UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 6 Laboratory . Environmental Services Branch
10625 Fallstone Road, Houston, TX 77099 Phone: (281)983-2100 Fax: (281)983-2248
Final Analytical Report
13 J U L - ! PH U-3U
i .vi .•;•' •!*
Site Name Marion Pressure Treating
Sample Collection Date(s)~ 03/24/13 - 03/26/13
Contact- Bart Canellas (6SF-RL)
Report Date 06/11/13
Project # 13SF074
Work Order(s) 1303019 1303021 1303022
Analyses included in this report:
Chloride 300.0 (#) Nitrate - 353.2 Nitrite - 353.2 Sulfide 376.2
Report Narrative
Sample Management:
Metals ICP CLP Nitrate + Nitrite 353.2 Sulfate 300.0 Total Organic Carbon
686467
This report contains the chloride, nitrate, nitrite, nitrate-l-mtrite, sulfate, sulfide, and TOC are analyses done by the TCEQ Laboratory as well as the redigestion/reanalysis of sample 1303019-09 for metals by ICP. The semi-volatile and total metals data was previously reported.
Metals ICP:
Batch B3E0905:
Sample 1303019-09 was re-digested and analyzed due to prior QC problems. The prior analysis for the sample matrix spike and matrix spike duplicate had nearly all unacceptable recoveries except for the major analytes. Following the re-digestion and analysis the afifected analytes now fall within acceptable control limits. A corrective action (CA) was initiated and states a likely pipette malfimction as the reason for the initial QC failures.
MSl/MSDl: The sample concentration for iron exceeds the spike added concentration by a factor of foiu" or more and can not be reliably calculated.
005498
Report Narrative (cont'd)
TCEQ Data:
TOC-NPOCB:
Sample 1303019-06: The reproducibility of replicate sample injections was 17.94%, which is outside the acceptance limits of 10%. At low concentrations the variability of the measurement increases. The data is not likely afifected.
Sample 1303019-08: The reproducibility of replicate sample injections was 32.83%, which is outside acceptance limits of 10%. At low concentrations the variability of the measiu-ements increases. The data is not likely affected.
Sample 1303021-03: The reproducibility of replicates sample injections was 11.90%, which is outside the acceptance limits of 10%. At low concentrations the variability of measurements increase. The data is not likely afifected.
Sample 1303021-06: The reproducibility of replicate sample injections was 15.36%, which is outside the acceptance limits of 10%. At low concentrations the variability of the measurements increases. The data is not likely afifected.
Sample 1303021-07: The reproducibility of replicate sample injections was 16.39%, which is outside the acceptance limits of 10%. At low concentrations the variability of the measurements increase. The data is not likely affected.
N02:
Sample 1303019-08: The matrix spike recovery was 192%,which is outside of the acceptance limits. The precision of the matrix spike and the matrix spike duplicate was 73.7%, which is outside acceptance limits. The data is likely afifected.
Standard procedures for quality assurance and quality control were followed in the analysis and reporting of the sample results. The results apply only to the samples tested. This final report should only be reproduced in full.
Reporting limits are adjusted for sample size and matrix interference.
Lichard McMilliir ' ^ David Neleigh Region 6 Laboratory Manager Region 6 Laboratory Br^ch Chief
005499
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 6 Environmental Services Branch Laboratory
10625 Fallstone Road Houston, Texas 77099
Sample Receipt and Disposal
Site Name: Marion Pressure Treating Project Number: 13SF074
Data Management Coordinator: Christy Warren
Data Management Coc^nator Signature Date
Date Transmitted: C^ / ( ( / 1 ^
Please have the U.S. EPA Project Manager/OfiBcer call the Data Management Coordinator at 3-2137 for any comments or questions.
Please sign and date this form below and return it with any comments to:
Christy Warren Data Management Coordinator Region 6 Laboratory 6MD-HS
/ / Received by and Date
Comments:
The laboratory routinely disposes of samples 90 days after all analyses have been completed. If you have a need to hold these samples in custody longer than 90 days, please sign below.
Signature Date
Please provide a reason for holding:
005500
Environmental Protection Agency
Region 6 Laboratory 10625 Fallstone Road, Houston, TX 77099
Phone:(281 )983-2100 Fax:(281)983-2248
ANALYTICAL REPORT FOR SAMPLES
Station ID Laboratory ID Sample lype Date Collected Date Received
MW-1
MW-15
MW-15-D
MW-18
MW-21
MW-4
MW-5
MW-16
MW-2
MW-20
MW-20-D
MW-3
1303019-03
1303019-04
1303019-05
1303019-06
1303019-07
1303019-08
1303019-09
1303021-03
1303021-05
1303021-06-
1303021-07
1303021-09
Liquid
Liquid
Liquid
Liquid
Liquid
Liquid
Liquid
Liquid
Liquid
Liquid
Liquid
Liquid
3/25/13
3/25/13
3/25/13
3/25/13
3/25/13
3/25/13
3/24/13
3/26/13
3/26/13
3/26/13
3/26/13
3/26/13
11:25
8:56
8:56
13:55
11:48
9:30
10:30
8:45
13:00
9:39
9:39
10:25
03/26/13 09:10
03/26/13 09:10
03/26/13 09:10
03/26/13 09:10
03/26/13 09:10
03/26/13 09:10
03/26/13 09:10
03/27/13 09:20
03/27/13 09:20
03/27/13 09:20
03/27/13 09:20
03/27/13 09:20
ReportName: 1303019,1303021,1303022 FINAL06 11 13 1452 Page 1 of 27 005501
Environmental Protection Agency
Region 6 Laboratory 10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100 Fax:(281)983-2248
Lab ID: 1303019-09RE1 Batch: B3E0905 SampleType: Liquid
Metals by CLP ILM05.3 - ICP
Date Collected: 03/24/13 Sample Vol: 50ml
Station ID: MW-5
Sample Qualifiers:
Targets
Analyte (CAS Number) Result lig/L
U 107 U
u 8,390
U
u u
18,000 3,160 258 U
2,400 U
19,000
u u
Analyte Qualifiers
Reporting Limit
100 10.0 5.0 5.0 150 10.0 20.0 20.0 25.0 150 5.0
20.0 1,000 10.0 500 20.0 20.0
Dilution Prepared Analyzed Aluminum (7429-90-5) Barium (7440-39-3) Beryllium (7440-41-7) Cadmium (744043-9) Calcium (7440-70-2) Chromium (7440-47-3) Cobalt (7440-48-4) Copper (7440-50-8) Iron (7439-89-6) Magnesium (7439-95-4) Manganese (7439-96-S) Nickel (7440-02-2) Potassium (7440-09-7) Silver (7440-22-4) Sodium (7440-23-5) Vanadium (7440-62-2) Zinc (7440-66-6)
1 05/09/13 05/14/13
ReportName: 1303019,1303021,1303022 FINAL 06 11 13 1452 Page 2 of27 005502
Environmental Protection Agency
Region 6 Laboratory 10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100 Fax:(281)983-2248
Metals by CLP ILM05.3 - ICP - QuaUty Control
Batch: B3E0905 Sample Type: Liquid
Blank (B3E0905-BLK1) Prepared: 5/9/2013 Analyzed: 5/14/2013
Targets
ANALYTE Result AnalyteReporting ^g/L Qualifiers Limit
Aluminum Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron
Magnesiimi Manganese
Nickel Potassixmi Silver
Sodium
Vanadium Zinc
u u u u u u u u u u u u u u u u u
100
10.0
5.0
5.0
150
10.0
20.0
20.0
25.0
150
5.0
20.0
1,000
10.0
500
20.0
20.0
LCS (B3E0905-BS1) Prepared: 5/9/2013 Analyzed: 5/14/2013
Targets
ANALYTE Result AnalyteReporting Spike fig/L Qualifiers Limit Level
%REC %REC Limits
Aluminum Barium Beryllium Cadmium
Calcium Chromium
953
1,810
46.4
46.4
92,200
368
100
10.0
5.0
5.0
150
10.0
1,000
2,000
50.0
50.0
100,000
400
95.3
90.5
92.8
92.8
92.2
92.0
75-125
75-125
75-125
75-125
75-125
75-125
ReportName: 1303019,1303021,1303022 FINAL 06 11 13 1452 Page 3 of27 005503
Environmental Protection Agency
Region 6 Laboratory 10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100 Fax:(281)983-2248
Metals by CLP ILM05.3 - ICP - Quality Control
Batch: B3E0905 Sample lype: Liquid
LCS (B3E0905-BS1) Prepared: 5/9/2013 Analyzed: 5/14/2013
Targets (Continued)
ANALYTE Result AnalyteReporting Spike ^g/L Qualifiers Limit Level
%REC %REC Limits
Cobalt Copper Iron Magnesium Manganese Nickel Potassium Silver Sodium Vanadium Zinc
175
361
923
94,300
357
341
98,000
41.9
93,800
381
867
20.0
20.0
25.0
150
5.0
20.0
1,000
10.0
500
20.0
20.0
200
400
1,000
100,000
400
400
100,000
50.0
100,000
400
1,000
87.5
90.4
92.3
94.3
89.3
85.3
98.0
83.9
93.8
95.1
86.7
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
Source: 1303019-09RE1 Matrix Spike (B3E0905-MS1)
Prepared: 5/9/2013 Analyzed: 5/14/2013
Targets
ANALYTE Result AnalyteReporting Spike Som-ce ^g/L Qualifiers Limit Level Result %REC
%REC Limits
Aluminum Barium Beryllium
Cadmium Calcium
Chromium Cobalt
Copper Iron
Magnesium
Manganese
Nickel
964
1,940
46.2 .
46.6
99,700
364
171
364
16,800
97,500
591
333
100
10.0
5.0
5.0
150
10.0
20.0
20.0
25.0
150
5.0
20.0
1,000
2,000
50.0
50.0
100,000
400
200
400
1,000
100,000
400
400
14.0
107
0.04
1.1
8,390
18,000
3,160
258
0.4
95.0
91.5
92.4
90.8
91.3
90.9
85.6
91.0
NR '
94.3
83.3
83.2
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
»75-125
75-125
75-125
75-125
ReportName: 1303019,1303021,1303022 FINAL 06 11 13 1452 Page 4 of27 005504
Environmental Protection Agency
Region 6 Laboratory 10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100 Fax:(281)983-2248
Metals by CLP ILM05.3 - ICP - Quality Control
Batch: B3E0905 Sample lype: Liquid
Source: 1303019-09RE1 Matrix Spike (B3E0905-MS1)
Prepared: 5/9/2013 Analyzed: 5/14/2013 .
^Targets (Continued)
ANALYTE Result AnalyteReporting Spike Source %REC Hg/L Qualifiers Limit Level Result %REC Limits
Potassium Silver Sodium Vanadium Zinc
100,000
42.7
111,000
384
872
1,000
10.0
500
20.0
20.0
100,000
50.0
100,000
400
1,000
2,400
0.8
19,000
0.4
3.9
97.9
83.7
92.2
96.0
86.8
75-125
75-125
75-125
75-125
75-125
Source: 1303019-09RE1 Matrix Spike Dup (B3E0905-MSD1)
Prepared: 5/9/2013 Analyzed: 5/14/2013
Targets
ANALYTE Result AnalyteReporting Spike Source %REC ^g/L Qualifiers Limit Level Result %REC Limits RPD
RPD Limit
Aluminimi Barium Beryllium Cadmiimi Calcium Chromiimi Cobalt Copper Iron
Magnesiimi
Manganese Nickel
Potassium Silver Sodium
Vanadium
Zinc
974
1,940
46.6
46.9
101,000
367
172
366
16,900
98,400
592
339
101,000
43.0
112,000
386
877
100
10.0
5.0
5.0
150
10.0
20.0
20.0
25.0
150
5.0
20.0
1,000
10.0
500
20.0
20.0
1,000
2,000
50.0
50.0
100,000
400
200
400
1,000
100,000
400
400
100,000
50.0
100,000
400
1,000
14.0
107
0.04
1.1
8,390
18,000
3,160
258
0.4
2,400
0.8
19,000
0.4
3.9
96.0
91.8
93.0
91.6
92.2
91.7
86.2
91.5
NR
95.2
83.6
84.7
98.8
84.4
93.1
96.4
87.3
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
»75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
1.04
0.30
0.73
0.83
0.91
0.82
0.70
0.64
0.40
0.94
0.22
1.76
0.91
0.85
0.82
0.44
0.57
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
ReportName: 1303019,1303021,1303022 FINAL 06 11 13 1452 Page 5 of 27 005505
Environmental Protection Agency
Region 6 Laboratory 10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100 Fax:(281)983-2248
Results
from
TCEQ Laboratory 5144 E. Sam Houston Prkwy N.
Houston, TX 77015
ReportName: 1303019,1303021,1303022 FINAL 06 11 13 1452 Page 6 of27 005506
Environmental Protection Agency
Region 6 Laboratory 10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100 Fax:(281)983-2248
Batch: TCEQ
Batch: TCEQ
Miscellaneous Results (TCEQ)
Matrix: Liquid
Laboratory ID
1303019-03
1303019-04
1303019-05
1303019-06
1303019-07
1303019-08
1303021-03
1303021-05
1303021-06
1303021-07
1303021-09
Station ID
MW-1
MW-15
MW-15-D
MW-18
MW-21
MW-4
MW-16
MW-2
MW-20
MW-20-D
MW-3
Chloride
mg/L
41
50
51
30
8
9
26
8
14
14
11
Analyte Qualifier
Specific Method
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0
Date Analyzed
04/03/13
04/03/13
04/03/13
04/03/13
04/03/13
04/03/13
04/03/13
04/03/13
04/03/13
04/03/13
04/03/13
Matrix: Liquid
Laboratory ID
1303019-03
1303019-04
1303019-05
1303019-06
1303019-07
1303019-08
1303021-03
1303021-05
1303021-06
1303021-07
1303021-09
Station ID
MW-1
MW-15
MW-15-D
MW-18
MW-21
MW-4
MW-16
MW-2
MW-20
MW-20-D
MW-3
Nitrate as N
mg/L
<0.02
<0.02
<0.02
<0.02
<0.02
0.18
<0.02
<0.02
<0.02
<0.02
<0.02
Analyte Qualifier
Specific Method
353.2
353.2
353.2
353.2
353.2
353.2
353.2
353.2
353.2
353.2
353.2
Date Analyzed
03/28/13
03/28/13
03/28/13
03/28/13
03/28/13
03/28/13
04/05/13
04/05/13
04/05/13
04/05/13
04/05/13
ReportName: 1303019,1303021,1303022 FINAL 06 11 13 1452 Page 7 of27 005507
Environmental Protection Agency
Region 6 Laboratory 10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100 Fax:(281)983-2248
Batch: TCEQ
Batch: TCEQ
Miscellaneous Results (TCEQ)
Matrix: Liquid
Laboratory ID
1303019-03
1303019-04
1303019-05
1303019-06
1303019-07
1303019-08
1303021-03
1303021-05
1303021-06
1303021-07
1303021-09
Station ID
MW-1
MW-15
MW-15-D
MW-18
MW-21
MW-4
MW-16
MW-2
MW-20
MW-20-D
MW-3
Nitrate+Nitrite as N
mg/L
<0.04
<0.04
<0.04
<0.04 .
<0.04
0.18
<0.04
<0.04
<0.04
<0.04
<0.04
Analyte Qualifier
Specific Method
353.2
353.2
353.2
353.2
353.2
353.2
353.2
353.2
353.2
353.2
353.2
Date Analyzed
03/28/13
03/28/13
03/28/13
03/28/13
03/28/13
03/28/13
04/05/13
04/05/13
04/05/13
04/05/13
04/05/13
Matrix: Liquid
Laboratory ID
1303019-03
1303019-04
1303019-05
1303019-06
1303019-07
1303019-08
1303021-03
1303021-05
1303021-06
1303021-07
1303021-09
Station ID
MW-1
MW-15
MW-15-D
MW-18
MW-21
MW-4
MW-16
MW-2
MW-20
MW-20-D
MW-3
Nitrite as N
mg/L
<0.02
<0.02
<0.02
<0.02
<0.02
<0.02
<0.02
0.04
<0.02
<0.02
<0.02
Analyte Qualifier
TQ06
Specific Method
353.2
353.2
353.2
353.2
353.2
353.2
353.2
353.2
353.2
353.2
353.2
Date Analyzed
03/26/13
03/26/13
03/26/13
03/26/13
03/26/13
03/26/13
03/27/13
03/27/13
03/27/13
03/27/13
03/27/13
ReportName: 1303019,1303021,1303022 FINAL 06 11 13 1452 Page 8 of 27 005508
Environmental Protection Agency
Region 6 Laboratory 10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100 Fax:(281)983-2248
Batch: TCEQ
Batch: TCEQ
Miscellaneous Results (TCEQ)
Matrix: Liquid
Laboratory ID
1303019-03
1303019-04
1303019-05
1303019-06
1303019-07
1303019-08
1303021-03
1303021-05
1303021-06
1303021-07
1303021-09
Station ID
MW-1
MW-15
MW-15-D
MW-18
MW-21
MW-4
MW-16
MW-2
MW-20
MW-20-D
MW-3
Sulfate
mg/L
23
<5
<5
<5
<5
<5
<5
5
<5
<5
<5
Analyte Qualifier
Specific Method
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0
Date Analyzed
04/03/13
04/03/13
04/03/13
04/03/13
04/03/13
04/03/13
04/03/13
04/03/13
04/03/13
04/03/13
04/03/13
Matrix: Liquid
Laboratory ID
1303019-03
1303019-04
1303019-05
1303019-06
1303019-07
1303019-08
1303021-03
1303021-05
1303021-06
1303021-07
1303021-09
Station ID
MW-1
MW-15
MW-15-D
MW-18
MW-21
MW-4
MW-16
MW-2
MW-20
MW-20-D
MW-3
Sulfide
mg/L
<0.01
<0.01
<0.01
0.02
<0.01
<0.01
<0.01
0.13
<0.01
<0.01
<0.01
Analyte Qualifier
Specific Method
376.2
376.2
376.2
376.2
376.2
376.2
376.2
376.2
376.2
376.2
376.2
Date Analyzed
03/27/13
03/27/13
03/27/13
03/27/13
03/27/13
03/27/13
03/27/13
03/27/13
03/27/13
03/27/13
03/27/13
ReportName: 1303019,1303021,1303022 FINAL06 11 13 1452 Page 9 of 27 005509
Environmental Protection Agency
Region 6 Laboratory 10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100 Fax:(281)983-2248
Batch: TCEQ
Miscellaneous Results (TCEQ)
Matrix: Liquid
Laboratory ID
1303019-03
1303019-04
1303019-05
1303019-06
1303019-07
1303019-08
1303021-03
1303021-05
1303021-06
1303021-07
1303021-09
Station ID
MW-1
MW-15
MW-15-D
MW-18
MW-21
MW-4
MW-16
MW-2
MW-20
MW-20-D
MW-3
Total Organic Carbon, NPOC
mg/L
2
2
2
1
<1
<1
<1
15
<1
<1
<1
Analyte Qualifier
TQ07
TQ08
TQ09
TQIO
TQll
Specific Method
SM21 5310B
SM21 5310B
SM21 5310B
SM21 5310B
SM21 5310B
SM21 5310B
SM21 5310B
SM21 5310B
SM21 5310B
SM21 5310B
SM21 5310B
Date Analyzed
04/04/13
04/04/13
04/04/13
04/09/13
04/04/13
04/09/13
04/09/13
04/04/13
04/09/13
04/09/13
04/04/13
ReportName: 1303019,1303021,1303022 FINAL 06 11 13 1452 Page 10 of 27 005510
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Marion Pressure TreaUng (Company Superfund Site
Marion, LA
P r < ^ Coda; 1434262
No: 6432513-132943-0006
Lab: U ^ . EPARegbi 6 Laboslor^
Lab Contact: Ctutsty Wanen
Lai,PtKBier28i;.^2137-
Sampled
MW-15-0
ER-2
ER-3
MW.15
mv-i
' Matrix/Sampler
Water/Ryan
Gutti
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TtJ+Hg(35).T»W<g(35)
Tag/Preservatlva/Botttes
6-490255 (Ice tti 4 C,pH< 2
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tm03) t1 ) " i
1 W90270( lca lB4C.pM<2 | HN03y(1)
6-490226(!cB(o4C,pH<2 , HH03). 6-490227 (toe to 4 C, •
Station
Location
rjIW-15-0
ER-2
ER-3
(JlW-15
MW-5
\ Collected
0305001308:56
'. maizoia08:55
()3«a201308i00
03/75/201303:56
03/24E01310:30
For.LabUsa Only
pH<2HN03)(2)
MW.6
t/IW-7
1 Water/Mark
Kelly
Water/Mark
Kelly
Grab
ISrab
TM«Hg(35)
TMtHa(3S)
6^9f l230( lc8to4C.pH«2 HN03)(1)
6-!90236(lceto4C,pH<2 HN03)(1)
MW«
MW-7
03M2D1313:15.
03124/201,314;50
— 1 _
I Shipment for Case Coinpltts? N
SaiTiple(s) to be used lor Lab QC: MW.5
Ana ly^ Key: fM«Hg-Total Me^is + Hg
Samplea Tiansfened From Chain of Custody fl
Items/Rsason Rdnqutebad by i Dats
\Jk^ ttsms/Reason Relinquished By Data
i
RscEivadby Date
1
1
Time
a OS
> i . <^
22 e. 00 o <.»> a
!-: (a 2 o O to
fi-
X
^ I VO ^
Si o ts> VO . ^ VO o o
» i ON S
n
o g 3 ^
t&
005511
o
O
fro o H ^
t o n «> | v j
^
o ON i _ ^
»—» _ u>
^ 4^ l ^ I O
Page 1 of 1
USEPA CLP Generic COC (LAB COPY)
DataShfpped: 3/25/2013
CairierName: FedEx
AirbillNff. 7993 43191352
CHAIN OF CUSTODY RECORD
Marion Pressure Traattno Company Supetfimd Si!4.
Marlon, LA
Projecl Code: 1434252
Na:'6-032513-13504$-00p7 l ^ ^ ,U^ . , EPA;!:t$8i(»i S' l ibosloiy
lab Contatt OutstyWaiten
:UbPhonK2ai:9S3-2l37
Sample 9 ' Matrht^ampler' CoU. ! Method
" ^ - 2 ' ^
MW-6
MW-7
Water/Mark _ _ M y _
• Water/Mari'" Kely
WalBtf Marls' Kelly
Grab
Glab
Grab
Analysis/Turnaround
l;owA8N(35),lowABN(35)
LowABN(35).LoivA8N(35)
Lw/ABN(35),Lo«yABN(35)
' Teg/Prcserratne/Bottbis :
; 1 6^90332 {lcotO'4 0 , 6 - i
\ 450333 (IC8tO'4Ci'(2) 1
649(K28(IC81o4C),6.
49022:9 (I ts la 4 C) (2)
6-490234 (Ira to 4 q , 6- | , 490235(lcet<!,4iCl(2) j
1
SbUon Locatimi
ER^2
MW.€
WM7
Collected
0304/2013 08:55
03/24/201313:15
03B4)20W4:50
Fo rUbUse Only
,
i
—-I
"H
j _
TSilpmenl for Cass C a r r o t s ? N
I Special Instructions; i 'Samples Ttansfemtf From Chain q tCi tA i t ly <
:/Analysis Key: Low ABN=ljwr ABN
Tina I Jtems/Raasm J RelJrvqu^edBy ] Data ' ' (tecet/edby I ' D a a 1 T i i ta l
6 > o ( - ^ " p ^
§ • 5 O Ov
a t o
(O ^
£2 E. "vo a 00 o t>> a ' n
^ ^ 2 ° 0 w
P-SC
>fl 2 S I ^ P VO ^ 1 ^
t o o t o VO 4^ VO 00
lAJ m fD 2
dQ -
P i 5-
? a-. O g
? i
005512
o T3 O
z B l
• T O ei m n H - . UJ
o -»> t o - J
§ -* •—•
,_. U ) _ _ t
• u cy» K )
Page l o l l
USEPA CLP Generic COC (LAB COPY)
DateSH^ped: 3/25/2013 GarrififNama; FedEx AiiblNo: 7933 431S 9713
CHAIN OF CUSTODY RECORD
Marion Pressure Tnsalng.Comiiani/.SupeifUnd SIta
lil3iipn.LA
Project Cijda: 1434262
No:6432513-141207-0008: LdrU.Si EPA.R^lonS Ubojatbry
U b Coitacj: Oifls^'MVarten
tab:P)isne;281-983.2137
Sample It • Matrii/Sampler Coll. ; Method
Analyslsfrumaraund Tag/Presaivativii/Botllss StaUon Location
Collactttl^
MW-15-D Water/Ryaii Gutli
Grab LowABN(35),U)wABN(35) 6-4902&1jlcel».'(C),6-'490262 (Its to4.(;f(2)
MW.1SD i 03/25/201308:56
For Lab Use
ER-3
~MW-f5
Water/Ryan Guth
Water/Ryan Gu!h
Grab
""Grab'
Lov/ABN(3S).Lp\vAfiN(35)
L(wABM3S),UwrABN(35)
&4g033S(lcstg44:).6-48gH6(lcetb4q(2)
ER-3 0305001308:00
6-490266 (lcsti>4C),'8. <902S7(teMC)(2)
MW-15 0305/201308:56
, Shipment for Case Complota? N
Special Instnjtiions:
Ana^'sis Key. Low A B N = L I W S N ^
Items/Reason '• ReBraulstieilby Date 1 Ri
; /§Z^ .&'_'.
: Samplestransferred From Cltaln of Custody "
2(l:3:1-i-?i
13
§•5 a a\ a to to » 22 e! 00 o <.>! P
* z 2 o o ei
fi-X
•fl 2
^ I 2 H VO ^ 0 0 . L J - J I ^
to o (O VO -(^ VO 00
« 2 dQ • ® B
^ I ^ 3
O o ora
005513
Page 1 of 1
USEPA CLP Generic COC (LAB COPY)
OateStiipped: 3/250013
CanierName: FedEx
AirbSINo: 7993 4318 3976
CHAIN OF CUSTOOY RECORD
Maran Pressure Treating Conpsny Superfund Site
Marion, LA
Project Coda: 1434262
No:6432513-1S243»l010 Lab: U.S, EPARegjon 6 laboratory
Lab Contact: duisty Waiisn
labPhani>:281-£!8MI37
73 •S o a z B> 3 o
u> o u> o
Sample t MatriifSampler CoO. MaUiod
' m i - \ '\ ' Watei/Ryan ' Grab
Guth^
M W 5 i " " ' ' Wtita/ Josa ' Grab ' Fbres
' " l . i w - 4 " " Water/Mark KsUy
Anatysls/Tumaround
Grab
L0'.vABN(35), LowABNiaS)
L(rjvABK(35)7LTOABS(35
L«/ABN(35).l.owABH(35)
Tsg/Prcsorvathre/Bpttles
WS0272( lcat04O.8. 490273 (lcet04C) (2)
F : W 9 0 2 » ( t e t o 4 C ) , 6 -; 490297 (Its t D 4 Q (2)
fr490290(l«il»4C).6-1 430281 (lea to 4 C) (2)
i ^.-- - -
Sbtlbn
Location
MW-1
HW-Z)
' MV\M
, Cdllocied
03/2500131125
"" 0305(21131^48
0305001309:30
—
ForUbtJso' :
billy.
1
1
.
-U
• • 1 ; :
' ; • i ' • • i
' ShlpniDotfbf.CaseXonipuite? N |
ll Instructions;
^ A i i a ^ Key: low ABN^Low ABN
Samplos Tianstemd Ernn ChiiniOl Ciistody.|)
• f l pr o s o
t o 00
VO oo u> .1) o o
s is 0 0
0 0
I O t o *. 0 0
1—.
o Ov t o \ J \
^ a o 13 n JO K p
J^ ffi o
§
d - J
o VO VO
« dQ ^^« O 0 ON
»9
o-o »9 p ^
o ^
B
|2' o B
5 B
£ s J o B >
OQ A B
«<
• f l IS
OQ
u> O LP O to
u> o o to to •fl
> r o Ov
Hems/Reason Retimiulshedb'f Date
% {Lk/^3.%
'/»d by ^ " Date 7 1"tw Items/Reason i Re|(nu^hedBy ! Paia^ | Recejiral'by
. . . ^ • ^ J r l ^ ^ ^ l Oo^ i ^ ^ O T
•&• UJ
o ^ to l/l ^ to
005514
Pago 1 of 1
USEPA CLP Conoric COC (LAB COPY)
OateShtpped: 305/2013
CairierKams: FedEx
AlrbilNo: 7993 43137630
CHAIN OF CUSTODY RECORD
fteton Pressuns Treating Cmipaiir Superfund SIta
Marion, LA
P n ^ Code: 1434262
No: 6432513-130552-0005 L ^ U.S. EPAf tagb i erlabOtatpiy
Lab Coitact ChrislyWanen
LabPlien9:281JB834l3»"
Sampio # Matrix/Samplor
• f l e i
f t
70 a o a. z 3
UJ O UJ o
UJ
o UJ o t o
o UJ o t o t o
> r o o\
Mlft^S Water/Mark Kelly
ColL fJethod^
Grab
Analysis/Turnaround
low ABN(35), Low ABN(35), Low A8N(3S). Low ABNtSS), l ow ABN(35).
low/\BN(35)
Tag/Pressrvative/Botlles Statlan Location
Collected
6^90220 (lea to 4,0).$-490221 (IC8 lo4C),-8. 490222 (Ice to 4 q , 6-490223 (ha to 4 0 ,6-490224 (lc« 194 C), 6-490225 (Ice ta 4 G) (6)
For Lab Usa <>tily
MW'S 03/24/201310:30
Ssmpie(s) 10 be used lor Lab QC: MW-5
Shipmenlfbr Case Completg? N
SaiTiptas Transferred From C M i ) o fCus tody*
Analysis Key: Low ABM'lov/ ABN
Items/Reason ; Relinquished by : Oato _Receivedby : Date Time Items/Reason ' ReSnquished By Date T Received by Date i Tons
I ,-_
4 - i -
G H ^ T ^ ' - o^<^' GioX fei-?^)
•fl §"5 P Ov a to
!S "fl oo p '
"vo a 0 0 o UJ a * n ^% 2 ° O (S
fi-X
•flg 2 H VO ^ 0 0 , UJ ^ I ^
t o o t o VO .U VO 0 0
dQ •
® i * I
o g 2 ^ O B
Lft UJ
to u< -J to
005515
Pagel o f l
USEPA CLP Generic COC (LAB COPY)
DateShJpped:3O5O013 Cairiertfame: FedEx AWlWa 7393 43187537
CHAIN OF CUSTODY RECORD
Marlon Pressure Treaiirig^Company Superfund Site
Marion. LA
Project Code; 1434262
No:6W2513-1S1107-0009 lab>U.S. EPA Region eiaboait ty
Ub^onlact Christ^ Warren
LabPhoiie:.28l433^2'i37
?0 •§ o a. Z
UJ o u>
o
UJ O UJ o t o
UJ
o UJ o t o t o
•fl g 00 ^ CT I—
Sample tt MatrixISamplor CoU. Method
AnalyBls/Tumaround Tag/Pmeivadve/Botlles Station Location
Collected
MW-1 Water/Ryan Gulh
Gtab I N02SD4CU35),TOCN03TN(35),S. (35)
MVJ-18 Water/ Ryan Gulh
MW-21 Water/Joss Flares
Grab
Grab
N02 S04 CL(35). TOC N03 TN(36). S-(35)
&490274(lceta4C).6-430275(lcaiO4C.pH<2 H2S04), 6490277 (pH> 3
w/NaQH,ZnOAe,lCB4C)(3)
&49028D(icela4C),6-43028i(ltst()4C,p}f<2 H2SO4).W902a3(pM»9
«IN30RZnQAc: la4Q(3)
MW-I 0305001311:25
l iW^ia i 03^001313;55
For lab Use \ Only I
N02 S04 CL(35). TOC N03 TN(35), S-(35)
8-430^8<(lcs»4C),$-490299(lceia4C,pH<:2 H2SO4),6.4a)30ttpH>g '
usrNsOH.ZnOAc.lcs4C)(3)
MW-21 03/KOI513.11:48.
Special Instructions:
j Shiprnent forCase C ^ l e l B ? H
Samples TnnsIsmiS FnniCiialn oi Custoity^
i Analysis Kay; N02 S04 a=Nilt iM, Sullale. ChkirMe. TOC HS3 TN^TQC, NUrala, Nitrats^itite. 3^=$uaide
iby"
C o c i ^ p2AMfl «(/t i y ^ i ^ )
• f l I ' ' S o o B Ov <K t o
> v '•'<
K •fl 00 03
^ a 00 o UJ s
2 o O IS
fi-
il ^ ^ VO ' ^ o o . L.J ^
to o KJ VO 4k VO OO
« 2 dQ ^• ® B
^ I ? &•
o g
0 \ UJ o • -
t o L») ^ t o
005516
70 ft •a o a
UJ
o UJ
o UJ
o o to
UJ
o UJ o to to
> r •fl g o ^-• — ' t - ^
^ UJ o ^ t o Ln ^ t o
Page 1 of 1
USEPA CLP Generic COC (LAB COPY)
Da-£Shipped:3O3S013
CarrterNams; FedEx
AirtiilMo: 799343195259
1 Samples , Matrix/Sampler
M W - i M ; Waiei/Ryan i Gulh
Co l l Method
Grab
! r/IW-15 i water/Ryan ' Gtab Gulh
fX'W-4 Water/Mark ' Grab KeBy i
CHAIN OF CUSTODY RECORD
MaiTO PresSBB Trealiig Company Supeifural Site
Maiton,lA
Project Code. 1434262
' Analysis/Turnaround ; Tao/Presorvative/Bottlas |
, N 6 2 5 0 4 0 ( 3 5 ) , TOC N 6 3 T N P 5 ) , S - | 6-49Q2S3(lcoto4C).6-(35) i 490254(lceto4C,pH<2 1
H2S04), 6-490256 (pH>9w/ NaOH, ZnOAc; lea 4 q ( 3 )
NO2S04CK35),T0CNO3TN(35).S- 9-49(1266 (Ice to 40 ) . 6- ; (35) j 490ffi9(lcel64C.jiH<,2 1
! H2S04). 6^90271 (pH> 9 tt/N30H.aOAclca4C)(3)
NO2SCMCl(35).T0CNO3TNt35).S- W90232( lca (»4O.e- , |35) 490293 (Ice to 4 C P H < 2 |
H2S04), 6-460295 (pH> 9 , i w/MaOH.ZnOAclca4C)t3)
; 1
Station
Location
MW15:( r
MW.,15
MW^
No:6r032513-120446-q004
late U.S.-EPA Ragbn 6 Labostoiy
l a b Coitlad: Qvisly Waiten
lab Phone; 281.9SJ.2137
Collected
' 03O6O01309;S6
, 0305/3)13 0 8 i 6 i
ForLabUss '••
1 O"" / '
1
i
03O5Q013J19.'30 < i 1 i
Special Instniaions
Analysis Key: N02 S04 Cl=Nitrite. Sulfate'Cliiorae; TOC_N03 TN^TOC] Hitr3te7NiJatet>iilrite.S-='SulfidB"
i^oelvedby ' Dale t m e i ltems/Reason~ Relini;uished By { Date
Shiprnent (or C a a ComplelB? N
Samptes transferred From ( ^ i n of Custody #
Items/Reason Relinquished by Daa Received by Date Tine
o o 0 Ov n to
- i i , Lr, to ^rt 00 g ~vo a 00 o UJ f3 • z 2 o
fi-ffi
•flg
VO ^ 00 , UJ ~J I ^
SJ o S> VO . U VO 00
dQ ^•
® B ^ I
o g
005517
TO n
T3 O
z Cl 3 f t
UJ
o UJ
o UJ
o UJ o to UJ
o UJ o to to
n o l i
USEPA CLP Generic COC (LAB COPY)
DateShipped: 306/2013
CerriertJeme' FedEx
AirbJlINo: 7993 4329 0374
Sampled Matrix/Sampler Co l l . Method 1
ER-4 Water/Ryan Grab | Gulh '
MW.16 Water/Ryan Grab Guth i
MW-18 Water/Ryan Grab Guth
CHAIN OF CUSTODY RECORD
Marion Pressure Treating Company Superfund Site
Marten, L«
Project fiixtti; 1434262
Analysis/Tumaround
LowABN(35). L0WABN(35)
lowABN(35).LowABN(35)
LowASNp5),lowABN(35)
— •
6-490338 (Its 104 Q , 6-490339 (lea to 4 0 ( 2 )
W90260( Ice to4e) ,6 -490261 (Ice lb 4 C) (2)
6^60278 ( t o to 4 0) . 6 , 490279 (Ice to 4 0 ( 2 )
Station Location
ER-4
' _ MW-16
MW-18
No: 64325l^'i328564()11 U b : U.S? EP« R e s M e Labdralbry
LebCantactiChttstyWarien
•Lab,Rione'.28l4sj-2f3f
Collected
\ 0306/2013 07;55
1 0306/201308:45
i 1 0305001313:55
For t a b Use
1
1 >
i
Special Insbuctkxis:
• f l
§"5 P ov f t t o
>lv <-n t o •_. 00 ( ?
"vo a 00 o UJ 13 < ft
2 o fi-ffi o ..* o a
B
O B
5 B
Shipment for .C^Coinpteto? Y
SampteeTiaitsfeitred Froth Chain of CCslody4
Analysis Key: low ABN=low ABN
- J • o to o
t o VO .U VO 00
dQ
o
ON
^ 3
^ a o B >
VQ
n
a
O
o
•fl g IB Ov
OQ ^ ft t—»
00 UJ
o — t o Ln ^ t o
005518
Pa^lofl
USEPA CLP Generic COC (LAB COPY)
OsteShipped: 3060013
CanierNaiia: FedEx
AirbiKNo: 7993 4328 4379
CHAIN OF CUSTODY RECORD
Marion Pressure Treating Company Superfund SHe
Marion, LA
ProjeaCode: 1434262
Nb :e432613-140647JOa i4
lab: U.'s:£PA Region 6 laboratory
. lab Contectv Christ/Warren
lab Phone; 281 •8a-2t37
?<3 ft •a o
z a 3 ft
U J
o
Sample tl Matrix/Sampler CoU. I Method
ER.4 Water/ Ryan Gulh
Grab
MW-1
M W i l
M W T "
Water/ Ryan i Grab
Gulh - _
Water/ R ^ n Grab
Gulh •
Water/Jose
Flores
WaterfMark" KsUy
Analysis/Turnaround
TMtHg{35)
Tag/Pieservative/BotUes Station Location
CoUected
Grab
Grab
TM+Hg{q5)
™*H3(35) '
~TM+Hg(35r
6-490340 (Ice to 4 C,pH< 2 I HN03)(1)
ER-4 0306001307:55
TMTHg(35)
6-490276 (Ice l b4C .pH< 2
I Hl«)3)ffl i "6430282( l<at i )4C,pH<2"
j HN03H1)
MW-1
"MW-IT
0305001311-.25
0305001313:55
6-190300 (Ice to 4 C,pH< 2 HN03)(1)
i 6490234 (Ice to 4 a p H < 2 •• HN03)(1)
MVV-21
' MW-4
0305001311:48
0305001309:30
For Lab Use Only
Special InstniclKns.
, /^nahj'Sis Key: THHHg=To|al Mejals t Hg
Shipment for Case Complete? Y
- I
Samples Transferred Fism Chain ot Custody t
• f l
§"5 a ov ft to
> N <-*> t o • r t 0 0 isV
"vo a 00 o UJ 3 > ft • z 2 °
P-ffi
• f lg
VO ^ 0 0 , UJ - J I ^ to o S> VO .U VO 0 0
dQ q*
p i B
^ 3
o g s SI
U J
o UJ o to
U J
o U J o to to
> r o Ov
• f l O Q > - ' f t • -
Items/Reason Relinquished by Date !
V ^ ^ 3- ) ' -1 ^ : t f f i i f L j i i v l
led by Date Tin» | i Items/Reason Relinquished By
MiJM, -)/!^L)ii : - .
Date Reoahed by [ Date Tune
VO UJ O ^ • < , ^
to Ol -J to
005519
Page 1 of 1
USEPA CLP Generic COC (LAB COPY)
DateShlpped: 3/260013
CatrjerName: FedEx
AirbllNo: 7993 43281630
CHAIN OF CUSTODY RECORD
Marioi Pressure TteaCng Company Superfund SSe
Marion, LA
Project Code: 1434262
No: 6r032613-1<l32164015 Lab; t L l E P A Reglotiie Idloiatory
iabConlaqu Christy Warren
LabPhbrie:'281-8S3>2137
TO f t
T3 O
a
UJ o UJ o so
UJ
o UJ o to U J
o UJ o to to •Tl
•fl g [o Ov
OQ ^ f t • -to — O UJ o ^ to Ln •^ to
Sampto 1}
MW-16
MW-2
MW-20
Matrix/Sampler
Water/Ryan ' Guth
Water/Ryan Guth
Water/Jose ,
CoU Method
Grab.
Grab
Grab
Anatysls/Tumaround
Flores
TM*H8t35)
" " t H i S g ^ ' "
"TMitigissT
MW-2frO Water/Joss Flores
Grab Tf.1+Hgi35)
MW-3 Water/Ryan ! Grab _ ^ ^ Gulh I
TM*Hg(35)
Tas/Pieservattve/Botflss
6490264 (Ice M C ; p H < 2 JfN03){1) _ _
8-490K4 (Ice ttVc. pH'< 2 HN03)(1)^
Station Locatlan
' I W 1 8 "~
CoDectsd : ForLabUss Oiily
MWr2
0306001308:45
0306001313.-00
e490306(lceti>4C.pH<2 HN03)(1)
MW.20 03 /a /»13 09:39
6490312(lcBlo4C,pH<2 HN03)(;t)
MW-20-D 0306001309:39
6-490318 (Ice b 4 C , p H < 2 MW-3 HN03)(1)
03O6O01J102S
^ Shipment to.r Case Complete? Y
. Special Instructions: : Samples Traosferred FromChabi of Custody #
• Analysis Key. TM->Ha=Tolal Metals • Hg
Items/Reason ReEnquished by (}ate
• f l
o o B Ov ft to >v <-n
^ a 00 o UJ p
^ ^ 2 » O ta
fi-ffi
•fl g ^ I 0 0 -VO r ^ OO , U J - J I ^ to O f O VO * > VO 0 0
/ ^ rt
dQ N^»
o p o\ ^ ^
o-o ^ » rt' o ^
w i. 1 o B 5 ffi B
£
1 {^ o B
n
«<
005520
•fl p
OQ f t t o
Page l o l l
USEPA CLP Generic COC (LAB COPY)
OateShipped; 306/2013
Carriert^ame: FedEx
Airi)iIINo; 7993 4329 4818
CHAIN OF CUSTODY RECORD
Marion Pressure Treating Company Superfund S
Merloni L/\
Ptoiect Code: 1434232
No: 6-032$13-13S320-0013 lab: U.S. EPA RegibnB l^oratory
U b Cotttecl: CI\rIsty:Wanei)
Lab Phone; 281-883^13;!
Sampte S '. MatrixISampler
f t t 3 O
a. Z p> 3 f t
UJ
o UJ
o UJ
o o to
UJ
o UJ o to to
MW-16 Wats/Ryan Gulh
MW.20
MW-20-O
Water/Jose Flotes
Water/ Jose Ftores
ColL Jlethod
GtST"
Grab
Grab
Atutysfs/Turnaround
N02 S04 CL(35). TOC N03 TN(35). S-(35)
taglPressrvatlve/Botlles
6490282 (Ics to 4 C j " . ? " " 490263 (Ice to4C,'PH< 2 H2S04), 6490265 ( p h > 9
WNaOH.ZnOAeilce4C){3)
Stalioii Locatian
Coltected
MW-16
N02 S04 a(35), TOC N03 TN|35). S-(35)
N02 S04 CL(35), TOC N03 TN(35), S-(35)
6490304 (Ice to 4 0 . 6 -4303b5( loeta4C,pH<2 H2S04), 6430307 (pH> 9 |
v</NaOH.ZnOAc, l ta40(3y | ~ 6480310 ( lce lo4 0 . 6 - " ^
490311( lceto4C.pH<2 ] H2SO4).6M90313(pH>3 !
w/NaOH,ZnOAc,lcs4C)(3)
MW-20
0306001308:45:
For Lab Use Only
0306001309:33
MW-20.D 0 3 0 6 0 0 1 3 0 9 3
Shipment for Case Complete? Y
Special Instructions;
Arialysirkey. N02 SCMClSi i r i te. Sr^teJCWoMe, TOC" N03"tN»f0Ci"Nitate, Kiirate^Nil'rile. S-°SulWe "
. Samples Transferred From Chahi of Custody It
Items/Reason Re&nqutshed by Date Received by Date i Time Relinquished By ; Dale ; Recei»edby Date T i ihe j
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Page 1 of 1
USEPA CLP Generic COC (LAB COPY)
OaieShipped; 3050013
CanierName; FedEx
Ai-bWo; 7993 4327 9050
CHAIN OF CUSTODY RECORD
Marian Pressure Treating Company Siqierfiind Site
Marian,'LA
Prajea Code: 14342S2
No:6-032613-144342-0016
Leh U:S. EPA Regteii.e^labpratey
Lab'Conlaci; Chris;y:Vyarren
labPlio>is:'2S1.r983.2137
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Tes/Preser\'ativ^i>ttIos
6490320 jlce 10 4 .0 .6 -490321 (Icslo 4 : 0 (2)
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' Station ^ i l lacted Location
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Special Insmrclions;
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Items/Reason , Reliiquished by ; Date, i Re<SKBdby : Date \ Tiqo | Itttns/Beason ' ^ I n q u i s t i e d ' ^ ^ Dais R e t e W b y
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Page i of 1
USEPA CLP Generic COC (LAB COPY)
DateShipped; 306/2013
CarrierName: FedEx
AirbiTNo: 7993 4327 6051
CHAIN OF CUSTODY RECORD
Marion Piessure Tiealuis Co/npsny Supertund.Site
Mariptt,bA
Project Code: 1434262
N o : 6W2613-14S400-0017
leb: US. EP/V Region€tabt^toTy
Leib-Goniacc Chtety Vt^rren
Lab PMite: 281^9^2137
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Water/Ryan Guth
Grab N02 S04 CL(35), TGC N03 TN(35), S-(35)
WaiaifRyan Gulh
Grab N02 S04 Cl(35). TOC N03 TN(35). S-(35)
6490322 (Ice 104 C), 6- , 490323 (ICS.Is.4G.pH< 2
H2S04).&49t)32S(pH>3 w/NaOH,ZnQA£,lce4C){3)'
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0306001313:00
&4903 t60 i» te4O,6 - ' 490317(lceto4C,pH<2 H3S04),&43d319(pH>9
w/N30H,a;0Actc64Q(3)
fJW-3 0306001310^
Special Instructions;
Analysis Key: N02S04"CL=Niirite~Sullate;Chloride, tOCNOiTMSrOCTNiiate,Ntoie^Nit i te,S-'^lWe""
Shipment for Case Complete? Y
! Samples Transferred From Chain of Custody S
lteiT\yReason Reiftiqu'ished by , Dais jie^eiittd by | Date j Time ItemslReason Relinquished By , Dote Recebtdby. T - — ~ \ " ' ' '
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USEPA CLP Generic COC (LAB COPY)
DateShlpped: 3060013 CamerNarrie: FedEx AirbilINo; 7993 4329 2463
CHAIN OF CUSTODY RECORD
MarionPressutetreaiihg Company Superfund Site
Marion, LA
Projed Code; 1434262
No: S:032613-1342S9:«012
lab;U.S:'EPA'Reg^n S tabiratory
Lab {Jqnla^Ghi&ty Warren lab:Plniie;28V;9mi37
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StaUon Location
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Sariipiea Tt^hsferrul-I^t'oii^ljhaln of Ciiietody4
Items/Reason : Re&iquished:by Date ;
o[jt^'p^A^'-~l o'c. Cnoifk^^j
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005524
Page t o l l
USEPA CLP Generic COC ( U S COPY)
DateSh%;!SJ; 3/23/2013
CarrisiNsni: FedEx
Aiblfi^o: 7933 8502 4219
CHAIN OF CUSTODYRECORD
Marioo Piessute Treaftig Cffinpany Superfund Sle
MartoiilA
Prc)>i9 Cods 1434262
No:64327tM54131.'«D1S LGb: IXSL EP/VR^cii'« Lsbiiiatoiy
U iCa i t ac t Christy Waiten
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Environmental Protection Agency
Region 6 Laboratory 10625 Fallstone Road, Houston, TX 77099
Phone:(281 )983-2100 Fax:(281 )983-2248
Notes and Definitions
TQl 1 The reproducibility (%CV) of replicate sample injections of AA53041 was 16.39%, which is outside the acceptance limits of 10%. At low concentrations the variability of the measurements increases. The data is not likely affected.
TQIO The reproducibility (%CV) of replicate sample injections of AA53040 was 15.36%, which is outside the acceptance limits of 10%. At low concentrations the variability of the measurements increases. The data is not likely afifected.
TQ09 The reproducibility (%CV) of replicate sample injections of AA53038 was 11.90%, which is outside the acceptance limits of 10%. At low concentrations the variability of the measurements increases. The data is not likely affected.
TQ08 The reproducibility (%CV) of replicate sample injections of AA53011 was 32.83%, which is outside the acceptance limits of 10%. At low concentrations the variability of the measurements increases. The data is not likely affected.
TQ07 The reproducibility (%CV) of replicate sample injections of AA53009 was 17.94%, which is outside the acceptance limits of 10%. At low concentrations the variability of the measurements increases. The data is not likely afifected.
TQ06 The matrix spike recovery was 192 %, which is outside of the (80-120%) acceptance limits. The precision (%RPD) of matrix spike and matrix spike duplicate was 73.7%, which is outside of the (20%) acceptance limits. The data is likely afifected.
A This sample was extracted at a single acid pH.
HTS Sample was prepared and/or analyzed past recommended holding time. Concentrations should be considered minimum values.
ABN Acid Base Neutrals (Semivolatile Compounds)
AES Atomic Emission Spectrometer
BS Blank Spike
CVAA Cold Vapor Atomic Absorption
DCB Decachlorobiphenyl
ECD Electron Capture Detector
GC Gas Chromatograph
ICP Inductively Coupled Plasma
ISTD Intemal Standard
LCS Laboratory Control Sample
ReportName: 1303019,1303021,1303022 FINAL 06 11 13 1452 Page 26 of 27 005526
Environmental Protection Agency
Region 6 Laboratory 10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100 Fax:(281)983-2248
MS Mass Spectrometer
MS/MSD Matrix Spike/Matrix Spike Duplicate
NA Not Applicable
NPD Nitrogen Phosphorous Detector
NR Not Reported
PCB Polychlorinatedbiphenyl
RL Reporting Limit
RT Retention Time
TCLP Toxicity Characteristic Leaching Procedure
TCMX Tetrachloro-meta-xylene
U Undetected
VOA Volatile Organic Analysis
# Out of QC limits
Initial pressure in air analyses is the pressure at which the canister was received in psia (pounds per square inch absolute pressure).
The pH reported for Volatile liquid samples was tested using a 0-14 pH indicator strip for the purpose of verifying chemical preservation.
The statistical software used for the reporting of toxicity data is ToxCalc 5.0.32, Environmental Toxicity Data Analysis System 1994-2007 Tidepool Scientific Software.
ReportName: 1303019,1303021,1303022 FINAL 06 11 13 1452 Page 27 of 27 005527
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