Post on 05-Mar-2021
Bromofluorobenzene (BFB)
CaseNo._^&M———— Contractor ^^^
instrument in V^A Date ^ i /^. . . . . / . /
Lab ID KPF^W 7^?/9, Data Release Authorized By:
^/o$-^ T
m/« ION ABUNDANCE CRITERIA ;
Contract No. 6? 9, - <^-^&
Time__^C3________
%RELATIVE ABUNDANCE
50
,75
95
96
173
1 7 4 ~ "
175
176
177
.15.0 - 40.0% of the base peak . . .
30.0 - 60.0% of the base peak
Base peak, 100% relative abundance '..
5.0 - 9.0% o< the base peak .... ;
Less than 1.0% of the base peak
5.0 - 9.0% of mass 174
Greater than 95.0%. but less than 101.0% of mass 174
5.0 • 9.0% of mass 176
• • -^9(z? ; : . • •
- 5Z fc /- /DO. Gb
^ fc3 •0
-.-- .u,.s9' .. . . . . . . . . . -^.^7 C%^)1,
' ^'^ ^^\
• H.^ -(-fc^5-2-.
-r,
e,—,
„
Value in parenthesis is % mass 174.
^ Value in parenthesis is % mass 175.
THIS PERFORMANCE TUNE APPLIES TO THE FOLLOWING
SAMPLES, BLANKS AND STANDARDS.
SAMPLE ID
r^i F41^r4o4-?7 - --F^SL-S 0 "P' /^2,0
/=^^S°• . . -—- . - ' '
-- • •-• • • • - • - •••—
" --—-———
LAB ID
5^%-)rf-7 -5( lS- ia
-fPS
•- - • —'^ — ----1.^- f5 A^S-if3-J^Jri5- ••
. :• -T2,b«k 7X
- - - - — - - • — - - • • • • • •
—„—--.^-,-———--••-- - • -— - . - . . - . - - • - - - • - - • - - - - - • — -
DATE OF
•B /
,. ,. ^
ANALYSIS
^^
1
/
TIME OF ANALYSIS
^•0^-
9:0^^'.of-'v <u &
:0'»-
G;o%-- . .. 4 .-,,-.—.-
..•.-..-^b.;- ..,;
4/84
80383 FORM V
MASS LIST DATA:08/19/84 2:07:00 + 35:16 CALI:SAMPLE: 50 UG/L STD, VERIFICATIONCONDS. :
EPAVOA1718 #1032EPAVOA1718 # 1
BASE M/E: 95RIC: 220416.
JW
50-51.57.61.62.63.68.69.73.74.75.76.78.80.86.88.93.94.95.96.
174.175.176.177.
50.77»SS
020404040406060606080808889694060810101000040000
3.
7.
24.6.4.5.5.4.
12.12.
6.20.59.
4.5.4.
• 4.5.4.
13.100...6.66.
5.65.4.
90
RA
969286415611443112906195327.1207657040063-59473900
0.
7. F
4.1.0.1.1.0.2.
• 2.• 1.4.
11.0.
. 1.0.
• 0.: 1.0.2.
19.1.
12.1.
12.8.
00
(1C
833494050879413818025396039181118852342888066577
0. MINIMA# 0 MAXIMAINTEN.
10640.2948.2072.23QS.2372.1750.5304.5248.2608.8864.
2540B.2112.2268.2008.1792.2456.1948.5560.
42624.2824.
28384.2332.
27872.1704.
MIN INTEN: 1662.
t 9 '• [- 0 .0
1
50
5.0iiu
MASS SPE03^19/84SAMPLE;CONDS.:
.0
1 5^01,
\M60
CTR'?
59"
68
UM;07;eUG/L
7E
1
w
38 ^STC
^.1
78
.
3.
<
8
35; 16UERIFICAT
95
;
!
3: 88.1u^0 '
ION
.1
,
104.0 117.8l., , , 1 .1 , , , . , . , . . • , - , . .100 123
DflTfl: EPAUOhll713 #1832 BASE M/CflLI; EPWOA1719 #1 RIC;
17'
<1
'
130.0 143-8
148 169
E^
..
1
; 9528416.
0
1
1 , , , ,1 . | . .
180
I- O Q
SCANS 1000 TO 1060ass; CHROMATOGRAII DATA; EPAUOAIZIS #10328/'1&/-S4 2;07;e0 ' CftLl! EPfl"Oftl71S <tlAMPLE: 50 UG/-L STO. UERIFICATIONONDS. • • • - - : • • • • . • • ! • . , . . ......flNGE! G 1,1309 LABEL: N 2, 3.9 QUAN; A 2, 2.0 J 0 'BASE: U 20, 3
• 1033'43113.490681. ;
1060 SCAN36;13 TIME
43264.
95.028± 0.509
Initial Calibration Data
Volatile HSL Compounds
Case No: - .^PS'?
Contractor: ^ S>T-e^-h'i^C
Instrument I D:
Contract No: h '?i— ^V"
Calibration Data- ?,J/c57bV- 7 T
Minimum RF for SPCC is 0.300 Maximum % RSD for CCC is 30%
/--
Laboratory )•
Compound
Chloromethane
Bromomethane
Vinyl Chloride
Chloroethane
Methylene Chloride
Acetone
Cartion Disulfide
1 . 1-Dichloroethene
1, 1-Dichloroethane
Trans-1, 2-DichloroeIheneChloroform
1. 2-Oichloroethane2-Butanone
1 . 1 . 1 -Trichloroothane
Carbon Tetrachloride - - -
Vinyl Acetate
Bromodichloromethane
1. 2-Dichloropropane
Trans-l. 3-Dichloropropene
Trichloroethene
Dibromochloromethane
1 . 1 . 2-Trichtoroethane
Beniene
cis-1, 3-Dichloropropene2-ChloroethylvmyletherBromoform
2-Hexanone
4-Melhyl-2-Penlanone
Tetrachloroelhene
1. 1 . 2, 2-Teirachloroethan<
Toluene
ChlorobenzeneElhylbeniene
SlyreneToial Xylenes
RFzo
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1: /./yy
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RF -Response Factor (subscript is itw amouni of UQ/LIR^ -Average Response Factor%RSD -Percent Relative Standard Deviation
CCC -Calibration Check Compounds (*)SPCC -System Performance Check Compounds (
Form VI
Environments) Prolecnon Agency,P.O. Box 616. Alexandria. Vtrgini
< 1 C
Lab SamplB ID No- -T T<2 •n
CLP Sample Management OMice,22313 703/557-2490
Organics Anal(Pa
-T-fs^m/ / G >-^ - J ,
, ^
. Volatile C
Concentration: (\.ow)
• ' OJ
Percent Moisture (Decan
ysisDgel)
Cas
QC
Oat
ompot
Mediu
^
^7^
led): -i-
)ata Sheet
<? Nn .:. .
Rnpnrt Nn / / -3
llrai-1 Nn- W 0 '
Jnds
m (Circle One)
/C? /^
'67'
pH
Sample Number
^ 1 1 ^
^6^Q
Ol-(c^%0
^\n^i i
CASNumber
74.87-3
74-83-9
75-01-4
75-00-3
75-09-2
67-64-1
7.5-15-0
-75..35-A- . -
75-34.3
156-60-5
67-66-3
107-06-2 '
78-93-3
71.55-6
56.23-5
108-05-4
75-27-4
Chloromeihane
Bromomethane
Vinyl Chloride
Chloroelhane
Methylene Chloride
Acetone
Carbon Disultide'- ' -:
1.'!-Dichtoroethene
1. 1-Dichloroethane
Trans-1, 2-Dichlofoethene '
Chloroform
1 , 2-Dichloroethane
2-Buianone
1 , 1 . 1-Trichloroeihane
Carbon Tetrachloride
Vinyl Acetate
Bromodichloromethane
ug/\0fi£p(CiTCte-O-
^^• uu^
^D
•a. -,^
' •^6a©^050-^0
- 5040S.U^0^0aw
Kg,
\
1
\
v
CASNumber
79-34-5
78-87.5
10061-02-6
79-01-6
124-48-1
79-00-5
71.43-2
10061-01-5
1'10-75-8
75-25-2
591-78-6
1 0 8 - 1 0 - 1
127 -18 -4
108.88.3
108.90-7
100-41-4
100.42-5
1 , 1 . 2 . 2-Tetrachtoroelhane
1 , 2-Dichloropropane
Trans-1, 3-Oichloropropene
Thchloroethene
Oibromochloromelhane
1 . 1 . 2-Trichloroeihane -
Benzene - • • • ; •-.
cis-1. 3-Dichloroorop-ene
2-Chloroethylvinylelher
Bromoform
2-Hexanone
4-Methyl 2 "entanons
Tetrachloroeihene
Toluene
Chlorobenzene
Elhylbenzene
Styfene
Total Xylenes
ug/l or i^/l(Circleon
^0^^•.?C>1
o®.• ^Q:
'): . , : : • so-^' ^
A-/^G? ^SO50^ao.^\
<9^Ie)
\
1-
^
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sl/
0»ta Reporting Qu
o'EPA. ttie lollowing rfl'
Addilionit flags 0( looinoiet ••plJining results are encourBQod Mowflvei.
dfidnilion of eact) flao must be •xoliot '
Vklu* H the fBtutI ii, • value graaier tti«n or oqu«l to 1*^
d«ieciion liniil. rool lf< value -
U lndic«t«( compound •w*t •fivred lo< birt "01 detected
Repon lha mmimun' Oeiflmon limn lor ihe MfnoK wth
the U (eg.. 10<J| b«»*d on f^cetMry concflnift'ort''
dilulion •Clioni fTh«S is not necorurily th« iritlium^nl
d«iaccon limit 1 The <o<rtrwle thould ffl U-
Compourtd we •fvlvied for but noi doieci«<] The
f\urrib«r <( i e mimriurn an«irmblft d laciion limit ICK
the urnple
'This llao apD'ies 10 pesticide infrnBiers wtiere (h<
tdeniilicaiion has bflen contifiTKil bv GC/MS Single
cornooneni peslicides>10 ng/ul in the <in«l eiirJd
should bt condfmed by GC/MS
used when ihe an«lvte it (our i i" ihe tilmk
i sarnpie Imvlicatet possible/'pfobable
minanon e"d warns the d»l* UM' fo lake
aciion
Hags ar^d footnotes "iay be lequi'ed 10
e the fflsuits M uted. ihey TiutI be <ull>«iu-^) rt-s^tioi'o" aliached to ih« daia
Othai dinei speCili
piocwfiv deti
Environmental Prelection Agency. CLP Sample MJniggmem Oftic*.P.O.Box 818. Alexandrie. Virginia 22313 703/557-2490
Sample Number
" ;3^Organics Analysis Data Sheet
(Page 2)
Semivolatile Compounds
Concentration: •(^vi/ Medium . (Circle One)
Date Extracted/Prepared:
'dium . (Cir(
v^\s±Date Analyzed:
Conc/Dil Factor
CASNumber
62-75-9
108-95-2
62-53-3
111.44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
'95-48-7
39638-32-9
106-44-5
621-64.7
67-72-1
98.95-3
78-59-1
88-75.5
105-67-9
65-85-0
1 1 1 - 9 1 - 1
120-83-2
120-82-1
91-20-3
106-47-8
87.68-3
59.50-7
91-57 -6
77-47-4
88-06-2
95-95-4
91-58.7
68-74-4
1 3 1 - 1 1 - 3
N-Nnrosodimethytamine
Phenol
Aniline
bis(-2-Chloroelhyl)Elher
2-Chlorophenol
1. 3-Dichlorobenzene
1. 4-Dichlorobenzene
Benzyl Alcohol
1 , 2-Dichlorobenzene
2-Melhylphenol
bis(2-chloroisopropyl)Etner
4-Methylphenol :
N-Nrtroso-Di-n-Propylarnine
Hexachtocoethane
Nitrobenzene
Isophorone
2-Nitrophenot
2. 4-Dimethylphenol
Benzoic Acid
bis(-2-ChloroeihoxytMeihane
2. 4-Dichlorophenol
1 , 2, 4-Thchloroben2ene
Naphthalene
4-Chloroaniltne ;
Hexachlorobutadiene
4-Chloro-3-Methytphenol
2-Meihylnaph(halene
HeKachlorocyclopentadiene •;
2, 4. 6-Trichlorophenol :
2. 4, 5-Tnchlorophenol
2-Chloronaphihalene
2-Niuoanilme
Dimeihyl PhihalaTe
ug/lorfia^(CireieCT
T-KPOVTl!5Q•nmo-TUTO1-1 (TO1-1 (TO'ntm'nisv-nro"M3t)'MTOTPirD'nvT>/7-,rro-ncn>-runi•T-im>'TT<n)^W:-nTO-ni11^'^ff&"iro'""y&^TO-nst)111^.3?^^fcsro'no-o^ (ro-nro
^^
CASNumber
83-32-9
51-28-5
100-02-7
132-64-9
I'ZI-14-2
606-20-2
84-66-2
7005-72-3
86-73-7
100-01-6
534-52-1
86-30-6
101-55-3
118 -74 -1
87.86.5
8501-8
120-12-7
84-74.2
206-44-0
92-87.5
129-00-0
85-68-7
9)-94-1
56-55-3
1 1 7 - 8 1 - 7
218 -01 -9
117 -84 -0
205-99-2
207.08-9
50-32-8
193-39-5
53-70-3
191.24.2
Acenaphihene
2, 4-Dinitrophenol
4-Nitfophenol
Oibenzofuran
2, 4-Dinitrotoluene
2, 6-Dinitrotoluene
Oiethyfphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroaniline :
4, 6-Dmttro-2-MethylphenoI
N-Nnrosodiphenylamine (1)
4-Bromophenyl-phenylether
Hexachlorobcnzene
Pentach lorophenol
Phenanthrene
Anthracene
Di-n-Bmylphihalale'
Fluoranthene
Ben^idine
Pyrene
Buiylbenzylphthalale
3. 3'-Dichlorobenz»dine
Ben20<alAnthracene
bis(2-Elhylhexy()Phthatale
Chrysene
Di-n-Ociyt Phlhalate
Benio(b)Fluoranlhene
BenTo(k)Fluoranthene
Banzo(alPyrene
lndeno<1, 2. 3-cd)Pyfene
Dibenz(a, h)Anthracene
Benzofg. h. itPeryiene
u
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^
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?,
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g/l or(Jg^CircieT
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100
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"lOT)ITO
r^1-not>^113&'.IS?nini1,^L^BO ^^0^rw \n^-n^ncor^Tiro1-1 rDsT.yo'
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Environmental Prot«cl(onAg«nCY. CLP Sample Man«g«m«nl Office.P.O. Bo* 618. AI«Mndru,Vln)inr22313 703/557-2490
Organics Analysis Data Sheet(Page 4)
Tentatively Identified Compounds
CASNumbor
1
2
3.
4.
S
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7.
B
9.
in1112
13
14
TS7
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17
in1 9 .
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17
23
24
25.
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27
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29.
in
Compound Narne
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WtNJZ/n^^xrv.——r(—<—-'———————————————————^k/>s-k/i' <v^
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etion
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QUANTITATION REPORT FILE: EPAVOA1725
DATA: EPAVOA1725. TI88/19/84 9:06:00SAMPLE: 77.1.13-12
SUBMITTED BY SPA ANALYST: RJM
AMOUNT=AREA(HGHT) » REF. AMNT/(REF. AREA<HGHT)* RESP.FACT).RESP. FAC. FROM AVERAGE OF WHOLE . RL
NAME«
HSLHSL
HSLHSLHSL
HSLHSLHSLHSL
BROMOCHLORMETHANE (INTERAL STANDARD)P-DIFLUOROBENZENE (INTERNAL STANDARD)DXCHLOROBENZENE-D5 (INTERNAL STANDARD)CHLOROMETHANEBi"<OMOMETHANEVINYL CHLORIDECHLOROETHANEMETHYLENE CHLORIDEACROLEINACRYLONITRILE
1,1-DICHLOROETHYLENE1.1-DICHLOROETHANETRANS-1,2-DICHLOROETHYLENECHLOROFORM1.2-DICHLOROETHANE1, l., 1-TRICHLOROETHANEACETONECARBON DISULFIDECARBON TETRACHLORIDEBROMODICHLOROMETHANE1,2-OICHLOROPROPANETRAN5-1-3-DICHLOROPROPYLENETRICHLOROETHYLENEB£NZENE 'DIBROMOCHLOROMETHANE1, -., 2-TRICHLOROETHANECIE-1,3-DICHLOROPROPYLENE2-CHLOr.:OETHYL VINYL ETHEREROMOFORMMETHYL ETHYL KETONEVINYL ACETATEMTTHYL ISOBUTYL KETONE1,2-DICHLOROETHANE-D4 (SURROGATE)B£N2:ENE-D6 (SURROGATE)DJr^ROMOTETRAFLUOROETHANE (SURROGATE»
B-T:S ' PERFLUOROISOPROPYL > KETONE ( SURROGATE )FL'JOROBENZENE (SURROGATE)TCThACHLOROETHYLENE1.1,2,2-TETRACHLOROETHANETOLUENE
CHLOROEENZENEE-KYLBENZENE2-HEXANONES"i'RENE
0-XYLEMEM- XYLENE
M-&ROM&BENZOTRIFLUORIDE < SURROGATE)D-5 ETHYLBENZENE (SURROGATE)TOLUENE-DS (SURROGATE)P-E:ROMC'FLUOROBENZENE (SURROGATE)
SCAN3RO-W?8S7
FOUNDFOUNDFOUNDFOUNDFOUNDFOUND
TIME REF13:07 123: 53 229: 17 3
RRT METH1. 000 A BB1. 000 A BB1. 000 A BB
AREA(HGHT)39526.
387673.2666B8.
AMOUNT 7.TOT50. 000 UG/L 9. 1150. 000 UG/L 9. 1150. 000 UG/L 9. 11
M/ENOTNOTNOTNOTNOTNOTNOT58
NOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOT
436584
NOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOT9895
SCANFOUNDFOUNDFOUND
FOUNDFOUNDFOUNDFOUND
304FOUNDFOUNDPOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
7254o7
616FOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUND'FOUNDFOUNDFOUNDFOUNDFOUNDFOUND
S.1510-3&
TIME
10: 23
24: 4615: 5721: 03
27: 5135: 20
REF
1
222
33
RRT
0. 792
1. 8370. 6630. 881
0. 9511. 207
METH
A BB
A BBA BBA BB
A BBA BB
AREA(HGHT)
3513.
19684.335240.672514.
742869.456286.
AMOUNT
19. 273 UG/L
12. 819 UG/L90. 726 UG/L90. 032 UG/L
98. 352 UG/L87. 898 UG/L
7.TOT
3. 51
2. 3316. 5216. 40
17. 9116. 01
DUAL MOSS SPECTRUM03/'19./84 9;0e;08 + 18:23SAMPLE: 77113-12CONDS.!ENHANCED (S 15B 2N 0T)
DATA: EPAUOA1725 #304 BASE M/E! 43/- 43CALl! EPSWOA1725 #1 RIC; 3351. / 6131.
35 45 . . y 55
DUAL MASS SPECTRUM DATA: EPWOA1725 #725 BASE M/'E; 43/- 4383/'19/84 3!06!00 + 24!46 CALI; EPftWftl725 ttl RIC; S399./ 11999.SAMPLE; 77113-12CONDS.:ENHANCED (S 15B 2N 0T;'
100.9-] r 3920.
50.0-
—i 'l111 i—|—P"1—i—r i—I—I—\—'——1—I—1—I—1—[""T—I—<—|—>—I—1—I—'—!—'—1—i—|—^
M/E 58 100 150 200
50,0- r-i iI r
^ i ^
| 0 0 1 . 7 2 : : ' " 392e-
SCANS 1 TO 2860RIC DATA: EPABN1368 #1CALI; EPABH136S ftl63/18 84 14:01:60
SAMPLE; 77113-12CONDS.:RANGE; G 1,2860 LABEL; N 2, 2.8 QUAN: A 1, 3.0 J 8 BASE; U 20,
'J\
LA
5007:55
100015;50
1500
23:45200031:40
250039:35
3UANTITATIGN REPORT
3ATA: EPABN1368.TI39/18/84 14:01:003AMPLF: 77113-123UBMITTE.D BY:
FILE: EPABN1368
ANALYST:
•\MOUNT=AREA(HGHT) * REP. A(";NT/(REF. AREA(HGHT X RESP.FACT)teSP. FAC. FROM AVERAGE OF WHOLE . RL
NO NAMfe.1 * D-4 1,4-DICHLOR03ENZENE2 * D-8 NAPHTHALENE3 » D-8 ACENAPTHENE4 » D-10 PHENANTHRENE5 » D-12 CHRYSENF6 * D-12 PERYLENE7 2-FLUOROPHENOL (SURROGATE)8 D-5 PHENOL (SURROGATE)9 D-5 NITROSENZENE (SURROGATE)10 2-FLUOROBIPHENYL (SURROGATE)11 2,4,6-TRIBROMOPHENOL (SURROGATE)12 D-14 T6.RPHENYL (SURROGATE)13 N-NITROSODIMETHYLAMINfc14 2-CHLOROPHENOL15 PHENOL16 BIS (2-CHLOROETHYL) ETHER17 I,3-DICHLOROBENZENE18 1,4-DICHLOROBENZEME19 I,2-DICHLOROBENZENE20 HSL ANILINE21 HSL BENZYL ALCOHOL2? BIS(2-CHLOROISOPROPYL)ETHER23-. - HEXACHLOROETHANE.34. N-NITROSODIPROPYLAMIN&25 NITROBENZENE26 ISOPHORONE27 2 NITROPHE.NOL28 2,4-DIMETHYLPHENOL29 BIS(2-CHLOROETHOXY»METHANE30 2,4-DICHLOROPHENOL31 I,2,4-TRICHLOROBENZENfc32 NAPHTHALENE33 HEXACHLOROBUTADIENE34 P-CHLORO-M-CRESOL35 HEXACHLOROCYCLOPENTADIENE36 2,4,6-TRICHLOROPHENOL37 HSL 2-METHVLPHENOL38 HSL 4-METHYLPHENOL39 HSL BENZOIC ACID40 HSL 4-CHLOROANILINE41 HSL 2-METHYLNAPHTHALENE42 2-CHLORONAPHTHALENE43 DIMETHYL PHTHALATE44 ACENAPHTHYLENE45 2,6-DINITROTOLUENE46 ACENAPHTHENE
NO NAME47 ' 2,4-DINrTROPHEMOL48 4-NITROPHENOL49 2,4-DINITROTOLUENE50 FLUORENE51 4-CHLOROPHENYL PHENYL ETHER52 DI ETHYL PHTHALATE53 4< 6-DINITRO-2-METHYLPHENOL54 N-NITROSODIPHENYLAKINE55 1,2-DIPHENYLHYDRAZINE56 4-BROMOPHENYL PHENYL ETHtR57 HEXACHLOROBENZENE58 PENTACHLOROPHENOL59 PHENANTHRENE60 AN1HRACENE61 DI-N-BUTYL PHTHALATE62 FLUORANTHFNE63 HSL 2,4,5-TRICHLOROPHENOL64 HSL 2-NITROANILINE65 HSL 3-NrTROANILrNE66 HSL DIBENZOFURAN67 HSL 4-NITROANILINE68 BENZIDINE69 PYRENE70 BENZYL BUTYL PHTHALATE71 BENZCK A)ANTHRACENE72 3,3'-DICHLOROBENZIDrNL73 CHRYSENE74 BIS(2-ETHYLHEXYL> PH7HALATE75 DI-N-OCTYL PHTHALATE76 BENZCK B>FLUORANTHENE77 BENZO(K>FLUORANTHENE_7S________BENZO (A > PYRENE79 INDENOd, 2, 3-CD1PYRENF80 DIBENZOCA,H>ANTHRACENE81 BENZCHGHDPERYLENE
NO M/E SCAN TIME REt- RRT KFTH AREA(HSHT) AMOUNT 7.TOT
NO123456789
10111213141516171819202122232425262728293031I?3334 -353637383940
424344454647434950515253545556
M/E'152136164188240264NOT
•NOTNOTNOTNOTNOTNOT
'NOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOT
.NOTNOTNOT
.NOT• i ya
:NOT107-NOTNOTNOTNOTNOT•NOT
NOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOT
SCAN702942
1280155920672320
FOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
9A4—FOUND
-—WtWJ~FOUNDFOUNDFOUNDFOUNDFOUNDFOUND
FOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
T111420243236
17
IME075516414441
06
REI-123456
2
1.1.1.1.1.1.
1.
RRT000000000000000000
146
'146
MEAAAAAA
A
£THBBBVBBBBBBBV
T?B———
ua
AREA<H3HT2&364.72157.41305.78294.73583.52?87.
—————3Tt-.———
"——271-———
) AMOUNT40.00040. 00040.00040.00040-00040.000
————0.154-
—"0. ^04
———©-£83-
UO/MLUO/MLUO/MLUG/MLue/MLUG/ML
US/ML
-O&TfH——
-Ue^SL-
•/.TOT15. 6415. 6415. 6415. 6415. 6415. 64
—8-06———
—0—24
n 11
NO
58
60^—6263646566 .67
697e~717273747576777879 :8081
M/E
NOT
NOT
NOTNOTNOTNOTNOTNOT
NOT-*-49-NOTNOTNOT149
NOTNOTNOTNOTNOTNOT
SCAN TIME RE
FOUND
FOUND—IWt——2S-59——-AFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
FOUND—T7B7—31: 2B——5FOUNDFOUNDFOUND2106 33:21 S
•—SPly—35. 06——tFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
:F RF
t——1-0<5
1. 01
^T MET
?3——ft-Bl
sn—a-w
9 A*B^ 5 A S ^
H AREAO
B————————794
B 13057B—————- 5004
4-3HT) AMOUNT,
! 0 . c 7 5 u G /
h—————- 0. 338 W71
r:——————0. ^^6 UG/
6.896 UG/———— 1 , p7-4 UP/I
%TOT
«fc—&-+a——
HI.——U. 14——
Mt——O-O?"^" '''
/
ML 2. 70 Qt-LQ^3—— o
DUAL MASS SPECTRUM89/18/84 14:01:00 + 14:57SAMPLE; 77113-12CONDS.!ENHANCED <S 15B 2H 6T)
DATA: EPABH1368 ft944CALI: EPABN13G8 #1
BASE M/E; 128/ 136RIC: 212./ 6495.
p ' I ' M ' ' i i t u 1 \ r
DUAL MASS SPECTRUM09/18/-84 14:91:00 + 17:06SAMPLE: 77113-12CONDS.!ENHANCED <S 15B 2N 0T)
DATA! EPABN1368 #1080 BASE H/-E! 82/ 82CALI: EPABN13£8 #1 RIC; 17823./ 23551.
160
•a- <s>oo (M
,
(M
L
oo '•-C--4
•0-1
— in
UJ —
i
UJ
So-
^5
0000
LO U
id
CT
55
CQ C
O<
r<r
UJ UJ
liQ 00 —
I
UJO
CT
Cl_
•• •u"i •
- »-* in
Ln p~
i-n •i-
0^
00
••
•• LU^
S
. U
J .
1_)
co _i m
z-i-rt CL. Q
<r<r '-. •z- z
i=< cri <r o
z0
0 IT
l 0 U
J
en
3
t-n
o<s
> \
o
CT•
m
• •
CZ"
CT
G*
mo
w o
o3: 0
3>
LO C
o-
m •
s 3
(n •
• ••
oo
o
-s-
LTI
^J
LH/
. -J
>-*
Ln
^ -
fcin
»-*
—
•vw
<sm
i —
• o
^s >— 3
>
??
M W
cn e
nC
O 0
0
SC
D
^^
2§o
DUAL MASS SPECTRUM09/18/84 14:01:00 + 26:59SAMPLE: 77113-12CONDS.:ENHANCED <S 15B 2N 8T)
DATA: EPABN1368 #1704CALI; EPABN1368 #1
BASE 11/Ei 149/ 149RIC; 592./ 1327.
DUAL MASS SPECTRUM09/18/84 14:61:09 + 29:44SAMPLE: 77113-12CONDS.:ENHANCED (S 15B 2N 0T)
DATA; EPABN1368 #1878 BASE M/E: 67/ 67CALI: EPABH13G8 «1 RIC: 150527./ 221439.
r 63872.
289 256*—l—i
DUAL MASS SPECTRUM09/18/84 14:01:60 + 31:28SAMPLE; 77113-12
• CONDS.sENHANCED <S 15B 2N 6T)
DATA: EPABN1368 #1987 BASE 11/E: 149/ £7CALI; EPABN1368 #1 RIC: 467./ 7743.
~I——r
00 1
DUAL MASS SPECTRUM09/-18/-84 14:31:00 + 33:21SAMPLE; 77113-12CONDS.;ENHANCED <S 15B 2N OT)
DATA: EPABN1368 »2106 BASE 11/E: 149/- 149CALI: EPABN1368 #1 RIC: 17023./- 25183.
i I i I i
m>-•! < i 1 - 1 i i
250
DATA: EPABN1368 #2217 BASE M/E; 149/ 149CALI: EPABN13G8 ttl RIC; 4719./ 16511.
DUAL MASS SPECTRUM69/18/84 14;01:00 + 35;06SAMPLE; 77113-12CONDS.;ENHANCED (S 15B 2N 0T)
i 1 1 | i
200 250
0 0
i " : ' i. U 0 I
LIBRARY SEARCH , DATA: EPABH1368 ft 709 BASE M-'E: £609/18/84 14:01:00 + 11:14 ! CALI: EPABH1368 ft 1 RIC: 208447.SAMPLE: 77113-12CONDS.:
1233 i r ••
SAMPLE
C1U.H18.0 CYCLOHE^AHOL-1-METHYL-4-(1-MET
N NT1?^' 13 PK 6bRANK 1W 6537m 961-1 •
Cla.H12 4,7-METHAHO-1H-IHOEHE...3H..4..7;7
M m r , rB PK 66RAHK 2IN 3648FIT 957 -
C1".H12_ 1-2,4-METHEHO-1H-CYCLOBUTA[CD3
,'1 NT fs5 1B PK 66RANK 3IN 3664FIT 946' •
r'l/E 40 60 59 100 120 140
1080
SAMPLE
J S . H l U.1 m'•S PK 91WNK 1W 1441"IT 935
:.11.H14.0
.1 ^?94 1?. PK 91W. 2W 1199671T 983
;9.H10.02
• NT1?^3 FK 91W, 3I N £071^IT 88U
t-l/'E
r
3f
r
1 ,
4
LI09SACO
3
BRftRY SEARC/18/S4 14:0•1PLE: 7711;NDS.s
l l l . l , . , , , ,cy
5,
BE
, , . , , ,L,60
'€'• • •
H1:00 + It
-12
CLOPEHTEt
1, , , . , 1
3,7-1:1,2,
NZEHEPROF
, 1
S.-52
E.I
11 ,33P
l4Lw.
S0
0 0
-ETHEt
ROPAHE
ICACIC
1 1 , . . . i . 1IYL-3-METh
TRIVLBEH^
1
J
1 i
106
I h , ,^Y
I ' l , , , , , ,0
OftTA: ECALI: E
120
PABN136S #166PABN1368 »
140
5 BASE M/E: 661 RIC:. 212479.
160 180
0 0
LIBRARY SEARCH09/18/84 14:01:06 + 17;34SAMPLE: 77113-12CONDS.:
DATA: EPABN1368 ft 111 8CALI: EPABN1368 » 1
BASE t1/E! 154RIC; 62143.
1099 i
SAMPLE
C8.H4.03
t-1 HT^JS3 PK 1@4RANK 1IN 5821.-"IT 993
C.P..H6.04
n NT1!^B PK 76RANK 2IN 8447FIT 979
1,2-BEHZEHEDICftRBOCTLICAC10
C9.H8.04
.•1 MT 185E; PK 76RdNK 3IN 10402FIT 930
1 - 2-BEHZEHEDICARBOWLICACID/ NO
M./E 40 69 80 10U 120 140 160
ez.z. @e7. esi es i OI'T ezi sen e's 09 et- 3/u •————————————————^———————^————————————————————————^
• It'8 lidS,8 N1e '>fny;aI£I »d 3931 1M ^
•i -' L
aRni-('lAN3irig-3-OamH3-.3) '3N32H3a U • nH •ei3
——————————^————^————————^———^
St'S lidSZ38 MIz »nyaic i Md a931 1H U J J
OU0I2'?' -"i.'.n3Hd-1 -ciaoiH';i-e '• 3H3ina-s no • T i H • e i o
I———————————————————————^r^—————"^r^————————————[n^——————1
• ;S3 II;SSt'S HIi waISI Md ?3H Itl H
•' -' Sum3HIG-T •• I-OailtHIQ-S '3 '3H30HI-HI t'TH • 1 T::i
1———-———————————————————————.——————————r-hfJl————^——————mrfp———m————[|||"l"l'|l"|"l|-'
31dU9S
•• '• H00I: s'SONOO
zi-snz^ :3-idnys•i3i'si ^la i ft 83£ingyd3 'iiyo 3i:z? + @@!i0=t'i t'8/8T/'6993 :3/'n 3sy'a sz/Tft 83sinayd3 sylw . mms Aayaan
0 0 1 ^ -; 0
L 00
LIBRARY SEARCH39-/18/84 14:01:88 + 29:44SAMPLE: 77113-12CONDS.:
DATA: EPABN1368 «1878CALI: EPABH1368 tt 1
BASE M./E: 67RIC: 211711.
l@i3Ei ^ ,
SAMPLE
C8 .H7 .U .NIHHO -
n MT IS.S3 PK 133 .RAHK 1I N 3839 •m 911 -
BEH2EHEACETON I TR I LE, 4-H'iORU;-:Y-
CU3.HU3.0.M2.SlOyQ i '•
H NT 255B PK 133RANK 2IH 13494FIT S98 •
C8.H7.0.H
;'l NT I'S^6 PK 133RhHK 3IN 3827FIT 886 •
1H-IHDOL-5-OL
r'l/E 56 ln0 15S 258
Z ( ; 1. 0 0 : :
LIBRARY SEARCH DATA: EPABH1368 #2120 E:ASE M/E; 9109/18/84 14:01:00 + 33:34 CALI; EPABH1368 # 1 RIC : 24319.SAMPLE: 77113-12COHDS.:
1008 i
SAMPLE ^
I I ,1 | 1 . llll.l lll.ll ..ll . ., ll|l . |.. . lll| . . . I... . |. . .ll. . 1 | 1 . . , 1 1 III,____________________T-———_____________________| , , ,
U15.H14.H. I PHEHHHTHRIDINIUt1 - 5,b-DIMETHYL-
M NT 335 13 PK 287RAHK 1IH 24387-"IT 867 •
[ _ _ _ _ _ , - . , . • . . • • . . ,' . . . . .11._____,..-. , j. , ..li, . | , 1 1 . , . 1 1 1 ' , ______________________, . , .1
C22.H2^S BEHZEHE, \, \' -[:2-t'1ETH'('L-2-(PHEH
M HT ^i \B PK 129RANK 2IN 23226FIT 857 • i
C15.H13.H 1H-IHDCILE,2-HETHYL-3-PHEHYL-
,1 ^287 1 •B PK 207RANK 3I N 13732F I T 79S •
, , . , . , . , . , . , 1 1 , ,_____| . , . , i . . n| , .nil, . . . , l|il, _____^_,___________, . , . ,
M/E 50 1UU 150 200 250 3m3
0 0
LIBRARY SEARCHeo/-18/'S4 14:91:00 + 36:44SAMPLE: 77113-12COHDS. -.
DATA: EPABH1368 tt232QCALI: EPABH1368 # 1
BASE M/E: 264RIC: 41823.
1608 i
SAMPLE
C15.H24.02.H2 SPARTEIHE/14. ALPHA. -HYDROi/Y-17
M 1.JT 2£43 Pf; 264RAHK 1IH 19233HT 727
C17.H12.0.H2
. m}E; PK 26HRHHK 2IN 18957FIT 719
4 (1 H) -U.U I HftZOL I HOME.. 2-PHEHVL-1
C13.H8.U.SE
;•] HT 26.§B PK 268RANK 3IN 1 8 9 1 1FIT 694 •
I'l/E 10t3 159 200
. - . 1 0 0 , , . . .
LIBRARY SEARCH : I DATA: EPABH1368 S2453 BASE M/E; 6709/18./84 14:01:00 + 38:58 : , • ' , CALI: EPABH1368 # ' 1 RIC: 241663.SAMPLE; 77113-12 :CONDS.:
1069 Y .
SAMPLE ) I ^: I
. . j . ...^ . . . . . .
,i ,...ii. |1, .lil.k l.i,I. i.L.JI.___^______________,C8.H7.U.H BENZENEACETOHITRILE-4-HYDROW- ' !
N 1-JT 133 r :3 PK 133 'RANK 1 :W 3830r I T 901 • ! •
. 1 1 1 ! .u — i i i i , . . . , , 1 1 , , i . , i i i , . , , ,11..,.,____,, i , , . : , , , . , _ _ _ _ , , , , , , , , , , , , , , . , . , , , >Cy.H12.H2 H'('DRH2IHE,';'2-PHEH''f'LETHYL'-
nHT^r ; ' [B PK 105RANK 2IH 4161FIT 834 - :
C3. H 11. H AZ I R I D I NE. 2- (PHEHVLMETH'i'L ;• -1 FIH0 ^ r r
;1 W 133B PK 91RANK 3I N 3839FIT 877 J
I. .1 . . I . II. !.ll,.^.J__________________________^__________________________
M/'E 59 168 150 200 . : 250 300 350
EnvironmentsP. 0 Box 818.
Protection AgerAlexandria. V
' ;
ID No
n. ^
ncy. CLPSampleManagementOffice,f0inia22313 703/557-2490
Organics Analysis D(Page 1)
.^-T^S-h/^ r,.7 7 / ^ - < / z ^ .Ll————.J—————————— Cor
By. y^ • " • Dal
v , Volatile Cornpol
Concentration: ^[.ow} Med<u• — — O."
nato Analyrcri- 0 f 1^ J
Percent Moisture (Decanted): •
)ata Sheet
o Mn-
Rt.n"rt Nn /./ —'
Trad Nn- t? fc
JndsJm (Circle One)
^IW
^1
pH .... ....
Sample Number
/^ /^3
^0^
o/-fcys^^j^?^// '
CASNumber
74-87-3
74-83-9
75-01-4
75-00-3
75-09-2
67-64-1 .
75-1'5:Q::.';,:
75-3.5-4;-.: 7.
^5-34-3: -/
156-60-5
67-66-3
107-06-2
78-93-"3'
71-55-6
56.23.5
108-05-4
75-27-4
Chloromethane
Bromomethane
Vinyl Chloride
Chloroethane
Melhylene Chloride
Acetone .
CSrtidn.Disul'ida"-' .-"" ~
.L l OichloroethBta-^^-;-
1 , 1-Dichlofoethane
Trans-1, 2-Dichloroethene '
Chloroform
1, 2-OichIordelhane
2-8uianone
1 , 1 . 1-Trichloroelhane
Carbon Tetrachloride
Vinyl Acetale
Bromodichloromethane
ug7(C
:!
.^
ff
•'"•'•:
lor 16Yirclft
^ i%.
(7 t )/¥,-1TrY v^^•y•^—-
QJ
t6 4
^^ ^i,rs
/jKg,onef/ '
f^/
V
Jh
^
CASNumber
79-34-5
78-87-5
10061-02-6
79-01-6
124-48-1
79-00-5
.71-43-2
10061 -01 -5
110-75-8
75.25-2
591-78-6
108-10-'
127-18-4
108-88-3
108-90-7
100-41-4
100-42-5
1. 1,2. 2-Telrachloroeihane
1, S-Dichloropropane
Trans-1. 3-Dichloropropene
Trichlofoeihene
Dibromochforomethane
1. I, 2-Thchloroelhane
Benzene •...,..:.:. . - ; , '.
CtS-1. 3-DfcMoropropene "
-2-Chloroethylvinylelher
Bromotorm
2-Hexanone
A.Mel^v!-2-P""t3r:cne
Tetrachloroeihene
Toluene
Chlorobenzene
Ethylbenzene
Stvrene
Total Xylenes
ug/f or w/^(CircleW
^ fu -y •q :• c? •
Q- :-r^—f
^^^^^S^ u^ ;q \^?1u
Kg^rreii
/ .
: OJU Raponiofl Qualifiefi
Addilional 11ao&or looinoiafplatning results •re en
- (l^tnit'on of eacti tlag musl tr •H{3l(C<tJraQftd How<»<' ina
f than of w^l 1rf ihe fetuh <
tffllOCIion lirr
lodicatflt compouruS was Jnalyz«d ftx but not fl«t«CHd
Rapon ih< minimum daiecrion Iwn Kx ihc Mmplawnth
<h< Utco . 10U)t>B»«lon ^^®ce..MfVCortc«nlf»^^o"rF
dilution •ctionc fThit ix noi n«c«tUfilv the iniifm"-»il
d»i»<nion limn .) The (oolnole Tioutd r»»d U-
Compound was •rv*lYtO<J for bul not d«rccd Th«
nufntKf i« ih« m.nimu<ri •na<n«b4a d«teClion lirmi <e'
tha t*mpl<
lridic«ta« •n ««nmatBd v«lu«. Thr 41«Q'rt ufted •iltwr
Kl«nm»»d compoundt wt^f • 1 1 TCSOO"M it •tuxwd
Tins (l<fl •ppl<«t 10 p«siiC<d< DflrarrmiBft »vh»re iht
•dem location has txan condfrrwd by GC/MS Singit
comporwni p<siic»des^l0 ng/ul in the Unal flmraci
Should be confirmed by GC/MS
This Hag <s uted wtten ihe •nalflo it found ni the blank
•i. wall «S a urnol« It indicales pofSible/prooable
blank coniarn<n«iion •nd wfni ih« data u4Cf 10 take
apo'op'n't aciio"
Olher tpecilic t i tos and looinoiei may be Kguirsd 10
prooerly deiine Ihe r«sultt M u**d. they mud be tul'v
d««cnt>«d •nd •uch d«&cnpliori •nuchad (o irw data
tumrnary fcpor't
Environm«nfl Protection Agency. CLP Sampte Management Office.P. 0. Box 818, Alexandria. Virginia 22313 703/S57-2490
Organics Analysis Data Sheet(Page 2)
Sample
^
i Number
5V
Semivolatile Compounds
Concentration: • (U>y/ Medium .(Circle One)
Date Extracted/Prepared:
edium .(Circit
•pared: ^^\&4
^VBVgADate Analyzed:
Conc/Dil Factor:
CASNumber
62-75-9
108-95-2
62-53-3
1 1 1 - 4 4 - 4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
39638-32-9
106-44-5
621-64-7
67-72-1
98-95-3
78.59-1
88-75-5
105-67-9
65-85-0
1 1 1 - 9 1 - 1
120-83-2
120-82-1
91-20-3 •
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
8B-06-2
95-95-4
91 .58 -7
88.74-4
1 3 1 - 1 1 . 3
208-96.8
99.09.2
N-Nitrosodimethylamine
Phenol
Aniline
bis(-2-Chlofoethyl)Elher
2-C+itorophenol i
1 . 3-Dichlorobenzene
1,4-Dichforobenzene
Benzyl Alcohol - -——— '.-'—'.'-
1,.2-Drchlorobenzene !
2-Meihylphenol ;
bis(2-chtoroisopropyl)Elher ,
4-Methylphenol ^
N-Nitroso-Di-n-Prdpylamine
Hexachtoroethane •
Nitrobenzene
Isophorone
2-Nilrophenol
2, 4-Dimethylphenol
Benzoic Acid :
bis(-2-ChloroeihoxY)Methane
2. 4-Dichlorophenol
1 , 2. 4-Trichlorobenzene .
"Naphthalene ' '
4-Chloroaniline i
Hexachlorobuiadiene :
4-Chloro-3-Meihylphenol
2-Meihylnaphthalene -
Hexachlorocyclopflniadiene ;
2. 4. 6-Tnchlorophenol i
2. 4. 5-Tcichlorophenol :
2-ChIoronaphthatene
2-Nilroaniline
Dimethyl Phihalate . !
Acenaphthylene i
3-Nitroaniline
ug/l wftg/(CircieOn
^^0^
^^0
?,<=> 0
^^0^5^0A5\0^^•Sf5^5K^fA.O
te^D t^\o^2>oIS-SO^^0
te>- o^to^5^0-1LRT>^^^^^\Q
i nAts^n^Xn^^^^0^>^IJO
n^c?oassonL^o^^3<io\->^C3-)\
K»?a)
^
\/
CASNumber
83-32-9
51-28-5
100-02-7
1J32-64-9
121-14 .2
606.20.2
84-66-2
7005-72-3
86-73-7
100-01-6
534-52-1
86.30-6
101-55-3
1 1 8 - 7 4 - 1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
92-87-5
129-00-0
85-68-7
91-94.1
56-55-3
1 1 7 - 8 1 - 7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53.70-3
191-24 .2
Acenaphthene
2, 4-Dinitrophenol
4-Niirophenol
Dibenzofuran
2,4-Dinnrotoluene •
2. 6-Dinitrotoluene
Diethylphthalale
4-Chlorophenyl-phenyletrier
Ftuorerie"." :" '^
4-Nitroaniline - - - . - - ;
4, 6-Dinitro-2-Methylphenol
N-Nilrosodiphenylamine ( 1 )
4-Bromophenyl-phenylether
Hexachlorobenzene
Penlachlorophenol
^enanthrene
Anthracene
Oi-n-Butylphlhatale
Fluoranthene
Be mid me
Pyrene
Butylbenzylphthatate
3. 3'-0ichlorobenzidine
Ben2o(a)Anthracene .
bis(2-Ethylhexyl)Phlhalaie
Chrysene
Oi-n-Ociyl Phthalate
Benro(b|Fluoranthene
8enzo(k)F(uoranIhene
Benzo(alPyrene
lndeno(l. 2. 3-cd|Pyrene
Dibenz(a, htAnlhracene
Genzofg. h, i)Perylene
ug/lor^/Kg^(CircleCne
^^0^
ni,« \h .<=?D:SS^o3 ioio
A5^o^^03%>>o -n\os&.\-lL^O35^^^lo
rn.cDS- o^^Sssoi ^o^^•y.^)F5^-'101,0 ,te^^-70^-rlo^
^A^\S5io^5^03G30^5^0^Ao'SS' o^-
Envifonnwiul Protection AQ«IKY. CLPS«(npl«Maruo«fn«nt Office.P. 0. Bo» 818. Ateundni. Virgin- 22313 703/S57-2490
Organics Analysis Data Sheet(Page 4)
Sample Number
f^fl'^
Tentatively Identified Compounds
CASNumtxr
l^
7
3
A.
5.
fi
7
a9
in1 1 -ii
13, .
14
1!;
16
17
m19
20
71 .
71
23
24
2?
7fi
27
7R
29
-in
Compound Nama
LUlOHU^^
^, s , - •-rr i ^-M- p^ - •///^1^.iGUJ>Y'(jl ^
U»"-(<'v\J»vi i :
..,.. -.„.-„——..^-..^-^-..^-.——— ' ^ — ^
: -.' -—-.-. •
^
'
!
Fraction
. uoft-\,/
'ftfl
RT or SonNumbor
.
-^H'W^.
3^^
•
EatirnatadConca nt ro{ia&
(ug/1 oc-tig/kgl/
^05&^0
^-l o
QUANTITATION REPORT FILE: EPABN1369
DATA: EPABN1369. TI09/18/84 15:01:00SAMPLE: 77113-13SUBMITTED BY: ANALYST:
AMOUNT°AREA(HGHT) • REF.AMNT/(REF.AREA(HQHT)» RESP.FACT)RESP. FAC. FROM AVERAGE OF WHOLE . R L
NO NAME1 * D-4 1,4-DICHLOROBENZENE2 •» D-8 NAPHTHALENE3 » D-8 ACENAPTHENE4 » D-10 PHENANTHRENE5 » D-12 CHRYSENE6 » D-12 PERYLENf-7 2-FLUOROPHENOL (SURROGATE)B D-5 PHENOL (SURROGATE) •9 D-5 NITROBENZENE (SURROGATE) .-.
10 2-FLUOROBIPHENYL (SURROGATE) Q11 2i4,6-TRIBROMOPHENOL (SURROGATE)12 D-14 TERPHENYL (SURROGATE.)13 N-NITROSODIMETHYLAMIN?14 2-CHLOROPHENOL :
15 PHENOL16 BIS (2-CHLOROETHYL) ETHFR17 1,3-DICHLOROBENZENE18 I,4-DICHLOROBENZENEI? 1,2-DICHLC)R6BENZENE20 HSL ANILINE21 HSL BENZYL ALCOHOL23 B.IS(2-CHLOBOISOPROPYL)ETHER , .23 ' HEXACHU3ROETHSKEr-^.::::::=::-——" - -- ;; : - . : ; . . ' . ;24 ' N-NITROSODIPROPYLAt+INe " • ' • . . . . - -- .—.^—^^^.''. ^ " • - . ^25 NITROBENZENE26 ISOPHORONE'27 2-NITROPHENOL28 2,4-DIMETHYLPHENOL "29 BIS(2-CHLOROETHOXY)METHANE30 2,4-DICHLOROPHENOL31 1,2,4-TRICHLOROBENZENE32 NAPHTHALENE33 HEXACHI-OROBUTADIENfc34 P-CHLORO-M-CRESOL35 HEXACHLOROCYCLOPENTADIENF36 2,4,6-TRICHLOROPHENOL37 HSL 2 METHYLPHENOL38 HSL 4-METHYLPHENOL .39 HSL BENZOIC A C I D ;40 HSL 4-CHLOROANILINE41 HSL 2-METHYLNAPHTHALENE42 2-CHLORONAPHTHALENE43 DIMETHYL PHTHALATE44 ACENAPHTHYLENE45 2,6-DINITROTOLUENE46 ACENAPHTHENE
I/ 0 0
SCANS 1 TO 1300RIC DATA; EPAWA1719 #1CftLI: EPAUOA1719 ftl03/13^34 3:07:60
SAMPLE; 77113-13CONDS.;RANGE: G 1-1300 LABEL: N 0, 4.0 QUAN: A 9- 1.0 J 8 BASE: I) 20- 3
725
QUANTITATION -.EPORT FILE: EPAVOA1719
DATA: EPAVOA-'l1?. "I08/19/84 3:>i7:eeSAMPLE: 7711:—1;SUBMITTED BY iPf-. ANALYST: RJM
AMOUNT»AREA -.- »£?-. AMNT/(REF. AREA>» RESP.FACT)RESP. FAC. F-tOM AVERAGE OF WHOLE . RL
NAME*«•»
HSLHSL
HSLHSLHSL
HSLHSLHSLHSL
BrtOMOCHLORMETHANE (INTERAL STANDARD)P-DIFLUOROBENZENE (INTERNAL STANDARD)DrCHLOROBENZENE-05 (INTERNAL STANDARD)CHLOROMETHANEB.TOMOMETHANEVINYL CHLORIDECuLOROETHANEM£THVLENE CHLORIDEA!:F<OLEINACRYLONITRILE1 -—D.ICHLOROETHYLENE1 i-DICHLOROETHANET'-fANS-l, 2-DICHLOROETHYLENECHl-OROFORM1 ,;-DICHLOROETHANE1. -. . .1-TRICHLOROETHANEACETONECARBON DISULFIDECWWh TETRACHLORIDEB 'OMOUICHLOROMETHANE1 £-DICHLOROPROPANETRANS-i, 3-DICHLOROPROPYLENETi^ICHLOROETHYLENEBENZENEDIBROMOCHLOROMETHANE1 1.2-TRICHLOROETHANEC1S-J., 3-DICHLOROPROPYLENE2-CHt.OROETHYL VINYL ETHERBF,OriOFORMM^TRYI- ETHYL KETONEVJ.".';'L. ACETATEM?7HV1- ISOBUTYL KETONE1, L--D-I CHLOROETHANE-D4 ( SURROGATE )BLNZENE-D6 (SURROGATE)D-LE'KOMOTETRAFLUOROETHANE (SURROGATE)BJ.;, < PERFLUOROISOPROPYL ) KETONE ( SURROGATE )FLUOROBENZENE (SURROGATE)TCTXACHLOROETHYLENE1 .., S, 2-TETRACHLOROETHANETi.Ll'^NECI--L.OKOBENZENEE1HV!.BENZENE2- :r>'ANONES'Yf<i--M£0 •:'.'(LeNEM ..Vi.i-NE
NO474B4950
N0123456789
1011121314
NAME
M/E130114117NOTNOTNOTNOT
84NOTNOTNOTNOTNOTNOT
M- ;.-<RD ••••-Tu'.. :lP - ;-;h
S C - ,3--,6-1.-B.--.t..
FOUN;:-FOUNC.FOUNnFOU^C
2.;;"FOU-.-;.FOU^"FOU.-iFOU^::FOU"i:'FOU:v.:-
OrlOBENZE.IHYLBE^Nt-DBOi'lOFLUO
IME.-:0723: 312°: 15
''•. 4B
OTRIFNZENt(SURFROBEI'
REF123
1
^LUORID; (SURR
DOGATE)>IZENE <
RRT1. 0001. 0001. 000
0. 747
E (SURROGATE)OGATE)
SURROGATE >
METH AREA BB 24A BB 10&A BB 57
A BB 24
AMOUNT 7.TOT30. 000 UG/L 1. 6730. 000 UG/L 1. 6730. 000 UG/L 1. 67
2B. 336 UG/L 0. 94
NO151617181920212223242526272B2930313233343536.^7:
3Q—39—404142
4445 .46-47484950
M/ENOT
9758
NOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOT
436584
NOTNOTNOT-t66
NOTNOTNOT
NOTNOTNOT•NOTNOT
9895
• SCA1VFOUND
5;-3y'
FOUNDFOUNDFOUND
FOUNDFOUNDPOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
FOU.iDFOUND
7 •:••?-4s-6-c
FOU. .:-FOUNDFOUN^
/
FOUMDFOU.M^FOUM;:.
——T~"—FOUMUFOUNDFOUNDFOUNDFOUND
8-;'10:;::
TIME
'-?: 3616: 23
:-4: 46•^=••57--:-:03
- ?l::37
—S I'. 25 ~-
"'--: 51::::=: 22
REF
1 1.1 0.
2 1.2 0.2 0.
—3——07
-—3——0—
3 0.3 1.
RRT
341792
039669B83
'91 y -
?Q3—
952209
METH
A BBA BB
A BBA BBA BB
-~A-B&——
A BBA BB
AREA(HGHT)
49334.7767.
920137.97680.
191749.
374B. —
" 8 3 2 0 ;
177012.10BB53.
AMOUNT
43. 194 UG/L156. 133 UG/L
2198. 620 UG/L96- 641 UG/L93. 845 UG/L
I'-i'i - ^
24. 256~nG7I~
108. B29 UG/L97. 376 UG/L
•/.TOT
1. 445. 20
73. 023. 223. 13
——&-T4-
3. 633. 25
DUAL MASS SPECTRUM88/'13/'84 3:07; 68 + 9; 48SAMPLE! 77113-13COHDS.!ENHANCED <S 15B 2H 0T>
DATA: EPAUOA1719 #237 BASE M/'E: 49.-- 49CALIi EP'r)UOA17l3 »1 RIC: 21631./ ' 25433.
-i—i—i—|—r
159
ou83SACOEN
-^;
AL M/13/MPLENDS.HflMCE
0
ASS SPECTRUM84 3;07;e9 + 17
77113-13
ED <S 15B 2N 0T>
1 • ] i ]
50
H—————————T]
3£
6i0
•:
' 1 ' I70 8e
-rJ——————|—————1——,———L
DATA; EPAWA1Cfti-I: EPflUOAl
i•
i
• • , ' 1 1 '901 i
i i ] ' 1 |
7171
1
T
9 #515 BflSE M/'E: 97.-'9 #1 RIC; 31£73./'
' 1 ' 100 110 120
-L i i i .. i ,
9735833.
r 9'
DUAL MASS SPECTRUM DATA! EPAWA1719 #384 BASE M.-'E! 43/ 4383/19/34 3;07:00 + 10! 23 CftLIi EPWOA1719 #1 RIC,- 6967. / 18343.SAMPLE: 77113-13CONDS.!ENHANCED <S 15B 2H 0T)
100.0-1 • r 449£.
50.0-
M/E 50 108 158 200——J—————————1—————————^—————————L
^n.n -I
i i
100.9-' ' ' • : : 0 0 1 ' ('! ^ ' 4496-
DUAL MASS SPECTRUM83/19/'S4 3; 67; 00 + 24:46SAMPLE; 77113-13CONDS.;ENHANCED (S 15B 2N 0T)
DATA; EPAUOA1719 »725 BASE M-'E; 43/ 43CfiLIi EFATOA1719 ftl RIC; 410623.-' 430591.
289
OWL MASS SPECTRUM OUTA: EPWOA1719 <t773 BflSE tl/'E; 43/ 4483/19/84 3! 87; 09 + 26; 25 CALIi EPAUOA1719 «1 RIC; 802..-' 12847.SAMPLE; 77113-13CONDS.;ENHANCED <S 15B 2N 8T.''
100.0-] r- 2868.
50.0- '
M-/E 56 100 ' 150 280i 1 I - 1 l I i 1 i 1 ^ 1 . 1 i I i I i l i I i 1 i I i—1—1—I i I i I i
c.n a -i
i i
I I : ;
100.0-1 ; : 0 0 1 ' " 0 7 286e-
cs
,n0
3
(s
a
3
(Jl
••s
(0m
0
0
z L
II r~
Eo
•
m •-
> 3
m —
•"
co
x>0
A
LT]
-\J
LO
-~.
'JLT
] >—
(0
L>"
l»-
- —
"D
»--
o c
o rn
Ul
I --
1 0
ro
^ —
—
iCL
> CO
;0
r-i
o c
:
m m
•o •
nJ>
3-
•I:
•C:
0 0
X>
I>
tt <
t^
^J
-J LD
OT
l— 0
00
3>
— L
n m
co m
^ ••> e
n o-i •-,
-l——
i——
l——
i——
i——
i r,)
' '
— -
o.(0
-0.
DUAL MASS SPECTRUM DATA! EPAUOA1719 #782 BASE fl/'E: S3/' 440S/19/'S4 3!07:00 + 26;43 CftLl! EPftUOfll719 #1 RIC! 7873./ 19887.SAMPLE: 77113-13CONDS.:ENHANCED (S 15B 2N 0T>
180.0-1 r 3140.
50.0-
' i , ln, i i l i i i ,.i,., Jj.i,iiiii i , , , , , 1 , 1 , , , i , , 1 , 1 , , , , , , i , 'M/E 50 100 150 230
I I llll'illllll ' |li|'|%' Il||1' ' ' 1 ' ' | ' | i ' ' ' ' ' ' I ' l l ' ' ' " ' ' ' | 1
.n n J (-
.100.0- . . . . | i i 0 0 1 ^ ; 0 9 3l4e-
' ! i
. 0 i- ?;• 1 0 0
LIBRARY SEARCH DATA: EPAUOA1719 tt 763 BASE M/E; 5508/19/64 3;07;00 + 26:04 CALI: EPAWA1719 ft 1 RICi 20895.SAMPLE; 77113-13CONDS.:ENHANCED <S 15B 21-1 0T)
1902 i
SAMPLE
1 , 1 , 1 , . . . . i j i i , , . ii,_____L___LC8.H16_ 2-PEHTENE,2,3,4-TRIHETHYL-
11 W^i ]B PK 55RANK 1IN 1813F I T 982
;8. H 16 2-PEHTENE ,3,4,4-TR I riETHYL-
n m1B Pr<; 55WW. 2IN 1S21FIT 973
C8. H16 2-F'ENTEHE, 2 ,4 ,4-TRIMETHYL-
n m} iB PK 55RANK 3IN 1815FIT 978 •
M-'E 4n 50 60 70 80 90 lUU 110
. I I- b I- 0 0
LIBRARY SEARCH DATA: EPAUOA1719 ft 8&4 BASE M./E: 5708/19/84 3: £17:08 + 27:28 CALI: EPAUOA1719 « 1 RIC: 33215.SAMPLE; 77113-13CONDS.;ENHANCED (S 15B 2N 0T>
1088 1 r
SAMPLE
C8.H18 ' PENTANE,2,2,4-TRIMETHYL-
M W^ } \B PK 57RANK 1IN 2074FIT 987 •
1 i , I , I_______J____________________________^J;8.H18 _ - BJTANE,2,2,3,3-TETRAMETHYL-
M HT1?^ 1E; PK 57RANK 2I N 2687FIT 984 •
C8.H18 HErtAHE,2/2-OIMETHYL-10F;B 1 r
M NT H4B PK 57RW, 3IN 2084FIT 383 •
fl/E 4£t 58 be 7y 80 90 100
\ [
. ?; ;. i:. I. 0 0
LIBRARY SEARCH08/19/84 3:67:65 + 28:4£SAMPLE: 77113-13COHDS.:ENHANCED (S 15B 2H 0T>
DATA; EFAWA1719 tt 842CALI: EPWOA1719 # 1
BASE 1'1/E: 56RIC: 39231.
58 ee 78 8L1 98 1UO 119 126
1 . 0 0
SCANS 1 TO 2880DATA; EPABN1369 #1CALI; EPABN1369 #1/•1S/84 15:01:00 j
MPLE: 77113-13 ' ' 1 0NDS.: 'NGEi G 1,2808 LABEL: N 2, 2.0 QUAN: A 2, 3.0 J 0 BASE: U 20,
(S
5007:55
1800
15!50150023; 451
2000
31:40256839:35
NO NAi^ . . . . . . . . .47 2.4-DINITROPHENOL48 4-NITROPHENOL49 2,4-DINITROTOLUENE .50 FLUORENE51 4-CHLOROPHENYL PHENYL ETHER52 DIE1HYL PHTHALATE53 4,6-DINITRO-2-METHYLPHENOL54 N-NITROSODIPHENYLAMIN&55 1,2-DIPHENYLHYDRAZINE56 4-BROMOPHENYL PHENYL ETHER57 HEXACHLOROBENZENE58 PENTACHLOROPHENOL5'? PHENANTHRENE60 ANTHRACENE61 DI-M-BUTYL PHTHALATE62 FLUORANTHENE63 HSL 2.4,5-TRICHLOROPHENOL64 HSL 2 -NITROANILINE65 HSL 3-NITROANILINE66 HSL DIBENZOFURAN67 HSL 4-NITROANILINE68 BENZIDINE69 PYRENF70 BENZYL BUTYL PHTHALAT&71 BENZO(A>ANTHRACENE72 3,3 ' -DICHLOROBENZIDINF73 CHRYSENE74 BIS<2-ETHYLHEXYL> PHTHALATE75 DI-N-OCTYL PHTHALATE76 BENZO(B)FLUORANTHENE.77..,- .. BENZO<K.)FLUORANTHENE .. _ L :--;^—^-.--^- .^-.-::^-;."78'- B E N Z O < A ) P Y R E N E . : . . .. ..- . _ . . .-:7•? I N D E N O C I - 2 . 3-CDlPYRENe . . - - . - .80 DIBENZO<A,H1ANTHRACENF81 BENZCKGHDPERYLENE
NO M/E SCAN TIME REF RRT MFTH AREA(HGHT) AMOUNT 7.TOT
NO M/E SCAN TIME REF RRT METH AREA(HOHT) AMOUNT XTOT1 152 700 11 03 1 1 000 A BB 23464. 40.000 UG/ML 16.432 136 942 14 5S 2 1.000 A BB 59358. 40.000 UG/ML 16.433 164 12BO 20 16 3 1.000 A BB 37147. 40.000 UG/ML 16.434 1B8 1559 24 41 4 1.000 A BB 64255. 40.000 UG/ML 16.435 240 2065 32 42 5 1.000 A BB 24S12. 40.000 UG/ML 16.436 264 2320 36 44 6 1.000 A BB 38429. 40.000 UO/ML 16.437 NOT FOUND8 NOT FOUND9 NOT FOUND
10 NOT POUND11 NOT FOUND12 NOT FOUND ^_____ —————V3———74——Sga———3-31———1-—6-34-7——A-B&-———————S^3r.—————e-43T~UG7ML0. 1814 NOT FOUND '^15 .MOT FOUND16 NOT FOUND ,17 NOT FOUND _18 NOT FOUND _19 NOT FOUND °20 NOT FOUND 021 NOT FOUND23 NOT FOUND23 NOT FOUND24 NOT FOUND25 NOT FOUND26 NOT FOUND27 NOT FOUND28 NOT FOUND29 NOT FOUND30 NOT FOUND31 NOT FOUND
.32 NOT FOUND_.33;.. NOT FOUND
34 NOT FOUND35 NOT FOUND36 NOT FOUND37 NOT FOUND38 NOT FOUND39 NOT FOUND40 NOT FOUND41 NOT FOUND42 NOT FOUND43 NOT FOUND44 NOT FOUND45 NOT FOUND46 NOT FOUND47. NOT FOUND48 NOT FOUND49 NOT FOUND50 NOT FOUND51 NOT FOUND52 NOT FOUND53 NOT FOUND54 NOT FOUND55 NOT FOUND56 NOT FOUND [.
\
NO5758M—606162-636465666768
707173737475767778798081
M/E'NOTNOT
NOTNOT«^u«^NOTNOTNOTNOTNOTNOT
NOTNOTNOTNOT149NOTNOTNOTNOTNOTNOTNOT
SCANFOUNDFOUND
FOUNDFOUND
—1793FOUNDFOUNDFOUNDFOUNDFOUNDFOUND
FOUNDFOUNDFOUNDFOUND2106
FOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
TIME
SB: Sg -
33:21
RE^
—V~
5
RRT
TTTiPT-
1. 020
METH
A UU——
A BB
AREA(i!-3HT)
6ifi>3.
1586.
AMOUNT
0.583 UG/ML
2.484 UG/ML
7.TOT
~0~34
1. 02
DUAL MASS SPECTRUM DATA; EPABH1369 'H222 BASE M/E: 45/ 4509/18/84 15:01:06 + 3:31 CALI; EPABH1369 »1 RIC; 2183./ 4599.SAMPLE! 77113-13CONDS.:ENHANCED (S 15B 2H 0T)
108.0-1 r 1632.
58.0-
M/E 56 100 150 283 250
||j|l ' i"i l j| ' j]" l" l""" l"""" l l""" l" l"""ll
50.0-
100.0-' L 1632.: ; 0 0 1 .? 1 7
DUAL MASS SPECTRUM09/18/'84 15!61:08 + 24:44SAMPLE; 77113-13COHDS.;ENHANCED <S 158 2N 6T)
DATA: EPABN1369 it 1562 BASE M/-E: 178/ 188CALI: EPABN1363 Itl RIC: 243. / 5815.
0 0 1 :' -1 8
DUAL MASS SPECTRUM09/18-'84 15:01:60 + 28:22SAMPLE; 77113-13CONDS.;ENHANCED <S 15B 2N 6T)
DATA: EPABN1369 #1792 BASE M/E: 202/ 202CALI: EPABN13G9 111 RIC; 277./ 767.
100 150J_L.
0 0 1 ° 1 ^
DUAL MASS SPECTRUM09./18/84 15:61:00 + 29:91SAMPLE: 77113-13CONOS.:ENHANCED <S 15B 2N 8T>
DATft! EPft3Hl369 #1833 BASE M/'E: 202/' 282CftLI: EPABN1369 iti RIC; 157./• 521.
_l__L158
i .1 i
0 0 1
DUAL MASS SPECTRUM09/18/84 15;61;00 + 33;21SAMPLE: 77113-13CONDS.:ENHANCED <S 15B 2N 0T>
DATA: EPABH1369 #2106CALI; EPABN1369 #1
BASE M/E: 149/ 149RIC: 2283./ 2931.
0 0
LIBRARY SEARCH09/-18/-84 15:01:00 + 37:52SAMPLE; 77113-13CONDS.!ENHANCED (S 15B 2N 0T>
DATA: EPABN1369 S2392CALI: EPABN13G9 f t ' 1
BASE r'l./E; 269RIC: 7111.
1421-1
SAMPLE
C12.H10 .U.N2
H HT1!^;B PK 198RANK 1IH 12569F I T 655
9H-PYRI DO[3.. 4-B 31NDOL-7-OL.1-11
::14.H21.C
11 NT^^B PK 2i39RANK 2IN 15552FIT G45
C7.H5.U.C,.1 mB PK 195RhNK 3It-1 14124FIT 635
t'l/E
L3
59
i
,11 , l l
BENZ&
. 11
BENZEt
"1
C, D I -TERT-BUTYLCHLCiRO-
C, 1,3,5-TRICHLuRO-2-riETH
1 i l l
10U 15t3
iL-.
: • :
4-
'.
J-i,—200
1
iL-
1
! . , , . [
250, 306
Environfnent&l ProlAclkP.O.Box8!3, Atoun
Lab Sample ID No:
on Agency.Kjria. Virgini
'.{•^^7^
CLP Sample Manage men* Office.223)3 703/557-2490
Organics Ana)(Pa
-T^s-hmn^ -/i^
i f - , - • .
. . Volatile C
Concentration: /Cow)
. . . . . . . . . : . .Q.I
Percent Moisture (Decan
ysisGgel)
Cas
QC
Cor
Oat
ompol
MediL<^S
^
^
tea):;
)ata Sheer- - -"
a Nn-
RapnrtNn . . iJ .S>
itrar-tNn- W
Linds ;
Jm (Circle One)
/Q/9^^1
pH
0a
-
Sample Number
/^^
^9
1- fc7SO^^........
0;'
•0
p
CASNumber
74-87-374-B3-975-01 -475-00-375-09-2-67-64-175-15-Q7.5,35-4-..75-34-3156-60-567-66-3107-06-278-33-371.55-656-23-5108-05-475-27-4
ChloromethaneBromomeihaneVinyl Chloride 1
ChloroethanaMethylena Chloride :Acetone-CarbonDisuUide--•- - • - • - • <1 , I-Dichforoethene1. 1-Dichloroethane •Trans-1. 2-Dichloroelhene " -Chloroform ;1.2-Dichloroethane :
2-6ulanone1 , 1 . 1-TrichlocoethaneCarbon TetrachlorideVinyl AcetateBromodichloromethane
ug/lotw/(Circle-01
^^• ^4' W
SLU't,
•^
ft^...-1.-3. b
:.l
; !•&.
^^
- 19-,
^^S^^-Sl
lAu^1^
Kg.
u,
A;
/
=
CASNumber
79-34.578-87-510061-02-6:79-01 -61124.48.1r79-00-5 -31-43-210061-01-5-110-75-8.75-25-2591-78-6 .,.108-10-1127-18-4
108-88-3108-90-7100-41-4
100-42-5
1.1.2. 2-TeirachloroeIhane1. 2-DichloropropaneTrans-1, 3-DichloropropeneTrichloroetheneDibromochtoromethanelTl^-2-TrichlQroeihaneBeriene- - - . . - • -.--•-
cis-1. 3-Oichloropropene—2-ChloroeihYlvinylelher 'Bromoform
2-Henanone4-MB!hy|-3-Pontano.,^
TetrachloroeiheneTolueneChlorobenieneElhytbenzeneSlyreneTotal Xylenes -
ug/1 orufl^(CircleTO
3-
^
1^•»aIS
.- l^• ••-.•(p4
" fa i,^
ft^'6^^-
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rt
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D«t» Rtportinc Qualifiers
Fof raporiiofl resulti to EPA. V^e (o<low<r>o rasvlis quxliliers afe uted
Addilional (lags or fooinoiftiflKOCining recullfTe encouragad However, (he
Oflltnmon of each flag rtiust fae axolic't
H ir»« rexull r J v«lu« gra«(«r Trvan or •qua! to Tr%«
do(»Ct<on lirrnl. rooort Ihfl vlue, ;
(ndicaiec compound was «nalvi«d for bui not o«t«ct«d
flvpOfl tha minimum d«l»C1ton limit for lh» Mmpte inlh
th« u <« g.. 10U) bJfcod on nflce«&arv conceniranon/
dilution •ctions. |Thi» IB nol n»ca«—rilvthe iritKunwn
d«l6ctt0i limit .) The (ootnole fhould raad U-
Cornpgurtd w«t «riJilyi«d lor but not dflt«ci«d Tt-K
number r thfl minimum •riBirroi» o«tecnon I'mn <ot
me sample
Ttiis flag .ipolxs 10 pcsitCide (Mramalert wtietB ihe
td«nr1ication hai b«n confirfn^d bv GC/MS Siniil<
lnd)c«l«« •
whamlir
i ••(imafd vlufl Th»t fl«g j| u««d •KrMf
>Bling « co<*c»ntranon <0t lflnt«tiv«ly
Should be confirmed by GC/MS
This (lag <& uwd wtxin th< enalvie is found in me blank
•& wflll as • lamptc. t1 <r»d«CB;»» poisiblc/pfobable
bl<oh coriiaminaiio" •r>d warnt iho dan ut«! 10 latie
•ppropnalC •Cl-O"
Olher soecitic 11«g» •"d fooinoiai •"*V b< f<iuir»d 10
pfQp«f(Y dfldnc ttt r<tul1t M Li»*d, t^flY mull tx lul ly
d«scnb«d •nd tucfi detcuption «n«ch«d to tr»fl dar
Environmental ProfctionAgancv, CLP Stmpit Managanwnt Oftic*.P. 0 Box 81 a. Al«un4ri«. Virginr 22313 703/557-2490
Sample Number
^^c5°|Organics Analysis Data Sheet
(Page 2)
Semivolatile Compounds
Concentration: (Gw^ MedJUJn (Circle One)
Date Extracted/Prepared: __,_&t^2
Dale Analyzed: ^^^V^M
Cone/Oil Factor: "S^—^i.^A.'^O^ O^X
CASNumber
62-75-9
108-95-2
62-53-3
111-44-4
95-57-8
541-73-1
106-46-7
100-51.6-
95-50-1
95-48-7
39638-32-9
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
1 1 1 - 9 1 - 1
120-83-2
120-82.1
91-20-3
106-47-8
87.68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
1 3 1 - 1 1 - 3
208-96.8
N-Nncosodtmethylamine
Phenol
Aniline
bis(-2.Chloroethyi)Ether
2-Chlorophenol '•
1, 3-Dichlorobenrene
1, 4-Dichlorobenzene
Benzyl Alcohol '""' •-'•""""
1 , 2-Drchlofobenzene
2-Methylphenol
bis(2-ch)oroisopropyllEther
4-Meihylphenol
N-Nitroso-Di-n-Propylaminie"
Hexachloroethane ~ •'
Nitrobenzene
Isophorone
2-Nitrophenol
2, 4-Ormelhyfphenol
Benzoic Acid
bis(-2-Chloroethoxy)Melhane
2. 4-Dichlorophenol
1. 2. 4-Trichlor-obenzene
Naphthalene •
4-Chloroanitine i
Hexachlorobuladiene
4-Chloro-3-Meihyiphenol '.
2-Meihyfnaphihalene
Hexachlorocyclopentadiene;
2. 4, 6-Trichlorophenol '.
2. 4, 5-Tfichlorophenol :
2-Ch)oronaphlhalene
2-Nitroaniline
Dimethyl Phlhalale
Acenaphthyfene
ug
J
4••«.ti.L
»,<,
V.\,
\.viLL1L^
^L
LT
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L
t.
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-11^-IITO
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1TO-|0^-1TOiro•1TO
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^
^
; CASNumb«r
83-32-9
51-28-5
100-02-7
32-64-9
121 -14 -2
606-20-2
84-66-2
7005-72-3
86-73-7
100-01-6
534-52-1
86-30-6
101-55-3
'18-74-1
87-86-5
85-01-8
120-12-7
84-74-2
206-44-0
92.87-5
129-00-0
85-68-7
91-94-1
56-55-3
1 1 7 - 8 1 - 7
218-01-9
117-84-0
205-99-2
207-08-9
50.32-8
193-39-5
53-70-3
191-24-2
Acenaphthene
2.4-Dinitrophen6l
4-Nnrophenol
Dibeniofuran
2. 4-Dinitrotoluene
2, 6-Dinitrotoluene
Oiethvlphthalate
4-Chloropnenyl-phenYle(her
^luorane.
4-Nitroaniline :
4. 6-Dinitro-Z-Methylphenol
N-Nnrosodiphenvlamine ( 1 )
4-BromophenYl-phenylether
Hexach lorobenzene
Pentachlorophenol
Phenanlhrene
Anthracene
Di-n-ButYlpMhalare'
Fluoranthene
Benzidine
Pyrene
Butyl be nrylphihalate
3. 3'-Dichlocoben2idine
Ben2o{a lAnthracene
bis(2-E>hylhexYl)Phthalale
Chrysene
Di-n-Octyl Phthalate
Ben20(b)Fluofanlhene
Ben20<k)Fluoranthene
8enzo(atPyfene
(ndenoO, 2. 3-cd|Pyrene
Dibenria, h)Anihracene
Benro<g. h, i)Perylene
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Organics Analysis Data Sheet(Page 4)
Sample Number
T'^?q
Tentatively Identified Compounds
CASNumbar
l
?
1
-1
K
K
7
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in
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if
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17
1R
19
70
?1.
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71
?a
2S
26
77
2R
29
.-in
Compound Nona
(Lv^^sc^n^- '•LA^A'k>v\S>\J^t^-—
V^v4 iAJ»^ -i
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.
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1/1 0
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. IN
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3UANTITATION -REPORT FILE: EPAVOA1720
3ATA: EPAVOA172C'. -I3B/19/B4 4:••.)?: 0C-SAMPLE: 7 7 1 1 — - TSUBMITTED BY -?i- ANALYST: RJ1.)
AMOUNT=AREA (-iGH'? : « REF. AMNT/(REF. AREA(HGHT)» RESP. FACT)^EBP. FAC. F--'OM AVERAGE OF WHOLE . RL
NAME«««
HSLHSL
HSLHSLHSL
HSLHSLHSLHSL
Bn-OMOCHLORMETHANE (INTERAL. STANDARD)'P-OIFL'JOROBENZENE (INTERNAL STANDARD)D;CHLOR;OBENZENE-D5 (INTERNAL STANDARD)CHLOROfiETHANEB-^OMOMETHANEVINYL CHLORIDECHL ORO^THANEMeTHYi.-ENE CHLORIDEA':;?(OLE=NACKVLONITRILE1 --OICHLOROETHYLENE1 i-OTCHLOROETHANETi;'AN&-_. a-DICHLOROETHYLENEC-LOROrORM1 —DICHLOROETHANE1 .. --"'RICHLOROETHANEA::S:TONE:CARBON'DISULFIDECARBON TETRACHLORIDEB-tOMOD ICHLOROMETHANE1 r-a^CHLOROPROPANETSAMS-4- 3-DICHLOROPROPYLENETSICH'-^ROETHYLENEB^NZEN^D JTBROMOC HLOROMETHANE1 L. ^-"RICHLOROETHANEC:=-_.;-DICHLOROPROPYLENE2-C:-iLOF:OETHYL VINYL ETHERBSOMOF'^RMM£THYL. ETHYL KETONEV:NYL ACETATEM'ET-iyL ISOBUTYL KETONE1 r-^'ICHLOROETHANE-DA (SURROGATE)B€N2ENE:-D6 (SURROGATE)D ZBROMCTETRAFLUOROETHANE (SURROGATE)BIS i PEF:FLUOROISOPROPYL) KETONE ( SURROGATE)F-UOROEENZENE (SURROGATE)T-£";RACHLOROETHYLENE1 _, 1. 1-TETRACHLOROETHANET::-LL»ENEC-LOR05ENZENEE'^YLBENZENE2—EXANONES'YRENS:0-yYLElvEM-yVLS'YE
NO47484950
N01234 -
67B9
10111213141516171B
NAM1
M/E130114117
NOTNOT84
NOTNOTNOTNOTNOTNOTNOT
9759
NOT
M-SRD-5TOi-UP-SR
SC-w33;fc-^ar"
FOU. CFOUNC
2S-FOUNCFOU-'JCFOU-MCFOUM!:FOUMCFOUNDFOUNC
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DTRINZEN(SURROBE
REF.123
1
11
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0.
1.0.
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340790
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AREA(HGK135492.
1&23B7.83833.
45154.
167183.9474.
r) AMOUNT50. 000 UG/L50. 000 UC/L50.000 UG/LI. aa? \\^/\
J 1 1 7^ L' 1^4—
35. B00 UG/L
100. 76& UG/L131.106 UG/L
•/.TOT1. 521. 521. 52
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NO19202122232425262728293031323334353637
39404142
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NOTNOTNOTNOTNOT9895
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0. 66S
1. 0370. 6700. 883
0. 958
0. 9511. 208
METH
—fit-SB——
A BB
A BBA BBA BB
A BB
A BBA BB
AREA(HGHT)
——Brew:—-
10984.
1459700.13904S.285592.
23334.
278347.157623.
AMOUNT
—1 S6. 7S6'—ULi/l-
121.S7S UG/L
2269. 420 UG/L89. 835 UG/L91. 276 UG/L
[S. 602 UG/L
8.195 UG/L
117. 231 UG/L96.594 UG/L
7.TOT
57827
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3. 71
69. 1B2. 74 c\i
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3. 572. 94
DUAL MASS SPECTRUM DATA: EPAUOA1720 #83 BASE M/-E! 50/ 4408/19/84 4:83!e8 + 2:50 CALl! EPAWA1728 ftl RIC; 737. / 4047.SAMPLE; 77113-14CONDS.;ENHANCED (S 15B 2N 0T)
100.6-1 r 2536.
58.0-
\—,—,—,———,—,——————,————l—,—i———————————UM/E 35 49 45 50
SO,Q- , , . . . . . . . . . . . . . . 1 . . : . . . . . . . . . . . . .
100.0J ''• Q 0 1 .' ;' 0 l- 2536.
DUAL MASS SPECTRUM DATA; EPAUOA1728 #143 BASE H/Ei 45/ 4499/19/W 4S08S08 + 4:53 CftLI; EPAUOfll726 ftl RIC: 4647.•/ 9919.SAMPLE:!77113-14CONDS.:ENHANCED (S 15B 2N 0T)
109.0-1 (- 3048.
50.0-
————l—————F^-.——[J———^—————,—————^—————i—————^—————,————L^J————,—————^——I I i I I
M/E 40 50 60 70 80 90
"w»,a-l
100.0-1 0 0 1 ; ? 'I 3048-
DUAL MASS SPECTRUM08/19-'84 4; 08; 00 + 9 ; 48SAMPLE; 77113-14CONOS.:ENHANCED <S 15B 2N 0T>
DATA; EPAUOA1729 #287CALI; EPAUOA1729 «1
BASE fl/E; 49/ 49RIC; 38271,/ 44479.
40 60 70 80
0 0 1
: . \ : \ li
DUAL MASS SPECTRUM ! ; DATA:- EPAUOA1720 #725 BASE M/E: 43/ 43; 98/19^84 4!@8;80 + 24:46 : CALIs EPAUOA1720 #1 RICi 686079./ 736559.
SAMPLE: 77113-14 ; ;
CONDS.;' ' •ENHANCED <S 15B 2N 0T) ' i ;
180.0-1 : ; ! r 232966.
59.8- : ; ; !:
M/E 50 108 |; 150 208
TO Q-i S . I . . . . . i. : . . ' .'.. . . . . .
•• ; i • •
100.0-' ; ; 0 0 1 ^ 33 L 232960.
DUAL MASS SPECTRUM DATA; EPAUOA1728 #516 BASE M/E: 97/ 97QQ/l9''Q4 4;0.°;8a + 17!.38 CALl! EPAUOA1720 #1 RIC; 1818S7,/ 18S799,
, ., SAMPLEl,77U3-.14 „. , „ . . . . , , . , . . . . , ; . , , . , .CONDS.;' • : i • • .ENHANCED <S'15B 2H 9T)
100.e-| [- 31680.
50.0-
l 1 " . • • '••|——---N-1———————r^————M^—.—————Ll^.11/E 40 50 68 70 80^ 90 100 110 120
— — — j p , l . . , , | i . , ' — — — ' i l n r - — — — — — — — ' • 1: i ; : . 1 ——————t- iMi i , '———————^Lr
^ft^n-1
100.8-' | • 0 0 1 ' 3 'A 31680.
DUAL MASS SPECTRUM08/19/34 4!08;09 + 10:23SAMPLE: 77113-14CONDS.;ENHANCED <S 15B 2N 0T)
DATA: EPAUOA1720 #304 BASE M/E; 43/ 43CALI; EPAUOA1720 #1 RIC; G553.-' 11583.
100
l i
DUAL MASS SPECTRUM3S/-19/S4 4; 68; 38 + 21; 13SAMPLE: 77113-14CONDS.:ENHANCED <S 15B 2N 0T)
DATA: EPAUOA1720 #621CALI; EPAWA1720 #1
BASE ri/'E; 78.'' 78RIC: 30847./ 5S623.
40 60 70
0 0 •!
DATA: EPAUOA1720 #467 BASE M/'E: 65/ 65CALl! EPAUDA1728 #1 RIC; 62911./ 69887,
r 21760.
DUAL MASS SPECTRUM08-/19''S4 4:98; 08 + 15; 57SAMPLE; 77113-14CONDS.;ENHANCED <S 15B 2H 0T>
-i————i————i————|————r
70 ; 86 9068 193
l- 21760.
c-n
CDC
O
CD
en
CD
DUAL mSS SPECTRUM : DATA; EPAUOA1720 #821 BASE M/'E; 91/ 9188/'19^84 4;08;e9 + 2S;63 CALIs EPAUOA1720 #1 RICi 3QQ7,/ 32543.SAMPLE: 77113-14 :CONDS.iENHANCED (S 15B 2N 0T) :
100.8-1 r 4604.
50.0- : -
—r^i—i j1 i I11!—l—i—I—1 'I" i—[—1—1—i—|—r—i—i—|—i—)—i—\—i—|—i—|—i—r~i—1—"^
n/E 50 190 150 200' i i l i i i i i 1 ^ | l l l | ^ l l l ' ' l l l l ^ l l l ' l l | l ' ' ' " i i ' r i i i ' ' 1 1 ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ic;n,0 -' ! . . . . -
100.0- ! 0 0 1 3 ' 4084-
DUAL MASS SPECTRUM , DATA; EPAUOA1720 #768 BASE M/E: 44/ 4408-/19/'84 4iB8!00 + 26! 14 : !. ' CALIs EPWOA1729 #1 RIC; 1425. / 17599.SAMPLE: 77113-14 ; .CONDS.; !
ENHANCED <S 15B 2N 0T) . !
100.0-]1 ; I . r 3166.
50.8-
II/'E 59 160 : 150 200
. ' )hn|| l|Him1 l|il||'ii|' ^ ' i i ' j l • i \ < 1 • 1 • ' ' 1 ' ' ' ' ' l ' ' • 1 ' 1 1
w^a -1 - . . . . . .. • . ; • • • • •
i :
100.0-1 ; ' 0 0 1 ' 4 0 L- 3160.
. i. I7 ( • i- 0 0
LIBRARY SEARCH DATA; EPAUOA1720 ft 763 BASE tl/E: 5508/-19/84 4:68:60 + 26:84 CALI; EPAUOA1720 # 1 RIC: 36931.SAMPLE; 77113-14CONDS.:ENHANCED <S 15B 2N 9T)
1005 i
SAMPLE
• I i l l I . .———————I. I I I . . ,————,,J |————————^———————————————L———————————^LC8.H16 • 2-PENTENE/2,4-4-TRIHETHYL-
ri NT 1 1 2 }B PK 55RANK 1IN 1815FIT 997 • :
n',i, 1 . , . . . , , i i . i , , . ,,,.i__________L^___JLJ38.H16 2-PENTENE-2-3-4-TRiriETHYL-
1R85 i rt1 W 1 1 2B PK 55RANK 2 . . . • •IN 1819FIT 9S6 • • : .
____________________________________C8.H16 2-PEHTENE/3<4,4-TRir€THYL- :
1005 i i • ; rt1 MT 1 1 2B P K : 97 . . . . . . .. ! . . . . . . . . . . • • • • •R A N K : 3 i ! i ;
F^jji- h ' ! : ? 1
-Lu——^uJ———1^——^————J-^——J^M/'E 40 \ 50 60 :70 ; : 80 90 1@0 110
• 6 ' : I. 0 0
LIBRARY SEARCH ' DATA; EPAIX)A1720 « 8@5 BASE N.-'E: 5708^19/'84 4:08:00 + 27:30 CALI; EPAWA1720 # I RIC; 58175.SAMPLE; 77113-14CONDS.;ENHANCED <S 15B 2N 0T> ;
1688 i ' ; :
SAMPLE ,
i 1111,1,,————J-L—————————————————^C8.H18 BUTANE, 2,2/3- 3-TETRAMETWL-
M WT1?^ 1B PK' 57 • :RANK 1 .IN 2087FIT 989 • : •
1 i , I ' . i———————M-^————————————————————————^;8.H18 PENTANE-2-2,4-TRINETHYL-
N MT1?^ "]B PK 57RAHK 2 . . ^ .IN 2674 : • . ;FIT ;983 • ; : :
I '
C8.H18 ; HEXAHE/2,2-DIMETHYL- : :
M^4] ! I : : [B PK: 57 . . , . . . . . . . . . . . . . ..! . . .-..-... . . . . . . . .RANK 3 ! , ! :IN 2084 ! . :
FIT 987 • ; . •
M/E 49 50 60 79 80 96 100
!- 0 0
SCANS 1 TO 2808RIC DATA: EPABM1370 #1CALI; EPABN1370 #169/18/84 15;51;08
SAMPLE; 77113-14 ABN 1/-10CONDS.:RANGE; G 1/2&00 LABEL; N 1, 2.0 QUAN; A 2^ 3.0 J 0: BASE: U 20- 3
lA
M^
500,7:55
\'
!
\
J100015:50
>
;
^J^; 1500
23:4
1
^
1
J^
1<
A
^"^w^
200031:46
^ • 1
„
UJ
3
^ .
^^^^,——i——(——i——i——i
250039:35
OUANTITATION REPORT FILE: EPABN1370
DATA: EPABN1370. TI09/18/84 13:51:00SAMPLE: 77113-14 ABNSUBMITTED By:
1/10ANALYST:
AMOUNT-AREA(HOHT) «REF. AMNT/(REI-. AREA(HGHT)* RESP. FACT)RESP. FAC. FROM AVERAGE OF WHOLE . RL
NO NAME
20 HSL21 HSL
37 HSL38 HSL39 HSL40 HSL41 HSL
-D-4"l;4-DrCHLORaBENZENE ' "D-8 NAPHTHALENED-8 ACENAPTHENED-10 PHENANTHRENED-12 CHRYSENFD-12 PERYLENF2-FLUOROPHENOL (SURROGATE)D-5 PHENOL (SURROOATE)D-5 NITROBENZENE (SURROGATE)2-FLUOROBIPHENYL (SURROGATE)2.4,6-TRIBROMOPHENOL < SURROGATE.)D-14 TERPHENYL (SURROGATE)N-NITROSODIMETHYLAMINE2-CHLOROPHENOLPHENOLBIS (2-CHLOROETHYL) ETHER1.3-DICHLOROBENZENE1.4-DICHLOROBENZENE1,2-DICHLOROBENZENEANILINfcBENZYL ALCOHOLSIS(a-CHLOROISOPROPYL)ETHERHEXACHLOROETHAME - . . -H-NITROSODI PROP YLAMINFNITROBENZENEISOPHQRONE2-NITROPHENOL2,4-DIMETHYLPHENOLBIS(2-CHLOROETHOXY)METHANE2,4-DICHLOROPHENQL1< 2.4-TRICHLOROBENZENENAPHTHALENEHEXACHLOROBUTADIENfcP-CHLORO-M-CRESOL
HEXACH1OROCYCLOPENTADIENE2,4,6-TRICHI. OROPHENOL2-METHYLPHENOL4-METHYLPHENOLBENZOI-C ACID4-CHLOROANILINE2-METHYLNAPHTHALENE2-CHLORONAPHTHALENEDIMETHYL PHTHALATEACENAPHTHYLENE2, 6-DINITROTOLU6.NEACENAPHTHENE
NO NAMF •47 2,4-DINITROPHENOL48 4 NITROPHEMOL49 2,4-DINITROTOLUENE50 FLUORENE51 4-CHLOROPHENYL PHENYL E1HER52 DIETHYL PHTHALATE53 4,6-DINITRO-2-METHYLPHENaL54 N-NITROSODIPHENYLAMINE.35 1,2-DIPHENYLHYDRAZINE
..56 - - 4-BR0110PHENYL PHENYL ETHFR"- "57 HEXACHLOROBENZENE58 PENrACHLOROPHENOL59 PHENANTHRENE60 ANTHRACENE61 DI-N-BUTYL PHTHALATE62 FLUORANTHENE63 HSL 2, 4, 5-TRICHLOROPIIENOL64 HSL 2-NITROANILINE63 HSL 3-NrTROANILINE66 HSL DIBENZOFURAN67 HSL 4-NITROANrLINE68 BENZIDINE69 PYRENE70 BENZYL BUTYL PHTHALATE71 BENZO(A)ANTHRACENE72 3,3'-DICHLOROBENZIDINE73 CHRYSENE . . . . - . . -74 BISC2-ETHYLHEXYL) FHTHALATE75 DI-N-OCTYL PHTHALATE76 BENZO(B)FLUORANTHENE77 . BENZO(K)FLUORANTHENE78 . .BENZO(A»PYRENE•79; • INbENO(1.2,3-CD>PYRENe'80 DrBENZO(A,H>ANTHRACEN£81 BENZO (GH I»PER YLE-NE
NO M/E SCAN TIKE REF RRT M&TH AREA(HGHT) AMOUNT 7.TOT
,N0 M/E SCAN . TIME REI- RRT KE.TH AREA<HCHT) AMOUNT . XTOTI 132 699 11 04 1 1.000 A BV 31080. 40.000 UG/ML 1-6. 022 136 939 14 52 2 1.000 A BV 7S560. 40.000 UG/ML 16 023 164. 1277 20 13 3 1.000 A BB 47012. 40.000 UG/ML 16.024 188 1337 24 39 4 1.000 A BV 73911. 40.000 UG/ML 16.023 240 2066 32 43 3 1 . 000 A BB 39317. 40. 000 UG/ML 16. 026 264 2322 36 46 6 1.000 A BB 117837. 40.000 UG/ML 16.027 NOT FOUND8 NOT FOUND9 NOT FOUND
10-WIT-FOUNT* •— —— •11 NOT FOUND -•12 NOT FOUND13 NOT FOUND. - . . .:14 "NOT FOUND VJJ
15 NOT FOUND .-• - . :16 NOT FOUND17 NOT FOUND -*8 t46——-?04—-1-1—06———1——1. 003——A-&B——•—~——S9S-.——————0. C3T UQ/ML——6-1-6-- Q19 NOT FOUND20 NOT FOUND °21 NOT FOUND22 NOT FOUND23 NOT FOUND24 NOT FOUND23 NOT FOUNDVtr——-BE;——U63 13: 4U 2 0. 919 A BB 416^————"——0-337 OS/ML -& -L3—27 NOT FOUND . • • . . , . . . - . . - - — — • -.28 NOT FOUND29 NOT FOUND30 NOT FOUND31—-NOT-TDUND - - ";
32 NOT-FOUND . - . • • • - • • -33 NOT FOUND34 NOT FOUND35 NOT FOUND36 NOT FOUND37 NOT FOUND38 NOT FOUND19 1?=' 9^9 —t-S—H-——•?——1 0?1——ft»fiB———————-6>OS^—— 1.270 UG/ML 051-^40 NOT FOUND41 NOT FOUND42 NOT FOUND43 NOT FOUND44 NOT FOUND45 NOT FOUND46 NOT FOUND47 NOT.FOUND48 NOT.FOUND49 NOT FOUND50 NOT FOUND51 NOT FOUNDSa—-Wf T38'? 2 ? r 0 0 3 1.08S A BE 708. 0.075 UG/ML ~0~03—-53 NOT FOUND54——1-69——T4TS——2e" 23——4——0—709——A—Bfl————————&6-4-——————F^&^—LlC.^m n 1755 NOT FOUND56 NOT FOUND
N357585960
6263646366676869•TO-71.727374
767778798081
M/ENOTNOTNOTNOT
NOTNOTNOTNOTNOTNOTNOTNOT14<?
.NOTNOTNOT149
NOTNOTNOTNOTNOTNOT
SCANFOUNDFOUNDFOUNDFOUND
1703FOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
—X987-FOUNDFOUNDFOUND
2105
FOUNDFOUNDFOUNDFOUNDFOUNDFOUND
TIME
-- - • •
-31.3.B
33:20
REF
5
RRT
I. 019
MFTH
. - - ,.
A»BB———
A VB
AREA(«GHT)
9002.531.
AMOUNT
0. 8Q<? \ia/w
—U. W^. UU/HL"
5.878 UG/ML
. XTOT
/2. 35-
DATA: EPABH1370 #701CALI; EPABN1370 ttl
BASE n/'E: 146/- 156RIC; 327. / 16695.
DUAL MASS SPECTRUMB9/-18/84 15;51;08 + 11:86SAMPLE: 77113-14 ABN 1/10CONDS.:ENHANCED <S 15B 2N 0T)
0 0 1
DUAL MASS SPECTRUM09/18/84 15:51;00 + 13:40SAMPLE; 77113-14 ABN 1/18CONDS.;ENHANCED <S 15B 2N 0T)
DATA; EPABN1370 #863CALI; EPABH1370 #1
BASE 1-1/E; 82/RIC: 165./
81 82
DUAL MASS SPECTRUM89/18/84 15:51:09 + 15;11SAMPLE: 77113-14 ABN 1/18CONDS.:ENHANCED <S 158 2N 0T)
DATA: EPABH1370 »959 BASE H/E: 41/ 122CALI; EPABN1370 #1 RIC: 42./ 366.
-r——\———r
120 130i- 1 -
60 70 80 90 100 110
i I '-
0 0 1 - 5 0
DUAL MASS SPECTRUM DATA: EPABN1370 #1389 BASE V\/i: 149/ 149I 69/18/'84:15:51;00 + 22:00 CALI; EPABN1370 #1 RICi 395./ 1205.I SAMPLE; 77113-14 ABN 1/10. CONOS.! ;;
ENHANCED:<S 15B 2N 0T) i100.0-| : ; ; j :. I r- 364.
50.04 '
t1/E '; 50 160
50.0- | '.
100.0-' 1- 304.; . 0 0 1 ° t-' 1
DUAL MASS SPLCTRUM i : DATA; EPABN1370 #1416 BASE M/-E; 169/ 4109/18^84 15!51;09 + 22:25 CALI; EPABN1370 #1 RIC: 510./ 1667.
! SAMPLE; 77113-14 ABN 1/-10COMDS.! I ;ENHANCED <S 15B 2N 8T) ;
1B0.0)-] I r 231.I : , : _
59.0^- ' ' . • !
' t ! . ! ! . ' :
1 , '
M/E 50 iee 150- - t 1 ^ I I -I • -I- I I I 1 I 1 • I I , 1 I I I 1 • I I -
50.0- I
100.0-^ i L 231.I I . ; • • • 0 0 1 ^ 5 2
DUAL MASS:SPECTRUM09/18/84 15:51:00 + 26:58SAMPLE; 77113-14 ABN 1/18CONDS.;ENHANCED <S 15B 2N 0T)
DATA: EPABN1370 )fl703CALI: EPABN1370 #1
BASE M/E: 59/ 43RIC; 888. / 56639.
150 256i I
! DUAL HA5S SPECTRUM ' DATA; EPABN1370 #1987 BASE M/E: 121/- 43i Q9/IQ/Q4 15;51;00 + 31:28 CALI: EPABN1370 #1 RIC; 829./ 7527.I SAMPLE; 77113-14 ABN 1./10; CONDS.;' ENHANCED <S 15B 2N 0T>
106.0-| ; [- 637.
50,8" . \ ' \ '.
[ | ; • ' .'
;1-L,—^———| r ' \—i—)—i—i—r^-^—S—|—\J-Y—r—|—I—i—i—y—\—\—I—i—i—i—i—r
n/E ! 50 100 : 150;—i 1 4 — 1 , 1 — 1 - i - ,4 . . -^ ' i T t . T T 4 T V T ^ T 1 '77T 1 t ' ' TT ' ' t ' ' 1 ' 1 i
50.0- ' ^
100.0-1 ' L 637.' , \ • • 0 0 1 ^.' 5 4
DUAL MASS SPECTRUM DATA: EPABN1370 #2105 BASE H/E: 149/ 14909/18/84;15;51;00 + 33:20 CALI: EPABN1370 #1 RIC: 11503./ 21119.SAMPLE; 77113-14 ABN 1/10CONDS.i :ENHANCED;<S 15B 2N 0T)
100.0-1 ' : r 3456.
I ' • ' ; ' : , ' ' ' "; ' '! I ; , ; .' i
1 ' ' , ' ' . ' ' . ! •'.': \
56.9- ' '. '^ . ;
M/E 59 100 1 0 200 250' ti ft |t ' jtt '^^ i , . , . . ^ , . 1 1 1 1 . 1 . i , , . i , 1 , 1 , 1 , , . ,
50.6 - !
100.0- \ ' ' . L 3456.^ . : i ; 0 0 1 " 3 5
•^
f
DUAL09/1SAMPCONDENHA
11 r-"
MASS8/84 1LE; 77S.i: •NCED <
1 :
,1 ,lll
' " I
SPEC75:51:113-1
5 15B
i
I I I
RU064
3 2
ll11
11
JI1i + 3
ABN
?N 8T
0
F
5:121/1
)
IIIilLT-J^-
r
0
4^4-
^}]\
\ i • \
: ; , :
1 1 1 ' 1
1. 1 1 1 1 1
DATA; EPABH1370 #2223 BASE M^E: 57/CALI; EPABN1370 »1 RIC: 10319./
' 1 ' | ' 1 ' 1 ' 1 ' 1 ' | ' 1 ' l i l200 250
i .1 » 1 i . l • 1 < 1 i 1 < 1 i 1 » 1 . 1.
| ;
5717599.
- IS
•
10
I. ^ 0 0
LIBRARY. SEARCH03/-18/84 15:51:00 + 27:18SAMPLE; 77113-14 ABN 1/18CONDS,^;' ... - .•,. .ENHANCED (S 15B 2H 0T)
DATA; EPABN1370 #1716 BASE M/-E; 43CALI; EPABH1370 tt 1 RIC; 68991.
1394 i
SAMPLE
C16.H32.02
11 NT125(1B PK 43RANK 1IN 1S616FIT 986
HEXADECANOICACIO
:18.H26.02
M m 1B PK 66RANK' 2IN: 9172FIT: 975 •
C9.H18.02: 1394 ^
t1 HT 158B PK 66RANK . 3IN '73S4FIT, 963 •
M/E
1 1 , 1
56
-L L
:
; !
,1
1
, , 1 1 , , 1
DECANOICACID
ll 1NONANOICACIO
1 1 1.
i
;
S———^
~i—'—'—"00 i|50.; 208 259
0 0
LIBRARY SEARCH ,B9/18/84 15;51 see + 29:19SAMPLE;; 77113-14 ABN 1/16CONDS.?. • . ;'. . i •
DftTA: :EPflBN1379 #1852CALI: -EPftBN1370 # 1
BASE M/E: 43RIC: 45867.
DECANOICftCID
NONAMOICACID
(56'
; " ' ' "1
• " ^ • 1 . 1 • ,.'—————————————.————————————-——————^————————————r-:iee 150 ! 288 250 ; 38i3 350 480 . 450 500
Environmental Proieciion Agency, CLP Sample Management OHice.P. 0. Box Bl 8. Alomndra, Virginr 2231.3.703/557-2490
Sample Number
^^36Organics Analysis Data Sheet
(Page1)
.^^•fs-n-^Laboratory Name: Case No:
QC Report No:
Contract No:
Lab Sample ID No:
Sample Matrix: ~-y)
nate~Sa-m-pleReceive-d:"-Z l-Z3-iS^_
rids
n (Circle One)
fl W •
^1 '.
Data Release Authorized By:
^ ;;y.o.la.tiJe Compounds
Concentration: ('tow) Medium (Circle One)•"•'' '-' '• " ::- r\c-—^— -Q"Date Extracted/Prepared: 0
Date Analyzed::——,0-^—1—1
Conc/0-iLEacloc- .-
Percent Moisture:
-PH.
Percent Moisture (Decanted):
CASNumber
74-87-3
74-83-9
75-OT-4
75-00-3
76-09-2
67-64-1
75-15-0' "
75-35-4
75-34-3
156-60-5
67-66-3
107-06-2
78-93-3
71-55-6
56-23-5
108-05-4
75-27-4
Chloromethane
BroiTio methane
Vinyl Chloride
Chldroathane
Melhytene Chloride
Acetone , - . . - . - . . -
Carbon Bisulfide
1;"1-OichT6roflthsne" ~ •-—
1 , 1 -Dichloroeihane
Trans-1. 2-Oichloroethene '
Chloroform
1. 2-Dichloroelhane " " ' •
2-Bmanone
1 . 1 . 1-Trichloroethane
Carbon Tetrachlonde
Vinyl Acetale
Bromodichloromeihane
. ufl/l of^Jla/(CircleTB'
• -H .i/'/
•:-#; / 4 s
. , p.,:.;;a-••-!^-.
., .5.., ; :•?• ^ 7
, .-. 7-. ^ ,- bS• : 7 -^—^• • -/- ^.
Kg<fs8,
<
/
A,
....
,
^
y
>
-.—
CASNumber
79-34-5
78.87.5
10061.02-6
79-01-6
124-48-1
79-00-5 .
71-43-2 • -
10061-OK-'
110-75-8
75-25-2
591-78-6
t08-10-l ,
127-18-4
(08.88-3
108-90-7
t00-41-4
100-42-5
-i——————————
1 . 1 .2 . 2-Tetrachloroethane
1, 2-Dichloropropane
Trans-1. 3-Dichloropropene
Trichloroeihene
Otbromochtoromelhane
1 , 1 , 2-Tnchloroethane,
•Bentene - • - • — : - - — • •- •;
cis^: 3-Dichloropropehe'" "
2-Chtoroelhvlvinytether
•Brornoform
2-HftKanone
4-Melhy! -2-Pentanonc
Telrachforoelhene
Toluene
Chlorobenzene
Elhylbenzene
Slyrene
Toial Xylenes
ug/lori^(Circlen
J, ^
?-?
- 7 ••. ? .-.•-2, !
• • • - ? " • ---^-;
-^" i' 'VL\f^^
^ry-^^-f?-?>
me}
{——
/ -
.f
/
'. D«u Reporting Qualffien
For reponin^ rexditt 10 EPA. th« following rflsuht OUJ
cfflfiniHon ol aach" tlag musi be txolicil p
<f<ers •re used
Vclu« tf the raiufi i« « v«lue graarr lh«n or equfll to the
(tBiwnon limn. repon the vlue
U IndiCJios cornpound wat •nalyiBti *&r hul "ol d<t»c«ad
Rflport the minimum d«t«ci<on hfnil (or ihe umple with
lh» U (a o . 10U)bJt«d on fi«CBtMrYCOOcentr«lK>r»/
dilution •c1ion« (This is not i-xcesfcirity me iniirum«nt
d«l«ctton limit .[The (ootr>ot« xhould r««d U-
Cowpound wt Tflyied (of but nol d«rct«d. Th«
riumtxr ic 1rr« minii ufri •naifvbia d«(«cii0fi I'mn (o*
ihe Mmple
•J l<^diCJl«& •n etiirm«d vlo«. The fl«g r u—d •ittf
when •«tim«t4ng • conc»nir»lKXi (or mni«li<Mlv
»d«niifi*d compoundi •vt^re • 1 : 1 f«ippn«« <« •*su»TVt»d
of when the man Bp»cir«( dar indicatfi« 11- rvi-.»"^-
C Thit <lag •[Kilies to p«stic*d« p«ram«rrs where the
identiftcation h«s t»en confirrrwi by GC/MS Sinflle
component pecrcioes^l 0 ng •'ul m ihfl final eKHaci
Shoutd be confirmed DY GC/'MS
B This 1\»g if uKd when ih« «nJilyie is found in the blank
•s well <i J Mmpiff h >nd»caies pos&ible/protiable
bl«nk coni«mination and wwrns the daU u&er 10 lake
•op«op*me •ci'on
OthT Olher specific (lag* «nd toolnolat may tK raqyired to
properlv dedne the retullt tl utftd. they mult be fully
oe»cnb«d •od «uch deicnpiion •n«ched lo ihe d«f
HJmmarv rapon
EnvifonintnttlPtofeclionAflOTcv. ClPS»np(«Mln*g«in«<itOff>c«.P.O..Bo«8»8; Aleyndn>.VIreinr22313 703/'S57-1490
Organics Analysis Data Sheot(Page 4)
Tentatively Identified Compounds
CASNumber
1
2 ' ' • ^ ' - ' • •
3
d -
s6
7.
R
9.
in.
11
17
it14.
IS
Ifi
17
1R.
1 9
20.
71..
22
23
24
2!,
?S
27
28
29
30
Compound Nama ' ..
Uol/OK\^ C^i^Jf
. • • ' ' '
. .. ..- -..-...-...
• . — . - - ' • •
. .. . .. . . .. - , . . . - - . . . .
; . ; • . - . ..-.-.
• • . 1
• 1'
; '. [ .
• ~i :., •
r
• • T
Fr»etior).
.-•..-.-.—-..--.:
... . ..
RT or Scan; Mumbar
.;:'.•; :. . . . •
- ;-., . -.
CttimatedConcartttation
(ug/1 OffigTkg^.
r
£
. . . — , . ; .
-^^o
tiY
ea^o
CT1
X> 0
3>
CO '-'
•Z.-
Z.-
3. \
<-
)C
T C
l "0
-
mL
nr-
m" .
m s
.. ..
co"
^^.
^"
^"
Co
.-
( -^
(M^U
^
• -
: ••
-g B
^>^^(^
^^^^^_^^^^y
/^ A
^A
^^A
^^
i^^
C^^
^-I
'/•
00 ^
^-.-^--M
^-t^A
^^..C
S^^V
. )
QUANTITATION REPORT FILE: EPAVOA1721
DATA: EPAVOA1721. TI08/19/84 5:07:00SAMPLE: 77113-15SUBMITTED BY: EPA ANALYST: RJW
AMOUNT=AREA(HGHT) * REF. AMNT/(REF. AREA(HGHT)* RESP.FACT)RESP, FAC. FROM AVERAGE OF WHOLE . RL
MO NAME1 *2--.B.--
3 »
H3LHSL
HSLHSLHSL
HSLHSLHSLHSL
BROMOCHLORMETHANE^ (INTERAL STANDARD)P-DIFLUOROBEN2ENE ^INTERNAL'STANDARD)D.ICHLOROBENZEIME-D5: < INTERNAL STANDARD)CHLOROMETHANE ;BROMOMETHANEVINYL CHLORIDE : •CHLOROETHANE , .METHYLENE CHLORIDEACROLEINACRYLONITRILE1, -L-DICHLOROETHYLENE1. -L-DICHLOROETHANETRANS-1,2-DICHLOROETHYLENECHLOROFORM :1, a-OICHLOROETHANE'1, 1, 1-TRICHLOROETHANEACETONE :
CARBON DISULFIDE • " 'CftRBON TETRACHLORIDEBROMODICHLOROMETHANE1,2-DICHLOROPROPANETRANS-l.^-DICHLOROPROP-YLENE " - '-TRICHLOROETHYLEN^BSNZENEDIBROMOCHLOROMETHANE1, -L, 2-TRICHLOROETHANECIS-i. 3-DICHLOROPROPYLENE2-CHLOROETHYL VINYL ETHER8ROMOFORMMETHYL ETHYL KETONEVJN'YL ACETATEMETHYL ISOBSJTYL KETONE1. 2-OICHLOROETHANE-D4 (SURROGATE)BENZENE-DA (SURROGATE)D1EROMOTETRAFLUOROETHANE (SURROGATE)Brs'PERFLUOROISOPROPYL)KETONE (SURROGATE)Fi.L'OROEENZENE (SURROGATE)TSTRACHLOROETHYLENE1,1,2,2-TETRACHLOROETHANETOLUENE ' ^ '/ 'CHLOROBENZENEErHYLBENZENE2-:-!EXANONESrYRENE
0-^YLENEM-:<YLENE
NO47484950
NAMEM-eROl-IOBENZOTRIFLUORIDE (SURROGATE >D-5 ETHYLBENZENE (SURROGATE) .TOLUENE-DB (SURROGATE)P-BROMOFLUOROSENZENE (SURROGATE)
NO--1
234567B9
1011
M/E SCAN-130 - 385114 699117 BS8NOT'FOUNDNOT FOUNDNOT FOUNDNOT FOUND
B4 237NOT FOUNDNOT FOUNDNOT FOUND
T313:23:29;
9:
:ME09S319
45
REF123
1
: RRT1.-0001. 0001. 000
0. 745
MlAAA
A
:THBBBBBB
BB
AREA(HGHT)14133.64337,39B14.
14343.
AMOUNTS0. 000 UG/L30. 000 UG/LS0..00e :UG/L
•/.TOT4. 344. 344. 34
38. 357 .UG/L 2. 59
NO121314151617i a
1920212223a425262728293031323334353637'10
394041424344454647484950
- M/ENOTNOTNOTNOT97
NOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOT436584
NOTNOTNOT
- 3AA
NOTNOTNOTNOTNOTNOTNOTNOTNOTNOT
9B95
SCANFOUNDFOUNDFOUNDFOUND
516FOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUND'FOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
726468617
FOUNDFOUNDFOUND- 7RPfFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
8151036
TIME
17: 3B
24: 4815:5921: 05
27:5135: 24
REF
1
222
—3—
33
; RR
1.. 34
.,;..—..
:.:^
l.:03'i0.; 67t0.: 88:
-o.'7e'=
0. 95Cl.:20-3
' • • tt
0 A
?- A3 A3 A
9 A?• A
ETH
BB
SBBBBB
-DD—
BBBB
; AREA<HGHT»
30551.
125202.61726.
114230.
——38BB.'
116166.65834.
AMOUNT
46. 243,
491. 155100. 627
92. 11B
ia
103. 01984. 949
: • •-^; -
UG/L
UG/LUG/LUG/L
UG/LUG/L
•'XTOT •
4. 20 «
44. 62 •-"9. 148. 37
- 44-
9. 367. 72
DUAL MASS SPECTRUM83/19^84 5!07!00 + 9:48SAMPLE: 77113-15CONDS.:ENHANCED <S 15B 2N 0T)
DATA; EPAUOA1721 #287 BASE M/'E: 49/- 49CALIi EPAUOA1721 #1 RIC; 13103./' 14927,
49 60 70 80
DATA: EPAUOA1721 #515 BASE M/E; 97/- 97CALI; EPAUOA1721 #1 RICi 17343./ 18697.
DUAL MASS SPECTRUM ;
98/19/34 5i07!00 + 17S3SSAMPLE:'77113-15CONDS.:; IENHANCED <S'15B 2N 6T)
80 90 190 110 1201
40
-\——r—r—r-50 60 70
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i DUAL MASS SPECTRUM DATA; EPAWA1721 #780 BASE M/E: 166/- 4498/19/84 5;07;00 + 26:39 ! CALI; EPAWA1721 #1 RIC: 3967./ 11327.SAMPLE:|77113-15 ' . , :CONOS.sl IENHANCED <S 158 2N 0T>
100.0-1 : : r 1374.
50.0- . , , . . , . . . .
—I—i—r1-]—I' 'l I J I ;i | "i ; 1 ! 'i' | •• i |—i—|—r- '^—|—f—|—i i ' i 1 'I———I 1 I 1—|—r-1
M/E 50 . S ; '. \ . \ 100 . i Ui 150 ' 200| I I I I I • ] ' • j l j • I . 1 . 1 , 1 . ! 1 ll I i 1 i I i I l I I 1 i 1 i
59,9- ' ; : • ;' , •. : ' .
100.0- : • ; L 1374.: ; 0 0 •i •' 6 S
Environmental Protecnon Agency.P.O.Bo«8l8. Alexandria.Virgin!
1 1 ^
lab Sample in No- 1 T<7 •n
CLP Sample Management OMice., 22313 703/S57-2490
Organics Anal(Pa
.^s4im^ -;5^Y.
. yL . . .U Volatile C<
Concentration: (Vow)
. . . . ... 0 . 1
Percent Moisture (Oecan
ysis Dgel)
Gas
(?C
Cor
Oat
omROL»
Mediu
^ 1
Q'tted):'.
)ata Sheet
H Nn
RBport Nn 7 7 —'
•ilrarl Nn V o
Jnds
m (Circle One)
i^W^i
r
Sample Number
/^w
^Q
OJ-^~7?,D^]nt-W
l i
D
CASNumber
74-87-3
74.83-9
75-01-4
75-00-3
75-09-2
67-64-1
75-15-0
75-35-4
75-34-3
156-60.5
67-66-3
107-06--2
78-93-3
71-55-6
56-23-5
108-05-4
75-27-4
Chloromethane
Bromomethane
Vinyl Chloride
Chloroethane
Methylene Chloride
Acetone
.Carbon Disulfide ;
1 , 1-Dichloroethene
^.-l-Dichloroethane
Trans-1, 2-Dichloroelhene
Chloroform ;
1 : 2-Dichloroeihane
2-Bulanone
1 , 1 , 1 -Trichloroelhane
Carbon Telrachloride
Vinyl Aceiate
Bromodichloromethane
ug/lori^(CircleTS
^l.. .
• ^
• •eJV,
~^t~^\
~"T'"• •l-• ^^
-^^^ iM '^
^-J
^
J-
,
^
/
CASNumber
79-34-5
•78-87-5
'10061-02-6
'79.01 -6
124-48-1
79-00-5
71-43-2 ; •
10061-01-5
110-75-8
75-25-2
591-78-6
.108-10-1
127 -18 -4
108-88-3
108-90-7
100-41-4
•100-42-5
1 . 1 .2 . 2-Teirachloroethane
1 , 2-Dichl.oropropane •
Trans-1, 3-D(chloropropene
Trichloroethene
Dibromochloromethane
1 , 1 . 2-Trichloroelhane
Benzene '- :;
cis-1. 3-Dichioropropene
2-ChIoroethylvinylether
Bromoform
2-Hexanone
4-Methyl-2-Penianone
Tetrachforoelhene
Toluene
Chlorobenzene
Elhyl benzene
Slyrene
Total Xylenes
ug/l orw/(CircleW
^ 1-s-•T
?3 •
? .? i
3 •
• =? -
'.y-•- 7"H^H^ ^~}
•4
?-J - ^
Kg/^ne|
y
\
D«ta R«E>oning Qualifiers
< reponiitfl rosults lo EPA, th« following resiflis aualifiei
definition O* BBCh tiflfl rnust t>B •KpltCll '
V«lu« H the fetuti K • vlu« gr««taf than or equal \o lh«
<tci®ct*o" (<mn. r«oon thfl value
U indicatet compound w«s analyzed for.but "01 o<itec(«d
Rapon ilw mir>imum d«(flciion fimil <(K lha umpl«wrth
tn< U (fl .g,. I OU| ba*«d 0" nacit—rY CO"CBnn*HKm/
dilution •ctions. (Th»t is noi n«c«furily the inurunwnl
<*B(BCI'O I limit .1 Th« fooinof xnould r«ad U-
C(xnpound Wt •n«lyi«<J (or but noi (»«(«ci«d Th«
numbflr i« in« minimum TUinJbl* dataction limit to*
the Mmpic
J lndic*l«k •n «»(imal«d vlu« Th<« fl«g i« u*«d edhf
w+ien ttumating e co"cflmr«non for iBntfllivflly
This flag •ppties to pesliCtde par»fTKier$ •vhere the
idennficaiion has baari condrmcd Oy GC/MS S»ngle
coniponeni p^tticid^s^l 0 nfl/ul in the linnl aKtraci
snouki be confirmed Ov GC/MS
This (lag is ui»d wtwn ih< •nal^e 11 found in th« blank
as w<ll as J sample H indtcates polt'ole/protxble
«ppro<in«ie action
Ot"«» Olh<r loeciltC Hags and (oolnows m*Y t>e requi(e0 to
proo«rlv delinfl the reculif M usftd, tt'<Y fnuti tx tulli
d«u:nb«d and BUC" dfltcftption •nach»d 10 (hfl dar
turnmAry feport
Environmental Protection Agency. CLP Sample Management Office.P. O.Box818. Alexandria. Virginia 22313 703/557-2490
Sample Number
H^nO^SOrganics Analysis Data Sheet
(Page 2)
Semivolatiie Compounds
Concentration: (to / Medium i (Circle One)
Date Extracted/Prepared: IJ l^-5
Date Analyzed: c \ \^n•^~\
CASNumber
62-75-9
108-95-2
62-53-3
111.44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
39638-32-9
106-44-5
621-64-7
67.72-1
98-95-3
78-59.1
88-75-5
105-67-9
65-85-0
1 1 1 - 9 1 - 1
120-83-2
120-82-1
91-20-3 .
•106.47.8
87.68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91.58-7
88.74.4
1 3 1 - 1 1 - 3
208-96-8on f-in i
N-Nilrosodimelhylamine
Phenol
Aniline
bis(-2-Chloroelhyt)Elher
2-Chlorophenol
1. 3-Dicntorobenzftne
1. 4-Dichlorobenzene
Benzyl Alcohol.
1; 2-DichIorobenzene
2-Methylphenol
bis(2-chlorotsopropvl}£tner
4-Methyiphenof
N-Nitfoso-Di-n-Propylamine
Hexachforoeihano
Nitrobenrene
Isophorone
2-Nilrophenol
2, 4-DimethY)phenol
Benzoic Acid
bis(-2-Chforoethoxy)Methane
2, 4-DtChlorophenol
1 , 2. 4-Trichloroben2ene
Naphthalene
4-ChIoroaniline
Heitachlorobyladiene
4-Chloro-3-Melhylphenol
2-Methylnaphthatene
HexachlorocYclopentadiene
2.4. 6-Trichlorophenol
2, 4, 5-Trichlorophenot
2-Chforonaphihalene
2-Nitroaniline
DtmelhYl Phihatate
Acenaphihylene" .,
iia/lorCa/Kg?(CircieOne)
CASNumbef
83-32-9
51-28-5
100-02-7
•I.32-64-9
^21-14-2
606-20-2
84-66-2
7005-72-3
86-73-7
100.01-6
534-52-1
86-30-6
101-55-3
1:18-74-1
87-86-5
35-01-8
120-12-7
84-74-2
206-44-0
S(2-87.5
r29-00-0
85-68-7
31-94-1
36-55-3
1;17-81.7
2'18-01-9
1,17-84-0
205-99-2
207-08-9
SO-32-8
1.93.39-5
53-70-3
1'9I-24-2
Acenaphthene
2. 4-Oinitrophenol
4-Niirophenol
)ibenzofuran
2. 4-Dinitrotoluene
2, 6-Dinitrotoluene
Diethylphthatate
4-Chforophenyl-p'henyfethef
Fluorene
4-Nitro3niline
4, 6-Dinitro-2-Meihyiphenol
N-Nitrosodiphenytamine ( 1 )
4-Bromophenyl-pheny<ethet"
Hexachlorobenzene
Pentachlorophenol
Phenanihrene
Anthracene
Di-n-Butylphthalale"
Fluoranthene
Benzidine
Pyrene
Buiylbenzylphthaiate
3. 3'-Dichlorobenzidine'
Benzo(atAnthracene '
bis(2-Ethy(hexyl)Phihalaie
Chrysene
Oi-n-Odyl Phlhalale
Benzo(b)Fluoranthene
Benzo(klFluoranthene
Benzo(a>Pyrene
lndeno(1. 2. 3-cd)Pyrene
Diben^a, h)Anthracene
Benzo(g. h, i)Perylene
ug/lor^g/Kg^(CircieOn?
EnvKonnKfual Promotion Agency, CLPSafnp(«MJn«gam«nlOnic«.P.O.BoxSIS. AlnxirKlru.VirB.no 22313 703/557.2490
Organics Analysis Data Sheet(Page 4)
Sample Number
Tentatively Identified Compounds
CASNumb«r
l
•>
1
a
•i
fi
7
R
l
in
n
17
n
1 A
Ti
1 R
17
in
19
?0
21
77
23
24
7fi
3B
27
2B
29
in
Compound Name
-
. ; .. ..-...„
FractionRT or Scan
NumberEstimated
Concentration(ug/1 o^tiO/kgL
0
0
0 0
RIC08/19/-84 7:67:09SAMPLE; 77113-15 MSDCOHDS.:RANGE; G 1,1330 LABEL; N
DATA;CALI:
EPAWA1723 #1EPAUOA1723 #1
0, 4.0 QUAN; A 0, 1,0 J 0
SCANS
BASE: U 20,815
1 TO 1300
QUANTITATION REPORT FILE: EPAVOA1723
DATA: EPAVOA1723. TI8B/19/84 7:07:00SAMPLE: 77113-15 MSDSUBMITTED BY EPA ANALYST: RJM
AMOUNT=AREA(HGHT) « REF. AMNT/(REF. AREA<HGHT)* RESP.FACT)RESP. FAC. FROM AVERAGE OF WHOLE . RL
MO NAME1 »2 »3 »
HSLHSL
30 HSL31 HSL32 HSL
HSLHSLHSLHSL
BROMOCHLORMETHANE (INTERAL STANDARD)P-DIFLUOROBENZENE (INTERNAL STANDARD)DICHLOROBENZENE-D5 (INTERNAL STANDARD)CHLOROMETHANEBROMOMETHANEVINYL CHLORIDECHLOROETHANEMETtiYLENE CHLORIDEACROLEINACRYLONITRILE1,1-DICHLOROETHYLENE1, 1-DICHLOROETHANETRANS-1,2-DICHLOROETHYLENECHLOROFORM1, 2-DICHLOROETHANE1,1,1-TRICHLOROETHANEACETONECARBON DISULFIDECARBON TETRACHLORIDEBROMODICHLOROMETHANE1, 2-DICHLOROPROPANETRANS-1, 3-DICHLOROPROPYLENETRICHLOROETHYLENEBENZENEDXERGMOCHLOROMETHANE1,1,2-TRICHLOROETHANEC;S-1,3-DICHLOROPROPYLENE2-CHLOROETHYL VINYL ETHERBROIIOFORMMETHYL ETHYL KETONEVINYL ACETATEMCTHVL ISOBUTYL KETONE1,2-OICHLOROETHANE-D4 (SURROGATE)B£N2ENE-D6 (SURROGATE)DIBPOMOTETRAFLUOROETHANE < SURROGATE)B1E(FERFLUOROISOPROPYL)KETONE (SURROGATE)F^UOROE.ENZENE (SURROGATE)TETRACHLOROETHYLENE1, - , £ , 2-TETRACHLOROETHANETOLUENECHLOROBENZENEETriYLBENZENE2-HE;'A^ONESTYREME0-XYLEMEM-<YLENE
NO474B4950
N0123456789
1011
1213141516
NAMI
M/E130114117NOTNOTNOTNOT
84NOTNOT
61NOTNOTNOTNOT
97
M-BID-5TOUP-SI
SCAN384
698857
FOUNDFOUNDFOUNDFOUND
287FOUNDFOUND
369
FOUNDFOUNDFOUNDFOUND
515
M-BROMOBENZOTRIFLUORIDE (SURROGATE)D-5 ETHYLBENZENE (SURROGATE)TOLUENE-DS (SURROGATE)P-SROMOFLUOROBENZENE (SURROGATE)
TIME REF RRT METH AREA(HGHT)51590.
268497.159081.
13: 07 1 1. 000 A BB
23: 51 2 1. 000 A BB29; 17 3 1. 000 A BB
9: 48 1 0. 747 A BB 34. 137 UG/L 4. 09 62586.
12: 36 1 0. 961 A BB 57. 746 UG/L 6. 93 111121.
17: 36 1 1. 341 A BB 49. 385 UG/L 5. 92 119099.
AMOUNT 7.TOT50. 000 UG/L 6.0050. 000 UG/L 6. 0050, 000 UG/L 6. 00
NO1718192021222324252627282930313233343536373B394041424344454647484950
M/ENOTNOTNOTNOTNOTNOT
9578
NOTNOTNOTNOTNOTNOTNOT436584
NOTNOTNOT166NOT
91112NOTNOTNOTNOTNOTNOTNOT
9895
SCANFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
605621
FOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
72546861&
FOUNDFOUNDFOUND
780FOUND
821861
FOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
8151036
TIME
20: 4821: 13
24: 4615: 5921: 03
26: 39
28:0329:25
27: 5135: 24
REF
22
222
3
33
33
RRT
0. 8670. 890
1. 0390. 6700. 883
0. 910
0. 9581. 005
0. 9511. 209
METH
A BBA BB
A VBA BBA VB
A BB
A BBA BB
A BBA BB
AREA<HGHT)
87953.181042.
31812.211691.469033.
24796.
199880.138976.
475220.269712.
AMOUNT
33.165 UG/L33. 352 UG/L
29. 912 UG/L82. 719 UG/L90. 662 UG/L
9. 94S UG/L
36. 991 UG/L33. 426 UG/L
105.475 UG/L87.102 UG/L
•/.TOT
3. 984. 00
!r',
3. 599. 92 '~
10. 87 0
0
1. 19
4. 444. 01
12. 6510. 45
DUAL MASS SPECTRUM08/19/84 7;07s68 + 9:48SAMPLE; 77113-15 MSDCONDS.!ENHANCED (S 15B 2N 6T)
DATA; EPAUOA1723 #287CALI; EPAUOA1723 Sl
BASE N./E: 49/ 49RIC: 5S255./ 53263.
40 60 79 80
0
DUAL MASS SPECTRUM08/13/84 7;07!00 + 12:3£SAMPLE: 77113-15 USDCONDS.!ENHANCED (S 15B 2N 0-0
DATA; EPAWA1723 tt369CALI; EPAUOA1723 <tl
BASE M/E; 61/ 61RIC; 62713.-' 66047.
40 60
-T"
78 89 30 100
0 0 1 :1 "/ 7
DUAL MASS SPECTRUM03/19/84 7;87;09 + 17;36SAMPLE: 77113-15 MSDCOHDS.:ENHANCED <S 15B 2N 9D
DATA: EPAUDA1723 #515CALI; EPAUOA1723 #1
BASE M/'E: 97•/ 97RIC; 74379./ 78335.
40 60 70 80 S6 110 129
'- 21888.
DUAL MASS SPECTRUM08/19/84 7:07:88 + 28;48SAMPLE; 77113-15 MSDCOHOS.;ENHANCED <S 15B 2N 0T)
DATA; EPAUOA1723 TO5CALIs EPAUOA1723 ftl
BASE n/-E; 95/ 35RIC; 34531./ 97731.
0 0 1
DATA: EPAUOA1723 #621CALI; EPA1JOA1723 »1
BASE ri/E: 78/ 78RIC: 675S3./ 184S31.
DUAL MASS SPECTRUM88/19/34 7:07:00 + 21;13SAMPLE: 77113-15 MSDCONDS.:ENHANCED <S 15B 2N 0T)
60 70
0 0
49
DUAL MASS SPECTRUM03/'19/84 7; 07; 88 + 24:46SAMPLE: 77113-15 MSDCONDS.: .ENHANCED <S 15B 2H 0T)
DATA; EPAWA1723 #725CALI; EPIWOA1723 Dl
BASE ri/'Ei 43/ 43RICi S335./ 13E63.
40 68 70 30 90
0 0
DUAL MASS SPECTRUM DATA: EPAWA1723 <t78@ BASE M.-'E; 166/ 16683/'13/84 7:07!00 + 26!39 CALI! EPAUOA1723 #1 P^IC! 32415./ 39743.SAMPLE: 77113-15 MSDCONDS.:ENHANCED <S 15B 2N 0T>
100.8-1 r 4G88.
59.0-
tl/E 50 100 150 200
j ||||[|])|| ||j))'| • | 1 | | 1 ' j l ^ l ' j ' j l 1 1 1 ' ' • | ' ] ] 1 ' • ' ' ' j ' ) j | ' ' ' ' ' ' ' I
50, 0 -
100.0-^ , \- 4688.0 0 1 ' • ; 2
DUAL MASS SPECTRUM DATA: EPAUOA1723 #321 BASE M/E; 91/ 9188/13/'84 7!e7!00 + 28;83 CALI; EPWOfllPSS til RIC; 73993./ 113£63.SAMPLE: 77113-15 MSDCONDS.:ENHANCED (S 15B 2M eT)
199.0-1 r 34432.
50.0-
—r i—I—•L-I—^U—| "I ' |—I--11111"!—j—i—\—v—|—i—|—i—|—i—|—i—|—i—|—i—|—i—|———|—T^
M/E ^0 ^0 1^8 2^0
, ',|i|i|||^L..I.irlTji1r.l-^ I •^I'j,'^. < I———' • ' • ' • ' ' ' • ' •———^-^-J———|
50.3-
109.0-^ '- 34432.0 0 1 ' n ?
DUAL MASS SPECTRUM03/19/S4 ?!e7:00 + 29;25SAMPLE; 77113-15 MSDCONDS.:ENHANCED <S 15B 2N 8T>
DATA; EPAWA1723 #861 BASE M/E; 112/' 112CALI; EPWOftl723 #1 RIC; £2331./' 118655.
1 1| , " 1C
-^hh. ,„ J||
0i| | l | . H i . ' , . l . i j j
' ' I T 1 • • I ' I 1100
- 1—t 1 I 1 1 -I 'llli 'Tiiii—^~~——-
1 |
—1——
^
1 i I i 1 i | i 1 i 1 i I i 1 i i
153 230-1 i 1 < 1 i 1 i 1 i 1 i 1 i 1 i 1 i
t-
00
SCANS 1 TO 2800RIC DATA: EPABN1361 #1CALI; EPABN1361 ttl09/17/84 19:16:00
SAMPLE: 77113-7 1/10 ABNCONDS.:RANGE: G 1,2808 LABEL: H 2, 2.0 QUAN: A 2, 3.0 J 0 BASE; U 20, 3
i5
5007:55
1009l5;50
150023:45
2000
31:40250039:35
QUANTITATICN REPORT FILE: EPABN1361
DATA: EPABN1361.TI09/17/84 19:16:00SAMPLE: 77113-7 1/10 ABNSUBMITTED BY: A?<1ALYST:
AMOUNT-AREA<HQHT) » REF.AMNT/(REF.AREA(HGHT)* RESP.FACT)RESP. FAC. FROM AVERAGE OF WHOLE . R L
MO NAME1 »2 •»3 »4 *5 »6 »
20 HSL21 HSL
HSLHSLHSLHSLHSL
D-4 1,4-DICHLOROBENZENED-8 NAPHTHALENED-8 ACENAPTHENED-10 PHENANTHRENED-12 CHRYSENFD-12 PERYLENF2-FLUOROPHENOL < SURROGATE. >D-5 PHENOL (SURROGATE)D-5 NITROBENZENE (SURROGATE)2-FLUOROBIPHENYL (SURROGATE)2.4,6-TRIBROMOPHENOL (SURROGATE)D-14 TE.RPHENYL (SURROGATE)N-NITR OSODIMETHYLAMINE2-CHLOROPHENOLPHENOLBIS (2-CHLOROETHYL) ETH6.R1,3-DICHLOROBENZENE1<4-DICHLOROBENZENEI,2-DICHLOROBENZENEANILINEBENZYL ALCOHOLBIS(2-CHLOROISOPROPYL)ETHERHEXACHLOROETHANEN- NITROSODIPROPYLAMIN6NITROBENZENEISOPHORONE2-NITROPHENOL2,4-DIMETHYLPHENOLBIS(2-CHLOROETHOXY)Mm HANE2,4-DICHLOROPHENOL1,2,4-TRICHLOROBENZENE-NAPHTHALENEHEXACHLOROBUTADIENEP-CHLORO-M-CRESOLHEXACHLOROCYCLOPENTADI EN?2,4.6-TRICHLOROPHENOL2-MFTHYLPHENOL4-METHYLPHENOLBENZOIC ACID4-CHLOROANILINE2-METHYLNAPHTHALENE2-CHLORONAPHTHALENEDIMETHYL PHTHALATEACENAPHTHYLENE2,6-DINITROTOLUENEACENAPHTH£NE
/
//'
NO NAME2,4-DINITROPHENOL4-NITROPHENOL2.4-DINITROTOLUENEFLUORENE4-CHLOROPHENYL PIIENYL ETHERDI ETHYL PHTHALATE4, 6-DINITRO-2-METHYLPHENOLN-NITROSODIPHENYLAMINF1. 2-DIPHENYLHYDRAZINE4-BROHOPHENYL PHENYL ETH6.RHEXAC.HLOROBENZENE .PENTACHLOROPHENOLPKENANTHRENEANTHRACENEDI-N-BUTYL PHTHALATEFLUORANTHENE
HSL 2,4,5-TRICHLOROPHENOLHSL 2-NITROANILINEHSL 3-NITROANILINEHSL DIBENZOFURANHSL 4-NITROANILINE
BENZIDINEPYRENEBENZYL BUTYL PHTHALATE.BENZOCA)ANTHRACENE3.3'-DICHLaROBENZIDINfcCHRYSENEBIS<2-ETHYLH£XYL) PHTHALATEDI-N-OCTYL PHTHALATEBENZO(B > FLUORANTHENEBENZQ(K»FLUORANTHENEBENZO<A)PYRENEINDENO(I. 2,3-CD)PYRENFDIBENZO<A.H>ANTHRACENEBENZO<GHI )PERYLF:NE
M/E SCAN TIME REF RRT METH AREA(H5MT) AMOUNT 7.TOT
NO1234S6789
1011121314151617181920212?23242526272829303132333435363738394041424344454647484950515253545556
M/E1S2136164188240264NOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOT
SCAN699942
1280133820632320
FOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDPOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
T111420243236
IME043316404244
REF1234S6
RRT1. 0001. 0001. 0001. 0001. 0001. 000
MEAAAAAA
:THBVBBBVBBBBBB
AREAd-iSHT21323.30/18.33937.32489.30900.39094.
) AMOUNT40.00040.00040.00040. 00040.00040.000
UG/MLUC/MLUG/MLUS/MLus/Mi-ne/ML
7.TOT16. 7116. 7116. 7116. 7116. 7116. 71
NO M/E SCAN TIME. REf- RRT METH AREA(HSHT) AMOUNT y.TOT57 NOT FOUND58 NOT FOUND59 NOT FOUND60 NOT FOUND61 NOT FOUND62 NOT FOUND63 NOT FOUND64 NOT FOUND65 NOT FOUND66 NOT FOUND67 NOT FOUND68 NOT FOUND69 NOT FOUND70 NOT FOUND71 NOT FOUND72 NOT FOUND73 NOT FOUND "'74 NOT FOUND75 NOT FOUND ~-76 NOT FOUND Q77 NOT FOUND _78 NOT FOUND79 NOT FOUND80 NOT FOUND81 NOT FOUND
Environmental Protection Aflency, CLP Sample Management OHice,P. 0.80x618. Alexandria. Virginia 22313 703/557-2490
Sample Number
P'H^D^
Laboratory Name:
Lab Sample ID No:
Sample Matrix:
Organics Analysis Data Sheet(PageD
'.{.^•^S^m case No:
^^il^l^A^ QC Report No:
Contract No:
Date Sample Received: 6j'/~f'l'h^Data Release Authorized By:
~D Volatile Compounds
Concentration: /Cow) Medium _ (Circle One)
Date Extracted/Prepared: 0,
Dale Analyzed: ——,° 1 , 1
Conc/Dil Factor: ————(_
Percent Moisture: ——d
Percent Moisture (Decanted): .
^1^
<2,iy/ .
-PH-
CASNumber
74-87-3
74-83-9
75-01.4
75-00-3
75-09-2
67-64.1
75-15-0' "
75-35-4
75-34-3 •
156.60.5
67-66-3
107-06-2
78.93-3
71-55-6
56-23-5
108-05-4
75-27.4
Cnloromethane
Bromomethane
Vinyl Chloride
Chloroethane
Methytene Chloride
Acetone
Gaboon Drsulfide;
T. 1-Oichloroethene
1, 1-DtChloroelhane
Trans-1, 2-Dichloroethene
Chloroform
1 . 2-Dichloroeihane
2-Bulanone
1 . 1 , 1-Trichloroethane
Carbon Tetrachloride
Vinyl Acetate
Bromodichloromelhane
ug/lortijTK(CireleTrfl
IK 1
1<4
- i n: ^ Y /
^5—. —i
' • ^?-
.: ... ...•T -
N\?11-.^.
——^7. 1 4 1^^
aT
^
^
CASNumb«r
7.9-34-5
78-87-5
10061-02-6
7S-01-6
124-48-1
79-00-5
;7'1 -43-2 .
1D061-01-5
110-75-8
75.25-2
S91-78-6, .
108.10-1
127.18-4
108.88.3
108-90-7
100-41-4
100-42-5;
1 , 1 , 2 . 2-Teirachloroeihane
1, 2-Dichloropropane
Trans-1, 3-DichlofOpropene
Trichforoethene
Oibfoinochloromelhane
1. 1 . 2-Trich(orbethane
SenTene : - •': -• - •"- ••;
cis-1-. 3-Oichloropropene
-2-C+doroethylvinYlether
Bromoform
2-Hexanone
4-Me!hYl-2-Pentano^^':
Telrachloroeihene
Toluene
Chlorobenzene
Elhylbenzene
Styrene
Total Xylenes
ug/l or m/(CircleU?
-? 1
-?
^
'?^••
7..... ^ .
^.- -r-^^^
-^^?^\
Kg^is)
1
-\
/Dau Reporting Qualifaers
For faporting refuitt io;EPA. the following resists Qualifiers «re usod
Ad<liii(n-ial 41*gs Of (ootnotet «xolinni"g fsutts rfie' <rtcou<'*i3»d Howev<f.
d«1infi<on of ««ch flag mull be expl.cil \
M th« r««uh it a wlu« gr««t«r t^<" or »qual lo t^e
cf4l«ciion limit, fport lh« v«tu«
li-idiCaK- compound wi anJtyred lor bui noi d«!eci<d
Rtpon lh» rninifnum dflteciiO" limn Iw the sJmDiawnih
tho U (B.B . 10U) b.isod on Mceswn/ conccntfinon/
diluiion Jict*on«. (Th)* it not necaKUtily (he iniirufneni
d«teciion limit .) The footnor should read U-
Compound w«( analyzed lor bul f>o< d«l«ct»d Th«
numbflf it the mintmyrn «rfir^ab>e oelection limit (of
the umole
lndic«l«f •n ••ti'rrfd wlu«. Thi< (t«o <• u»9d •ith—'
wh«n cilirming a cooc«r»tf«HKKl f(K Knuii^ily
This (l«g T>pl<«s 10 peSUCKit par«m<taft whar® (he
•dent ideation h»s t>*<n confiffrwd by GC/MS Single
componcni petttCtd«t£10ng/u) in the final axifCt
should be confirmed by GC/MS
B This {lag if u(«d wh<in IMC •rutyte it found in (h« bl»i
•s ovall «t • umpl« H <ndicaics poisible/pfobabi*
tilank contamination •nd wrns ih« datJ us«f to t«ke
•Dpioome •ciion
OTh»f Olh<r ipecidc llagi •wl k*o«noie» mav b< r«<iuif»d <o
(KQp«irlv d«tin« lha rsulis rf uwJ, thav mu»i tx luH^
ooicnb*d and «uch deicupiion «nach»d lo the dar
Environmental Protection Ag«ncY. CLP Sample Management Office.P.O Bo«B18. Alexandria. Virginia 21313 703/557-2490
Sample Number
Hm-hsOrganics Analysis Data Sheet
(Page 2)
Semivolatile Compounds
Concentration: (to / Medium i (Circle One)
Date Extracted/Prepared: ^ ) 3 \ ~\
Dale Analyzed: 4 ^ ^ ^•\ ________
Conc/Dil F . ~>\^.^ \0^d^-
CASNumber
62-75-9
108-95-2
62-53-3
1 1 1 -44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
39638-32-9
106-44-5
621-64-7
67-72-1
98.95-3
78-59-1
88.75-5
105-67.9
65.85-0
1 1 1 - 9 1 - 1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59.50-7
91-57-6
77-47-A
88-06.2
95-95-A
91-58-7
88-74.4
1 3 1 - 1 1 - 3
208.96-8
N-Niirosodimethylamine
Phenol
Aniline
bis(-2-Ch,oroethyl)Elher
2-Chlorophenol
1. 3-Dichlorobenzene
1. 4-Dichlorobenzene
Benzyl Alcohol
1.-2.Dich!orobenzene
2-Melhyiphenol
bis(2-chloroisopropvl)Elher
4-Methylphenol
N-Nitroso-Di-n-Propylamine
Hexachloroethane
Nitrobenzene
Isophorone
2-Nitrophenol
2, 4-Dimethvfphenol
Benzoic Acid
bis(-2-Ch)oroethoxy)Methane
2, 4-Dichlorophenol
1 , 2. 4-Trichtorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chtoro-3-Melhylphenol
2 -Methyl naphthalene
Hexachforocyclopentadiene
2. 4. 6-Trichlorophenol
2. 4. 5-Trichlorophenol
2 -Chloconaphthalene
2-Nilroanitine
Dimelhyl Phthalate
Acenaphihvlene
ug/l ortfd/Ka^(CircieDne)
CASNumber
83-32-9
51-28-5
100-02-7
132-64-9
121-14-2
606-20-2
84-66-2
7005-72-3
86-73-7
100-01-6
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-B
120-12-7
84.74-2
206-44-0
92-87-5
129-00-0
85-68-7
91-94-1
56-55-3
1 1 7 - 8 1 - 7
218-01-9
117-84-0
205-99-2
207-08-9
50-32-8
193-39-5
53.70-3
191-24.2
Acenaphthene
2, 4-Dinnrophenol
4-Nitrophenol
Dibenrofuran
2, 4-Oinitrotdluene :
2,G-Dinilrotoluene
Diethylphthalate
4-Chlorophenyl -phehylether
Fluorene
4-Nitroaniline
4. 6-Dinitro-2-Methylphenol
N-Nilrosodiphenyfamine 0)
4-Bromophenyl-phenyleiher
Hexachlorobenzene
Pemachlorophenol
Phenanihrene
Anthracene
Di-n-Butylphihalate-
Fluoranihene
Benzidine
Pyrene
BuTylbenzytph^halate
3, S'-Dichlorobenzidine
Benzo{a|Anthracene
bis(2-Elhy(hexy()Phihalaie
Chrysene
Di-n-Octyl Phihalale
Benzo(b)Ffuoranihene
Benzo(k)Fluoramhene
Benzo(a)Pyrene
lndeno<1. 2. 3-cd)Pyrene
Dibenz(a. h)An[hracene
Benzo(g. h. i)Perylene
ug/1 or(tfg/Kg^(Circleune
Environm«nul Prot«ctionAQ«ncv. CLP S«mpl« M«n«g«m4nl Office.P O.Bo.eiB. Ataundri*. Virgin.* 22313 703/557-2490
Organics Analysis Data Sheet(Page 4»
Sample Numbar
Tentatively Identified Compounds
CASNumb«r
1
2
3
4
S.
e7
aain1113
13, ,
14 •
1 R
16
17
1R.
1 9
2C-
.?!
27
23
24
2S
26
27
2S
29.
in
Compound Name
.
'•
;
- ' • . . . t.-
:. •': --•-'.
'•
'. ". 1
•
•;
r
FractionRT or Scan
NumberEstimatad
ConcentrBtiQA(ug/1o^Og/kg),
<M
0
0
.... -
I- 0 0
SCANS 1 TO 1300RIC DATA: EPAUOA1722 ftlCALl! EPAUOA1722 #1eg/-19/84 6:08:00
SAMPLE; 77113-15 MSCONDS.;RANGE; G 1,1308 LABEL: N 0, 4.0 QUAN: A 0, 1.8 J 0 BASE: U 20, 3
817
37
2£
.
1 •
\ 96 178 .V-—'"—————•""—"J
' 12806:50
3737
-\^J'
04£
..„.„..
40013;40
5
39
U'
6
6
|
•w- J60
20!
18
6S
l^J^J
933
33
7(
|UU
OJ
ai
^i
80627:2
f
8E
J-/•'3>0
;1
10
.J^J
100034:10
132512
36
}
\J0^7^206^^
i | i1200 SCAN41:00 TIME
QUANTITATION REPORT FILE: EPAVOA1722
DATA: EPAVOA1722. TI08/19/84 6:08:00SAMPLE: 77113-15 MSSUBMITTED BY USTCO ANALYST: RJM
AMOUNT=AREA(HGHT) » REF. AMNT/(REF. AREA<HGHT)« RESP.FACT)RESP. FAC. FROM AVERAGE OF WHOLE . RL
NAME«•*•••
17 HSL18 HSL
30 HSL31 HSL32 HSL
HSLHSLHSLHSL
BROMOCHLORMETHANE (INTERAL STANDARD)P-DIFLUOROBENZENE (INTERNAL STANDARD)DICHLOROBENZENE-D5 (INTERNAL STANDARD)CHLOROMETHANEBROMOMETHANEVINYL CHLORIDECHLOROETHANEMETHYLENE CHLORIDEACROLEINACRYLONITRILE1, l-DICHLOROETHYLENE1, J.-DICHLOROETHANETRANS-1, 2-DICHLOROETHYLENECHLOROFORM1,2-DICHLOROETHANE1.li1-TRICHLOROETHANEACETONECARBON DISULFIDECARBON'TETRACHLORIDEBROMODICHLOROMETHANE1,2-DICHLOROPROPANETRANS-iL, 3-&ICHLOROPROPYLENETRICHLOROETHYLENEBENZENEDZBROMOCHLOROMETHANE1,1,2-TRICHLOROETHANEC;S-1,S-DICHLOROPROPYLENE2-CHLOROETHYL VINYL ETHERBSOMOF&RMM£THVL ETHYL KETONEVINYL ACETATEM.TTHYL ISOBUTYL KETONE1.2-DICHLOROETHANE-D4 (SURROGATE)BENZENE-D6 (SURROGATE)
D-IPROMOTETRAFLUOROETHANE (SURROGATE)B.rS(PERFLUOROISOPROPYL)KETONE (SURROGATE)FL-UOROEENZENE (SURROGATE)TS'-'RACHLOROETHYLENE1, J-, 2, 2-TETRACHLOROETHANETOLUENECl-iLOROKENZENE
•Er!-!YLBENZENE2-HE:XAN.ONESn'RENE;'
0-^VLElvEM'-XYLENE
M-SROMOBENZOTRIFLUORIDE (SURROGATE)D-5 ETHYLBENZENE (SURROGATE)TOLUENE-OB (SURROGATE)P-SROMOFLUOROBENZENE (SURROGATE)
SCAN335699858
FOUNDFOUNDFOUNDFOUND287
FOUNDFOUND370
FOUNDFOUNDFOUNDFOUND
511.
TIME REF RRT METH13: 09 1 1. 000 A BB23: 53 2 1, 000 A BB29: 19 3 1. 000 A BB
V: 48 1 0, 745 A BB
12: 38 1 0. 961 A BB
17: 38 1 1. 340 A BB
AREA(HGHT)S0103.
330407.100748.
95372.
116910.
231014.
AMOUNT 7.TOT50. 000 UG/L 4. 9350. 000 UG/L 4. 9350. 000 UG/L 4. 93
53. 5&4 UG/L 5. 28
62. 557 UG/L 6. 17
98. 634 UG/L 9. 73
<-
NO
171819202122232425262728293031323334353637383940414243
44454647484958
M/ENOTNOT
NOTNOTNOTNOT9578
NOTNOTNOTNOTNOTNOTNOT
436584
NOTNOTNOT166NOT
91112NOTNOTNOTNOTNOTNOTNOT
9895
SCANFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
60&632
FOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
725469617
FOUNDFOUNDFOUND
731FOUND
822B&3
FOUNDFOUNDFOUNDPOUNDFOUNDFOUNDFOUND
Bl.t,1026
T3:ME REF
20:42 2 0.21:13 2 0.
24: 46 2 1.•1&:01 2 0.21:05 2 0.
26:41 3 0.
2B: 05 3 0.2T: 29 3 1.
27: 53 3 0.35:24 3 1.
RRT
867890
037671883
910
958806
951207
METH
A BBf\ BB
A BBA BBA VB
A BB
A BBA BB
A BBA BB
AREA(HGHT)
97014.207121.
41561.189218.419548.
52173.
197572.110880.
359064.151348.
AMOUNT
42. 629 UG/L44. 464 UG/L
45. 540 UG/L86. 160 UG/L94. 504 UG/L
33. 025 UG/L
57. 735 UG/L42. 110 UG/L
125. 837 UG/L77. 176 UG/L
7.TOT
4. 214. 39
\'^
4. 498. 509. 32 0
0
3. 26 "•
5. 704. 15
12. 417. 61
DUAL MASS SPECTRUMe8^19/-84 6!98;0@ + 9; 48SAMPLE: 77113-15 MSCONDS.:ENHANCED (5 15B 2N OT)
DATA; EPAUOA1722 #237CALI; EPAUOA1722 #1
BASE M/E: 49/ 49RIC; 81919./' 86527,
48 60 70 80
0 0
DUAL MASS SPECTRUM08 19/84 6;08:80 + 12i38SAMPLE; 77113-15 MSCONDS.:ENHANCED <S 15B 2N BT)
DATA: EPAWA1722 #378CALI; EPAWA1722 #1
BASE n/'E: 61/ 61RIC; 89471./' 93823.
-i—'-J-^———i———• | ' • • • i————i————r
40 50 68 70 80 90 100
0 0 1 '
DUAL MASS SPECTRUMBS/19^84 G!08;00 + 17;38SAMPLE: 77113-15 MSCONDS.;ENHANCED <S 15B 2N 0T)
DATA; EPAUOA1722 #516 BASE n/E: 97/' 97CALl! EPAWA1722 #1 RICi 146637. / 151807.
48 60 79 80 90 100 110 129
1
DUAL MASS SPECTRUM DATA: EPAUOA1722 tt606 BASE M/Ei 95/- 95eS/19/SA 6s08s00 + 29S42 CALI; EPAUOA1722 #1 RICi 103887./ 187519.SAMPLE: 77113-15 fISCOMDS.;ENHANCED <S 15B 2N UT)
198.0-1 r 16496.
50.9-
M/E 53 190
|———1|| ' ' • | 1 | | |1———' |t|| I———I——————L-^^———I lt|TT|1———————————————————ITTTT^
50.9- . . - •
100.0-^ - 18496.^ • 0 0 2 - 0 0
DUAL MASS SPECTRUM DATA; EPAWA1722 #622 BASE M.-'E; 78/ 7803/19784 6!3.S!09 + 2l!l5 CALI!! EPAUOA1722 #1 RICi S3327./ 114175.SAMPLE: 77113-15 MSCONDS.:ENHANCED (S 15B 2N eT)
186.0-1 r 36672.
58.9-
M/E 48 58 63 • 79 88
TO.a-
0 0 2 - 0 1
DUAL MASS SPECTRUM DATA: EPAUOA1722 #725 BASE M/E: 43/- 4303/'19-'84 6!0?.s0e + 24!46 CALl! EPAWA1722 «l RIC! 14431,/ 19263.SAMPLE; 77113-15 MSCONDS.;ENHANCED (S 15B 2N 0T>
109.0-1 r- 6976.
- I
561.0-
————,——' ' | I I '—i————j————l ' ' ! ' |————i—'—h————i————I————I——'—1————i————J
M/E 49 53 69 70 80 93 100————• ,,|,y,|————3————^-1————-^—————————————^————————^
59.9-1
-!
100.0-' i - 6976.| O 0 2 ' ) ' i ^
DUAL MASS SPECTRUM38---19/84 6; 98s 30 + 26; 41SAMPLE: 77113-15 MSCONDS.:ENHANCED (S 15B 2N @T)
DATA; EPAWA1722 #781 BASE M/'E; 166/ 166CALI; EPAWA1722 #1 RICi 66943,/' 74239.
__i—i—,- i i~i—1—r" "i—I—r
109 150 200
0 0 2 " u :"
DUAL MASS SPECTRUM08/'19/84 6;08i00 + 28s 85SAMPLE: 77113-15 t1SCONDS.!ENHANCED <S 15B 2N 0T>
DATA: EPAUOA1722 #822CALl! EPAWA1722 #1
BASE M/E: 91.-- 91RIC; S93S3./ 107135.
109 150
DUAL MASS SPECTRUMQ8/19/S4 6108;60 + 29!29SAMPLE; 77113-15 MSCONDS.sENHANCED (S 15B 2N 8T)
DATA: EPAUOA1722 #863CALI; EPAUOA1722 #1
BASE M/'E: 112/ 112RIC! 55167./- 81919.
199i I ' —I., 7
0 0 2 • 1 .' :'
'. "6 0 0
SCANS 1 TO 2800RIC DATA: EPABN1360 »1CALI: EPABN1360 #109/17/84 18:18:00
SAMPLE; 77113-7 1/10CONDS.;RANGE; G 1,2800 LABEL: N 2, 2.0 QUAN: A 2, 3.0 J 0 BASE: U 20- 3
IS
5007:55
100015:50
150023:45
200031:40
250939:35
QUANTITATION REPORT FILE: EPABN1360
DATA: EPABN1360-'TI — — — — — — -09/17/84 18:18:00SAMPLE: 77113-7 1/10SUBMITTED BY: ANALYST:
AMOUNT°AREA(HOHT) * REf-. AMNT/(REF, AREA(HGHT)* RESP.FACT)RESP. FAC. FROM AVERAGE OF WHOLE . R L
NAME•»»•»«•
20 HSL21 HSL
HSLHSLHSLHSLHSL
D-4 1-4-DICHl.OROBENZENED-8 NAPHTHALENED-8 ACENAPTHENED-10 PHENANTHRENED-12 CHRYSENED-12 PERYLENt-2-FLUOROPHENOL <SURROSATE»D-5 PHENOL (SURROGATE)D-S NITROBENZENE (SURROGATE)2-FLUOROB IPi-tFNYL (SURROGATE >2,4.6-TRIBROMOPHENOL (SURROGATfc)D-14 TERPHENYL (SURROGATE)N-NITROSODIMETHYLAMIN62-CHLQROPHENOLPHENOLBIS (2-CHLOROE1HYL) ETHER1.3-DICHLOROBENZENF1.4-DICHLOROBENZENE1.2-DICHLOROBENZENEANILINEBENZYL ALCOHOLBIS(2-CHLOROISOPROPYL)ETHERHEXACHLOROETHANEN-NITROSODIPROPYLAMINENITROBENZENEISOPHORONE2-NITROPHENOL2,4-DIMETHYLPHENOLBIS(2-C HLOROETHO X Y)ME IHANE2.4-DICHLOROPHENOL1.2.4-TRICHLOROBENZEMENAPHTHALENEHEXACHLOROBUTADIENEP-C HLORO-M-C RESOLHEXACHLOROCYCLOPENTADIENF2,4,6-TRICHLOROPHENOL2-METHYLPHENOL4-METHYLPHENOLBENZOIC ACID4-CHLOROANILINE2-METHYLNAPHTHALENE2-CHLORONAPHTHALENEDIMETHYL PHTHALATEACENAPHTHYLENE2,6-DINITROTOLUENEACENAPHTHENE
NO NAME47 2, 4-DINITROPHENOL48 4-NITROPHENOL49 3.4-DINITROTOLUENE50 FLUORENE51 4-CHLOROPHENYL PHENYL ETHER52 DIE1HYL PHTHALATE53 4.6-DrNITRO-2-METHYLPHENOL54 N-NITROSODIPHENYLAMINE55 1,2-DIPHENYLHYDRAZINF56 4-BROMOPHENYL PHENYL ETHFR57 HEXACHLORQBENZENE58 PENTACHLOROPHENOL59 PHENANTHRENE60 ANTHRACENE61 DI-N-BUTVL PHTHALATE62 FLUORANTHENE63 HSL 2.4,5-TRICHLOROPHENOL64 HSL 2-NITROANILINE65 HSL 3-NITROANILINE66 HSL DIBENZOFURAN67 HSL 4-NITROANILINE68 BENZIDINE69 PYRENE70 BENZYL BUTYL PHTHALATE71 BENZO(A>ANTHRACENE72 3,3'-DICHLOROBENZIDINF73 CHRYSENE74 BIS<2-ETHYLHEXYL) PHTHALATE75 DI -N-OCTYL PHTHALATE76 BENZO < S »FLUORANTHENE77 BENZO(K>FLUORANTHENE78 BENZO(A)PYRENE79 INDENOd, 2, 3-CD)PYRENF80 DIBENZO(A.H)ANTHRACEN&81 BENZO(GHI)PERYLFNE
NO M/E SCAN TIME REF RRT METH AREA(!-!5HT> AMOUNT 7.TOT
NO123456789
1011121314151617181920212723242526272829303132333435363738394041424344454647484950515253545556
M/E152136164188240264NOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOT
SCAN699942
1280135920662320
FOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
TIME11: 0414; 3520: 1624: 4132:4336:44
REF1 1.2 1.3 1.4 1.3 1.6 1,
RRT000000000000000000
METHA BVA SBA BVA SBA BVA SB
AREA<«8HT»16491.34717.23606.39260.24930.38459.
AMOUNT40.000 UO/ML40.000 UG/ML40.000 UG/ML40.000 UG/ML40.000 UG/ML40.000 UG/ML
XTOT16. 7216. 7216. 7216. 7216. 7216. 72
NO M/E SCAN TIME REF RRT KETH AREA(HSHT) AMOUNT 7.TOT57 NOT FOUND - - -58 NOT FOUND :
59 NOT FOUND60 NOT FOUND61 NOT FOUND62 NOT FOUND63 NOT FOUND64 NOT FOUND65 NOT FOUND66 NOT FOUND67 NOT FOUND68 NOT FOUND :69 NOT FOUND ;-.70 NOT FOUND ' ";71 NOT FOUND "•_73 NOT FOUND ;-73 NOT FOUND C\!74 NOT FOUND ' C75 NOT FOUND 076 NOT FOUND77 NOT FOUND78 NOT FOUND79 NOT FOUND80 NOT FOUND81 NOT FOUND
Sample NumberEnvifonmenlfitProleciion Agency. CLP Sample Management OMicc.P.O B0..818. Aleundna. Virginia 22313 703/557.2490
Orgaoics.AnalysisOata Sheet(Page 1 )
'^^s4imLaboratory Name:
Lab Sample ID No,<2_^ •g
Sample Mairix: —30 \. X
Oa(a Release Aulhorired By: Dale Sample Re<
u^^,<&-o/-WS^
.oi^. ^i/m^V Volatile Compounds
Concentration: /'Low) Medium (Circle One)
Percent Moistur<
0 ,
^
>•
i(0e
l/^^ • /
/ ' PH
i-anlflril
7.0
CASNumber
74-87-3
74.83-9
75-01.4
75-00-3
75-09-2
67-64-1
75-15-0
75-35-4
75-34-3
156-60.5
67-66-3
107.06-2
78-93.3
71-55-6
56-23.5
108-05-4
75-27-4
Chtoromethane
Bromomelhane
Vinyl Chloride
Chtocoelhane
Methylene Chloride
Acetone
Carbon Oisulfide
1 , 1 -Dichtoroethene "
1, 1-Oichloroeihane
Trans-1. 2-Oichlofoelhene '
Chloroform
1 , 2-Dichloroeihane
2-Butanone
1 , 1 . 1 •TrichloroeThane
Carbon Telrachloride
Vinyl Aceiale
Bcomodichloromelhane
ug/loiulg(CirdaT:
/ o u-'o/to
/O.</o.5
-- 6"5"
-ir-5'/&2^ -/O.5'
^
\i1
*-/
CASNumber
79-34-5
78-87-5
10061-02-6
79-01.6
124-48-1
79-00-5
71.43-2
tOOfil.01.5
110-75-8
75-25-2
591-78-6
1 0 8 - 1 0 - 1
1 2 7 - 1 8 - 4
108-88.3
108.90-7
100 -41 -4 ,
100.42-5
1 , 1 , 2 . 2-Tetrachtoroethane
1 , 2-0tch(oropropane
Trans-1, 3-Dichloropropene
Trichloroethene
O'bromochloromelhane
1 , \. 2-Trichloroclhane
Benzene
C f S - 1 . 3-OichlofOpropene
2-Chloroeihv(vinyte(her
Bromoform
2-Hexanone
4-MelhY(-2-Penianone
Telrachloroelhene
Toluene
Chlorobenzene
Eihylbenzene
Styrene
Total Xylenes
ug/l or i q^(Circle^O
^6 \/^'
6<5',1;^( 0A"" /
/O 1
/^A^£'S- i3~ 1s-\/
Kg^mel
/
D«U R«poning Quilifie's
F.or i«poriir>B <flt"llt lo EPA. t < <ol(£>»vir fl results gu^
Addition*! <Ugs o» (ooirtoi<>»<iu>l*i"if\g r««ulls a«e Bf
dflfinHion of •«Ch 11«Q musl tr •«fllic<;
c a'aJi«f ;h«n ex •qu«l 10 (ric
lr*d«CalBl compound «VJS •(^•lyrftd (or t)u1 "01 d«1«0«d
Report th« minimum d«<9C1<on IITMI (<K ir»« Mfnpt<w1h
lh« U <« o . 10U] bJi*d on n«ce«urv cooc«nif«l>on^
dilution action* {This <s no( ri«c«turilv (FM? irMCfu'n«n(
dawction limn | The (001001® «houtd i»*a U-COTipourtd w( »n«lYi*<} lot but noi dfltacied Th«
nurritxir if ih« fninimum T(*irL«b^a d«l*cti0« lirnrltor
l"< K/npio
•«rs •re uwd
>UfJQ«d Mo'"^Cv<f. the
C Tnn fl«g •ppiies lo peilicidc pT«"tfltef» iwnare ir>«
id<r>ii(ic*('o" hai t>«n co"Hrmw3 bv GC/MS S>ftfl(«
corr>po"trtl p<tticxlet?10 "g I'ul i" ine linal oiract
should &e co"*'*"'«3 by GC/MS
B Ttiit <1<B ls "*w3 wt^en ih» «rulYifl it (ouwJ '" ' bl<"k
•s bv«tl «> • MfTiDH- li ind<cai«i poa.s-ble/rKOtMbk
bifh comamimiion artd v/a'nt if* <l»r ut« 10 laht
JC>p<aoriJI« •CtiO"
Ot»x' Ol"tt IpocifiC <rg» <fid (ootnolti mflY b< *equif*<3 lo
prcuwrlv Afifin? Ihr mt.irn H 11*-^ "'--• •"• •" K- (' •"•
Env«ronm«ntal Protect«on Agency. CLP Sample Management OfftCfl.P. 0 Bo« 818.- Ate«aniffi»: Virginia 22313 703/557-2490
Organics Analysis Data Sheet(Page 2)
Semivolatile Compounds
Concentration: (toy^ Medium > (Circle One)
Date Extracied/Preparedi <j|o-^ ^ y"\
Date Analyzed: \ \ \ 1 6\____
Conc/Dil Facior: \ "^ \1^~^—-
Sample Number
^LA^AL/^
CASNumber
62-75-9
108-95-2
62-53-3
111-44 .4
95-57-8
541-73-1
106-46-7
100-51-6 -
95-50-1
95-48-7
39638-32-9
106-44-5
621-64-7
67.72-1
98.95-3
78.59-1
88-75-5
105-67-9
65-85-0
1 1 1 - 9 1 - 1
120-83-2
120-82-1
91-20-3
106-47-8
B7-68-3
59.50-7
91 -57 -6
77-47-4
88-06-2
95.95-4
9 1 - 5 8 - 7
88.74-4
1 3 1 - 1 1 . 3
^-Nilrosodimelhytamine
Phenol
Aniline
bis(.2-Chtofoeihy()Elher
2-Chloropheno!
1. 3-Dichlorobenzene
1.4-Dichtorobenzene
-Benryl-Alco+iot
1, 2-Oichlorobenzeoe
2-Meihylphenol
bis(2-chloroisopropyllEther
4-Methylphenoi . -
N-Niuoso-Di-n-Propylamioe
Hexachloroethane
Nitrobenzene
Isophorone - .————.- . —
2-Nitcophenot
2. 4-0ime(hy(phenol
Benzoic Acid
bis<-2-ChloroethoKy)Melhane
2, 4-Dichlorophenol
1. 2. 4-Trichlorobenzene
Naphthalene
4-Ch(oroaoi)«ne
Hexachlorobutadiene
4-Chlofo-3-Meihylpheno<
2-Meihylnaphihalene
HeKachlorocyclopeniadiene
2. 4. 6-TrichlorophenoI
2. 4. S-Trichlorophenol
2-Chloronaphlhalene
2-Nitcoan<line
Dimethyl Phthalale
ug/lortfg/(CirclaCT
; OU
) \
$uSO^0
MO^2^0<W>A^^rU^( ~0
^^0r OiTD
o^OiS rt)5^0\BTS^)?WDr O^sn^s-o^^0^CTS?U-05J5D5^T>^r0\t^~^codc^o^-ro
^ne)
\,
t
CASNumber
83-32-9
51-28-5
100-02-7
132-64-9
1 2 1 - 1 4 - 2
606-20-2
84-66-2
7005-72-3
86-73-7
100-01-6
534-52-1
86-30-6
101-55-3
118-74-1
87-86-5
85-01-8
1 2 0 - 1 2 - 7
84.74-2
206-44-0
92-87-5
129-00-0
85-68-7
91.94-1
56.55-3
1 1 7 - 8 1 - 7 •
218 -01 -9
117 -84 -0
205.99-2
207-08-9
50.32-8
193-39.5
53-70-3
1 9 1 . 2 4 - 2
Acenaphlhene
2. 4-Dinitrophenol
4-Nitrophenol
Dibenzofuran
2. 4-Dinitroioluane
2, 6-OinitroMfuene
Oiethylphthalate
4-Chloropheny(-phenylether
Fluorene
4-N.iroaniline
4, 6-Oinitro-2-Methylphenol
N-Nnrosodiphenylamine ( 1 )
4-Bromophenyl-phenylelher
Hexachtorobenzene
Pentachlorophenot
Phenanihrene
Anthracene
Oi-n-ButylphthalaTe
Fluoranlhene
Benzidine
Pyrene
Bulylbenzylphthalate
3. 3'-0ichlorobenzidme
Benzo<a)Anihracene
bis<2-6thylhexy,}Phthatate
Chrysene
DJ-n-Ociyl Phihalale
Benzo<b)Ftuoranihene
Benzo^Huoranihene
Benzo<a)Pyrene
lndeno<1, 2. 3-cd|Pyrene
Oibenz(a. h)Anthraccne
Benro/n h ilPo'-"!"""
ug/l or^ig/(CirciSui
SJ£O u-
L^JS?\6^ba-eo^0O^^C>
^>rWS
5^0
\^0
[ -PJ&^D
^SD\^^yn>^0$JSt>p^O^^y^>"0u^
^>STi^^^1?^SD^^0^n^eo^S?^o;u?o »,-^ ^-?-' \
KQ^ne
iA
£nvtfonm«m«l Proi«ctiof\A^anCY. CLPS«mp(aMJnaga<nantOrftca,P.0.8o«818. Al«undri«. Virginia 22313 703/SS7-2490
Organics Analysis Data Sheet(Page 4)
Tentatively Identified Compounds
CASNumber
l
••>
3
d - ...
S.
K
7
R
1
m
11
17
TI
14
1';
Ifi
17
in
iq
7f
71 .
77
71
74
7R
7fi
77
7fl
7<)
in
Compound Nama
• : --.---
FractionRT or Scan
NumbarEalimatod
Concentration<ug/l o^iflg/kg^
§
^-Y
V7<
)^^-
01|
^ (^S
/')-^ -irp'^^a^y^Tv
s-
mr~-1\- o
^ g
___
v^^^^^^-'
L<! <c0- Q-
<I
LU LD
<C "
<
II—
_J
=3
gs
y^^^ry^^T
/^ ^
// s-
m ( /s/7~^^ l^ cy7
:?^' \^7yc
) • :s n^<^^g s-
0 <
X
®C
T^ ^
?3A -:
—i—
——
——
——
——
F0
WANT I TAT I ON REPORT FILE: EPAVOA1717
^ATA: EPAVOA17:7.TI)8/18/84 21:23:00iAMPLE: 77113-BLANKSUBMITTED BY: USTCO ANALYST: RJH
•.MOUNT=AREA(HGHT) •» REF. AMNT/(REF. AREA(HGHT)•» RESP.FACT)•;ESP. FAC. FROM AVERAGE OF WHOLE .RL
NAME•»»»
HSLHSL
HSLHSLHSL
HSLHSLHSLHSL
BROMOCHLORMETHANE (INTERAL STANDARD)P-D:FHJOROBENZENE (INTERNAL STANDARD)DICHLOROBENZENE-D5 (INTERNAL STANDARD)CHLOROMETHANEBROMOMETHANEVINYL CHLORIDECHLOROETHANEME1HYLENE CHLORIDEACROLEINACRYLGNITRILE1,1-DICHLOROETHYLENE1.1-DICHLOROETHANETRANS-1,2-DICHLOROETHYLENECHLOROFORM1.2-DICHLOROETHANEI,1,I-TRICHLOROETHANEACE I ONECARBON DISULFIDECARBON TETRACHLORIDEBROMODICHLOROMETHANE1 , 2-DICHLOROPROPAIMETRANS-1,3-DICHLOROPROPYLENETRICHLOROETHYLENEBENZENEDIBROKOCHLOROMETHANE1,1,2-TRICHLOROETHANECIS-1,3-DICHLOROPROPYLENE2-CHLOROETHYL VINYL ETHERBROMOFORMMETHYL ETHYL KETONEVINYL ACETATEMETHYL .ISOBUTYL KETONE1,2-DICHLOROETHANE-D4 (SURROGATE)QENZENE-D6 (SURROGATE)DIBROMOTETRAFLUOROETHANE (SURROGATE)BIS(PERFLUOROISOPROPYL)KETONE (SURROGATE)FLUOROBENZENE (SURROGATE)TETRACHLOROETHYLENE1,1,2,2-TETRACHLOROETHANETOLUENECHLOROBENZENE .ETHYLBENZENE2-HEXANONESTYRENE0-XYLENEM-XYLENE
NO47484950
NO .1234567
NAM
M/E130114117NOTNOTNOTNOT
E • •:- - M-BF
D-5TOU.P-BF
SCAN384699857
FOUNDFOUNDFOUNDFOUND
TOMOETH
JENEWHO
T132329
BENZYLBE-D8FLUO
I ME075317
OTRIFNZENE(SURRROBEN
REFI23
LUORI(SUR
OGATEZ.ENE
RRT1. 0001. 0001. 000
DEROG>(SU
MAAA
(SUFtROGAATE)
RROGATE)
ETHBBBBBB
TE)
AREA(HGHT)107878.440907.284791.
AMOUNT 7.TOT50.000 UG/L 9.6650.000 UG/L 9.6650.000 UG/L 9. 66
NO89
101112131415161718192021222324252627282930313233343536373839WU1-3435.4-5-6:7•'BW;0
M/ENOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOT
6584
NOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOT9895
SCANFOUND-FOUNDFOUNDFOUNDFOUNDFOUNDPOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
468617
FOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
8151036
TIME
15: 5921.05
27: 5135:24
REF
22
33
RRT
0. 6700.883.
0. 9511. 209
METH
A SBA BB
A BEA BB
A R E A ( H G H T )
379961.748701.
808970.491932.
AMOUNT
90.413 UG/L88.130 UG/L
100.295 UG/L88.741 UG/L
7.TOT
17. 4717. 03
19. 3817. 15
i. ; • 2 0 0
SCANS 1 TO 2809RIC DATA; EPABN1352 #1CALI: EPABN1352 #109/16/-84 22:36:08
SAMPLE; BLANK ABNCONDS.;RANGE; G 1-2800 LABEL; N 2, 2.0 QUAN: A 2- 3.0 J 8 BASE: U 26- 3
s S
5007:55
100015:50
150023:45
200031:40
250039:35
QUANTiTATION REPORT FILE: EPABN1352
DATA: EPABN1352.TI09/16/84 22:36:00SAMPLE: BLANK ABNSUBMITTED BY: ANALYST:
AMOUNT-AREA(HQHT) ». REF. AMNT/<REF.AREA(HGKT>» RESP.FACT)RESP. FAC. FROM AVERAGE OF WHOLE . R L
40 NAME1 •2 »3 »4 »5 •6 •
HSLHSL
37 HSL38 HSL39 HSL40 HSL41 HSL
D-4 1.4-DICHLOROBENZENED-8 NAPHTHALENE . . . . . . . . .6-8 ACENAPTHENED-10 PHENAN1HRENED-12 CHRYSENED-12 PERYLENF2-FLUOROPHENOL (SURROGATE)D-5 PHENOL (SURROGATE)D-5 NITROBENZENE (SURROGATE)2-FLUOROBIPHENYL (SURROGATE)2,4,6-TRIBROMOPHENOL (SURROGATt)D-14 TERPHENYL (SURROGATfc.)N-NITROSODIMETHYLAMINb2-CHLOROPHENOLPHENOLBIS (2-CHLOROETHYL) ElH£R1.3-DICHLOROBENZENE1.4-DICHLOROBENZENE1,2-DICHLOROBENZENEANILINE.BENZYL ALCOHOLBIS(2-CHLOROISOPROPYL)ETHERHEXACHI. OROETHANEN-NITROSODIPROPYLAMINENITROBENZENEISOPHORONE2-NITROPHENOL2.4-DIMETHYLPHENOLBIS(2-CHLOROETHOXY)METHANE2,4-DICHLOROPHENOL1,2,4-TRICHLOROBENZEN&NAPHTHALENEHEXACHLOROBUTADIENEP-CHLORO-M-CRESOL
HEXACHLOROCYCLOPENTADIENfc2,4,6-TRICHLOROPHENOL2-METHYLPHENOL4-METHYLPHENOLBENZOIC ACID4-C HLOR OANILINE2-METHYLNAPH1HALENE2-CHLORONAPHTHALENEDIMETHYL PHTHALATEACENAPHTHYLENE2,6-DINITROTOLUENEACENAPHTHENE
NO NAME47 2, 4-DINITROPHENOL48 4-NITROPHENOL49 2,4-DINITROTOLUENE50 FLUORENE
.51 - „ - ...4-CHLOROPHENYLPHENYL ETHER52 DIETHYL PHTHALATE53 4,6-DINITRO-2-METHYLPHENOL54 N-NITROSODIPHENYLAMIME55 1,2-DIPHENYLHYDRAZINE-56 4-BROMOPHENYL PHENYL ETH6R57 HEXACHLOROBENZENE .58 PENTACHLOROPHENOL59 PHENANTHRENE60 ANTHRACENE61 Dr-N-BUTYL PHTHALATE62 FLUORANTHENE63 HSL 2-4, 5-TRrCHLOROPHENOL .64 HSL 2 NITROANILINE65 HSL 3-NITROANILINE66 HSL DIBENZOFURAN67-HSL---4-^^•TROAI]<^LINE68 BENZIDINE69 PYRENE70 BENZYL BUTYL PHTHALATE71 BENZOCA)ANTHRACENE72 3.3'-DICHLOROBENZIDIN£73 CHRYSENE74 -B-IS-C2-ETHYLHEXYL) PHTHALATE75 DI-N-OCTYL PHTHALATE76 BENZO < B > FLUORANTHENE77 BENZO(K)FLUORANTHENE78 BENZO<A)PYRENE79 INDENOd. 2, 3-CD?PYRENF80 DIBENZO<A,H»ANTHRACENE81 BENZO<GHI>PERYLENE
NO M/E SCAN TIME REF RRT KFTH AREA(HSHT) AMOUNT 7.TOT
NO M/E SCAN TIME REF RRT MFTH AREA(HSHT) AMOUNT XTOT1 152 702 11 07 I 1.000 A BB 29547. 40.000 US/MI. 4.602 136 942 14 55 2 1.000 A BB 68417. 40.000 UG/ML 4.603 164 1279 20 15 3 1.000 A BB 8248. 40.000 UG/ML 4.604 188 1558 24 40 4 1.000 A BB 63272. 40.000 US/ML 4.605 240 2064 .32 41 5 1.000 A B B 31?97. 40.000 UG/ML 4.606 264 2318 36 42 6 1.000 A BB 19608. 40. 000 UQ/ML 4.607 112 483 7 39 1 0.688 A BV 71371. 89.408 U8/ML 10.278 99 675 10 41 1 0.962 A BB 73400. 77. 941 UG/ML 8.959 82 819 12 58 2 0.869 A SB 91124. 97.434 UG/ML 11.19
10 172 1162 18 24 3 0.909 A BB 157194. 112.693 UG/ML 12.9511 330 1434 S3 42 3 1.121 A BV 6864; 92. 135 UG/ML 10.5912 241 1877 29 43 5 0.909 A 3B 77955. 62.312 UG/ML 7.1613 NOT FOUND . . . .—14 NOT FOUND CV15 NOT FOUND16 NOT FOUND ,,17 NOT FOUND ••Ifl 1/IA •7ns 1-1 • i n 1 1 r^La—-ff--Pff————————-372-——————0. 240 UG/l-iL——0-OT~~ "-19 NOT FOUND 020 NOT FOUND21 NOT FOUND — — - - — -22 NOT FOUND23 NOT FOUND24 NOT FOUND25 NOT FOUND ________________ ______26-——83-——S6^——fJ: 4 5 2 0 . 923——ff»VB——————-4190.——————i—OSa- UG/I'lL:——0. 12——•—27 NOT FOUND28 NOT FOUND ..29 NOT FOUND30 NOT FOUND31 NOT FOUND32 NOT FOUND33 NOT FOUND" '34 NOT FOUND35 NOT FOUND36 NOT FOUND37 NOT FOUND38 NOT FOUND39 NOT FOUND40 NOT FOUND41 NOT FOUND42 NOT FOUND43 NOT FOUND44 NOT FOUND45 NOT FOUND46 NOT FOUND47 NOT FOUND43 NOT FOUND .49 NOT FOUND50 NOT FOUND51 NOT FOUND52 NOT FOUND53 NOT FOUND54 NOT FOUND55 NOT FOUND56 NOT FOUND
t
NO M/E SCAN TIME REf- RRT METH AREA(HSHT) AMOUNT 7.TOT57 NOT FOUND58 NOT FOUND59 NOT FOUND60 NOT FOUND61 NOT FOUND :62 NOT FOUND63 NOT POUND64 NOT FOUND65 NOT FOUND66 NOT FOUND
69 NOT FOUND i"i i70 NOT FOUND71 NOT FOUND • ' . . "72 NOT FOUND73 NOT FOUND '-\;74 NOT FOUND C-75 NOT FOUND 076 NOT FOUND77 NOT FOUND78 NOT FOUND79 NOT FOUNDSO NOT FOUND81 NOT FOUND
^
DUAL MASS SPECTRUM09/-16/'84 22; 35; 08 + 11:16SAMPLE! BLANK ABNCONDS.!ENHANCED (S 15B 2N 0T>
OftTA; EPABN1352 ft705CALI; EPABN1352 #1
BASE n/E: 57/ 150RIC: 30e..'- 15983.
0 0 2
DUAL MASS SPECTRUM09/16/-84 22s 36:00 + 13:4SSAMPLE; BLANK ABNCONDS.:ENHANCED <S 158 2N 0T>
DATA! £PABN1352 #869 BASE ri/E; 54/ 82CALI; EPABN1352 til RIC; 22. / 253.
55 6@ £5 78 75 80- I , , , . 1 , . , . I , . , , I , , , , I . , , . 1
DUAL MASS SPECTRUM09/16/84 22;3£:00 + 29-.43SAMPLE:. BLW ABN ,.CONDS.; 'ENHANCED <S 15B 2N 8T>
DATA; EPABN1352 i»1877 BASE M/E: 244/ 244CALI: EPABH1352 #1 RIC; 83S39./ 101563.
r 23008.
i l• , r ^ - 1' 'i "100
r^U^^ ^..^t ,T»J7l . 'i, ^f^it ^j -.<^^
Environments! Proleclion Agency. ' CLP Sample Management Office.P.0.fio«8)8. Alexandria. Virginia 22313 703/557-2490
Organics Analysis Data Sheet.(Pagel)
Sample Number
^U^-vJi-'P^^
Laboraiory Name: f^ ' ' -n rY>
Lab Sample ID No: _ "7 7 f I a) - &1 .1^
Sample Matrix:.
CaseNo: ^-(^-(^0
SmTQC Repon No:
Contract No:
. Data Release Authorized By: Date Sample Received: 6 I 1 ^ ! m
Volatile Compounds
Concentration: (Low) Medium (Circle One)
Date Arialyrpri- ..?i,/n, j
1 1 '
Percfnt Moisture' -
^• . /
pH 7.0
Percent Moisture (Decanted):
CASNumber
74-87-3
74-83-9
75-01-4
75-00-3
75-09-2
67-64-1
75-15-0
75-35-4
75-34-3
156-60-5
67-66-3
107-06-2
78-93-3
71-55-6
56-23-5
108-05-4
75-27-4
Chloromethane
Bromomethane
Vinyl Chloride
Chloroelhane
Mathylene Chloride
Acetone
Carbon Oisuldde
1, 1-Dichloroethene
1, 1-Dichloroeihane
Trans-1. 2-Oichloroeihene '
Chloroform
1 , 2-Dichloroflthane
2-Butanone
1 . 1 . 1-Trichloroelhane
Carbon Tetrachloride
Vinyl Acelate
Bromodichloromethane
ug/lori^r(CirdaC
/ O LA.
/o/o/o-</os<,5"
-HGi b5^/OS' >
/Kg
li/
CASNumber
79-34-5
78-87-5
10061-02-6
79-01-6
124.48-1
79-00-5
71,43-2..
10061-01-5
110-75-8
75.25-2
591-78-6
1 0 8 - 1 0 - 1
1 2 7 - 1 8 - 4
108-88.3
108-90-7
100-41-4
100-42-5
1 , 1 . 2 , 2-Teirachloroethane
\. 2-Dichloropropane
Trans-l, 3-Dichloropropene
Trichloroethene
Dibforriochloromelhane
1 , 1 . 2-Trichtoroethane
Benzene
cis -1 , 3-Dichloroprop^ne
2-ChloroethylvinYlelher
Bromoform
2-Hexanone
4-Melhyl-2-Penianone
Tetrachloroelhene
Toluene
Chlorobenzene
Ethyl benzene
Slyrene
To^al Xylenes
ug/t or iw(Circlet
'S'^t—
'^\
- ^ - -&
•S
^
-^-
/ 0
£'/O!^A^^S-5S-^
/^We)
/
D«t* flflporting Qua liters
Fof repoflinQ reiuitt 10 EPA, tha following results qualif'ers •r<
Addmonal flags or fooinoies«Kpl«ining fesi
dflfindion of •«ch flag must t— axJilioi
Valu* rt Ihe resurt it • value gr««ter irrn or ftqual 10 t^«
detection limil. r«po<1 irr vlu«
U Irtdicfllci cofTipound wat •nalyred for but nol d«i«cted
R«oo<i iht minimum d<l<cnon tifrni (r>f the w-npK wiih
(n» U <e.o.. 10U) txi»«l on rmcctwry concen (ration/
dilution •Cttoni, fThit 1C noi necetunly ih« incirufn«ni
d«tl«K:lion limit .) The (ootno(« »ho<Jk3 read. U-
Compound «v«C •nalyfd for but noi d«i»ci«d The
"umfaflf i« Irw minimum an«in«bl« 0«i«ction limit «o*
lit* &«mpl«
iitirnaied v«lu« Thif flag n LIndicitf •nwti^n »T..^
C In's tlao npplies 10 pesnc<d« p*ifam«><ar» w+^fe lh«
ideniidcaiion ITS b«an cor'firm<d bv GC/MS Singit
comporient pesiiCidti^lO ng/ul m the final Brtraci
should tK conl.ffTiBd by GC/MS
6 this 1iag is uiw3 wtien lha analvie i» found in ihfl blank
as well «s J tamole H indicales Dossible/pfobabit
blank coniamrnaiion aod wtfris Ihe data user to take
Bpp(ociiaie action
Oth«r 0<htr sptCifiC flags arKi looinolfls may be fffq"11'®^ 'o
piope'-'y delinc ir>e rsuttS M UWKJ. <h»v muH b« fully
Ocsct'fawd and such oetcnpiion BnachaO 10 th« ABta
EnvKonJn«nu( Protection Agency, CLP Sflmple M«nagern«nt On>c«.P.O.B«818. AI«K<ndrn.Virg>nr22313 703/557.2490
Organics Analysis Data Sheet(Page 4)
Tentatively Identified Compounds
CASNumbar
1
7
3
4.
*>
6
7
a1
10
n
17
13. ,
14
15
1 6
17
1 R
19
20
7-1-
22
23
24
2S
2fi
27
?R
71)
30
Compound Name
. ; ... ..-..-
FractionRT or Scan
NumborEstimated
Concentration^(ug/1 opCg/kgi^
0>'
(.V;
0
i'Y-^
-W -w
m^L
CO
-, /^^-^
f^^^l^
w^©
•-W^^^
o \
'
^
.^pT
rT-'ir^^si
-4^3
1 'T
n^J
'--
"—'/,
enI
1 L
Cl-
^^
(y^
ir ^
1 ^n
/,
''~r
-<p^^?^
©S
C
O0
—I
CT
• .. CD
nr^.
i T-4
G) n
•• T
^
f-<
CO •rt1
-r^-
oS
...."\
LJ
• ..
(n —i in
UJ
•^o
-o
o
Q^
<S* L
t'l O Q
^
iUANTITATION REPORT FILE: EPAVOA1724
WTA: EPAVOA1724.TI :^8/19/84 8:07:00iAMPLE: 77113-BLANKiUBMITTEn BY^. USTCO ANALYST: RJM . . . . .
»MOUNT=AREA * REF.AMNT/(REF.AREA)* RESP.FACT);ESP. FAC. FROM AVERAGE OF WHOLE .RL
NO NAME1 * BROMOCHLORtlETHANE (INTERAL STANDARD)2 * P-DIFLUOROSENZENE (INTERNAL STANDARD)3 * DICHLOROBENZENE-D5 (INTERNAL STANDARD)4 CHLOROMETHANE5 BROMOMETHANE6 VINYL CHLORIDE7 CHLOROETHANE8 METHYLENE CHLORIDE9 ACROLEIN
10 ACRYLONITRILE
1 1 1,1-DICHLOROETHYLENE12 1,1-DICHLOROETHANE13 TRANS-1,2-DICHLOROETHYLE^E14 CHLOROFORM15 1,2-DICHLOROETHANE16 1,I,1-TRICHLOROETHANE17 HSL ACETONE18 HSL CARBON DISULFIDE.19 CARBON TETRACHLORIDE20 BROMODICHLOROMETHANE21 1,2-DICHLOROPROPANE22 TRANS-1,3-DICHLOROPROPYLENE23 ' TRICHLOROETHYLENE24 BENZENE25 DIBROMOCHLOROMETHANE26 1,I,2-TRICHLOROETHANE27 CIS-1,3-DICHLOROPROPYLENE28 2-CHLOROETHYL VINYL ETHER29 BROMOFORK30 HSL METHYL ETHYL KE'l ONE31 HSL VINYL ACE1ATE32 •HSL • METHYL -ISOBUTYL KETONE"33 I,2-DICHLOROETHANE-D4 (SURROGATE)34 BENZENE-D6 (SURROGATE)35 DIBROMOTETRAFLUOROETHANE (SURROGATE)36 BIS(PERFLUOROISOPROPYL)KETONE (SURROGATE)37 FLUOROBENZENE (SURROGATE)38 TETRACHLOROETHYLENE39 1,1,2,2-TETRACHLOROETHANE40 TOLUENE
41 CHLOROEENZENE42 ETHYLEENZENE43 HSL 2-HEXANONE44 HSL STYRENE45 HSL 0-XYLENEt& HSL M-XYLENE
NO47484950
N01334567
NAM(
M/E130114117NOTNOTNOTNOT
M-BRD-5TOLUP-BR
SCAN384&99858
FOUNDFOUNDFOUNDFOUND
OMOBENZETHYLBEENE-D8OMO.FLUC
TIME13 0733 5329 19
^OTRI:NZEN
(5UR1ROBE
REF123
FLLE (ROGNZE
1.1.1.
JORIDESURRC
;ATE >:NE .(S
PRT000000000
E (SURROGATE)3GATE)
SURROGATE)
METH AREA(HGHT)A BB 97489.A BB 412319.A BE 370291.
AMOUNT50. 00050.00050.000
UG/LUG/LUQ/L
7.T9.9.9.
roT616161
NU
89
101112131415161718'192021222324252637282930313233343536373839404142tS4445^6\7485.950
M/ENOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOT
6584
NOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOTNOT9895
.- a<;AN- - T-IM&-FOUND .FOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
469 16:01618 21:07
FOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUNDFOUND
816 27:531035 35:22
REF-
22 .
33
——RRT-
0. 6710,884
0. 9511. 206
—M&t+t-———
A BBA BB ..
A BBA BB
—ARtAt H G H T 1 ~ '
362227..718271.
763931.463798.
AMOUNT
92.170 UG/L90-.4.10 UG/L
99. 792 UG/L88.154 UG/L
Y.TOJ
17. 711-7. 37
19. 1716;. 94