USE UNtT.ED STATES ENVIRONMENTAL PROTECTION AGENCY · THROUGH: ^Charles Matkovich * ESAT Team...

<r?

UNtT.ED STATES ENVIRONMENTAL PROTECTION AGENCYREGION II:

CENTRA. REGIONAL LABORATORY63r BES'GATE ROAD

(3011266-9180

USE

. ^ January 4. 1989DATE :Organic Data Validation for the CryoChem Site

. ,-,_„„ i f\ t- -> rCase 10636

FROM : Theresa A.Region III Acting ESAT DPO (3ES23)

TO : Christoper PillaRegional Project Manager (3HW12)

Thru: Pat Krantz *~ ~* f*Chief, QA Section (3ES23)

Attached is the organic data review for the CryoChem Site (Case10636) completed by the Region III Environmental ServicesAssistance Team (ESAT) contractor under the direction of RegionIII ESD.

If you have questions regarding this review, please call me.

Attachment

cc: Paul Wooldridge, VersarT1D File: 038801001 Task #1419

""30061,6

2568A RIVA ROADSUITE 300ANNAPOLIS. MD 2U01PHONE 301-266-9837

DATE: December 28, 19S8

SUBJECT: Organic Data Validation for Case 10636Site: Cryo Chem

FROM: William D. Zimmerman/CHMM Albert T.Hydrogeolcgist >„- Senior Organic Data Reviewer

£0: Diana J. BaldiESAT Deputy Project Officer

THROUGH: Charles Matkovich* ESAT Team Manager

Overview

Case 10636 consisted of seven (7) water samples taken from theCryo Chen site on October 13, 1988. The seven (7) samples, whichinclude one (1) field blank and one (1) field duplicate pair,were analyEed for volatile organics, semi-volatile organics andpesticides/PCB's. The laboratory analyzed all samples accordingto the Contract Laboratory Program (CLP) Routine AnalyticalServices (RAS).

Summary

All samples were successfully analyzed for all target compoundswith the exception of 2-butanone. All instrument and methodsensitivities were according to the Contract Laboratory Program(CLP) Routir.e Analytical Services (RAS) protocol.

Haior Problems

o The response factor for 2-butanone was less than 0.05 inall initial and continuing calibration standards. Quantitationlimits for the affected samples were qualified "R" forunreliable. (See Table I and Forms VI and VII in Appendix F) .

Hinor Problems . •• -

o Several volatile and semi-volatile compounds failed precisioncriteria for the continuing calibration standards. Theguantitation limits are qualified "UJ" for those samplesaffected. (See Table I and Forms VI and VII in Appendix F) .

o The holding time for the extraction of semi-volatile organiccompounds was exceeded by twenty-one (21) days for SampleCY365. Quantitation limits for these compounds werequalified "UL". (See the Data Summary Forms in Appendix B).

Notes

o The maximum concentrations of all compounds found in themethod and/or trip blanks are listed below. All samples withconcentrations of common laboratory contaminants that wereless than ten times (<10x) the blank level and uncommoncontaminants that were less than five times (<5x) the blanklevel have been qualfied "B11 on the data summary forms. (SeeData Summary Fora in Appendix B).

Ccrtccur.d Concentration

Methylene Chloride* 6 B ug/LAcetone* 10 B ug/LChloroform 11 B ug/LToluene* 1 J ug/L

* = common laboratory contaminants

o The field duplicate pair did not yield data that was usablefor precision accuracy.

All data for Case 10636 was reviewed in accordance with theFunctional Guidelines for Evaluating Organic Analyses withModifications for Use Within Region III. This report addressesonly those affected problems.

Attachments

1) Appendix A - Glossary of Data Qualifier Codes2) Appendix B - Data Summary. These include:

(a) All positive results for target compounds withqualifier flags where applicable;

(b) All unusable detection limits (qualified "R").3) Appendix C - Results as Reported by the Laboratory for .

all Target Compounds.4) Appendix D - Reviewed and Corrected Tentatively

Identified Compounds5) Appendix E - DPO Report for Contractual Compliance6) Appendix F - Support Documentation

Appendix A

Glossary cf Data Qualifiers

GLOSSARY OF DATA QUALIFIER CODES (ORGANIC)

CODES RELATING TO ID^TTIFICATION(confidence concerning presence or absence of compounds):

U = Not detected. The associated number indicatesapproximate sample concentration necessary to bedetected.

(NO CODE) ~ Confirmed identification.

B = Net. detected substantially above the level reportedin laboratory or field blanks.

R = Unreliable result. Analyte may or may not bepresent in the sample. Supporting data necessary toconfirm result.

N = Tentative identification. Consider present.Special methods may be needed to confirm itspresence or absence in future sampling efforts,

CODES RELATED TO QUANTITATION(can be used for both positive results and sample quantitationlimits):

J = Analyte present. Reported value may not be accurateor precise.

K = Analyte present. Reported value may be biased high.Actual value is expected to be lower.

L = Analyte present. Reported value may be biased low.Actual value is expected to be higher.

UJ = Not detected, quantitation limit may be inaccurateor imprecise.

UL = Not detected, quantitation limit is probably higher,

OTHER CODES

Q = No analytical result.

AR300650

Appendix B

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Appendix C

Results as Hepcrted by the Laboratoryfor All Target Compounds

AR300658

C:\J> TAVC'-A'I-E C="3AN;CS ANA..Y5ZS DATA SHEET _r

| CY865*b Na.-ae: IT CHR.nlTCS______________ Contract: 63-01-7252 j______

Lab Cede: 1£_____ Case Nc.: 1QS36 SAS No.: _______ SDG No.: CY865

Matrix: (scl1/ware-} V^"R Lab Sample ID: CYSS5

Sample wt/vcl : 5.C (g/mL) ML Lab File ID: 48870EC1

Level; (Icw/mec) L0! Date Received: T 0 /1A / 8 S

% Moisture: net dec. ____ Dare Analyzed*: 10/20/88

Column: (pack/Gas) PACK Dilution Factor: 1.00

CONCENTRATION UNITS:CAS NC. COMPOUND (ug/L or ug/Kg) UG/L

74-87-3 —————74-8 ~ — ° — —— — —75-01-4 ————75-OC-3 —————7s — Dis — .£ — — — — —67 — S f* — T — — ._—._( —— Qir —— I —— ——

7S-15-C —————/ »• J w *•7 C _O «» _ ~ __*.( O » — w

<^ A n — c r.6-7 ,_c .r __ ~ ___t — 0 D " O — — — — —

I u (— uc~"<;— — — —78-93-3 —————7 T 5- — c_ ——— _56-23-5 —————108-05-4 ————7F ^ r» x5-27-4- —— --78-87-s —— - ——1 W d 1 w

10061-01-5 —7Q-.D1— K -. — _.-1 O A —A ft 17Q — n n — t? .y — u u — D —71-43-2 —————10061-02-6 —/ 3 i O i —1 n o T n T ^

Os 1— / o — D — — — —127-18-4 ————

108-8S-3 ————103-20-7 ————100-41-4 ————100-42-5 ————1330-2C-7 ——

- —— Chl orome thane— — Ercmcmethane——— V-" nyl Chloride——— Chl crce thane- — -Metr,y ? ene Chloride- —— Acetone-- — Car oon Dlsulflce

——— 1 ,2-Dlchloroethene (total) __——— Chl c^of orm——— 1 , 2-D1chl orcethane——— 2-Butancne——— -. 9 \ r i-Tr Ichloroethane——— Carson Tetrachl or ide——— Vinyl Ace rate——— Bromodlchl orome thane——— 1 r 2-D1chl oropropane- —— cls-1 , 3 -Die hi oropropene——— Trlchloroethene——— Dlbromoc hi orome thane——— 1 , 1 , 2-Trlchloroethane— — Benzene——— trans- 1 , 3-Dichl oropropene ___———— Bromoform v——— 4 -Me thy 1 -2-Pentanone——— 2-Hexanone——— Tetrachloroethene

——— Toluene——— Chlorobenzene——— Ethyl benzene——— Styrene——— Xy lenes ( Iota 1 )

10101 0102

. 101 5

595

; 5

510

140

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1UUUUBJUUuuuuuuuuuuuuuuuuuuuuuuuuu—

FORM 1 VOA {\R3QQ659 1/f37 *ev

1A EPA SAMPLEVOLATILE ORGANIC* ANALYSIS DATA SHEET

II CY866

b Name: IT CE3RITCS ____ Contract: 68-01-7252 |

Lab Code: IT Case No.: 10536 _ SAS No.: SDG No.: CY85=

Matrix: (soil/water) ftAT£3 • Lab Sample ID: CY86S

Sample wt/vcl : 5,C (g/mL) ML Lab File ID: 48S70EC4_

Level : (1 cw/med) L.QW Date Received : .1.0/14/8 S

% Mo-rsture: not dec. ____ Date Analyzed: 10/20/88

Column : (pack/cap) PACK__ Dilution Factor: 1.00

CONCENTRATION UNITS:CAS NC. CCMPCUNO (ug/t or ug/Kg) UG/L

j 74-B7-3 ————————— Chlcromethane________________ | 1 0 |Uj 74-63-9 ————————— Ercmcmethane_______"__III" I 1 Q |Uj 75-01-4————————Vinyl Chloride^"_II_IIIIIII I "• 0 |U| 75-00-3—————————Chlcrce thane_____"___III" 1 1 ° |Ut 75-09-2 ————————— Mstnylene ChTorTde________I_I j 4 | 8Jj 67-54-1————————Acetcne__________III^IIIIIII! ^ I 6Jj 75-T5-C———————— Careen DIsuTfTce____I__I_H j 5 |U| 75-35-4————————1 , 1-DlchloroetheneII_I_™HI | 5' |U| 75-34-3—————————1 , 1-DlchloroethaneIIH_III™ | 5 |U| 540-59-0 ———————— 1 , 2-D1chloroethene (total")_I 5 JU

.1 67-55-3 ————————— Chloroform_________________~ j 5 |U| 107-06-2- —————— 1 , 2-D1chlcrcethane__________I| S |U1 7 8-S 3-3 ————————— 2-Sutancne______II-.I_I_II_I j 10 luI 71-55-6 ———————— 1 , 1 , 1-Tn"chToroetnane_I_II™ | 5 JU| 56-23-5 ———————Carbon Tet rachl orl de________j 5 |U| 108-05-4————————Vinyl Acetate_______™_HI™ { 10 |U] 75-27-4- — --- —— Bromodlchl cromethane_______ | 5 | U| 78-87-5 ————————— 1 ,2-Dichloropropane_I_I_IIHIl 5 |U| 10061-0 1-5 ————— cls-1 ,3-D1chloropropene_____ j 5 JUj 7 9-01-6-- —————— Trlchloroethene_____________ | 5 JUj 124-48-1 ————————D1 bromochl orome thane________ | 5 j UI 79-00-5————————1 , 1 . 2-Trlchloroethane_HH™ | 5 |U| 7 1 -43-2 ———————— Benzene_____________IIIIIIIII 5 | UI 10061-02-6 —— —— trans-1 ,3-01ch1oropropene___ j 5 | U| 75.-2S-2 ————————— Bromof crm_______________IIIII 5 |U| 108- 10-1-:—————4-Methyl-2-Pentanone______-_ j 10 JU| 591-78-6 ——————— 2-Hexanone___________IIIII__ I TO 1UI 127-18-4 ————— — Tet rachl or oethene__________3 I 5 lu} 79-34-5 ————— —— 1 ,1.2, 2-Tet rachl or oethane__I| 5 JU! 108-88-3————————Toluene__________________I_II I 5 luj 1 OS-9 0-7———————Chl or o benzene_____________11 5 |U| 100-4 1-4———-- — Ethyl benzene_____________ j 5 JU| 100-42-5-——————Styrene_____IIII_II____II 5 luI 1330-20-7——————Xylenes ?Tcta 1 )_____________I S |U

VOAAR300660 1/B7

•^ EPA SAMPLE NCVOLATILE C^AMCS ANALYSIS DATA SHEETI CY8S7 0

a Name: IT CE33ITCS ___________ Contract: 68-01-7262 1

Lab Cede: .IT_____ Case No.: 1C55S SAS No.: _______ SDG No.: CY8S5

Matrix: (scll/wacar) £"5 • Lab Samole ID: CY.S6J!____

Sample wt/vol : 5.0 (g/mL) ML Lab File ID: 4 3 87 DECS

Level: (Icw/mec) LC' J Date Received: 10/14/88

% Moisture: not dec. ____ Date Analyzed: 10/20/88

Column: (pack/cap) PACK Dilution Factor: 1.00

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L

7 A — Q 7 — '3 — —

f •* W w •*

75 C1— 4 ——I *J V t •*

75-00-3 ————75-OS-2 —————6*7 ._ R -* ^

75-15-0 ————7 C — "S E^— A — —7^ *-i 4 *N

S40-53-0 ————$7 — 65-3 —— --i n 7 — n R 9— —

108 05 4- —

7 Q O7 —C _

10061-01-5 ——79-01-6 —————1 •? A — A R— 1 —

71-43—2 —10061-02-6 ——7e? _ *} r; *>

inA— in— i — —

107 10 _A — —79-34 — 5- —— - —1 J V •» ^i*

1 op-gn 7— ^100-41-4 ———100-42-5 ———

——— Ercmcme thanei l y l W i i ! I— ' I Iwc

-• —— C hi crce thane— - — Yi ethyl ene Chlcrlce——— Acaione——— Carbon Dlsulflde

_ . ^<^.U.li^rt^*«^^^.F*j-y

——— 1 , 2-D1cnl crcethene (total ) __

—— -1 , 2-21 c hi o roe thaner> •** *-

——— 1 ,1 r 1-Trlchloroethaoe-• —— Carbon Tet rachl cr Ide

——— Bromod Icnl oromethane——— 1 r 2-D1chloropropane——— cls-1 , 3-D1chloropropene——— Trlchloroethene——— Dlbromochl oromethane——— 1 , 1 r 2-Trlchl o roe thane——— Benzene——— trans- 1 , 3 -Die hi oropropene ___——— Bromof orm——— 4-Methyl-2-Pentenone——— 2-Hexanone——— Tet rachl or oet hen e—— 1 ,1 ,2 , 2-Tetrachloroethane ___——— Toluene

r* K i K& Tc « ^ L _ _ ^^* t- —i n

\

10 |U1C |U10 |U10 |U3 |3J3 | BJ5 1 U5 | U5 | U5 |U5 | U5 | U

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10 |U5 1 U5 j U5 | U5 |U5 |U5 ]U5 |U5 |U5 [U

10 |U10 |U5 j U5 |U5 j U5 | U5 j U5 |U |5 |U

FORM 1 VOA HR3UU661 1

*

"A EPA SAMP.E NC.VOLATILE CR3AMCS ANALYSIS DATA SHEET

| CY868 0010Name: IT CE3SITC5______________ Contract: 68-01-7262 j_______

Lab Cede: IT_____ Case Nc.: 1CS36 SAS No.: SDG No.: CY855

Matrix: (soil/water) WA~y_ • Lab Samcle ID: CY868

Sample wt/vcl: 5.0 (c/mL) ML Lab File ID: 48670EC6

Level: (low/mec) LCW Date Received: 1D/14/8S

% Moisture: not dec. ____ Date Analyzed: 10/20/8S

Column: (pack/cap) PACK Dilution Factor: 1.00

CONCENTRATION UNITS:CAS NC. COMPOUND • (uc/L or ug/Kg) UG/L

74-87-3 ————— —— Chlcromethane_______________ ] 1 0 JU74-83-S ———————— Srcrr.omethane_______IIIIIII_1 10 | U75-01-4—————————Y-;r.y1 Celeries__________III_ I 1 0 j U75-00-3—————————On Icrcethane_I_HI__I__I_I | 10 | U75-09-2 — —— ——— Metr.ylene Chlorlae_________ j 3 j BJ67-64-1—————————Acetcne___________IIIIIII«II_ I 3 | 8J75-1 5-0 ———————— Carocn Dlsulflce____________ | 5 | U75-35-4 ———————— 1 , l-D1chlcroetheneI_IIII_I_H| 5' JU75-34-3—————————1 , 1-DlchlorcethaneIIII_I_I™ | 5 |U540-59-0 — —————1 , 2-C-ichlcroethene (tot a !*)"_" ( 1 j J67-66-3 ————————— Chlcrcrcrm________________"I | 5 | U107-06-2 ——————— 1 , 2-D1chlcroethane_IIH_™I_ [ 5 | U78-93-3 ————————— 2- = utancns______________I___ j 10 [U71-55-5—————————1 , , 1-Trlcnloroethane_I___I| S |U5S-23-5————————Carbon Tet rachl or 1 de___™__ j 5 |U103-05-4————————Vinyl Acetate______^1__II_ I 10 | U75-27-4-- ——— - — Bromodl chl oromethane________ | 5 | U78-87-5 ———————— 1 , 2-D1chloropropane____I_I_ j 5 |U10051-01-5—————cls-1 , 3-D1 chl oropropene_____ j 5 j U79-01-6————————Trlchlcroethene________II_| 73 |1 24-48-1 ———————— D1 bromochl oromethane________ | 5 j U79-00-5 ———————— 1 , 1 ,2-TrichloroethaneII__I_I | 5 |U71-43-2 ———————— Benzene_____________I.I_II_I I 5 |U1 0061-02-6 —————— trans-1 , 3-D1chi oropropene___ j 5 | U75-25-2 ———————— Bromof orm________________III 1 • 5 |U108-10-1————————4-Methyl-2-PentanoneIIIIHIII j 10 |U591-78-6 ———————— 2-Hexanone__________"I_II" 1 -10 |U127-18-4———————Tecrach"loroec^eneIIIIIII"_IIJ 5 |U79-34-5 ———————— 1 .1,2 ,2-TetrachloroethaneII^Il 5 )U108-88-3————————Toluene__________________ _II! 5 | U108-90-7———————Chlcrob^2eneII_IIIIIII_IIH- | 5 |U100-41-4 ——— ——— Ethylbenzens_HI.IIH___III I 5 Iu100-42-5————————Styrene____III_IIII"IIII III 5 I u1330-20-7 —————— Xy I enes~( TotaTJ" | 5 |U

FORM I VGA _ r V'87 Rev

'** £PA SAMPLEVOLATILE cs2~\:::s ANA_VS:S DATA SHEET

I CY859 nfi LZ2•3 Name : I* CE^RITQS______________ Contract: 63-0 1-7262 j __________

Lab Ccce: 17_____ Case Me.: 1 0535 SAS No.: _______' SDG No.: CY865

Matrix: (sell/water) UA"3 * Lab Sample ID: CY869____

Samole wz/vol : 5.0 (g/mL) ML Lab File ID: 4887QEC7

Level : (Icw/med) LO^ Date Received: 10/14/88

% MoTsture: not dec. ___ Date Analyzed-: .10/20/88

Column: (pack/cap) PACK__ Dilution Factor: 1 .00

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L

74-87-3—————————Chl orcmethane________________ I 1 074-83-S ————————— 5rorr.cme'chane___-_________ | 1 075-01-4—————————Vinyl Chl or Ice"_I_I__II_H I 1075-00-3————————Ch~. crcether.e_____________ I 1 C75-0£-2 ———————Vetrwlene Chloride_________ 1 667-64-1————————Acetone____________________ j t 275-15-0————————Car ben DIsuTflce____________ | 575-35-4 ———— ——— 1 , 1-Dlch" oroethene__________ j 575-34-3—————————1 , 1-D1chlorcethane_____I_™_ | 5540-59-0———————1 ,2-Dlchlorcethene ^ total")__| 567-66-3—————————Chl crof crm___________________ | 5107-05-2 ——————— -1 , 2-D1chlcrcetnane___________ j 57E-93-3 ————————— 2-Eutancne I 1 0

UUUUBBJUUUuuuu

7l_5 = ™c ————————— T t -. f 1-Trichloroethane______ | 5 U55-23-5————————Carbon Tet rachl or 1 de________ | 5 U108-05-4————————Vinyl Acetate_______I_IIIIIII 1 1075-27 — 4 ————————— Srcmcdi chl oromethane________ ] 5 U78-87-5 ———————— 1 , 2-D1cnlcropropane_I_I~~~_I | 5 |U10061-01-5—————cls-1 , 3-D1 chl oropropene_____ j 5 JU79-01-6 ————————— Trl chl oroethene________IIIIII! 5 |U124-48-1 ——————— Dlbromochl orome thane__ _ _ j 5 JU79-00-5 ———————— 1 , 1 r2-Tr1chloroethaneI_IIIIH( 5 JU71-43-2 ———————— Benzene_____________IIIIIIIII 5 |U10061-02-6—————trans-1 , 3-5lchToropropeneI__ J 5 |U75-25-2 ————————— Bromcform________________~_| 5 |U108-10-1———————4-Methyl-2-Pentanone_II_IIHIj 10 |U591-78-5———————2-Hexanone_________I_I_II_11 -10 |U127-18-4————————Tet rachl oroethene_I_II_II_II I 5 |U79-34-5 ———————— 1 , 1 , 2 . 2-Tet rachl or oethane" ~_ | 5 |U108-88-3———————Toluene_________________III. I 5 I U1 08-90-7———————ChlorobenzeneI_H______I_™ j 5 |U100-4 1-4 ——————— Ethy 1 benzene______________ [ 5 j U10G-42-5———————Styrene____H_IIIH_I_IHII | 5 JU1330-20-7——————Xylenes~(TotaT) ~ _ j 5 |U

FORM I VGA RKoUUOO^ 1/S7

'A EPA SAMPLE NOVOLATILE C^SANICS ANALYSIS DATA SHEET

Name: IT CERRITCS ______________ Contract: 68-01-7262

Lab Code: IT_____ Case Nc.: 10635 SAS No.: _____ SDG No.: CYE55

Matrix: (so11/water) frA"5 • Lab Sample ID: CYS70

Sample wt/vcl : 5 . 0 (g/mL) ML Lab File ID: 48e70EC3

Level: (low/mec) UC^ • Date Received: 10/14/63

% Moisture: not dec. ____ Date Analyzed: 10/2Q/i!3

Column: (pack/cap) PACK Dilution Factor: 1.PC

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

74-87-3 ————————— Ch'crcmethane ________________ | 1 0 |U74-83-9 ————————— Brcmomethare__ _________ _ ____ j 1 C j U75-01-4 ————————— Vinyl Chloride _ II_I_II_IH_I | 10 |U75-00-3 —— — ——— Chlcrcethane _ ____________ _ j 1 0 j U7 5-0 S- 2- — —— —— Methyl en e Chlorine _________ _ j 6 j B67-64 -1 ———————— Acetone ______________ I __ "I [ 10 | B75-1 5-0 ——— —— — Ca~bcn Disu Trice ____________ ] 5 JU75-35-4 ———— ——— i , 1 -Die hi oroethene ________ _ j 5' j U75-34-3 —————————— 1 , l-Dichloroethane _______ III.! 5 I u540-59-0-- ————— 1 , 2-Dichloroethene ("total") __ j 5 JU67-55-3 —— —— - — Chloroform _ _________________ j 1 1 |107-06-2 ————— —— 1 , 2-D1 chl ores thane ___________ | 5 j U78-93-3 ————————— 2-Sutanone ________ I-I_IIIII_I I 1 ° lu71-55-5- ———— —— 1 , 1 , 1-Trlchl croethane _______ j 5 | U55-23-5 ———————— Carbon Tet rachl or Ide ____ I_I_ i 5 |U108-05-4 —————— — V-inyl Acetate ________________ | 1 0 |U75-27-4 — ----- — Bromcdlchl oromethane _ _ ___ _ | 5 | U78-87-5 —— ————— 1 , 2-Dichloropropane_ ________ | 5 j U10061-01-5 ——— — cls-1 . 3-D1chl oropropene _____ j 5 |U79-0 1-6 ————— —— Trie hi oroethene _____________ | 5 | U124-48-1 ——————— Dibrcmoc hi orome thane ________ | 5 | U79-00-5 ———————— 1 . 1 ,2-TrichloroethaneII _ I_I_ | 5 |U7 1 -43-2 ————————— Benzene _________________ IIIII I 5 j U10061-02-6 ————— trans-1, 3-D i chl oropropene _ j 5 JU75-25-2 ————————— Brcmoform ________________ II _ | 5 |U108-10-1 ——————— 4-Methyl-2-Pentanone ________ j 10 |U591-78-6 ——————— 2-Hexanone _________ II _ HI™ | TO |U127-1 8-4 —— ———— Tet rac.hl oroethene _________ ~ j 5 [U79-34-5 ———————— 1 . 1 ,2,2-TetrachloroethaneII _ | 5 JU108-88-3 ——————— Toluene _________________ IIII I 5 JU108-90-7 ——————— Chlorobenzenel _ I_I_H_IIII_1 1 5 JU100-4 1-4 — — - —— Etny 1 benzene __ _ __ ___ ____ _ j 5 j U100-42-5 ——————— Styrene _______ I.IIIIIIIIIIII I 5 lu1330-20-7 ————— — Xy1enes~(TctaT)~" | 5 JU

FORM I VGA - _ - - - - 1/8 7 Re

TA E^A SAMPLE NC.VOLATILE CRGAMCS ANALYSIS DATA SHEET

|~j CYS71

Name: IT CE39ITCS______________ Contract: 63-01-7252

Lab Code: IT_____ Case Nc.: 10635 SAS No.: _______ SDG No.: CY865

Matrix: (soil/water) WATER. ' Lab Sample ID: CY871

Sample wt/vol: £.0 (g/mL) ML Lab File ID: 4387QEC9

Level: (low/mec) LOW Date Received: 10/14/38

% Moisture: not dec- ____ Date Analyzed-: _10/20/88

Column: (, pack/cap) PACK Dilution Factor: 1.00

CONCENTRATION UNITS:CAS NO. CCMPCUND (ug/L or uq/Kg) UG/L.

74-37-3————————Chl crome thane______________ I 10 JU74-33-S ———————— ~rcrncmethane______________ j 10 | U75-0 1-4 ————————— Vinyl Chloride_____________I | 1 0 |U75-00-3————————Chlcrcethane____________IIII I 1 0 |U75-OS-2 ————————— Methylene ChTcrice______IIII I 2 | BJ67-64-1————————Acetone___________IIIIIIIIIII . 3 | BJ75-15-0 ————————Carbon 5isulf ice____________ j 5 j U75-35-4—————————1 , 1-Dichlcroethene_"_I__~ | 5 |U75-34-3 ——————— —1 f 1 -DichTercethene______II_11 5 I U540-59-0————————1 . 2-Dichlorcethene (totsT^__ I 5 |U67-6S-3—————————Chlcrcf crm________________~_~ j 5 | U107-05-2————————1 ,2-Dichlorcethane______I_II! 5 |U7B-93-3 ———————— 2-Sutancne______________I_I | 10 JU71-55-5-———————1 , 1 , 1-Trichlorcethane______I j 5 |U56-23-5————————Carbon Tet rachl oride_____I_I ] 5 |U108-05-4————————Vinyl Acetate______________~ | 1 0 |U75-27-4 ———————— Brcmodi chl orome thane________ | 5 j U78-87-5 ———————— 1 , 2-Dichloropropane_____II.I! 5 |U10061-01-5—————cis-1 ,3-DichloropropeneI_"I | 5 |U79-01-6————————Trichl oroethene_______IIIIIII 5 |U1 24-48-1 ——————— Di bromoc hi orome thane________ j 5 | U79-00-5————————1 ,1 ,2-TrichloroethaneIH_3_^1 5 lu71-43-2 ———————— Benzene______________I-IIIIII 5 |U10061-02-6—————trans-1 . 3-Dichl oropropene_I_3 I 5 |U75-25-2 —————————— Bromof orm______________'___I_H 1 5 -| U108-10-1———————4-Methy1-2-Pentanone___IIIIII 10 |U591-78-6 ———————— 2-Hexanone__________III_I_III 10 |U127-18-4 ——————— Tetrach"loroetheneII_IIII_I<_I~ | 5 | U79-34-5————————1 ,1 .2, 2-TetrachloroethaneII_I| 5 |U108-88-3———————Toluene_______________I_II I S |U108-90-7 ——————— Chl or o benzene_____I_II_IIII I 5 |U100-41 -4 ——————— Ethyl benzene_HI_III_IIIIIH~ j 5 | U100-42-5 ——————— Styrene____IIIIIIIIII I 1 5 |U1330-20-7——————Xylenes"(TotalT 5 U

i VGA AR300665 1/gv

1- ErA SAMPLE NC.SSMIVCLATILE CFPANICS ANALYSIS DATA SHEET

Nome: I1" CE=:=!"C£_____________ Contract: 68-01-7262CYS65 C023

Lab Cede: IT____ Ca = e No.: 10636 SAS No.: ______ SDG No.: CY86l:

Mstri;:: (soil/watsr) ld&"= Lab Sample ID: CYS65

Sample wt/vcl: 1000 (g/mL) ML__ Lab File ID: 4Sg70Rkp2_

Level: (Icw/med) LCUJ ' Date Received: 1O/14/88

%" "Moisture: not dec. ___ dec. ___ Date Extracted: 11/09/SS

Extraction: (SepF/'Cent/Sonc) CON" Date Analyzed: 11/16/8S

GFC Cleanup: (Y/N) N__ pH: ____ Dilution Factor: 1.00

CONCENTRATION UNITS:NO. COMPOUND (ug/L or ug/Kg) L'E/L G

108-95-2———————Phenol__________________111-44-4 ——————— bis(2-Chlcroethyl ) Ether.95-57-8————————2-Chlcrophericl__________

106-46-7———————1 „ 4-D i c h 1 oreben z ene________100—51 —a————— — r»en zy 1 A1 echo 1 _____________95-50-1 ———————— i ,2-Dichlcrobenrene________95-43-7————————2-Methyl phenol_____________108-60-1 ——————— bis(2-Chlorci=opropy! ) Ether106-44-5———————4-Methylphenol_____________621-64—7-——————N—Nitroso—di—n—propylamine_67-72-1————————Hexachloroe thane___________9S-95-3-———————Nitrobenzene_______________3-59-1 ———————— Isophorone___j-75-5————————2-Nitrophenol.

105-67-9———————2 ?4-Dimethyl phenol________65-85-0————————Ben zoic Acid______________111-91-1 ——————— bis(2-Chloroethoxy)methane.120-83-2———————2,4-Dichlorophencl________120-82-1 ——————— 1,2.4-Trichlorobenzene____

-Naphthalene____-4-Chloreaniline

87-63-3————————Hexachlorobutadiene______59-50-7————————4-Chloro-3-methyl phenol__91-57-6————————2-Methyl naphthalene______77-47-4————————He:-;achlorocyclopentadiene_8S-06-2————————2,4,6-Trich lore-phenol___95-95-4————————2,4, 5-Trichlorophenol____91-5B-7————————2-Chloronaphthalene______

—2-Nitroani1ine131 — 11-3———————Dimethyl phthal ate_208-96-8———————Acenaphthylene____606-20-2———————2,6-Dinitrotoluene

10 JU10 :u1O !U10 !U10 JU10 JU1O !U10 :u1C JU10 JU10 iu10 JU1O JU10 JU10 JU10 :u50 1 U1O !U1O JU10 :u10 :u10 :u1O JU10 :u10 !U1O !U10 JU5O J U10 JU50 J U10 JU10 JU10 :u

FORM I SV-1 ~ - ~ * ' 1/S7 Rev

1C E=A SAMPLE NC.SEMIVCLATILE Or.'cArilCS ANALYSIS DATA SHEET ________________.

Name: IT CEBITS___________ Contract: 68-01-7262CYS65 00^3*

Lab Code: .IT_____ Case No.: 10676 SAS No.: ______ SDG No.: CY865

Matrui: (sail/wat*r) l'JA~E= Lab Sample ID: CY865____

Sample wt/vol: 1'X'O (g/mL) ML Lab File ID: 48S70RK2

Level: (Icw/msd) LCid Date Received: 10/14/95

fc" Moisture: not dec. ___ dec. ___ Date Extracted: 11/0^/BS*

E;; traction: (SepF/Cont/Scnc) CCNT Date Analyzed: 11/16/88

GF'C Cleanup: (Y/N) N__ pH: ____ Dilution Factor: 1.00

CONCENTRATION UNITS:CAS NO. CONFOUND (ug/L or tig/Kg) UG/L Q

CC — ,"~)Q — ""•— — —— • — — —

100-02—7 —————

1*"* * i .T «*i__. -_„— 1 1 *T —

64— 66— — !— — ~~ — * — "—70O5-72-3 ————86-73-7 ——————1 0 *.) — O j. — 6 — — ™" "™* — —

C A— ~*r*\ A —

101-55-3 ——————iie-74-1 ————B5-01-S ———————

84-74-2 —— - ——206-44-0 —————

ic Ao 7C~91-94-1 ——————

^1 R" • 1 P1 1 T— O 1 "7 —11 / Ol /11 / — 0*4— U" —205-99—2 ——————

193-39-5 ——————

I/- < _*-*.a_' _ _ _ _ _7 1 -*T *-

— 3-^i troani 1 ir.e— -Acsr.aDhthen^— "".-i-Dinitro phenol— 4— Nitre-phenol— n-; b-nzoTLiran— 2 ,4-Dinitrctoluene— Disthvlchthslate— 4— Chlorophenyl— phenyl Ether __— F luc re-ne— 4-Nitroani 1 ine— 4, 6-Dini tro-2— methyl phenol— N— Ni trosodi ph«-nvlamine ( 1 )— 4-Eromopheny 1 — phenvl" Ether

u- w-cni QroKpan-^-ne— Pen tachlcrop hen o 1— Phenanthrene— Anthracene— Di-n-butyl phthalate— Fluoranthene— Pyrene— Bu t v 1 ben zvlohthalate— 3.3' -Dichlorobenzidine— Banzo ( a ) an thracene— Chrysene— bis(2-Ethvlhexvl ) phthalate— Di-n-octvl Dhthalate— BenzoC b) f luoranthene— Benzo( k ) f luc ran then e— BsnzoCa) pyrene.— Indeno £1,2, 3-cd ) pyrene— Dibsnz ( a . n ) anthracene— E<enzo (a , h, i ) P-ery lene

5010505 0101010 '1010505010101050101010101010201010101010101010101C)

1

!U!UJU!U:u!U!U!U!U!U!U;u:u:u!Usu:u:uIU:u!U:u!U:u!Usu:u!U!U:u:u!U

(1) - Cannot be separated from Diphenylamine

FORM I SV-2 1/87 Rev

1£ EFA SAMPLE NC.SE:I:VCL-T;LE C?.SAN:CS ANALYSIS DATA SHEET __________

v Name: IT CE=~ I"£_____________ Contract: 68-01-7262CY366

Lab Cede: IT_____ Case Nc. : 10676 SAS No.: ______ SDG No.: CYS6*

Matrix: (soil/water) UJATE=. Lab Sample ID: CY966

Sample wt/vol: 1000 (c/mL) ML__ Lab File ID: APP70K26

Level: (low/med) LC-'-'J Date Received: 10/14/88

%*Moisture: not dec. ___ dec. ___ Date Extracted: 10/16/8S

Extraction: (SepF/Ccnt/Scnc) CONT Date Analyzed: 11/06/88

GFC Cleanup: (Y/N) N__ pH: ____ -Dilution Factor: 1 .00

CONCENTRATION UNITS:COMPOUND (ug/L or ug/Kg) UG/L D

111-44-4-95— 57— £ —541-73-1-106-46-7-100-51-6-

O e. A C "7V »: ** C /

108-60-1-

621-64-7-6 "7 ~7^ 1/ / *. i

7 •=•"' VCG "7C CO / w' D105-67-9-65-85-0 —111-91-1-

1 *"*("] R*"* 101 r»r> ^r__7j- —V o — —1 r'lA— A7— P1 vO *r / — C87-68-3 —57-50-7 —91-57-6 —

PG (")A *— .—DO VO -i — —9^. — O A

91-5B-7 —P-3 — 7JL AGO / *r *t

131-11-3-Or'iCt QA PA.'.'C TO a

_ c- u, _ ,., — , i— r 1 1 e r ! o i—————— bis (2-Chlcrcetnvl ) Ether

L_ '_/ h 1 •_' r i_- D h tsr n O 1—————— 1 , 3-Dichlorobenzene

— ————— Benzyl Al cc-hol——————— i „ 2-Dichlorobenzene—————— 2-Methyl phenol—————— bis ( 2-Chloroiscpropyl ) Ether_—————— 4-jv;sthy 1 phenol—————— N-NitroEO-di-n-propvlamine—————— Hexach 1 oroe thane—————— Nitrobenzene—————— I SOD ho rone—————— 2-Nitrophenol—————— 2 , 4-Dimethy 1 pheno 1——————— Ben zoic Acid—————— bis C 2-Ch 1 oroe t ho xy) me thane—————— 2,4-Dichlorophenol—————— 1 ,2,4-Trichlorobenzene—————— Naphthalene—————— 4-Chloroaniline—————— Hexachlorobutadiene—————— 4-Ch 1 ord-3-me t hy 1 oheno 1—————— 2-Methyl naphthalene—————— Hexachlorocyclopentadiene—————— 2,4,6-Trichlorophenol—————— 2,4,5-Trichlorophenol—————— 2-Chloro.naphthalene—————— 2-Ni troani 1 ine—————— Dimethyl ohthalate———— — Acenaph thy lene—————— 2, A-D in i tro toluene

101010101010101010101010101010105O1010101010•10101C1010501C50101010

t1J UJUJUJ U!UJ UJUJ UJUJUJUJU:u;uJ U:uJU:u!UJUJU!U!UJU!UIU

JU:u:uJUJU:u

r!pU

FORM I SV-1 "" " i/£7 Rev

1C E.-A SAMPLE WCSE>'IVCL*~I-E CF.3ANI3S ANALYSIS DATA SHEET __ ________ f, n p_-

b N*me: IT CE"!"? ____________ Contract: 65-01—262CY366

Lab Code: U_____ Case Nc. : 10636 SAS No.: ______ SDG No.: CY865

Matrix: ( sci 1/wats-r > UJ£~E= Lab Sample ID: CY866

Sample wt/vol : Iv'Xv (g/mL) ML Lab File ID: gS OK'26

Level : (low/med: LCa Date Received: 10/1 A/SS

^""Moisture: net dec. ___ dec. ____ Date Extracted: 1O/16/3S

Extraction: (Sep^/Ccnt/Scnc) CONT Date Analyzed: 11/06/88

GFC Cleanup: (Y/N) N_ pH: ____ Dilution Factor: 1.00

CONCENTRATION UNITS:CAS NO. CCMFCUND (ug/L or ug/Kg) UG/L D

99-0^-2———————3-Nitrcsniline.o-_«—^i—— T———'————Hcs1"!^ z-h 11 iene__51-2S-5————————2, -Dinitrophenol__________100-O2-7———————4-Nit re-phenol______________132-64—c———————Dibenzofuran_______________121-1-1—2———————2,4-Dinitro toluene_________£4—66—"'————————n •*^J-uvlDKth~"1 't*27005—72—3——————4-Chl ore-phen y 1 — pheny 1 Ether.£6—73—7—————————F 1 L:C r«ne___________________100-01-6———————4-Nitroaniline_____________*.«««'' :2-l———————~.6-Dinitrc-2-frie~hyl phenol.66—30-6————————N-Ni trosodipheny 1 amine (1).101-55-3———————4-B r curio phen yl-p hen yl Ether.US— 74 — 1———————Hexschlorobenzene_________87—S6—5————————Pentachlorophenol_________S5—01—E————————Fhenanthrene______________120-12—7———————Anthracene________________

-Di-n-buty 1 phthalate.•Fl uo rant hen e_______

129—OO—O———————Pyrene________________85-6S-7————————Butyl benzyl phthalate__91-94-1————————3j,3'-Dichlorobenzidine.56—55—3————————Benzo( a ) anthracene____

.—9———————Chrysene.117-81-7———————bis(2-Ethylhexyl) phthalate.117-S4-O———————Di-n-octyl phthalate_______205-99—2———————Benzo ( b) f luoranthene______207-08-9———————Benzo ( k ) f luoranthene______

-Benzo (a) pyrene.1*3-39—5———————Jndeno( 1,2 .3—cd ) pyrene.;_7£_3————————j-l^fcen-: f-^ n ) anthracene

191-24-2———————Benzo (g , h, i ) pery 1 ene.

50 J U10 JU50 J U5O ! U10 ' JU10 JU10 " JU10 JU1O JU5O ! U50 ! U10 JU10 JU10 JU50 ! U10 JU10 JU10 :u10 JU10 :u10 !U20 ! U10 !U1O !U10 :u10 :u10 iu10 JU10 JU10 JU10 JU10 JU

(1) — Cannot be separated from Dipheny lamine - o <An

FORM I SV-2 - 1/S7 Rev

-5 Er'A SAWfLE NC.i— ,— _.», , — . /, — - , •— ,—n— — -. K i T ,—"— A i. i ,1 I V C T C T-. ,"' —— *" '! C" —— TS — * v!_:_.— , . L— i-r~.;j — i J i u— HrJr-—rcii L'f-i i r-t cnE=.T ________

b Name: I~ CE==!"C£______________ Contract: 68-01-7262CY867 CQ262

Lab Cede: IT____ Case No. : 10636 SAS No.: ______ SDG No.: CY86!

Matrix: (soil/^ater) u~"= Lab Sample ID: CY867

Sample wt/vol: 1000 (c/.T,L) ML__ Lab File ID: 4Sg70K27_

Level: (Icw/med) LCUJ 'Date Received: 1O/1A/8S

•//Moisture: net dec- ___ dec. ____ Date Extracted: 10/16/38

Extraction: (SepF/Ccnt/Scnc) CONT Date Analyzed: 11/07/Se


CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

10S-95-Z —— -———=henol__________________iii-44-4———————bis (2-Ohlorcethyi ) Ether.95-57-E ———————— 2-2 h lore-phenol__________1-73-1- — -- —— i , 3— Dichlorcbenzene.

106-46-7 ——————— 1 .-^-Dichlorobenzene.100- 51-6 ——————— Sen zy 1 A 1 echo 1 _____95-50-1————————1,2-Dzch lore-benzene________95-48-7—————————2-Merhyl phenol______________108-60-1 ——————— bis (2-Chloroiscpropyl ) Ether.106-44-5———————i-Methyl phenol ____________]621—6-4-7———————N-Ni troso-di—n-propy lamine__67-72-1————————He ;rac hi oroe thane____________93-95-3————————Nitrobenzene________________78-59-1 ————————— Iscphorone__________________ES-75-5—————————2-Nitrophenol_______________105-67-9———————2, 4-Dimethylphenol__________65-B5-0—————————renzoic Acid________________111-91-1 ——————— bis (2-Chl oroe thoxy)methane__120-83-2———————2,4-Dichlorophenol__________120-82-1 ——————— 1.,2,4-Trichlorobenzene______91-20-3————————Naphthalene_________________106-47-8———————4-Chloroani 1 ine_____________87-68-3————————Hexachlorobutadiene_________59-5.0-7————————4-Chloro-3-methyl phenol_____91-57-6————————2-Methylnaphthalene_________77-47-4————————Hexachlorocycl open tad iene___88-06-2————————2 , 4 , 6-Trichlorophenol _______95-95-4————————2,4,5-Trichlorophenol_______91-58-7————————2-Chloronaphthalene_________SS-74-4————————2-Nitroaniline_____________131-11-3———————Dimethyl phthalate___________203-96-S———————Acenaphthylene_____________606-20-2———————2. 6-Dinitrotoluene__________

iO JU10 iU10 iU10 :u10 JU10 JU10 JU10 J U10 JU10 JU10 JU10 JU10 JU10 JU10 JU10 JU5O ! U10 JU10 JU10 JU10 JU10 JU10 JU10 JUIO JU10 JUIO !Uso : u10 JUso ; u10 :uIO JU10 :u

flR3Q06O£LFORM I SV-1 1/87 Rev

SE"1I VCLAT I_E C^3—*JI CS ANALYS IS EAT A SHE- i _________^

Name; IT CE=;F:"S_____________ Contract: 68-01-7262CY867

Lab Cede: U_____ Case Nc . : 10636 SAS No.: ______ SDG No.: CYS65

Matrix: (soil/water) UJA"^ Lab Sample ID: CYS67

Sample wt/vol: lOOO Cg/mL) ML Lab File ID: 4887QK27

Level: (Icw/med) LCuj Dats Received: 10/14/83

7/Moisture: not dec. ___ dec. ___ Date Extracted: 10/16/88

Extraction: (SepF/Ccnt/Sonc) CENT Date Analyzed: 11/07/88


CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L D—

co-09-2 ———————— 3-Nitroar.il ine83- 2- T ———————— s^wena chthene51-2&-5 ———————— 2,^-Dir.itrcphenol100-02-7 ——————— 4-Nitrcohenol132-6--9 ——————— DitenzoTuran121-14-2 ———————— 2, 4-Dinitro tolueneB' .._ f. f. l~> .... . , ~. -— J-l— .,1.— U,^l--1 - — —— — OO — -'-S «-i r/ 1 pn -_i id 1 =i us7005-72-3 —————— 4-Chlorophenyl-phenyl Ether _c6— 7..- 7 rluu,rene100-01-6 ——————— 4-Ni t roan i line534-52-1 ——————— 4 j,6-Dinitro-2-methyl phenol __86-30-c ————————— N-Nitrosod-i pheny 1 amine (1 )101—55—3 ———————— 4-3romoBhenyl -pheny 1 Ether118-74-1 ——————— Hexac hi ore-benzene67-86-5 ———————— Pentachloroohenol85-01— S ————————— Phenanthrene120-12-7 ——————— Anthracene84-74-2 ———————— Di-n-butyl phthalate206-44-O ———————— F luoranthene129-OO-O ———————— Pvrene85-68-7 ———————— Butyl benzyl phthalate91-94-1 ————————— 3,3'-Dichlorobenzidine56-55— s_. ———————— Benzo (a ) anthracene*?1 P — C» 1 — O________pKrv^(=,nci•H A Uv V J. * W 1 * 1 f •' W I 1 *—

117-S1-7 ———————— bis(2-Ethylhexyl ) phthalate __117-84-0 ——————— Di-n-octvlphthalate205-99-2 ———————— Ben zo ( b ) f 1 uoran t hene207-08-9 ——————— Benzo ( k ) f luoranthene50-32— S ———————— Benzo (a) pyrenei v\.» ._'7 ».• i no eno 1 1 «-£«-.:« cc i pyrene53-70-3 ———————— Dibenz ( a , h ) anthracene191-24—2 ———————— Benzo Co , h , i ) perylene

SO1050501010IO '10105050101010501010IOIO10102010IO10IOIOIO101010IO

t1

;uJUJU!UJ UIUJU:uJU:uJU!U!UJUiU!U:u:u;uJUJUJU!U!U:u;uJU:u:uJUJUJUi•

(1) — Cannot be separated from Diphenylamine

. „.. ftR30067i

i* ErA SAMPLE NC.SE^IVOLATILE C^S^NICS ANALYSIS DATA SHEET _______________

b Name: IT CE=.= !"£_____________ Contract: 6S-01-7262CY26S 00275

.---.b Code: U_____ Case No.: 10676 SAS No,: ______ SDG No.: CYSd*

Matrix: (soi 1/warsr) WA"= Lab Sample ID: CYg£ =

Sample wt/vol: 100C_ ic/mL) ML Lab File ID: 4887Qfc-2£

Level: (Icw/med) LC^ . Bate Received: IQ/l-* /££

7." Moisture: net dec. ___ dec. ___ Date Extracted: 10/16/9'c

Extraction: (SepF/Ccnt/Scnc) CONT Date Analyzed: 11/07/gg

6PC Cleanup: (Y/N) N__ pH: _____ Dilution Factor: 1.00

CONCENTRATION UNITS:CA3 NO. CCr.POL'ND (ug/L or ug/Kg) UG/L Q

108-95-2———————P111-44-4———————tis(2-Chloroethyl ) Erher_95-57-8———————2-Chlorcphenol__________541-73-1 ——————— 1,3-Dichlorobenzene_______106-46-7———————i .-i-Dichlcrobenzene_______i 00- 51-6———————Ben z y 1 A1 c o ho 1 _____________95-5O-1 ———————— 1, 2-Dic hi ore benzene_______95-43-7————————2-Methyl phenol_____________1OS-6O-1 ——————— bis (2-Chloroisopropyl ) Ether106-44-5————————4-Methyl phenol_____________621-64-7———————N-N'itroso-ci-n-propylamirie_67-72-1————————He xac hi oroe thane__________9S-95-3————————Nitrobenzene_______________7S-59-1 ———————— I so p ho rone_________________S3-75-5—————————2-Nitrophenol______________105-67-9———————2 . 4-Dimetnyl phenol_________65-85-0————————Ben zoic Acid_______________111-91-1 ——————— bis(2-Chloroethoxy)roethane_.120-83-2———————2?4-Dichlorophenol_________120-82-1 ——————— i ,2.4-Trichlorobenzene_____91-2O-3————————Naphthalene_______________106-47-8———————4-Chlcroaniline___________87-68-3————————Hexachlorobutadiene________59-5O-7————————4-Ch 1 oro-3-me thy 1 phenol____91-57-6————————2-Methyl naphthalene________77-47-4————————Hexachlorocyclopentadiene__88-06-2————————234,6-Trichlorophenol______95-95-4————————2',,4,,5-Trichlorcphenol______9!-53-7————————2-Chloronaphthalene________SS-74-4————————2-Ni troani 1 ine_____________131-11-3———————Dims-thy 1 phthalate_________2OS-96-S-:——————Acenaphthylene_____________606-20-2———————2, 6-Dinitrotoluene_________

10 IU10 ! Ui o ; u10 !U10 :u10 JU10 ' iu10 !U10 !U10 :u10 :u10 ;uIO !U10 :u10 !U10 !U50 ! UIO IU10 !U10 JU10 JU10 :u10 IU10 :u10 :u10 iu10 :u50 ! U10 :u50 ;u10 ;u10 JU10 :u

FORM I SV-1 1/E7 Rev,AR30067Z

1C EPA SAMPLE NO.L^TILS C-3A::;CS ANALYSIS DATA SHEET ____________

ab Name: IT CE" :"S ____________ Contract: 65-01-72*2CYS6S 002 /

..»D Cede: H_____ Ca = £ Nc. : 10£"e SAS No.: ______ SDG No.: CYE65

Matri:;: (tcil/watsr) i':-"S= Lab Sample ID: CYS63____

Sample wt/vol: 1C CO (o/mL) ML Lab File ID: cS7QK'2S

Level: (low/mec) LCa Date Received: 10/1-a/gq

7." Moisture: not dec. ___ dec. ___ Date Extracted: 10/16/88

E::trAcrion: (SepF/Ccnt/Scnc) CDNT Date Analyzed: 11/07/SS

GPC Cleanup: (Y/N) N__ pH: _____ Dilution Factor: 1.00

CONCENTRATION UNITS:CAS NO. CC-MrCUND (ug/L or ug/Kg) UG'L D

99_r)C-2 —

e, i _^ S— c — _

100-02-7-I—**1—' ** .~*1 i_i,ii-->-CA 1*1- ~>

7005-72-3Ee-73-7 ——100-01—6—e— Jl S™ "— 1

101-55-3-118-74-1-S«~t r^ • c7— oo— 5- —Se ."i i G

120-12—7-B4-74-2 ——206—44—0—129-OO-0-85-68-7 —91-94-1 —E;A— ^ — —OO Ow «-•*>i Q r» 1 — o-i J. D l.' J. 7

117-S1-7-11 7 PA AJ. / C*T V*^rte^ OQ— *^

*>A"7 — AS — O»iy / vo T5f'i— — "? P_ —_ v -. -i c— —1 e— — —c— s—J. T «— • s.1 / %_>

53-70—3 —1 O 1 — *?A *"*i . J. — -L.*T A.

—————— ,_.— Ni troar.i 1 ins——————— £ceriachth&n<*—————— 2 ,4-I-initroDhsnol——————— 4-NitrcDhencl—————— D i b ", z c f u r an—————— *-• . A-Oini trot*- lu=ne—————— r-igt hvloht ha late

—————— F 1 ucren e—————— 4-Nitroctnil me—————— 4. 6-Dinitro-2-fn'=thyl phenol—————— N-Nitrosodiphenylamine ( 1 ) __— ———— j.-Sromophenyl -pheny 1 Ether __——————— He :c c c h 1 o r o ben z en e—————— j= en tachloro phenol—————— Phenanthrene——————— Anthracene—————— Di-n -butyl phthalate—————— F luoranthene—————— Pyrene—————— Butyl benzyl phthalate—————— 3,3' -Dichlorobenzidine—————— Eenzo £a ) anthracene—————— Chrysene—————— bis(2-Ethylhexvl ) phthalate—————— Di-n-octyl phthalate—————— Benzo( b) fluoranthene—————— BenzoC k) fluoranthene——————— Benzo(a) pyrene——————— Indeno( 1 ,2 ,3-cd ) pyrene————— • — Dibenz ( a , h) anthracene—————— Benzo (c , h , i ) pery lene

501050eo

. 101010101050501010105O101010IO1010201010IO10101010101010

11!U:uJU!U;uJ U!UJUiUJUJU!UJUJUJUIUIU!U!UIU:u!U!U:u!U!U:u!U!UJUJUJUt1

(1) — Ctnnot be separated from Diphenylamine

FORM i sv-2 fiR3006731/S7 Rev

:S ANALYSIS DATA SHEET _______________

CYS69 C02ib Name: IT rg=-P'!TCg______________ Contract: 65-01- 262

i_ab Cede: U_____ C«ss No.: 10636 SAS No.: ______ ' SDG No.: CYS6?

Matrix: (soil/wate-) UJ£"=- Lab Sample ID:

Sample wt/vcl: 1000 (g/mL) CL__ Lab File ID: *gS70K'2e

Level: (low/med) LCU Date Received: lO/14/gs

m/J Moisture: not dec. ___ dec. ___ Date Extracted: 10/16/85.

Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 11/1S/SS

Gr'C Cleanup: (Y/N) N__ pH: ____ Dilution Factor: 1 • 00

CONCENTRATION UNITS:CAS NO. CQnFOUND (ug/L or ug/Kg) UG/L Q

1 OS-95-2————————Phsncl111-4-1-4———————bis (2-Chloroeth/l ) Ether.95-57-9- ——————2--nlo541-73- i ——————— 1,3-Di c h lore oen z enet:

106-46-7 ——————— i . 4-Dichlorobenzens-_________100-51-6———————Benzyl Alcohol_____________95-50-1 ————— —— 1, 2-Dichlorobenzene_________95-4S-7————————2-Methyl phenol_____________108-60-1 ——————— bis (2-Chloroisopropyl) Ether.106-44-5————————4-Methyl phenol _______________'621-64-7———————N-Ni trcso-d i-n-propy 1 amine__67-72-1—————————He:,-sen lore-ethane____________9S-c?5-3————————Nitrobenzene_______:________78-59-1————————-Isophorcne__________________88-75-5————————2-Nitro phenol______________105-67-9———————2, 4-Dimethyl phenol__________65-S5-O————————Benzoic Acid_______________111-91-1 ——————— bi s £ 2-Chl oroe thoxy) me thane__120-83-2———————2,4-Dichlorophenol__________120-82-1 ——————— 1,2.4-Trichlorobenzene_____91-20-3————————Naphthalene_______________106-47-3———————4-Chloroaniline____________87-68—3————————HexachlorobLttadiene________59-50-7————————4-Chloro-3-methyl phenol_____91-57-6————————2-Methyl naphthalene_________77-47-4————————Hexachlorocyclopentadiene___83-O6-2————————2,4 , 6-Tric h 1 oropheno 1 _______95-95-4————————2,4,5-Trichlorophenol_______91-53-7————————2-Chloronaphthalene_________83-74-4————————2-Nitroaniline_____________131-11-3————————Dimethyl phthalate___________208-96-3———————Acenaphtnylene_____________606-20-2———————2,6-Dinitro toluene__________

IO JU10 IU10 !U10 :u10 !U10 ! U10 ' :LIIO !U10 JU10 JU10 !U10 !Ui o : u10 !UIO JU10 !U50 :uIO !UIO !UIO iU10 iU10 iU10 !U10 !UIO iUIO !UIO JU50 ! U10 :u50 J U10 :u10 !U10 !U

FORM I SV-i ^^OUUb/ii 1/57 Rev

1C E=A SAMPLE NC.SE-TVCL-TI-E C=3-NII= ANALYSIS DATA SHEET _______________

Name: IT CE=c:"'=_______.____ Contract: 65-01-7262CYE69

L-O Code: IT_____ Css= No.: 10676 SAS No.: ______ ' SDG No.: CY865

Matri;:: (soil/water) l-J~"= Lab Sample ID: CY96°

Sample wt/vol: ICO* (g/mL) ML__ Lab File ID: 4£g70K>2Q

Level: (Iww/ms-zj LCU' Date Received: 1.0

"//Moisture: not dec. ___ -dec. ___ Date Extracted: 10/16/39

Extraction: (SepF/Ccn fc/Scr.c) CC'NT Date Analyzed: 11/19/SS

GPC Cleanup: (Y/N) N__ pH: _____ Dilution Factor: 1 -00

CONCENTRATION UNITS:CAS NO. CCKFGUND (ug/L or ug/Kg) UG/L Q

99—09—2————————3—Mi troani 1 ins-_______________£3-32-9————————Acenaphthene_______________51-2S-5————————2, 4-Di.n it re-phenol__________100-02-7———————4-Nitrcphenol______________132-64-9———————Dibsnzof uran_______________121-14-2———————2,A-Dinitrotoluene_________S4-66-2————————Diethylphthslate___________7005-72-3——————4-ChlorophenyI-phenyl Ether,S6-73-7————————Fluorene__________________100-01-6———————4-Ni troani 1 ine_____________534-52-1 ——————— 4.6-D ir.it ro-2-me thy 1 phenol _66-30-6————————N-Nitrosodiphenylamine ( i )_101-55-3———————4-Bromophenyl -phenyl Ether_1 IB-74-1———————r-e:tachlorobenzene__________S7-S6-5————————rente-chlcrophenol__________85-01-S—————————Phenanthrene_______________120-12-7———————Anthracene________________S4-74-2————————Di-n-butyl phthalate________206-44-0———————Fluoranthene______________129-00-0———————Pyrene____________________85-63-7————————Butyl benzyl phthalate_____91-94-1————————3j3'-Dichlorobenzidine___;56-55—3————————Benzo (a) anthracene_______218-01-9———————Chrysene_________________117-81-7———————bis(2-Ethy Ihexyl) phthalate.117-84-0———————Di-n-octyl phthalate_______205-99-2———————Benzo(b) fluoranthene______207-OS-9———————BenzoCk) fluoranthene_____50-32-3————————Benzo (a ) pyrene____________193-39-5————————Indenod ,2,3-cd ) pyrene____53-70-3————————Diber.z (a=, h) anthracene_____191-24-2————————BenzoCg , h. i ) perylene______

50 ! U10 JLl50 ! U50 : u10 !U10 !U10 JU10 !U10 JU50 J U50 ! U10 JU10 {U10 JU50 J U10 ;uIO- JU10 IU10 :u10 ;u10 :u20 ! U10 :u10 !U10 JU10 :u10 !U10 :u10 iu10 :u10 tu10 !U

1


FORM I SV-2 Mt\OUUU/^I/e7 Rev

13 E.-A SAMPLE NG££"._ v_.u-i I-E CrSANJCS ANALYSIS DATA SHEET ______________.

^b Name: IT C£=;c:^rs____________ Contract: 65-01-7261CY370 CO-

Lab Code: IJ Case No.: 10636 SAS No.: ______ ' SDS No.: CY865

Matrix: (soil/water) U!£" = Lab Sample ID: CV97Q

Sample wt/vol : 1000 (g/mL) ML__ Lab File ID: ££70100

Level : (low/me-r) LCU Date Received: 10/l*/g£

5C" Moisture: not dec. ___ dec. ___ Date Extracted: 10/16/55

Extraction: (SepF/Cont/Scnc) CDNT Date Analyzed: ll/18/9ir

BFC Cleanup: (Y/N) N__ pH: _____ Dilution Factor: 1 .00

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L... Q

1 OS-95-2———————Fhencl__________________111-44-i———————bis(2-ChlorceT:nyl ) Ether.°5-57-S————————2-Chlorcphenol__________541-73-1 ——————— 1,3-Dichlorobenzene________106-46-7 ——————— 1. 4-Dichlorobenzsne________100-51-6———————Benzyl Alcohol_____________95-50-1 ———————1, 2-Dichlorobenzsns_____•95-4S-7—————————2-ttsthy1 phenol_____________10S-60-1———————bis (2-Chlorcisoprop/l) Ether106-44-5———————4-Methyl phenol_____________621-64-7———————N-Nitroso-di-n —propylamine_67—72-1 ————— -—Hsxachloroethans___________98-95—3-——————Nitrobenzene_______________78-59-i ———————— I sop ho rone_________________SS-75-5————————2-Nitrophenol______________105-67-9————————2,4-Dimethyl phenol_________65-85-0————————Ben zoic Acid_______________111-91-1———————bi=(2-Chloroethoxy)methane__120-33-2———————2,4-Dichlorophenol_________120-82-1———————1,2,4-Trichlorobenzene_____91-20-3————————Naphthalene________________106-47-8-——————4-Chloroani 1 ine____________87-63-3————————Hexschlorobutadiene_______59-50-7————————4-Chloro-3-metnyl phenol____91-57-6————————2-Methyl naphthalene________77-47-4————————Hexachlorocyclopentadiene__88-O6-2————————2,4,6-Trich lore-phenol______95-95-4————————2,4?5-Trichlorophenol______91-53-7————————2-Chloronaph thai ens-________S8-74-4—————————2-Ni troani line_____________131-11-3———————Dime thy Iph thai ate__________208-96-E———————Acenaphthylene_____________606-20-2———————2,6-Dinitrotoluens_________

10 !U10 !U10 JU10 ! U10 JU10 JU10 ' JU10 JU10 JUi o : u10 :u10 JU10 JU10 JU10 JU10 !U50 !U10 !U10 !UIO !U10 :uIO !U10 :uIO !U1O !UIO !U10 :u5O i U10 ;uso ; u10 :u10 JU10 JU

FDF;;i I SV-1 ^ - ~ - - - 1/87 Rev

1C EPA SAMPLE N2.SE^:VCLAT:LE c=3-rj;cs ANALYSIS DATA SHEET __________

-b Name: IT C£=g I"S°____________ Contract: 68-01-7262CY870

L*o Cede: IT_____ Case No.: 106T6 SA3 No.: ______ ' SDG No.: CY565

Matrix: (soi1/wste-) WA"= Lab Sample ID: CYSTO

wt/vcl: 100C (c-'mL) t_L__ Lab File ID: ASg7QV30

Lavcl: (low/med' LCM Date Received: 10/14/88

3t~Mciature: not dec. ___ dec. ___ Date Extracted: 10/16/8S

Extraction: (SepF/Ccnt/Scnc) CDNT Date Analyzed: 11/18/89

GPC Cleanup: (Y/N) N__ pH: ____ Dilution Factor: 1 • 00

CONCENTRATION UNITS:CAS NO. CCMFCL'ND (ug/L cr ug/Kg) UG/L Q

CC — £|C — *?. ———————

c * _^C_e_'_.— —— C —— w ———— ———————

100-02-7 ————132-6 -c ————121-14-2 ————S4-66-" —————/V.'Vs.( / — s.'

S6— 73— 7 ————_/'»("»— 01— 6 — — —c— j.-.c* i».« •_•**— -•— iC A. —— — ' **1 __ A. - . —— __ __ ——C C ---' *.' —4 ,•, - e = --X V JL. *. *-• _•1 1 O_"Tirt--1 _ _ _ _JL.1C t -r »— — — —37_3,L._5 —————ES-Ol-c —————120-12-7 ————S" _"7 A — *—— ,__ —T""/ •*+— «•""" "" ~" —206-44-0 ————129-OO-0 ————85-68-7 —————O1 — QA— 1 — —^7 J.— VH1 — i — —

^A — SS— "^— — —

213-01-9 ———4 « •» ~\ < — r117— o I—/ ————117-84-0 ———205-99-2 ———207-08-9 ———50-32-3 ————193-39-5 ———c."~ "7(") —_'•_• / '.' •-•

191-24-2 ———

— — — — ~— M •» "t "• D^n ^ line——— t-!C=rnsphti iei it?——— ^ a 4-r n •; trcchenol——— 4-Nit re-phenol——— 34 b^nzofuran——— -- m 4_r,-i n -; tr~ toluene——— n-. pf-i'-'l^htha1 at0— — - — ._t— r^j-ii ,— . K~f~ n hi^n v 1 — ohen v 1 Ethe*^——— tri LiDrene——— --Ni troani 1 ine— — j. s 6— Dini tro— 2— me thy 1 phenol——— N-Nitrosodiphenylamine ( 1 ) __——— .i-B romo pheny 1 - p hen y 1 E t her __——— Hs;:ac h 1 or o ben zene———— p-n-t tachloroDhenol——— Phenanthrene———— Anthracene———— Di-n-butylohthalate———— Fluoranthene———— Pyrene——— Butvl benzyl phthalate——— 3.3' -Dichlorobenzidine——— Benzo fa) anthracene———— Cnrysene——— bis(2-Ethylhexyl ) phthalate——— Di-n-octyl phthalate——— Benzo f b) f luoranthene——— Benzof k ) fluoranthene——— Benzo( a) pyrene——— Indeno( 1 .2. 3-cd ) pyrene ,_ .,,..„„ „——— Dib&nz fa . h ) anthracene———— Ben so f q . h . i } pery lene

50105O50

. I'-5101010105050IOIOIO5OIOIOIOIO10IO2010101010IO10IOIO1CIO

11JUJUJUJUJUJU;uJU!UJUJUJU!UJU!U!UIU!U!U!U!U;u!UJU":u:u!UJU!U!U;uJU11

(i) - Canno1-: be separated from Di pheny lam ineftR3fl0677

FORM I SV-2 - - - - 1/B7 Rev

IB EFA SAMPLE NCSEM:VCLAT:LE CP.SANICS ANALYSIS DATA SHEET ____

Name: IT CE='F I'C£_______________ Contract: 63-01-7262CW71

Lab Cede: IT____ Case No.: 10676 SA3 No.: ______ SDG No.: CYS6*

Matrix: (soil/water) N£" = Lab Sample ID: CYS71

Sample wt/vol: 1000 (g/mL) ML Lab File ID: agS70K31

Level: (Icw/med) LCU Date Received: 10/1*1/58

'//Moisture: not dec. ___ dec. ___ Date Extracted: 10/16/88

Extraction: (Sepr/Ccnt/Scnc} CONT Date Analyzed: 11/13/38

SPC Cleanup: (Y/N) N_ pH: ____ Dilution Factor: 1.00

CONCENTRATION UNITS:CAS NC. COMPOUND (ug/L or ug/Kg) UG/L 0

103-95-"' ———144 * 1 t11 —— **-. —— *. ———— —— ——

9c e-r <— •-' Zi / —

54I-7T.-1 ————106-46-7 ————100-51-6 ———O G — ("i •* — —C? = A 'Z 7

108-60-1 ————106-44-5 ————621-64-7 ————67-72-1 —————oo c= —7 O y w* w<

78-59-1 —————CC 7*^ eCO / D «.<105-67-9 ————65-85-0 —————111-91-1 ————1 *•>••* _ m -T _ "i-iU O-.1 _. —1->i*» QO 1 _*.*.' O-. 1. —p i _r>ri T _,1 (")A A 7 n —f57 AC TO / OO _.*^Q r"i— >"7 —

91-57-6 ————77— A7— A — —PQ r\A-»*^— - _ .OO l.*O fc * —

95-95-4 —————Q 1 RQ 7

8S-74-4 —————131-11-3 ————f~,,~t(~, i~t f ,~i*: .'d— ro — = — — ——VO *;v «. —

„„ _ __C- K - - i-. 1' . itr i Q *

— — bisCZ-Cniorcsthyl ) Ether ____——— 2-ChloroDhenc-l

——— 1 .--Die hi orcbenzene——— Ben z v 1 Alcohol——— 1 . 2-Dic hi ore-benzene——— 2-Methvl phenol——— bis (2-Chloroiscpropyl ) Ether_——— 4-Methvl phenol——— N-Nitroso— di— n-propvlamine——— hexachlcroethan^——— Ni tro benzene— — — I ophoron*1——— 2-Nitrophenol——— 2 . 4 -Dimethyl phenol——— £(=nzoic Acid——— bis t 2-Chl oroe thoxy ) me thane——— 2. 4-Dichlorophenol——— 1. 2. 4-Tr ic h 1 or o benzene——— Naphthalene——— 4-Chloroani line——— Hexachlorobutadiene——— 4-Chloro-3-methy 1 phenol——— 2-Methyl naphthalene——— Hexachlorocyc lopentadiene——— 2,4.6-Trichloroohenol——— 2.4. 5-Trichloroohenol——— 2-Chloronaphthalene——— 2-Ni troani 1 ine——— Dimethyl phthalate——— Ac en a o h thy 1 en e——— 2«6-DinitrotclusTie

1010IO10101010IO101010101010101050IO1010101C)10IOIOIOIO5O1050101010

______

11

!U!U:u:uJU!U!UIU;uiU:u;u:u:u;u:uJU!U!UJU:u!U:uIU!U!UIU!U!U!UJUJU!U

FORM I SV-1 «PQnnC70 i/S7AR300678

i~ EPA SAMPLE NC.SEMIVCL-TILE CRS-NICS ANALYSIS DATA SHEET ___________

b Name: IT CE=?=r~C-£ ____________ Ccntract: 6S-01-7262CYS71

Lab Code: I_T _____ Cass Nc . : 10676 SAS Nc . : ______ SDG No.: CYS65

Matrix: (scil/wate-) n-"= Lab Sample ID: CYg^l

Sample wt/vol: 1CCO (c/mL) ML__ Lab File ID: 49S70K31

Level: (lcw/meti» LCUl Date Received: 10/1^/56

2* Moisture: not dec. ___ dec. ____ Date Extracted: 10/16/S3

Extraction: (SepF/Ccr.t/Sonc) CCNT Date Analyzed: 11/1S/SS

GPC Cleanup: (Y/N) N__ pH: _____ Dilution Factor: 1 • 00

CONCENTRATION UNITS:CAS NO. C2r.FCUND (ug/L or tig/Kg) UG/L Q

co_o9-2 ———————— 3-Ni troani linesr.-r -c ————————— Ac = naphtnene5 • _^s-5 —— . ————— . --I--1 nit re phenol^ (") __ ) __ —— —— —— - .. ——————————— .1 — M ' •*• r'O'^h—— HI"! 1

132-64— * — • ————— Diber.zof uran

94-66-2 ————————— Dietrivlchthalate7005—72-3 —————— 4-Chloropheny 1 -pheny 1 Ether _S6-73-7 ———————— F luoreneiOO-01-6 ———————— 4-Ni troani 1 ine534-52-i ——————— 4. 6-Dinitro-2-fr:etnyl phenol96-3O-6 ———————— N-Nitro = c.diphenvlamine ( 1 )101-55-3 ——————— 4-Brcinopheny 1 — pheny 1 Ether116-74-1 ———————— K*::schloroben = eneS7-S6-5 ———————— PentachloroohenolE5-O1-S ————————— Phenanthrene1 0-1 -7 ———————— AnthraceneSA-74- ————————— Di-n-butyl phthalate2O6-44-O ———————— Fluor an thene129-OO— 0 ———————— PyreneS5-68-7 ———————— Butyl benzyl Phthalate91-94-1 ———————— 3.3'-Dichlorobenzidine56-55—3 ———————— Benzo fa) anthracene21S-01-9 ——————— Chrysene117-31-7 ——————— bis(2-Ethylhexyl) phthalate __117-84-0 ——————— Di-n-octvl phthalate2O5-99-2 ——————— Benzo( b) fluoranthene

5O-32-3 ———————— E-*nzo< a) pvrene193-39-5 ——————— IndenoC 1 .2,3-cd ) pyrene53-70—3 ———————— Dibenz (a , h) anthracene191-24-2 ——————— B»=nzo(Q ,h,i ) perylene

50105050101CIO '10105050101010501010IO10101020IO101C)10IO10IO101010

tI

JUtuJUJ UJUJUJUJUJ UJUJU!U!UJUJU!UJUJUJ UJU!U:u1U!U:u;u!U'.LIJU:uJUJU

(i) — Ccinnc-t be separated from Dipheny 1 amine

flR300679rnE1- T c-;_-. /S7 Re-/

10 EFA SAMPLE MO.FEET 1C ICE Cr£AN!CS ANALYSIS D«TA SHEET

i CY865 Q043L«D Nane: 1 T lE-g^rS___________. Contract: 69-01-^2^2 1_____________ I

Lab Ccce: H____ Case Nc . : 10^"-= SAS No.:_____ SCG No.: Cvtrt?

Matrix: (soil/wate-) '.-J '£s Lao Sample 10: CV3±?______

Sample wt/vol: 1000 '(c/ml) rL... Lab File ID: F

Lcve 1: f low/me c 5 L"'J Da t e Rece ived:

X Moisture: not dec.___ dec.____ Date Extracted:

Ext r act ion: (SepF/Cor. t /Scnc) SESC Date Ana lyzec: 1.0 xi 9/98

GPC Cleanup: (Y/N)_i_ FJH:___ D i l u t i o n Factor: __. 1 . 0

CONCENTRATION UNITS:CP.S NC. COMPOUND Cug/L or ugXKG) ugXL Q -

0.05 IU0.05 IU0.05 IU0.05 IU0.05 IU0.05 IU

1024-57-3----- — ---Heptachlcr epoxide.________ 0 . 05 IU

? 19-85 - 7- ---------- bet a- BHC319-86-!=-----------isl ta-BHC?6-89-9------------csmma-BHCCLindane76 -44-3- --------- — Hep t ach lor309-00-2- — — -- — — fildr in

9<?9-.9g_3____..-__ —— Endosu 1 fan IcO-?7-l------------Dieldr in72-55-9--- —— -- ——— 4^4 '-DOE72-2 0-3 -- — ---- ——— Endr in33213-65-9--- ————— Endosulfan I I72-54-8- — ------ — -4, 4 '-ODD1031-07-8~---------£ndo»ul fan sulfate.50-29-3- —————————— 4,4'-DDT __________72-43-5----- — ———— hethoxychlor ______53 494-70- 5-- — ———— Endnn Ke tone _____5103-71-9---- ————— a Ipha-Ch lordane ___5l03-74-2----------gamma-Ch lordane ___8001-35-2-------- — Toxaphene _________12674-11-2 ——————— -Ar odor- 10 16 ______11104-28-2--- ————— Aroc lor- 1221 ______11141-16-5 ———————— Aroc lor- 1232 ______53469-21-9 ———————— Aroc lor- 1242 ______12672-29-6 ———————— Aroc lor- 1248 ______11097-69-1--- ————— Aroc lor- 1254 ______11 096-82-5- - —————— Aroc lor- 1260 ______

0.05 IU0.10 IU0. 10 IU0.10 IU0.10 IU0.10 IU0.10 IU0.10 IU0.50 IU0.10 !U0.50 IU0.50 IU1.00 IU0.50 IU0.50 IU0.50 IU0.50 IU0.50 IU1.00 IU1.00 IU

FORM I PEST 1/87 Rev.

ID EPA SAMPLE NC£ = ~:CIC.E CC(3ANlCS ANALYSIS DATA SHEET

1 CYS66,0 Name : 1 T CEgc?rTQS_____________ Contract : 69-01-7242 I_______

Lab Code: J£___ Case Nc. : 196?6 SAS No.:_____ SDG No.: CY9e?

Matrix: (soilxuater) U^"- Lab Sample ID: CY3*6

Sample wtXvol: 10 0 0 CcXml) r L, _ Lab File ID:

Leve \ : C IcwXmeS J LOW Date Rece ived t 10x14x88

N Moisture: not dec,___ dec.____ Date Extracted: 10x15/88

Ext r act ion: tSepr xCcn txSonc) ^E~c Date Analyzed: 10xl9xtJ9

GPC Cleanup: <YXN)_JL pH:___ Dilution Factor: 1. 0

CONCENTRATION UNITS:CAS NO. COMPOUND CugXL or ugxKG) unXL Q

319-9^-6 —— ————— --alpha-EHC_________________I 0.05 tU319-S5-7——————————beta-BKC__________________i 0. 05 IU

0.05 IU319-86-S —— - ————— -de 1 ta-EHC5S-89-9---- —------ctmme-SKCCLindane76-A4-6---------—-Heptachlor309-00-2 —————————— Aldrin1024-57-3------—--Keptachlcr eocxider-959-96-6- — - —————— Endosul fan I ______60-57-1 — — — ———— -Disldr in __________72-55-9 ——————————— 4,4 '-DDE __________72-2Q-S ——— - — --- — Endr in ____________33213-65-9 ———————— Endosul fan I I _____72-54-S ———————————— 4,4'-DDD __________1031-07-S----------Endcsulfan su 1 f ate.50-29-3 ———————————— 4,4'-DDT72-43-5------- ———— Methoxych lor53494-70-5 — —————— Endr in Ketone5103-71-9- — ————— -a Ipha-Ch lordane5103-74-2- — ———— — gamma-Ch lordane800 1-35 -2-- — ------Toxaphene12674-11-2 ———————— Aroc lor- 10 1611104-28-2 ———————— Aroc lor- 122111141-16-5 ———————— Aroc lor- 123253469-21-9 ———————— Aroc lor- 124212672-29-6 ———————— Aroc lor- 124811097-69-1 ———————— Aroc lor- 125411096-82-5 ———————— Aroc lor- 1260

0.05 IU0.05 IU0.05 IU0.05 IU0.05 IU0.10 IU0.10 IU0.10 IU0.10 1U0.10 IU0.10 IU0.10 IU0.50 IU0.10 IU0.50 IU0,50 IU1.00 tU0.50 IU0.50 IU0.50 IU0.50 IU0.50 IU1.00 IU1.00 IU

FORM 1 PEST . 1X87 Rev.

/1R3Q068I

ID E=£> SAMPLE NO.FE=TIC:CE CPGANIC5 ANALYSIS DATA SHEET _____________

I 1i CYS67 00462

Name: IT Cr = Pr"9_____________ Contract: 68-01-72*2 I_____________I

Lab Coce: U___ Case No.: lQ*.?v SAS No.:_____ SDG No.: CYS6?

Matrix: isciixwater) b'^^E* Lab Sample ID: CY367_______

Samcle wtxvol: 1000 CgXml) r*L_ Lab File ID: PM-292-104?.

Level: ClcwXmed) LC'.J Date Received: 10x14x83

H Moisture: not dec.___ dec.___ Date Extracted: 10Xl?xg8

Extraction: (SepFxCon t xScnc) SE = C Date Analyze-.: 10x19x88

GPC Cleanup: (YxN)N__ pjri:__ Dilution Factor: 1 . 0

CONCENTRATION UNITS:CAS NO, COMPOUND (ugxu Or ugXKG) uexL Q •

319-84-^-----------alpha-£HC_________319-85-7-------———beta-EHC__________319-66-a--------~--i_el ta-BHC_________58-89-9----------—camma-EhCCLindane).76-44-8------------Heptachlor________309-00-2--------—-fildrin____________102 4-5 7- 3---------- Hep tach Icr epox ide.959-98-8----------- Endosulfan I ______60-57-l------------Oieldr in __________72-55-9--------- —— 4, 4 '-DDE __________72-20-8------- — —— Endr in ____________33213-65-9----- —— -Endosul fan I I72-54-8 —————— ————— 4, 4 '-ODD1031-07-8------ — --Endosul fan sulfate.50-29-3--- — ---- — -4, 4 '-DOT __________72-43-5------- — ---Methoxych lor ______53494-70-5 — ---- —— Endr in Ke tone _____5103-71-9- — -------alpha-Ch lordane ___51 03-74-2 -- — ----- -gamma -Ch lo rdane ___8001-3 5-2----------Toxaphene _________12674-11-2 ————————— Aroclor-1016 ______11104-28-2 ————————— Aroc lor-: 1221 ______11141-16-5 ———————— Aroc 1 or- 1232 ______53469-21-9 ——— ———— Aroc lor- 1242 ______12672-29-6 ———————— Aroc lor- 1248 ______11097-69-1 ———————— Aroc I or- 1254 ______11096-82-5 ———————— Aroc lor- 1260 ______

0.05 IU0.05 IU0.05 IU0.05 IU0.05 IU0.05 IU0.05 IU0.05 IU0.10 IU0.10 1U0.10 IU0.10 IU0.10 IU0.10 IU0.10 IU0.50 IU0.10 IU0.50 IU0.50 IU1.00 IU0.50 IU0.50 IU0.50 !U0.50 IU0.50 IU1,00 IU1.00 IU

I

FORM I PEST K 1x87 Rev.

AR300S82'

13* Esft SAMPLE NC.F£ST!C:'-E CrGf^MCS PNPLYSIS DATA SHE£T _____________

1 r>nj-I CY368 UUo Name: tT CE=s&rT',S_____________ Contract: 69-01-72f2 1____________

Lab Code: TT Case No.: 106.76 SAS N o . : S D G No.:

Matrix: CsoiIxuater ) Ufc'Es Las Sample ID: CY9*S

Sample utXvoI: 1000 .(-/mi) rr__ Lab File ID: PM-S0'

Level: ClouXmec") LO-J Date Received: 10x14/95

56 Moisture: not dec.___ dec.___ Date Extracted: 10X15/88

Extraction: (SepF/ContxSonc) SHpr Date Analyzed: 10x19/88

GPC Cleanup: CY/N)N pri:___ D i l u t i o n Factor: 1 .0———. r ____—.———_

CONCENTRATION UNITS:CAS NO. COMPOUND CugxL or ucXKG3 UCXL Q

319-34-0-----------2icna-HHC_________319-65-7--——---——beta-£HC__________319-36-8--- — - ———— eel ta-EHC_________58-89-9---------———gamma-SHCCLindane).76-44-8—--—--—--He2tachlor________309-00-2 —————————— Aid r in___________1024-57-3------ — --Hep tscr. lor epoxide.959-99-e- —— - ————— Endosul fan I______

0.05 IU0.05 IU0.05 IU0.05 IU0.05 IU0.05 IU0.05 iU

______________ 0.05 IU60-57-1 — —— - ————— Dieldr in __________________ 1 0.10 IU72-35-9 ——————————— 4 ,4 '-DDE __________________ I 0.10 IU72-2Q-S ——————————— Endr in t 0.10 IU

0.10 IU0.10 IU0.10 IU0.10 IU0.50 IU0.10 IU0.50 IU0.50 IU1.00 IU0.50 IU0.50 IU0.50 IU0.50 IU0.50 IU1.00 IU1.00 IU

33213-65-9————————Endosulfan I I_____72-54-3 —— ——— — - — 4,4'-DDD__________1031-07-8-- —— ———— Endosulfan su 1 fate.50-29-3 ——————————— 4,4'-DOT__________72-43-5-------———ttethoxychlor______53494-70-5 ———————— Endr in Ketone_____5103-71-9 ———— ———— a Ipha-Ch lordane___5103-74-2 — - —————— gamma-Ch lordane___8001-35-2- ——— ——— -toxaphene_________12674-11-2 ———————— Aroclor-1016______11104-28-2————————Aroc lor-1221______11141-16-5 ———————— Aroc lor-1232______53469-21-9 ———————— Aroc I or-1242______12672-29-6 ———————— Aroc lor-1248______11097-69-1————————Aroc lor-1254______11096-82-5 ———————— Aroc lor-1260______

FORM I PEST * 1/87 Rev.

AR300683

10 E=P SAMPLE HO.ps*—Ti'~i_,'E £ p ~ A ?s £ ~ (H fii Y s i s DATA SHEET ___I CYS

Name: IT rr-cTrrg_____________ Contract: 6g-Oi869 0047<j

Lad Code: IT Case No.: 106?* SAS No.:_____ SDG No,: CY96?

Matrix: (soilxwater) ua"s Lab Sample ID: CY96.'3____

Sample wtxvol: 100•? CcXml ) rL_ Lab File ID: F__

Level: (iowxmed) LCvi Date Received: 10x14x39

S Moisture: not dec.___ dec.____ Date Extracted: lOXlF/88

Extraction: C SesF/Ccn t/Sonc) '-E- Date Analysed: 10/19/99

GPC Cleanup: (Y/N)N dH:___ Dilution Factor: 1 .0

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or uc/KG).' uc/lL.. Q

319-S4-6---——_----2Ipha-EHC_________3 19-85 -7-- ——— - ——— beta-EHC__________319-86-3 ——— ——— ---celta-BHC_________5S-89-9------------camma-EHCCLindane).-44-S------------Hep tachlor76

309-00-s2-----------Pldr in____________1024-57-3---———---Heptachlor epoxide.959-99-8--—-------Endosulfan I______60-57-1----- — -----Oieldr in_________72-55-9-------- — --4^--DDE_________72-20-8--- — -- — ---Encr in____________33213-65-9 ———————— Endosul fan I I_____72-54-8 ——— ---- ————— 4,4 '-ODD___________1031-07-8------—--Endosulfan sulfate.50-29-3 ———————————— 4, 4'-DOT__________72-43-5------------Methoxychlor___53494-70-5 — - ————— Endr in Ke tone__5103-71-9 ————————— a Ipha-Ch lordane.5103-74-2----------gamma-Chlordane.8001-35-2- — —————— Tcxaphene_____12674-11-2 ———————— Aroc lor-1016___11104-28-2 ———————— Arocjor-1221___11141-16-5 ———————— Aroc I or-1232___53469-21-9 ———————— Aroc lor-1242___12672-29-6 ———————— Aroc lor-1249___11097-69-1 ———————— Aroc lor-1254___11096-92-5 ———————— Aroc lor-1260___

0.05 IU0.05 IU0.05 IU0.05 IU0.05 IU0.05 IU0.05 IU0.05 IU0.10 IU0.10 IU0.10 IU0.10 IU0.10 IU0.10 IU0.10 IU0.50 IU0.10 IU0.50 IU0.50 IU1,00 IU0.50 IU0.50 IU0.50 IU0.50 IU I0.50 IU I1.00 IU E1.00 IU I

I_____1

FORM I PEST K 1X87 Rev.

AR3Q068U

ID E=A SAMPLE NC.PESTICIDE CrSiiNlCS ANALYSIS DATA SHEET _________

I CY870-> Name: I7" CE-ctTQS_____________ Contract: feg-01-724? i_______

0040

Lab Cede: T~ Case Nc.: 1063- SAS No.:_____ SCG No.:

Mat r ix : tao i Ixu-ater) Uifi"~ Lab Samp I e ID: CV370

Sample wtXvol: 1C00 (c.Xml) ML Lab File ID: P -29:

Level : ( low/med) J.CM Date Rece ived: 10/14/98

* Moisture: not dec.___ dec.____ Date Extracted: 10xl?xgg

Extraction: cSepFxContxScnc) SE" Date Analyzed: 10/19/Q8

GPC Cleanup: (Y/N)N__ pH:__ Dilution Factor: 1.0

CONCENTRATION UNITS:CAS NO. COMPOUND CugxL or ugXKG) ucZL Q

319-85-7—— ——— — — bsta-EHC__________319-36-3 ——————————— delte-SHC_________58-89-9- ———— - ———— gamma-EHCCLi ndane ).76-44-8-—-—---—-Heptachlor________309-00-2 —————————— Aldrin____________1024-57-3-----——-Heptachlor epoxide.959-98-8 —————————— Endosul fan I_____"60-57-1 ——————————— Dieldrin__________72-55-9 ——————————— 4,4'-DDE__________72-20-S ——————————— Endr in__________'33213-65-9 —— ————— Endosul fan II72-54-8 ——————————— 4,4'-DDD1031-07-8-- — - — ---EndosuIfan su Ifate.50-29-3 ——————————— 4,4 '-DOT__________72-43-5 ———————————— Methoxych lor______53494-70-5 ——————— -Endr in Ketone_____5103-71-9 ————————— alpha-Ch lordane___5103-74-2--------—gamma-Chlordane___8001-35-2- ———————— Toxaphene_________12674-11-2 ———————— Aroc lor-1016______11104-28-2 ———————— Aroc lor-1221______11141-16-5 ————————— Aroc lor-1232______53469-21-9 ———————— Aroc lor-1242______12672-29-6 ———————— Aroc lor-1248______11097-69-1 ———————— Aroc lor-1254______11096-82-5 ———————— Aroc lor-1260______

0.05 IU0.05 IU0.05 IU0.05 IU0.05 IU0.05 ID0.05 IU0.05 iU0.10 i U0.10 IU0.10 IU0.10 IU0.10 IU0.10 IU0.10 IU0.50 IU0.10 IU0.50 IU0.50 IU1.00 IU0.50 IU0.50 IU0.50 IU0.50 IU0.50 IU1.00 IU1.00 IU

I

FORM I PEST 1X87 Rev.AR300685

SAMPLE NC.PESTICIDE C^G^isICS ANPLYSIS DATA SHEET ________

T o Name: IT CE^P!TCS ______________ Contract: 69-01-^2^2

Lab Code: ! Case No.: 106?4 SAS No.: _____ SCG No.:

Matrix: tsoilxwater) U<-"r Lab Sample 10:

Sample wtXvol: 1000 -C g / m l ) r_... Lab File ID: PM-2Q2-105j

Level: (IcwXmed) LO'J Date Received: 10x14x39

N Moisture: not dec.___ dec.___ Date Extracted: 10x15/88

Ex tract i en: CSepF/Cont xSonc J *=£ac Date Ana lyzefi: 10X19/99

GPC Cleanup: CY/N;h±_ pH:__ Dilution Factor: 1 . Q

CONCENTRATION UNITS:CAS NC. COMPOUND CugXL or ucXKG) ucXL Q -

319-34-6--——------_Ipha-EKC_________319-85-7——--------beta-EHC__________319-36-8-—---———eelta-EHC_________5S-89-9------------gamma-5H.C(Lincane ).76-44-3----- — -----H.eptacnl or________309-00-2------- —— -Aldr in_____________1024-57-3--------—Heptachlor epoxide.959-9S-8---—----—Endosulfan I______60-57-l------------Dieldrin__________72-55-9 ——————— ———— 4, 4 '-DDE_________^_72-20-8--- — - —— —— Endr in____________33213-65-9- —— ———— Endosul fan 1 I72-54-8- — - — ----- 4,4'-DDO1031-Q7-8----------Endosulfan sulfate.50-29-3 ———————————— 4,4 '-DDT __________72-43-5----- — - — — Methoxychlor ______53 49 4- 70-5--------- Endr in Ketone _____5103-71-9 ————————— a lpha-Ch lordane ___5103-74-2---- — ----gamma-Ch lordane ___8001-35-2----------Toxaphene _________12674-11-2 ———————— Aroc lor- 10 16 ______11104-2S-2 ———————— Aroc lor- 1221 ______11141-16-5- ——————— Aroc 1 or- 1232 ______53469-21-9 ——— ———— Aroc lor- 1242 ______12672-29-6 ———————— Aroclor-1248 ______11097-69-1- ——————— Aroc I or- 1254 ______11096-32-5 ———————— Aroclor-1260 ______

I0.05 fU0.05 IU0.05 IU0.05 IU0.05 IU0.05 IU0.05 IU0.05 IU0.10 IU0.10 IU0.10 IU0.10 IU0.10 IU0.10 IU0.10 IU0.50 m0.10 IU0.50 IU0.50 IU1.00 IU0.50 IU0.50 IU0.50 IU0.50 IU0.50 IU1.00 IU1.00 IU

FGRH i PEST 1/87/1^00G86

Appendix D

Reviewed and CorrectedTentatively Identified Compounds

BR300687

"IE E ? A S A M P L E N C .VOLATILE CRGANICS ANALYSIS DATA SHEET

TENTATIVE.Y IDENTIFIED COMPOUNDS |i CY855 000

ab Name: IT CESRITOS______________ Contract: 68-01-7262 |_____________

Lab Code: IT_____ Case No.: .1 Q S 3 S SAS Nc.: _______ SDG No.: CYE65

Matrix: (sc-M/'"ater ) WATE=! " Lac Sample 10: CY8£ =

Sample wt/vol : 5 ,0 (g/mL) ML Lab File ID: ASS70EC1

Level: (low/mec) LO^ Date Received: .1D/1 A/88

% MoTsture: not dec. ____ Date Analyzed: 10/20/g 8

Column (pack/cap) PACK Dilution Factor: T .00

CONCENTRATION UNITS:Number TICs found: __C (ug/L or uc/Kg) UG/L

I j II CAS NUMBER I COMPOUND NAME 1 RT I EST . CCNC

FORM I VGA-TIC . ^ Ke\

IE EPA SAMPLE NVOLATILE CRGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS || CY866

^b Name: IT CERRITQS______________ Contract: 63-01-7252 |_________.

Lab Code: JTT_____ Case No.: 10S3S SAS Nc. : _______ SDG No.: CY865

Matrix: (soil/water) HATER • Lab Sample ID: CY8S6

Sample wt/vcl: 5.0 (g/mL) ML__ Lab File ID: A8870ECA

Lave!: (low/mec) LOW Date Received: 10/1 A/88

% Motsture; not dec. ____ Date Analyzed--. 10/20/88

Column (pack/cap) PACK Dilution Factor: 1 .00

CONCENTRATION UNITS:Number TICs f our.c : __0 (ug/L or ug/Kg) UG/L

i i i : i i i| CAS NUMBER j COMPOUND NAME | RT j EST. CONC. | Q |

AR300689FORM I VGA-TIC 1/67 RGV

1£ £?A SAMPLE NO.VOLATILE CRGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS I————————"«"JT"V"| CY8S7 0009*

b Name: IT CER3ITQS______________ Contract: 68-01-7252 j______________

Lab Cede: IT Case No.: 10635 SAS No.: SDG No.: CYBP5

Matrix: (soil/water) NATER • Lab Samole ID: CY857

Sample wt/vol: 5.0 (S/mL) ML Lab File ID: A897QECS

Level: (low/med) LOW Date Received: 10/1 A/38

% Moi"sture: not dec. ____ Date Analyzed: 10/20/38

Column (pack/cap) PACK Di Tution Factor: 1.00

CONCENTRATION UNITS:Number TICs fcunc: __0 (ug/L or uc/Kg) UG/L

• i i i i ij CAS NUMBER 1 COMPOUND NAME | RT | EST. CONC.'| Q

i i l i t

AR300690FORM 1 VOA-TIC . 1/*J7 Rev

1£ EPA SAMPLE NOVOLATILE CR3ANICS ANALYSIS DATA SHEET

TENTATIVE.Y IDENTIFIED COMPOUNDS | "

b Name: IT CERRITOS______________ Contract: 68-01-7262 |_________h

Lab Cede: .IT_____ Case Nc.: 10635 SAS No.: _______ SDG Nc.: CY355

Matrix: (soil/water) WATER ' Lab Sample ID: CY858____

Sample wt/vcl: 5.0 (g/mL) ML Lab File ID: A8870EC5

Level : (low/mec!) LOW Date Received: 10/1A/8S

% Motsture: not dec, ____ Date Analyzed-: 1Q/20/S8

Column (pack/cap) PACK Dilution Factor: 1 .00

CONCENTRATION UNITS:Number TICs found : __C (ug/L or ug/Kg) UG/L

i i——————————————j - j i] CAS NUMBER I COMPOUND NAME I RT I E5T. CCNC. I Q• *** «* ' ' l1 »5r m *c *H=. w?=- s := = s== I -e = £i = = s = = = = = s:=;s:= =: = ==: = = = = = = =: == I =:=-;=: = = = = I -: = = = =: = ==;= = ==:= I =:=: = :

FORM I VOA-TIC ---.-« v wt/87 RevAR3006U7

1E EPA SAMPLE NCVOLATILE CRGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS |[ CY665

b Name: IT CERRITCS ___________ Contract: 68-01-7263 I

Lab Code: IT Case No.: 10536 SAS No.: SDG Nc.: CY8S5

Matrix: (soil/water) WA'ER • Lab Sample ID: CY8S9

Sample wt/vcl : 5.0 (g/mL) ML__ Lab File ID: aSBTOEC'?

Level: (low/med) LOW Date Received: 10/1A/8S

% Motsture: not dec. ____ Date Analyzed: 10/20/85

Column (pack/cap) PAOK Dilution Factor: 1.00

CONCENTRATION UNITS:Number TICs found : __0 (ug/L or ug/Kg) UG/L

I———————————————j j————————j j jI CAS NUMBER | COMPOUND NAME j RT j EST. CONC. j Q |

AR300692FORM I VOA-TIC 1/87 Rev

15 EPA SAMPLE NOVOLATILE CRGANICS ANALYSIS DATA SHEET _______________

TENTATI'VE-Y IDENTIFIED COMPOUNDS |I CYS70 001'

Name: IT CERRITCS ____________ Contract: 68-01-7262 __ __.

Lab Cede: IT_____ Case Nc.: 1D53S SAS No.: _______ SDG No.: CY8S5

Matrix: (soil/water) WATER • Lab Sample ID: CY870____

Sample wt/vol : 5.. S (S/mL) ML Lab File ID: 4..8870ECB

Level: (Icw/mec) LO^ Date Received: 10/1 A/88

% Moisture: not dec. ____ Date Analyzed: 10/20/88

Column (pack/cac) PACK Dilution Factor : 1.00

CONCENTRATION UNITS:Number TICs found: __0 (ug/L or ug/Kg) UG/L

I 1 J J J II CAS NUMBER j COMPOUND NAME 1 RT | EST. CONC. I Q |

AR300693FORM I VOA-TIC 1/87 Rev

1£ EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS I| CY871

,.db Name: IT CERRITOS _________ __ Contract: 65-01-7252 |

Lab Cede: _T Case Nc.: 1CS35 SAS No.: SDG No.: CY86S

Matrix: (scil/water) WATER • Lab Sample ID: CY871

Sample wt/vcl : 5.0. (g/mL) ML Lab File ID: 48870E09

Level: (Icw/med) LOW - Date Received: 10/1 A/88

% Moisture: not dec. ___ Date Analyzed: 10/20/88

Column (pack/cap) PACK Dilution Factor: 1 - C C

CONCENTRATION UNITS:Number TICs found: __0 (ug/L or ug/Kg) UG/L

1 ICAS NUM2ER i COMPOUND NAME | RT

! ]

1EST. CONC. j Q

- = - —— = »:sj-;*;:_

___ . !„ __

AR30069UFORM I VOA-TIC , 1/97 Rev

1£ EPA SAMPLE NC.VOLATILE CRGANICS ANALYSIS DATA SHEET

TENTATIVE-Y IDENTIFIED COMPOUNDS ) " ~I VSLK1 0

db Name: IT CSRSITQS______________ Contract: 68-01-7262 |__________

Lab Cods: IT_____ Case Nc. : 1CS36 SAS Nc.: ______ SDG No.: CY8S5

Matrix: (soil/water) WA"£R ' Lab Sample ID: VSLK1

Sample wt/vcl : 5.0, (S/mL) ML Lab File ID: LWSEQA08

Level: (Icw/med) LOW Date Received: _______

% Moi"sture: net dec. ____ Date Analyzed: 1D/2D/88

Column (pack/cap) PACK Dilution Factor: _1 . Q C

CONCENTRATION UNITS:Number TICs found: __C (ug/L or ug/Kg) UG/L

I———————————————j j j————————————j |NUMBER 1 COMPOUND NAME | RT \ EST. CCNC. ) Q |

AR300595f-'ORM I VOA-TIC 1/87 he-

IF EPA SAMPLE NC .SEMIVOLATILE OF. SAN ICS ANALYSIS DATA SHEET

o

b

Name :

Code:

IT

IT

TEN

CEPP

TA i A

ITOS

VELY IDENTIFI

Case No.: 1067

s,l>

6

COMPOUNDS

Contract: 63-01-7:: 60CYS65 >

SAS No. : SDG No. :CY86?

023

Matrix: (soil/water) WATE- Lab Sample ID: CYS65

Sample wt/vol: 1000 (g/mL) ML__ Lab File ID: Ag=70RKI

Level: (low/med) LOW Date Received: 10/14/88

/;* Moisture: not dec. ___ dec. ___ Date Extracted: 11/09/85

Extraction: (SepF/Cent/Sonc) CDNT Date Analyzed: 11/16/gE.


CONCENTRATION UNITS:Number TICs f cund : _1_ (ug/L or ug/Kg) UG/L

CAS NUMBE". ! COMPOUND NAME

. 1 . S UNKNOWNi '

F.T i E3T. CONC.

4.7S ! 12ii

Q

FORM I SV-TIC AR300696 1/B7 Rev

IF EPA SAMPLE NC.r* 0 0_-.

TENTATIVELY IDENTIFIE

4 j Name: IT C£»FITOS

Lab Cede: IT Case No.: 10676

Matrix: (mail /water) WA E»

Sample wt/vol: 1000 (g/mL)

Level s 1 Icw/med) LCW

/."Moistures not dec. ___ dec.

Extraction: (SspF/Cont/Scnc )

GF'C Cleanup: (Y/N) N DH :

Number TICs found: 1

*.. •» , iCAS NUMBER ! COMPOUND

1 . i UNKNOWNii

D COMPOUNDS

Contract: 6S-01-7C62

SAS Nc. : SDG

Lab Sample ID:

ML Lab File ID:

Date Received:

Date Extracted:

CCNT Date Analyzed:

Dilution Factor

CONCENTRATION UNITS:(ug/L or ug/Ka) UG/L

NAME RT EST.

31.27

V J *-

CYS66 JJ*

Mo.: CYS6?

CY866

AES70K26

10/1^/88

1O/16/8S

11/06/98

: 1.00

i iiCDNC. ! D

12 ! JJ ritt

AR300597 1/B7RFORM I SV-TIC 1/87 Rev

IF ErA SAMPLESEMIVCLATILE CRSANIC3 ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS

Name: IT CERPITCS_____________ Contract: 68-01-7262CY867 C02G4

Lab Code: IT_____ Case Nc. s 10636 SAS No.: ______ " SDG No.: CY96*

Matrix: (soil/water) WATE= Lab Sample ID: CYS67

Sample wt/vol: 1000 (g/mL) ML Lab File ID: 4gS70K27

Level: (low/med) LOW Date Received: 10/14/88

7." Moisture: not dec. ___ dec. ____ Date Extracted: 10/16/88

Extraction: (SepF/Cont/Sonc) CQNT Date Analyzed: 11/QT/ea

GPC Cleanup: (Y/N) N__ pH: _____ _ Dilution Factor: 1.00

CONCENTRATION UNITS:Number TICs found: _1. (ug/L or ug/Kg) UG/L

CAS NUMBER ! COMPOUND NAME

1. J UNKNOWN^ !

RT

•— • « r\—tO 1 • -i /

EST. CONC.

10

i! Q

- t — w — — —

! Ji

FORM I SV-TIC -"wwuu 301/87 Rev

IF E=A SAMPLE N-.SEMivcLfi-T.LE CP/SANICS ANALYSIS DATA SHEET __________


b Name: IT r^FITCS ____________ Contract: 68-01-7262CYS63

f • n 9 *v *-• *-» *

Lab Code: U_____ Case No.: 10636 SAS No.: ______ SDG No.: CYS65

Matrix: (soil/water) WATE" Lab Sample IDs CYS68

Sample wt/voZ: 1000 (c/mL) ML__ Lab File ID: A8£70K2£

Level: (low/med) LOW Date Received: 10/1-t/eg

/."Moisture: not dec. ___ dec. ___ Date Extracted: 10/16/88m

Extraction: (Ss-F/Ccnt/Scnc) CONT Date Analyzed: 11/07/88

EPC Cleanup: (Y/N) N__ pH: _____ Dilution Factors 1 - 00

CONCENTRATION UNITS:Number TICs found: _1. (ug/L or ug/Kg) UG/L

CAS*'NUM£ER

1.

COMPOUND NAME

UNKNOWN

P;T

31 . 27

t ii i1 E3T. CONC. ! D

! 14 ! Ji i

FORM i SV-TIC AR3QQ699 1/87RevHllOwwW Jf J

IF EPA SAMPLE NC.SEMIVCLAT.LE CF.GANICS ANALYSIS DATA SHEET _______________


b Name: IT CE-PI"'S __________ Contract: 68-01-7262CYB69 C029(

Lab Cede: rr____ Case Nc.: 10636 SAS Nc. : ______ 'SDG No.: CY86?

Matrix: (soil/water) WA"=. Lab Sample ID: CV869

Sample wt/vol: 1000 (g/mL) QL__ Lab File ID: 48870K29

Levels (Icw/med) LOW Date Received: 10/14/86

% Moisture: not dec. ___ dec. ___ Date Extracted: 10/16/88

Extraction: (SepF/Cont/Sonc) CC'NT Date Analyzed: 11/18/88

GPC Cleanup: (Y/N) N__ pH: _____ Dilution Factor: 1.OO

CONCENTRATION UNITS:Number TICs found: _0 (ug/L or ug/Kg) L'G/L

1

CAS NUMBER ! COMPOUND NAME

it

RTit

EcT. CCNC. ! 0

ii

FORM I SV-TIC ~~W/VV1/B7 Rev

IF EPA SAMPLE NCSEMIVOLATILE OP.SANICS ANALYSIS DATA SHEET ________-«

TENTATIVELY IDENTIFIED CCMPCUNDSb Name: IT CE=P'I_TCS____________ Contract: 68-01-7262

CYE70

Lab Code: U____ Case No.: 10636 SAS No.: ______ ' SDG No.: CY865

Matrix: (soil/water) U£TE=: Lab Sample IDs CY870

Sample wt/vol: 1000 (g/mL) ML__ Lab File ID: 48870K30

Level: (Icw/med) L~w Date Received: 10/14/88

K* Moisture: not dec. ___ dec. ___ Date Extracted: 10/16/83

Extraction: (SepF/Ccnt/Scnc) CONT Date Analyzed: 11/18/88

GPC Cleanups (Y/N) N__ pH: _____ Dilution Factors 1 • 00

CONCENTRATION UNITS:Number TICs found: _0 (ug/L or ug/Kg) Ug/L

*CAS NUMBER COMPOUND NAME RT E5T. CDNC. Q

AR30070IFORM I SV-TIC ~ ~ " " 1/87 Rev

IF EP'A SAMPLE NC.SEMI VOLATILE CRGANICS ANALYSIS DATA SHEET __________^-v-

TENTATIVE-Y IDENTIFIED COMPOUNDS

TT_,j Name: IT CE=RITCS______________ Contract: 68-01-T262CYS71

Lab Code: U_____ Case No.: 10636 SAS No.: ______ SDG No.: CY86?

Matrix: (soil/water) WATE-: Lab Sample ID: CYE71____

Sample wt/vcl: 1000 (g/mL) ML Lab File ID: 48870k'31

Levels (low/med) LOW Date Received: 10/14/88

*// Moisture: not dec. ___ dec. ___ Date Extracted: 10/16/88

Extraction: (SepF/Cont/Sonc) CDNT Date Analyzed: 11/18/88

GPC Cleanup: (Y/N) N__ pH: ____ Dilution Factor: 1.00

CONCENTRATION UNITS:Number TICs found: _0 (ug/L or ug/Kg) UG/L

*-•

j ; :CAS NUMBER ! COMPOUND NAME ! RT 1 EST . CONC,

i i 'I i i

Q

AR300702

FORM I SV-TIC 1/87 Rev

1- - EPA SAMPLE NC.SES'. I'-CL~T ILE C^3A:JlC-= f-n L'-'S IS DATA SHEET _______________

TENT-T IVE-v I DENT I r I ED C OMP GUND3

Name: |T CH^S:~C'=____________ Contract: 68-01-7262SBLK1 GO'lQt

Lub Code: U_____ CSES Nc. s 10636 SA3 No.: ______ SDG No. s CY865

Matrix: (soil/water) UJ~"=- Lab Sample IDs SBLl-:'l____

Sample wt/vol: 1000 (g/mL) ML Lab File ID: 4887QK2:

Level: (Icw/med) LOW - Date Received: ______

"/. Moisture: nc-z dec. ___ dec. ___ Date Extracted: 1O/16/83

Extraction: (SecF/Ccnt/Scr.c) CONT Date Analyzed: 11/06/88

GPC Cleanup: (Y/N) N__ pH: _____ Dilution Factor: 1 .00

CONCENTRATION UNITS:Number TICs found: _0. . (ug/L or ug/Kg) Ug/L

«T ' *

CAB NUM3E=. ! CCMFCL'ND NAME ! RT

i ii »

"1

E5T. CCNC. ! D

J

FORM I SV-TIC flfc^nnTHQ i/B7 Rev.

lr ' E=A SAMPLE NO.SEMlVCLf-TIL.^ CP.3-NICS ANALYSIS DATA SHEET _______________

TENTAT IVE_ f IDENTIFIED COMPOUNDS

Name: IT CE=PI^CS_____________ Contract: 68-01-7262SBLK2 CO 417

Lab Cede: U_____ Case No.: 10636 SAS No.: ______ S-G No.: CV86?

Matrix: (soil/water) UJA"=: Lab Sample ID: S5LK2

Sample wt/vol: 1000 _(c/mL) ML Lab File ID: 48S7QRK'l

Levels (low/med) LGi'J Date Received: _______

!•: Moisture: not dec. ___ dec. ___ Date Extracted: ll/0°/88

Extractions (SepF/Ccnt/Sonc) . CDNT Date Analyzed: 11/16/SS


CONCENTRATION UNITS:Number TICs found: _2 , (ug/L or ug/Kg) UG/L

CAS NUMBER

i•k Z ">2

COMPOUND NAMEi

CYCLOHEXANONETRICHLORO-1-PROPENE I SOMES

F:T

5.236.73

EST. CONC."

8.01 * '

Q= KES =

J

J

FORM I SV-TIC 1/87 Rev

Appendix E

D?0 Report for Contractual Compliance

1R300705

of 3—*M— r-

\1 15<5L\__O- ORGANIC DATA VALIDATION SUMMARY

Date Review Completed: 12-20-88 Contract Lab: IT CerritosCase Nc. 10636 " Contract No. 63-01-7262Site Name: Cryo Chem Lab DPO: Diana BaldiSample Ncs.: CY365,CY366, CY867, CY868, Reviewer: William Zimnerman

CY869, CYS70, and CY871 from Region III/ESATPhone: (301) 266-9887

MATRIXCONCENTRATION! low

soil/sclid iacueous

med

! 7other ' i

hicrh! MATRIX RELATED COMMENTS1 !! 1i 1

70LATILESGC/MS tunir.a — 3FBInitial CalibrationContinuinc CalibrationSurrocate RecovervMatrix SoikesReaaent BlanksHoldina Times

OKX

XX

X

FYI

XX

Action

11X

COMMENT

See Note 1See Note 2

See Note 3

3EMI-VOLATILESGC/MS tunina — D7T?PInitial CalibrationContinuinc CalibrationSurroaate RecovervMatrix SoikesReaaent BlanksHoldina TiT.es

OKXX

FYI

1 X

XX

X

1

Action

X

COMMENT

See Note 4See Note 5

See Note 6

PESTICIDESInstrument PerformanceInitial CalibrationContinuinc CalibrationSurroaate RecovervMatrix SoikesReaaent BlanksHoldina Times

OKXXXXXXX

FYI Action COMMENT

DVERALL CASECompound IdentificationData Cornel eteness

OKXX

FYI Action

REVIEWER'S COMMENTS:

DOCUMENTATION ATTACHED (see following pages)

AR300706

Case 10636 Page 2 of 3

Organic Data Validation Summary

Note 1 - The response factor for 2-butanone was less than 0.050in the initial calibration. (See Form VI in Appendix*)•

Note 2 - The response factor for 2-butanone was less than 0.050in the continuing calibrations. In addition, severalcompounds, including 2-butanone, exceeded the maximumpercentage difference (25%D) precision criteria in thecontinuing calibrations. (See Form VII in Appendix F).

Note 3 - The r.aximum concentrations of compounds observed in thelaboratory method blanks are listed below. (See Form Iin Appendix F).

Compound Concentration

methylene chloride* 3J ug/Lacetone* 5J ug/Ltoluene* U ug/L

* Common laboratory contaminants

Note 4 - Several compounds exceeded the maximum percentagedifference (25%D) precision criteria in the continuingcalibrations. (See Form VII SV-1 in Appendix F).

Note 5 - Three samples, CY865, CY867 and CY865MS were outside thesurrogate recovery QC limits for S4 (Phenol-d5) recoveryas required by the contract. (See Form II SV-1 inAppendix F).

Note 6 - The holding times for the extraction of the semi-volatileorganic compounds was exceeded by twenty-one (21) daysfor sample No. CY865. (See Form I SV-1 in Appendix F),

Appendix F

SUDDort Documentation

3*300708

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n inu> OiOH

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O 4-J O rHnj tt td O "HJZ O O 4-> JH 4-J4-) rH C O O *CGJ JS O O rH r-Jg o u c (3 x: cO C-H to U >JH O *G 4J rH (C IO 4J I ^ >* IH -HrH QJ CNJ J2 C 4J E,C U ^ I -iH. G> GJU RJ rH M > 4J CO

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AH300709

6AVOLATILE CRGANICS INITIAL CALIBRATION DATA 00154

b Name: IT CE3SITCS_____________ Contract: 63-01-7252

Lab Code: U_____ Case Nc.: 10535 SAS Nc.: ______ ' SDG No.: CY8G5

Instrument 10: GCMSC Calibration Date(s): 08/15/S8 Q £/15/8 8

Matrix: (soil/water) WA"E3 Level : (Icw/med) LC»* Column: (pack/cap) PACK

Win RRF for S?CC(S) = 0.300 (0.250 for Brcmcfcrm) Max %RSD for CCC(*) « 30.0%

RRF>OO= twvscsas __ RRFISO= LWVECS^T RRF200=\

COMPOUND JRRF20

| Chl cromethane____________S 0| Brcmcmethane______________ | 1jVinyl Chlori ce_____________|Chloroetnane______________| Methyl er.e Chlcr-ice_________| Acetone_____„________-|Carben Disu1f ice_________| 1,1-Dichlorcethene______1,1-Dichlcrcethane________,2-Dichlorcethene (total)_."il ore-form^____________

| 1 ,2-Dichl crcetnsr.e________| 2-But a none________________jl,1;1—Trichlcroetnane____|Carbon Tetrachlcrice______|Vinyl Acetate^_____________|Bromcdichlorcmethane_____| 1 ,2-Dichl ore propane_____*|cis—1,3-Dichlcroprcpene___| Trie hi oroethene__________IDi bromcchlcrcmethane_____J1,1,2-Trichlorcethane_____j Benzene___________________j trans-T,3-Dichloropropene_| Bromof orm_______________|4-Methyl-2-Pentanone______j 2-Hexanone_______________|Tetrachloroethene_________j1,1.2,2-Tetrachloroethane_8| Toluene____________________*jchlorobenzene____________8I Ethyl benzene____________x(Styrene_________________ I 0Xylenes ((Total)__________| 0

.M-ene-dB__________ __| 1.2i2| 1.255| 1.388[ 1.362| 1.264| 1|Bromofluorcbenzene " _~] 0.725] 0.709J 0.781| 0.7S1J 0.7Aij 0| 1 ,2-Dichlorcethane-dZ~ ~~ ~1 2.099| 2.282) 2.488| 2.480| 2.328\ 2

FORM V: VGA AR30Q7IO 1/B7 Re-r* .-* ,, ••* t

7A 00175VOLATILE CONTINUING CALIBRATION CHECK

Name: I"" CH" IT.r '____________. Contract: 65-01-7262

Code: U_____ C*s* Nc.: 10636 SAS No.: ______ .SDG No.: CY865

Instrument ID: ECN'sC Calibration date: 10/20/85 Time: O°27

Lab File ID: LMVEIO"2 Init. Calib. Date(s): 08/15/88 08/15/85

Matri;;: (sell/water) W^"= . .Level:(low/med ) LOW Column :( pack/cap) PACK

Min RP.F50 fcr SrCC(#) * 0.300 (0.250 for Bromo-form) Max 7.D for CCC (*) = 25.07.

CONFOUND

Chlcrometn&ne *B r GiTicme t l~ian eVinvl Chloride *ChlcrccthonsMethvlene Cnlorids 'Ac 5 -3H5C a. r t c n DisulfideI . I— Dirhicroethene -1 , 1— Dichlc^oeihane *1 ,2-Dicnlcrc.sthene (total ) __Cr.lcr-Z'f C-.TI1 * 2-Dicnlcr-stnane2-Hut«ncne1.1. 1-TricMcrcethaneCa-rbcn Tetrschlcride1 1 4 — , , 1 A. ~ - * _ i. _viny 1 n<_^r*at:=r

B r c me d i c h 1 c r erne t nan e1 . 2-D i - h 1 or -3 c ropan ecic— I .3— Dichloroprop^neTriCMlorc-sther.eD i b r Gmcc h 1 o r cms thane1 , 1 ,2— Trie hi or oet haneBenzenetrans-1 ,3-Dichloropropene __Brcmoform 44-Methvl-2-Fentanone2-He:;anoneTet rachl oroethene1,1 , 2 ? 2-Tet rachl oroe thane _ 4Toluene SChlopobenzene 4Ethylbenzene sStvreneXylenes (Total)

Toluene— d£Bromoflucrobenzenel,2-Dichloroethane-d4

RRF

t 0.65S1.366

ft 1.74?1.0351.9090.5524.424

K 1 . 223t 2.915

1.976It 3.5452 . 3330 . 03o0 . 3340 . 3030 , 7470.441

C 0.3670.6360.3470.3660 . 290O.9480.225

* 0.2710.457aT'Q'~V. vr_:0.353

* 0.576K 0.765* 0.938S 0.4730 . 9430.553

1.3020.74S2 . 335

RRF 50

1 . 6S31.4661 . 6700 . 9271.8420.6913.3361.2502.8991 . 3923.0172.4680 .0180 . 3260.3290.5110.3850 . 3220.4770 . 3720 . 3700.2640.8120.224O.2S80.4670.3250 . 4990 . 5000.7210.9750.4770.827.-. c «-\ -7U . w*-i /

0.4990.6762*248

7.D

Cr96.2)fl-7.7-4.510 ".4

-r e:.' • i»<_ _*• > c "%^

24.6-i.S0,5 4=

, 14.9_ e o— .' • O££oTo52.4

-B.6(5i7eT)12.712.325.0-7.2-1.19 . 0

14.40.4

-6.3 #_-^ o-. » 117.1

t_41._413.2 *5.8 4

, -3.9 *, 0.2 4. 12.3! 5.6

61.7,-17.1

3.7it _ ^1TR3GQ7II

FORM VII VGA 1/B7 Rev-

EE~:VCLA-:LE CONTINUING CALIBRATION CHECK C03GOName: IT Cg= =!"?_._____________ Contract: ec-01-T2&2

Code: U____ Case Nc. : 10636 SAS No.: ______ SDG No.: CY86?

Instrument ID: ECST- Calibration date: 11 /0&/SS Time: 1630

Lab File ID: &LCE-'2^2 Init. Calib. DatsCs): 10/27/88 10/27/88

Min RRF50 for &FCC:*} = 0.050 Ma;: '/ID -for CCC(*) = 25.0V.

CCrPC.UND

F' h e r, c 1bis (2-Chlorre-_hvl ) Ether2-Chlcrcohenol1 , 3-3i chl ore-ben rene1 , 4-2ichlcrCfDsnreneBenrvl Alcohol1 , 2-Dichlcrobenrsne2-Nsthylchenclbis ' 2-Ch:crci = oprc-pyl ) Etne

N-N itrcsz-di-n-pro py 1 a!?, i n e_

Mi J-w-,-'--!-— — F- —t -J i i.tC.wftr !!_._• fie:

I sc pn or one2-Nitrophsr.cl2 , 4-Dimethy 1 phenolEenzzic Aridbis ( 2-Chlcroethoxy ) methsne_'',4-Dichloroohenol1 < 2 , 4-TricnlcrobenzeneNaphthalene4-Chlc-rc-ani 1 ineHexachlorobutadiene4 -C h 1 o r o -3-me t h v 1 D hen o 12-Methy I naphthaleneHexachlorocyclopentadiene _ *2,4.6-Trichlorophenol2,4, 5-Trichlorophenol2— Chloronaphthalene2-Ni troani 1 ineDimethyl oh thai ateAc e n a p h t hy 1 en e2 , 6-Dinitro toluene3-Ni troe.ni 1 ineAcenaphthene2,4-Dinitrophenol ±4-Nitrophenol *

_____RRF

1.6S61 .7901 .5911.6590.6851 . 60?1.3941.5931 . 491

* 0.9450.6 = 20.3310.7150 . 2400 . 3500.2530.4960.3550.3460.97S0 . 5020.1950 . 432i . 0390.296O.445O.4841.235O.3561.3961.76&0 . 3730.4951.1190.1850.145

RRF 50

2.0562.0711.6611 .6011.6370.9691 .65?1 . 303

1 . 500i . 0090.71 £0 .-"-540.7580.2440 .3260.1440.4930 . 3380.3441.0930.4360. ISO0 .4061 . 0230.2590.4440 . 4791.3240.4551.5122.0850.3440 . 5231.1970.1390.115

V.D-1.3 *-9.87.2-0.61.3 S41.5;

-3.16.5

-0 . 6-6.3 4-3.8

G*29 . 3iJ-6.0-1.7 *6.9

(43". ij)0.64.8 *0.6

-11.83.27.7 S6.0 *1.5 !12.5 *0.2 *1.0

-7.2(£2778)-8.3

-18.17.S-5.7-7.0 424.9 *20.7 41

i

AR5007S2FORM VII SV-1 1/E7 Rev

EE^IVCLATI'-E CONTINUING CALIS-R A7ICN CHECK G Q ° 6 1

ab Name: IT CE==:~CS-_______;_____ Contract: 6S-01-T262

..-b Code: £T_____ Cass Nc.: 10636 SAS No.: ______ SDG No.: CY865

Instrument ID: GCM£^' Calibration date: 11/06/88 Time: 1630

Lab File ID: &rCE---Z^2 Init. Calib. Dats(s): 10/27/S8 10/27/8S

Min RRF50 fcr SrCC(S) = 0.050 Max ED for CCC(*) = 25.0V.

11! CONFOUND

I Dibenzof uran! 2. -i-Din it re-toluene!Di*tiv/lDhtRola«i-i-Chlorcphenyl-phenyl Ether! Flucr=-e!A-Nitr=*nilineI 4,6-Dinitro-2-methylph5nol_• ivj— Ni tresodipheriylamine ( i )_J! --Broffic-Dhenyl-phenyl Ether_! Her: ? c n I c r c b en z =n e! Per "ir-zhl z^ccnenol •\ F hensnizhrer.e1 1— n thracensJ Di-n-butvlph-halateI Fluoranthene ?> Cl 1* »- — r- —i r y r cr n tr!5utvlban=vlphthelate'3,3' -DichloroDenzidineI Ersnzc ( a } anthraceneSChrvsene1 bis (2-Ethylhe::yl ) phthalate_IDi-n-octvlDhthalate >! Ben re C b) fluoranthene! Benzo C k ) f luorantheneI Benzo ( a) pyrene '! Indeno( 1 ,2.3-cd ) pyrene1 Dibenz (a . h) anthraceneIBenzoCcj , h. i ) perylenet!Nitrobenzene-d5I 2-FluorobiDhenyl!Terphenvl-dl4!F*henol-d6! 2-FluoroohenolI 2, 4,6— Tribromophenolt*

RRF

1.714O.4971.3580.7611.3230.3 20.147

K 0.4360 . 2620.315

< 0 . 1920.9310.9031.171

C 1.1851.0250 . 5420 . 3200 . 9920.9 IS0.765

C 1.4851.4361.166

K 1.1360.9330 .7300.896

O.3631.2740 . 9401.7321.2790 . 336

RRF50

1.8240 .5201 . 5930.7901.4700.3510.1330.4740.2470.2790.1451.0180.9541.2*01.1061.0760.6600.3611.1080 . 9 S30.9371.5771.4041.2701.2151.1091.0711.036

0.3611.3780.9361.5761.1990.2B5

vn

-6.4-4.6

-17.3-3.B-11 .1-2.69.52.55.7

11.4O * c_. T » t.' '

— ? .3-5.6-7 .66.7

-5.0-21. S-12.8-11.7-7.1

—6 .2 3O *?

-8.9-7.0

-18.9*r37.5?-15.6

0.6-8.20.49.O6.315,2

(1) Cannot be separated from Diphenylamine

AR300713

SEM.:VCLAT:LE CONTINUING CAL:EKATICN CHECK: j-A •*-.•-0 0 J o 'fb Name: I" CE = ? ITCH '____________ Contract: 68-01-7252

*.-D Code: H____ Case Nc.: 10676 SAS No.: ______ SDG No.: CY8c5

Instrument ID: GCr=;i' Calibration date: 11 '16 'gg Time: 1719

Lab File ID: r!T-CEK2"72 Init. Calib. Da.te(s): 10/2"/8g 10/27/gg

r sFcccs) = o.oeo

CCMFDUND

Rhenc 1bis(2-Chlcri.ethyl ) Ether __2— Chl croc henol1 , 3-Dichlcrobenzenei . 4— Dichlcrocsnzenec-enzvl Alcohc 11 ,2-Dicr.lcrobenzene2-Msthvl Phenolt is ( 2-C~ 1 oroisoprcpvl ) Ethe^-Me thy 1 Dhenc 1N - N .1 1 r c s -• - d i - n - p r o p y 1 a m i n e _JKeitschlcrcstnaneNa. trobenzeneIscchorcr.s2-Nitro phenol a2 , 4-D i me t hv 1 p hen o 1Benzoic Acidbis ( 2-Chloroethoxy )methane_2 , 4-DichloroDhenol ai , 2, 4-Tric hi ore benzeneNaphthalene4— Chlorosni 1 ineHe xach lore-butadiene 34 -C h 1 o r o~3-me thv 1 phenol *2-Me t h v 1 na ph t ha 1 en eHexac h lorocycl open tad iene __ *2,4,6-Trichlorophenol *2,4, 5-Trichlorophenol2-Chloronaphthalene2— Ni troani 1 ineDimethyl phthalateAc en a ph thy Iene2, 6-D in i tro toluene3— Ni troani 1 ineAcenaphthene ^2,4-Dinitrophenol *4 — N i t r o p hen o 1 *

j

RRF

; 2 . 02Q

1.7901.591

lc 1.65?0.6S51.6091 . 3?41 . 5931.491

0 .6920.3510.715

C 0.2400 . 3500.2530.496

t 0.3550.3460.9730 . 502

i 0.195t 0 . 4321 . 039

* 0 . 296c 0.4450.4341 .2350.3561.3961.7660.3730.495

c 1.119* 0.185t 0.145

Ma

FRF50

_i • •_' / •_*•i ' —1.7831.6421.7210 . 8281 . 6561 . 40^2. S311.550i 1 ~*~*_.»•>„'/0.71 00.4710.7710.2320.3160 . 2390.4750 . 3370 .3431.11S0.4840.18S0.4041 .0760.1 SB0.463O.4971.3270.4311.4971.927O.3500 . 5071 - 3090.1550.153

;:D for

-17.0 )e; •«s.' • J.

0.4-3.2-3.7-20 . 9

-2.9-0 . 6

y 77 tr^-4 . 0

—20 .3 3

Cr^-2j-7.3

-T ~ )

9.75.54.2cr -f j

-0 . 6-14.33.63.6 i6.5 'A

-3.6

-5.2 31-2.7-7.4£35.1)

-7.2-9.16.2

-2.4-17.0 U

16.2 *-9.0 *

- cccc*> =. 25. o::

K

It

< . is-* 2_--2-l:

c

fc

cK

*I:

ctt

FORM VII SV-1 1/67 Rev

7CSEM:VOLATILE CONTINUING CALIBRATION CHECK 00368

^b Names IT C£==.:"r'____________ Contract: 63-01-7262 jj*PP

u*b Code: II____ Case Nc. : 10676 SAS No.: .______ SDG No.: CVE65

Instrument ID: GCMsr Calibration date: 11/16/88 Time: 1719

Lab File ID: BOCH-'2T2 Init. Calib. Datefs): 10/27 /£S 10/27/89

Min RRF50 for SPCC (£) = 0.050 Max %D for CCC(*) = 25.0/:

I COMPOUND

* Dibenzcf uran!2.4-DinitrctcluengSDiethylDhthelateI -Chlcrc-c-henyl-phenyl EtherI Fluorene! 4-Nit ream line1 -2-?6-Dinitro-2-methylphenol_• N— Nitrcsociphenylamine ( i ) _J! -*.— r r omc phen •/ 1 - p hen y 1 E t he r_1 K=;:achlcrobsnzeneJ Fen tach Ic re phenol• Phensnzhrene! Anthracene!Di-n-tutvl phthalateI FluorsntheneI Pyrene! Eutylbenzyl phthalate13,3' -Dichlorobensidine! Benzc- f a > anthracene! Chrysene! bis (2-Ethylhexyl )phthalate_j Di-n-octylphthalateI Benzo ( b> f luorantheneI Benzo C k ) fluoranthenei Benzo ( a) pyrene 5• IndenoC i .2.3— cd ) pyrene; Dibenz (a. h) anthracene! Eenzo(q , h, i ) psrylene.

! Ni trobenzene-d5!2-Fluorobiphenyl;Terphenvl-dl4I Phenol— d6I 2— Fluoro phenol! 2,4 ,6-Tribromoohenol!

RRF

1.7140 . 4971.3580.761

0 . 3420.147

K 0 . 4360 . 26-Z0,31 5

K 0.1°20.9310 . 9031.171

It 1.1851.0250 .5420.3200.9920..91S0.765

It 1.4351.4361.166

K 1.1360 . 9330.7 SO0 . 896

0 . 3631.2740.9401.7321.2790.336

RRF 50

1.7420.4561 . 5080.7421.451< \ ~*~i e* '.•.•_.-'0.133. * n -f e* ' . "T / w'

* > . 2280.2610.173o.?SlU.9SO1.4121.2311.0590 . 5860 . 32 S1.0551.0660.9111.6561 . 3521.1731.1351.0250.9771.012

0.3811.374O.S511.7471.2690.2S6

'/.D

-1.68.2

-11.1~> c

-9.75.09.52.3 ;13.017.19.9 ;-5.4-5.5-20 . 6-3.9—3 ~T.-3.1-2 . 5-6.4

-16.1-19.1-11.5 15.9-0 . 60.1 *

-9.9£2573)-13.0

-5.0-7.89.5-0.90.314.9


AR3007I5

£=:-i: CL-TILE CCNTI.MUliMG CAL IBF ATICN CHEi:-:. C 0 3 T 5

4feb Name: I r CH-- I".'; '____________ Con tract : ec— M~T262

L j Cede: 1~____ Cass Nc. : 106Te SAS No.: ______ SDG No.: CY565

Instrument ID: GC^5-' Calibration date: 11/19/9= Tims: Ife-t"?

Lab File ID: g.-.CE-'2~ Init. Oalib. Dats(s): 10/2"V3S 10/2^/93

r ir'CC * ' ** i — '-. * * 0

COMPOUND

PhenolDJ.= f 2-Chl -rcg-nvl ) E -her2-C h i c r c c- he- o 11 . 3-Dicr. 1 crater, zsne

tenrvl Alccnol'1 , "'-Di^-hl c ct"=r.zer.£.2-Mi_nhvion5riclt-5 i'2-Chloroisepre-pyl > Ethe— — I"'1! *=•£"'"' I o!-iS:",C 1N-r-'i -ro=--z--r.-crocvl£irrr.e 4H -=•••-= - -i 1 r- -- c •=• *• - - - ~NitrooenceneIscchcrone2-Nitrc.Dhenol :2, A-OI ,-j hv'' -r-nolSenrcic Acicbis (2-Chlcrsethox'y )methane_2 , 4— Die hi ore phenol1,2, 4-Triehlc-rc-benrsneMoc-nthalene4— Chlcroanil ireHexachlcrobutaciiene4-Chloro-3-me thvl phenol :2-Methvl noDhtha IeneHex «c hlorccycl open tad iene __ *2,4,6-Trichlcroohenol a2,4, 5-TrichloroDhenol2-Ch lor on aphtha Iene2-Ni troani 1 ineDimethyl oh thai ateAcenaphthylene2 , 6-Dinitro toluene3-Ni troani lineAcenaohthene a2, 4-Dini troDhenol 44-Ni trophenol -

RFF

t 2.02?1 . Sec1 . 7901.591

ic 1.6590.6851 ,60?1 . 3^41.5=31.^91

* 0.9-150.6920.3510.715

It 0.2400 . 3 5 00 .2530 .496

C 0.3550.3460.978O. 502

H 0.195It 0.4321 . 039

* O.296K O.4450.4841.235O.3561.3961 .7660.3730.495

C 1.119* O.185* 0.145

Ma:

RRF50

2.3751.9041.76S1.6-141.677-0.7321 . 63?1 . 3773 '"'A

1 .4611 .205O.o? 00.34"'0.7450.2020 . 3010.2330 . A 630 .3170.3341.1430.4710.1850 . 43">LOSS0.2110.4370 . 5001 . 3020.4341.4961.9100.3580.5611.3700.1530 . 1 52

r.D for

"ID

-17.1-1.01.2

—3 . 3-O.S-6.9-1.91.2

<r*-= .2 . 0

* --T'T c "'

C1 . 32.6

-4.215.814.07.?6 .7

10.73.5

-16.?A ^O . _.

5.10 . 0

-4.7

1.8 *—3. 3-5.4

-21.9-7.2-8.24.0

-13.3-22.4 *17.3 f-4.S *

!

cyst?

FORM VII SV-1 "iiuuu/ I S>87 Key

S£:i:vC_-7IL=: CCNT_Vu:.V3 C.-LIBF^T.CN CHECK 00376

-b Name: IT CE--"3S_____________ Ccr.tract: fc.= —M-^O-O

L Code: H____ Case No.: 10636 SAS No.: ______ SDG No.: CVS65

Instrument ID: GC^S- Calibration date: 11/13 "=g Time: 16-*7

Lab File ID: £rC£v2~T Init. Calif. Dateis): 10/2^/BS 10/27/95

Min RRF50 fcr SFCC(3j = 0.050 Max '/.D for CCCC*) = 25.OX

CGPFCUND

I>ibenzcf uran2 . 4-Dini trztz-lueneDie thv 1 p h tna late--Chlcrc-phenvl-phe-yl EtherFluorer.e•i- Ni trc-sni 1 in*- 5 6-D i n i t r c-2-me t hy 1 p hen o 1 __N-Nitrcscctichenyl a/nine ( 1 )_--Ercfficchenyl-phenyl Ether__

F -£••*; = !-. threner-ntr.r_.c*n*Di-n-butvl ent-a lateF 1 u,o rant ne ~ eFyrensBut v 1 be-izvl Dhtnalats3,3' — Dicr.IcrecsnzidineB*snzo i a ) an .hracsner^ w *— . / « — p- *-bis (2-Ethylh*:!y 1 ) phthalate__Di-n-cctvlpr, thai ateBenzo ( b ) f luoranthene5er.zo( k ) f lucrantheneBenzo C a i pyreneIndenoC 1 .2 . 3-cd ) pyreneDibenz ( a. h) anthraceneBenzo Cq . h . i ) pervlene

Nitrobenzene-d52— Fluorobi pheny 1Terc-henyl— di4Phenol-d6 • ;2— Fluorophenol2 « 4 ? 6— Tribromophenol

RF.F

1.7140 . °71.3530.7611 . 3230 . 3420.--1470 . 4S60 . 2620.315

. 0.1920.9310 .9031.171

k 1.1E51.0250 . 5420 .3200.9=20 .9180.765

*c 1.4851.4361.166

K 1.1360.9330 . 7EOO.S96

0.3631.274O .9401.7321.2790 . 336

RRF 50

1.S330 .5301.531, -. -f — c-*j . / •-' '1.3980.3110.1320.5010.2340 . 2o20 . 176i .oes1 . 027•i -"-. CJ. .-_'_. w1

1 . 20S0. 810.6120.3121.0131 .012O.S911.7311 . 3371.2711.1951.0920.9811 . 029

0.3691.4190.8431.7031.22S0.297

•/.D-6.9—6 .6-12.7

T* O

-5.79.110.2

10.7ic . SS . 3 '

-16.?_ 1 — •"•-13.2-i.?4.3

-12.9*-i c

-2.1-10.2-16.5-16.66.9-9.0— c r? '

-17,0< 2 5 -IT)-14-8

-1.7-11.410.31.74.011.6


AR3007I7

2CWSTER SEMI VOLATILE SURROGATE RECOVERY

0 0 ° ° 0Name: IT CESRTTQS._____________„ Contract: 68-01-7262 *" ~

Code: IT_____ Case Nc.: 10636 SAS No.: ______ SDG No.: CV865

! EFA! SAMPLE NO.

01ICYS6502JCYS6603ICY367O4JCYS6SO5JCYS69O6SCY370071CYS71081CYS65MS09ICY865MSD10JSBLK111ISBLK2

c •*c NB : ) a£2S?5*S47670S67876SSSO

S2CF=P)#

SO8594S7747778867790S7

S3(TPH)#

94ge

926?eiS7e?9465E296

S4( PHL ) #

f^B ——— St^ V » *^92

Cl02 T]SO767390

(5 02 *T9391S?

55(2FP)#

e?82

? 85746773S7S3SS7785

SoCTBP)^

105666741 •7947621001045994

OTHER TOTOUT

0300oC'Joo0

GC LIMITSSI (Nrl) = Nitroben=ene-d5 ( 35-114)S2 (FrF) = 2-F1uorobipheny1 ( 43-116)£3 (TPH) = Terphenyl ( 33-141)S4 (PHL) = Fhenol-d5 ( 10-94 )S5 (2FP) = 2-Fluorophenol ( 21-100)So C TEF•) = 2 ? 4 s6-Tribromophenol ( 10-123)

# Column tc be used to -flag recovery values* Values outside of contract required DC 1imitsD Surrooatss diluted out

AR3007J8page 1 of 1

FORM II SV-1 1/B7 Rev,

Ir EFA SAMFLE NC.SEMIVCLATILE CF.S^N.CS ANALYSIS DATA SHEET ________

Name: IT C£=="C£____________ Contract: 63-01-7262CYS65

Lab Cede: H_____ Case Nc.: 1067-6 SAS No.: ______ SDG No.: CV865

Matrix: (soil/wats-) bl&"= Lab Sample ID: CYS65

Sample wt/vcl: 1'X'O Cg/mL) CSL__ Lab File ID: 4SS70RK2

Level: (Icw/med) LCUJ Date Received:

•//"Moisture: not dec. ___ dec. ___ Date Extracted :(TI/09/SSJ

Extraction: (SepF/Ccr.t/Scnc > CONT Date Analyzed: (l 1/16/88 _)^*——__——x

GPC Cleanup: (Y/N) N__ pH: _____ Dilution Factor: 1•00

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) L'G/L Q

=105-? 5-2 ——————— FhEncl"111-44— i ——————— bis (2-Chl ores thvl ) Ether55-57-S ———————— 2-ChloroDhenol541-73-1 ——————— 1 . 7-Dichlcrobenrene106-46-" ——————— l . A-Dichlcrobenzsne100-51-6 ——————— =•-<-. = vl Alcohol95""50"~1— — — — * — — ' — 1 2— Dichlorobenzsne95-48-7 ———————— 2-MethvlDhenol108-60-1 ——————— tisf2-Chloroiscpropyl ) Ether_

- io_j-44-5 ——————— --Methvl phenol621-6-4—7 ——————— N— Nit roso-di-n — p ropy lamine __67-72-1 ———————— He : = c hi oroe thane9S-95-3 ———————— Nitrobenrene73—59-1 ————————— I = ophoroneSS-75-5 ———————— 2-Nrtrophenol105-67-9 ——————— 2 . A-Dimethvl ohenolo c— tJD u — _>&ri roic HCIO111-91-1 ——————— bis(2-Chloroethoxy)methane __120-33-2 ——————— 2.4-DichloroDhenol120-82-1 ——————— 1,2,4-Trichlorobenzene91-20-3 ———————— Naphthalene106-47-8 ——————— 4-Chloroaniline87-63-3 ———————— Hex schlorobu tad iene59-50-7 ———————— 4-Cnloro-3-methy iDhenol91-57-6 ————————— 2-Methyl naphthalen^77-47-4 ———————— He::achlorocycl open tad iene ___SS-06-2 ————————— 2.4.6-TrichloroDhenol95-95-4 ————————— 2 , 4 , 5-Tric hi oropheno 1.91-58-7 ————————— 2-ChloronaphthaleneSS-74-4 ———————— 2-Ni troani linel^i-li--' ——————— Dimethyl Dh thai ate20S-96-3 ——————— Acsnaoh thy Iene606-20-2 ——————— 2. 6-Dinitro toluene

10101010

. 1010101010101010101010IO5010IO10IO1010IO101010501050101010

1

:u!U:u!U!U!U:u!U!UiU:u:u!U;u!U:uIUJU:u;u:uiU!U:u:u:u!U:u;u!UJU;u:u*i

FORM I SV-1 1/37 Rev,

1C -. ..._ . EPA SAMPLE NC.SEM:VCL-T:LE CRSANICS ANALYSIS DATA SHEET

Name: IT Q£= = :*C.C_____________ Contract: 65-01-7262CYB65 0 0 £O :

Lab Cede: IT_____ Case No.: 106-76 SAS No.: ______ 'SDG No.: CY86*-

Matri::: (sell/water) l "= Lab Sample ID: CY865

Sample wt/vol: 1000 (g/mL) t*L Lab File ID: A8870RK2

Level: (low/mec1) LCUJ Date Received:

'/. Moisture: net dec. ___ dec. ____ Date Extracted:

Extraction: (SepF/Cont/Scnc) CSNT Date Analvred: QTl/16/66 J———— >•».••• • '• —_.......j/-

GFC Cleanup: (Y/N) N_ pH: ____ Dilution Factor: 1.00

CONCENTRATION UNITS:CAS NC, CCMFOUND (ug/L or ug/Kg) US/L G

99-09-2————————3-Nitroani 1 ir.e,£3-32-9————————Acsnsphthene__51—28 — 5———————2 , 4-Dini trochencl.100—02—7 ——— -——4—Nit re phen cl ____132—6-—9 ——————Dihenzof uran_____121-14-2———————2,4-Dinitrotoluenetr84-66-2————————Diethyl phthalate__________7005-72-3——————4-Chl or c-phenyl-pheny 1 Ether.S6-73-7————————Fluorene_________________100-01-6———————4-Ni troani linet534-52-1———————4 , 6-Dinitrc—2-methyl phenol.86-30-6————————N-Nitrosodipheny 1 ami He (1).101 -5 5-3———————4-Bromophenyl-pheny1 Ether.11S-74-1———————Kenachlorobenzene.87-86—5————————Pentachlorophencl.B 5-01—8————————Phenanthrene_____120-12-7———————Anthracene_______84-74-2————————Di-n-butylphthalate_206-44-0———————Fluoranthene________129-00-0———————Pyrene______________85-68-7————————Butyl benzyl phthalate.L-94-1————————3,3'-Dichlorobenridine

-Benzo(a)anthracene218-01-9———————Chrysene.

-Si-7———————bis(2-Ethylhe:cyl ) phthalate.-84-0———————Di-n-oc ty 1 pht ha 1 ate_______

205-99-2———————Benzo(b)fluoranthene.207-08-9———————Benzo ( k ) flue ran then e

-..•-£ — o- -Benzo( a) pvrene.193-39-5———————IndenoC 1,2, 3-cd ) pyrene.53-70-3————————Dibenr (a, h) anthracene

•Benrofg,h,i)perylene.

50 IU10 i U50 ! U50 ! U10 !U10 !U10 ' :u10 :u10 JU50 ! U50 ! U10 :uIO iU10 :u50 S U10 :u10 :u10 :u10 :u10 iu10 iu2O !U10 :u10 !U10 !U10 SU10 !U10 :uIO !U10 :u10 ;u10 !U

(1) - Cannot be- separated from Diphenylamine

FOFM I SV-2 ' "I- 7 Rev

IF EF'A SAMPLE NCSEMI VOLATILE CF.GAN1CS ANALYSIS DATA SHEET ______________


3 Name: IT CE=P.ITCS_____________ Contract: 65-01-7262CYS65

Lab Code: JT____ Case No,: 10636 SAS No.: ______ ' SDG No.: CYB65

Matrix: (soil/water) l*J£"= Lab Sample ID: CYS65

Sample wt/vol: 1000. (g/mL) tJL __ Lab File ID: AgS70RK2

Level: (low/med) LSd Date Received:

/'/Moisture: not dec. ___ dec. ___ Date Extracted:* ——— -

Extraction: (SepF/Ccnt/Scnc ) COMT Date Analyzed:

6FC Cleanup: (Y/N) N __ pH : ____ Dilution Factor: 1 . 00

CONCENTRATION UNITS:Number TICs found: _ 3^ (ug/L or ug/Kg) UG/L

CAS NUMPEF;

1.

iiCC-MPQUND NAME J RT

UNKNCWN 1 4.7Stt

EST. CDNC.

12

Q

J. 4.

FORM I SV-TIC flf?^nn79[ 87 Rev

'A EPA SAMPLE NCVOLATILE CR3ANZCS ANALYSIS DATA SHEET

i V8LK1 HO ISr,ab Name: IT CE=?R:TCS______________ Contract: 68-01-7252 |_______

Lab Cede: IT_____ Case Nc.: 1C636 SAS Nc. : ____ SDG No.: CY8S5

Matrix: (scil/water) WA*£R Lab Sample ID: VBLK1

Sample wt/vol: £ .0 (g/mL) P"L__ Lab File ID: LW5ECA06

Level: <1cw/mec} LC^ Date Received: ________

% Motsture: not dec. ____ Date Analyzed-: 10/20/8S

Column: (pack/cap) PACK Dilution Factor: _1. • 00

CONCEMTRATION UNITS:CAS NC. COMFCUN2 (ug/L or ug/Kg) UG/L Q

. . .

74-87-3——— ———— Chlcrcrnethane_______________ | 1 0 |U |74-8 3-S-————— —— c~cmomethar.e_____________ [ 1 0 j U j7 5-01-A ————————— V-:rwl Chloride_II_IIIII~~~™I| 1 0 IU I7 5-0 C-3 —— ————— ChTercethane_~"__III_I_I_ I 1C I u I75-OS-2 ————————— Merr.ylene Ch~crTce_"IIIIIIII! 3 ] J |67-64-1—————————Ace-one____________IIIIII_III . S | J75-15-0 —— —————— Carbon 5-; suTi i de_____________j " 5 JU75-35-4 ——————— 1 , l-D-ichlorcethene__________ j 5 j U75-34-3 ————————— 1 , 1-D-: chl oroethene___________ | 5 |U5iO-5£-C———————1 ,2-Dichl oncer hene (tctaT)__]_( 5 [U57-56-3 ——— ————— Chlcrcfonm________________ | 5 | U1 07-05-2 ——————— 1 , 2-Dichlonoer hane__________ j 5 [U78-93-3 ———————— 2-3utancne_______~.III.~_ I 1 ° iu7 1-55-6--———————1 , 1 , 1-Tr T ch 1 oroet ha'ne_______ j 5 j U55-23-5 — ——————— Carbon Tet rachl or T de_________ j 5 JU108-05-4————————Vinyl Acetate_______I_II_I_ I 10 \V75-27-4 — ——————— Sromodichl oromethane________ j 5 | U78-87-5 ———— ————— 1 , 2-Dichloropropane________ j 5 j U10061-0 1-5—————cis-1 , 3-Di chl oropropene_____ | 579-0 1-6 ———————— Trie hi oroethene____________ j 51 24-48-1 —————— — Dibromochl oromethane________ j 579-00-5———————— 1 , 1 , 2-Trichloroethane_______ j 571-43-2 ———————— Benzene_____________________ j 510061 -02-6 —————— trans- 1 , 3-D i chl oropropene___ j 575-25-2 ————————— Bromof orm______________,_____ j 5108-10-1———— ——— 4-Nethyl-2-Pentanone_________ | 1 0591-78-6 ———————— 2-Hexanone___________IIII.I_ I 10127-1 8-4. ——————— Tet rachl oroethene___________ j 579-34-5- ———— ——1 , 1 ,2, 2-Tet rachl or cet hane___ j 5108-88-3 ———————— Toluene__________________IIII I 11 08-90-7- ——— ——Chlorobenzene____________ j 5100-41-4--- ————— Ethyl benzene^_______________ | 5100-42-5———————Styrene____I_II_I_IHIIIIII I 51330-20-7——————Xylenes" Total )______I___I_ | 5

FORM I VGA ftR 300722 " ~ ' ry-wi? Rev

Name: IT CE = =:T7.'= ________ Contract: 65-01-7262

£=A SAMPLE NC .

SSLK1

Lab Cede: IT_____ Css~ NC.: 10cT6 SAS No.: ______ SDG No.: CY865

Ma t-i •: f 5 = il/wfft=^> U'-"= L = b Sample ID: EeLKl____

Sample w.'-vol: .,•:*:••: CC -uL) f_L __ Lab File ID: ASS70K22

L*vel: ilow/med) LC'.-i Date Received: _______

tur*: net cec . ___ c*c. ____ Date E;:tract*d: 10/16/S3

Extraction : (£e-5F'Ccn-/ = ..nci CCMT Date Ana ly red: 11/06/53

GFC Cleanup: (Y/N; rj __ pH: _____ Dilution Factor: 1 - CO

CONCENTRATION UNITS:CAS NO. Crr-.POL'NO (ug/L or ug/Kg) L'G/L Q

-i|>f%5_c = _2 ——— — — F h-nc 1-Hl-ia-J. ——————— tisi^-CMc-r-e-hyl ) Etherc f.-57-s ————————— Z-CMc-ro-.t-encl

^5-- 1 -7C- 1 ——————— i .3-3ic!-.lcrcDenzEnej_t%^_. _^ £,— 7*— — — — — — — — • si__.ni n^l'^rcb^nz^-ns100-Sl-o ——————— Bsnzvl AlcoholC5-5O-1 ———————— 1 .2-I-ich lore benzenecf=t— 49— "7— ——————— ""'— Cite~hvl pheno 110S-60-1 ——————— bis (2-Chlorcisc-propy 1 ) Ether_1,06-4-1-3 ——————— -Methvlchenol621-6-1—7 ——————— N— Ni r rose— di-n — D ropy laminamm ""^ __ "™ '^ _ . « . , , _. . • ; r- - l —— *— 1 —— If- —— —— -*-1— -1—— "C ,' "~ , *."*-, . .£ ; =r.t_ : i 1 wr Uitr •_ i tc-ri-?

c 'c— ° 5— 3 ———————— — Nitrz benzene7£_«io_i —_-:->,-, horon^-£2— 7 5™- 5 ——— — — — 2— Ni tro pheno 1105-67-9 ——————— 2.4-DimethvlDhenol65-95-0 ———————— renzoic Acid111-91-1 ——————— his(2-Chlorowthcn:y)methane __120-B3-2 ——————— 2»4-DichloroDhenol120-82-1 ——————— 1.2.4-Trichlorobenzeneci-20-3 ———————— Naohthal ene106-47-S ——————— 4-Chloroanil ine87-63— 3 ———————— Hexachlorobutadiene59-50-7 ———————— 4-Ch 1 or o-3-me t hy 1 p heno 191-57-6 ———————— 2-Methyl naphthalene77—47—4 ———————— Hei-;auhlorocycl open tad iene ___88-06-2 ———————— 2.4.6-Trichlorophenol95-95-4 ———————— "*,4.5-TrichloroDhenol

= 91-53-7 ———————— 2-ChloronaDhthsleneS3-74-4 ———————— 2-Nitroanil ine131-11-3 ——————— Dimethylohthalate20S-96-3 ——————— Acenaohth-ylene606-20-2 ——————— 2 , 6-Din i tro to 1 uene

1010101010101010101010101010101050101010101010101010IO5O10501010IO

t1!UJU!U!U!U;u;u!U!U!U!USU!UiU:u!U:uJU!U!U:u:u:uiU!U;u!U!U!U!U:u!U!Ut1

FORM I SV-1 ' '67 RevHR300723

r S B L H 1•; Name: IT CE=- t"1.______________ Ccntract: 6c-01-7262 00405

Lab Ccds: !T____ Co = = Nc . : IvcTc SAS No.: ______ SDG No.: CYB6"

M a t r i::: tsoil/water) U~."= - ™" "™ L —:,-—|_sb Sample ID: ScLk'l____

Sample wt/vol: i•>:••. (o/mL) !HL__ Lab File ID: Agg7C^22

Level: •; lew-'mec ) L'"'••' Date Received: _______

"/. Moisture: no:. <_•=•<_. ___ u*=c. ___ Dare Extracted: 1O/16/SS

Extraction: (SecF -'Cc-n - ' Scnc) C2MT Date Analyzed.: 11/06/SE

Gr C Cleanup: i. Y/Nj N____ pi-l: _____ Dilution Factor: 1 .00____

CONCENTRATION UNITS:CAS NC. CDMPCUMD (ug/L or ug/Kg) US/L Q

.-.- (V? -.•--- — ' c51—28—5 — —100—02—""— —

i'. ,1 ' v .— \Q -..—— ,= —— _^—— —— ——

7005—72—3—

r* — - •

11S-74-1 ——£7-36-5 ———Se _ f-\1 _ C _ _ __' V X w

120-12-7 —S4-74-2 ———

129-OO-0 —C^ AO— 7

" 213-01-9 —11 ** _., • "T1 / Oi /

1 1 / — b4 U

50-32-8 ———1 7 -J« •-• 7 C»

191-24-2 —

--- —— 7 -Nit roan i line

—————— 1 . 4-Dini troc-henc 1——— — ^-Nitroc-r.e'-ic.l—— —— r.^tjsnzo^uran—— —— 2, -i-Dinitrotol uene_ _ _ _ _ _ r\ •> s H h v 1 p h *" h <r 1 n " =

—————— -L-ChiorcDneny 1 -pheny 1 Ether __————— F 1 u c r e n e—— — ---Nitroaniline— ——— — — -'• 4 ~ — Di n i t r c *"2~~iT;t= t hv 1 pheno 1————— N-Nitrc-.cdi z-henv lamine ( 1)————— -i-S r oiTio D hen v .1 - p hen v 1 Ether__ —— -r->xachlcro benzene__ — — Pen tach loro phenol- ———— Phenanthrene- —— --Anthracene————— Di-n-buty 1 phthalate————— Fluoranthene—— —— Pyrene————— Butyl benzvlph thai ate————— 3 .3'— Dichlorobenzidine————— Senzo( a) anthracene

— _. —— bis(2-Ethylhexyl ) phthalate __————— Di-n— octvl phthalate————— Benzo ( b) f luoranthene————— Benzof k ) fluoranthene————— Benzo (a)pyrene————— Indeno (1,2, 3— cd ) pyrene————— Dibenz ( a . h) an thracene—————— Benzo ( a . h, i ) perylene

5010505O10101010105O50101C105010IOIO1010IO20IOIO1010101010101010

1t

:u!UIU:u:u!UJU!UIUIU:u!U:uIUIUIUIU:u!U:u;uIU!UIU:uIU:uIUIUIUIU:u


FORM I SV-2 AR30072-U- - X/S7 Rev

lir EPA SAMPLE NCc to»—" t—— - ~ 3r-r* i „— r-NAL vs i c _. A i A SHEET

Name: IT CH=rTTi=_____________ Contract: 68-01-7262S5LK2

L&b Ccds: H_____ C* = e Nc. : 10676 SAS No.: ______ SDG No.: CYS6

Matrix: (_•::_. l/w*t»*-} &-"= Lab Sample ID: S5LK2

Sampls wt. vci: 1000 Cg-'-.L) ML Lab File ID: gS70RK'l

Level: ( lcw/«Ti=-2 ; LC^J Date Received: _______

% Mciatura: net d*c . ___ dec. ____ Date Extracted: ll/0Q/Sc

Extraction: ( SepF ./Ccnt/Scnc ) CCNT Date Analyzed: 11/16/BB

GP'C Clea-nuc: CY/r-J." N __ pH: _____ Dilution Factor: 1 . 00

CONCENTRATION UNITS:CAS NO. COMPOUND <ug/L or ug/Kg) L'G/L D

1 OS-*? 5-2 ——————— Fher.cl111----- ——————— ti- i2-Chlorcethv 1 ) Ethtrr->c e: -T r .— •"• i" 'k-i— «--- r- ,- ,-. ,— 1^ ta« .? ' c _ _ n _ i_- r c D n — n o iC A 1 — — * _ * — _n -i — '-1 — *-— *- i— — -r-c-W * 1 / •-* — — _. « --- V — U : i 1 '_• I L. L.' t: : l - r ~. s;

lOc-^6-7 ——————— 1 , 4-D^ chlorcbenzene100-51-6 ——————— E?enzvl Alcohcl95-50-1 ———————— 1,2-DichlorCibenzene95--B-7 ———————— 2-Methyl phenol

; 10S-60-1 ——————— bis (2-Chlorcisc.propyl ) Ether_106-44-5 ——————— -2— Methyl phenol621-t4-7 ——————— rJ-Mitroso-di-n-propvlamine67— / *J— 1 — He'CffChlorcethane93— 05—— ————————— Nit re benzene/ C5~ V — i — — I SuphorufTig68-75-5 ———————— -Nitre-phenol105-67-9 ——————— 2, 4-Dimethyl phenol65-S5-0 ———————— Benzoic Ac id111-91-1 ——————— bis £2-Chl oroe thoxy) me thane __120-83-2 ——————— 2,4-Dichlorophenol120-82-1 ——————— 1,2,4-Trichlorobenzeneo i — r>(i_— ——————. — — MAnh'hha 1 =np/ J. _. '»• •— i' txd^fi i ul 'V\ i L_ I 1 w

106-47-S ——————— 4-Chloroaniline87-6S-3 ———————— Hex&c h 1 orobu tad i ene59-50-7 ———————— 4-Chloro-3-methvl Phenol91-57-6 ———————— 2-Methyl naphtha Iene77—47—4 ———————— Hexach 1 or ocycl open tad iene ___83-06-2 ———————— 2,4,6-Trichlorophenol95-95-4 ———————— 2,4,5-Trichlorcphenol91-58-7 ———————— 2-Chloronaph thai eneQS-74_4 ———————— 2-Mi troani line131-11-3 ——————— Dimethyl phthalate203-96-8 ——————— Acenaoh thy Iene606-2O-2 ——————— 2, 6-Dinitro toluene

•1010"IO* '"lJ. .'1010101010IO1010101010105010101010101010IO101C)501050101010

1tIUIU!UJU:uIU!UIUIU!UIUsuI LlIUtuIUIU!UIU!UIUIDIU!U:u!U:u!U!UIU:uIUIU11

FORM I SV-1 AR300725

'. I ErA SAMFL£ NC .

Name: I" CE=c:~Cz _________ Contract: 68-01-7262SBLK2 " V

-ab Code: U_____ Case No.: 106T6 SAS No.: ______ SDG No.: CY965

latri::: (scil/'water i a^"= Lao Sample ID: SBLK'2____

Sample wr/vol: l.CC (c • mL) ML .._ Lab File ID: -&S STORK!

.svel : ( Icw/mec!) LOW__ Date Received: _______

'•: Moisture: no- <i*c . ___ dec. ___ Date Extracted: 11/0°/B£

Extraction: (SepF/Cc-r. t/Sonc J C~NT Date Analyzed: 11 /16/BS

3r*C Cle ni.'.:?: sY'N; N pH: ____ Dilution Factor: 1.00

CONCENTRATION UNITS:CAS NC. Cir.FQL'ND (ug/L or ug/Kg) Ug/L Q

99-09-2 — —————~-Ni trcan i 1 ine

100-02-7————————--Mi trophenol ___

121-1--2———————2,4-DinitrotDlLiene.S^-66-2————————Diethvlphthalate7005-72-3——————4-Chl or ophenyl-pheny 1 Ether,•S6-73-7————————Finer ens___________________100-01-6———————4-Nitrosniline_____________534-52-1 ——————— 4 ,, 6-Dini tro-2-msthy 1 phenol_£6-30-6--——————N-Ni trosodi pheny 1 amine (1) _

•—3———————4—Bromo pheny 1—pheny 1 Ether_US-74-1———————He x ac h 1 or o benzene__________J. '.'-,

-Pen tach lor ophenol.85—01 — 3—————————Phenan threne__________120-12-7———————Anthracene____________Q4-74-2————————Di-n-butyl phthalate___206-44-0———————Fluoranthene__________129-OO—0———————Pyrene________________S5-63-7————————Butylbenzylphth&late__91-94-1————————3,3* -Dichlorobenzidine

•Benzo (a) anthracene.-Chrysene__________

117-31-7———————bis (2-E thy Ihexyl) phthalate.117-84-0———————Di-n-octyl phthalate_______

_2———————Benzot b ) f luoranthene^-9———————&enzo( I:) fluoranthene

50-32-3————————Benzo(a) pyrene________193-3^-5--—————Indeno(1,2,3-cd)pyrene.53-70-3————————Dibenz ( a, h) anthracene^191-24-2———————&enzo( g , h ? i ) pery Iene__

50 1U10 IU50 JU50 ! U10 J U10 JU10 JU10 JU10 !U50 J U50 J U10 JU10 !U10 JU50 J U10 IUIO JU10 IU10 :u10 !U10 iU20 IUIO .IU10 "su10 IU10 IU10 IU10 iU10 JU10 JU10 ID10 !U

(1) - Cannot be separated from Dipheny1amine

AR3007261/B7 Rev

USE UNtT.ED STATES ENVIRONMENTAL PROTECTION AGENCY · THROUGH: ^Charles Matkovich * ESAT Team...

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Transcript of USE UNtT.ED STATES ENVIRONMENTAL PROTECTION AGENCY · THROUGH: ^Charles Matkovich * ESAT Team...