 16:39

10/24/12 16:39

10/24/12 16:39

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 25%

D

MDL

73.2

300.

102.

60.9

74.6

42.4

12.8

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-23Lab ID:



DateAnalyzed


Date Prepared


Antimony, Total

Silver, Total

0.326

1.56

mg/kg

mg/kg

2

2

0.067

0.067

10/24/12 19:40

10/24/12 19:40

1,6020A

1,6020A

PD

PD

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 35%

MDL

0.012

0.003

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-23Lab ID:



DateAnalyzed


Date Prepared



PrepMethod

Percent Solids: 35%

R

MDL

0.701

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-23Lab ID:



DateAnalyzed


Date Prepared


Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Thallium, Total

Vanadium, Total

12.9

26.0

0.506

1.31

37.4

7.05

87.6

97.7

178

22.6

2.34

0.282

44.4

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

10

10

10

10

10

10

10

10

10

10

10

10

10

0.360

2.16

0.216

0.144

1.44

0.360

1.44

0.431

1.44

0.719

0.719

0.144

0.719

10/24/12 17:59

10/24/12 17:59

10/24/12 17:59

10/24/12 17:59

10/24/12 17:59

10/24/12 17:59

10/24/12 17:59

10/24/12 17:59

10/24/12 17:59

10/24/12 17:59

10/24/12 17:59

10/24/12 17:59

10/24/12 17:59

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 35%

D2

MDL

0.044

0.552

0.063

0.019

0.337

0.038

0.081

0.139

0.320

0.108

0.179

0.019

0.033

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-23Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Calcium, Total

Iron, Total

Magnesium, Total

Potassium, Total

Sodium, Total

Zinc, Total

7950

15000

26000

5750

2280

16300

217

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

50

50

50

50

50

50

50

360

1800

719

360

360

360

36.0

10/24/12 16:43

10/24/12 16:43

10/24/12 16:43

10/24/12 16:43

10/24/12 16:43

10/24/12 16:43

10/24/12 16:43

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 35%

D

MDL

53.3

219.

74.1

44.3

54.3

30.9

9.34

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-25Lab ID:



DateAnalyzed


Date Prepared


Antimony, Total

Silver, Total

0.464

1.80

mg/kg

mg/kg

2

2

0.086

0.086

10/24/12 19:41

10/24/12 19:41

1,6020A

1,6020A

PD

PD

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 28%

MDL

0.015

0.004

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-25Lab ID:



DateAnalyzed


Date Prepared



PrepMethod

Percent Solids: 28%

R

MDL

0.921

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-25Lab ID:



DateAnalyzed


Date Prepared


Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Thallium, Total

Vanadium, Total

14.8

36.6

0.665

1.37

49.6

8.83

112

120

235

26.7

2.96

0.366

57.9

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

10

10

10

10

10

10

10

10

10

10

10

10

10

0.473

2.84

0.284

0.189

1.89

0.473

1.89

0.568

1.89

0.947

0.947

0.189

0.947

10/24/12 18:01

10/24/12 18:01

10/24/12 18:01

10/24/12 18:01

10/24/12 18:01

10/24/12 18:01

10/24/12 18:01

10/24/12 18:01

10/24/12 18:01

10/24/12 18:01

10/24/12 18:01

10/24/12 18:01

10/24/12 18:01

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 28%

D2

MDL

0.059

0.727

0.082

0.025

0.444

0.050

0.107

0.183

0.421

0.142

0.236

0.026

0.043

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-25Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Calcium, Total

Iron, Total

Magnesium, Total

Potassium, Total

Sodium, Total

Zinc, Total

10600

4510

31700

7430

3200

21400

270

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

50

50

50

50

50

50

50

473

2370

947

473

473

473

47.3

10/24/12 16:44

10/24/12 16:44

10/24/12 16:44

10/24/12 16:44

10/24/12 16:44

10/24/12 16:44

10/24/12 16:44

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 28%

D

MDL

70.2

288.

97.6

58.4

71.5

40.7

12.3

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-27Lab ID:



DateAnalyzed


Date Prepared


Antimony, Total

Silver, Total

0.284

1.46

mg/kg

mg/kg

2

2

0.069

0.069

10/24/12 19:42

10/24/12 19:42

1,6020A

1,6020A

PD

PD

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 34%

MDL

0.012

0.003

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-27Lab ID:



DateAnalyzed


Date Prepared



PrepMethod

Percent Solids: 34%

R

MDL

0.731

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-27Lab ID:



DateAnalyzed


Date Prepared


Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Thallium, Total

Vanadium, Total

13.3

29.3

0.630

1.00

43.7

7.46

82.2

89.0

219

22.3

2.37

0.278

47.0

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

10

10

10

10

10

10

10

10

10

10

10

10

10

0.350

2.10

0.210

0.140

1.40

0.350

1.40

0.420

1.40

0.701

0.701

0.140

0.701

10/24/12 18:03

10/24/12 18:03

10/24/12 18:03

10/24/12 18:03

10/24/12 18:03

10/24/12 18:03

10/24/12 18:03

10/24/12 18:03

10/24/12 18:03

10/24/12 18:03

10/24/12 18:03

10/24/12 18:03

10/24/12 18:03

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 34%

D2

MDL

0.043

0.538

0.061

0.019

0.329

0.037

0.079

0.135

0.312

0.105

0.174

0.019

0.032

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-27Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Calcium, Total

Iron, Total

Magnesium, Total

Potassium, Total

Sodium, Total

Zinc, Total

9520

4110

29400

6570

2860

17300

201

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

50

50

50

50

50

50

50

350

1750

701

350

350

350

35.0

10/24/12 16:45

10/24/12 16:45

10/24/12 16:45

10/24/12 16:45

10/24/12 16:45

10/24/12 16:45

10/24/12 16:45

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 34%

D

MDL

52.0

213.

72.2

43.2

53.0

30.1

9.10

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-29Lab ID:



DateAnalyzed


Date Prepared


Antimony, Total

Silver, Total

0.285

1.43

mg/kg

mg/kg

2

2

0.078

0.078

10/24/12 19:43

10/24/12 19:43

1,6020A

1,6020A

PD

PD

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 30%

MDL

0.014

0.004

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-29Lab ID:



DateAnalyzed


Date Prepared



PrepMethod

Percent Solids: 30%

R

MDL

0.777

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-29Lab ID:



DateAnalyzed


Date Prepared


Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Thallium, Total

Vanadium, Total

14.6

34.2

0.663

1.12

49.1

8.67

96.1

105

262

26.3

2.85

0.322

52.7

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

10

10

10

10

10

10

10

10

10

10

10

10

10

0.424

2.54

0.254

0.169

1.69

0.424

1.69

0.508

1.69

0.847

0.847

0.169

0.847

10/24/12 18:04

10/24/12 18:04

10/24/12 18:04

10/24/12 18:04

10/24/12 18:04

10/24/12 18:04

10/24/12 18:04

10/24/12 18:04

10/24/12 18:04

10/24/12 18:04

10/24/12 18:04

10/24/12 18:04

10/24/12 18:04

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 30%

D2

MDL

0.052

0.651

0.074

0.022

0.397

0.045

0.096

0.164

0.377

0.127

0.211

0.023

0.039

Serial_No:11051209:46

of 279

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

SAMPLE RESULTS



L1218042-29Lab ID:



DateAnalyzed


Date Prepared


Aluminum, Total

Calcium, Total

Iron, Total

Magnesium, Total

Potassium, Total

Sodium, Total

Zinc, Total

10800

4770

32900

7970

3260

22100

232

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

50

50

50

50

50

50

50

424

2120

847

424

424

424

42.4

10/24/12 16:46

10/24/12 16:46

10/24/12 16:46

10/24/12 16:46

10/24/12 16:46

10/24/12 16:46

10/24/12 16:46

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

EPA 3050B

PrepMethod

Percent Solids: 30%

D

MDL

62.8

258.

87.3

52.3

64.0

36.4

11.0

Serial_No:11051209:46

of 279

FF

Parameter

Parameter

Result

Result

Dilution Factor

Dilution Factor

Qualifier

Qualifier

Units

Units

RL

RL


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

DateAnalyzed

DateAnalyzed

AnalyticalMethod

AnalyticalMethod

Analyst

Analyst

Date Prepared

Date Prepared

11/05/12

Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Nickel, Total

Potassium, Total

Selenium, Total

Silver, Total

Sodium, Total

Thallium, Total

Tin, Total

Vanadium, Total

Zinc, Total

Antimony, Total

Silver, Total

J

J

J

J

J

J

J

J

J

J

J

ND

ND

0.0001

0.0001

ND

ND

ND

ND

ND

0.0003

0.009

ND

0.013

0.0004

0.0003

ND

ND

ND

0.017

0.00003

ND

0.001

0.003

ND

ND

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/l

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

2

2

0.100

0.0005

0.0005

0.0005

0.0005

0.0005

0.100

0.001

0.0002

0.0010

0.050

0.001

0.070

0.0005

0.0005

0.100

0.005

0.0003

0.100

0.00020

0.0005

0.005

0.010

0.050

0.050

10/23/12 18:02

10/23/12 18:02

10/23/12 18:02

10/23/12 18:02

10/23/12 18:02

10/23/12 18:02

10/23/12 18:02

10/23/12 18:02

10/23/12 18:42

10/23/12 18:02

10/23/12 18:02

10/23/12 18:02

10/23/12 18:02

10/23/12 18:02

10/23/12 18:02

10/23/12 18:02

10/23/12 18:02

10/23/12 18:02

10/23/12 18:02

10/23/12 18:02

10/23/12 18:02

10/23/12 18:02

10/23/12 18:02

10/24/12 19:24

10/24/12 19:24

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/17/12 12:00

10/23/12 10:15

10/23/12 10:15

Total Metals - Mansfield Lab for sample(s): 11 Batch: WG567654-1

Total Metals - Mansfield Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG568938-1

EPA 3020ADigestion Method:

Prep Information

MDL

MDL

0.023

0.00003

0.0001

0.0001

0.0001

0.0001

0.019

0.0003

0.00002

0.0003

0.008

0.0001

0.002

0.0001

0.0002

0.006

0.0003

0.00002

0.006

0.00001

0.0001

0.0001

0.001

0.009

0.002

Serial_No:11051209:46

of 279

Parameter

Parameter

Result

Result

Dilution Factor

Dilution Factor

Qualifier

Qualifier

Units

Units

RL

RL


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

DateAnalyzed

DateAnalyzed

AnalyticalMethod

AnalyticalMethod

Analyst

Analyst

Date Prepared

Date Prepared

11/05/12

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Nickel, Total

Potassium, Total

Selenium, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

Tin, Total

J

J

J

J

J

J

J

J

J

J

ND

0.014

ND

ND

ND

ND

ND

ND

0.039

2.96

ND

ND

0.068

0.041

2.20

ND

3.39

0.004

0.108

0.388

1.54

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

2

10.0

0.050

0.300

0.030

0.020

50.0

0.200

0.050

0.200

20.0

0.060

10.0

0.200

0.100

10.0

0.100

10.0

0.020

0.100

1.00

5.00

10/24/12 16:22

10/24/12 17:26

10/24/12 17:26

10/24/12 17:26

10/24/12 17:26

10/24/12 16:22

10/24/12 17:26

10/24/12 17:26

10/24/12 17:26

10/24/12 16:22

10/24/12 17:26

10/24/12 16:22

10/24/12 17:26

10/24/12 17:26

10/24/12 16:22

10/24/12 17:26

10/24/12 16:22

10/24/12 17:26

10/24/12 17:26

10/24/12 16:22

10/31/12 15:23

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

1,6020A

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

PD

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/23/12 10:15

10/30/12 15:23



EPA 3050B

EPA 3050B

Digestion Method:

Digestion Method:

Prep Information

Prep Information

MDL

MDL

1.48

0.006

0.077

0.009

0.003

6.08

0.047

0.005

0.011

2.06

0.019

1.23

0.045

0.015

1.51

0.025

0.860

0.003

0.005

0.260

0.505

Serial_No:11051209:46

of 279


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

EPA 3050BDigestion Method:

Prep Information

Serial_No:11051209:46

of 279

Aluminum, Total

Antimony, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Nickel, Total

Potassium, Total

Selenium, Total

Sodium, Total

Thallium, Total

Tin, Total

Vanadium, Total

94

92

91

92

87

89

94

90

105

94

90

92

94

90

92

93

87

92

90

88

94

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


Total Metals - Mansfield Lab Associated sample(s): 11 Batch: WG567654-2 SRM Lot Number: A2METSPIKE


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

Qual Qual Qual

Serial_No:11051209:46

of 279

Zinc, Total

Silver, Total

Antimony, Total

Silver, Total

94

91

105

104

-

-

-

-

80-120

80-120

75-125

75-125

-

-

-

-

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


Total Metals - Mansfield Lab Associated sample(s): 11 Batch: WG567654-2 SRM Lot Number: A2METSPIKE

Total Metals - Mansfield Lab Associated sample(s): 11 Batch: WG567654-3 SRM Lot Number: S3SPIKE

Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG568938-2 SRM Lot Number: S3SPIKE


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

Serial_No:11051209:46

of 279

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Nickel, Total

Potassium, Total

Selenium, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

107

92

88

98

97

103

96

103

98

99

95

108

100

97

100

92

107

94

101

103

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG568940-2 SRM Lot Number: A2METSPIKE


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

Serial_No:11051209:46

of 279

Tin, Total 112 - 75-125 - 20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG570724-2 SRM Lot Number: S3SPIKE


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

Serial_No:11051209:46

of 279

Antimony, Total

Silver, Total

0.062

0.682

0.398

1.97

25

96

-

-

-

-

75-125

75-125

-

-

20

20

ParameterNative Sample

MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits

Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG568938-4 QC Sample: L1218042-01 Client ID: TN005SG-000014-20121005

1.34

1.34

MS Added

Matrix Spike AnalysisBatch Quality Control

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

Qual

Q

Qual Qual

Serial_No:11051209:46

of 279

Aluminum, Total

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Calcium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Iron, Total

Lead, Total

Magnesium, Total

Manganese, Total

Nickel, Total

Potassium, Total

Selenium, Total

Sodium, Total

Thallium, Total

Vanadium, Total

Zinc, Total

2960

5.18

14.8

0.288

1.06

15800

18.6

3.68

27.8

6940

34.7

2660

161.

9.90

896.

1.98

3760

0.509

9.88

54.2

4100

120

127

61.4

61.0

20600

139

133

155

9390

155

3420

303

138

1590

118

4520

116

135

190

179

90

88

96

94

752

94

101

100

384

94

119

111

100

109

91

119

90

98

106

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

75-125

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits


638

128

128

63.8

63.8

638

128

128

128

638

128

638

128

128

638

128

638

128

128

128

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

Q

Q

Q

Serial_No:11051209:46

of 279

Tin, Total 5.14 22.5 98 - - 75-125 - 20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits


17.6

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

Serial_No:11051209:46

of 279

Antimony, Total

Silver, Total

Aluminum, Total

Calcium, Total

Iron, Total

Magnesium, Total

Potassium, Total

Sodium, Total

Zinc, Total

0.062

0.682

2960

15800

6940

2660

896.

3760

54.2

0.052

0.603

2910

31200

7190

2610

882

3920

70.7

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

18

12

2

66

4

2

2

4

26

20

20

20

20

20

20

20

20

20

Units RPDParameter Native Sample Duplicate Sample RPD Limits

Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG568938-3 QC Sample: L1218042-01 ClientID: TN005SG-000014-20121005


NEWTOWN CREEK RI

120782-01.01

Project Name:

Project Number:

L1218042Lab Number:

Report Date:

Lab Duplicate AnalysisBatch Quality Control

11/05/12

Qual

Q

Q

Serial_No:11051209:46

of 279

Arsenic, Total

Barium, Total

Beryllium, Total

Cadmium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Selenium, Total

Thallium, Total

Vanadium, Total

Tin, Total

5.18

14.8

0.288

1.06

18.6

3.68

27.8

34.7

161.

9.90

1.98

0.509

9.88

5.14

4.87

52.7

0.166

0.366

18.4

3.43

29.4

95.2

171

9.15

0.424

0.094

9.84

4.32

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

6

112

54

97

1

7

6

93

6

8

129

138

0

17

20

20

20

20

20

20

20

20

20

20

20

20

20

20




NEWTOWN CREEK RI

120782-01.01

Project Name:

Project Number:

L1218042Lab Number:

Report Date:


11/05/12

Q

Q

Q

Q

Q

Q

Serial_No:11051209:46

of 279

Aluminum, Total

Calcium, Total

Iron, Total

Magnesium, Total

Sodium, Total

Arsenic, Total

Barium, Total

Chromium, Total

Cobalt, Total

Copper, Total

Lead, Total

Manganese, Total

Nickel, Total

Vanadium, Total

2960

15800

6940

2660

3760

5.18

14.8

18.6

3.68

27.8

34.7

161.

9.90

9.88

2730

15800

7210

2460

3630

4.92

14.7

17.5

3.42

27.8

36.2

158

9.96

10.2

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

8

0

4

8

3

5

1

6

7

0

4

2

1

3

10

10

10

10

10

10

10

10

10

10

10

10

10

10

Units % DParameter Native Sample Serial Dilution RPD Limits



NEWTOWN CREEK RI

120782-01.01

Project Name:

Project Number:

L1218042Lab Number:

Report Date:

Lab Serial Dilution Analysis

Batch Quality Control 11/05/12

Qual

Serial_No:11051209:46

of 279

INORGANICS&

MISCELLANEOUS

Serial_No:11051209:46

of 279

FF


Parameter ResultDilution Factor

Matrix: Sediment


L1218042-01Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified

Total Organic Carbon - Mansfield Lab

General Chemistry - Westborough Lab

General Chemistry - Mansfield Lab

Total Organic Carbon (Rep1)


Cyanide, Total

pH

Nitrogen, Ammonia

Nitrogen, Nitrate/Nitrite

Nitrogen, Total Kjeldahl

Solids, Total

% Soot (Rep 1)

% Soot (Rep 2)

0.522

0.601

ND

8.0

13

3.7

640

71.9

0.162

0.163

%

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

%

%

%

1

1

1

1

1

1

1

1

1

1

0.010

0.010

1.3

-

10

2.3

190

0.100

0.010

0.010

10/24/12 07:14

10/24/12 07:14

10/18/12 15:39

10/10/12 14:30

10/18/12 21:42

10/16/12 03:35

10/18/12 22:06

10/09/12 16:25

10/24/12 07:14

10/24/12 07:14

1,9060

1,9060

1,9010B/9012A

1,9045C

30,4500NH3-BH

30,4500NO3-F

30,4500N-C

30,2540G

91,-

91,-

NR

NR

JO

ML

AT

DB

AT

KB

NR

NR

Date Prepared

-

-

10/16/12 15:00

-

10/16/12 14:45

10/15/12 01:00

10/16/12 23:45

-

-

-

11/05/12

MDL

0.010

0.010

0.30

NA

1.8

0.39

74.

0.100

NA

NA

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-01Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified

General Chemistry - Westborough LabPhosphorus, Total

Sulfide

110

230

mg/kg

mg/kg

1.8

100

12

70

10/18/12 11:00

10/10/12 14:30

30,4500P-E

1,9030B

SD

MP

Date Prepared

-

10/10/12 12:45

11/05/12

D

MDL

3.5

16.

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-03Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified






Cyanide, Total

pH

Nitrogen, Ammonia



Solids, Total

% Soot (Rep 1)

% Soot (Rep 2)

2.05

1.60

ND

7.8

15

6.0

1600

55.4

0.689

0.899

%

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

%

%

%

1

1

1

1

1

1

1

1

1

1

0.010

0.010

1.8

-

13

3.0

250

0.100

0.010

0.010

10/24/12 07:14

10/24/12 07:14

10/18/12 15:40

10/10/12 14:30

10/18/12 21:43

10/16/12 03:39

10/18/12 22:07

10/09/12 16:25

10/24/12 07:14

10/24/12 07:14

1,9060

1,9060

1,9010B/9012A

1,9045C

30,4500NH3-BH

30,4500NO3-F

30,4500N-C

30,2540G

91,-

91,-

NR

NR

JO

ML

AT

DB

AT

KB

NR

NR

Date Prepared

-

-

10/16/12 15:00

-

10/16/12 14:45

10/15/12 01:00

10/16/12 23:45

-

-

-

11/05/12

MDL

0.010

0.010

0.41

NA

2.4

0.51

96.

0.100

NA

NA

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-03Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified


Sulfide

320

480

mg/kg

mg/kg

4.6

100

42

90

10/18/12 11:00

10/10/12 14:32

30,4500P-E

1,9030B

SD

MP

Date Prepared

-

10/10/12 12:45

11/05/12

D

MDL

12.

20.

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-05Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified






Cyanide, Total

pH

Nitrogen, Ammonia



Solids, Total

% Soot (Rep 1)

% Soot (Rep 2)

2.68

2.49

ND

7.8

26

6.4

3000

41.4

0.599

0.581

%

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

%

%

%

1

1

1

1

1

1

1

1

1

1

0.010

0.010

2.4

-

18

4.0

350

0.100

0.010

0.010

10/24/12 07:14

10/24/12 07:14

10/18/12 15:41

10/10/12 14:30

10/18/12 21:44

10/16/12 03:40

10/18/12 22:08

10/09/12 16:25

10/24/12 07:14

10/24/12 07:14

1,9060

1,9060

1,9010B/9012A

1,9045C

30,4500NH3-BH

30,4500NO3-F

30,4500N-C

30,2540G

91,-

91,-

NR

NR

JO

ML

AT

DB

AT

KB

NR

NR

Date Prepared

-

-

10/16/12 15:00

-

10/16/12 14:45

10/15/12 01:00

10/16/12 23:45

-

-

-

11/05/12

MDL

0.010

0.010

0.55

NA

3.2

0.68

140

0.100

NA

NA

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-05Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified


Sulfide

540

2500

mg/kg

mg/kg

4.9

100

59

120

10/18/12 11:00

10/10/12 14:32

30,4500P-E

1,9030B

SD

MP

Date Prepared

-

10/10/12 12:45

11/05/12

D

MDL

17.

27.

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-07Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified






Cyanide, Total

pH

Nitrogen, Ammonia



Solids, Total

% Soot (Rep 1)

% Soot (Rep 2)

1.29

1.20

ND

7.9

16

6.2

1500

50.5

0.338

0.208

%

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

%

%

%

1

1

1

1

1

1

1

1

1

1

0.010

0.010

1.8

-

14

3.3

290

0.100

0.010

0.010

10/24/12 07:14

10/24/12 07:14

10/18/12 15:43

10/10/12 14:30

10/18/12 21:45

10/16/12 03:41

10/18/12 22:09

10/09/12 16:25

10/24/12 07:14

10/24/12 07:14

1,9060

1,9060

1,9010B/9012A

1,9045C

30,4500NH3-BH

30,4500NO3-F

30,4500N-C

30,2540G

91,-

91,-

NR

NR

JO

ML

AT

DB

AT

KB

NR

NR

Date Prepared

-

-

10/16/12 15:00

-

10/16/12 14:45

10/15/12 01:00

10/16/12 23:45

-

-

-

11/05/12

MDL

0.010

0.010

0.43

NA

2.4

0.56

110

0.100

NA

NA

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-07Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified


Sulfide

400

1000

mg/kg

mg/kg

4.9

100

48

99

10/18/12 11:00

10/10/12 14:32

30,4500P-E

1,9030B

SD

MP

Date Prepared

-

10/10/12 12:45

11/05/12

D

MDL

14.

22.

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-09Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified






Cyanide, Total

pH

Nitrogen, Ammonia



Solids, Total

% Soot (Rep 1)

% Soot (Rep 2)

J

5.09

4.78

0.47

8.0

ND

2.9

360

77.8

0.047

0.047

%

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

%

%

%

1

1

1

1

1

1

1

1

1

1

0.010

0.010

1.2

-

9.1

2.1

190

0.100

0.010

0.010

10/24/12 07:14

10/24/12 07:14

10/18/12 15:44

10/10/12 14:30

10/18/12 21:46

10/16/12 03:41

10/18/12 22:10

10/09/12 16:25

10/24/12 07:14

10/24/12 07:14

1,9060

1,9060

1,9010B/9012A

1,9045C

30,4500NH3-BH

30,4500NO3-F

30,4500N-C

30,2540G

91,-

91,-

NR

NR

JO

ML

AT

DB

AT

KB

NR

NR

Date Prepared

-

-

10/16/12 15:00

-

10/16/12 14:45

10/15/12 01:00

10/16/12 23:45

-

-

-

11/05/12

MDL

0.010

0.010

0.29

NA

1.6

0.36

73.

0.100

NA

NA

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-09Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified


Sulfide

130

35

mg/kg

mg/kg

2

2

13

1.3

10/18/12 11:00

10/10/12 14:33

30,4500P-E

1,9030B

SD

MP

Date Prepared

-

10/10/12 12:45

11/05/12

D

MDL

3.6

0.29

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-13Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified






Cyanide, Total

pH

Nitrogen, Ammonia



Solids, Total

% Soot (Rep 1)

% Soot (Rep 2)

3.73

4.11

ND

7.7

120

9.8

8100

26.7

0.066

0.084

%

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

%

%

%

1

1

1

1

1

1

1

1

1

1

0.010

0.010

3.6

-

28

6.2

520

0.100

0.010

0.010

10/24/12 07:14

10/24/12 07:14

10/18/12 15:44

10/10/12 14:30

10/18/12 21:46

10/16/12 03:42

10/18/12 22:11

10/09/12 16:25

10/24/12 07:14

10/24/12 07:14

1,9060

1,9060

1,9010B/9012A

1,9045C

30,4500NH3-BH

30,4500NO3-F

30,4500N-C

30,2540G

91,-

91,-

NR

NR

JO

ML

AT

DB

AT

KB

NR

NR

Date Prepared

-

-

10/16/12 15:00

-

10/16/12 14:45

10/15/12 01:00

10/16/12 23:45

-

-

-

11/05/12

MDL

0.010

0.010

0.83

NA

5.0

1.0

200

0.100

NA

NA

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-13Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified


Sulfide

650

5500

mg/kg

mg/kg

4.7

200

88

370

10/18/12 11:00

10/10/12 14:34

30,4500P-E

1,9030B

SD

MP

Date Prepared

-

10/10/12 12:45

11/05/12

D

MDL

25.

84.

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-15Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified






Cyanide, Total

pH

Nitrogen, Ammonia



Solids, Total

% Soot (Rep 1)

% Soot (Rep 2)

4.34

4.40

ND

7.7

120

7.3

6500

25.4

0.094

0.091

%

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

%

%

%

1

1

1

1

1

1

1

1

1

1

0.010

0.010

3.9

-

28

6.5

580

0.100

0.010

0.010

10/24/12 07:14

10/24/12 07:14

10/18/12 15:45

10/10/12 14:30

10/18/12 21:47

10/16/12 03:43

10/18/12 22:11

10/09/12 16:25

10/24/12 07:14

10/24/12 07:14

1,9060

1,9060

1,9010B/9012A

1,9045C

30,4500NH3-BH

30,4500NO3-F

30,4500N-C

30,2540G

91,-

91,-

NR

NR

JO

ML

AT

DB

AT

KB

NR

NR

Date Prepared

-

-

10/16/12 15:00

-

10/16/12 14:45

10/15/12 01:00

10/16/12 23:45

-

-

-

11/05/12

MDL

0.010

0.010

0.91

NA

5.1

1.1

220

0.100

NA

NA

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-15Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified


Sulfide

680

5800

mg/kg

mg/kg

5

200

98

390

10/18/12 11:00

10/10/12 14:35

30,4500P-E

1,9030B

SD

MP

Date Prepared

-

10/10/12 12:45

11/05/12

D

MDL

28.

88.

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-17Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified






Cyanide, Total

pH

Nitrogen, Ammonia



Solids, Total

% Soot (Rep 1)

% Soot (Rep 2)

2.85

2.31

ND

7.7

96

9.3

4300

34.3

0.070

0.068

%

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

%

%

%

1

1

1

1

1

1

1

1

1

1

0.010

0.010

2.9

-

21

4.8

430

0.100

0.010

0.010

10/24/12 07:14

10/24/12 07:14

10/18/12 15:46

10/10/12 14:30

10/18/12 21:51

10/16/12 03:43

10/18/12 22:15

10/09/12 16:25

10/24/12 07:14

10/24/12 07:14

1,9060

1,9060

1,9010B/9012A

1,9045C

30,4500NH3-BH

30,4500NO3-F

30,4500N-C

30,2540G

91,-

91,-

NR

NR

JO

ML

AT

DB

AT

KB

NR

NR

Date Prepared

-

-

10/16/12 15:00

-

10/16/12 14:45

10/15/12 01:00

10/16/12 23:45

-

-

-

11/05/12

MDL

0.010

0.010

0.67

NA

3.8

0.82

160

0.100

NA

NA

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-17Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified


Sulfide

660

1700

mg/kg

mg/kg

4.6

100

67

140

10/18/12 11:00

10/10/12 16:48

30,4500P-E

1,9030B

SD

MP

Date Prepared

-

10/10/12 12:45

11/05/12

D

MDL

19.

33.

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-19Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified






Cyanide, Total

pH

Nitrogen, Ammonia



Solids, Total

% Soot (Rep 1)

% Soot (Rep 2)

4.68

5.10

ND

7.8

140

12

7100

25.5

0.121

0.136

%

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

%

%

%

1

1

1

1

1

1

1

1

1

1

0.010

0.010

3.8

-

27

6.5

540

0.100

0.010

0.010

10/24/12 07:14

10/24/12 07:14

10/18/12 15:47

10/10/12 14:30

10/18/12 21:52

10/16/12 03:44

10/18/12 22:16

10/09/12 16:25

10/24/12 07:14

10/24/12 07:14

1,9060

1,9060

1,9010B/9012A

1,9045C

30,4500NH3-BH

30,4500NO3-F

30,4500N-C

30,2540G

91,-

91,-

NR

NR

JO

ML

AT

DB

AT

KB

NR

NR

Date Prepared

-

-

10/16/12 15:00

-

10/16/12 14:45

10/15/12 01:00

10/16/12 23:45

-

-

-

11/05/12

MDL

0.010

0.010

0.90

NA

4.9

1.1

210

0.100

NA

NA

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-19Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified


Sulfide

680

6000

mg/kg

mg/kg

4.8

100

94

200

10/18/12 11:00

10/10/12 16:49

30,4500P-E

1,9030B

SD

MP

Date Prepared

-

10/10/12 12:45

11/05/12

D

MDL

26.

44.

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-21Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified






Cyanide, Total

pH

Nitrogen, Ammonia



Solids, Total

% Soot (Rep 1)

% Soot (Rep 2)

4.39

4.05

ND

7.8

140

9.8

7000

25.2

0.141

0.193

%

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

%

%

%

1

1

1

1

1

1

1

1

1

1

0.010

0.010

3.7

-

29

6.6

560

0.100

0.010

0.010

10/24/12 07:14

10/24/12 07:14

10/18/12 15:48

10/10/12 14:30

10/18/12 21:52

10/16/12 03:45

10/18/12 22:17

10/09/12 16:25

10/24/12 07:14

10/24/12 07:14

1,9060

1,9060

1,9010B/9012A

1,9045C

30,4500NH3-BH

30,4500NO3-F

30,4500N-C

30,2540G

91,-

91,-

NR

NR

JO

ML

AT

DB

AT

KB

NR

NR

Date Prepared

-

-

10/16/12 15:00

-

10/16/12 14:45

10/15/12 01:00

10/16/12 23:45

-

-

-

11/05/12

MDL

0.010

0.010

0.87

NA

5.3

1.1

220

0.100

NA

NA

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-21Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified


Sulfide

610

7000

mg/kg

mg/kg

4.7

200

93

400

10/18/12 11:00

10/10/12 17:08

30,4500P-E

1,9030B

SD

MP

Date Prepared

-

10/10/12 12:45

11/05/12

D

MDL

26.

89.

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-23Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified






Cyanide, Total

pH

Nitrogen, Ammonia



Solids, Total

% Soot (Rep 1)

% Soot (Rep 2)

3.64

3.88

ND

7.8

56

8.8

5100

35.3

0.182

0.184

%

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

%

%

%

1

1

1

1

1

1

1

1

1

1

0.010

0.010

2.8

-

21

4.7

410

0.100

0.010

0.010

10/24/12 07:14

10/24/12 07:14

10/18/12 15:50

10/10/12 14:30

10/18/12 21:53

10/16/12 03:48

10/18/12 22:17

10/09/12 16:25

10/24/12 07:14

10/24/12 07:14

1,9060

1,9060

1,9010B/9012A

1,9045C

30,4500NH3-BH

30,4500NO3-F

30,4500N-C

30,2540G

91,-

91,-

NR

NR

JO

ML

AT

DB

AT

KB

NR

NR

Date Prepared

-

-

10/16/12 15:00

-

10/16/12 14:45

10/15/12 01:00

10/16/12 23:45

-

-

-

11/05/12

MDL

0.010

0.010

0.65

NA

3.7

0.80

160

0.100

NA

NA

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-23Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified


Sulfide

570

3400

mg/kg

mg/kg

4.8

100

68

140

10/18/12 11:00

10/10/12 16:50

30,4500P-E

1,9030B

SD

MP

Date Prepared

-

10/10/12 12:45

11/05/12

D

MDL

19.

32.

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-25Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified






Cyanide, Total

pH

Nitrogen, Ammonia



Solids, Total

% Soot (Rep 1)

% Soot (Rep 2)

J

4.43

4.52

1.2

7.7

82

9.6

6600

27.8

0.179

0.168

%

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

%

%

%

1

1

1

1

1

1

1

1

1

1

0.010

0.010

3.5

-

26

6.0

520

0.100

0.010

0.010

10/24/12 07:14

10/24/12 07:14

10/18/12 15:52

10/10/12 14:30

10/18/12 21:54

10/16/12 03:48

10/18/12 22:18

10/09/12 16:25

10/24/12 07:14

10/24/12 07:14

1,9060

1,9060

1,9010B/9012A

1,9045C

30,4500NH3-BH

30,4500NO3-F

30,4500N-C

30,2540G

91,-

91,-

NR

NR

JO

ML

AT

DB

AT

KB

NR

NR

Date Prepared

-

-

10/16/12 15:00

-

10/16/12 14:45

10/15/12 01:00

10/16/12 23:45

-

-

-

11/05/12

MDL

0.010

0.010

0.82

NA

4.6

1.0

200

0.100

NA

NA

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-25Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified


Sulfide

640

4600

mg/kg

mg/kg

4.9

100

88

180

10/18/12 11:00

10/10/12 16:50

30,4500P-E

1,9030B

SD

MP

Date Prepared

-

10/10/12 12:45

11/05/12

D

MDL

25.

40.

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-27Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified






Cyanide, Total

pH

Nitrogen, Ammonia



Solids, Total

% Soot (Rep 1)

% Soot (Rep 2)

J

3.61

3.43

0.67

7.9

77

8.5

5300

33.5

0.161

0.189

%

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

%

%

%

1

1

1

1

1

1

1

1

1

1

0.010

0.010

2.7

-

21

5.0

410

0.100

0.010

0.010

10/24/12 07:14

10/24/12 07:14

10/18/12 15:53

10/10/12 14:30

10/18/12 21:55

10/16/12 03:49

10/18/12 22:19

10/09/12 16:25

10/24/12 07:14

10/24/12 07:14

1,9060

1,9060

1,9010B/9012A

1,9045C

30,4500NH3-BH

30,4500NO3-F

30,4500N-C

30,2540G

91,-

91,-

NR

NR

JO

ML

AT

DB

AT

KB

NR

NR

Date Prepared

-

-

10/16/12 15:00

-

10/16/12 14:45

10/15/12 01:00

10/16/12 23:45

-

-

-

11/05/12

MDL

0.010

0.010

0.64

NA

3.8

0.84

160

0.100

NA

NA

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-27Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified


Sulfide

500

3800

mg/kg

mg/kg

4.9

100

73

150

10/18/12 11:00

10/10/12 16:51

30,4500P-E

1,9030B

SD

MP

Date Prepared

-

10/10/12 12:45

11/05/12

D

MDL

20.

33.

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-29Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified






Cyanide, Total

pH

Nitrogen, Ammonia



Solids, Total

% Soot (Rep 1)

% Soot (Rep 2)

4.07

3.95

ND

7.8

110

9.2

6500

29.8

0.278

0.270

%

%

mg/kg

SU

mg/kg

mg/kg

mg/kg

%

%

%

1

1

1

1

1

1

1

1

1

1

0.010

0.010

3.2

-

23

5.6

490

0.100

0.010

0.010

10/24/12 07:14

10/24/12 07:14

10/18/12 15:54

10/10/12 14:30

10/18/12 21:56

10/16/12 03:50

10/18/12 22:20

10/09/12 16:25

10/24/12 07:14

10/24/12 07:14

1,9060

1,9060

1,9010B/9012A

1,9045C

30,4500NH3-BH

30,4500NO3-F

30,4500N-C

30,2540G

91,-

91,-

NR

NR

JO

ML

AT

DB

AT

KB

NR

NR

Date Prepared

-

-

10/16/12 15:00

-

10/16/12 14:45

10/15/12 01:00

10/16/12 23:45

-

-

-

11/05/12

MDL

0.010

0.010

0.76

NA

4.2

0.95

190

0.100

NA

NA

Serial_No:11051209:46

of 279

FF



Matrix: Sediment


L1218042-29Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified


Sulfide

610

5200

mg/kg

mg/kg

4.6

100

77

170

10/18/12 11:00

10/10/12 16:52

30,4500P-E

1,9030B

SD

MP

Date Prepared

-

10/10/12 12:45

11/05/12

D

MDL

22.

38.

Serial_No:11051209:46

of 279

FF

SRM 1650BClient ID:10/06/12 12:00Date Collected:10/08/12Date Received:


Matrix: Sediment


L1218042-32Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Field Prep:

DateAnalyzed


Not Specified





% Soot (Rep 1)

% Soot (Rep 2)

1.73

1.76

5.52

6.96

%

%

%

%

1

1

1

1

0.010

0.010

0.010

0.010

10/24/12 07:14

10/24/12 07:14

10/24/12 07:14

10/24/12 07:14

1,9060

1,9060

91,-

91,-

NR

NR

NR

NR

Date Prepared

-

-

-

-

11/05/12

MDL

0.010

0.010

NA

NA

Serial_No:11051209:46

of 279

FF



Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

DateAnalyzed


Date Prepared

11/05/12

Sulfide



% Soot (Rep 1)

% Soot (Rep 2)


Cyanide, Total

Cyanide, Total

Nitrogen, Ammonia


Phosphorus, Total

J

ND

ND

ND

ND

ND

ND

ND

ND

1.4

ND

ND

mg/kg

%

%

%

%

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

1

1

1

1

1

1

1

1

1

1

1

0.50

0.010

0.010

0.010

0.010

1.0

0.94

0.94

7.5

150

5.0

10/10/12 14:29

10/24/12 07:14

10/24/12 07:14

10/24/12 07:14

10/24/12 07:14

10/16/12 03:32

10/18/12 15:34

10/18/12 15:34

10/18/12 21:40

10/18/12 22:04

10/18/12 11:00

1,9030B

1,9060

1,9060

91,-

91,-

30,4500NO3-F

1,9010B/9012A

1,9010B/9012A

30,4500NH3-BH

30,4500N-C

30,4500P-E

MP

NR

NR

NR

NR

DB

JO

JO

AT

AT

SD

10/10/12 12:45

-

-

-

-

10/15/12 01:00

10/16/12 15:00

10/16/12 15:00

10/16/12 14:45

10/16/12 23:45

-

General Chemistry - Westborough Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566113-1

Total Organic Carbon - Mansfield Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566725-1

General Chemistry - Mansfield Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566732-1


General Chemistry - Westborough Lab for sample(s): 01,03,05,07,09,13,15,17,19,21 Batch: WG567329-1

General Chemistry - Westborough Lab for sample(s): 23,25,27,29 Batch: WG567330-1




MDL

0.11

0.010

0.010

NA

NA

0.02

0.22

0.22

0.01

0.04

1.4

Serial_No:11051209:46

of 279

Sulfide

pH


Cyanide, Total

Cyanide, Total

Nitrogen, Ammonia


88

100

98

110

112

99

101

-

-

-

112

110

-

-

75-125

99-101

90-110

80-120

80-120

83-115

84-115

-

-

-

2

2

-

-

25

20

35

35

20

26

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery


General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566113-2



General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21 Batch: WG567329-2 WG567329-3

General Chemistry - Westborough Lab Associated sample(s): 23,25,27,29 Batch: WG567330-2 WG567330-3




Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

Qual Qual Qual

Serial_No:11051209:46

of 279

Phosphorus, Total 103 - 52-148 - 20

ParameterLCS

%RecoveryLCSD

%Recovery%Recovery




Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

Serial_No:11051209:46

of 279

Sulfide



% Soot (Rep 1)

% Soot (Rep 2)


Cyanide, Total

Cyanide, Total

Nitrogen, Ammonia

1000

0.522

0.601

0.162

0.163

3.7

ND

ND

110

1100

2.71

2.93

1.23

1.33

170

14

25

1300

390

118

123

93

93

93

100

90

90

-

-

-

-

-

-

13

24

-

-

-

-

-

-

-

98

90

-

70-130

75-125

75-125

75-125

75-125

80-120

65-135

65-135

55-144

-

-

-

-

-

-

7

4

-

25

25

25

25

25

20

35

35

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits

General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG566113-4 QC Sample: L1218042-07 Client ID: TN004SG-000015-20121005

Total Organic Carbon - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG566725-4 QC Sample: L1218042-01 Client ID: TN005SG-000014-20121005

General Chemistry - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG566732-4 QC Sample: L1218042-01 Client ID: TN005SG-000014-20121005


General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21 QC Batch ID: WG567329-4 WG567329-5 QC Sample: L1218042-01 Client ID: TN005SG-000014-20121005

General Chemistry - Westborough Lab Associated sample(s): 23,25,27,29 QC Batch ID: WG567330-4 WG567330-5 QC Sample: L1218042-23 Client ID: HB004SG-000015-20121006

General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG567349-4 QC Sample: L1218042-29 Client ID: HB001SG-000015-20121006

25.8

1.85

1.95

1.14

1.26

180

14

28

1300

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

Qual

Q

Qual Qual

Serial_No:11051209:46

of 279


Phosphorus, Total

6500

610

19000

720

102

14

-

-

-

-

43-160

75-125

-

-

26

20


MS Found

MS%Recovery

MSD Found

MSD %Recovery

RecoveryLimits RPD

RPD Limits



12500

782

MS Added


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

11/05/12

Q

Serial_No:11051209:46

of 279

Solids, Total

Sulfide

pH



% Soot (Rep 1)

% Soot (Rep 2)


29.8

2500

8.0

0.522

0.601

0.162

0.163

3.7

30.1

1800

8.0

0.614

0.779

0.070

0.154

5.0

%

mg/kg

SU

%

%

%

%

mg/kg

1

33

0

16

26

79

6

30

10

25

5

25

25

25

25

20


General Chemistry - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG565958-1 QC Sample: L1218042-29 Client ID: HB001SG-000015-20121006



Total Organic Carbon - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG566725-3 QC Sample: L1218042-01 Client ID: TN005SG-000014-20121005

General Chemistry - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG566732-3 QC Sample: L1218042-01 Client ID: TN005SG-000014-20121005


NEWTOWN CREEK RI

120782-01.01

Project Name:

Project Number:

L1218042Lab Number:

Report Date:


11/05/12

Qual

Q

Q

Q

Q

Serial_No:11051209:46

of 279

Nitrogen, Ammonia


Phosphorus, Total

110

6500

610

110

6500

600

mg/kg

mg/kg

mg/kg

0

0

2

20

26

20





NEWTOWN CREEK RI

120782-01.01

Project Name:

Project Number:

L1218042Lab Number:

Report Date:


11/05/12

Serial_No:11051209:46

of 279


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Parameter

11/05/12

% Recovery QC CriteriaTotal Organic Carbon (Rep1)


96

111

75-125

75-125


Qual

Serial_No:11051209:46

of 279


Project Name:

Project Number:

Lab Number:

Report Date:

NEWTOWN CREEK RI

120782-01.01

L1218042

Parameter

11/05/12

% Recovery QC Criteria% Soot (Rep 1)

% Soot (Rep 2)

100

100

75-125

75-125


Qual

Serial_No:11051209:46

of 279

*Values in parentheses indicate holding time in days

L1218042-01A

L1218042-01B

L1218042-01D

L1218042-01E

L1218042-01F

L1218042-01G

L1218042-01H

Amber 100ml unpreserved


Glass 60mL unpreserved



Vial MeOH preserved split

Vial Water preserved split

E

E

A

E

E

A

A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

1.7

1.7

2.1

1.7

1.7

2.1

2.1

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

A

D

B

C

E

Absent

Absent

Absent

Absent

Absent

CoolerCustody SealCooler Information

NEWTOWN CREEK RI

120782-01.01

A2-FE-6020T(180),A2-PB-6020T(180),A2-BA-6020T(180),A2-NI-6020T(180),A2-SB-6020T(180),A2-ZN-6020T(180),A2-K-6020T(180),A2-CR-6020T(180),A2-TL-6020T(180),A2-AS-6020T(180),A2-CO-6020T(180),A2-MN-6020T(180),A2-BE-6020T(180),A2-CD-6020T(180),A2-V-6020T(180),A2-MG-6020T(180),A2-PREP-3050:2T(180),A2-SE-6020T(180),A2-AG-6020T(180),A2-AL-6020T(180),A2-CA-6020T(180),A2-CU-6020T(180),A2-NA-6020T(180),A2-PREP-3050:1T(180),A2-SN-6020T(180)

A2-SHC(14),A2-ALKPAH(14),A2-SOOT(28),A2-TS(7),A2-TOC-9060-2REPS(28)

8260HLW(14)

TCN-9010(14),TKN-4500(28),TPHOS-4500(28),PH-9045(1),NO3/NO2-4500(28),NH3-4500(28)

SULFIDE-9030(7)

8260HLW(14)

8260HLW(14)

Project Name:

Project Number:

L1218042Lab Number:

Report Date:

Sample Receipt and Container Information

Container ID Container Type Cooler pHTempdeg C Pres Seal

Container Information

Analysis(*)

11/05/12

Were project specific reporting limits specified? YES

Reagent H2O Preserved Vials Frozen on: NA

Serial_No:11051209:46

of 279


L1218042-01I

L1218042-01X

L1218042-02A

L1218042-02B

L1218042-03A

L1218042-03B

L1218042-03D

L1218042-03E

L1218042-03F

L1218042-03G

L1218042-03H

L1218042-03I

L1218042-03X

L1218042-04A

L1218042-04B




Plastic 250ml unpreserved












A

E

E

E

E

E

A

E

E

A

A

A

E

E

E

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

2.1

1.7

1.7

1.7

1.7

1.7

2.1

1.7

1.7

2.1

2.1

2.1

1.7

1.7

1.7

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

NEWTOWN CREEK RI

120782-01.01

8260HLW(14)

A2-AG-6020T(180)

SUB-GEOTESTING(28)

SUB-BROOKS(28)



8260HLW(14)


SULFIDE-9030(7)

8260HLW(14)

8260HLW(14)

8260HLW(14)

A2-AG-6020T(180)

SUB-GEOTESTING(28)

SUB-BROOKS(28)

Project Name:

Project Number:

L1218042Lab Number:

Report Date:



Analysis(*)

11/05/12

Serial_No:11051209:46

of 279


L1218042-05A

L1218042-05B

L1218042-05D

L1218042-05E

L1218042-05F

L1218042-05G

L1218042-05H

L1218042-05I

L1218042-05X

L1218042-06A

L1218042-06B












E

E

A

E

E

A

A

A

E

E

E

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

1.7

1.7

2.1

1.7

1.7

2.1

2.1

2.1

1.7

1.7

1.7

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

NEWTOWN CREEK RI

120782-01.01



8260HLW(14)


SULFIDE-9030(7)

8260HLW(14)

8260HLW(14)

8260HLW(14)

A2-AG-6020T(180)

SUB-GEOTESTING(28)

SUB-BROOKS(28)

Project Name:

Project Number:

L1218042Lab Number:

Report Date:



Analysis(*)

11/05/12

Serial_No:11051209:46

of 279


L1218042-07A

L1218042-07B

L1218042-07D

L1218042-07E

L1218042-07F

L1218042-07G

L1218042-07H

L1218042-07I

L1218042-07X

L1218042-08A

L1218042-08B












E

E

A

E

E

A

A

A

E

E

E

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

1.7

1.7

2.1

1.7

1.7

2.1

2.1

2.1

1.7

1.7

1.7

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

NEWTOWN CREEK RI

120782-01.01



8260HLW(14)


SULFIDE-9030(7)

8260HLW(14)

8260HLW(14)

8260HLW(14)

A2-AG-6020T(180)

SUB-GEOTESTING(28)

SUB-BROOKS(28)

Project Name:

Project Number:

L1218042Lab Number:

Report Date:



Analysis(*)

11/05/12

Serial_No:11051209:46

of 279


L1218042-09A

L1218042-09B

L1218042-09D

L1218042-09E

L1218042-09F

L1218042-09G

L1218042-09H

L1218042-09I

L1218042-09X

L1218042-10A

L1218042-10B












E

E

A

E

E

A

A

A

E

E

E

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

1.7

1.7

2.1

1.7

1.7

2.1

2.1

2.1

1.7

1.7

1.7

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

NEWTOWN CREEK RI

120782-01.01



8260HLW(14)


SULFIDE-9030(7)

8260HLW(14)

8260HLW(14)

8260HLW(14)

A2-AG-6020T(180)

SUB-GEOTESTING(28)

SUB-BROOKS(28)

Project Name:

Project Number:

L1218042Lab Number:

Report Date:



Analysis(*)

11/05/12

Serial_No:11051209:46

of 279


L1218042-11A

L1218042-11B

L1218042-11C

L1218042-11D

L1218042-11E

L1218042-11G

L1218042-11H

L1218042-11I

L1218042-12B

L1218042-13A

Plastic 500ml HNO3 preserved





Vial HCl preserved

Vial HCl preserved

Vial HCl preserved



D

D

D

D

D

A

A

A

D

B

<2

7

7

7

7

N/A

N/A

N/A

N/A

N/A

1.9

1.9

1.9

1.9

1.9

2.1

2.1

2.1

1.9

1.9

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

NEWTOWN CREEK RI

120782-01.01

A2-FE-6020T(180),A2-PB-6020T(180),A2-BA-6020T(180),A2-NI-6020T(180),A2-SB-6020T(180),A2-ZN-6020T(180),A2-K-6020T(180),A2-CR-6020T(180),A2-TL-6020T(180),A2-AS-6020T(180),A2-CO-6020T(180),A2-MN-6020T(180),A2-BE-6020T(180),A2-CD-6020T(180),A2-PREP-3020(180),A2-V-6020T(180),A2-MG-6020T(180),A2-SE-6020T(180),A2-AG-6020T(180),A2-AL-6020T(180),A2-CA-6020T(180),A2-CU-6020T(180),A2-NA-6020T(180),A2-SN-6020T(180)

A2-SHC(7)

A2-SHC(7)

A2-ALKPAH(7)

A2-ALKPAH(7)

8260(14)

8260(14)

8260(14)

SUB-BROOKS(28)


Project Name:

Project Number:

L1218042Lab Number:

Report Date:



Analysis(*)

11/05/12

Serial_No:11051209:46

of 279


L1218042-13B

L1218042-13D

L1218042-13E

L1218042-13F

L1218042-13G

L1218042-13H

L1218042-13I

L1218042-13X

L1218042-14A

L1218042-14B

L1218042-15A

L1218042-15B

L1218042-15D

L1218042-15E

L1218042-15F

L1218042-15G

L1218042-15H

L1218042-15I



















B

A

B

B

A

A

A

B

B

B

B

B

A

B

B

A

A

A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

1.9

2.1

1.9

1.9

2.1

2.1

2.1

1.9

1.9

1.9

1.9

1.9

2.1

1.9

1.9

2.1

2.1

2.1

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

NEWTOWN CREEK RI

120782-01.01


8260HLW(14)


SULFIDE-9030(7)

8260HLW(14)

8260HLW(14)

8260HLW(14)

A2-AG-6020T(180)

SUB-GEOTESTING(28)

SUB-BROOKS(28)



8260HLW(14)


SULFIDE-9030(7)

8260HLW(14)

8260HLW(14)

8260HLW(14)

Project Name:

Project Number:

L1218042Lab Number:

Report Date:



Analysis(*)

11/05/12

Serial_No:11051209:46

of 279


L1218042-15X

L1218042-16A

L1218042-16B

L1218042-17A

L1218042-17B

L1218042-17D

L1218042-17E

L1218042-17F

L1218042-17G

L1218042-17H

L1218042-17I

L1218042-17X

L1218042-18A

L1218042-18B















B

B

B

B

B

A

B

B

A

A

A

B

B

B

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

1.9

1.9

1.9

1.9

1.9

2.1

1.9

1.9

2.1

2.1

2.1

1.9

1.9

1.9

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

NEWTOWN CREEK RI

120782-01.01

A2-AG-6020T(180)

SUB-GEOTESTING(28)

SUB-BROOKS(28)



8260HLW(14)


SULFIDE-9030(7)

8260HLW(14)

8260HLW(14)

8260HLW(14)

A2-AG-6020T(180)

SUB-GEOTESTING(28)

SUB-BROOKS(28)

Project Name:

Project Number:

L1218042Lab Number:

Report Date:



Analysis(*)

11/05/12

Serial_No:11051209:46

of 279


L1218042-19A

L1218042-19B

L1218042-19D

L1218042-19E

L1218042-19F

L1218042-19G

L1218042-19H

L1218042-19I

L1218042-19X

L1218042-20A

L1218042-20B












B

B

A

B

B

A

A

A

B

B

B

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

1.9

1.9

2.1

1.9

1.9

2.1

2.1

2.1

1.9

1.9

1.9

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

NEWTOWN CREEK RI

120782-01.01



8260HLW(14)


SULFIDE-9030(7)

8260HLW(14)

8260HLW(14)

8260HLW(14)

A2-AG-6020T(180)

SUB-GEOTESTING(28)

SUB-BROOKS(28)

Project Name:

Project Number:

L1218042Lab Number:

Report Date:



Analysis(*)

11/05/12

Serial_No:11051209:46

of 279


L1218042-21A

L1218042-21B

L1218042-21D

L1218042-21E

L1218042-21F

L1218042-21G

L1218042-21H

L1218042-21I

L1218042-22A

L1218042-22B











A

A

A

A

A

A

A

A

A

A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

2.1

2.1

2.1

2.1

2.1

2.1

2.1

2.1

2.1

2.1

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

NEWTOWN CREEK RI

120782-01.01



8260HLW(14)


SULFIDE-9030(7)

8260HLW(14)

8260HLW(14)

8260HLW(14)

SUB-GEOTESTING(28)

SUB-BROOKS(28)

Project Name:

Project Number:

L1218042Lab Number:

Report Date:



Analysis(*)

11/05/12

Serial_No:11051209:46

of 279


L1218042-23A

L1218042-23B

L1218042-23D

L1218042-23E

L1218042-23F

L1218042-23G

L1218042-23H

L1218042-23I

L1218042-23X

L1218042-24A

L1218042-24B












C

C

A

C

C

A

A

A

C

C

C

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

1.8

1.8

2.1

1.8

1.8

2.1

2.1

2.1

1.8

1.8

1.8

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

NEWTOWN CREEK RI

120782-01.01



8260HLW(14)


SULFIDE-9030(7)

8260HLW(14)

8260HLW(14)

8260HLW(14)

A2-AG-6020T(180)

SUB-GEOTESTING(28)

SUB-BROOKS(28)

Project Name:

Project Number:

L1218042Lab Number:

Report Date:



Analysis(*)

11/05/12

Serial_No:11051209:46

of 279


L1218042-25A

L1218042-25B

L1218042-25D

L1218042-25E

L1218042-25F

L1218042-25G

L1218042-25H

L1218042-25I

L1218042-25X

L1218042-26A

L1218042-26B












C

C

A

C

C

A

A

A

C

C

C

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

1.8

1.8

2.1

1.8

1.8

2.1

2.1

2.1

1.8

1.8

1.8

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

NEWTOWN CREEK RI

120782-01.01



8260HLW(14)


SULFIDE-9030(7)

8260HLW(14)

8260HLW(14)

8260HLW(14)

A2-AG-6020T(180)

SUB-GEOTESTING(28)

SUB-BROOKS(28)

Project Name:

Project Number:

L1218042Lab Number:

Report Date:



Analysis(*)

11/05/12

Serial_No:11051209:46

of 279


L1218042-27A

L1218042-27B

L1218042-27D

L1218042-27E

L1218042-27F

L1218042-27G

L1218042-27H

L1218042-27I

L1218042-27X

L1218042-28A

L1218042-28B












C

C

A

C

C

A

A

A

C

C

C

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

1.8

1.8

2.1

1.8

1.8

2.1

2.1

2.1

1.8

1.8

1.8

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

NEWTOWN CREEK RI

120782-01.01



8260HLW(14)


SULFIDE-9030(7)

8260HLW(14)

8260HLW(14)

8260HLW(14)

A2-AG-6020T(180)

SUB-GEOTESTING(28)

SUB-BROOKS(28)

Project Name:

Project Number:

L1218042Lab Number:

Report Date:



Analysis(*)

11/05/12

Serial_No:11051209:46

of 279


L1218042-29A

L1218042-29B

L1218042-29D

L1218042-29E

L1218042-29F

L1218042-29G

L1218042-29H

L1218042-29I

L1218042-29X

L1218042-30A

L1218042-30B

L1218042-31A

L1218042-31B












Vial HCl preserved

Vial HCl preserved

C

C

A

C

C

A

A

A

C

C

C

A

A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

1.8

1.8

2.1

1.8

1.8

2.1

2.1

2.1

1.8

1.8

1.8

2.1

2.1

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Y

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

Absent

NEWTOWN CREEK RI

120782-01.01



8260HLW(14)


SULFIDE-9030(7)

8260HLW(14)

8260HLW(14)

8260HLW(14)

A2-AG-6020T(180)

SUB-GEOTESTING(28)

SUB-BROOKS(28)

8260(14)

8260(14)

Project Name:

Project Number:

L1218042Lab Number:

Report Date:

Sent to GeoTesting Express

Sent to Brooks Rand Lab



L1218042-02A

L1218042-02B

L1218042-04A

L1218042-04B



Analysis(*)

11/05/12

Container Comments

Serial_No:11051209:46

of 279


NEWTOWN CREEK RI

120782-01.01

Project Name:

Project Number:

L1218042Lab Number:

Report Date:


























L1218042-06A

L1218042-06B

L1218042-08A

L1218042-08B

L1218042-10A

L1218042-10B

L1218042-12B

L1218042-14A

L1218042-14B

L1218042-16A

L1218042-16B

L1218042-18A

L1218042-18B

L1218042-20A

L1218042-20B

L1218042-22A

L1218042-22B

L1218042-24A

L1218042-24B

L1218042-26A

L1218042-26B

L1218042-28A

L1218042-28B

L1218042-30A

L1218042-30B



Analysis(*)

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Container Comments

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Report Format: DU Report with "J" Qualifiers

GLOSSARY

Project Name:

Project Number:

Lab Number:

Report Date:

L1218042NEWTOWN CREEK RI

120782-01.01 11/05/12

Acronyms

EPA

LCS

LCSD

LFB

MDL

MS

MSD

NA

NC

NI

RL

RPD

SRM

Environmental Protection Agency.

Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes.Laboratory Control Sample Duplicate: Refer to LCS.

Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes.Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any adjustments from dilutions, concentrations or moisture content, where applicable.Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for which an independent estimate of target analyte concentration is available. Matrix Spike Sample Duplicate: Refer to MS.

Not Applicable.

Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit.Not Ignitable.

Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL includes any adjustments from dilutions, concentrations or moisture content, where applicable.Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precisionof analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report.Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the associated field samples.

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Terms

Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum.

Data Qualifiers

A

B

C

D

E

G

H

I

M

NJ

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-

-

-

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Spectra identified as "Aldol Condensation Product".

The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that have detectable concentrations of the analyte at less than five times (5x) the concentration found in the blank. For MCP-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ-Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the reporting limit.Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted analyses.Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations of the analyte.Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument.

The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should be considered estimated.The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection.

The RPD between the results for the two columns exceeds the method-specified criteria; however, the lower value has been reporteddue to obvious interference.Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte.

Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where the identification is based on a mass spectral library search.

1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the originalmethod.

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Footnotes

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Report Format: DU Report with "J" Qualifiers

Project Name:

Project Number:

Lab Number:

Report Date:


120782-01.01 11/05/12

Data Qualifiers

P

Q

R

RE

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-

-

-

The RPD between the results for the two columns exceeds the method-specified criteria.

The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing CalibrationStandard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoverieswhen the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are lessthan 5x the RL. (Metals only.)Analytical results are from sample re-analysis.

Analytical results are from sample re-extraction.

J

ND

-

-

Estimated value. The Target analyte concentration is below the quantitation limit (RL), but above the Method Detection Limit (MDL) or Estimated Detection Limit (EDL) for SPME-related analyses. This represents an estimated concentration for Tentatively Identified Compounds (TICs).Not detected at the method detection limit (MDL) for the sample, or estimated detection limit (EDL) for SPME-related analyses.

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Alpha Analytical performs services with reasonable care and diligence normal to the analytical testinglaboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analyticalshall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liablefor any incidental, consequential or special damages, including but not limited to, damages in any wayconnected with the use of, interpretation of, information or analysis provided by Alpha Analytical.

We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling,containers, sampling procedures, holding time and splitting of samples in the field.

LIMITATION OF LIABILITIES

1

30

91

Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW-846. Third Edition. Updates I - IIIA, 1997.

Standard Methods for the Examination of Water and Wastewater. APHA-AWWA-WPCF. 18th Edition. 1992.

Analysis of Soot by Accardi-Dey, Gschwend, 2003; Gustafsson (et. al.), 1997.

Project Name:

Project Number:

Lab Number:

Report Date:


120782-01.01

REFERENCES

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Certificate/Approval Program SummaryLast revised August 3, 2012 – Mansfield Facility

The following list includes only those analytes/methods for which certification/approval is currently held.For a complete listing of analytes for the referenced methods, please contact your Alpha Customer Service Representative.

Connecticut Department of Public Health Certificate/Lab ID: PH-0141.

Wastewater/Non-Potable Water (Inorganic Parameters: pH, Turbidity, Conductivity, Alkalinity, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Strontium, Thallium, Tin, Titanium, Vanadium, Zinc, Total Residue (Solids), Total Suspended Solids (non-filterable). Organic Parameters: PCBs, Organochlorine Pesticides, Technical Chlordane, Toxaphene, Acid Extractables, Benzidines, Phthalate Esters, Nitrosamines, Nitroaromatics & Isophorone, PAHs, Haloethers, Chlorinated Hydrocarbons, Volatile Organics.)

Solid Waste/Soil (Inorganic Parameters: pH, Aluminum, Antimony, Arsenic, Barium, Beryllium, Cadmium,Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Thallium, Titanium, Vanadium, Zinc, Total Organic Carbon, Corrosivity, TCLP 1311, SPLP 1312. Organic Parameters: PCBs, Organochlorine Pesticides, Technical Chlordane, Toxaphene, Volatile Organics, Acid Extractables, Benzidines, Phthalates, Nitrosamines,Nitroaromatics & Cyclic Ketones, PAHs, Haloethers, Chlorinated Hydrocarbons.)

Florida Department of Health Certificate/Lab ID: E87814. NELAP Accredited.

Non-Potable Water (Inorganic Parameters: SM2320B, SM2540D, SM2540G.)

Solid & Chemical Materials (Inorganic Parameters: 6020, 7470, 7471, 9045. Organic Parameters: EPA 8260,8270, 8082, 8081.)

Air & Emissions (EPA TO-15.)

Louisiana Department of Environmental Quality Certificate/Lab ID: 03090. NELAP Accredited.

Non-Potable Water (Inorganic Parameters: EPA 180.1, 245.7, 1631E, 3020A, 6020A, 7470A, 9040, 9050A, SM2320B, 2540D, 2540G, 4500H-B, Organic Parameters: EPA 3510C, 3580A, 3630C, 3640A, 3660B, 3665A,5030B, 8015D, 3570, 8081B, 8082A, 8260B, 8270C, 8270D.)

Solid & Chemical Materials (Inorganic Parameters: EPA 1311, 3050B, 3051A, 3060A, 6020A, 7196A, 7470A,7471B, 7474, 9040B, 9045C, 9060. Organic Parameters: EPA 3540C, 3570, 3580A, 3630C, 3640A, 3660,3665A, 5035, 8015D, 8081B, 8082A, 8260B, 8270C, 8270D.)

Biological Tissue (Inorganic Parameters: EPA 6020A. Organic Parameters: EPA 3570, 3510C, 3610B, 3630C, 3640A, 8270C, 8270D.)


New Hampshire Department of Environmental Services Certificate/Lab ID: 2206. NELAP Accredited.

Non-Potable Water (Inorganic Parameters: EPA 180.1, 1631E, 6020A, 7470A, 9040B, 9050A, SM2540D, 2540G, 4500H+B, 2320B, 3020A, . Organic Parameters: EPA 3510C, 3630C, 3640A, 3660B, 8081B, 8082A, 8270C, 8270D, 8015D.)

Solid & Chemical Materials (Inorganic Parameters: SW-846 1311, 3050B, 3051A, 6020A, 7471B, 9040B, 9045C. Organic Parameters: SW-846 3540C, 3580A, 3630C, 3640A, 3660B, 3665A, 8270C, 8015D, 8082A, 8081B.)

New Jersey Department of Environmental Protection Certificate/Lab ID: MA015. NELAP Accredited.

Non-Potable Water (Inorganic Parameters: SW-846 1312, 3020A, SM2320B, SM2540D, 2540G, 4500H-B, EPA 180.1, 1631E, SW-846 7470A, 9040C, 6020A, 9050A. Organic Parameters: SW-846 3510C, 3580A, 3630C, 3640A, 3660B, 3665A, 8015D, 8081B, 8082A, 8270C, 8270D)

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Solid & Chemical Materials (Inorganic Parameters: SW-846 1311, 1312, 3050B, 3051A, 6020A, 7471B, 7474,9040B, 9040C, 9045C, 9045D, 9060. Organic Parameters: SW-846 3540C, 3570, 3580A, 3630C, 3640A, 3660B, 3665A, 8081B, 8082A, 8270C, 8270D, 8015D.)

Atmospheric Organic Parameters (EPA 3C, TO-15, TO-10A, TO-13A-SIM.)

Biological Tissue (Inorganic Parameters: SW-846 6020A. Organic Parameters: SW-846 8270C, 8270D, 3510C, 3570, 3610C, 3630C, 3640A)

New York Department of Health Certificate/Lab ID: 11627. NELAP Accredited.

Non-Potable Water (Inorganic Parameters: SM2320B, SM2540D, 6020A, 1631E, 7470A, 9050A, EPA 180.1, 3020A. Organic Parameters: EPA 8270C, 8270D, 8081B, 8082A, 3510C.)

Solid & Hazardous Waste (Inorganic Parameters: EPA 6020A, 7471B, 7474, 9040C, 9045D. Organic Parameters: EPA 8270C, 8270D, 8081B, 8082A, 1311, 3050B, 3580A, 3570, 3051A.)

Air & Emissions (EPA TO-15, TO-10A.)

Pennsylvania Certificate/Lab ID: 68-02089 NELAP Accredited

Non-Potable Water (Inorganic Parameters: 1312, 1631E, 180.1, 3020A, 6020A, 7470A, 9040B, 9050A, 2320B, 2540D, 2540G, SM4500H+-B. Organic Parameters: 3510C, 3580A, 3630C, 3640A, 3660B, 3665A, 8015D, 8081B, 8082A, 8270C, 8270D .)

Solid & Hazardous Waste (Inorganic Parameters: EPA 1311, 3051A, 6020A, 7471B, 7474 9040B, 9045C, 9060.Organic Parameters: EPA3050B, 3540C, 3570, 3580A, 3630C, 3640A, 3660B, 3665A, 8270C, 8270D, 8081B,8015D, 8082A.)

Rhode Island Department of Health Certificate/Lab ID: LAO00299. NELAP Accredited via NJ-DEP.

Refer to NJ-DEP Certificate for Non-Potable Water.

Texas Commission of Environmental Quality Certificate/Lab ID: T104704419-08-TX. NELAP Accredited.

Solid & Chemical Materials (Inorganic Parameters: EPA 6020, 7470, 7471, 1311, 9040, 9045, 9060. Organic Parameters: EPA 8015, 8270, 8081, 8082.)

Air (Organic Parameters: EPA TO-15)

Virginia Division of Consolidated Laboratory Services Certificate/Lab ID:460194. NELAP Accredited.

Non-Potable Water (Inorganic Parameters:EPA 3020A, 6020A, 245.7, 9040B. Organic Parameters: EPA 3510C,3640A, 3660B, 3665A, 8270C, 8270D, 8082A, 8081B, 8015D.)

Solid & Chemical Materials (Inorganic Parameters: EPA 6020A,7470A,7471B,9040B,9045C,3050B,3051, 9060.Organic Parameters: EPA 3540C, 3580A, 3630C, 3640A, 3660B, 3665A, 3570, 8270C, 8270D, 8081B, 8082A,8015D.)

Washington State Department of Ecology Certificate/Lab ID: C954. Non-Potable Water (InorganicParameters: SM2540D, 180.1, 1631E.)

Solid & Chemical Materials (Inorganic Parameters: EPA 6020, 7470, 7471, 7474, 9045C, 9050A, 9060. OrganicParameters: EPA 8081, 8082, 8015, 8270.)

U.S. Army Corps of Engineers

Department of Defense, L-A-B Certificate/Lab ID: L2217.01.

Non-Potable Water (Inorganic Parameters: EPA 6020A, SM4500H-B. Organic Parameters: 3020A, 3510C,8270C, 8270D, 8270C-ALK-PAH, 8270D-ALK-PAH, 8082A, 8081B, 8015D-SHC, 8015D.)

Solid & Hazardous Waste (Inorganic Parameters: EPA 1311, 3050B, 6020A, 7471A, 9045C, 9060, SM 2540G, ASTM D422-63. Organic Parameters: EPA 3580A, 3570, 3540C, 8270C, 8270D, 8270C-ALK-PAH, 8270D-ALK-PAH 8082A, 8081B, 8015D-SHC, 8015D.


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Analytes Not Accredited by NELAP Certification is not available by NELAP for the following analytes: 8270C: Biphenyl. TO-15: Halothane, 2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-1-pentene, Thiophene, 2-Methylthiophene, 3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, Benzothiophene, 2-Methylnaphthalene, 1-Methylnaphthalene.

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Certificate/Approval Program Summary Last revised August 16, 2012 - Westboro Facility

The following list includes only those analytes/methods for which certification/approval is currently held.

For a complete listing of analytes for the referenced methods, please contact your Alpha Customer Service Representative.

Connecticut Department of Public Health Certificate/Lab ID: PH-0574. NELAP Accredited Solid Waste/Soil. Drinking Water (Inorganic Parameters: Color, pH, Turbidity, Conductivity, Alkalinity, Chloride, Free Residual Chlorine, Fluoride, Calcium Hardness, Sulfate, Nitrate, Nitrite, Aluminum, Antimony, Arsenic, Barium, Beryllium, Cadmium, Calcium, Chromium, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Nickel, Selenium, Silver, Sodium, Thallium, Zinc, Total Dissolved Solids, Total Organic Carbon, Total Cyanide, Perchlorate. Organic Parameters: Volatile Organics 524.2, Total Trihalomethanes 524.2, 1,2-Dibromo-3-chloropropane (DBCP) 504.1, Ethylene Dibromide (EDB) 504.1, 1,4-Dioxane (Mod 8270). Microbiology Parameters: Total Coliform-MF mEndo (SM9222B), Total Coliform – Colilert (SM9223, Enumeration and P/A), E. Coli. – Colilert (SM9223, Enumeration and P/A), HPC – Pour Plate (SM9215B), Fecal Coliform – MF m-FC (SM9222D), Fecal Coliform-EC Medium (SM 9221E). Wastewater/Non-Potable Water (Inorganic Parameters: Color, pH, Conductivity, Acidity, Alkalinity, Chloride, Total Residual Chlorine, Fluoride, Total Hardness, Silica, Sulfate, Sulfide, Ammonia, Kjeldahl Nitrogen, Nitrate, Nitrite, O-Phosphate, Total Phosphorus, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Strontium, Thallium, Tin, Titanium, Vanadium, Zinc, Total Residue (Solids), Total Dissolved Solids, Total Suspended Solids (non-filterable), BOD, CBOD, COD, TOC, Total Cyanide, Phenolics, Foaming Agents (MBAS), Bromide, Oil and Grease. Organic Parameters: PCBs, Organochlorine Pesticides, Technical Chlordane, Toxaphene, Acid Extractables (Phenols), Benzidines, Phthalate Esters, Nitrosamines, Nitroaromatics & Isophorone, Polynuclear Aromatic Hydrocarbons, Haloethers, Chlorinated Hydrocarbons, Volatile Organics, TPH (HEM/SGT), CT- Extractable Petroleum Hydrocarbons (ETPH), MA-EPH, MA-VPH. Microbiology Parameters: Total Coliform – MF mEndo (SM9222B), Total Coliform – MTF (SM9221B), E. Coli – Colilert (SM9223 Enumeration), HPC – Pour Plate (SM9215B), Fecal Coliform – MF m-FC (SM9222D), Fecal Coliform – A-1 Broth (SM9221E), Enterococcus - Enterolert. Solid Waste/Soil (Inorganic Parameters: pH, Sulfide, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Thallium, Tin, Vanadium, Zinc, Total Cyanide, Ignitability, Phenolics, Corrosivity, TCLP Leach (1311), SPLP Leach (1312 metals only), Reactivity. Organic Parameters: PCBs, PCBs in Oil, Organochlorine Pesticides, Technical Chlordane, Toxaphene, CT-Extractable Petroleum Hydrocarbons (ETPH), MA-EPH, MA-VPH, Dicamba, 2,4-D, 2,4,5-T, 2,4,5-TP(Silvex), Dalapon, Volatile Organics (SW 8260), Acid Extractables (Phenols) (SW 8270), Benzidines (SW 8270), Phthalates (SW 8270), Nitrosamines (SW 8270), Nitroaromatics & Cyclic Ketones (SW 8270), PAHs (SW 8270), Haloethers (SW 8270), Chlorinated Hydrocarbons (SW 8270). ) Maine Department of Human Services Certificate/Lab ID: 2009024. Drinking Water (Inorganic Parameters: SM9215B, 9222D, 9223B, EPA 180.1, 353.2, SM2130B, 2320B, 2540C, 4500Cl-D, 4500CN-C, 4500CN-E, 4500F-C, 4500H+B, 4500NO3-F, EPA 200.7, EPA 200.8, 245.1, EPA 300.0. Organic Parameters: 504.1, 524.2.) Wastewater/Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664A, 350.1, 351.1, 353.2, 410.4, 420.1, SM2320B, 2510B, 2540C, 2540D, 426C, 4500Cl-D, 4500Cl-E, 4500CN-C, 4500CN-E, 4500F-B, 4500F-C, 4500H+B, 4500Norg-B, 4500Norg-C, 4500NH3-B, 4500NH3-G, 4500NO3-F, 4500P-B, 4500P-E, 5210B, 5220D, 5310C, 9010B, 9040B, 9030B, 7470A, 7196A, 2340B, EPA 200.7, 6010B, 200.8, 6020, 245.1, 1311, 1312, 3005A, Enterolert, 9223D, 9222D. Organic Parameters: 608, 624, 625, 8081A, 8082, 8330, 8151A, 8260B, 8270C, 3510C, 3630C, 5030B, ME-DRO, ME-GRO, MA-EPH, MA-VPH.) Solid Waste/Soil (Inorganic Parameters: 9010B, 9012A, 9014A, 9030B, 9040B, 9045C, 6010B, 7471A, 7196A, 9050A, 1010, 1030, 9065, 1311, 1312, 3005A, 3050B. Organic Parameters: ME-DRO, ME-GRO, MA-EPH, MA-VPH, 8260B, 8270C, 8330, 8151A, 8081A, 8082, 3540C, 3546, 3580A, 3630C, 5030B, 5035.) Massachusetts Department of Environmental Protection Certificate/Lab ID: M-MA086. Drinking Water (Inorganic Parameters: (EPA 200.8 for: Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,Tl) (EPA 200.7 for: Ba,Be,Ca,Cd,Cr,Cu,Na,Ni) 245.1, (300.0 for: Nitrate-N, Fluoride, Sulfate); (EPA 353.2 for: Nitrate-N, Nitrite-N); (SM4500NO3-F for: Nitrate-N and Nitrite-N); 4500F-C, 4500CN-CE, EPA 180.1, SM2130B, SM4500Cl-D, 2320B, SM2540C, SM4500H-B. Organic Parameters: (EPA 524.2 for: Trihalomethanes, Volatile Organics); (504.1 for: 1,2-Dibromoethane, 1,2-Dibromo-3-Chloropropane), EPA 332. Microbiology Parameters: SM9215B; ENZ. SUB. SM9223; ColilertQT SM9223B; MF-SM9222D.) Non-Potable Water (Inorganic Parameters:, (EPA 200.8 for: Al,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,Tl,Zn); (EPA 200.7

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for: Al,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,Tl,V,Zn); 245.1, SM4500H,B, EPA 120.1, SM2510B, 2540C, 2340B, 2320B, 4500CL-E, 4500F-BC, 426C, SM4500NH3-BH, (EPA 350.1 for: Ammonia-N), LACHAT 10-107-06-1-B for Ammonia-N, SM4500NO3-F, 353.2 for Nitrate-N, SM4500NH3-BC-NES, EPA 351.1, SM4500P-E, 4500P-B,E, 5220D, EPA 410.4, SM 5210B, 5310C, 4500CL-D, EPA 1664, SM14 510AC, EPA 420.1, SM4500-CN-CE, SM2540D. Organic Parameters: (EPA 624 for Volatile Halocarbons, Volatile Aromatics),(608 for: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT,Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs-Water), (EPA 625 for SVOC Acid Extractables and SVOC Base/Neutral Extractables), 600/4-81-045-PCB-Oil. Microbiology Parameters: (ColilertQT SM9223B; Enterolert-QT: SM9222D-MF.) New Hampshire Department of Environmental Services Certificate/Lab ID: 200307. NELAP Accredited. Drinking Water (Inorganic Parameters: SM 9222B, 9223B, 9215B, EPA 200.7, 200.8, 300.0, SM4500CN-E, 4500H+B, 4500NO3-F, 2320B, 2510B, 2540C, 4500F-C, 5310C, 2120B, EPA 332.0. Organic Parameters: 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: SM9222D, 9221B, 9222B, 9221E-EC, EPA 3005A, 200.7, 200.8, 245.1, SW-846 6010B, 6010C, 6020, 6020A, 7196A, 7470A, SM3500-CR-D, EPA 120.1, 300.0, 350.1, 350.2, 351.1, 353.2, 410.4, 420.1, 426C, 1664A, SW-846 9010B, 9030B, 9040B, SM2120B, 2310B, 2320B, 2540B, 2540D, 4500H+B, 4500CL-E, 4500CN-E, 4500NH3-H, 4500NO3-F, 4500NO2-B, 4500P-E, 4500-S2-D, 5210B, 5220D, 2510B, 2540C, 4500F-C, 5310C, 5540C, LACHAT 10-204-00-1-A, LACHAT 10-107-06-2-D, 3060A. Organic Parameters: SW-846 3510C, 3630C, 5030B, 8260B, 8270C, 8270D, 8330, EPA 624, 625, 608, SW-846 8082, 8082A, 8081A, 8081B, 8151A, 8330, 8270C-SIM, 8270D-SIM.) Solid & Chemical Materials (Inorganic Parameters: SW-846 6010B, 6010C, 7196A, 7471A, 1010, 1030, 9010, 9012A, 9014, 9030B, 9040B, 9045C, 9050, 9065,1311, 1312, 3005A, 3050B, 3060A. Organic Parameters: SW-846 3540C, 3546, 3050B, 3580A, 3630C, 5030B, 5035, 8260B, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330, 8151A, 8015B, 8015C, 8082, 8082A, 8081A, 8081B.) New Jersey Department of Environmental Protection Certificate/Lab ID: MA935. NELAP Accredited. Drinking Water (Inorganic Parameters: SM9222B, 9221E, 9223B, 9215B, 4500CN-CE, 4500NO3-F, 4500F-C, EPA 300.0, 200.7, 200.8, 245.1, 2540C, SM2120B, 2320B, 2510B, 5310C, SM4500H-B. Organic Parameters: EPA 332, 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: SM5210B, EPA 410.4, SM5220D, 4500Cl-E, EPA 300.0, SM2120B, 2340B, SM4500F-BC, EPA 200.7, 200.8, 351.1, LACHAT 10-107-06-2-D, EPA 353.2, SM4500NO3-F, 4500NO2-B, EPA 1664A, SM5310B, C or D, 4500-PE, EPA 420.1, SM510ABC, SM4500P-B5+E, 2540B, 2540C, 2540D, 2540G, EPA 120.1, SM2510B, SM2520B, SM15 426C, 9222D, 9221B, 9221C, 9221E, 9222B, 9215B, 2310B, 2320B, 4500NH3-H, 4500-S D, EPA 350.1, 350.2, SW-846 1312, 7470A, 5540C, SM4500H-B, 4500SO3-B, SM3500Cr-D, 4500CN-CE, EPA 245.1, SW-846 9040B, 3005A, 3015, EPA 6010B, 6010C, 6020, 6020A, 7196A, 3060A, SW-846 9010B, 9030B. Organic Parameters: SW-846 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 3510C, EPA 608, 624, 625, SW-846 3630C, 5030B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8330, 1,4-Dioxane by NJ Modified 8270, 8015B, NJ EPH.) Solid & Chemical Materials (Inorganic Parameters: SW-846, 6010B, 6010C, 6020, 6020A, 7196A, 3060A, 9010B, 9030B, 1010, 1030, 1311, 1312, 3005A, 3050B, 7471A, 7471B, 9014, 9012A, 9040B, 9040C, 9045C, 9045D, 9050A, 9065, 9251. Organic Parameters: SW-846 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8330, 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 3540C, 3546, 3580A, 3630C, 5030B, 5035L, 5035H, NJ OQA-QAM-025 Rev.7, NJ EPH.) New York Department of Health Certificate/Lab ID: 11148. NELAP Accredited. Drinking Water (Inorganic Parameters: SM9223B, 9222B, 9215B, EPA 200.8, 200.7, 245.2, SM5310C, EPA 332.0, SM2320B, EPA 300.0, SM2120B, 4500CN-E, 4500F-C, 4500NO3-F, 2540C, SM 2510B. Organic Parameters: EPA 524.2, 504.1.) Non-Potable Water (Inorganic Parameters: SM9221E, 9222D, 9221B, 9222B, 9215B, 5210B, 5310C, EPA 410.4, SM5220D, 2310B-4a, 2320B, EPA 200.7, 300.0, SM4500CL-E, 4500F-C, SM15 426C, EPA 350.1, SM4500NH3-BH, EPA 351.1, LACHAT 10-107-06-2, EPA 353.2, SM4500-NO3-F, 4500-NO2-B, 4500P-E, 2540C, 2540B, 2540D, EPA 200.8, EPA 6010B, 6010C, 6020, 6020A, EPA 7196A, SM3500Cr-D, EPA 245.1, 245.2, 7470A, SM2120B, LACHAT 10-204-00-1-A, 4500CN-CE, EPA 1664A, EPA 420.1, SM14 510C, EPA 120.1, SM2510B, SM4500S-D, SM5540C, EPA 3005A, 3015, 9010B, 9030B. Organic Parameters: EPA 624, 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 625, 608, 8081A, 8081B, 8151A, 8330, 8082, 8082A, EPA 3510C, 5030B.) Solid & Hazardous Waste (Inorganic Parameters: EPA 1010, 1030, EPA 6010B, 6010C, 7196A, 7471A, 7471B, 9012A, 9014, 9065, 9050A, EPA 1311, 1312, 3005A, 3050B, 9010B, 9040C, 9045D. Organic Parameters: EPA 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8015B, 8015C, 8081A, 8081B, 8151A, 8330, 8082 8082A, 3540C, 3546, 3580, 3580A, 5030B, 5035A-H, 5035A-L.)

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North Carolina Department of the Environment and Natural Resources Certificate/Lab ID : 666. (Inorganic Parameters: SM2310B, 2320B, 4500Cl-E, 4500Cn-E, 9014, Lachat 10-204-00-1-X, 1010A, 1030, 4500NO3-F, 353.2, 4500P-E, 4500SO4-E, 300.0, 4500S-D, 5310B, 5310C, 6010C, 6020A, 200.7, 200.8, 3500Cr-B, 7196A, 245.1, 7471A, 7471B, 1311,1312. Organic Parameters: 608, 8081B, 8082A, 624, 8260B, 625, 8270D, 8151A, 8015C, 504.1, MA-EPH, MA-VPH.) Drinking Water Program Certificate/Lab ID: 25700. (Inorganic Parameters: Chloride EPA 300.0. Organic Parameters: 524.2) Pennsylvania Department of Environmental Protection Certificate/Lab ID : 68-03671. NELAP Accredited. Drinking Water (Inorganic Parameters: 200.7, 200.8, 245.2, 300.0, 332.0, 2120B, 2320B, 2510B, 2540C, 4500-CN-CE, 4500F-C, 4500H+-B, 4500NO3-F, 5310C. Organic Parameters: EPA 524.2, 504.1) Non-Potable Water (Inorganic Parameters: EPA 120.1, 1312, 3005A,3015, 3060A, 200.7, 200.8, 410.4, 1664A, SM2540D, 5210B, 5220D, 4500-P,BE, 245.1, 300.0, 3501., 350.2, 353.2, 420.1, 6010B, 6010C, 6020, 6020A, 7196A, 7470A, 9010B, 9030B, 9040B, Lachat 10-107-06-2-D, NJ-EPH, 2120B, 2310B, 2320B, 2340B, 2510C, 2540B, 2540C, 3500Cr-D, 436C, 4500CN-CE, 4500Cl-E, 4500F-B, 4500F-C, 4500H+-B, 4500NO2-B, 4500NO3-F, 4500S-D, 4500SO3-B, 5310BCD, 5540C. Organic Parameters: EPA 3510C, 3630C, 5030B, 625, 624, 608, 8081A, 8081B, 8082, 8082A, 8151A, 8260B, 8270C, 8270D, 8330, 8015B, ) Solid & Hazardous Waste (Inorganic Parameters: EPA 350.1, 1010, 1030, 1311, 1312, 3005A, 3050B, 3060A, 6010B, 6010C, 6020A, 7196A, 7471A, 7471B, 9010B, 9012A, 9014, 9040B, 9045C, 9050, 9065, SM 4500NH3-BH, 9030B, 9038, 9251. Organic Parameters: 3540C, 3546, 3580A, 3630C, 5035, 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8260B, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330, NJ-EPH.) Rhode Island Department of Health Certificate/Lab ID: LAO00065. NELAP Accredited via NJ-DEP. Refer to MA-DEP Certificate for Potable and Non-Potable Water. Refer to NJ-DEP Certificate for Potable and Non-Potable Water. Texas Commisson on Environmental Quality Certificate/Lab ID: T104704476-09-1. NELAP Accredited. Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664, 200.7, 200.8, 245.1, 245.2, 300.0, 350.1, 351.1, 353.2, 410.4, 420.1, 6010, 6020, 7196, 7470, 9040, SM 2120B, 2310B, 2320B, 2510B, 2540B, 2540C, 2540D, 426C, 4500CL-E, 4500CN-E, 4500F-C, 4500H+B, 4500NH3-H, 4500NO2B, 4500P-E, 4500 S2¯D, 510C, 5210B, 5220D, 5310C, 5540C. Organic Parameters: EPA 608, 624, 625, 8081, 8082, 8151, 8260, 8270, 8330.) Solid & Hazardous Waste (Inorganic Parameters: EPA 1311, 1312, 9012, 9014, 9040, 9045, 9050, 9065.) Virginia Division of Consolidated Laboratory Services Certificate/Lab ID: 460195. NELAP Accredited. Drinking Water (Inorganic Parameters: EPA 200.7, 200.8, 300.0, 2510B, 2120B, 2540C, 4500CN-CE, 245.2, 2320B, 4500F-C, 4500F-C, 4500NO3-F, 5310C. Organic Parameters: EPA 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664A, 200.7, 2..08, 245.1, 300.0, 3005A, 3015, 1312, 6010B, 6010C, 3060A, 353.2, 420.1, 6020, 6020A, SM4500S-D, SM4500-CN-CE, Lachat 10-204-00-1-X, 7196A, 7470A, 9010B, 9040B, 2310B, 2320B, 2510B, 2540B, 2540C, 3500Cr-D, 426C, 4500Cl-E, 4500F-B, 4500F-C, 4500PE, 510AC, 5210B, 5310B 5310C, 5540C. Organic Parameters: EPA 3510C, 3630C, 5030B, 8260B, 608, 624, 625, 8081A, 8081B, 8082, 8082A, 8151A, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330, ) Solid & Hazardous Waste (Inorganic Parameters: EPA 1010A, 1030, 3060A, 3050B, 1311, 1312, 6010B, 6010C, 6020, , 7196A, 7471A, 7471B, 6020A, 9030B, 9010B, 9012A, 9014 9040B, 9045C, 9050A, 9065. Organic Parameters: EPA 5035, 3540C, 3546, 3550, 3580, 3630C, 8260B, 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330.) Department of Defense, L-A-B Certificate/Lab ID: L2217. Drinking Water (Inorganic Parameters: SM 4500H-B. Organic Parameters: EPA 524.2, 504.1.) Non-Potable Water (Inorganic Parameters: EPA 200.7, 200.8, 6010B, 6010C, 6020, 6020A, 245.1, 245.2, 7470A, 9040B, 9010B, 180.1. 300.0, 332.0, 6860, 353.2, 410.4, 9060, 1664A, SM 4500CN-E, 4500H-B, 4500NO3-F, 4500CL-D, 5220D, 5310C, 2130B, 2320B, 2540C, 3005A, 3015, 9010B, 9056. Organic Parameters: EPA 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330A, 8082, 8082A, 8081A, 8081B, 3510C, 5030B, MassDEP EPH, MassDEP VPH.)

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Solid & Hazardous Waste (Inorganic Parameters: EPA 200.7, 6010B, 6010C, 7471A, 6860, 1311, 1312, 3050B, 7196A, 9010B, 9012A, 9040B, 9045C, 3500-CR-D, 4500CN-CE, 2540G, Organic Parameters: EPA 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330A/B-prep, 8082, 8082A, 8081A, 8081B, 3540C, 3546, 3580A, 5035A, MassDEP EPH, MassDEP VPH.) The following analytes are not included in our current NELAP/TNI Scope of Accreditation: EPA 8260B: Freon-113, 1,2,4,5-Tetramethylbenzene, 4-Ethyltoluene. EPA 8330A: PETN, Picric Acid, Nitroglycerine, 2,6-DANT, 2,4-DANT. EPA 8270C: Methyl naphthalene, Dimethyl naphthalene, Total Methylnapthalenes, Total Dimethylnaphthalenes, 1,4-Diphenylhydrazine (Azobenzene). EPA 625: 4-Chloroaniline, 4-Methylphenol. Total Phosphorus in a soil matrix, Chloride in a soil matrix, TKN in a soil matrix, NO2 in a soil matrix, NO3 in a soil matrix, SO4 in a soil matrix. EPA 9071: Total Petroleum Hydrocarbons, Oil & Grease.

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ENVIRONMENTAL SAMPLE CHAIN OF CUSTODY~ ~ANCHOR'/..., OEA~305 W Grand Ava Sullo 300, Monlvolo, Now Jer.oy 07545; ph: 201.930.9890

Client: Newtown Creek Group Project: Newtown Creek

COCID:

Sample Custodian:

Lab:

AAL-20121 006-164742

Ib

Alpha Analytical Labs

cocCollected # LabSample Field Sample ID Matrix Containers Analytical Program ac'Number Date Time

001 TN005SG-000014.20121005 SE 10/05/2012 09:32 B Newtown Creek Surface Sediment 0002 TN002SG-000011-20 121005 SE 10/05/2012 10:41 8 Newtown Creek Surface Sediment 0003 TN003SG-000015-20121005 SE 10/05/2012 11:24 8 Newtown Creek Surface Sediment 0

<t 004 TN004SG.000015-20121005 SE 10/05/2012 11:46 8 Newtown Creek Surface Sediment 0/0 005 TN006SG.000015.20121 005 SE 10/05/2012 13:16 8 Newtown Creek Surface Sediment 0

I 12 006 SG.RB.20121006 wa 10/06/2012 09:05 9 Newtown Creek Rinse Blank Sediment Surface 0N 007 HB008SG.000015.20121006 SE 10/06/2012 09:55 8 Newtown Creek Surface Sediment 0(c" 008 HB007SG-000015.20121 006 SE 10/06/2012 10:45 8 Newtown Creek Surface Sediment 0Cb 009 HB006SG-000015-20121 006 SE 10/06/2012 11:30 8 Newtown Creek Surface Sediment 0;;. 010 HB005SG.000015.20121 006 SE 10/06/2012 12:19 8 Newtown Creek Surface Sediment 0Itt 011 HB1005SG.000015-20121006 SE 10/06/2012 12:19 7 Newtown Creek Surface Sediment 0

02"" 012 HB004SG.000015-20121 006 SE 10/06/2012 13:27 8 Newtown Creek Surface Sediment 0,Z~ 013 HB003SG.0000 15-20 121006 SE 10/06/2012 14:21 8 Newtown Creek Surface Sediment 0,t6 014 HB002SG-000015-20121 006 SE 10/06/2012 15:05 8 Newtown Creek Surface Sediment 0!fJ 015 HB001 SG.000015.20121 006 SE 10/06/2012 15:54 8 Newtown Creek Surface Sediment 0I 016 SG.TB.20121 006 WQ 10/06/2012 16:23 2 Newtown Creek Trip Blank 0

<1,I,{;L -':>,ll,{'1.-Zt.1,3,25).1,2Q.}

Comment:

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Serial_No:11051209:46

of 279

SAMPLE_CUSTO

LAB_QC COC_ID DIANNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006.164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-2"0121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL.20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006.164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 Ib

TURN_A CONTAINROUND_ TAT_UN I ER_COUTIME T NT-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1-1 DAYS 1

METHODNAASTM D7263ASTM D422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 90450SM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BNAASTM 07263ASTM 0422EPA 601OB/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 9045DSM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BNAASTM D7263ASTM D422EPA 601OB/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 90450SM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BNA

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SAMPLE_ SAMPLEMATRIX DATE 31ME TEST_REQUEST

SE 10/6/2012 15:54 ArchiveSE 10/6/2012 15:54 DensitySE 10/6/2012 15:54 GrainsizeSE 10/6/2012 15:54 Metals, totalSE 10/6/2012 15:54 n-alkanes & isoprenoids (inc. DRO & TPH)SE 10/6/2012 15:54 PAHs & alkyl PAHsSE 10/6/2012 15:54 pHSE 10/6/2012 15:54 Sediment AmmoniaSE 10/6/2012 15:54 Sediment Cyanide, TotalSE 10/6/2012 15:54 Sediment MercurySE 10/6/2012 15:54 Sediment Nitrate/NitriteSE 10/6/2012 15:54 Soot CarbonSE 10/6/2012 15:54 Sediment Phosphorus, TotalSE 10/6/2012 15:54 SedimentTKNSE 10/6/2012 15:54 Sediment TOCSE 10/6/2012 15:54 SulfideSE 10/6/2012 15:54 Total SolidsSE 10/6/2012 15:54 VOCsSE 10/6/2012 15:05 ArchiveSE 10/6/2012 15:05 DensitySE 10/6/2012 15:05 GrainsizeSE 10/6/2012 15:05 Metals, totalSE 10/6/2012 15:05 n-alkanes & isoprenoids (inc. DRO & TPH)SE 10/6/2012 15:05 PAHs & alkyl PAHsSE 10/6/2012 15:05 pHSE 10/6/2012 15:05 Sediment AmmoniaSE 10/6/2012 15:05 Sediment Cyanide, TotalSE 10/6/2012 15:05 Sediment MercurySE 10/6/2012 15:05 Sediment Nitrate/NitriteSE 10/6/2012 15:05 Soot CarbonSE 10/6/2012 15:05 Sediment Phosphorus, TotalSE 10/6/2012 15:05 Sediment TKNSE 10/6/2012 15:05 Sediment TOCSE 10/6/2012 15:05 SulfideSE 10/6/2012 15:05 Total SolidsSE 10/6/2012 15:05 VOCsSE 10/6/2012 14:21 ArchiveSE 10/6/2012 14:21 DensitySE 10/6/2012 14:21 GrainsizeSE 10/6/2012 14:21 Metals, totalSE 10/6/2012 14:21 n-alkanes & isoprenoids (inc. ORO & TPH)SE 10/6/2012 14:21 PAHs & alkyl PAHsSE 10/6/2012 14:21 pHSE 10/6/2012 14:21 Sediment AmmoniaSE 10/6/2012 14:21 Sediment Cyanide, TotalSE 10/6/2012 14:21 Sediment MercurySE 10/6/2012 14:21 Sediment Nitrate/NitriteSE 10/6/2012 14:21 Soot CarbonSE 10/6/2012 14:21 Sediment Phosphorus, TotalSE 10/6/2012 14:21 Sediment TKNSE 10/6/2012 14:21 Sediment TOCSE 10/6/2012 14:21 SulfideSE 10/6/2012 14:21 Total SolidsSE 10/6/2012 14:21 VOCsSE 10/6/2012 13:27 Archive

FIELD_SAMPLE_IDHBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HB001SG-000015-20121 006HB001SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-0000 15-20121006HB002SG-0000 15-20121006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-0000 15-20121006HB003SG-000015-20121 006HB003SG-000015-20121 006HB004SG-000015-20121 006

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SAMPLE_CUSTO

LAB_QC COC_'D DIANNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 Ib

TURN_A CONTAINROUND_ TAT_UNI ER_COUTIME T NT30 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1-1 DAYS 130 DAYS 0

METHODASTM D7263ASTM D422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 9045DSM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, e1aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BNAASTM D7263ASTM D422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 9045DSM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BNAASTM D7263ASTM D422EPA 601OB/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 9045DSM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGus1afsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BNAASTM D7263

Page 2 of 5

SAMPLE_ SAMPLEMATRIX DATE _TIME TEST_REQUEST

SE 10/6/2012 13:27 DensitySE 10/6/2012 13:27 GrainsizeSE 10/6/2012 13:27 Metals, totalSE 10/6/2012 13:27 n-alkanes & isoprenoids (inc. DRO & TPH)SE 10/6/2012 13:27 PAHs & alkyl PAHsSE 10/6/2012 13:27 pHSE 10/6/2012 13:27 Sediment AmmoniaSE 10/6/2012 13:27 Sediment Cyanide, TotalSE 10/6/2012 13:27 Sediment MercurySE 10/6/2012 13:27 Sediment Nitrate/NitriteSE 10/6/2012 13:27 Soot CarbonSE 10/6/2012 13:27 Sediment Phosphorus, TotalSE 10/6/2012 13:27 SedimentTKNSE 10/6/2012 13:27 SedimentTOCSE 10/6/2012 13:27 SulfideSE 10/6/2012 13:27 Total SolidsSE 10/6/2012 13:27 VOCsSE 10/6/2012 12:19 ArchiveSE 10/6/2012 12:19 DensitySE 10/6/2012 12:19 GrainsizeSE 10/6/2012 12:19 Metals, t01alSE 10/6/2012 12:19 n-alkanes & isoprenoids (inc. DRO & TPH)SE 10/6/2012 12:19 PAHs & alkyl PAHsSE 10/6/2012 12:19 pHSE 10/6/2012 12:19 Sediment AmmoniaSE 10/6/2012 12:19 Sediment Cyanide, T01alSE 10/6/2012 12:19 Sediment MercurySE 10/6/2012 12:19 Sediment Nitrate/NitriteSE 10/6/2012 12:19 Soot CarbonSE 10/6/2012 12:19 Sediment Phosphorus, TotalSE 10/6/2012 12:19 Sediment TKNSE 10/6/2012 12:19 Sediment TOCSE 10/6/2012 12:19 SulfideSE 10/6/2012 12:19 Total SolidsSE 10/6/2012 12:19 VOCsSE 10/6/2012 11:30 ArchiveSE 10/6/2012 11:30 DensitySE 10/6/2012 11:30 GrainsizeSE 10/6/2012 11:30 Metals, totalSE 10/6/2012 11:30 n-alkanes & isoprenoids (inc. DRO & TPH)SE 10/6/2012 11:30 PAHs & alkyl PAHsSE 10/6/2012 11:30 pHSE 10/6/2012 11:30 Sediment AmmoniaSE 10/6/2012 11:30 Sediment Cyanide, TotalSE 10/6/2012 11:30 Sediment MercurySE 10/6/2012 11:30 Sediment Nitrate/NitriteSE 10/6/2012 11:30 Soot CarbonSE 10/6/2012 11:30 Sediment Phosphorus, TotalSE 10/6/2012 11:30 Sediment TKNSE 10/6/2012 11:30 Sediment TOCSE 10/6/2012 11:30 SulfideSE 10/6/201211:30 TotalSolidsSE 10/6/2012 11:30 VOCsSE 10/6/2012 10:45 ArchiveSE 10/6/2012 10:45 Density

FIELD_SAMPLE_IDHB004SG-000015-20121 006HB004SG-000015-20121006HB004SG-000015-20121006HB004SG-000015-20121 006HB004SG-000015-20121 006HB004SG-0000 15-20121006HB004SG-000015-20121 006HB004SG-000015-20121 006HB004SG-000015-20121 006HB004SG-000015-20121 006HB004SG-000015-20121 006HB004SG-000015-20121 006HB004SG-000015-20121 006HB004SG-000015-20121006HB004SG-000015-20121006HB004SG-000015-20121006HB004SG-000015-20121006HB005SG-000015-20121006HB005SG-000015-20121 006HB005SG-000015-20121 006HB005SG-000015-20121006HB005SG-000015-20121 006HB005SG-000015-20121 006HB005SG-000015-20121006HB005SG-0000 15-20121006HB005SG-000015-20121 006HB005SG-000015-20121006HB005SG-000015-20121006HB005SG-000015-20121 006HB005SG-0000 15-20121006HB005SG-000015-20121 006HB005SG-000015-20121 006HB005SG-000015-20121 006HB005SG-000015-20121 006HB005SG-000015-20121 006HB006SG-000015-20121 006HB006SG-000015-20121 006HB006SG-000015-20121006HB006SG-000015-20121 006HB006SG-000015-20121 006HB006SG-000015-20121 006HB006SG-000015-20121 006HB006SG-000015-20121006HB006SG-000015-20121006HB006SG-000015-20121006HB006SG-000015-20121006HB006SG-000015-20121 006HB006SG-000015-20121006HB006SG-000015-20121 006HB006SG-000015-20121 006HB006SG-000015-20121 006HB006SG-000015-20121006HB006SG-000015-20121006HB007SG-000015-20121006HB007SG-000015-20121 006

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of 279

FIELD_SAMPLE_IDHB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-0000 15-20121006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121006HB008SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121006HB008SG-000015-20121006HB008SG-000015-20121006HB008SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121 006HB1005SG-000015-20121 006HBI 005SG-000015-20121 006HB1005SG-000015-20121 006HB1005SG-000015-20121 006HB1005SG-000015-20121 006HB1005SG-000015-20121 006HB1005SG-000015-20121006HB1005SG-000015-20121 006HB1005SG-000015-20121 006HB1005SG-000015-20121 006HB1005SG-000015-20121 006HB1005SG-000015-20121006HBI 005SG-000015-20121 006HB1005SG-000015-20121006HBI 005SG-000015-20121 006HB1005SG-0000 15-20121006HBI 005SG-000015-20121 006SG-RB-20121 006SG-RB-20121 006SG-RB-20121006SG-RB-20121 006


SE 10/6/2012 10:45 GrainsizeSE 10/6/2012 10:45 Metals, totalSE 10/6/2012 10:45 n-alkanes & isoprenoids (inc. ORO & TPH)SE 10/6/2012 10:45 PAHs & alkyl PAHsSE 10/6/2012 10:45 pHSE 10/6/2012 10:45 Sediment AmmoniaSE 10/6/2012 10:45 Sediment Cyanide, TotalSE 10/6/2012 10:45 Sediment MercurySE 10/6/2012 10:45 Sediment Nitrate/NitriteSE 10/6/2012 10:45 Soot CarbonSE 10/6/2012 10:45 Sediment Phosphorus, TotalSE 10/6/2012 10:45 Sediment TKNSE 10/6/2012 10:45 Sediment TOCSE 10/6/2012 10:45 SulfideSE 10/6/2012 10:45 Total SolidsSE 10/6/2012 10:45 VOCsSE 10/6/2012 9:55 ArchiveSE 10/6/2012 9:55 DensitySE 10/6/2012 9:55 GrainsizeSE 10/6/2012 9:55 Metals, totalSE 10/6/2012 9:55 n-alkanes & isoprenoids (inc. ORO & TPH)SE 10/6/2012 9:55 PAHs & alkyl PAHsSE 10/6/2012 9:55 pHSE 10/6/2012 9:55 Sediment AmmoniaSE 10/6/2012 9:55 Sediment Cyanide, TotalSE 10/6/2012 9:55 Sediment MercurySE 10/6/2012 9:55 Sediment Nitrate/NitriteSE 10/6/2012 9:55 Soot CarbonSE 10/6/2012 9:55 Sediment Phosphorus, TotalSE 10/6/2012 9:55 SedimentTKNSE 10/6/2012 9:55 Sediment TOCSE 10/6/2012 9:55 SulfideSE 10/6/2012 9:55 Total SolidsSE 10/6/2012 9:55 VOCsSE 10/6/2012 12:19 DensitySE 10/6/2012 12:19 GrainsizeSE 10/6/2012 12:19 Metals, totalSE 10/6/2012 12:19 n-alkanes & isoprenoids (inc. ORO & TPH)SE 10/6/2012 12:19 PAHs & alkyl PAHsSE 10/6/2012 12:19 pHSE 10/6/2012 12:19 Sediment AmmoniaSE 10/6/2012 12:19 Sediment Cyanide, TotalSE 10/6/2012 12:19 Sediment MercurySE 10/6/2012 12:19 Sediment Nitrate/NitriteSE 10/6/2012 12:19 Soot CarbonSE 10/6/2012 12:19 Sediment Phosphorus, TotalSE 10/6/2012 12:19 Sediment TKNSE 10/6/2012 12:19 Sediment TOCSE 10/6/2012 12:19 SulfideSE 10/6/2012 12:19 Total SolidsSE 10/6/2012 12:19 VOCsWQ 10/6/2012 9:05 Metals, totalWQ 10/6/2012 9:05 n-alkanes & isoprenoids (inc. ORO & TPH)WQ 10/6/2012 9:05 PAHs & alkyl PAHsWQ 10/6/2012 9:05 Sediment Mercury

METHODASTM 0422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 90450SM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BNAASTM 07263ASTM 0422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 90450SM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BASTM 07263ASTM 0422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 90450SM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BEPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 1631M

TURN_A CONTAINROUND_ TAT_UNI ER_COUTIME T NT30 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 245 DAYS 237 DAYS 1

SAMPLE_CUSTO

LAB_QC COC_ID DIANNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20t21006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 Ib

Page 3 of 5

Serial_No:11051209:46

of 279

SAMPLE_CUSTO

LAB_QC COC_ID DIANNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 lbNO AAL-20121006-164742 lbNO AAL-20121006-164742 lbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 lbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 lbNO AAL-20121006-164742 lbNO AAL-20121006-164742 lbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 lbNO AAL-20121006-164742 lbNO AAL-20121006-164742 lbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 lbNO AAL-20121006-164742 IbNO AAL-20121006-164742 lbNO AAL-20121006-164742 lbNO AAL-20121006-164742 lbNO AAL-20121006-164742 lbNO AAL-20121006-164742 lbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 Ib

TURN_A CONTAINROUND_ TAT_UNI ER_COUTIME T NT30 DAYS 345 DAYS 2-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 0

METHODEPA 8260BEPA 8260BNAASTM D7263ASTM D422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 9045DSM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BNAASTM D7263ASTM D422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 9045DSM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BNAASTM D7263ASTM D422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 9045DSM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3

Page 4 of 5

SAMPLE_ SAMPLEMATRIX DATE _TIME TEST_REQUESTWQ 10/6/2012 9:05 VOCsWQ 10/6/2012 16:23 VOCsSE 10/5/2012 10:41 ArchiveSE 10/5/2012 10:41 DensitySE 10/5/2012 10:41 GrainsizeSE 10/5/2012 10:41 Metals, totalSE 10/5/2012 10:41 n-alkanes & isoprenoids (inc. DRO & TPH)SE 10/5/2012 10:41 PAHs & alkyl PAHsSE 10/5/2012 10:41 pHSE 10/5/2012 10:41 Sediment AmmoniaSE 10/5/2012 10:41 Sediment Cyanide, TotalSE 10/5/2012 10:41 Sediment MercurySE 10/5/2012 10:41 Sediment Nitrate/NitriteSE 10/5/2012 10:41 Soot CarbonSE 10/5/2012 10:41 Sediment Phosphorus, TotalSE 10/5/2012 10:41 Sediment TKNSE 10/5/2012 10:41 SedimentTOCSE 10/5/2012 10:41 SulfideSE 10/5/2012 10:41 Total SolidsSE 10/5/2012 10:41 VOCsSE 10/5/2012 11:24 ArchiveSE 10/5/2012 11:24 DensitySE 10/5/2012 11:24 GrainsizeSE 10/5/2012 11:24 Metals, totalSE 10/5/2012 11:24 n-alkanes & isoprenoids (inc. DRO & TPH)SE 10/5/2012 11:24 PAHs & alkyl PAHsSE 10/5/2012 11:24 pHSE 10/5/2012 11:24 Sediment AmmoniaSE 10/5/2012 11:24 Sediment Cyanide, TotalSE 10/5/2012 11:24 Sediment MercurySE 10/5/2012 11:24 Sediment Nitrate/NitriteSE 10/5/2012 11:24 Soot CarbonSE 10/5/2012 11:24 Sediment Phosphorus, TotalSE 10/5/2012 11:24 Sediment TKNSE 10/5/2012 11:24 Sediment TOCSE 10/5/2012 11:24 SulfideSE 10/5/2012 11:24 Total SolidsSE 10/5/2012 11:24 VOCsSE 10/5/2012 11:46 ArchiveSE 10/5/2012 11:46 DensitySE 10/5/2012 11:46 GrainsizeSE 10/5/2012 11:46 Metals, totalSE 10/5/2012 11:46 n-alkanes & isoprenoids (inc. DRO & TPH)SE 10/5/2012 11:46 PAHs & alkyl PAHsSE 10/5/2012 11:46 pHSE 10/5/2012 11:46 Sediment AmmoniaSE 10/5/2012 11:46 Sediment Cyanide, TotalSE 10/5/2012 11:46 Sediment MercurySE 10/5/2012 11:46 Sediment Nitrate/NitriteSE 10/5/2012 11:46 Soot CarbonSE 10/5/2012 11:46 Sediment Phosphorus, TotalSE 10/5/2012 11:46 SedimentTKNSE 10/5/2012 11:46 Sediment TOCSE 10/5/2012 11:46 SulfideSE 10/5/2012 11:46 Total Solids

FIELD_SAMPLE_IDSG-RB-20121 006SG-TB-20121 006TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20 121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN003SG-000015-20121 005TN003SG-000015-20121 005TN003SG-000015-20121 005TN003SG-000015-20121 005TN003SG-000015-20121005TN003SG-000015-20121005TN003SG-000015-20121005TN003SG-000015-20121005TN003SG-000015-20121005TN003SG-0000 15-20121005TN003SG-000015-20121005TN003SG-000015-20 121005TN003SG-0000 15-20121005TN003SG-000015-20 121005TN003SG-000015-20121005TN003SG-000015-20 121005TN003SG-000015-20 121005TN003SG-000015-20 121005TN004SG-000015-20121005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121005TN004SG-000015-20121 005

Serial_No:11051209:46

of 279

FIELD_SAMPLE_'DTN004SG-000015-20121005TN005SG-000014-20 121005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-000014-20121005TN005SG-000014-20 121005TN005SG-000014-20121005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-0000 14-20121005TN006SG-000015-20121 005TN006SG-000015-20121 005TN006SG-000015-20121 005TN006SG-000015-20121 005TN006SG-000015-20121 005TN006SG-000015-20121 005TN006SG-000015-20121 005TN006SG-000015-20121 005TN006SG-000015-20121005TN006SG-000015-20121 005TN006SG-000015-20121 005TN006SG-0000 15-20121005TN006SG-000015-20121005TN006SG-000015-20121005TN006SG-000015-20121005TN006SG-000015-20 121005TN006SG-000015-20 121005TN006SG-0000 15-20121005


SE 10/5/2012 11:46 VOCsSE 10/5/2012 9:32 ArchiveSE 10/5/2012 9:32 DensitySE 10/5/2012 9:32 GrainsizeSE 10/5/2012 9:32 Metals, totalSE 10/5/2012 9:32 n-alkanes & isoprenoids (inc. DRO & TPH)SE 10/5/2012 9:32 PAHs & alkyl PAHsSE 10/5/2012 9:32 pHSE 10/5/2012 9:32 Sediment AmmoniaSE 10/5/2012 9:32 Sediment Cyanide, TotalSE 10/5/2012 9:32 Sediment MercurySE 10/5/2012 9:32 Sediment Nitrate/NitriteSE 10/5/2012 9:32 Soot CarbonSE 10/5/2012 9:32 Sediment Phosphorus, TotalSE 10/5/2012 9:32 Sediment TKNSE 10/5/2012 9:32 Sediment TOCSE 10/5/2012 9:32 SulfideSE 10/5/2012 9:32 Total SolidsSE 10/5/2012 9:32 VOCsSE 10/5/2012 13:16 ArchiveSE 10/5/2012 13:16 DensitySE 10/5/2012 13:16 GrainsizeSE 10/5/2012 13:16 Metals, totalSE 10/5/2012 13:16 n-alkanes & isoprenoids (inc. DRO & TPH)SE 10/5/2012 13:16 PAHs & alkyl PAHsSE 10/5/2012 13:16 pHSE 10/5/2012 13:16 Sediment AmmoniaSE 10/5/2012 13:16 Sediment Cyanide, TotalSE 10/5/2012 13:16 Sediment MercurySE 10/5/2012 13:16 Sediment Nitrate/NitriteSE 10/5/2012 13:16 Soot CarbonSE 10/5/2012 13:16 Sediment Phosphorus, TotalSE 10/5/2012 13:16 Sediment TKNSE 10/5/2012 13:16 Sediment TOCSE 10/5/2012 13:16 SulfideSE 10/5/2012 13:16 Total SolidsSE 10/5/2012 13:16 VOCs

METHODEPA 8260BNAASTM D7263ASTM D422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 9045DSM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA.160.3EPA 8260BNAASTM D7263ASTM D422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 9045DSM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260B

TURN_A CONTAINROUND_ TAT_UN I ER_COUTIME T NT30 DAYS 1-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1

SAMPLE_CUSTO

LAB_QC COC_ID DIANNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 Ib

Page 5 of 5

Serial_No:11051209:46

of 279

CHAIN OF CUSTODY-. PAGE 1 OF 1

nA. ... • • ~ ~:X · .. ~ ~~;L. .. . ~ sa:e as~Iien; inf: PO #:NALYTlCAL

Westborough, MA Mansfield, MA Project Name: Newtown CreekTEL: 508-898;9220 TEL: 508-822-9300

o ADEx o Add'i Deliverables

FAX: 508-898C9193 FAX: 508-822-3288 .- . . . .- . . - ....- • . • Project Location: StatelFed Proaram

t

Criteria

Client: Aloha Amtlvtical Proiect#: ~-...Address: 320 Forbes Blvd Proiect Manaoer: Chris Anderson DYes o No Are MCP Analvtical Methods Reauired?

Mansfield. MA 02048 ALPHA Quote #: DYes 10 No Are CT RCP (Reasonable Confidence Protocols) Reauired?

Phone: 508-8¥-4' 22. • • - ANALYSIS •

Fax: 508-822-3288 181 Standard o Rush (ONLY IF PRE-AP,PROVED)

SAMPLE HANDLING

:Filtr.atlon

.Email: [email protected]

o Done

o These samples have been Previously analyzed by Alpha Due Date: Time:

o Not Needed

o Lab to do :

Otl:ler Project Specific Requirements/Comments/Detection Limits:N

Preservation •N

l"l -=t -0 Lab to do

<0 0

Please provide ANCHOR EQUIS EDD and reference Newtown CreekN ~

(Please specify•....~ I-

beloW)

enI- ~en~ wN

?,~t;~~~W~~;:":;:I.'.1 Sample 10 ollection Sample I Sampler's ~ CiiCii z .

I Date I Time 1Matrix Initials Z ~W

Sample Specific

0 C>Comments

TN005SG-000014-20121 005 10/5/12 0932 sediment !XI !XI D D D D D D D D D D L1218042-02 1

TN002SG-000011-20121005 10/5/12 1041 sediment !XI !XI D D D D D D D D D D L1218042-04 1

TN003SG-000015-20121005 10/5/12 1124 sediment !XI !XI D D D D D D D D D D L1218042-06 1

TN004SG-000015-20121005 10/5/12 1146 sediment !XI !XI- D D D D D D D D D D L1218042-08 1

TN006SG-000015-20121 005 10/5/12 1316 sediment-[gJ !XI D D D D D D D D D D L1218042-10 1

HB008SG-000015-20121 006 10/6/12 0955 sediment !XI !XI D D D D D D D D D D L1218042-14 1

HB007SG-Q00015-20121 006 10/6/12 1045 sediment [gJ !XI D D D D D D D D D D L1218042-16 1

HB006SG-000015-20121006 10!6/12 1130 sediment !XI !XI D D D D D D D D D D L1218042-18 1

HB005SG-000015-20121006 10/6/12 1219 sediment [gJ !XI D D D D D D D D D D L1218042-20 1

HB1005SG-000015-20121006 10/6/12 1219 sediment !XI !XI D D D D D 0 D D 0 0 L1218042-22 1

PLEASE ANSWER QUESTIONS ABOVEl Container Type - - - - - - - - - -

/7 Preservative - - - - - - - - - ,

IS YOUR PROJECT ,ij Re~ished By: qiltemme Received By: Datemme

.I /7 A V9#.( /7~MA MCP or CT RCP?FORM NO: 01..01(1)

{/ // f ,(nlv.»-JUl.QT) //

-- '-.'

----'

Serial_No:11051209:46

of 279

mailto:[email protected]

Sample 10 ollection Sample I Sampler's

I Date I Time I Matrix Initials

~> L'i HB004SG-000015-20121 006 10/6/12 1327 sediment.~!

II HB003SG-000015-20121006 10/6/12 1421 sedimentj

HB002SG-000015-20121006 10/6/12 1505 sediment

HB001 SG-000015-20121006 10/6/12 1554 sediment

''../;..'

'.:

PI~ase provide ANCHOR EQUIS EDD and reference Newtown Creek

•SAMPLEHANDLINGFiltration

DOoneo NotNeededo LabtodoPresentationo Labto do(Please specifybeloW)

Somple SpecificCommenta

0 L1218042-24 1

D L1218042-26 1

D L1218042-28 1

D L1218042-30 1

D .

DDDDD

:.,'-. ,,, .:.,.. I'i':k :

- Ii'

.• .Criteria

~

.. ' .."".~.',::>..' :;i( ••..::.,':",";r."\'," LriHA': ::::;fhb.•../.;C:);... ;. .... ..',' .i;';':!;i.,

:\!r'}::',;'''~~.;f~.e;'fri;;~;.;' ....

IF.1F.11IJ: '.. - : • • ••

o EMAIL 0 Same as Client info PO #:

o Add'i Deliverables

... . . ....

....o FAX

o ADEx

State/Fed Prooram

__ {elltreT••.e

~ Are MCPAnalvtical Methods Reauired?o Yes I 0 No Are CT RCP (Reasonable Confidence Protocols) Reauired?

ANALYSIS

;

,

NN

C')' ..,.<0 0N :Er--

~l-f/)

f/) «« w

N

~ (i)

(i) ZZ ~W0 Cl

~ ~ D D D D D D D D D~ ~ D D D D 0 D ODD~ ~ D D D D 0 D DOD~ ~ D D D D D D D D D0 0 D D 0 D D D DOD'0 D D D D D D D ODD0 D D D 0 DDDDDD0 o D. D 0 DOD D D 00 D D D D DOD D 0 00 D D D D D D D D D D

Container Type -

Preservative

PAGE1 OF 1

Time:

o Rush (ON~Y IFPRE-APPROVED)

. ..

... .•.

Due Date:

ALPHA Quote #:

Project Location:

Proiect#:

Project Manager: Chris Anderson

181 Standard,

. . -Project Name: Newtown Creek

CHAIN OF CUSTODY

Mansfield,MATEL:508-822-9300FAX:508-822-3288

1;;\ANALYT~L

Other Project Specific Requirements/Comments/Detection limits:

. ..Client: Aloha Analytical

Addr~s: 320 Forbes Blvd

Westborough,MATEL:508-898.9220FAX:508-898-9193

PLEASE ANSWER QUESTIONS ABOVEI

Mansfield, MA 02048

Phone: 508-844-4122

Fax: 508-822-3288j , • .,

Email: [email protected]

o ThesesampleshavebeenPrelliouslyanalyzedbyAlpha

IS YOUR PROJ.ECTMA MCP or CT RCP?FORMNO: 01~1(1)(rw.3G-JUL.(7)

/? Relinquisjled By:

./ /.h. .L/"-/ /?'1/

DatelTime

/2lAV ~ /70--,

Received By: Daternme

Serial_No:11051209:46

of 279


SAMPLE HANDLING

Rltratlon,

o Doneo Not Needed

o Labtodo

Preservationo Labtodo

(Please specifybeloW)

" ,

Time:

o Rush (ONLY IF PRE.APPROVI"D)~ Standard

Due Date:

Turn-Around Time

Pro'ect#:

ALPHAQ t #

Project Location:

CHAIN OF CUSTODY1-iA.

ANALYTICAL

Other Project Specific Requirements/Comments/Detection Limits:

o These samples have been Pr~viouSlyanalyzed by Alpha

PI(:lase provide ANCHOR EQUIS EDD and reference Newtown Creek

Mansfield, MA 02048

Phone: 508-844-4122

Fax: 508-822-32l;l8,"

Email: [email protected]

~:>

AtPi-q:~~~!fq';f'~

Sample ID Sampler'sQ):2

.""(L~~U~.gn)YF.' Initials (;j

~S.mpkl SpecificComments

TN005SG-000014-20121 005 1015/12 0932 sediment [gI 0 0 0 0 0 0 0 0 0 0 0 L1218042-02

TN002SG-000011-20121005 10f5f12 1041 sediment [gI 0 0 0 0 0 0 0 0 0 L1218042-04

TN003SG-000015-20121 005 10f5f12 1124 sediment [gI 0 0 0 0 0 0 0 0 0 0 0 L1218042-06

TN004SG-000015-20121 005 10f5f12 1146 sediment [gI 0 0 0 0 0 0 0 0 0 0 0 L1218042-08

TN006SG-000015-20121 005 10f5f12 1316 sediment [gI 0 0 0 0, 0 0 0 0 0 0 0 L1218042-10

HB008SG-000015-20121006 10/6f12 0955 sediment '[gI 0 0 0 0 D 0 0 0 0 0 0 L1218042-14

HB007SG-000015-20121006 10f6/12 1045 sediment [gI 0 0 0 0 0 0 0 0 0 0 0 L1218042-16

HB006SG-000015-20121006 10f6f12 1130 sediment [gI 0 0 0 0 0 0 0 0 0 0 0 L1218042-18

HB005SG-000015-20121 006 10f6f12 1219 sediment [gI 0 0 0 0 0 0 0 0 0 0 0 L1218042-20

HB 1005SG-000015-20121 006 10f6f12 1219 sediment [gI 0 0 0 0 0 0 0 0 0 L1218042-22

PLEASE ANSWER QUESTIONS ABOVEI Container Type

Preservative

15 YOUR PROJECT By: Datemme

MA MCP or CT RCP?FORM NO: 01-01(1)(rev.3O-JUL.o7)

Serial_No:11051209:46

of 279


.'

AJ:iO,CHAIN OF CUSTODY PAGE 1 OF 1

. • . • . • ~_.~:X • .• ~ ~':;L-.. ' . ~ ::':::;i:~PO' .Westborough, MA Mansfield, MA Project Name: Newtown Creek 0TEL: 508~98-9220 TEL: 508~22-9300

\, AOEx o Add'i Deliverables

FAX: 508~98.9193 FAX: 508~22-3288 ... • ... . . ....... • . • Project Location: State/Fed Proaram Criteria

Client: Alpha Analvtical Proiect#:... ~_:l.lIf'.nf.

Addrehs: 320 Forbes Blvd Proiect Manaaer: Chris AndersonI DYes 0 No Are MCP Analvtical Methods Reauired?

Mansfield, MA 02048 ALPHA Quote #: DYes 10 No Are CT RCP (Reasonable Confidence Protocols Reauired?

Phone: 508-844-4122 . • • . ANALYSIS •Fax: 508-822-3288 181 Standard o ~ush (ONLY IF PRE-APPROVED)

SAMPLE HANDLING

": Filtration \

Email: [email protected] " o Done

o These samples have been Previously analyzed by Alpha Due Date: Time:o Not Needed

o Lab to do :

Other Project Specific Requirements/Comments/Detection Limits: Preservation •o Labtodo

PI~ase provide ANCHOR EQUIS EDD and reference Newtown Creek(Please specifybeloW)

~::>

. 'ALPPi..i.Jb.ablp'.:'> \:\!:?

Sample 10 ollection Sample I Sampler'sQ)

:;;E"i(~~,bWsel()n~¥2}: " I Date I Time I Matrix Inilials "iii

(5 Sample Specific~ Comments

".'.yy on ..,....../'{:,'\.SiHB004SG-000015-20121 006 10/6/12 1327 sediment ~ 0 0 0 0 0 0 0 0 0 0 0 L1218042-24 1

'.",}' :'~'I,".'. HB003SG-000015-20121 006 ~ 0 0 0 0 0 0 0 0 0 0 0 1

10/6/12 1421 sediment L1218042-26

Ii'" HB002SG-000015-20121006 10/6/12 1505 sediment ~ 0 0 0 0 0 0 0 0 0 0 0 L 1218042-28 1

,::,i HB001 SG-000015-20121006 10/6/12 1554 sediment ~ 0 0 0 0 0 0 0 0 0 0 0 L1218042-30 1

....' ..lrSG-RB-20121006 10/6/12 0905 water ~ 0 0 0 O. 0 0 0 0 0 0 0 L1218042-12 1

~' ,.,1:,/,," '0 0 0 0 0 0 0 0 0 0 0 0,i;,,:' ,;;>:' 0 0 0 0 0 0 0 0 0 0 0 0' .. '.:',. .••.:;<.". 0 0 0 D 0 0 0 0 0 0 0 0,""ii", ";"H; 0 0 0 0 0 0 0 0 0 0 0 0.....f.! " ;", .1' 0 0 0 0 0 D 0 0 0 0 0 0"

PLEASE ANSWER QUESTIONS ABOVEl Container Type - . . . - . - -

Preservative - - . - . . - -

IS YOUR PROJECT 4 Relinquished By: Datemme Received By: Oalemme i,

MA MCP or CT RCP? / ~- A jtJJ a/IL. 0700 ur0\" >'FORM NO: 01-01(1)

,~ I I ~j.(teY.3O-JUL.()1) ';']j? Ii:

..,"-

Serial_No:11051209:46

of 279


Serial_No:11051209:46

of 279

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