shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web...

33
MATERIALS AND FABRICATION TECHNOLOGY FOR RF-MEMS 3.1: Introduction In a general way, RF-MEMS is at the same time a objective product and a technological aspect. As the name implies, “RF” denotes radio frequency that includes range of frequencies between 0.1 GHz and 300GHz that comprises of applications concerning microwave and sub-millimeter wave; “Micro” describes the size of the component; “Electro” refers to both the electricity and electronics in the system; and “Mechanical” points towards the involvement of a few moving mechanical parts. In this chapter, we will focus on the material issues for RF-MEMS switches, tunable capacitors, MEM resonators and film bulk acoustic resonators etc and on the fabrication technologies. Materials and process technologies are key constraints to the design of RF-MEMS components, including the package. Materials and process technology are basic factors for the realization of RF-MEMS products. The choice of materials and the process flow is evidently governed by the details of the device to be fabricated. 3.2: Materials used for MEMS fabrication process Material and mechanical science is being revolutionized and rejuvenated. Poly-silicon is still the prevailing material used in both mechanical parts and electronic parts 47

Transcript of shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web...

Page 1: shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web viewMaterials typically used for wet etching include silicon and quartz, while dry etching

MATERIALS AND FABRICATION TECHNOLOGY

FOR RF-MEMS3.1: Introduction

In a general way, RF-MEMS is at the same time a objective product and a

technological aspect. As the name implies, “RF” denotes radio frequency that includes

range of frequencies between 0.1 GHz and 300GHz that comprises of applications

concerning microwave and sub-millimeter wave; “Micro” describes the size of the

component; “Electro” refers to both the electricity and electronics in the system; and

“Mechanical” points towards the involvement of a few moving mechanical parts.

In this chapter, we will focus on the material issues for RF-MEMS switches,

tunable capacitors, MEM resonators and film bulk acoustic resonators etc and on the

fabrication technologies. Materials and process technologies are key constraints to the

design of RF-MEMS components, including the package. Materials and process

technology are basic factors for the realization of RF-MEMS products. The choice of

materials and the process flow is evidently governed by the details of the device to be

fabricated.

3.2: Materials used for MEMS fabrication process

Material and mechanical science is being revolutionized and rejuvenated. Poly-

silicon is still the prevailing material used in both mechanical parts and electronic parts in

MEMS devices. VLSI fabrication technique has advanced to build mechanical

components with electronic components. Just like IC technology in 1970s, MEMS

technology is still immature. Most of the RF-MEMS products are still lab toys.

RF-MEMS are constructed from materials, which have unique reliability results.

Different materials have different responses to failure mechanisms that need to be

understood to increase reliability of device. The materials used in designing and

fabrication of RF-MEMS devices and components are given in the following Figure 3.1.

The choice of the right material for an RF-MEMS component requires knowledge of the

many factors about the application of the material. Apart from availability and cost,

factors guiding in choosing the suitable materials are:

o Fundamental material properties and their controllability.

47

Page 2: shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web viewMaterials typically used for wet etching include silicon and quartz, while dry etching

Substrates

Polymers

Thin Films

Semiconductors like Si, GaAs, InP, Ge

Metals like Al, Au, Cu, etc. & their Alloys

Polysilicon

Special Materials like PZT, BST

Insulators like SiO2, Si3N4, and PMMA

Packaging

Ceramics like MgO, Al2O3, and Saphire

Glass

Semiconductors like Si, GaAs, InP, Ge

PolymersCeramics

Metals

Materials for RF-MEMS

o Ease of processing (like etching, deposition, conformal step coverage etc.)

o Processing compatibility (adhesion, diffusion, temperature, packaging, etc.)

o Reliability characteristics (fatigue, creep, dielectric charging, long-term drift, etc.)

Figure 3.1: Various materials employed for fabrication of RF-MEMS devices.

3.2.1: Single Crystal Silicon

Silicon is a good mechanical material with high precision, high strength, and high

reliability. Like diamond, silicon is a very hard material. It is a tetrahedral covalent

bonded structure. It has better mechanical strength and yield strength than steel, but is

more brittle. Its highest fracture strength makes silicon perfect for many MEMS

structures.

Silicon is the most widely used material for manufacturing RF-MEMS because it

has excellent mechanical and electrical properties. Diamond structure and low

crystallographic index planes of silicon are shown in Figure 3.2. Silicon is resistant to

most acids, except HF or HNO3 and certain bases. Main physical characteristics of silicon

are listed in Table 3.1.

The four factors that have made silicon vital as a mechanical material are:

48

Page 3: shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web viewMaterials typically used for wet etching include silicon and quartz, while dry etching

(b)

(a) It is available in large quantity, cheap, can be produced and processed

controllably with supreme purity and perfection.

(b) Silicon processing is based on very thin deposited films which can be

easily miniaturized.

(c) It can be batch fabricated.

(d) The device shapes and patterns can be defined and reproduced using

lithographic techniques.

Figure 3.2: (a) Crystal structure of silicon and (b) Low crystallographic index

planes of silicon.

Table 3.1: Well defined characteristics of Silicon.

Sr. No. Characteristics Value

1. Melting point 14150C

2. Young’s modulus <100> 130 GPa

3. Poisson’s ratio <100> orientation 0.28

4. Fracture strength 0.9 MPa m^.5

5. Thermal conductivity 1.56 W/cm-0C

6. Coefficient of thermal expansion 4.2 x 10-6 0C-1

7. Heat Capacity 20.07 J/mol-K

8. Breakdown Field ~3 x 105 V/cm

9. Resistivity 2.3 x 105Ω-cm

10. Band Gap 1.12 eV

11. Electron mobility 1500 cm2 /V-s

49

Page 4: shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web viewMaterials typically used for wet etching include silicon and quartz, while dry etching

Electrons in solids can only occupy discrete energy levels, separated into distinct

bands. At the lowest potential, all valence electrons occupy the valence band. The band-

gap determines the electrical and optical properties of a device. However, electrical

properties of silicon are sensitive to magnetic fields, stress, heat, and radiation, which is a

characteristic that is beneficial in many solid-state sensors. It exhibits high resistivity of

silicon wafers for RF-MEMS. It is opaque to UV and transparent to infra-red.

Figure 3.3: Energy band structure of silicon and gallium-arsenide.

In direct bandgap semiconductors, like GaAs, conduction band and valence band

are in line. Electrons only need energy to transit levels. When an electron de-excites, a

photo emits. In indirect bandgap semiconductor, like silicon, electrons need to change

both momentum and energy to change levels, as shown in Figure 3.3. Thus, silicon

cannot be used in semiconductor lasers and LEDs. This limit to silicon led to explore new

semiconductors that can emit light.

3.2.2: Gallium Arsenide

After silicon, gallium arsenide is most common semiconductor. It has better

optical and electrical properties. Being a direct band gap semiconductor, it is used in

semiconductor lasers and LEDs. It will help in developing micro-opto-mechanical

devices. The fundamental characteristics of gallium arsenide are mentioned in Table 3.2.

Being brittle and poor mechanical performance, it is not used in the

semiconductor industry. Due to low Young’s modulus, it is weak. It is a poor thermal

conductor and becomes ductile at much lower temperatures than its melting point. So, its

hardness decreases and fatigue increases at high temperatures. GaAs can work at higher

frequencies than silicon, which makes it ideal for communications applications.

50

Page 5: shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web viewMaterials typically used for wet etching include silicon and quartz, while dry etching

However, there are unstable insulating oxides and nitrides of GaAs that make it difficult

to reproduce passivation layers.

Table 3.2: Fundamental characteristics of Gallium Arsenide.

Sr. No. Characteristics Value

1. Crystal structure Zinc-blende

2. Melting point 12370C

3. Heat capacity 47.02 J/mol-K

4. Breakdown field ~400000 V/cm

5. Thermal conductivity 0.46 W/cm-°C

6. Young’s modulus 85.5GPa

7. Poisson’s ratio 0.31

8. Fracture strength 0.44 MPa m^.5

9. Constant of thermal expansion 6.86 x 10-6 °C-1

10. Band gap 1.424eV

11. Resistivity 108 Ω-cm

12. Electron mobility 8500 cm2/V-s

3.2.3: Polycrystalline Silicon (Polysilicon)

Polysilicon is used as a structural material in the surface micromachining process.

Thin films of silicon are difficult to grow, but that of polysilicon can be grown.

Polysilicon crystallized by metal induced lateral crystallization (MILC) gives improved

performance. It finds many uses in the RF-MEMS industry. The mechanical properties

(Young’s modulus 140-210GPa) of polysilicon films depend greatly upon the deposition

process. Depositing its films at 5900C (transition point between polycrystalline and

amorphous silicon), is useful method of forming an isotropic film of polysilicon.

3.2.4: Silicon Dioxide

Silicon dioxide is an excellent thermal and electrical insulator and commonly

used in integrated circuits. So, it can be used to separate different layers of conductors

and components with little electrical interference effectively in MEMS. It is used recently

as a structural material. Its basic properties are listed in Table 3.3.

Table 3.3: Remarkable characteristics of Silicon Dioxide.

51

Page 6: shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web viewMaterials typically used for wet etching include silicon and quartz, while dry etching

Sr. No. Characteristics Value

1. Density 2.65 g/cm3

2. Melting point 17280C

3. Young’s modulus 66 GPa

4. Tensile strength 69 MPa

5. Thermal conductivity 1.4 x10-2W/0C-cm

6. Constant of thermal expansion 7 x 10-6 0C-1

8. Resistivity 1012Ωcm

9. Band gap 8 eV

However, due to high anisotropy, it is more difficult to etch than silicon. Silicon

dioxide can be used as the sacrificial layer material in the surface micromachining

process because it is prone to etching with hydrogen fluoride whereas silicon is resistant

to etching. It is a commonly used in glasses. Due to low thermal conductivity, it is a

thermal insulator. Having low tensile strength, it is prone to mechanical fracturing and

rarely used as a mechanical material. Due to the inherent advantages in being able to

integrate such an effective insulator, it has become the semiconductor material of

selection for most applications.

3.2.5: Silicon Carbide

Recently, silicon carbide is being used as a material for RF-MEMS. Its

characteristics depend much upon processing. It offers advantages in hardness and

resistance to harsh environments and high temperatures. It does not have a sharp melting

point (2830 0C). At this temperature, it decomposes into graphite and a silicon rich-melt.

It oxidizes to silicon dioxide above 600 0C.

Several SiC structures are less elastic than silicon, which is useful in certain

MEMS applications. Its Poisson’s ratio varies between 0.183 and 0.192. Its main

drawback is that the wafer growth technology used to grow its wafers results in high

dislocation densities. It weakens its strength that impedes its use in many applications. It

is a wide-bandgap semiconductor with a band-gap around 3eV. It acts as a good insulator.

It has a resistivity of 108 Ω-cm that varies with doping.

3.2.6: Silicon Nitride

52

Page 7: shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web viewMaterials typically used for wet etching include silicon and quartz, while dry etching

Silicon nitride is a useful masking material for alkaline etch solutions and also as

an insulating thin film. It can also be used to make MEMS membranes, plates and

cantilevers. It does not react well with many etching solutions; hence, it is often used to

stop impurity dispersion and ionic contamination. The silicon nitride films used in most

MEMS devices are amorphous and are either sputtered or deposited by CVD. It has a

bandgap much smaller than that of silicon dioxide, so, it facilitates much less electrical

isolation than that of silicon dioxide. Crucial characteristics of silicon nitride are given in

Table 3.4.

Table 3.4: Crucial characteristics of silicon nitride at room temperature.

Sr. No. Characteristics Value

1. Density 3.1 g/cm-3

2. Resistivity 1015W-cm

3. Breakdown field 107 V/cm

4. Band gap 3.9eV to 4.1 eV5. Thermal conductivity 0.28 W /cm-°C

6. Young’s Modulus 73 GPa

7. Coeff. of thermal expansion 3×10-5/°C

8. Fracture strength 460 MPa

9. Melting point 19000

Silicon nitride (Si3N4) has vital mechanical properties that make it an attractive

material to work with. It is a better thermal insulator than polysilicon, so it is used for

isolating surface micro-machined structures. Also, due to high mechanical strength, it is a

perfect film for dust barriers and friction. Furthermore, it makes a low energy barrier

towards silicon and metals that causes the injection of holes into the dielectric at electric

fields > 2×106 V/cm. So, a designer likes to form insulators with SiO2 and seals it with

silicon nitride.

3.2.7: Other Materials

Metals such as aluminium, gold, copper etc, are used in MEMS as electrical

conductors and occasionally as structural material. The metals used in MEMS are, unlike

the materials discussed previously, ductile. That means that they will plastically deform if

53

Page 8: shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web viewMaterials typically used for wet etching include silicon and quartz, while dry etching

stressed past the yield strength. Aluminum is commonly used as an electrical conductor

in semiconductor technologies. Aluminum, like most metals, is often alloyed with other

substances to enhance its structural properties. The mechanical properties of aluminum

are considerably poorer than Si and GaAs. Gold is a soft, ductile material that is easily

deformed. Consequently, it is not used as structural material. Instead, it will almost

always be layered on top of a more rigid material or be used in applications that do not

require mechanical motion.

Polymers are useful in sensing of chemical gases because of their absorption and

adsorption properties and polymethylmethacrylate (PMMA) is a useful polymer in the

LIGA process for forming high aspect ratio structures. Plastic micro devices are useful

for micro fluidic applications for biosensors. As no batch process fabrication techniques

are recognized for plastics, the University of Michigan is finding surface and bulk

micromachining of plastics and the embedding of silicon devices into cast plastic

substrates. Harvard University is also exploring new organic polymers and processes

such as micro molding and micro printing to produce structures from them.

Ceramics are also employed for RF-MEMS for some particular applications.

Ceramic pressure sensors have been developed for pressure computation of the high

temperature surroundings. Moreover, some functional ceramics like ZnO, PZT, etc, have

also been incorporated in the RF-MEMS devices. The fabrication processes for ceramic

MEMS are screen printing, micro-moulding, micro-stereo-lithography, Sol-Gel, etc.

Research in new materials for MEMS is also active. For example:

Amorphous alloys can be extruded and forged using micro-dies and so,

these assure as future materials for MEMS;

Poly-caprolactone is a biodegradable polymer that makes it beneficial for

implantable biomedical micro-devices;

Tantalum oxide can be active as a protective coating for sensors; and

Polycrystalline silicon-germanium can be deposited and annealed to

trigger dopants (impurities added to affect the semiconductor properties)

at much lower temperatures than polysilicon and becomes a good

contender for structural material.

3.3: RF-MEMS Fabrication Techniques

54

Page 9: shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web viewMaterials typically used for wet etching include silicon and quartz, while dry etching

Obviously, MEMS are the integration of electronic and mechanical components

on a same silicon chip using microfabrication processes. The mechanical parts (actuators

and sensors) are manufactured by micro-fabrication approaches. Electronics and

electrical circuits are used to make signal processing, control units etc. The electrical and

electronics is fabricated by IC process like CMOS. In this way, the entire system can be

fabricated on a single chip as shown in the Figure 3.4. In this figure cross-sectional view

of the Sandia MM or CMOS integrated MEMS technology is represented. The

mechanical structure fabricated prior to the electronics is embedded down inside a

planarized well.

Micromachining is the combination of design and fabrication tools that precisely

make microstructures and components at the microscale. Micromachining is the basis for

RF-MEMS devices fabrication. Normally, in micromachining, parts of the silicon wafer

are selectively etched away or new structural layers are added to make the mechanical

and electromechanical devices. Several processes and tools used in the design and

fabrication of RF-MEMS devices are taken from IC technology.

Figure 3.4: Cross-section representation of the Sandia MM/CMOS integrated

MEMS technology.

Common fabrication techniques that are used for machining structures include

bulk micromachining, wafer-to-wafer bonding, surface micromachining, and high-aspect

ratio micromachining (like LIGA). Flip chip technique is employed when silicon is not

used as substrate. High-aspect ratio micromachining is a new technique that facilitates

55

Page 10: shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web viewMaterials typically used for wet etching include silicon and quartz, while dry etching

the fabrication of layers (generally thickness lies between hundreds of microns to a few

centimeters), precisely, high-aspect ratio MEMS structures (structures with almost

vertical sides).

3.3.1 Bulk Micromachining

The most mature and familiar micromachining fabrication technique is the bulk

micromachining. This micromachining is employed to fabricate micromechanical

structures inside the bulk of a wafer by selectively etching material of the wafer. Bulk

micromachining involves the selective removal of considerable amount of silicon from

any part of the bulk substrate. It is a subtractive process that uses wet anisotropic etching

or a dry etching method such as reactive ion etching (RIE), to create three dimensional

microstructures such as large pits, grooves, membranes, trench holes, cavities, nozzles,

cantilevers, channels, etc. different bulk micromachining microstructures are shown in

the Figure 3.5. Materials typically used for wet etching include silicon and quartz, while

dry etching is typically used with silicon, metals, plastics, ceramics etc.

Figure 3.5: Different structures obtained by using bulk micromachining process.

Bulk micromachining is based on etching single-crystal silicon either chemically

(wet etching) or using plasma etching or reactive ion etching (RIE) techniques (dry

etching). Bulk micromachining involves the various etching procedures that selectively

remove material with a chemical enchant whose etching properties depend on the

crystallographic structure of the bulk material. Wet etching removes material by

immersing it in a liquid bath of a chemical etchant. These etchants can be isotropic or

anisotropic. HNA, a mixture of hydrofluoric acid (HF), nitric acid (HNO3) and acetic

acid (CH3COOH), is the most common isotropic silicon etch.

56

Page 11: shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web viewMaterials typically used for wet etching include silicon and quartz, while dry etching

Dry etching involves vapor phase or plasma-based methods of etching using

suitable reactive gases or vapors at high temperatures. The most used dry etching for

MEMS is reactive ion etching (RIE) that uses an additional energy (radio frequency

power) to start the chemical reaction. Energetic ions are accelerated towards the material

to be etched within a plasma phase. Irrespective of crystal planes RIE can etch any shape

with vertical walls like deep trenches and pits. Deep Reactive Ion Etching (DRIE) is a

much higher-aspect-ratio etching method that involves an alternating process of high-

density plasma etching and protective polymer deposition to get higher aspect ratios of

the microstructures.

Figure 3.6: Bulk micromachining along crystallographic planes.

Figure 3.6 shows the steps of a typical bulk micromachining technique. Here,

anisotropic wet etching is used to make microstructures from the silicon substrate. Bulk

micromachining has a few basic shortcomings. For example, the orientation of crystal

planes of wafer determines the highest attainable aspect ratios. The more aspect ratios

need bigger sizes as compared to the other micromachining processes. Obtaining

complex microstructures by employing this process is also very difficult.

3.3.2 Surface Micromachining

57

Page 12: shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web viewMaterials typically used for wet etching include silicon and quartz, while dry etching

(a)

(e)

(c)

(b)

(d)

(f)

Surface micromachining involves processing on the substrate that is used as a

support for the desired structure. It was initiated in the 1980’s to produce MEMS.

Material is added to the substrate in the shape of layers of thin films on the surface of the

substrate. These layers can either by structural layers or act as spacers or sacrificial layers

(that are removed later). Hence, the process typically involves films of two different

materials: a structural material (popularly polysilicon, silicon nitride and aluminium) out

of which the free standing structure is built and a sacrificial material (popularly an oxide),

deposited wherever either an open area or a free standing mechanical structure is vital.

The desired structure is shaped by removing the sacrificial layer and releasing the

structure.

Figure 3.7: Various processing steps involved in typical surface micromachining.

In surface micromachining (SMM), layers of structural and sacrificial material are

deposited alternatively and etched to get the desired shape. Surface micromachining

facilitates the construction of free-shape, complex and multi-fabricate systems without

limitations on materials, geometry, assembly and integration that are the source for the

58

Page 13: shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web viewMaterials typically used for wet etching include silicon and quartz, while dry etching

richness and depth of MEMS applications. The various steps involved in the fabrication

of microstructures using surface micromachining are shown below in the Figure 3.7.

Surface micromachining involves the fabrication of the devices from thin films

deposited on the surface of a silicon wafer. Hence, this technique needs a well- matched

set of sacrificial layer, structural layer and etchants. All these materials must be proper

for the application. The size of the SMM structures can be of much lower than structures

got from bulk micromachining. These are also easy to integrate in IC circuits. These

structures are normally planar. The success of the surface micromachining process

depends on the ability to remove all of the sacrificial layers effectively so that the

structural elements become free for actuation. The key benefits of surface

micromachining are the use of standard CMOS fabrication and the ease of the process.

3.3.3: Wafer-to-wafer Bonding

There is a fundamental limitation to bulk micromachining that it cannot produce

complex three dimensional microstructures. This problem is overcome by fabricating and

then assembled altogether the micro-components of a complex structure. In wafer

bonding technique, different wafers are almost integrated together without any fault. It

can be divided into three well-known types: intermediate layer assisted bonding, anodic

bonding, and direct bonding.

Intermediate layer assisted bonding needs an intermediate layer that can be metal,

glass, polymer, solder etc to fulfill bonding between wafers. Anodic bonding is

developed normally between a sodium glass and silicon for MEMS. A voltage is applied

between the glass and silicon, and a heater also maintains bonding temperature around

180-500 ºC simultaneously. A strong hermetic chemical bond is formed between silicon

and glass during the bonding.

Direct bonding (or silicon fused bonding) is used for silicon wafer to silicon wafer

bonding, so, also termed as. The basis of this type of bonding is the chemical reaction

between the hydroxyl groups present on the surface of native silicon or developed oxide

films covering the wafers involved. Wafer-bonding continues to progress with vertically

integrated micromachined filters which are demonstrated at frequencies ~ 10GHz. In

wafer bonding, bulk-micromachined substrates are bonded together.

3.3.4: LIGA (High-Aspect-Ratio Micromachining)

59

Page 14: shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web viewMaterials typically used for wet etching include silicon and quartz, while dry etching

High-aspect-ratio micromachining (HARM) is a process that involves

micromachining as a tooling step followed by injection moulding and, if required, by

electroforming to replicate microstructures in metal from molded parts. It is one of the

most attractive technologies for replicating microstructures at a high performance-to-cost

ratio. LIGA is an important tooling and replication method for high-aspect-ratio

microstructures. LIGA products are high aspect ratio fluidic structures such as molded

nozzle plates for inkjet printing. The materials that can be used are electro-formable

plastics (including acrylate, polycarbonate, styrene, polyimide) and metals.

LIGA (Lithographie Galvanoformung Abformung – German acronym for

lithography, electroplating and molding) is a process for producing high aspect ratio

microstructures (HARMs). Unlike usual optical lithography, X-rays are used to produce

the mould made from a polymer resist (e.g. polymethylmethacrylate (PMMA)) and a thin

metal base. Electroplating is used to fill the mould with a metal and the remainder of the

resist is removed, leaving high aspect ratio microstructures. X-ray lithography allows the

creation of HARMs with aspect ratios of greater than 100; however, the use of collimated

X-rays from synchrotrons makes this process expensive. LIGA is used to produce HARM

structures in Ni-Co and PZT (lead zirconate titanate).

The technique employs X-ray synchrotron radiation to expose thick acrylic resist

of PMMA under a lithographic mask. The exposed areas are chemically dissolved and, in

areas where the material is removed, metal is electroformed, thereby defining the tool

insert for the succeeding moulding step. LIGA is capable of creating very finely defined

three dimensional microstructures having heights of many hundred micrometers, which is

impossible with other micromachining techniques using silicon. Various metal ceramics,

plastics, or their combinations can be used to obtain difficult and complex

microstructures. An illustration representing the LIGA technique is shown in Figure 3.8.

60

Page 15: shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web viewMaterials typically used for wet etching include silicon and quartz, while dry etching

(a) (e)

(b) (f)

(c)

(d)

(g)

(h)

Figure 3.8: Various steps involved in a typical LIGA process.

LIGA is limited by the need to have access to an X-ray synchrotron facility. A

compromise which combines some features of LIGA with surface micromachining

eliminating the need for exposure to X-rays has been developed and is known as SLIGA

(Sacrificial LIGA). It replaces the thick PMMA photoresist with polyimide as the

electroplating mould, thus enabling compatible conventional IC batch processing. HARM

production methods have provided radically new ways to produce micromachined parts

for MEMS devices at relatively low cost. In particular, techniques such as SLIGA enable

the production of MEMS components with much lower manufacturing infrastructures in

terms of investment, facilities and access to advanced materials and technology.

61

Page 16: shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web viewMaterials typically used for wet etching include silicon and quartz, while dry etching

3.3.5: Flip Chip Method

In the flip chip method, a chip is mounted on a substrate with an interconnect

material by employing methods like tape-automated bonding, fluxless solder bumps,

metallurgy bumps, wire interconnects, pressure contacts, and compliant bumps,

conductive polymers, anisotropy conductive adhesives, etc. The components used in flip

chip are mainly semiconductor devices. With the progress in this technology, now-a-

days, MEMS devices have started replacing in the flip chip shape.

In the flip chip process, gold transfer bumps and the anchor bump are placed

properly on the transfer pads that are made on the MEMS host substrate. These transfer

pads are merely connected to the host substrate with the silicon dioxide sacrificial layer.

These transfer pads and hence, the MEMS devices are entirely disconnected from the

host substrate when the silicon dioxide sacrificial layer is dissolved in the hydrofluoric

acid. There is permanent connection between the anchor and the host substrate. Due to

this reason, the anchor prevents the contact between the host substrate and the device

after release. In addition to it, it also suspends the substrate to act as a shield during the

drying and the release processes.

Then the gold bumps are pressed against a smooth glass substrate. This pressing is

done before bonding the MEMS device to other substrates. The pressing is needed to

compress any trailing wires from the top of the bump left by the wire bonding machine.

Moreover, the pressing of the bumps facilitates improved planarity of the bumps

throughout the actual bonding. Then the complete structure MEMS flip chiplet bonded to

a target substrate such as coplanar waveguide (CPW) using thermal sonic bonding. The

silicon substrate is anchored on an anchor bump. Then silicon dioxide is removed with

the help of HF (hydrofluoric acid). Then, the host substrate is removed with the help of

clamps to crack the anchor without any harm to the MEMS device.

After that, HF is prevented from doing more etching inside the devices by

washing the flip chip devices thoroughly with methanol so that the HF is removed. The

devices are rinsed in the methanol for some time and then these devices are well-dried

properly with the help of a special drying chamber. This chamber uses liquid carbon-

dioxide to displace the methanol. This step is needed because, otherwise, methanol would

pull devices below and would make contact with the substrate and therefore, the desired

62

Page 17: shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web viewMaterials typically used for wet etching include silicon and quartz, while dry etching

(a) MEMS Chip with Gold bumps.

(b) Pressing Gold bumps on a smooth glass substrate.

(c) Bonding MEMS chip to CPW substrate by thermal sonic bonding.

(d) Removing Silicon Dioxide using Hydrofluoric acid etchant.

(e) Removing MEMS host substrate.

devices would be damaged. In the end, the MEMS device can be transferred to the other

substrate effectively. The schematic diagram of flip chip technique is shown in the Figure

3.9.

This technology has benefits of highest electrical performance, smallest size (due

to no requirement of package and bond wires, the desired area get reduced), more

reliability, greatest input and output density, lower cost, and more flexibility as compared

to other technologies. In addition to these benefits, there is better availability of devices,

materials, and apparatus employed for flip chip technology. Also, flip chips are solid tiny

blocks of cured epoxy when finished with adhesive; hence, these are the most rugged

structures mechanically.

Figure 3.9: Various steps involved in a typical flip chip technique.

63

Page 18: shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web viewMaterials typically used for wet etching include silicon and quartz, while dry etching

The MEMS organizations and industries are attracted by the flip chip technology,

due to its ability to integrate a system on a chip by packaging many dies on the same

substrate. Also, many MEMS fabrication techniques only limited structural layers due to

problems relating to price and time. But, in this process, many structural layers are

presented to the MEMS designers. This technology provides more space and many

releasable layers to manufacture the designs. MEMS devices can be easily transferred to

the other substrates. Moreover, flip chip technology is also employed for the production

of extremely advanced MEMS that are much appropriate for the applications concerning

to radio frequency, microwave, sub-millimeter wave, and optical frequency.

3.4: Computer Aided Design

Computer Aided Design (CAD) is, in general, used in RF-MEMS for the design

of photolithographic masks. This is a simple process as MEMS structures are relatively

large in comparison to the sub-micron structures usually associated with the silicon chip

components. In addition to the use of CAD for mask designing, CAD and finite element

analysis (FEA) are important simulation tools for the designing MEMS applications.

Unluckily, so far there is a short of acceptable extremely developed software based

design tools to model, analyze and simulate MEMS microstructures completely. This has

acted as a stumbling block to the advancement of RF-MEMS devices and components.

In these days, MEMCAD is most familiar, successful and commercially

obtainable software design tool. Microcosm Technologies in North Carolina, USA, has

evolved this package. The MEMCAD package would be capable of quickly solving

thermal, mechanical, magnetic, electrostatic, fluidic, and optical and radio frequency

solutions in a united manner. The MEMCAD system specifies layout and process of a

device, and then constructs the three dimensional geometry of the device, assembles a

comprehensive three dimensional model and analyses performance of device. Besides all

these activities, this MEMCAD system also performs the variations in the design

manufacturing and sensitivity of a device.

MEMS Pro is another package from Tanner Research in California. It provides

RF-MEMS designers to simulate the development or deposition, implantation or

dispersion. It also facilitates simulation of any of the etch step concerned within a MEMS

fabrication technique. However, the problems wanting solutions in the MEMS are much

64

Page 19: shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web viewMaterials typically used for wet etching include silicon and quartz, while dry etching

diverse and hence need many more solvers and a more sophisticated CAD tool. Without

the standard CAD tool, it is difficult to provide cost minimized solutions guaranteed to

work in the present systems.

However, the complete simulation of the MEMS that are integrated with the

circuits is a challenge. A novel model is generated each time the geometry is altered.

Now-a-days, a concerted step is being done to grow methods to decompose an integrated

MEMS design into a hierarchical design of fundamental MEMS elements. Then, such a

design can be completely integrated into the IC CAD tool. Then, IC and MEMS solutions

can be solved at the same time by the same tool and variations in the size of the

fundamental MEMS elements can be computed at once. Existing solvers do the balanced

solutions by a lengthy iterative method.

3.5: Summary

After many decades of progress, the RF-MEMS field is growing exponentially,

due to the high volume commercial markets and innovative research fields enabled by

novel functions made possible by MEMS technology. In this chapter, several materials

employed to fabricate the RF-MEMS devices, components or systems are described. The

prominent, well-defined characteristics or parameters are also given or tabulated.

Materials and process technology are basic factors for the realization of RF-MEMS

products. Silicon is still the prevailing and widely used material in both mechanical parts

and electronic parts in MEMS devices; because it is easily and economically available

with excellent mechanical and electrical properties.

After silicon, gallium arsenide is most common semiconductor. Gallium arsenide

finds most of its uses due to its better optical and electrical properties. Polycrystalline

silicon (polysilicon) is used as a structural material in the surface micromachining

process. Since it is difficult to grow thin films of single crystal silicon, thin films of

polysilicon are grown. Silicon dioxide can be used as the sacrificial layer material in the

surface micromachining process because it is prone to etching with hydrogen fluoride

acid whereas silicon is resistant to etching. Silicon nitride is a useful masking material for

alkaline etch solutions and also as an insulating thin film. Silicon nitride (Si3N4) has vital

mechanical properties that make it an attractive material to work with. It is a better

65

Page 20: shodhganga.inflibnet.ac.inshodhganga.inflibnet.ac.in/bitstream/10603/6904/5/cha… · Web viewMaterials typically used for wet etching include silicon and quartz, while dry etching

thermal insulator than polysilicon, so it is used for isolating surface micromachined

structures.

The most common fabrication techniques employed for microelectromechanical

systems such as bulk micromachining, wafer-to-wafer bonding, fusion bonding, surface

micromachining, the LIGA process and flip chip technique are briefly described here.

The most mature and familiar micromachining fabrication technique is the bulk

micromachining. This micromachining is employed to fabricate micromechanical

structures inside the bulk of a silicon wafer by selectively etching material of the wafer.

In surface micromachining, thin films are sequentially deposited and patterned on

top of the substrate, with the final removal of the sacrificial layer to release the movable

structures. The LIGA process involves X-ray lithography of thick photo-resist on

conductive substrate, plating through the developed resist, and injection molding with the

plated components. The flip chip technology has benefits of more electrical performance,

smallest size, more reliability, greatest input/output density, lower cost, and more

flexibility as compared to other technologies. The progress of material technology and

fabrication techniques are the key to the success of novel RF-MEMS systems.

66