XRD ANALYSIS REPORT - Paladin Geo · Report For: 2 13832 Santa Fe Crossing Dr. Edmond Ok...

XRD ANALYSIS REPORT CLIENT: Confidential

Andrew Sneddon/Manager

Report For:

1 13832 Santa Fe Crossing Dr. Edmond Ok 73013|405.463.3270 Innovative Geochemistry Services

Summary: 1. Conducted multiple Phase ID XRD Powder Diffraction on 4 Separate Wells

I. Well 1: 12 Samples

II. Well 2: 14 Samples

2. Quantitative Analysis Conducted Using Reitveld Refinement Modeling (Rwp ≈10% ±1)

3. Determine Mineralogy of all samples, including an in-depth 10-20 (deg ϴ) .01 deg step @2 deg/min clay analysis

4. Analysis conducted by Andrew Sneddon and Dr. Fei Meng. Detailed report compiled by Andrew Sneddon for:

XRD-ANALYSIS RESULTS REPORT SUMMARY

Report For:


Measurement conditions

X-Ray 40 kV , 15 mA Scan speed / Duration time 10.0000 deg/min

Goniometer MiniFlex 300/600 Step width 0.0200 deg

Attachment ASC-6 Scan axis Theta/2-Theta

Filter None Scan range 3.0000 - 70.0000 deg

CBO selection slit - Incident slit 1.250deg

Diffrected beam mono. None Length limiting slit 10.0mm

Detector Receiving slit #1 13.0mm

Scan mode CONTINUOUS Receiving slit #2 13.0mm

Qualitative analysis results

Phase name Formula Figure of merit Phase reg. detail DB card number

Quartz low Si O2 0.375 User (COD) 1011097

Calcite C Ca O3 1.045 User (COD) 4502441

Muscovite Al2.88 Fe0.12 K O12 Si3 1.712 User (COD) 9015386

Kaolinite Al2 O9 Si2 1.620 User (COD) 9014999

Pyrite Fe S2 2.746 User (COD) 5000115

Phase name Formula Space group Phase reg. detail DB card number

Quartz low Si O2 152 : P3121 User (COD) 1011097

Calcite C Ca O3 167 : R-3c,hexagonal User (COD) 4502441

Muscovite Al2.88 Fe0.12 K O12 Si3 15 : C12/c1,unique-b,cell-1 User (COD) 9015386

Kaolinite Al2 O9 Si2 9 : C1c1,unique-b,cell-1 User (COD) 9014999

Pyrite Fe S2 205 : Pa-3 User (COD) 5000115

GENERAL MEASUREMENT CONDITIONS

Report For:


Refinement

Measurement range: 3.0000-70.0000deg Refinement range: 3.0000-70.0000deg (1.34 A)

Number of refined parameters: 81

Phase name Atomic coords # of indep. reflns

Quartz low Fractional coords 27

Calcite Fractional coords 19

Muscovite Fractional coords 201

Kaolinite Fractional coords 146

Pyrite Fractional coords 12

Rwp = 10.20% S = 1.3070

Report For:


XRD MEASUREMENT PROFILE 9660-9990

Well 1 (9660-9990)

Report For:


1

1

Report For:


Genesis GeoChem LabsInnovative Geochemistry Services REPORT OF X-RAY DIFFRACTION ANALYSIS13832 Santa Fe Crossing Dr.

Edmond, Ok 73013 (RESULTS REPORTED AS WT.% OF CRYSTALLINE PORTION)Ph: (405)-563-3270

www.ggclab.com Well:

Client: New Gulf Resources File No: NG7000Project: Unknown Date: 07/31/15 Area: West Texas Analyst: Andrew Sneddon and Dr. Fei Meng

Sample Type: Shale, Eagle Ford Analysis Type: Bulk and Clay

Well

Flyswatter 1A Top Bottom Kaolinite Ill ite/Mica Calcite Dolomite Quartz K-Feldspar Plagioclase Pyrite Clays Carb. Other

9660 21 29 7.9 0 40.8 0 0 2 50 7.9 42.8

9680 32.3 5.2 8.7 0 52.3 0 0 1.6 37.5 8.7 53.9

9710 34 13 8.5 0 42.2 0 0 1.7 47 8.5 43.9

9710 14.9 27 19.9 0 35.4 0 0 2.7 41.9 19.9 38.1

9770 16.2 14.7 20.6 0 45.6 0 0 2.9 30.9 20.6 48.5

9800 23.8 39 10 0 26.9 0 0 0 62.8 10.0 26.9

9830 9.2 43 17.9 0 27.9 0 0 2 52.2 17.9 29.9

9860 8.4 41 21 0 29.9 0 0 0 49.4 21.0 29.9

9890 8.9 36 19.3 0 35.7 0 0 0 44.9 19.3 35.7

9920 11.5 43 14.5 0 28.6 0 0 2.91 54.5 14.5 31.51

9960 8.4 27 31 0 32 0 0 1.23 35.4 31.0 33.23

9990 1.6 12 21.5 0 60.7 0 0 4 13.6 21.5 64.7

Flyswatter 1A

OTHER MINERALS _TOTALS_Depth CARBONATES

Well No. 1 (example)

Well No. 1 (example)

Report For:


0 20 40 60 80 100

9660

9680

9710

9740

9770

9800

9830

9860

9890

9920

9960

9990

DEP

TH (

FT)

FLYSWATTER 1AMINERALOGY (%)

Quartz

Calcite

Pyrite

Vclay

0% 20% 40% 60% 80% 100%

9660

9680

9710

9740

9770

9800

9830

9860

9890

9920

9960

9990

FLYSWATTER 1ACLAY DATA (%)

Kaolinite

Illite/Mica

Report For:


0.0

10.0

20.0

30.0

40.0

50.0

60.0

70.0

9660 9680 9710 9740 9770 9800 9830 9860 9890 9920 9960 9990

Wt.

%

Depth (ft)

Flyswatter A1- Mineralogical Breakdown

Quartz low(%) Calcite(%) Kaolinite(%) Muscovite(%) Pyrite(%)

Well 1

Report For:


Pie Charts representing the mineralogy of Well 1 samples 9660-9990:

52%

9%

32%

5%

2%

9680


40%

8%21%

29%

2%

9660


42%

9%

34%

13%

2%

9710


35%

20%15%

27%

3%

9740


Report For:


45%

21%

16%

15%

3%

9770


27%

10%

24%

39%

9800

Quartz low(%) Calcite(%) Kaolinite(%) Muscovite(%)

28%

18%9%

43%

2%

9830


30%

21%8%

41%

9860


Report For:


36%

19%9%

36%

9890


29%

14%

11%

43%

3%

9920


61%21%

2%12%

4%

9990


32%

31%

9%

27%

1%

9960


Report For:


XRD MEASUREMENT PROFILE (9740-10130)

Well 2 (9740-10130)

Report For:


2

Report For:


Genesis GeoChem LabsInnovative Geochemistry Services REPORT OF X-RAY DIFFRACTION ANALYSIS13832 Santa Fe Crossing Dr.

Edmond, Ok 73013 (RESULTS REPORTED AS WT.% OF CRYSTALLINE PORTION)Ph: (405)-563-3270

www.ggclab.com Well:

Client: New Gulf Resources File No: NG7001Project: Unknown Date: Area: West Texas Analyst: Andrew Sneddon and Dr. Fei Meng

Sample Type: Shale, Eagle Ford Analysis Type: Bulk and Clay

Well

Iron Duke 1 Top Bottom Kaolinite Montmorill ite Il l ite/Mica Calcite Dolomite Quartz K-Feldspar Plagioclase Pyrite Marcasite Clays Carb. Other

9740 8 0 12.1 53.8 0 26 0 0 0 0 20.1 53.8 26

9770 19.5 0 33.3 8.7 0 35.5 0 0 2.9 0 52.8 8.7 38.4

9800 2.4 0 47 7.9 0 42.7 0 0 0 0 49.4 7.9 42.7

9830 8.9 0 39.1 11.4 0 30 0 0 11 0 48 11.4 41

9860 15 0 34.2 12.1 8 30.3 0 0 0 0 49.2 20.1 30.3

9890 10.8 0 46.9 10.9 0 29.1 0 0 2.22 0 57.7 10.9 31.32

9920 9.6 0 50.7 15.3 0 22.5 0 0 1.93 0 60.3 15.3 24.43

9950 9.6 0 16 32.1 12 27.4 0 0 2 0 25.6 44.1 29.4

9980 3.5 0 31 33.8 0 31.6 0 0 0 0.3 34.5 33.8 31.9

10010 12.1 0 27 27.2 0 32.1 0 0 2 0 39.1 27.2 34.1

10040 1.28 0 45.6 19.7 0 28.2 0 0 5 0 46.88 19.7 33.2

10070 12.3 0 10.1 39.1 0 36.9 0 0 1.5 0 22.4 39.1 38.4

10100 10.3 16.1 14 30.8 0 28.2 0 0 0.3 0 40.4 30.8 28.5

10130 0.7 0 23 38 0 37 0 0 1.7 0 23.7 38.0 38.7

Iron Duke 1

OTHER MINERALS _TOTALS_

07/31/15

Depth CARBONATES

Well #2

Well #2

Report For:


0 20 40 60 80 100

9740

9770

9800

9830

9860

9890

9920

9950

9980

10010

10040

10070

10100

10130

DEP

TH (

FT)

IRON DUKE 1MINERALOGY (%)

Quartz low

Calcite

Pyrite

Marcasite

Dolomite

Vclays

0% 20% 40% 60% 80% 100%

9740

9770

9800

9830

9860

9890

9920

9950

9980

10010

10040

10070

10100

10130

DEP

TH (

FT)

IRON DUKE 1CLAY DATA (%)

Kaolinite

Illite/Mica

Montmorillite

Report For:


0

10

20

30

40

50

60

9740 9770 9800 9830 9860 9890 9920 9950 9980 10010 10040 10070 10100 10130

Wt.

%

Depth (ft)

Iron Duke 1- Mineralogical Breakdown

Quartz low(%) Calcite(%) Kaolinite(%) Muscovite (%) Pyrite(%) Marcasite Dolomite Montmorillite

Well 2

Report For:


Pie Charts Representing the Mineralogy of Well 2 (9740-10130)

26%

54%

8%12%

9740


36%

9%19%

33%

3%

9770


43%

8%2%

47%

9800


30%

11%9%

39%

11%

9830


Report For:


31%

12%15%

34%

8%

9860

Quartz low(%) Calcite(%) Kaolinite(%) Muscovite (%) Dolomite

29%

11%11%

47%

2%

9890


22%

15%

10%

51%

2%

9920


28%

32%10%

16%

2% 12%

9950

Quartz low(%) Calcite(%) Kaolinite(%)

Muscovite (%) Pyrite(%) Dolomite

Report For:


32%

34%

3%

31%0.3%

9980


Muscovite (%) Pyrite(%) Marcasite

32%

27%12%

27%

2%

10010

Quartz low(%) Calcite(%) Kaolinite(%) Muscovite (%) Pyrite(%)

28%

20%1%

46%

5%

10040


37%

39%

12%10%

2%

10070


Report For:


28%

31%11%

14%

0.3 % 16%

10100


Muscovite (%) Pyrite(%) Montmorillite

37%

38%

1%

23%

1%

10130


XRD ANALYSIS REPORT - Paladin Geo · Report For: 2 13832 Santa Fe Crossing Dr. Edmond Ok...

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