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1- Scanning Electron Microscope BACK JSM-6380 LA The jsm-6380 la is a high-performance, scanning electron microscope with a high resolution of 3.0NM. The intuitive pc interface allows the instrument to be easily operated with a mouse only. Its 5 axis, computer controlled, specimen chamber can accommodate a specimen of up to 8-inches in diameter and its standard automated features include auto focus/auto stigmator, auto gun (saturation and alignment), and automatic contrast and brightness. Other features include eucentric stage and a super conical lens . The jsm-6380LA is used in many and varied applications

Transcript of sciences.ksu.edu.sasciences.ksu.edu.sa/.../files/imce_images/jhzlmkhtbr.docx · Web viewThe...

Page 1: sciences.ksu.edu.sasciences.ksu.edu.sa/.../files/imce_images/jhzlmkhtbr.docx · Web viewThe TEM-1011 is a high performance, high contrast, 100kV TEM with excellent imaging, easy-to-use

1-Scanning Electron Microscope BACK

JSM-6380 LAThe jsm-6380 la is a high-performance, scanning electron microscope with a high resolution

of 3.0NM. The intuitive pc interface allows the instrument to be easily operated with a mouse

only. Its 5 axis, computer controlled, specimen chamber can accommodate a specimen of up

to 8-inches in diameter and its standard automated features include auto focus/auto stigmator,

auto gun (saturation and alignment), and automatic contrast and brightness.

Other features include eucentric stage and a super conical lens. The jsm-6380LA is used in

many and varied applications with several options that increase its versatility and can be

expanded to an analytical sem by the addition of optional eds and/or wds

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2-Transmission Electron Microscope (TEM)

The TEM-1011 is a high performance, high contrast, 100kV TEM with excellent imaging, easy-to-use instrument with an acceleration voltage of 40 to 100kV. TEM has been used in all areas of biological and biomedical investigations because of its ability to view the finest cell structures. It is also used as a diagnostic tool in hospital pathology labs. Apart from Biological sample polymer and Nano-materials can be analyzed. The magnification of TEM 1011 is raging from 50X - 600000X

The new Gathan™ software included with the JEM-1011 offers a set of tutorials and user guides designed to help beginning microscopists familiarize themselves with the microscope, but also allows experienced users to explore and understand advanced features.

3-TEM Tissue Processing Machine

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النافذ االلكترونى للمجهر البيولوجية العينات تدوير جهازيقلل * مما بشرى تدخل دون الكيميائية بالكواشف والنباتية الحيوانية لالنسجة التلقائية بالمعالجة يقوم

للعينات والطمر والتجفيف والترويق التثبيت عمليات فى تستخدم التى الخطرة الكيميائية للمواد التعرضالمختبر داخل السالمة عوامل يحسن .مما

الوقت * توفير من يزيد مما محددة زمنية برامج وفق تلقائى .يعمل

من * أثر تحضير يمكن حيث عالية انتاجية واحد 32ذات وقت فى عينة .

. الكميائية* كاشف انخفاضاستهالك حيث من التكاليف في يوفر

Features

Automatic processing of tissue

Automatic processing of tissue minimizes contact with hazardous reagents, provides reproducible results, increases time savings and improves user safety in the laborator.

Closed processing chamber

Closed processing chamber with fume extraction system reduces chemical exposure for the user.

High throughput

Up to 168 EM samples per run ensures high throughput, which results in increased efficiency and time savings in the laboratory.

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4-TEM Strainer Machine

النافذ االلكترونى للمجهر الدقة فائقة القطعات صباغة جهاز

الدقة يقوم * فائقة القطعات مما بصبغ بشرى تدخل دون المشعة الكيميائية الكواشف باستخدام تلقائيا عوامل يحسن مما تلقائيا القطاعات هذه بغسيل يقوم وايضا الخطرة الكيميائية لمواد لهذه التعرض يقلل

المختبر داخل .السالمة

الوقت * توفير من يزيد مما محددة زمنية برامج وفق تلقائى .يعمل

من * أثر تحضير يمكن حيث عالية انتاجية واحد 25ذات وقت فى قطاع .

. الكميائية* كاشف انخفاضاستهالك حيث من التكاليف في يوفر

Features

Safer working conditions

Minimum user contact with reagents provides safer working conditions in the laboratory.

More efficient laboratory operation

60 runs per one set of Ultrostains, and short washing cycles result in faster, more efficient laboratory operation.

Cost savings

Low reagent consumption results in cost savings.

The Leica EM AC20 automatic contrasting system for ultrathin sections ensures minimum user contact with reagents and reduced reagent consumption.

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5-AutoChem Analyzer

AutoChem Analyzer(Automated catalyst characterization system)Type of Analyses

1. Temperature-Programmed Desorption (TPD)2. Temperature-Programmed Reduction (TPR)3. Temperature-Programmed Oxidation (TPO)4. Temperature-Programmed Reaction5. Pulse Chemisorption6. BET Surface Area 7. Langmuir Surface Area8. Total Pore Volume

- كيم أوتو تحليل جهاز( المحفزات( لتوصيف آلي جهاز

: المتاحة التحاليلالحرارة (.1 برمجة مع اإلمتزاز )TPDفكالحرارة .2 برمجة مع )TPR( اإلختزالالحرارة .3 برمجة مع )TPO( األكسدةالحرارة .4 برمجة مع التفاعلالنبضي .5 الكيميائي اإلمتزازبطريقة .6 المساحة سطح BETتقديربطريقة .7 المساحة سطح Langmuirتقديرالكلي .8 المسامات حجم تقدير

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6-Thermal Analysis

Thermal Analysis Differential Scanning Calorimetry (DSC) Applications

1. Curing rate, dynamic measurements2. Separation of the glass transition and post curing 3. A comparison of the glass transition measured by DSC, TMA and DMA4. Influence of curing conditions (temperature, time)5. Curing of a powder coating6. Determination of the glass transition of CF-reinforced resins7. Quality assurance in the production of printed circuit boards8. Determination of crystallinity

الحراري التحليلالتفاضلي الحراري )DSC(المسح

التطبيقاتديناميكية .1 قياسات المعالجة، نسبةالمتأخرة .2 المعالجة و الزجاجي التحول فصلالمقاسبطرق .3 الزجاجي التحول DSCمقارنة ، TMA وDMA4.( زمن ( حرارة، المعالجة ظروف تأثيرالطالء .5 مسحوق معالجةالمقواة .6 الصمغية للمواد الزجاجي التحول تقديرالمطبوعة .7 الدوائر لوحات إنتاج في الجودة ضمانالتبلور .8 قياسدرجة

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7-Thermo-gravimetric analysis (TGA)

Thermo-gravimetric analysis (TGA)Applications

1. Mass changes on heating a thermoset (Polymer)2. Content determination: moisture, filler and resin content3. TGA analysis of a phenol-formaldehyde condensation reaction4. Determination of the fiber content of composites by thermo-gravimetric analysis5. PE, compositional analysis by TGA6. Curing and Decomposition of an Amino Resin7. Thermal Degradation of BHET8. Influence of the Heating Rate on Moisture Content Determination, an O/W Cream 9. TGA of Sugar and Starch

الوزني الحراري )TGA(التحليل

التطبيقاتالحرارية .1 البولمريرات خالئط تسخين عند الكتلة تغيير2. : الصمغية المادة نسبة و الحشوة نسبة الرطوبة، نسبة كمي تقديرفورمالدهايد .3 و فينول تكثيف لتفاعل الوزني الحراري التحليلبا .4 الخالئط في األلياف نسبة الوزني تقدير الحراري لتحليل5. - الوزني الحراري بالتحليل إيثلين البولي تركيبة تقديراألمينية .6 األصماغ تكسير و معالجةلمادة .7 الحراري BHETالتكسيرالماء .8 و الزيت كريمات في الرطوبة نسبة تقدير على التسخين سرعة تأثيرالنشأ .9 و للسكر الوزني الحراري التحليل

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8-Thermo-mechanical Analyzer (TMA)

Thermo-mechanical Analyzer (TMA) Applications

1. Determination of the linear expansion coefficient2. Determination of the glass transition by means of the expansion curve3. Determination of the softening temperature of thin film4. Determination of the glass transition from bending measurements5. Investigation of the curing reaction using bending measurements6. A comparison of the glass transition measured by DSC, TMA and DMA7. Glass transition temperature and z-axis thermal expansion by TMA according ICP-TM-6508. Printed circuit boards, influence of fiber orientation on expansion behavior9. Determination of softening by penetration measurements by TMA10.Delamination of Printed Circuit Boards11.Expansion and Decomposition of the Polymer Used to Encapsulate a Blowing Agent

الميكانيكي الحراري )TMA(التحليل

التطبيقاتالخطي .1 اإلمتداد معامل تقديراإلمتداد .2 منحنى بطريقة الزجاجي التحول تقديرالرقيقة .3 لألغشية التليين حرارة تقديرالتقويس .4 قياسات من الزجاجي التحول تقديرالتقويس .5 بقياسات المعالجة تفاعل دراسةالمقاسبطرق .6 الزجاجي التحول DSCمقارنة ، TMA وDMAمحور .7 حسب الحراري اإلمتداد و الزجاجي التحول حرارة الحراري با zدرجة لتحليل

طريقة حسب ICP-TM-650الميكانيكياإلمتداد .8 سلوك على األلياف إتجاه تأثير المطبوعة، الدوائر لوحاتحسب .9 اإلختراق بقياس التليين درجة الميكانيكي تقدير الحراري التحليلعن .10 الخارجي الغشاء المطبوعة إزالة الدوائر لوحاتالفعالة .11 المواد لتغليف الخارجي البوليمر طبقة تكسير و إمتداد

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9-Dynamic mechanical Analyzer (DMA) الديناميكي الميكانيكي (DMA) التحليل

Dynamic mechanical Analyzer (DMA) Applications

1. Determination of the glass transition by DMA2. The frequency dependence of the glass transition3. The dynamic glass transition4. Master curve construction and mechanical relaxation spectrum5. Curing measured by DMA6. Change of the shear modulus during the curing reaction7. Frequency dependence of the shear modulus during a curing reaction8. Dynamic mechanical analysis of PET

9. Characterization of PTFE by DMA and DSC10. Crystallization and melting of PCL/PTHF copolymers11. Comparison of DSC and DMA measurements12. The frequency dependence of the glass transition13. Comparison of DSC and DMA measurements of polyurethane14. DMA measurements of a chloroprene elastomer15. Measurement of the amplitude dependence of the shear modulus of NR elastomers

1.(

التطبيقاتبا .1 الزجاجي التحول الديناميكي قياس الميكانيكي )DMA(لتحليلالزجاجي .2 التحول و التردد بين العالقةالديناميكي .3 الزجاجي التحولالميكانيكي .4 اإلسترخاء طيف و الرئيسي المنحنى على الحصولالديناميكي .2 الميكانيكي بالتحليل المعالجة )DMA(قياسالمعالجة .3 تفاعل خالل الجز معامل تغييرالمعالجة .4 تفاعل خالل الجز معامل و التردد بين العالقةتيريفثاالت .5 إيثلين للبولي الديناميكي الميكانيكي )PET(التحليلالتيفلون .6 المسح )PTFE(توصيف و الديناميكي الميكانيكي بالتحليل

التفاضلي الحراريالمشتركة .7 البولميرات إنصهار و PCL/PTHFتبلورالميكانيكي .8 التحليل و التفاضلي الحراري المسح قياسات مقارنة

الديناميكي الزجاجي .9 التحول و التردد بين العالقةالميكانيكي .10 التحليل و التفاضلي الحراري المسح قياسات مقارنة

يوريثان للبولي الديناميكي

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المطاطية .11 الكلوروبرين لبوليمرات الديناميكي الميكانيكي التحليل قياساتلبولميرات .12 الجز معامل مدى المطاطية NRقياسات

10- Gel Permeation Chromatography (GPC)

Gel Permeation Chromatography (GPC)Application

1. Molecular weight Determination of Polymers2. Determination Branching of Polymers

الهالم .5 نفاذ )GPC(كروماتوغرافيا

التطبيقاتللبوليمرات .1 الجزيئي الوزن قياسالبوليمرات .2 تفرع قياسدرجة

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11- Jeol Resonance ECX500II NMR spectrometer المغناطيسي النووي الرنين جهاز

Applications

1. To determine 1D Experiments (1H, 13C, DEPT, NOE)2. To determine 2D Experiments (COSY, NOESY, HMBC,

HMQC, HSQC)3. To determine Solid-state NMR (CPMAS, DDMAS)

Notes Liquid and Solid-state NMR experiments are performed on our Jeol Resonance ECX500II

NMR spectrometer operating at Jeol Delta v5.0.4.

Multinuclear instrument equipped with a sample changer (24 positions) and autotune probe. 

Used for routine 1H (including COSY, HSQC, HMBC), 13C, 31P, 11B and 19F. 

Solid-state NMR analyses cover a wide range of applications that cannot be addressed by

liquid-state experiments. In solid-state NMR samples are place in 7mm diameter spinning

rotors and spun at high speeds (3-20 kHz) in order to allow acquisition of NMR spectra with

sufficient resolution to allow chemical determinations to be made.

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12- Accu TOF (Accurate Time –of-Flight Mass Spectrometer)

Applications Generate exact mass spectra from chromatographic peaks

Non-contact surface sampling and identification by DART

Identification of Forensics, Drugs, Metabolites, Explosives…….

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13- Accu TOF

Accurate Time –of-Flight Mass Spectrometer

Applications Generate exact mass spectra from chromatographic peaks

Non-contact surface sampling and identification by DART

Identification of Forensics, Drugs, Metabolites, Explosives…….

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14- Mass Spectrometry Facility

Mass Spectrometry (MS) measures mass (m) to charge (z) ratio, i.e. (m/z).

Mass of a molecule can be categorized into two types: Exact Mass where the sum of the most abundant mono-isotopic masses of component elements is counted and Molecular Mass which sums the weighted averages of all the natural elements present in the molecule.

Generally the number of sites accessible for protonation [M+ H]+ or deprotonation [M- H]- determines the number of charges that a molecule can carry. Besides protonation, i.e. addition of H+ ion, adducts of other cations (most commonly Na), are frequently seen in the electrospray mass spectra on positive ion mode.

Services

MS MS/MS LC-MS LC-MS/MS

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15-ZEISS Spinning Disk Confocal Microscope

General Specifications Zeiss Observer Z1 Inverted Microscope NewPort Vision IsoStation anti-vibration isolation table Yokogawa CSU-X1 Filter Wheel and Spinning Disk Unit Photometrics Evolve 512 Delta EM-CCD camera (512 x 512 pixels) Applied Scientific MS2000 Piezo fast motorised Z focus (150μm range) Applied Scientific motorised XY stage Stage insert for glass slides and 3.5cm Petri dishes Definite Focus with NIR LED Hardware Focus to eliminate thermal drift PeCon Temp Module S1 and XL Multi S1 live cell stage incubator (rated 3oC to 45oC) 10x EC Plan Neofluar NA 0.3 air objective   40x C-Apochromat NA 1.2 water-immersion objective (with coverslip correction collar) 63x C-Apochromat NA 1.2 UV-VIS-IR water-immersion objective (with coverslip correction

collar) 100x Plan Apochromat NA 1.4 oil-immersion objective Zeiss HXP-120V short-arc fluorescence Hg lamp and controller (2,000h) DAPI, GFP and DSRed diochroic filters for eyepiece viewing 405nm line DAPI laser 480nm line GFP and 468nm line DsRed laser Zeiss ZEN Blue image aquisition software

Applications1. Study of Co-localization of fluorescent labeled proteins2. FRAP (FLUORESCENCE RECOVERY AFTER PHOTO BLEACHING)3. FLIP (FLUORESCENCE LOSS IN PHOTO BLEACHING)

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4. DIC (DIFFERENTIAL INTERFERENCE CONTRAST)

16-ICP-MS: Inuctive Coupled Plasma- Mass Spectrometer

Applications The determination of metallic species and metalloid

contaminants in ground waters, drinking water, industrial or

domestic waste waters, soils samples, foodstuffs…...

Total recoverable analytes in aqueous samples.

Roughly 25 elements can be analyzed with good precision in 1-

2 minutes.

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17- KONIK HRGC/MS 5000B

Gas Chromatography-Mass Spectrometry

ApplicationsUpgraded Multi-detectors instrument: FID, TCD, ECD and MS.Separation and molecular information of semivolatiles, volatiles compounds, alkaloids, drugs, pesticides, herbicides, hydrocarbons, aromas, solvents, isomers alcoholic drinks……