VOLUNTARY CLEANUP PROGRAM SITE ASSESMENT FORMER …€¦ · VOLUNTARY CLEANUP PROGRAM SITE...

VOLUNTARY CLEANUP PROGRAM SITE ASSESMENT

FORMER TYSON FOODSPROCESSING PLANT 9943 OLD OCEAN CITY BOULEVARD

BERLIN, MARYLAND 21811

Prepared For:

Mr. Doug Baxter Environmental Manager

Tyson Foods, Inc. 13264 Mountain Road

Glen Allen, Virginia 23059

Prepared By:

Froehling & Robertson, Inc. 2505 Hutchinson-McDonald Road Charlotte, North Carolina 28269

704-596-2889

F&R Project Number G63-9047E

October 11, 2005 Prepared by: Reviewed by: Ed Setzer Robert Jones, GC, E.I.T., MBA Project Manager Assistant Branch Manager

TABLE OF CONTENTS

1.0 Introduction.......................................................................................................1

2.0 Methodology .....................................................................................................1 3.0 Findings – Tank and Transformer Inventory .....................................................2

4.0 Findings – Soil Sampling ..................................................................................4 5.0 Findings – Groundwater Sampling ...................................................................6 6.0 Site Specific Water Level Information...............................................................6 7.0 Conclusions ......................................................................................................6 8.0 Limitations ........................................................................................................7 Appendix A – Site Vicinity Map / Site Map Appendix B – MDE Letter Appendix C – Probe Log and Well Construction Records Appendix D – Tabulations of Soil Results Appendix E – Soil Analytical Report Appendix F – Water Analytical Report Appendix G – Transformer Analytical Report

1.0 Introduction In 2004, Froehling & Robertson, Inc. (F&R) was contracted to perform a limited Phase II Environmental Site Assessment (ESA) of the Tyson Foods, Inc. Processing Plant located in Berlin, Maryland. This assessment was designed to assist the Maryland Department of the Environment (MDE) Oil Control Program (OCP) in closing all currently open case files at the Tyson Berlin Plant. In order to accomplish this objective, representatives of Tyson Foods, Inc., F&R, and MDE met on several occasions and developed an approved Scope of Services. On or around December 17, 2004, Tyson Foods, Inc. submitted a Voluntary Cleanup Program Application to MDE that included the Phase II Limited Environmental Site Assessment report prepared by F&R. The scope of services included in F&R’s December 2004, report included the installation of 20 monitoring wells for the purpose of testing groundwater for the presence of selected Volatile Organic Compounds (VOC’s), including benzene and methyl tertiary butyl ether (MTBE) and oxygenates. Eleven of the wells were installed to a depth of twenty feet and nine wells were installed to a depth of forty feet below subsurface. The scope of services for this assessment was set by the Maryland Department of the Environment (MDE). The results of this initial assessment revealed low levels of benzene in two of the wells. On August 12, 2005, Mr. James W. Metz, Chief of the Voluntary Cleanup / Brownfields Division of MDE issued a letter (Appendix B) proposing limited supplemental soil and groundwater samples to fulfill the principals for a Phase II site assessment, as defined by the American Society for Testing and Materials, for evaluating recognized environmental conditions identified at the property. The requested information included twelve items (ref. Appendix B) of which F&R was contracted to address items 4, 6, 7, 8, 11 and 12. This report includes our finding and where appropriate, our recommendations on these items. 2.0 Methodology Item 4 of the MDE letter requested a tabular summary and scaled site map of all underground and aboveground storage tanks. This information was gathered with the assistance of Mr. Bill Davis of Tyson Foods, Inc. Item 6 of the MDE letter requested a tabular summary and scaled site map of all transformers (ground and pole-mounted) on site. This information was also obtained with the assistance of Mr. Davis. For the supplemental site investigation (Item 7), the location and depth of the two

additional monitoring wells and probe points were predetermined by the MDE and plotted on a site map. The only changes to these locations were based on the location of underground utilities; none of the changes were significant from the original scope. F&R installed 1-inch diameter PVC pipe with 10 feet of slotted screen in these approximately 20 feet deep wells. The wells were installed in accordance with MDE requirements and good environmental practices. At the surface, flush mounted curb-boxes were installed to protect the well points. After proper development of the wells, F&R obtained one (1) sample from each well. Monitoring wells MW-10 and MW-16 were also sampled during this event since they previously revealed low level concentrations of benzene. These samples were then analyzed for Volatile Organic Compounds (VOCs) with a library search for non-targeted VOCs. Depending on the location of the probe point and the depth, soil samples were selected for analysis as suggested in the MDE letter. All soils were screened with a photo ionization detector (PID) during the probing process. 3.0 Findings – Tank and Transformer Inventory Item 4 of the MDE letter requested a tabular summary and scaled site map of all underground and aboveground storage tanks. This information was gathered with the assistance of Mr. Davis. The attached drawings show the areas of these tanks. Table 1

Tank # Size Contents AST or UST Status

001 2,000 G Gasoline UST Abandoned in Place – 1992

002 3,000 G Diesel UST Abandoned in Place – 1992

003 12,000 G Diesel UST Removed - 1988

004 2,000 G Heating Oil UST Abandoned in Place – 2003

005 2,000 G Heating Oil UST Abandoned in Place – 2004

006 16.4’ x 3.3’ D LPG AST In service


008 17.8’ x 5’ D Ammonia AST Permanently Out of service

009 2.3’ x 3.8’ x 5.1’ ob-round

Hydraulic oil AST “

010 5.4’ x 4.1’ D Used oil AST “


Tank # Size Contents AST or UST Status


013 200 G Fuel oil AST In service

014 4,000 G Gasoline UST Removed – 12 / 1991

015 10,000 G Diesel AST Removed – 2005 G – gallons, D-diameter All of the tanks are currently empty except for the hydraulic oil tank, the 200 gallon fuel oil tank which operates the fire pump and the used oil tank which has been pumped out but may have some residue. Item 6 of the MDE letter requested a tabular summary and scaled site map of all transformers (ground and pole mounted) on site. This information was obtained with the assistance of Mr. Davis. The attached drawings show the areas of these transformers except for transformer number 09 which is near the northwest corner of the lagoon depicted in Figure 1A of the MDE letter (Appendix B).

Table 2

Transformer(s) location # Type Date Installed Date Tested Other info

01 Non-PCB 1960’s 09/19/2005 (Appendix G)

Main Office near Worcester Highway

02 “ Late 80’s to early 90’s Tagged Westside Transclosure

03 “ “ “ Protein Plant Transcloser

04 “ “ “ # 1 Transcloser

05 “ “ “ # 2 Transcloser

06 “ 1970’s “ Office near WWTP

07 “ Late 80’s to early 90’s “ Step Down

Transformer

08 “ 2002 NA 3 pole-mounted

transformers (all others all on slabs)

09 “ “ NA Between lagoons

There is also one transformer from the late 80’s to early 90’s era that is in storage as a replacement for the other transformers installed at that time. The tagged transformers have tags that identify them as non-PCB; the NA transformers were manufacture after PCBs were banned. 4.0 Findings – Soil Sampling F&R used a push-probe type soil sampling unit to collected soil samples at various locations and depths. Depending on the location of the probe point and the depth, soil samples were selected for analysis as suggested in the MDE letter. All soils were screened with a Photo Ionization Detector (PID) during the probing process. Table 3 provides and overview of the probe depths and Appendix C contains copies of the probe logs.

Table 3

PROBE POINT

PRESCRIBED DEPTH

ACTUAL DEPTH SAMPLE DEPTHS

S-1 & GW-1 1’-5’ 15’-6” 1 and 6’ S-2 “ 8’ 1 and 5’ S-3 “ 8’ 1 and 5’

GW-2 “ 16’ 1 and 5’ S-4 “ 8’ 1 and 5’ S-5 “ 8’ 1 and 5’ S-6 “ 8’ 1 and 5’ S-7 “ Cancelled by

MDE NA

S-8 “ 12’ 1 and 6’ S-9 “ 8’ 1 and 6’

S-10 1’-2’ 1’ 1’ S-11 “’ 1’ 1’

The soil samples obtained from the subject site were tested according to the MDE schedule and included EPA Methods SW846 / 8260 with a library search, 8270 with a library search, 8081, 8151, and 200 series metals. Units of concentration are given in milligrams per kilogram (mg / kg) or parts per million for each of the tests conducted on the soil samples. The analytical results were compared to the Non-Residential Clean-up Standards listed in the State of Maryland’s Cleanup Standards for Soil and Groundwater. Concentrations above the laboratory’s detection limits were detected at nine of the ten sample points. Trace metals and / or low level VOCs were detected in the samples taken

near the former 4,000 gallon gasoline tank near the main office building (location S-1), in the field to the east of the plant formerly used for agriculture and as a spray irrigation site (location S-2), in the vicinity of the petroleum ASTs and dispenser near the truck scales (location S-3), in the former truck maintenance facility (S-4), in the vicinity of the waste water treatment plant (location S-5), in the vicinity of the former 3,000 gallon gasoline and 2,000 gallon diesel USTs (location S-8), 2-Methlynapthalene was also detected at this location, and in the vicinity of the abandoned 2,000 gallon heating oil USTs (location S-9). Sample location S-6 near the #6 heating oil AST did not reveal any target compounds. These results are tabulated in Appendix D; none of the target compounds that were detected were above the current standards. A copy of the laboratory analytical results (F&R work order # 050963) and chain of custody for the soil samples can be found in Appendix E. The Notes and Definition section at the end of the analytical report list the Q value associated with the detection of the non-target compounds. This value indicates a degree to which the detected compound has been matched to a compound in the library database. The higher the Q value, the better the match. When the Q value is below a certain range, the compound is reported as an unknown. The soil sample with the highest concentration of library search compounds was S-5 @ 1’ with ~7,752 ppm. This sample was collected near the wastewater treatment plant. These compounds included hexadecanoic acid (AKA palmitic acid) at an estimated concentration of 5,210 ppm; this chemical is a saturated fatty acid. It occurs in natural fats and oils and in tall oil and in most commercial-grade stearic acid. It is used to manufacture metallic palmitates, soaps, lube oils, waterproofing and food-grade additives. They included tetradecanoic acid (AKA Myristic acid) at an estimated concentration of 1,350 ppm; this chemical occurs in sperm oil and is used in soaps, cosmetics, synthesis of esters for flavors and perfumes, and a component of food-grade additives. They also included octadecanoic acid (AKA Stearic acid) at an estimated concentration of 1,060 ppm; which is the most common fatty acid occurring in natural animal and vegetable fats. Most commercial stearic acid is 45% palmitic acid, 50% stearic acid and 5% oleic acid. It is used in lubricants, soaps, pharmaceuticals and cosmetics, shoe and metal polishes, coatings, food packaging, suppositories and ointments. Sulfur was identified in five of the soil samples at a maximum estimated concentration of 86.2 ppm in S-9 @ 1’ collected in the vicinity of the abandoned 2,000 gallon heating oil USTs. In the United States of America, Sulfur is native in Texas and Louisiana and it is used to manufacture sulfuric acid, in pulp and paper manufacturing, carbon disulfide, rubber vulcanization, detergents, petroleum refining, dyes and chemicals, drugs and pharmaceuticals, explosives, insecticides, rodent repellents, soil conditioner, fungicide, coating for controlled-release fertilizers, nucleating agent for photographic film, cement sealant, binder and asphalt extender in road paving, base material for low-temperature mortars.

5.0 Findings – Groundwater Sampling F&R installed two 1-inch diameter monitoring wells using the push probe unit. GW-1 was installed to a depth of 15.5 feet and GW-2 was installed to a depth of 16 feet. The wells were installed in accordance with MDE requirements and good environmental practices. At the surface, flush mounted curb-boxes were installed to protect the well points; the construction records for these two wells are included in Appendix C. After proper development of the wells, F&R obtained one (1) sample from each well. Monitoring wells MW-10 and MW-16 were also sampled during this event since they previously revealed low level concentrations of benzene. These samples were then analyzed for Volatile Organic Compounds (VOCs) with a library search for non-targeted VOCs. A copy of the laboratory analytical results (F&R work order # 050963) and chain of custody for the groundwater samples can be found in Appendix F. Since no target compounds were detected above the laboratory’s quantitation limits, the results were not tabulated. The library search for the non-targeted compounds did reveal estimated concentrations of Propane at 1,460 micrograms per liter (ug/L) or parts per billion (ppb), Butane at 5 ug / L, and an unknown analyte at 164 ug/L in MW-10. Tetrahydrofuran was detected at an estimated concentration of 5 ug/L in MW-16. Propane and Butane are usually derived from petroleum and natural gas and are used for fuel, refrigerant and aerosol propellant. Tetrahydrofuran (THF) is used as a solvent for natural and synthetic resins. There are currently no established reporting standards for these compounds. 6.0 Site Specific Water Level Information Using MW-1 as a benchmark with an assumed elevation of 100 feet on the casing, the relative elevations on the casing of the original wells were surveyed to establish a relative elevation to the benchmark. Using this information the relative elevation of groundwater in selected monitoring well was calculated for the September 2, 2005, measurements. The resulting groundwater elevations and graphical groundwater flow representation are included on the Monitoring Well Location (Drawing No. 3.1) in Appendix A. 7.0 Quality Assurance / Quality Controls Since the push probe uses disposable soil sample collection tubes, no rinsate blank for the soil sampling equipment was needed. One field blank was prepared for the groundwater samples using distilled water. This sample was tested for VOCs using EPA method 8260 with a library search. The results of this test did not reveal and target or non-target compounds. The analytical report for this sample is included in Appendix F.

8.0 Conclusions Based on the results of the soil and groundwater sampling events, and the criteria established in the MDE letter dated August 12, 2005, it is the opinion of F&R that the former Tyson Foods Processing Plant at 9943 Old Ocean City Boulevard has supplied the requested information for MDE review and use. The non-target compounds noted in section 5.0, appear to originate from the chicken processing or routine maintenance of the facilities. Based on the findings and data gathered, F&R recommends that Tyson request a Notice of Compliance letter be issued for this site stating no further action is required. 9.0 Limitations This report has been prepared for the exclusive use of Tyson Foods and its subsidiaries for specific application to the Former Tyson Foods - Berlin processing plant. No other warranty, expressed or implied, is made. The evaluation and recommendations presented in this report were developed from a consideration of the project characteristics and an interpretation of observations made during completion of the test borings and of data recorded in the field using normally accepted environmental sampling protocol and reasonable professional judgment. Although individual test borings are considered to be representative of the subsurface conditions at the precise boring locations on the date shown, they are not necessarily indicative of the subsurface conditions at other locations or at other times of the year. Actual soil variations can be best evaluated during disturbance of subsurface conditions, and if necessary, minor changes can be made at that time. If such variations become apparent during any construction/soil disturbance, then it will be necessary to re-evaluate our recommendations based on these variations. References: Hawley’s Condensed Chemical Dictionary, Eleventh Edition

APPENDIX A

SITE VICINITY MAPS / SITE MAPS

APPENDIX B MDE LETTER

August 12, 2005 James H. Mardis, Group Director Environmental Services Tyson Foods, Inc. 2210 W. Oaklawn Drive (Mail Code AR058120) Springdale, Arkansas 72762-6999 Re: Voluntary Cleanup Program Application Tyson Chicken, Inc. Property Berlin, Maryland 21811 Dear Mr. Mardis:

The Voluntary Cleanup Program (“VCP”) of the Maryland Department of the Environment (“Department”) has reviewed the application package for the Tyson Chicken, Inc. property located at 9943 Old Ocean City Boulevard in Berlin, Worcester County, Maryland. Prior to a final evaluation of this application, you are requested to submit written responses to the enclosed comments. The requested information must be accompanied by another statement of certification (see Section XIII of the application).

The Department is proposing limited supplemental soil and ground water samples as described in the enclosed comments. The supplemental sampling will fulfill the principals for a Phase II site assessment, as defined by the American Society for Testing and Materials (E1903), for evaluating recognized environmental conditions identified at the property. If the requested sampling identifies additional contaminant levels of concern in the media sampled, the Department may request additional sampling for characterization purposes. Please notify the Department at least two weeks prior to beginning the sampling, so that we have an opportunity to oversee sampling activities and to collect split samples.

Both field screening technology and fixed laboratory sampling can be used to

characterize the property. A copy of the MDE Screening Sample Collection Protocol and Request For MDE Sample Screening Analytical Services are attached. If you would like additional information on utilizing the MDE field screening services, please contact Barbara Brown, the project manager, at 410-537-3493.

James H. Mardis, Group Director Page Two

You may be interested in participating in the Brownfields Site Assessment Initiative,

which provides funding to conduct site assessments at private and publicly owned Brownfields sites. Please contact James Carroll, Program Administrator, at 410-537-3493, if you would like additional information on the Brownfields Site Assessment Initiative.

After receiving and evaluating the additional information, we will notify you in writing

whether the property has been accepted for participation in the Voluntary Cleanup Program. If denied, the reasons for denial will be provided. This evaluation will be finalized as soon as possible following the Department’s receipt of the requested information.

If you have any questions regarding the enclosed comments or other aspects of the

program, please contact Barbara Brown, the project manager, or me at 410-537-3493.

Sincerely, James W. Metz, Chief Voluntary Cleanup/Brownfields Division JWM/bhb Enclosure cc: Mr. Horacio Tablada Mr. James R. Carroll Ms. Barbara H. Brown

of 8

Voluntary Cleanup Program

Tyson Chicken, Inc. Property 9943 Old Ocean City Boulevard

Berlin, Maryland 21811

Comments on the Application Package (1) Briefly describe the future plans for the property, if known. Such information

should include which existing buildings are to be demolished and/or renovated and whether the concrete slab(s) will also be removed.

(2) Indicate whether wastewater treatment system and lagoons will remain on site as

an operable wastewater treatment system. If the wastewater treatment system and lagoons are to be closed by Tyson, please provide a schedule and copy of the closure plan demonstrating that such actions are taken in accordance with applicable local, state and federal requirements.

(3) Please describe the intended usage for the three production wells located at the

property. (4) Provide a tabular summary and indicate on a scaled site location map all

underground and aboveground storage tanks. For each tank indicate the capacity, material stored and date removed/abandoned, if applicable.

(5) Provide a list of all hazardous chemicals (solvents, acids, petroleum products etc.)

used at the Tyson Chicken site. Briefly describe disposal procedures for any chemical wastes generated on-site.

(6) Provide a tabular summary and indicate on a scaled site location map all

transformers (ground and pole mounted) on site. For each transformer, please indicate the type (PCB or non-PCB), date installed and date tested, if available.

(7) Supplemental Site Investigation

Since the entire 68 acre site has not been adequately characterized and development plans for the property have not been finalized, additional sampling is requested because of the following: 1) to evaluate vapor intrusion or soil contact risks from petroleum contaminated soils resulting from past usage of underground and aboveground tanks; 2) to evaluate potential impacts from past agricultural usage on portions of the property; 3) to evaluate potential environmental impacts from the operation of the truck and plant maintenance shops; and 4) the site is located in a ground water use area with three existing production wells. a. Soil Sampling

Soil samples should be collected at the locations indicated on Figures 1 and 1A and analyzed for the parameters described in Table 1. Each surface (1-2

of 8

ft.) and subsurface (4-5 ft.) grab sample must be collected and analyzed for parameters outlined in Table 1.

Additional grab samples may be required if contamination is observed at depths other than those indicated in Table 1. If unusual conditions such as staining, discoloration, odor, and/or liquid are observed within the soil and/or overburden profile, a sample must be collected at this discrete depth and laboratory analyzed for the full suite of parameters (e.g. VOCs - EPA Method 8260; semi-volatile organic compounds - EPA Method 8270; priority pollutant metals-EPA Series 200.8; pesticides/herbicides, and PCBs, EPA Method 8081 and 8082) and/or field screen for the full suite of parameters (ie. VOCs, PCBs, cPAHs, metals).

b. Groundwater Sampling In order to characterize the shallow aquifer, two small diameter-monitoring wells should be installed at the locations indicated on Figure 1 and analyzed for the parameters outlined in Table 4.

(8) Gauge all existing and new monitoring wells and provide a tabular summary of the data that includes the casing elevation and depth to water. Based on the ground water data collected, prepare a ground water contour map and indicate the ground water flow direction.

(9) If additional fill is to be emplaced at the site, certified “clean fill” must be used.

Prior to placing fill at the site please provide the following information:

a. Submit a report to the Department outlining the protocol for ensuring that imported material is “clean” [e.g. source of material, quantity of imported material from each source, sample frequency, number of samples, volume of clean fill, type of sample (composite vs. grab), analytical parameters, quality assurance/quality control measures].

b. Any analytical data for imported material used to certify that the material is

“clean” must be submitted to the Department for review and approval prior to use on site.

(11) Quality Assurance/Quality Controls a. Please note that hazardous substances classified as carcinogenic generally

have a cleanup standard concentration established at a target cancer risk of 10-6. This level is one order of magnitude more protective than the remedial action requirement of 10-5 established by the Department. This safety factor allows for accounting of potential additive risk factors from a multiple of hazardous substances at a property (refer to MDE Cleanup Standards for Soil & Groundwater – August 2001, Interim Final Guidance, Update No. 1).

b. The Department recommends that quality assurance and quality control

measures be implemented during the sampling program. Refer to Attachment

of 8

A for details on the recommended project deliverables to submit to the Department for review.

c. Low detection limits must be obtained during sample analyses. The detection

limits for soil samples should be comparable to the Department’s residential clean-up standards for soil.

(12) Investigatory Derived Material

Please note that all drill cuttings and purged water generated from the installation of wells or piezometers must be properly containerized and characterized to determine appropriate disposal method. Any borehole (e.g. piezometer) that intercepts the water table for ground water monitoring purposes is considered a “well” and must be abandoned according to the State of Maryland well abandonment standards [Code of Maryland Regulations 26.04.04.11].

of 8

Attachment A Recommended Data Deliverables

Recommended

Submittals to MDE Do not submit unless requested by MDE1

Data Deliverable Level I: Analytical data X Sample collection date X Laboratory receipt date X Laboratory analysis date and time X Laboratory analysis Ids X Sample Ids X Surrogate spike recovery results (GC and GC/MS data) X

Copy-of-chain of custody X Data Deliverable Level II: Instrument calibration data X Method and reagent blank results X Data Deliverable Level III Sample preparation/extraction dates X MS/MSD results X Initial/continuing calibration verification results X

Reference standards and I.C.S. recoveries X Instrument time specifications for GC/MS analysis X

Internal standard summaries X Data Deliverable Level IV: Copies of internal chain-of-custody forms X Copies of preparation logs X Tentatively Identified Compound (TIC) results 2 X

Complete ICP information X Raw data X

SS The laboratory must be able to provide this information to MDE upon request. SS TICs presented in a summary table of the (10) most likely TIC VOCs and (20) most

likely TIC SVOCs for each sample ID

of 8

Table 1: Soil Sampling Plan for the Tyson Chicken, Inc. Property Berlin, Maryland 21811

Media Sample Location

Sample Depth

Analytical Parameters RATIONALE

Soil S-1

1 to 2 ft*. 4 to 5 ft.**

VOCs (EPA Method 8260), SVOCs (EPA Method 8270) and PPL metals (EPA Method 200 series).

To characterize soil conditions in the vicinity of the former 4000-gallon gasoline tank. To evaluate potential vapor intrusion pathways.

S-2

1 to 2 ft.* 4 to 5 ft.

VOCs (EPA Method 8260), SVOCs (EPA Method 8270) and PPL metals (EPA Method 200 series), Pesticides and Herbicides (EPA methods 8081 and 8151).

To characterize soil conditions in an area historically used for agricultural purposes and as a spray irrigation site for waste disposal.

S-3 1 to 2 ft.* 4 to 5 ft**

VOCs (EPA Method 8260), SVOCs (EPA Method 8270) and PPL metals (EPA Method 200 series)

To characterize soil conditions in the vicinity of the petroleum ASTs and dispenser. This area was not previously sampled.

S-4 1 to 2 ft.* 4 to 5 ft


To characterize soil conditions in the former truck maintenance facility near an abandoned drain identified in the Phase I report. This area was not previously sampled.

S-5 1 to 2 ft.* 4 to 5 ft


To characterize soil conditions in the vicinity of the waste water treatment plant. This area was not previously sampled.

S-6 1 to 2 ft.* 4 to 5 ft**


To characterize soil conditions in the vicinity of the #6 Oil above ground tank. This area was not previously sampled.

S-7 1 to 2 ft.* 4 to 5 ft**


To characterize soil conditions in the vicinity of the 12,000- gallon UST tank removed in 1988.

S-8 1 to 2 ft.* 4 to 5 ft**


To characterize soil conditions in the vicinity of the former tank field containing the 2,000 and 3,000 -gallon tanks

S-9 1 to 2 ft.* 4 to 5 ft**


To characterize soil conditions in the vicinity of the previously abandoned UST. Samples were not collected from intervals where odors and elevated field screening readings were observed during the previous site investigation

S-10 1 to 2 ft.

PCBs (EPA Method 8082) To characterize soil conditions in the vicinity of the pad mounted transformers.

S-11 1 to 2 ft. PCBs (EPA Method 8082) To characterize soil conditions in the vicinity of the pad mounted transformers.

*Surface (1-2’) VOC analysis is not required unless field conditions warrant (i.e. visual or olfactory observations and/or elevated PID readings). **All borings in former tank field areas should be extended to 15 feet below grade or to the shallow ground water interface- subsurface sample locations will be selected based on field screening and other field observations. Soil QA/QC Parameters

Rinsate Blank (one sample/sampling episode)


Rinsate blank if soil sampling equipment is decontaminated. One sample per sampling episode. Not required if dedicated sampling equipment is used.

of 8

Table 2: Ground Water Sampling Plan for Tyson Chicken, Inc. Property Berlin, Maryland 21811

Sample Location Analytical Parameters RATIONALE

Proposed Monitoring Wells GW-1 VOCs (EPA method 8260) To characterize ground water conditions in the

vicinity of the former 4000-gallon gasoline underground storage tank.

GW-2 VOCs (EPA method 8260) To characterize ground water conditions in the vicinity of the former truck maintenance facility. This area was not previously characterized.

Existing Monitoring Wells MW-16 VOCs (EPA method 8260) To verify previous sample results

Ground Water QA/QC Parameters Blank

(Field Blank) VOCs (EPA method 8260) One field blank is required per matrix for

approximately every 10 samples submitted to the lab.

of 8

Figure 1 Sample Location Plan Tyson Chicken, Inc. Property Berlin, Maryland 21811

S-1

S-2

S-3

S-4

GW-2

See Figure 1A for additional sample locations

GW-1

of 8

Figure 1A Sample Location Plan Tyson Chicken, Inc. Property

Berlin, Maryland 21811

S-5

S-6

S-7 S-8

S-9

S-11

S-10

Legend

Soil Sample Ground Water Sample

*Approximate sampling locations shown on Figures 1 and 1A. Exact sampling locations will be determined in the field.

APPENDIX C PROBE LOG AND WELL CONSTRUCTION RECORDS

S1/GW1

Sample Depth in ft. Soil Characterization PID Result

1-4 Loam, Sand, Clay 0.0 ppm

4-8 Sand, Clay Light Gray 0.0 ppm


Well set at 15’6”, sand packed, bentonite, grout, flush mount cover

10’ slotted screen, 6’ riser

S2




S3


1-4 Dark Brown, Med Brown, Odor 25.5 ppm

7.5 ppm

3.1 ppm

4-8 Med Brown, Sand Moist Odor 22.0 ppm

0.0 ppm

0.0 ppm

GW2

Well set at 16’, sand packed, bentonite, grout, flush mount cover

10’ slotted screen, 6’ riser

S4




S5



0.0 ppm

3.1 ppm

4.6 ppm

4-8 Sand, Clay Light Gray 0.0 Ppm

4.4 ppm

4.0 ppm

0.0 ppm

S6



0.3 ppm

6.7 ppm

4.0 ppm


0.9 ppm

1.6 ppm

1.9 ppm

S7 This testing location was cancelled by MDE on-site representative

S8


1-4 Loam, Sand, Clay,odor 22.6 ppm

8.1 ppm

0.0 ppm

4.6 ppm

4-8 Sand, Clay Light Gray 0.0 Ppm

3.4 ppm

1.2 ppm

0.9 ppm

8-12 Clay, Sand 3.4 ppm

3.4 ppm

5.2 ppm

S9


1-4 Loam, Sand, Odor 1.3 ppm

17.3 ppm

27.6 ppm

0.0 ppm

4-8 Sand, Loam, Moist 0.3 ppm

3.0 ppm

1.6 ppm

0.0 ppm

S10 Sampled for PCB’s only

S11 Sampled for PCB’s only

APPENDIX D TABULATIONS OF SOIL RESULTS

Summary of Soil Laboratory Analytical ResultsTyson Foods, IncBerlin, Maryland

Analyte S-1 @ 1' S-1 @ 6' S-2 @ 1' S-2 @ 5' S-3 @ 1' S-3 @ 5' sample ID Non-Res. Cleanup Standard*

Date 9/1/2005 9/1/2005 9/1/2005 9/1/2005 9/1/2005 9/1/2005 VOCs (mg/kg)Acetone 0.032 0.052 2.0E+042-Butanone (MEK) 0.011 1.2E+05Xylenes 0.032 4.1E+05Library Search <1 1 NSE

SVOCs2-Methylnapthalene 4.1E+03Library Search 3 9 3 2 26 <1 NSE

Pesticides / PCBs

InorganicsArsenic 3.8E+00Beryllium 0.21 0.22 0.26 0.29 0.22 4.1E+02Copper 0.8 2 1 3 2 8.2E+03Chromium** 3.1E+05Lead 2 3 7 6 3 4.0E+02Nickel 2.5 5 4 4.2 3.3 4.1E+03Zinc 6 6.7 9 9.8 6.20 6.1E+04

NA = Not AnalyzedBlank = Below Detection Limit or Not AnalyzedNSE = No Standard Established* ref. Table 1 of MDE Cleanup Standards for Soil and GW** The standard for this analyte is based upon the standard for Chromium III

1



Date 9/1/2005 9/1/2005 9/1/2005 9/1/2005 9/1/2005 9/1/2005 VOCs (mg/kg)Acetone 0.018 0.035 2.0E+042-Butanone (MEK) 1.2E+05Xylenes 4.1E+05Library Search NSE

SVOCs2-Methylnapthalene 4.1E+03Library Search <1 <1 7,752 60 59 15 NSE

Pesticides / PCBs

InorganicsArsenic 3.8E+00Beryllium 0.36 0.24 4.1E+02Copper 0.6 2 3 2 8.2E+03Chromium** 3.1E+05Lead 4 4 8 2 4.0E+02Nickel 5.2 3.3 2.3 2.6 4.1E+03Zinc 10.9 6.4 34.3 7.3 6.1E+04


2



Date 9/1/2005 9/1/2005 9/1/2005 9/1/2005 9/1/2005 9/1/2005 VOCs (mg/kg)Acetone 0.065 0.075 0.043 0.052 2.0E+042-Butanone (MEK) 0.013 0.006 1.2E+05Xylenes 4.1E+05Library Search <1 NSE

SVOCs2-Methylnapthalene 0.3 4.1E+03Library Search 84 124 50 NSE

Pesticides / PCBs

InorganicsArsenic 1 3.8E+00Beryllium 0.53 22 0.36 0.29 4.1E+02Copper 5 2 2 1 8.2E+03Chromium** 7 7 3.1E+05Lead 8 5 7 2 4.0E+02Nickel 5.2 2.5 3.8 4.2 4.1E+03Zinc 19.3 10.4 16.8 6.7 6.1E+04


3

APPENDIX E SOIL ANALYTICAL REPORT

FROEHLING & ROBERTSON, INC GEOTECHNICAL ENVIRONMENTAL MATERIALS

ENGINEERS LABORATORIES “OVER ONE HUNDRED YEARS OF SERVICE”

CERTIFICATE OF ANALYSIS

Page 1 of 69September 23, 2005

RECEIVED: 09/06/05

PROJECT: PROJECT NO.:

Tyson Foods, Inc. (GA) 13264 Mountain Rd. Glen Allen VA, 23059

LAB#:

SAMPLED BY:

CLIENT:

Ed Setzer

Doug Baxter Berlin

0509063

Results to follow.

Audrey Brubeck Manager Analytical Laboratory Services HEADQUARTERS: 3015 DUMBARTON ROAD BOX 27524 RICHMOND, VA 23261-7524 TELEPHONE (804) 264-2701 FAX (804) 264-1202 www.FandR.com BRANCHES: ASHEVILLE, NC BALTIMORE, MD CHARLOTTE, NC CHESAPEAKE, VA CROZET, VA FAYETTEVILLE, NC FREDERICKSBURG, VA GREENVILLE, SC HICKORY, NC RALEIGH, NC ROANOKE, VA STERLING, VA

CERTIFICATIONS: VIRGINIA DRINKING WATER - 00150 NORTH CAROLINA DENR - 432 SOUTH CAROLINA DHEC- 93010001 & 93010 MARYLAND DRINKING WATER - 279

of 69

ResultAnalyte LimitQuant

Prepared Analyzed Method Notes Units

S-1 @ 1' 0509063-01 (Soil)

9/1/05 8:52 Client ID: Sampled Date/Time:

Analyst

Lab ID:

Metals BQL SW846/6010 mg/kg dry Silver 1 9/9/05 9:15 JLW 9/13/05 17:16 BQL " " Arsenic 0.5 9/9/05 9:15 JLW 9/12/05 14:00

" 0.21 " Beryllium 0.15 9/9/05 9:15 JLW 9/12/05 14:00 BQL " " Cadmium 0.5 9/9/05 9:15 JLW 9/12/05 14:00

" 4 " Chromium 0.5 9/9/05 9:15 JCM 9/12/05 14:03 " 0.8 " Copper 0.5 9/9/05 9:15 JLW 9/12/05 14:00

BQL SW846/7471 A " Mercury 0.07 9/8/05 9:05 JCM 9/8/05 16:18 SW846/6010 2.5 " Nickel 0.5 9/9/05 9:15 JLW 9/12/05 14:00

" 2 " Lead 0.5 9/9/05 9:15 JLW 9/12/05 14:00 BQL " " Antimony 10 9/9/05 9:15 JLW 9/13/05 13:27 BQL " " Selenium 0.5 9/9/05 9:15 JLW 9/12/05 14:00 BQL SW846 6010 " Thallium 0.5 9/9/05 9:15 JLW 9/12/05 14:00

SW846/6010 6.0 " Zinc 0.5 Blank, B9/9/05 9:15 JLW 9/12/05 14:00 Semivolatile Organic Compounds

BQL SW846/8270C mg/kg dry Acenaphthene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Acenaphthylene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Anthracene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Benzo(a)anthracene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Benzo(b)fluoranthene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Benzo(k)fluoranthene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Benzo(g,h,i)perylene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Benzo(a)pyrene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Bis(2-chloroethoxy)methane 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Bis(2-chloroethyl)ether 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Bis(2-chloroisopropyl)ether 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 4-Bromophenylphenylether 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Bis(2-ethylhexyl)phthalate 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Butyl benzyl phthalate 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 4-Chloroaniline 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 4-Chloro-3-methylphenol 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 2-Chloronaphthalene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 2-Chlorophenol 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 4-Chlorophenylphenylether 0.3 9/8/05 15:30 JHV 9/16/05 21:24

of 69



S-1 @ 1' 0509063-01 (Soil)


Analyst

Lab ID:

Semivolatile Organic Compounds BQL SW846/8270C mg/kg dry Chrysene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Dibenz(a,h)anthracene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Dibenzofuran 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Di-n-butyl phthalate 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 3,3'-Dichlorobenzidine 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 2,4-Dichlorophenol 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Diethyl phthalate 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 2,4-Dimethylphenol 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Dimethyl phthalate 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 4,6-Dinitro-2-methylphenol 0.5 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 2,4-Dinitrophenol 1.1 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 2,4-Dinitrotoluene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 2,6-Dinitrotoluene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Di-n-octyl phthalate 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Fluoranthene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Fluorene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Hexachlorobenzene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Hexachlorobutadiene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Hexachlorocyclopentadiene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Hexachloroethane 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Isophorone 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Indeno(1,2,3-cd)pyrene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 2-Methylnaphthalene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 2-Methylphenol 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 4-Methylphenol 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 2-Nitroaniline 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 3-Nitroaniline 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 4-Nitroaniline 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Nitrobenzene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 2-Nitrophenol 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 4-Nitrophenol 1.1 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " N-Nitrosodiphenylamine 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " N-Nitroso-di-n-propylamine 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Pentachlorophenol 1.1 9/8/05 15:30 JHV 9/16/05 21:24

of 69



S-1 @ 1' 0509063-01 (Soil)


Analyst

Lab ID:

Semivolatile Organic Compounds BQL SW846/8270C mg/kg dry Phenanthrene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Phenol 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " Pyrene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 1,2,4-Trichlorobenzene 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 2,4,5-Trichlorophenol 0.3 9/8/05 15:30 JHV 9/16/05 21:24 BQL " " 2,4,6-Trichlorophenol 0.3 9/8/05 15:30 JHV 9/16/05 21:24

Semivolatile Organic Compound Library Search SW846/8270C 1.11 mg/kg dry 2,3-dimethyl-2-nitro-butane 0.4 QVALe9/8/05 15:30 JHV 9/20/05 11:26

" 1.04 " Unknown compound 0.4 9/8/05 15:30 JHV 9/20/05 11:26 " 0.616 " Toluene 0.4 QVALt9/8/05 15:30 JHV 9/20/05 11:26

of 69



S-1 @ 6' 0509063-02 (Soil)


Analyst

Lab ID:



" 7 " Chromium 0.5 9/9/05 9:15 JCM 9/12/05 14:03 " 2 " Copper 0.5 9/9/05 9:15 JLW 9/12/05 14:00



SW846/6010 6.7 " Zinc 0.5 Blank, B9/9/05 9:15 JLW 9/12/05 14:00 Semivolatile Organic Compounds


of 69



S-1 @ 6' 0509063-02 (Soil)


Analyst

Lab ID:


of 69



S-1 @ 6' 0509063-02 (Soil)


Analyst

Lab ID:


Semivolatile Organic Compound Library Search SW846/8270C 3.51 mg/kg dry 2,3-dimethyl-2-nitro-butane 0.3 QVALe9/8/05 15:30 JHV 9/20/05 11:26

" 1.83 " 1-nonadecanol 0.3 QVALq9/8/05 15:30 JHV 9/20/05 11:26 " 0.392 " diethyl benzene 0.3 QVALs9/8/05 15:30 JHV 9/20/05 11:26 " 1.23 " Unknown compound 0.3 9/8/05 15:30 JHV 9/20/05 11:26 " 3.13 " Unknown compd 0.3 9/8/05 15:30 JHV 9/20/05 11:26 " 0.419 " Toluene 0.3 QVALaa9/8/05 15:30 JHV 9/20/05 11:26

Volatile Organic Compounds BQL SW846/8260B mg/kg dry Methyl tert-Butyl Ether 0.006 9/14/05 13:08 SS 9/14/05 22:21

" 0.032 " Acetone 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Benzene 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Bromochloromethane 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Bromodichloromethane 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Bromoform 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " 2-Butanone (MEK) 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Carbon disulfide 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Bromomethane 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Carbon tetrachloride 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Chlorobenzene 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Chloroethane 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Chloroform 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Chloromethane 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Dibromochloromethane 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " 1,2-Dibromo-3-chloropropane 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " 1,2-Dibromoethane 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " 1,2-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " 1,3-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/14/05 22:21

of 69



S-1 @ 6' 0509063-02 (Soil)


Analyst

Lab ID:

Volatile Organic Compounds BQL SW846/8260B mg/kg dry 1,4-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " 1,1-Dichloroethane 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " 1,2-Dichloroethane 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " 1,1-Dichloroethene 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " cis-1,2-Dichloroethene 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " trans-1,2-Dichloroethene 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " 1,2-Dichloropropane 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " cis-1,3-Dichloropropene 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " trans-1,3-Dichloropropene 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Ethylbenzene 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " 2-Hexanone 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Isopropylbenzene 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Methylene chloride 0.024 9/14/05 13:08 SS 9/14/05 22:21 BQL " " 4-Methyl-2-pentanone (MIBK) 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Styrene 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " 1,1,2,2-Tetrachloroethane 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Tetrachloroethene 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Toluene 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " 1,1,1-Trichloroethane 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " 1,1,2-Trichloroethane 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Trichloroethene 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Vinyl chloride 0.006 9/14/05 13:08 SS 9/14/05 22:21 BQL " " Total Xylenes 0.018 9/14/05 13:08 SS 9/14/05 22:21

Volatile Organic Compounds Library Search SW846/8260 B 0.012 mg/kg dry Hexane, 2,2-dimethyl 0.006 QVALb9/14/05 13:09 SS 9/14/05 22:21

" 0.010 " Nonane, 4-methyl- 0.006 QVALn9/14/05 13:09 SS 9/14/05 22:21 " 0.010 " Benzene, 1,2,4,5-tetramethyl- 0.006 QVALx9/14/05 13:09 SS 9/14/05 22:21 " 0.011 " Benzene, 1,3-diethyl- 0.006 QVALx9/14/05 13:09 SS 9/14/05 22:21 " 0.018 " Benzene, 1-methyl-2-(1-methylethyl) 0.006 QVALz9/14/05 13:09 SS 9/14/05 22:21 " 0.009 " Benzene, 1-methyl-3-propyl- 0.006 QVALk9/14/05 13:09 SS 9/14/05 22:21 " 0.012 " Benzene, 1-propenyl-, (E)- 0.006 QVALp9/14/05 13:09 SS 9/14/05 22:21 " 0.013 " Benzene, 1,2,3,4-tetramethyl- 0.006 QVALv9/14/05 13:09 SS 9/14/05 22:21 " 0.008 " 1H-Indene,2,3-dihydro-1,1,3-trimethyl 0.006 QVALz9/14/05 13:09 SS 9/14/05 22:21

of 69



S-1 @ 6' 0509063-02 (Soil)


Analyst

Lab ID:

Volatile Organic Compounds Library Search SW846/8260 B 0.009 mg/kg dry Hexane, 2,2,5-trimethyl- 0.006 QVALg9/14/05 13:09 SS 9/14/05 22:21

of 69



S-2 @ 1' 0509063-03 (Soil)


Analyst

Lab ID:






SW846/6010 9.0 " Zinc 0.5 B, Blank9/9/05 9:15 JLW 9/12/05 14:00 Chlorinated Herbicides (subcontracted to Primary Labs)

BQL SW846/8151A mg/kg dry 2,4-D 0.002 sub-19/16/05 10:58 sub 9/16/05 10:58 BQL " " Dinoseb 0.002 sub-19/16/05 10:58 sub 9/16/05 10:58 BQL " " Pentachlorophenol 0.002 sub-19/16/05 10:58 sub 9/16/05 10:58 BQL " " 2,4,5-T 0.002 sub-19/16/05 10:58 sub 9/16/05 10:58 BQL " " 2,4,5-TP (Silvex) 0.002 sub-19/16/05 10:58 sub 9/16/05 10:58

Organochlorine Pesticides (subcontracted to Primary Labs) BQL SW846/8081A mg/kg dry Aldrin 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " alpha-BHC 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " beta-BHC 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " delta-BHC 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " gamma-BHC 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " 4,4'-DDD 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " 4,4'-DDE 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " 4,4'-DDT 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Dieldrin 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Endosulfan I 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Endosulfan II 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Endosulfan sulfate 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Endrin 0.001 A-019/8/05 16:00 sub 9/21/05 17:10

of 69



S-2 @ 1' 0509063-03 (Soil)


Analyst

Lab ID:

Organochlorine Pesticides (subcontracted to Primary Labs) BQL SW846/8081A mg/kg dry Endrin aldehyde 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Heptachlor 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Heptachlor epoxide 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Methoxychlor 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Chlordane 0.002 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Toxaphene 0.002 A-019/8/05 16:00 sub 9/21/05 17:10

Semivolatile Organic Compounds BQL SW846/8270C mg/kg dry Acenaphthene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Acenaphthylene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Anthracene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Benzo(a)anthracene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Benzo(b)fluoranthene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Benzo(k)fluoranthene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Benzo(g,h,i)perylene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Benzo(a)pyrene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Bis(2-chloroethoxy)methane 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Bis(2-chloroethyl)ether 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Bis(2-chloroisopropyl)ether 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 4-Bromophenylphenylether 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Bis(2-ethylhexyl)phthalate 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Butyl benzyl phthalate 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 4-Chloroaniline 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 4-Chloro-3-methylphenol 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 2-Chloronaphthalene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 2-Chlorophenol 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 4-Chlorophenylphenylether 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Chrysene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Dibenz(a,h)anthracene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Dibenzofuran 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Di-n-butyl phthalate 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 3,3'-Dichlorobenzidine 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 2,4-Dichlorophenol 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Diethyl phthalate 0.3 9/8/05 15:30 JHV 9/16/05 22:36

of 69



S-2 @ 1' 0509063-03 (Soil)


Analyst

Lab ID:

Semivolatile Organic Compounds BQL SW846/8270C mg/kg dry 2,4-Dimethylphenol 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Dimethyl phthalate 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 4,6-Dinitro-2-methylphenol 0.6 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 2,4-Dinitrophenol 1.2 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 2,4-Dinitrotoluene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 2,6-Dinitrotoluene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Di-n-octyl phthalate 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Fluoranthene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Fluorene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Hexachlorobenzene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Hexachlorobutadiene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Hexachlorocyclopentadiene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Hexachloroethane 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Indeno(1,2,3-cd)pyrene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Isophorone 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 2-Methylnaphthalene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 2-Methylphenol 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 4-Methylphenol 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 2-Nitroaniline 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 3-Nitroaniline 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 4-Nitroaniline 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Nitrobenzene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 2-Nitrophenol 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 4-Nitrophenol 1.2 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " N-Nitrosodiphenylamine 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " N-Nitroso-di-n-propylamine 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Pentachlorophenol 1.2 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Phenanthrene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Phenol 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " Pyrene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 1,2,4-Trichlorobenzene 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 2,4,5-Trichlorophenol 0.3 9/8/05 15:30 JHV 9/16/05 22:36 BQL " " 2,4,6-Trichlorophenol 0.3 9/8/05 15:30 JHV 9/16/05 22:36

of 69



S-2 @ 1' 0509063-03 (Soil)


Analyst

Lab ID:

Semivolatile Organic Compound Library Search SW846/8270C 0.889 mg/kg dry Unknown compound 0.3 9/8/05 15:30 JHV 9/20/05 11:26

" 1.04 " Unknown compd 0.3 9/8/05 15:30 JHV 9/20/05 11:26 " 0.692 " Toluene 0.3 QVALy9/8/05 15:30 JHV 9/20/05 11:26 " 0.448 " 1-nonadecanol 0.3 QVALi9/8/05 15:30 JHV 9/20/05 11:26

of 69



S-2 @ 5' 0509063-04 (Soil)


Analyst

Lab ID:






SW846/6010 9.8 " Zinc 0.5 B, Blank9/9/05 9:15 JLW 9/12/05 14:00 Chlorinated Herbicides (subcontracted to Primary Labs)

BQL SW846/8151A mg/kg dry 2,4-D 0.002 sub-19/16/05 10:58 sub 9/16/05 10:58 BQL " " Dinoseb 0.002 sub-19/16/05 10:58 sub 9/16/05 10:58 BQL " " Pentachlorophenol 0.002 sub-19/16/05 10:58 sub 9/16/05 10:58 BQL " " 2,4,5-T 0.002 sub-19/16/05 10:58 sub 9/16/05 10:58 BQL " " 2,4,5-TP (Silvex) 0.002 sub-19/16/05 10:58 sub 9/16/05 10:58

Organochlorine Pesticides (subcontracted to Primary Labs) BQL SW846/8081A mg/kg dry Aldrin 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " alpha-BHC 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " beta-BHC 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " delta-BHC 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " gamma-BHC 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " 4,4'-DDD 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " 4,4'-DDE 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " 4,4'-DDT 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Dieldrin 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Endosulfan I 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Endosulfan II 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Endosulfan sulfate 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Endrin 0.001 A-019/8/05 16:00 sub 9/21/05 17:10

of 69



S-2 @ 5' 0509063-04 (Soil)


Analyst

Lab ID:

Organochlorine Pesticides (subcontracted to Primary Labs) BQL SW846/8081A mg/kg dry Endrin aldehyde 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Heptachlor 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Heptachlor epoxide 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Methoxychlor 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Chlordane 0.003 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Toxaphene 0.003 A-019/8/05 16:00 sub 9/21/05 17:10

Semivolatile Organic Compounds BQL SW846/8270C mg/kg dry Acenaphthene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Acenaphthylene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Anthracene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Benzo(a)anthracene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Benzo(b)fluoranthene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Benzo(k)fluoranthene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Benzo(g,h,i)perylene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Benzo(a)pyrene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Bis(2-chloroethoxy)methane 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Bis(2-chloroethyl)ether 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Bis(2-chloroisopropyl)ether 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 4-Bromophenylphenylether 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Bis(2-ethylhexyl)phthalate 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Butyl benzyl phthalate 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 4-Chloroaniline 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 4-Chloro-3-methylphenol 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 2-Chloronaphthalene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 2-Chlorophenol 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 4-Chlorophenylphenylether 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Chrysene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Dibenz(a,h)anthracene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Dibenzofuran 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Di-n-butyl phthalate 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 3,3'-Dichlorobenzidine 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 2,4-Dichlorophenol 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Diethyl phthalate 0.3 9/8/05 15:30 JHV 9/16/05 23:12

of 69



S-2 @ 5' 0509063-04 (Soil)


Analyst

Lab ID:

Semivolatile Organic Compounds BQL SW846/8270C mg/kg dry 2,4-Dimethylphenol 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Dimethyl phthalate 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 4,6-Dinitro-2-methylphenol 0.6 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 2,4-Dinitrophenol 1.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 2,4-Dinitrotoluene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 2,6-Dinitrotoluene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Di-n-octyl phthalate 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Fluoranthene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Fluorene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Hexachlorobenzene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Hexachlorobutadiene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Hexachlorocyclopentadiene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Hexachloroethane 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Indeno(1,2,3-cd)pyrene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Isophorone 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 2-Methylnaphthalene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 2-Methylphenol 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 4-Methylphenol 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 2-Nitroaniline 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 3-Nitroaniline 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 4-Nitroaniline 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Nitrobenzene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 2-Nitrophenol 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 4-Nitrophenol 1.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " N-Nitrosodiphenylamine 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " N-Nitroso-di-n-propylamine 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Pentachlorophenol 1.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Phenanthrene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Phenol 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " Pyrene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 1,2,4-Trichlorobenzene 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 2,4,5-Trichlorophenol 0.3 9/8/05 15:30 JHV 9/16/05 23:12 BQL " " 2,4,6-Trichlorophenol 0.3 9/8/05 15:30 JHV 9/16/05 23:12

of 69



S-2 @ 5' 0509063-04 (Soil)


Analyst

Lab ID:

Semivolatile Organic Compound Library Search SW846/8270C 0.894 mg/kg dry Unknown compound 0.4 9/8/05 15:30 JHV 9/20/05 11:26

" 0.694 " Toluene 0.4 QVALy9/8/05 15:30 JHV 9/20/05 11:26 Volatile Organic Compounds

BQL SW846/8260B mg/kg dry Methyl tert-Butyl Ether 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Acetone 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Benzene 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Bromochloromethane 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Bromodichloromethane 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Bromoform 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Carbon disulfide 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Bromomethane 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " 2-Butanone (MEK) 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Carbon tetrachloride 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Chlorobenzene 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Chloroethane 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Chloroform 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Chloromethane 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Dibromochloromethane 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " 1,2-Dibromo-3-chloropropane 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " 1,2-Dibromoethane 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " 1,2-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " 1,3-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " 1,4-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " 1,1-Dichloroethane 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " 1,2-Dichloroethane 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " 1,1-Dichloroethene 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " cis-1,2-Dichloroethene 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " trans-1,2-Dichloroethene 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " 1,2-Dichloropropane 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " cis-1,3-Dichloropropene 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " trans-1,3-Dichloropropene 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Ethylbenzene 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " 2-Hexanone 0.006 9/14/05 13:08 SS 9/14/05 23:00

of 69



S-2 @ 5' 0509063-04 (Soil)


Analyst

Lab ID:

Volatile Organic Compounds BQL SW846/8260B mg/kg dry Isopropylbenzene 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " 4-Methyl-2-pentanone (MIBK) 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Methylene chloride 0.025 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Styrene 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " 1,1,2,2-Tetrachloroethane 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Tetrachloroethene 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Toluene 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " 1,1,1-Trichloroethane 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " 1,1,2-Trichloroethane 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Trichloroethene 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Vinyl chloride 0.006 9/14/05 13:08 SS 9/14/05 23:00 BQL " " Total Xylenes 0.018 9/14/05 13:08 SS 9/14/05 23:00

Volatile Organic Compounds Library Search SW846/8260 B mg/kg dry No non target compounds were detected 0.006 9/14/05 13:09 SS 9/14/05 23:00

of 69



S-3 @ 1' 0509063-05 (Soil)


Analyst

Lab ID:






SW846/6010 11.1 " Zinc 0.5 B, Blank9/9/05 9:15 JLW 9/12/05 14:00 Semivolatile Organic Compounds


of 69



S-3 @ 1' 0509063-05 (Soil)


Analyst

Lab ID:


of 69



S-3 @ 1' 0509063-05 (Soil)


Analyst

Lab ID:


Semivolatile Organic Compound Library Search SW846/8270C 2.66 mg/kg dry octadecane 0.3 QVALs9/8/05 15:30 JHV 9/20/05 11:26

" 2.59 " Unknown compound 0.3 9/8/05 15:30 JHV 9/20/05 11:26 " 1.42 " 4,6-dimethyl-dodecane 0.3 QVALf9/8/05 15:30 JHV 9/20/05 11:26 " 1.07 " 3,6-dimethyl-undecane 0.3 QVALaa9/8/05 15:30 JHV 9/20/05 11:26 " 2.95 " 2-methyl-octadecane 0.3 QVALm9/8/05 15:30 JHV 9/20/05 11:26 " 2.59 " Unknown compd 0.3 9/8/05 15:30 JHV 9/20/05 11:26 " 4.34 " 2,6,10-trimethyl-dodecane 0.3 QVALs9/8/05 15:30 JHV 9/20/05 11:26 " 3.19 " Hexadecane 0.3 QVALo9/8/05 15:30 JHV 9/20/05 11:26 " 2.38 " 1H-Indene,2,3-dihydro-1,1,3-trimethyl 0.3 QVALu9/8/05 15:30 JHV 9/20/05 11:26

" 4.65 " 2,6,10,14-tetramethyl-pentadecane 0.3 QVALaf9/8/05 15:30 JHV 9/20/05 11:26 Volatile Organic Compounds

BQL SW846/8260B mg/kg dry Methyl tert-Butyl Ether 0.006 9/14/05 13:08 SS 9/15/05 0:59 " 0.052 " Acetone 0.006 9/14/05 13:08 SS 9/15/05 0:59

BQL " " Benzene 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " Bromochloromethane 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " Bromodichloromethane 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " Bromoform 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " Carbon disulfide 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " Bromomethane 0.006 9/14/05 13:08 SS 9/15/05 0:59

" 0.011 " 2-Butanone (MEK) 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " Carbon tetrachloride 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " Chlorobenzene 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " Chloroethane 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " Chloroform 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " Chloromethane 0.006 9/14/05 13:08 SS 9/15/05 0:59

of 69



S-3 @ 1' 0509063-05 (Soil)


Analyst

Lab ID:

Volatile Organic Compounds BQL SW846/8260B mg/kg dry Dibromochloromethane 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " 1,2-Dibromo-3-chloropropane 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " 1,2-Dibromoethane 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " 1,2-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " 1,3-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " 1,4-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " 1,1-Dichloroethane 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " 1,2-Dichloroethane 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " 1,1-Dichloroethene 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " cis-1,2-Dichloroethene 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " trans-1,2-Dichloroethene 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " 1,2-Dichloropropane 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " cis-1,3-Dichloropropene 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " trans-1,3-Dichloropropene 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " Ethylbenzene 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " 2-Hexanone 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " Isopropylbenzene 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " Methylene chloride 0.021 9/14/05 13:08 SS 9/15/05 0:59 BQL " " 4-Methyl-2-pentanone (MIBK) 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " Styrene 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " 1,1,2,2-Tetrachloroethane 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " Tetrachloroethene 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " Toluene 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " 1,1,1-Trichloroethane 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " 1,1,2-Trichloroethane 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " Trichloroethene 0.006 9/14/05 13:08 SS 9/15/05 0:59 BQL " " Vinyl chloride 0.006 9/14/05 13:08 SS 9/15/05 0:59

" 0.032 " Total Xylenes 0.018 9/14/05 13:08 SS 9/15/05 0:59 Volatile Organic Compounds Library Search

SW846/8260 B 0.140 mg/kg dry Naphthalene, 1,2,3,4-tetrahydro-m 0.015 QVALg9/14/05 13:09 SS 9/15/05 0:59 " 0.096 " Decane, 2-methyl- 0.015 QVALa9/14/05 13:09 SS 9/15/05 0:59 " 0.174 " Nonane 0.015 QVALv9/14/05 13:09 SS 9/15/05 0:59 " 0.155 " Dodecane, 4,6-dimethyl 0.015 QVALl9/14/05 13:09 SS 9/15/05 0:59

of 69



S-3 @ 1' 0509063-05 (Soil)


Analyst

Lab ID:

Volatile Organic Compounds Library Search SW846/8260 B 0.168 mg/kg dry Decane 0.015 QVALx9/14/05 13:09 SS 9/15/05 0:59

" 0.113 " Unknown compound 0.015 9/14/05 13:09 SS 9/15/05 0:59 " 0.210 " Undecane 0.015 QVALv9/14/05 13:09 SS 9/15/05 0:59 " 0.134 " Undecane, 3-methyl- 0.015 QVALg9/14/05 13:09 SS 9/15/05 0:59 " 0.235 " Undecane, 2,6-dimethyl 0.015 QVALk9/14/05 13:09 SS 9/15/05 0:59 " 0.124 " Unknown analyte 0.015 9/14/05 13:09 SS 9/15/05 0:59

of 69



S-3 @ 5' 0509063-06 (Soil)


Analyst

Lab ID:








of 69



S-3 @ 5' 0509063-06 (Soil)


Analyst

Lab ID:

Semivolatile Organic Compounds BQL SW846/8270C mg/kg dry Chrysene 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " Dibenz(a,h)anthracene 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " Dibenzofuran 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " Di-n-butyl phthalate 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " 3,3'-Dichlorobenzidine 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " 2,4-Dichlorophenol 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " Diethyl phthalate 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " 2,4-Dimethylphenol 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " Dimethyl phthalate 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " 4,6-Dinitro-2-methylphenol 0.6 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " 2,4-Dinitrophenol 1.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " 2,4-Dinitrotoluene 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " 2,6-Dinitrotoluene 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " Di-n-octyl phthalate 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " Fluoranthene 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " Fluorene 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " Hexachlorobenzene 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " Hexachlorobutadiene 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " Hexachlorocyclopentadiene 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " Hexachloroethane 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " Indeno(1,2,3-cd)pyrene 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " Isophorone 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " 2-Methylnaphthalene 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " 2-Methylphenol 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " 4-Methylphenol 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " 2-Nitroaniline 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " 3-Nitroaniline 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " 4-Nitroaniline 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " Nitrobenzene 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " 2-Nitrophenol 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " 4-Nitrophenol 1.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " N-Nitrosodiphenylamine 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " N-Nitroso-di-n-propylamine 0.3 9/8/05 15:30 JHV 9/17/05 0:24 BQL " " Pentachlorophenol 1.3 9/8/05 15:30 JHV 9/17/05 0:24

of 69



S-3 @ 5' 0509063-06 (Soil)


Analyst

Lab ID:


Semivolatile Organic Compound Library Search SW846/8270C 0.597 mg/kg dry 2,6,10-dodecatrien-1-ol,3,7,11-trimethyl 0.4 QVALf9/8/05 15:30 JHV 9/20/05 11:26

Volatile Organic Compounds BQL SW846/8260B mg/kg dry Methyl tert-Butyl Ether 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Acetone 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Benzene 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Bromochloromethane 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Bromodichloromethane 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Bromoform 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " 2-Butanone (MEK) 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Carbon disulfide 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Bromomethane 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Carbon tetrachloride 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Chlorobenzene 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Chloroethane 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Chloroform 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Chloromethane 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Dibromochloromethane 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " 1,2-Dibromo-3-chloropropane 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " 1,2-Dibromoethane 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " 1,2-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " 1,3-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " 1,4-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " 1,1-Dichloroethane 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " 1,2-Dichloroethane 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " 1,1-Dichloroethene 0.006 9/14/05 13:08 SS 9/14/05 23:40

of 69



S-3 @ 5' 0509063-06 (Soil)


Analyst

Lab ID:

Volatile Organic Compounds BQL SW846/8260B mg/kg dry cis-1,2-Dichloroethene 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " trans-1,2-Dichloroethene 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " 1,2-Dichloropropane 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " cis-1,3-Dichloropropene 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " trans-1,3-Dichloropropene 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Ethylbenzene 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " 2-Hexanone 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Isopropylbenzene 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Methylene chloride 0.024 9/14/05 13:08 SS 9/14/05 23:40 BQL " " 4-Methyl-2-pentanone (MIBK) 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Styrene 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " 1,1,2,2-Tetrachloroethane 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Tetrachloroethene 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Toluene 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " 1,1,1-Trichloroethane 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " 1,1,2-Trichloroethane 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Trichloroethene 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Vinyl chloride 0.006 9/14/05 13:08 SS 9/14/05 23:40 BQL " " Total Xylenes 0.018 9/14/05 13:08 SS 9/14/05 23:40


of 69



S-4 @ 1' 0509063-07 (Soil)


Analyst

Lab ID:








of 69



S-4 @ 1' 0509063-07 (Soil)


Analyst

Lab ID:


Semivolatile Organic Compound Library Search SW846/8270C 0.755 mg/kg dry 2,6,10-dodecatrien-1-ol,3,7,11-trimethyl 0.4 QVALd9/8/05 15:30 JHV 9/20/05 11:26

of 69



S-4 @ 5' 0509063-08 (Soil)


Analyst

Lab ID:








of 69



S-4 @ 5' 0509063-08 (Soil)


Analyst

Lab ID:


Semivolatile Organic Compound Library Search SW846/8270C 0.876 mg/kg dry 2,6,10-dodecatrien-1-ol,3,7,11-trimethyl 0.4 QVALh9/8/05 15:30 JHV 9/20/05 11:26


" 0.018 " Acetone 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Benzene 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Bromochloromethane 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Bromodichloromethane 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Bromoform 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Carbon disulfide 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " 2-Butanone (MEK) 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Bromomethane 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Carbon tetrachloride 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Chlorobenzene 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Chloroethane 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Chloroform 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Chloromethane 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Dibromochloromethane 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " 1,2-Dibromo-3-chloropropane 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " 1,2-Dibromoethane 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " 1,2-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " 1,3-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " 1,4-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " 1,1-Dichloroethane 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " 1,2-Dichloroethane 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " 1,1-Dichloroethene 0.006 9/14/05 13:08 SS 9/15/05 0:20

of 69



S-4 @ 5' 0509063-08 (Soil)


Analyst

Lab ID:

Volatile Organic Compounds BQL SW846/8260B mg/kg dry cis-1,2-Dichloroethene 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " trans-1,2-Dichloroethene 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " 1,2-Dichloropropane 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " cis-1,3-Dichloropropene 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " trans-1,3-Dichloropropene 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Ethylbenzene 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " 2-Hexanone 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Isopropylbenzene 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " 4-Methyl-2-pentanone (MIBK) 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Methylene chloride 0.024 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Styrene 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " 1,1,2,2-Tetrachloroethane 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Tetrachloroethene 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Toluene 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " 1,1,1-Trichloroethane 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " 1,1,2-Trichloroethane 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Trichloroethene 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Vinyl chloride 0.006 9/14/05 13:08 SS 9/15/05 0:20 BQL " " Total Xylenes 0.018 9/14/05 13:08 SS 9/15/05 0:20


of 69



S-8 @ 1' 0509063-09 (Soil)


Analyst

Lab ID:

Metals BQL SW846/6010 mg/kg dry Silver 1 9/9/05 9:15 JLW 9/13/05 17:16

" 1 " Arsenic 0.5 9/9/05 9:15 JLW 9/12/05 14:00 " 0.53 " Beryllium 0.15 9/9/05 9:15 JLW 9/12/05 14:00

BQL " " Cadmium 0.5 9/9/05 9:15 JLW 9/12/05 14:00 " 7 " Chromium 0.5 9/9/05 9:15 JCM 9/12/05 14:03 " 5 " Copper 0.5 9/9/05 9:15 JLW 9/12/05 14:00





of 69



S-8 @ 1' 0509063-09 (Soil)


Analyst

Lab ID:

Semivolatile Organic Compounds BQL SW846/8270C mg/kg dry Chrysene 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " Dibenz(a,h)anthracene 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " Dibenzofuran 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " Di-n-butyl phthalate 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " 3,3'-Dichlorobenzidine 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " 2,4-Dichlorophenol 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " Diethyl phthalate 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " 2,4-Dimethylphenol 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " Dimethyl phthalate 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " 4,6-Dinitro-2-methylphenol 0.5 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " 2,4-Dinitrophenol 1.1 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " 2,4-Dinitrotoluene 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " 2,6-Dinitrotoluene 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " Di-n-octyl phthalate 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " Fluoranthene 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " Fluorene 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " Hexachlorobenzene 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " Hexachlorobutadiene 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " Hexachlorocyclopentadiene 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " Hexachloroethane 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " Indeno(1,2,3-cd)pyrene 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " Isophorone 0.3 9/8/05 16:00 JHV 9/20/05 13:00

" 0.3 " 2-Methylnaphthalene 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " 2-Methylphenol 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " 4-Methylphenol 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " 2-Nitroaniline 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " 3-Nitroaniline 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " 4-Nitroaniline 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " Nitrobenzene 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " 2-Nitrophenol 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " 4-Nitrophenol 1.1 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " N-Nitrosodiphenylamine 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " N-Nitroso-di-n-propylamine 0.3 9/8/05 16:00 JHV 9/20/05 13:00 BQL " " Pentachlorophenol 1.1 9/8/05 16:00 JHV 9/20/05 13:00

of 69



S-8 @ 1' 0509063-09 (Soil)


Analyst

Lab ID:


Semivolatile Organic Compound Library Search SW846/8270C 10.8 mg/kg dry Unknown analyte 0.6 9/8/05 16:00 JHV 9/20/05 11:26

" 0.934 " Unknown compound 0.6 9/8/05 16:00 JHV 9/20/05 11:26 " 1.10 " Unknown compd 0.6 9/8/05 16:00 JHV 9/20/05 11:26 " 11.0 " 3,3-dimethyl-1-butene 0.6 QVALc9/8/05 16:00 JHV 9/20/05 11:26 " 0.750 " 1-Methylnaphthalene 0.6 QVALaa9/8/05 16:00 JHV 9/20/05 11:26 " 60.8 " Sulfur 0.6 QVALy9/8/05 16:00 JHV 9/20/05 11:26


" 0.065 " Acetone 0.005 9/14/05 13:08 SS 9/15/05 4:50 BQL " " Benzene 0.005 9/14/05 13:08 SS 9/15/05 4:50 BQL " " Bromochloromethane 0.005 9/14/05 13:08 SS 9/15/05 4:50 BQL " " Bromodichloromethane 0.005 9/14/05 13:08 SS 9/15/05 4:50 BQL " " Bromoform 0.005 9/14/05 13:08 SS 9/15/05 4:50 BQL " " Bromomethane 0.005 9/14/05 13:08 SS 9/15/05 4:50

" 0.013 " 2-Butanone (MEK) 0.005 9/14/05 13:08 SS 9/15/05 4:50 BQL " " Carbon disulfide 0.005 9/14/05 13:08 SS 9/15/05 4:50 BQL " " Carbon tetrachloride 0.005 9/14/05 13:08 SS 9/15/05 4:50 BQL " " Chlorobenzene 0.005 9/14/05 13:08 SS 9/15/05 4:50 BQL " " Chloroethane 0.005 9/14/05 13:08 SS 9/15/05 4:50 BQL " " Chloroform 0.005 9/14/05 13:08 SS 9/15/05 4:50 BQL " " Chloromethane 0.005 9/14/05 13:08 SS 9/15/05 4:50 BQL " " Dibromochloromethane 0.005 9/14/05 13:08 SS 9/15/05 4:50 BQL " " 1,2-Dibromo-3-chloropropane 0.005 9/14/05 13:08 SS 9/15/05 4:50 BQL " " 1,2-Dibromoethane 0.005 9/14/05 13:08 SS 9/15/05 4:50 BQL " " 1,2-Dichlorobenzene 0.005 9/14/05 13:08 SS 9/15/05 4:50 BQL " " 1,3-Dichlorobenzene 0.005 9/14/05 13:08 SS 9/15/05 4:50

of 69



S-8 @ 1' 0509063-09 (Soil)


Analyst

Lab ID:


Volatile Organic Compounds Library Search SW846/8260 B 0.020 mg/kg dry Indane 0.005 QVALk9/14/05 13:09 SS 9/15/05 4:50

" 0.021 " Unknown compound 0.005 9/14/05 13:09 SS 9/15/05 4:50 " 0.033 " 1H-Indene,2,3-dihydro-1,1,3-trimethyl 0.005 QVALad9/14/05 13:09 SS 9/15/05 4:50

" 0.069 " Unknown analyte 0.005 9/14/05 13:09 SS 9/15/05 4:50 " 0.062 " Indan, 1-methyl- 0.005 QVALz9/14/05 13:09 SS 9/15/05 4:50 " 0.041 " Benzene, 1,2,3-trimethyl- 0.005 QVALx9/14/05 13:09 SS 9/15/05 4:50 " 0.072 " Benzene, 1,2,4,5-tetramethyl- 0.005 QVALz9/14/05 13:09 SS 9/15/05 4:50 " 0.017 " Benzene, 1-methyl-2-(1-methylethyl) 0.005 QVALz9/14/05 13:09 SS 9/15/05 4:50 " 0.021 " Benzene, 1,3-diethyl- 0.005 QVALab9/14/05 13:09 SS 9/15/05 4:50

of 69



S-8 @ 1' 0509063-09 (Soil)


Analyst

Lab ID:

of 69



S-8 @ 6' 0509063-10 (Soil)


Analyst

Lab ID:








of 69



S-8 @ 6' 0509063-10 (Soil)


Analyst

Lab ID:



" 0.075 " Acetone 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Benzene 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Bromochloromethane 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Bromodichloromethane 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Bromoform 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " 2-Butanone (MEK) 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Carbon disulfide 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Bromomethane 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Carbon tetrachloride 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Chlorobenzene 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Chloroethane 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Chloroform 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Chloromethane 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Dibromochloromethane 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " 1,2-Dibromo-3-chloropropane 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " 1,2-Dibromoethane 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " 1,2-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " 1,3-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " 1,4-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " 1,1-Dichloroethane 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " 1,2-Dichloroethane 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " 1,1-Dichloroethene 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " cis-1,2-Dichloroethene 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " trans-1,2-Dichloroethene 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " 1,2-Dichloropropane 0.006 9/14/05 13:08 SS 9/15/05 5:27

of 69



S-8 @ 6' 0509063-10 (Soil)


Analyst

Lab ID:

Volatile Organic Compounds BQL SW846/8260B mg/kg dry cis-1,3-Dichloropropene 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " trans-1,3-Dichloropropene 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Ethylbenzene 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " 2-Hexanone 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Isopropylbenzene 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Methylene chloride 0.023 9/14/05 13:08 SS 9/15/05 5:27 BQL " " 4-Methyl-2-pentanone (MIBK) 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Styrene 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " 1,1,2,2-Tetrachloroethane 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Tetrachloroethene 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Toluene 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " 1,1,1-Trichloroethane 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " 1,1,2-Trichloroethane 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Trichloroethene 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Vinyl chloride 0.006 9/14/05 13:08 SS 9/15/05 5:27 BQL " " Total Xylenes 0.018 9/14/05 13:08 SS 9/15/05 5:27


Semivolatile Organic Compounds Library Search

No non target compounds were detected 0.3 mg/kg dry 9/8/05 16:00 9/20/05 10:00 SW846/8270 C JHV

of 69



S-9 @ 1' 0509063-11 (Soil)


Analyst

Lab ID:








of 69



S-9 @ 1' 0509063-11 (Soil)


Analyst

Lab ID:


Semivolatile Organic Compound Library Search SW846/8270C 3.07 mg/kg dry Hexadecane 1.09 QVALw9/8/05 16:00 JHV 9/20/05 11:26

" 1.48 " 2,3,6-trimethyl octane 1.09 QVALm9/8/05 16:00 JHV 9/20/05 11:26 " 13.9 " 3,3-dimethyl-1-butene 1.09 QVALc9/8/05 16:00 JHV 9/20/05 11:26 " 2.00 " 2,6,10-trimethyl-dodecane 1.09 QVALt9/8/05 16:00 JHV 9/20/05 11:26 " 2.15 " Pentadecane 1.09 QVALw9/8/05 16:00 JHV 9/20/05 11:26 " 6.06 " 2,6-dimethyl-heptadecane 1.09 QVALw9/8/05 16:00 JHV 9/20/05 11:26 " 2.24 " 2,6,10,14-tetramethyl-heptadecane 1.09 QVALj9/8/05 16:00 JHV 9/20/05 11:26 " 2.46 " 2,6,10,14-tetramethyl-hexadecane 1.09 QVALs9/8/05 16:00 JHV 9/20/05 11:26 " 2.17 " tetradecane 1.09 QVALaf9/8/05 16:00 JHV 9/20/05 11:26 " 86.2 " Sulfur 1.09 QVALy9/8/05 16:00 JHV 9/20/05 11:26 " 2.32 " octadecane 1.09 QVALaf9/8/05 16:00 JHV 9/20/05 11:26


" 0.043 " Acetone 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " Benzene 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " Bromochloromethane 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " Bromodichloromethane 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " Bromoform 0.005 9/14/05 13:08 SS 9/15/05 6:05

" 0.006 " 2-Butanone (MEK) 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " Bromomethane 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " Carbon disulfide 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " Carbon tetrachloride 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " Chlorobenzene 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " Chloroethane 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " Chloroform 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " Chloromethane 0.005 9/14/05 13:08 SS 9/15/05 6:05

of 69



S-9 @ 1' 0509063-11 (Soil)


Analyst

Lab ID:

Volatile Organic Compounds BQL SW846/8260B mg/kg dry Dibromochloromethane 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " 1,2-Dibromo-3-chloropropane 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " 1,2-Dibromoethane 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " 1,2-Dichlorobenzene 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " 1,3-Dichlorobenzene 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " 1,4-Dichlorobenzene 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " 1,1-Dichloroethane 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " 1,2-Dichloroethane 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " 1,1-Dichloroethene 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " cis-1,2-Dichloroethene 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " trans-1,2-Dichloroethene 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " 1,2-Dichloropropane 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " cis-1,3-Dichloropropene 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " trans-1,3-Dichloropropene 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " Ethylbenzene 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " 2-Hexanone 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " Isopropylbenzene 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " Methylene chloride 0.022 9/14/05 13:08 SS 9/15/05 6:05 BQL " " 4-Methyl-2-pentanone (MIBK) 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " Styrene 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " 1,1,2,2-Tetrachloroethane 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " Tetrachloroethene 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " Toluene 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " 1,1,1-Trichloroethane 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " 1,1,2-Trichloroethane 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " Trichloroethene 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " Vinyl chloride 0.005 9/14/05 13:08 SS 9/15/05 6:05 BQL " " Total Xylenes 0.016 9/14/05 13:08 SS 9/15/05 6:05


of 69



S-9 @ 6' 0509063-12 (Soil)


Analyst

Lab ID:








of 69



S-9 @ 6' 0509063-12 (Soil)


Analyst

Lab ID:


Semivolatile Organic Compound Library Search SW846/8270C 49.5 mg/kg dry Sulfur 0.4 QVALx9/8/05 16:00 JHV 9/20/05 11:26


" 0.052 " Acetone 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Benzene 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Bromochloromethane 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Bromodichloromethane 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Bromoform 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Carbon disulfide 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Bromomethane 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " 2-Butanone (MEK) 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Carbon tetrachloride 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Chlorobenzene 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Chloroethane 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Chloroform 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Chloromethane 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Dibromochloromethane 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " 1,2-Dibromo-3-chloropropane 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " 1,2-Dibromoethane 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " 1,2-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " 1,3-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " 1,4-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " 1,1-Dichloroethane 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " 1,2-Dichloroethane 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " 1,1-Dichloroethene 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " cis-1,2-Dichloroethene 0.006 9/14/05 13:08 SS 9/15/05 6:42

of 69



S-9 @ 6' 0509063-12 (Soil)


Analyst

Lab ID:

Volatile Organic Compounds BQL SW846/8260B mg/kg dry trans-1,2-Dichloroethene 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " 1,2-Dichloropropane 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " cis-1,3-Dichloropropene 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " trans-1,3-Dichloropropene 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Ethylbenzene 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " 2-Hexanone 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Isopropylbenzene 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " 4-Methyl-2-pentanone (MIBK) 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Methylene chloride 0.025 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Styrene 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " 1,1,2,2-Tetrachloroethane 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Tetrachloroethene 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Toluene 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " 1,1,1-Trichloroethane 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " 1,1,2-Trichloroethane 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Trichloroethene 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Vinyl chloride 0.006 9/14/05 13:08 SS 9/15/05 6:42 BQL " " Total Xylenes 0.018 9/14/05 13:08 SS 9/15/05 6:42


of 69



S-11 @ 1' 0509063-13 (Soil)


Analyst

Lab ID:

PCBs - Polychlorinated Biphenyls (subcontracted to Primary Labs) BQL SW846/8082 mg/kg dry Aroclor 1016 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Aroclor 1221 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Aroclor 1232 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Aroclor 1242 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Aroclor 1248 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Aroclor 1254 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Aroclor 1260 0.001 A-019/8/05 16:00 sub 9/21/05 17:10

of 69



S-10 @ 1' 0509063-14 (Soil)


Analyst

Lab ID:

PCBs - Polychlorinated Biphenyls (subcontracted to Primary Labs) BQL SW846/8082 mg/kg dry Aroclor 1016 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Aroclor 1221 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Aroclor 1232 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Aroclor 1242 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Aroclor 1248 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Aroclor 1254 0.001 A-019/8/05 16:00 sub 9/21/05 17:10 BQL " " Aroclor 1260 0.001 A-019/8/05 16:00 sub 9/21/05 17:10

of 69



S-6 @ 1' 0509063-15 (Soil)


Analyst

Lab ID:








of 69



S-6 @ 1' 0509063-15 (Soil)


Analyst

Lab ID:


Semivolatile Organic Compound Library Search SW846/8270C 53.9 mg/kg dry Sulfur 0.3 QVALy9/8/05 16:00 JHV 9/20/05 11:26

" 0.435 " Unknown compound 0.3 9/8/05 16:00 JHV 9/20/05 11:26 " 2.47 " 3-methyl-3-buten-2-one 0.3 QVALd9/8/05 16:00 JHV 9/20/05 11:26 " 2.24 " 2-methyl-3-penten-1-ol 0.3 QVALd9/8/05 16:00 JHV 9/20/05 11:26

of 69



S-6 @ 5' 0509063-16 (Soil)


Analyst

Lab ID:








of 69



S-6 @ 5' 0509063-16 (Soil)


Analyst

Lab ID:


Semivolatile Organic Compound Library Search SW846/8270C 0.987 mg/kg dry 1-docosene 0.4 QVALw9/8/05 16:00 JHV 9/20/05 11:26

" 0.495 " 7-hexyl-tridecane 0.4 QVALac9/8/05 16:00 JHV 9/20/05 11:26 " 7.02 " 3,3-dimethyl-1-butene 0.4 QVAL9/8/05 16:00 JHV 9/20/05 11:26 " 6.24 " Unknown compound 0.4 9/8/05 16:00 JHV 9/20/05 11:26 " 0.831 " nonadecane 0.4 QVALaa9/8/05 16:00 JHV 9/20/05 11:26 " 0.516 " Oleic Acid 0.4 QVALah9/8/05 16:00 JHV 9/20/05 11:26


" 0.066 " Acetone 0.006 9/14/05 13:08 SS 9/15/05 7:19 BQL " " Benzene 0.006 9/14/05 13:08 SS 9/15/05 7:19 BQL " " Bromochloromethane 0.006 9/14/05 13:08 SS 9/15/05 7:19 BQL " " Bromodichloromethane 0.006 9/14/05 13:08 SS 9/15/05 7:19 BQL " " Bromoform 0.006 9/14/05 13:08 SS 9/15/05 7:19 BQL " " Carbon disulfide 0.006 9/14/05 13:08 SS 9/15/05 7:19 BQL " " Bromomethane 0.006 9/14/05 13:08 SS 9/15/05 7:19

" 0.011 " 2-Butanone (MEK) 0.006 9/14/05 13:08 SS 9/15/05 7:19 BQL " " Carbon tetrachloride 0.006 9/14/05 13:08 SS 9/15/05 7:19 BQL " " Chlorobenzene 0.006 9/14/05 13:08 SS 9/15/05 7:19 BQL " " Chloroethane 0.006 9/14/05 13:08 SS 9/15/05 7:19 BQL " " Chloroform 0.006 9/14/05 13:08 SS 9/15/05 7:19 BQL " " Chloromethane 0.006 9/14/05 13:08 SS 9/15/05 7:19 BQL " " Dibromochloromethane 0.006 9/14/05 13:08 SS 9/15/05 7:19 BQL " " 1,2-Dibromo-3-chloropropane 0.006 9/14/05 13:08 SS 9/15/05 7:19 BQL " " 1,2-Dibromoethane 0.006 9/14/05 13:08 SS 9/15/05 7:19 BQL " " 1,2-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/15/05 7:19 BQL " " 1,3-Dichlorobenzene 0.006 9/14/05 13:08 SS 9/15/05 7:19

of 69



S-6 @ 5' 0509063-16 (Soil)


Analyst

Lab ID:



of 69



S-5 @ 1' 0509063-17 (Soil)


Analyst

Lab ID:

Metals BQL SW846/6010 mg/kg dry Silver 1 9/9/05 9:15 JLW 9/13/05 17:16 BQL " " Arsenic 0.5 9/9/05 9:15 JLW 9/12/05 14:00 BQL " " Beryllium 0.15 9/9/05 9:15 JLW 9/12/05 14:00 BQL " " Cadmium 0.5 9/9/05 9:15 JLW 9/12/05 14:00






of 69



S-5 @ 1' 0509063-17 (Soil)


Analyst

Lab ID:


of 69



S-5 @ 1' 0509063-17 (Soil)


Analyst

Lab ID:


Semivolatile Organic Compound Library Search SW846/8270C 40.0 mg/kg dry 1-eicosene 0.6 QVALd9/8/05 16:00 JHV 9/20/05 11:26

" 1350 " Tetradecanoic acid 0.6 QVALy9/8/05 16:00 JHV 9/20/05 11:26 " 1060 " Octadecanoic acid 0.6 QVALy9/8/05 16:00 JHV 9/20/05 11:26 " 6.97 " Unknown compound 0.6 9/8/05 16:00 JHV 9/20/05 11:26 " 5210 " Hexadecanoic acid 0.6 QVALah9/8/05 16:00 JHV 9/20/05 11:26 " 5.19 " N,N-bis(2-hydroxyethyl)-dodecanamide 0.6 QVALaa9/8/05 16:00 JHV 9/20/05 11:26

" 46.0 " Unknown compd 0.6 9/8/05 16:00 JHV 9/20/05 11:26 " 3.52 " Unknown acid 0.6 9/8/05 16:00 JHV 9/20/05 11:26 " 9.99 " cis-bicyclo[4.3.0]-3-nonene 0.6 QVALt9/8/05 16:00 JHV 9/20/05 11:26 " 19.9 " eicosanoic acid 0.6 QVALd9/8/05 16:00 JHV 9/20/05 11:26

of 69



S-5 @ 6' 0509063-18 (Soil)


Analyst

Lab ID:

Metals BQL SW846/6010 mg/kg dry Silver 1 9/9/05 9:15 JLW 9/13/05 17:16 BQL " " Arsenic 0.5 9/9/05 9:15 JLW 9/12/05 14:00 BQL " " Beryllium 0.15 9/9/05 9:15 JLW 9/12/05 14:00 BQL " " Cadmium 0.5 9/9/05 9:15 JLW 9/12/05 14:00






of 69



S-5 @ 6' 0509063-18 (Soil)


Analyst

Lab ID:


of 69



S-5 @ 6' 0509063-18 (Soil)


Analyst

Lab ID:


Semivolatile Organic Compound Library Search SW846/8270C 1.43 mg/kg dry Hexadecanoic acid 0.4 QVALae9/8/05 16:00 JHV 9/20/05 11:26

" 2.00 " Unknown compound 0.4 9/8/05 16:00 JHV 9/20/05 11:26 " 55.0 " Sulfur 0.4 QVALy9/8/05 16:00 JHV 9/20/05 11:26 " 2.13 " 2,3-dimethyl-butene 0.4 QVALe9/8/05 16:00 JHV 9/20/05 11:26


" 0.035 " Acetone 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Benzene 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Bromochloromethane 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Bromodichloromethane 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Bromoform 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Bromomethane 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Carbon disulfide 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " 2-Butanone (MEK) 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Carbon tetrachloride 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Chlorobenzene 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Chloroethane 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Chloroform 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Chloromethane 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Dibromochloromethane 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " 1,2-Dibromo-3-chloropropane 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " 1,2-Dibromoethane 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " 1,2-Dichlorobenzene 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " 1,3-Dichlorobenzene 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " 1,4-Dichlorobenzene 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " 1,1-Dichloroethane 0.005 9/14/05 13:08 SS 9/15/05 7:56

of 69



S-5 @ 6' 0509063-18 (Soil)


Analyst

Lab ID:

Volatile Organic Compounds BQL SW846/8260B mg/kg dry 1,2-Dichloroethane 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " 1,1-Dichloroethene 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " cis-1,2-Dichloroethene 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " trans-1,2-Dichloroethene 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " 1,2-Dichloropropane 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " cis-1,3-Dichloropropene 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " trans-1,3-Dichloropropene 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Ethylbenzene 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " 2-Hexanone 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Isopropylbenzene 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Methylene chloride 0.021 9/14/05 13:08 SS 9/15/05 7:56 BQL " " 4-Methyl-2-pentanone (MIBK) 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Styrene 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " 1,1,2,2-Tetrachloroethane 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Tetrachloroethene 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Toluene 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " 1,1,1-Trichloroethane 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " 1,1,2-Trichloroethane 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Trichloroethene 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Vinyl chloride 0.005 9/14/05 13:08 SS 9/15/05 7:56 BQL " " Total Xylenes 0.016 9/14/05 13:08 SS 9/15/05 7:56


of 69

Notes and Definitions

QVALac Estimated concentration with Q Value = 96. QVALe Estimated concentration with Q Value = 72. QVALd Estimated concentration with Q Value = 70. QVALc Estimated concentration with Q Value = 64. QVALb Estimated concentration with Q Value = 64 QVALah Estimated concentration with Q Value = 99. QVALag Estimated concentration with Q Value = 99 QVALaf Estimated concentration with Q Value = 98. # Does not pass acceptance criteria. QVALad Estimated concentration with Q Value = 97 QVALh Estimated concentration with Q Value = 78. QVALab Estimated concentration with Q Value = 96 QVALaa Estimated concentration with Q Value = 95. QVALa Estimated concentration with Q Value = 60 QVAL Estimated concentration with Q Value = 56. B-Q Method Blank contained Hexane, however it was not found in any of the samples for this analysis. Blank The Method Blank contained 0.0216 mg/L Zinc. B Analyte is found in the associated blank as well as in the sample (CLP B-flag). A-01 Subcontracted to Primary Laboratories, Inc. QVALae Estimated concentration with Q Value = 97. QVALp Estimated concentration with Q Value = 89 QVALz Estimated concentration with Q Value = 95 QVALy Estimated concentration with Q Value = 94. QVALx Estimated concentration with Q Value = 94 QVALw Estimated concentration with Q Value = 93. QVALv Estimated concentration with Q Value = 93 QVALu Estimated concentration with Q Value = 92. QVALt Estimated concentration with Q Value = 91.

of 69


QVALs Estimated concentration with Q Value = 90. QVALf Estimated concentration with Q Value = 74. QVALq Estimated concentration with Q Value = 89. QVALg Estimated concentration with Q Value = 78 QVALo Estimated concentration with Q Value = 86. QVALn Estimated concentration with Q Value = 86 QVALm Estimated concentration with Q Value = 83. QVALl Estimated concentration with Q Value = 83 QVALk Estimated concentration with Q Value = 81 QVALj Estimated concentration with Q Value = 80. QVALi Estimated concentration with Q Value = 80 sub-1 This analysis was subcontracted to Primary Laboratories. QVALr Estimated concentration with Q Value = 90

milligrams per kilogram mg/kg = micrograms per Liter µg/L = milligrams per Liter mg/L =

BQL =

Below the Quantitation Limit

su =

standard units ppm = parts per million

Colony forming units per milliliter CFU/mL = Nephelometric Turbidity Units

NTU = Most Probable Number per 100 milliliters MPN/100mL =

picocuries per Liter

pCi/L =

APPENDIX F

WATER ANALYTICAL REPORT

FROEHLING & ROBERTSON, INC GEOTECHNICAL ENVIRONMENTAL MATERIALS

ENGINEERS LABORATORIES “OVER ONE HUNDRED YEARS OF SERVICE”

CERTIFICATE OF ANALYSIS

Page 1 of 11September 23, 2005

RECEIVED: 09/06/05

PROJECT: PROJECT NO.:

Tyson Foods, Inc. (GA) 13264 Mountain Rd. Glen Allen VA, 23059

LAB#:

SAMPLED BY:

CLIENT:

Ed Setzer

Doug Baxter Berlin

0509063

Results to follow.

Audrey Brubeck Manager Analytical Laboratory Services HEADQUARTERS: 3015 DUMBARTON ROAD BOX 27524 RICHMOND, VA 23261-7524 TELEPHONE (804) 264-2701 FAX (804) 264-1202 www.FandR.com BRANCHES: ASHEVILLE, NC BALTIMORE, MD CHARLOTTE, NC CHESAPEAKE, VA CROZET, VA FAYETTEVILLE, NC FREDERICKSBURG, VA GREENVILLE, SC HICKORY, NC RALEIGH, NC ROANOKE, VA STERLING, VA

CERTIFICATIONS: VIRGINIA DRINKING WATER - 00150 NORTH CAROLINA DENR - 432 SOUTH CAROLINA DHEC- 93010001 & 93010 MARYLAND DRINKING WATER - 279

of 11



GW-1 0509063-19 (Water)


Analyst

Lab ID:

Volatile Organic Compounds BQL SW846/8260B µg/L Methyl tert-Butyl Ether 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Acetone 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Benzene 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Bromochloromethane 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Bromodichloromethane 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Bromoform 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Bromomethane 1 9/14/05 13:05 SS 9/14/05 18:16 BQL " " 2-Butanone (MEK) 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Carbon disulfide 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Carbon tetrachloride 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Chlorobenzene 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Chloroethane 2 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Chloroform 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Chloromethane 2 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Dibromochloromethane 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " 1,2-Dibromo-3-chloropropane 1 9/14/05 13:05 SS 9/14/05 18:16 BQL " " 1,2-Dibromoethane 1 9/14/05 13:05 SS 9/14/05 18:16 BQL " " 1,2-Dichlorobenzene 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " 1,3-Dichlorobenzene 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " 1,4-Dichlorobenzene 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " 1,1-Dichloroethane 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " 1,2-Dichloroethane 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " 1,1-Dichloroethene 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " cis-1,2-Dichloroethene 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " trans-1,2-Dichloroethene 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " 1,2-Dichloropropane 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " cis-1,3-Dichloropropene 1 9/14/05 13:05 SS 9/14/05 18:16 BQL " " trans-1,3-Dichloropropene 1 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Ethylbenzene 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " 2-Hexanone 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Isopropylbenzene 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Methylene chloride 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " 4-Methyl-2-pentanone (MIBK) 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Styrene 5 9/14/05 13:05 SS 9/14/05 18:16

of 11



GW-1 0509063-19 (Water)


Analyst

Lab ID:

Volatile Organic Compounds BQL SW846/8260B µg/L 1,1,2,2-Tetrachloroethane 1 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Tetrachloroethene 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Toluene 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " 1,1,1-Trichloroethane 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " 1,1,2-Trichloroethane 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Trichloroethene 5 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Vinyl chloride 2 9/14/05 13:05 SS 9/14/05 18:16 BQL " " Total Xylenes 5 9/14/05 13:05 SS 9/14/05 18:16

Volatile Organic Compounds Library Search SW846/8260 B µg/L No non target compounds were detected 5 9/14/05 13:12 SS 9/14/05 18:16

of 11



GW-2 0509063-20 (Water)


Analyst

Lab ID:

Volatile Organic Compounds BQL SW846/8260B µg/L Methyl tert-Butyl Ether 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " Acetone 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " Benzene 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " Bromochloromethane 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " Bromodichloromethane 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " Bromoform 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " Carbon disulfide 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " 2-Butanone (MEK) 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " Bromomethane 1 9/14/05 13:05 SS 9/14/05 18:47 BQL " " Carbon tetrachloride 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " Chlorobenzene 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " Chloroethane 2 9/14/05 13:05 SS 9/14/05 18:47 BQL " " Chloroform 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " Chloromethane 2 9/14/05 13:05 SS 9/14/05 18:47 BQL " " Dibromochloromethane 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " 1,2-Dibromo-3-chloropropane 1 9/14/05 13:05 SS 9/14/05 18:47 BQL " " 1,2-Dibromoethane 1 9/14/05 13:05 SS 9/14/05 18:47 BQL " " 1,2-Dichlorobenzene 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " 1,3-Dichlorobenzene 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " 1,4-Dichlorobenzene 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " 1,1-Dichloroethane 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " 1,2-Dichloroethane 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " 1,1-Dichloroethene 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " cis-1,2-Dichloroethene 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " trans-1,2-Dichloroethene 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " 1,2-Dichloropropane 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " cis-1,3-Dichloropropene 1 9/14/05 13:05 SS 9/14/05 18:47 BQL " " trans-1,3-Dichloropropene 1 9/14/05 13:05 SS 9/14/05 18:47 BQL " " Ethylbenzene 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " 2-Hexanone 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " Isopropylbenzene 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " 4-Methyl-2-pentanone (MIBK) 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " Methylene chloride 5 9/14/05 13:05 SS 9/14/05 18:47 BQL " " Styrene 5 9/14/05 13:05 SS 9/14/05 18:47

of 11



GW-2 0509063-20 (Water)


Analyst

Lab ID:



of 11



MW-16 0509063-21 (Water)


Analyst

Lab ID:

Volatile Organic Compounds BQL SW846/8260B µg/L Methyl tert-Butyl Ether 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " Acetone 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " Benzene 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " Bromochloromethane 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " Bromodichloromethane 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " Bromoform 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " Carbon disulfide 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " Bromomethane 1 9/14/05 13:05 SS 9/14/05 19:18 BQL " " 2-Butanone (MEK) 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " Carbon tetrachloride 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " Chlorobenzene 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " Chloroethane 2 9/14/05 13:05 SS 9/14/05 19:18 BQL " " Chloroform 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " Chloromethane 2 9/14/05 13:05 SS 9/14/05 19:18 BQL " " Dibromochloromethane 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " 1,2-Dibromo-3-chloropropane 1 9/14/05 13:05 SS 9/14/05 19:18 BQL " " 1,2-Dibromoethane 1 9/14/05 13:05 SS 9/14/05 19:18 BQL " " 1,2-Dichlorobenzene 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " 1,3-Dichlorobenzene 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " 1,4-Dichlorobenzene 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " 1,1-Dichloroethane 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " 1,2-Dichloroethane 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " 1,1-Dichloroethene 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " cis-1,2-Dichloroethene 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " trans-1,2-Dichloroethene 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " 1,2-Dichloropropane 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " cis-1,3-Dichloropropene 1 9/14/05 13:05 SS 9/14/05 19:18 BQL " " trans-1,3-Dichloropropene 1 9/14/05 13:05 SS 9/14/05 19:18 BQL " " Ethylbenzene 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " 2-Hexanone 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " Isopropylbenzene 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " Methylene chloride 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " 4-Methyl-2-pentanone (MIBK) 5 9/14/05 13:05 SS 9/14/05 19:18 BQL " " Styrene 5 9/14/05 13:05 SS 9/14/05 19:18

of 11



MW-16 0509063-21 (Water)


Analyst

Lab ID:


Volatile Organic Compounds Library Search SW846/8260 B 5 µg/L Furan, tetrahydro- 5 QVALb9/14/05 13:12 SS 9/14/05 19:18

of 11



MW-10 0509063-22 (Water)


Analyst

Lab ID:

Volatile Organic Compounds BQL SW846/8260B µg/L Methyl tert-Butyl Ether 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " Acetone 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " Benzene 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " Bromochloromethane 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " Bromodichloromethane 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " Bromoform 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " Bromomethane 1 9/14/05 13:05 SS 9/14/05 19:49 BQL " " 2-Butanone (MEK) 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " Carbon disulfide 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " Carbon tetrachloride 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " Chlorobenzene 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " Chloroethane 2 9/14/05 13:05 SS 9/14/05 19:49 BQL " " Chloroform 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " Chloromethane 2 9/14/05 13:05 SS 9/14/05 19:49 BQL " " Dibromochloromethane 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " 1,2-Dibromo-3-chloropropane 1 9/14/05 13:05 SS 9/14/05 19:49 BQL " " 1,2-Dibromoethane 1 9/14/05 13:05 SS 9/14/05 19:49 BQL " " 1,2-Dichlorobenzene 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " 1,3-Dichlorobenzene 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " 1,4-Dichlorobenzene 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " 1,1-Dichloroethane 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " 1,2-Dichloroethane 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " 1,1-Dichloroethene 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " cis-1,2-Dichloroethene 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " trans-1,2-Dichloroethene 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " 1,2-Dichloropropane 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " cis-1,3-Dichloropropene 1 9/14/05 13:05 SS 9/14/05 19:49 BQL " " trans-1,3-Dichloropropene 1 9/14/05 13:05 SS 9/14/05 19:49 BQL " " Ethylbenzene 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " 2-Hexanone 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " Isopropylbenzene 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " 4-Methyl-2-pentanone (MIBK) 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " Methylene chloride 5 9/14/05 13:05 SS 9/14/05 19:49 BQL " " Styrene 5 9/14/05 13:05 SS 9/14/05 19:49

of 11



MW-10 0509063-22 (Water)


Analyst

Lab ID:


Volatile Organic Compounds Library Search SW846/8260 B 1460 µg/L Propane 5 QVALa9/14/05 13:12 SS 9/14/05 19:49

" 164 " Unknown analyte 5 9/14/05 13:12 SS 9/14/05 19:49 " 5 " Butane 5 QVAL9/14/05 13:12 SS 9/14/05 19:49

of 11



Field Blank 0509063-23 (Water)


Analyst

Lab ID:

Volatile Organic Compounds BQL SW846/8260B µg/L Methyl tert-Butyl Ether 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " Acetone 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " Benzene 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " Bromochloromethane 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " Bromodichloromethane 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " Bromoform 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " 2-Butanone (MEK) 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " Bromomethane 1 9/14/05 13:05 SS 9/14/05 17:46 BQL " " Carbon disulfide 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " Carbon tetrachloride 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " Chlorobenzene 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " Chloroethane 2 9/14/05 13:05 SS 9/14/05 17:46 BQL " " Chloroform 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " Chloromethane 2 9/14/05 13:05 SS 9/14/05 17:46 BQL " " Dibromochloromethane 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " 1,2-Dibromo-3-chloropropane 1 9/14/05 13:05 SS 9/14/05 17:46 BQL " " 1,2-Dibromoethane 1 9/14/05 13:05 SS 9/14/05 17:46 BQL " " 1,2-Dichlorobenzene 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " 1,3-Dichlorobenzene 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " 1,4-Dichlorobenzene 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " 1,1-Dichloroethane 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " 1,2-Dichloroethane 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " 1,1-Dichloroethene 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " cis-1,2-Dichloroethene 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " trans-1,2-Dichloroethene 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " 1,2-Dichloropropane 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " cis-1,3-Dichloropropene 1 9/14/05 13:05 SS 9/14/05 17:46 BQL " " trans-1,3-Dichloropropene 1 9/14/05 13:05 SS 9/14/05 17:46 BQL " " Ethylbenzene 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " 2-Hexanone 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " Isopropylbenzene 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " 4-Methyl-2-pentanone (MIBK) 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " Methylene chloride 5 9/14/05 13:05 SS 9/14/05 17:46 BQL " " Styrene 5 9/14/05 13:05 SS 9/14/05 17:46

of 11



Field Blank 0509063-23 (Water)


Analyst

Lab ID:




QVALb Estimated concentration with Q Value = 91 QVALa Estimated concentration with Q Value = 83 QVAL Estimated concentration with Q Value = 72

milligrams per kilogram mg/kg = micrograms per Liter µg/L = milligrams per Liter mg/L =

BQL =

Below the Quantitation Limit

su =

standard units ppm = parts per million

Colony forming units per milliliter CFU/mL = Nephelometric Turbidity Units

NTU = Most Probable Number per 100 milliliters MPN/100mL =

picocuries per Liter

pCi/L =

APPENDIX G

TRANSFORMER ANALYTICAL REPORT

VOLUNTARY CLEANUP PROGRAM SITE ASSESMENT FORMER …€¦ · VOLUNTARY CLEANUP PROGRAM SITE...

Documents

Transcript of VOLUNTARY CLEANUP PROGRAM SITE ASSESMENT FORMER …€¦ · VOLUNTARY CLEANUP PROGRAM SITE...