XRDUG Seminar IV...DMSNT - [LaB6 11-9-06 - LaB6 660d std 11 -9-06 Edit Zoom An3iysls Took Window...

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XRDUG Seminar IV Edward Laitila 2/1/2007

Transcript of XRDUG Seminar IV...DMSNT - [LaB6 11-9-06 - LaB6 660d std 11 -9-06 Edit Zoom An3iysls Took Window...

Page 1: XRDUG Seminar IV...DMSNT - [LaB6 11-9-06 - LaB6 660d std 11 -9-06 Edit Zoom An3iysls Took Window File: LaB6 11-9-06, ID: LaB6 660a std 11-9-06 Date: 11/11/88 09:15 step : 0.0150 Cnt

XRDUG Seminar IV

Edward Laitila 2/1/2007

Page 2: XRDUG Seminar IV...DMSNT - [LaB6 11-9-06 - LaB6 660d std 11 -9-06 Edit Zoom An3iysls Took Window File: LaB6 11-9-06, ID: LaB6 660a std 11-9-06 Date: 11/11/88 09:15 step : 0.0150 Cnt

Figure 1 Inserting a Peak Manually

Page 3: XRDUG Seminar IV...DMSNT - [LaB6 11-9-06 - LaB6 660d std 11 -9-06 Edit Zoom An3iysls Took Window File: LaB6 11-9-06, ID: LaB6 660a std 11-9-06 Date: 11/11/88 09:15 step : 0.0150 Cnt

Figure 2 Profile Function from Manual Peak Insertion

Page 4: XRDUG Seminar IV...DMSNT - [LaB6 11-9-06 - LaB6 660d std 11 -9-06 Edit Zoom An3iysls Took Window File: LaB6 11-9-06, ID: LaB6 660a std 11-9-06 Date: 11/11/88 09:15 step : 0.0150 Cnt

Figure 3 Profile Function After Convergence

Page 5: XRDUG Seminar IV...DMSNT - [LaB6 11-9-06 - LaB6 660d std 11 -9-06 Edit Zoom An3iysls Took Window File: LaB6 11-9-06, ID: LaB6 660a std 11-9-06 Date: 11/11/88 09:15 step : 0.0150 Cnt

Figure 4 Deleting Peaks

Page 6: XRDUG Seminar IV...DMSNT - [LaB6 11-9-06 - LaB6 660d std 11 -9-06 Edit Zoom An3iysls Took Window File: LaB6 11-9-06, ID: LaB6 660a std 11-9-06 Date: 11/11/88 09:15 step : 0.0150 Cnt

Figure 5 Inserting Peaks with Minimal Features

Page 7: XRDUG Seminar IV...DMSNT - [LaB6 11-9-06 - LaB6 660d std 11 -9-06 Edit Zoom An3iysls Took Window File: LaB6 11-9-06, ID: LaB6 660a std 11-9-06 Date: 11/11/88 09:15 step : 0.0150 Cnt

Figure 6 Profile Functions Manually Fitting Kα2

Page 8: XRDUG Seminar IV...DMSNT - [LaB6 11-9-06 - LaB6 660d std 11 -9-06 Edit Zoom An3iysls Took Window File: LaB6 11-9-06, ID: LaB6 660a std 11-9-06 Date: 11/11/88 09:15 step : 0.0150 Cnt

Figure 7 Five Fingers of Quartz

Page 9: XRDUG Seminar IV...DMSNT - [LaB6 11-9-06 - LaB6 660d std 11 -9-06 Edit Zoom An3iysls Took Window File: LaB6 11-9-06, ID: LaB6 660a std 11-9-06 Date: 11/11/88 09:15 step : 0.0150 Cnt

Figure 8 Example of Low Intensity Peak Near a High Intensity Peak

Page 10: XRDUG Seminar IV...DMSNT - [LaB6 11-9-06 - LaB6 660d std 11 -9-06 Edit Zoom An3iysls Took Window File: LaB6 11-9-06, ID: LaB6 660a std 11-9-06 Date: 11/11/88 09:15 step : 0.0150 Cnt

Figure 9 Figure 8 Zoomed To Observe Low Intensity Peaks - Initial Peak Insertions

Page 11: XRDUG Seminar IV...DMSNT - [LaB6 11-9-06 - LaB6 660d std 11 -9-06 Edit Zoom An3iysls Took Window File: LaB6 11-9-06, ID: LaB6 660a std 11-9-06 Date: 11/11/88 09:15 step : 0.0150 Cnt

Figure 10 Curve Fit with Sigma = 1

Page 12: XRDUG Seminar IV...DMSNT - [LaB6 11-9-06 - LaB6 660d std 11 -9-06 Edit Zoom An3iysls Took Window File: LaB6 11-9-06, ID: LaB6 660a std 11-9-06 Date: 11/11/88 09:15 step : 0.0150 Cnt

Figure 11 Curve Fit with Sigma Deselected

Page 13: XRDUG Seminar IV...DMSNT - [LaB6 11-9-06 - LaB6 660d std 11 -9-06 Edit Zoom An3iysls Took Window File: LaB6 11-9-06, ID: LaB6 660a std 11-9-06 Date: 11/11/88 09:15 step : 0.0150 Cnt

Figure 12 Effects of Step Size on Profile Function SS = 0.03° 2θ

Page 14: XRDUG Seminar IV...DMSNT - [LaB6 11-9-06 - LaB6 660d std 11 -9-06 Edit Zoom An3iysls Took Window File: LaB6 11-9-06, ID: LaB6 660a std 11-9-06 Date: 11/11/88 09:15 step : 0.0150 Cnt

Figure 13 Effects of Step Size on Profile Function SS= 0.005° 2θ