UNDtROROUND ENCINEFRING & ENVIRONMENTAL SOLUTIONS · (0 026 milligrams per liter) in the composite...
Transcript of UNDtROROUND ENCINEFRING & ENVIRONMENTAL SOLUTIONS · (0 026 milligrams per liter) in the composite...
H A I I Y & :ALDKICII
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10 October 2003File No 29213020
US Environmental Protection Agency Region VIISuperrund Division901 North 5th StreetKansas City Kansas 66101
Attention Ms Mary Peterson
Subject September 2003 Monthly Progress ReportChemical Commodities Inc Olathe Kansas
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Dear Ms Peterson
The September 2003 Monthly Progress Report presents an update of Remedial Investigation(RI) and Feasibility Study (FS) activities conducted at the Chemical Commodities Inc site inOlathe Kansas This report has been prepared pursuant to Section XIV Docket NoCERCLA 7 2000-019
Table 1 specifies the work performed and any problems encountered analytical data receivedduring the reporting period and the developments anticipated during the next reportingperiod including a schedule of actions to be performed anticipated problems and plannedresolutions of past or anticipated problems Table 2 provides water quality data collectedduring groundwater sampling of newly installed bedrock wells and surface water sampling atMill Creek Table 3 summarizes constituents detected in the bedrock assessment groundwatersamples collected from newly installed bedrock wells Copies of the analytical data receivedduring September 2003 are provided as Attachment A Figure 1 identifies the bedrockassessment groundwater sampling locations and Mill Creek sediment and surface watersampling locations
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SUPERFUND RECORDS
RECEIVED
OC1 14 2lWSUPCKFUND DIVISION
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US Environmental Protection Agency Region VII
1 10 October 2003Page 2
Please call Brian Mossman (818 586 6015) or me (913 599 5802) if you have any questionsregarding this progress report
Sincerely yoursHAI EY & ALDRICH INC
Michael D Basel Ph D P EVice President
EnclosuresTable 1 - September 2003 Monthly Progress ReportTable 2 - Water Quality in Bedrock Assessment Groundwater and Mill Creek
Surface WaterTable 3 - Summary of Bedrock Assessment Groundwater Analytical ResultsFigure 1 - Phase II Bedrock Assessment Sampling LocationsAttachment A - Copies of Laboratory Analytical Reports
cc The Boeing Company Attn Brian MossmanKansas Department of Health and Environment Attn Rob WeberGeoSyntec Consultants Attn Mark Schultheis
TABLE 1SEPTEMBER 2003, MONTHLY PROGRESS REPORT
CHEMICAL COMMODITIES, INC SITE, OLATHE, KANSAS
ITEM TO BE ADDRESSED ACCORDING TO SECTION XTV of DOCKET No CERCLA-7-2000-019
Work Performed During Reporting Period and Any Problems Encountered
Remedial Investigation / Feasibility Study (RI/FS) activities conducted during the reporting period includeResponse to Kansas Department of Health and Environment s comments regarding the Phase n Bedrock Assessment (letter dated 3 September2003) was submitted to the U S Environmental Protection Agency (EPA) on 9 September 2003 Verbal approval of these responses werereceived by Mary Peterson in a phone conversation on 10 September 2003 so installation of the final Phase n bedrock well could proceed
Notification of Potassium Permanganate Pilot Testing being conducted by University of Waterloo The Boeing Company and Haley &Aldrich Inc was provided to the EPA on 5 September 2003Additional characterization of the bedrock was conducted from September 8 through September 18 2003 per the Phase II Bedrock AssessmentWorkplan (Haley & Aldnch Inc 23 June 2003) The field event included the following activities• Installation and development of seven bedrock monitoring wells (MW-22B MW-23B MW 26C MW-30B MW-31B MW-32B and MW
33B) Locations are shown m Figure 1 One planned bedrock well (MW-31C) was not installed because bedrock and the contact to theEudora Shale were encountered much shallower than expected while drilling at MW-31B (Figure 1)
• Slug testing on five of the seven newly installed bedrock wells MW-30B was dry after well completion and MW-26C could not be testeddue to extremely slow recovery
• Collection of groundwater samples for VOC analysis from five of the seven newly installed bedrock wells (MW-30B was dry and MW-26Ccould not be sampled due to slow recovery) and one prrvate unused well (Figure 1) Water quality parameters (pH temperature andconductivity) were measured during sampling and are provided in Table 2
• Collection of surface water and sediment samples from Mill Creek for VOC analysis Four surface water samples (MC001 throughMC004) and three sediment samples (MC001 MC002 and MC004 no sample collected from MC003 because Mill Creek has a concretebed at this location) were collected at locations shown in Figure 1 Water quality parameters were measured during sampling and areprovided in Table 2
• Collection of soil samples from drill cuttings from bedrock well installation Sample results will be used for profiling prior to disposal
Page 1 of 2 2003-09 CCI MPR Table I xls
TABLE 1SEPTEMBER 2003, MONTHLY PROGRESS REPORT
CHEMICAL COMMODITIES, INC SITE, OLATHE, KANSAS
ITEM TO BE ADDRESSED ACCORDING TO SECTION XTV of DOCKET No CERCLA-7-20CKMH9
Analytical Data Received During Reporting Penod
Analytical data received from the laboratory during the September reporting penod have been summarized as follows (copies of laboratory data areprovided as Attachment A)
Groundwater samples from five newly installed bedrock wells and one private unused well Detections are summarized in Table 3Sediment and surface water samples from Mill Creek No detectable concentrations were found in the Mill Creek sediment or surface watersamples with the exception of acetone (3 3 J [estimated value] micrograms per liter) in surface water at location MC001Soil samples from drill cuttings No detectable concentrations were found in the drill cuttings samples with the exception of trichloroethene(0 026 milligrams per liter) in the composite sample from MW-26C drill cuttings
Developments Anticipated During the Next Reporting Penod Including Schedule of Actions to be Performed, AnticipatedProblems, and Planned Resolutions of Past or Anticipated Problems_______________________________
Haley & Aldrich Inc will conduct a comprehensive round of groundwater sampling per the Phase II Bedrock Assessment Workplan (Haley &Aldnch Inc 23 June 2003)
Page 2 of2 2003-09 CCI MPR Table 1 xls
Table 2Water Quality in Bedrock Assessment Groundwater and Mill Creek Surface Water
Chemical Commodities, Inc SiteOlathe, Kansas
MonitoringLocation
GroundwaterPrivate Unused Welf
MW22BMW23BMW26Cb
MW30BC
MW31BMW32BMW33B
Mill Creek Surface WaterMC001MC002MC003MC004
MonitoringDate
9/9/039/17/039/17/03
NMNM
9/9/039/12/039/12/03
9/10/039/9/039/9/039/9/03
Conductivity(umho/cm)
630822635NMNM813880820
780620550520
pH
7376178NMNM797476
8 1799 799
Temperature(degrees C)
2323523
NMNM202120
22243028
" Private Unused Well is an inactive agricultural well located on property at 505 E Cedarb Groundwater recovery is extremely slow at MW 26C sample has not yet been collected at this locationc MW 30B was a dry after well installation no sample collected
degrees C degrees CelsiusNM Not measuredumho/cm micromhos per centimeter
Table 3Summary of Bedrock Assessment Groundwater Analytical Results
Chemical Commodities Inc SiteOlathe Kansas
MonitoringLocation
Private Unused Well d
MW22BMW23BMW26Cb
MW30BC
MW31BMW32BMW 32B (DUP)MW33B
DateSampled
9/9/20039/17/039/17/03
9/9/20039/12/039/12/039/12/03
Volatile Organic Compounds Results (jig/L) 'Acetone
39J<10<10NSNS<10<10<10<10
Carbon Disulfide
<10068J<10NSNS
<10<10<10<10
cis-1 2-Dichloroethene
047J<10<1 0NSNS
<10<10<10<10
Chloroform
<10<10<10NSNS
<10056J057J<10
2 Butanone
3 7 J<50<50NSNS
<50<50<50<50
Tnchloroethene
52<10<1 0NSNS
<10<10<10<10
Tetrachloroethene
082J<10<10NSNS
<10<10<10<10
a Only analytes detected above the reporting limit are provided in mis tableb Groundwater recovery is extremely slow at MW 26C sample has not yet been collected at this locationc MW 30B was a dry well no sample collectedd Private Unused Well is an inactive agncultural well located on property at 505 E Cedar
jtg/L micrograms per literDUP duplicateJ estimated result result is less than reporting limitNS not sampled
cn•<*•men03CM
oogo
ItoCMCDCM
oo
(JO
'215000 N
«o4.MW31B i^ MW-31C(N<rt Installed)
__ A HILL CSEQCdUng »o UM Cr-K
BASE MAP MOD'FIED FROM MONTGOMERY WATSON HARZA AUGUST 2001G \GRAPH1CS\PROJECTS\CCI\2B954B35 DWG
MC001LEGEND
MW 23B •» BEDROCK MONITORING WELL
® MONrTORING WELL
• SURFACE WATER & SEDIMENT SAMPLE
T GAGE STATION
TR1CHLOROETHYLENE CONCENTRATION (ug/L)DUPLICATE SAMPLES
300
SCALE IN FEET
600
HALEY&ALDRICHCHEMICAL COMMODITIES, INCOLATHE KANSAS
PHASE II BEDROCK ASSESSMENTSAMPLING LOCATIONS
SCALE AS SHOWN OCTOBER 2003
FIGURE 1
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ATTACHMENT A
Copies of Laboratory Analytical Reports
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ANALYTICAL REPORT
Boeing/CCI Olathe KS
Lot # E31100190
Haley & Aldrich Inc
SEVERN TRENT LABORATORIES INC
Diane SuzukiProject Manager
September 16 2003
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EXECUTIVE SUMMARY - Detection HighlightsE3I100190
REPORTING ANAL YTICALPARAMETER RESULT LIMIT UNITS METHOD
BOHL_WG090903_0001 09/09/03 10 10 001
Acetone 3 9 J 10 ug/L SW846 8260Bcis-1 2 Dichloroethene 0 47 J 10 ug/L SW846 8260B2 Butanone 3 7 J 50 ug/L SW846 8260BTrichloroethene 52 10 ug/L SW846 8260BTetrachloroethene 0 82 J 10 ug/L SW846 8260B
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METHODS SUMMARY631100190
PARAMETERANALYTICALMETHOD
Volatile Organics by GC/MSVolatile Organics by GC/MS
Reference s
SW846 8260BSW846 8260B
PREPARATI ONMETHOD_______
SW846 5030SW846 5030B/826
SW846 Test Methods for Evaluating Solid Waste Physical/ChemicalMethods Third Edition November 1986 and its updates
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SAMPLE SUMMARYE3I100190
SAMPLED SAMPWO # SAMPLED CLIENT SAMPLE ID________________________________________ DATE TIME
FX06JFX064FX07AFX07KFX07MFX07WFX079
NOTE(S)
001002003004005006007
BOHL_MC002MC003MC004
WG09090_WS0909_WS0909_WS0909
MW31B_WG0909MC002MC004
_STS090_STS090
3_000103_03_03_03_903903
0001000100010001_0001_0001
09/09/0309/09/0309/09/0309/09/0309/09/0309/09/0309/09/03
10111314151114
10252030302030
The analytical results of the samples listed above are presented on the following pagesAll calculations are performed before rounding to avoid round off errors in calculated resultsResults noted as ND were not detected at or above the stated limitThis report must not be reproduced except in full without the written approval of the laboratoryResults for the following parameters are never reported on a dry weight basis color corrosivily density flashpoint Igmtability layers odorpaint filter lest pH porosity pressure reactivity redox potential specific gravity spot tests solids solubility temperature viscosity and weight
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HALEY SL ALDRICH INC
Client Sample ID BOHL_WGO90903_0001
GC/MS Volatiles
Lot-Sample #Date Sampled
E31100190 001 Work Order f09/09/03 10 10 Date Recea.'wed
FX06J1AA BBattraa:09/10/03 10 00 MB Hfflum
Prep Date 09/10/03Prep Batch # 3254454Dilution Factor 1Analyst ID 004648
PARAMETERDlchlorodlfluoromethaneChloromethaneChloroethaneBromometh aneTrichloro f luoromethane112 Tnchlorotnf luoro
ethane1 1 DichloroetheneMethylene chlorideMethyl tert -butyl etherCarbon disulfideAcetonetrans 1 2 Dichloroethene1 1 Dichl oroethane2 2 Dichl oropropanecis-1 2 -DichloroetheneChloroformBromochlo romethane111 Tri chloroethane2-Butanone1 1 Dichl oropropeneCarbon te trachlonde1 2 DibromoethaneBenzeneTrichloro ethene1 2 Dichl oropropaneBromodich loromethaneDibromome thane4 Methyl 2 pentanoneToluene1 1 2 -Tri chloroethane1 2 -Dichl oroethaneTetrachlo roethene2 HexanoneDlbromoch loromethaneChloroben zene1 1 1 2 Tetrachloroethane
Analysis matteAnalysis Tmme
Instrument IDMethod
RESULTNDNDNDNDNDND
NDNDNDND3 9 JNDNDND0 47 JNDNDND3 7 JNDNDNDND5 2NDNDNDNDNDNDND0 82 JNDNDNDND
09/10/0319 06
MSHSW846 826
REPORTINGLIMIT1 02 02 02 02 01 0
1 01 01 01 010)1 01 01 01 a>1 01 01 05 CD1 00 501 01 01 CD1 01 01 05 01 01 00 501 CD5 01 01 01 0
OB
UNITSug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
(Continued on next page)
MDL0 400 300 301 00 300 40
0 300 300 500 303 00 300 200 300 300 300 300 203 00 300 300 300 300 300 300 300 403 00 300 300 400 303 00 400 300 30
WATER3254202
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Client Sample ID BOHL_WGO90903_0001
GC/MS Volatiles
Lot-Sample # E3I100190 001 Work Order # FX06J1AA Matrix
j Estimated result Result is less than RL
WATER
PARAMETEREthylbenzeneVinyl chlorideXylenes (total)StyreneBromoformI sopropyl benzene1 1 2 2 Tetrachloroethane123 Tri chloropropanen PropylbenzeneBromobenz ene135 Tnmethylbenzene2 Chlorotoluene4 Chlorotoluenetert Butylbenzene124 Trimethylbenzenesec Butylbenzenep Isopropyltoluene1 3 Dichlorobenzene1 4 Dichlorobenzenen Butylbenzene1 2 Dichlorobenzene1 2 Dibromo 3 chloro
propane124 Tri chloro
benzeneHexachlor obutadieneNaphthalene1 2 3 -Tri chlorobenzeneAcroleinAcrylonitrilelodomethane2 Chloroethyl vinyl etherTetrahydrofuranVinyl acetate
SURROGATEBromof luo robenzene1 2 Dichloroethane d4Toluene d8
NOTE(S)
RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
ND
NDNDNDNDNDNDNDNDND
PERCENTRECOVERY10091108
REPORTINGLIMIT1 00 501 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 02 0
1 0
1 01 01 020202 05 0105 0
RECOVERYLIMITS(75 130)(65 135)(80 130)
UNITSug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
ug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
MDL0 200 300 800 300 300 300 400 400 400 300 200 300 300 200 300 300 300 300 300 300 300 70
0 30
0 300 500 4012101 02 02 02 0
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Client Sample ID MC002_WS 090903_0001
GC/MS Volatiles
Lot-Sample # E3I100190 -002Date Sampled 09/09/03 11 25Prep Date 09/10/03Prep Batch # 3254454Dilution Factor 1Analyst ID 004648
PARAMETERDichlorod if luorome thaneChloromet haneChloroethaneBromomethaneTrichloro f luorome thane112 Trichlorotrifluoro
ethane1 1 DichloroetheneMethylene chlorideMethyl tert butyl etherCarbon disulfideAcetonetrans 1 2 -Dichloroethene1 1 Dichloroethane2 2 Dichloropropanecis 1 2 DichloroetheneChloroformBromochlo romethane111 Tri chloroethane2-Butanone1 1 Dichl oropropeneCarbon te trachlonde1 2 DibromoethaneBenzeneTrichloro ethene1 2 DichloropropaneBromodich loromethaneDibromome thane4 -Methyl 2 pentanoneToluene112 Tri chloroethane1 2 DichloroethaneTet rachlo roe thene2 HexanoneDlbromoch loromethaneChloroben zene1 1 1 2 Tetrachloroethane
Work Order tDate ReceivedAnalysis mateAnalysis TTmme
Instrument IDMethod
RESULTNDNDNDNDNDND
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
FX0641AA09/10/0309/10/0319 36
MSHSW846 826
REPORTINGLIMIT1 02 02 02 02 01 0
1 01 01 01 0101 01 01 01 01 01 01 05 01 00 501 01 01 01 01 01 05 01 01 00 501 05 01 01 01 0
Wattn10 00 MS Bo
OB
UNITSug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
ix WATERam f 325421
MDL0 400 300 301 00 300 40
0 300 300 500 303 00 300 200 300 300 300 300 203 00 300 300 300 300 300 300 300 403 00 300 300 400 303 00 400 300 30
(Continued on next page)
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Client Sample ID MC002_WS 090903_0001
GC/MS Volatiles
Lot-Sample # E3I100190-002 Work Order FX0641AA Matrix WATER
PARAMETEREthylbenzeneVinyl chlorideXylenes (total)StyreneBromoformI sopropyl benzene1 1 2 2 T etrachloroethane123 Tri chloropropanen-PropylbenzeneBromobenz ene135 Trimethylbenzene2 Chlorotoluene4 Chlorotoluenetert Butylbenzene124 Trimethylbenzenesec-Butyl benzenep Isopropyltoluene1 3 -Dichl orobenzene1 4 Dichl orobenzenen Butylbenzene1 2 Dichl orobenzene1 2 Dibromo 3 chloro
propane124 Tri chloro
benzeneHexachlorobutadleneNaphthalene123 Tri chlorobenzeneAcroleinAcrylonitrilelodomethane2 Chloroethyl vinyl etherTetrahydr of uranVinyl acetate
SURROGATEBromofluorobenzene1 2 Dichl oroethane d4Toluene d8
RESULTKDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
ND
NDNDNDNDNDNDNDNDND
PERCENTRECOVERY10090109
REPORTINGLIMIT1 00 501 01 01 01 0\ 01 01 01 01 01 01 01 01 01 01 01 01 0I 01 02 0
1 0
1 01 01 020202 05 0105 0
RECOVERYLIMITS(75 130)(65 135)(80 130)
UNITSug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
ug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
MDL0 200 300 800 300 300 300 400 400 400 300 200 300 300 200 300 300 300 300 300 300 300 70
0 30
0 300 500 401210I 02 02 02 0
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Client Sample ID MC003_WS 090903_0001
GC/MS Volatiles
Lot-Sample # E3I100190 -003Date Sampled 09/09/03 13 20Prep Date 09/10/03Prep Batch # 3254454Dilution Factor 1Analyst ID 004648
PARAMETERDichlorod if luoromethaneChloromet haneChloroe thaneBromometh aneTrichloro f luoromethane112 Trichlorotrifluoro
ethane1 1 Dichl oroetheneMethylene chlorideMethyl tert butyl etherCarbon disulfideAcetonetrans-1 2 Dichloroethene1 1 Dichl oroethane2 2 Dichl oropropanecis 1 2 DichloroetheneChloroformBromochlo romethane111 Tri chloroethane2 But anon e1 1 Dichl oropropeneCarbon te trachloride1 2 DibromoethaneBenzeneTrichloro ethene1 2 Dichl oropropaneBromodich loromethaneDibromome thane4 Methyl 2 pentanoneToluene112 Tri chloroethane1 2 -Dichl oroethaneTetrachlo roethene2-HexanoneDibromoch loromethaneChloroben zene1 1 1 2 Tetrachloroethane
Work Order fDate ReceoweedAnalysis matteAnalysis TTnraie
Instrument IDMethod
RESULTNDNDNDNDNDND
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
FX07A1AA09/10/0309/10/0320 07
MSHSW846 826
REPORTINGLIMIT1 02 02 02 02 01 0
1 01 01 01 0101 01 01 01 01 01 01 05 01 00 501 01 01 01 01 01 05 01 01 00 501 05 01 01 01 0
Mattouc10 00 MB Hftnnni
OB
UNITSug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
WATERf 32542i
MDL0 400 300 301 00 300 40
0 300 300 500 303 00 300 200 300 300 300 300 203 00 300 300 300 300 300 300 300 403 00 300 300 400 303 00 400 300 30
(Continued on next page)
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HALEY & ALDRICH INC
Client Sample ID MC003_WS090903_0001
GC/MS Volatiles
Lot-Sample # E3I100190 003 Work Order # FX07A1AA Matrix WATER
PARAMETEREthylbenzeneVinyl chlorideXylenes (total)StyreneBromofonnIsopropyl benzene1 1 2 2 Tetrachloroethane123 Tri chloropropanen PropylbenzeneBromobenzene135 Trimethylbenzene2 Chlorotoluene4 Chlorotoluenetert Butylbenzene124 Trimethylbenzenesec Butylbenzenep Isopropyl toluene1 3 Dichlorobenzene1 4 Dichlorobenzenen-Butylbenzene1 2 Dichlorobenzene1 2 Dibromo 3-chloro
propane124 Tri chloro
benzeneHexachlorobutadleneNaphthalene123 Tri chlorobenzeneAcroleinAcrylonitrilelodomethane2 Chloroethyl vinyl etherTetrahydrofuranVinyl acetate
SURROGATEBromof luo robenzene1 2 Dichloroethane d4Toluene d8
RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
ND
NDNDNDNDNDNDNDNDND
PERCENTRECOVERY9891106
REPORTINGLIMIT1 00 501 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 02 0
1 0
1 01 01 020202 05 0105 0
RECOVERYLIMITS(75 130)(65 135)(80 - 130)
UNITSug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
ug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
MDL0 200 300 800 300 300 300 400 400 400 300 200 300 300 200 300 300 300 300 300 300 300 70
0 30
0 300 500 4012101 02 02 02 0
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Client Sample ID MC004_WS 090903_0001
GC/MS Volatiles
Lot-Sample # E3I100190 004Date Sampled 09/09/03 14 30Prep Date 09/10/03Prep Batch # 3254454Dilution Factor 1Analyst ID 004648
PARAMETERDichlorod i f luoromethaneChloromet haneChloroethaneBromomethaneTrichloro f luoromethane112 Trichlorotrif luoro
ethane1 1 -DichloroetheneMethylene chlorideMethyl tert butyl etherCarbon disulfideAcetonetrans-1 2 Dichloroethene1 l Dichloroethane2 2-Dichloropropanecis 1 2 DichloroetheneChloroformBromochlo romethane111 Tri Chloroethane2 Butanone1 1 Dichl oropropeneCarbon te trachloride1 2 DibromoethaneBenzeneTrichloro ethene1 2 Dichl oropropaneBromodlchloromethaneDibromome thane4 -Methyl 2 pentanoneToluene112 Tri Chloroethane1 2 DichloroethaneTetrachlo roethene2-HexanoneDibromoch loromethaneChloroben zene1 1 1 2 Tetrachloroethane
Work Order fDate Race owedAnalysis ntatteAnalysis Tnrnie
Instrument IDMethod
RESULTNDNDNDNDNDND
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
FX07K1AA09/10/0309/10/0320 37
MSHSW846 826
REPORTINGLIMIT1 02 02 02 02 01 0
1 01 01 01 0101 01 01 01 01 01 01 05 01 00 501 01 01 01 01 01 05 01 01 00 501 05 01 01 01 0
Matt10 00 MB
OB
UNITSug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
:jnLX WATERSiunm f 325421
MDL0 400 300 301 00 300 40
0 300 300 500 303 00 300 200 300 300 300 300 203 00 300 300 300 300 300 300 300 403 00 300 300 400 303 00 400 300 30
(Continued on next page)
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Client Sample ID MC004_WS 090903_0001
GC/MS Volatiles
Lot-Sample # E3I100190 004 Work Ordeir FX07K1AA Katrajc WATER
PARAMETEREthylbenz eneVinyl chlorideXylenes (total)StyreneBromoformI sopropyl benzene1 1 2 2 Tetrachloroethane123 Tri chloropropanen-PropylbenzeneBromobenz ene135 Trimethylbenzene2 Chlorotoluene4 Chlorotoluenetert Butylbenzene124 Trimethylbenzenesec Butylbenzenep Isopropyltoluene1 3 Dichlorobenzene1 4 Dichlorobenzenen Butylbenzene1 2 Dichlorobenzene1 2 Dibromo 3 chloro
propane124 Tri chloro
benzeneHexachlor obutadieneNaphthalene123 Tri chlorobenzeneAcroleinAcrylonit rilelodomethane2 Chloroethyl vinyl etherTetrahydrofuranVinyl acetate
SURROGATEBromof luo robenzene1 2 Dichl oroethane d4Toluene d8
RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
ND
NDNDNDNDNDNDNDNDND
PERCENTRECOVERY9390102
REPORTINGLIMIT1 00 501 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 02 0
1 0
1 01 01 020202 05 0105 0
RECOVERYLIMITS(75 130)(65 135)(80 - 130)
UNITSug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
ug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
MDL0 200 300 800 300 300 300 400 400 400 300 200 300 300 200 300 300 300 300 300 300 300 70
0 30
0 300 500 4012101 02 02 02 0
IIIIIIIIIIIIIIIIIII
HALEY & ALDRICH INC
Client Sample ID MW31B_WG 090903_0001
GC/MS Volatiles
Lot-Sample # E3I100190 005Date Sampled 09/09/03 15 30Prep Date 09/10/03Prep Batch # 3254454Dilution Factor 1Analyst ID 004648
PARAMETERDichlorodif luoromethaneChloromet haneChloroe thaneBromomethaneTnchloro f luoromethane112 Trichlorotnfluoro
ethane1 1 DichloroetheneMethylene chlorideMethyl tert butyl etherCarbon disulfideAcetonetrans 1 2 Dichloroethene1 1 Dichl oroethane2 2 Dichl oropropanecis 1 2 DichloroetheneChloroformBromochlo romethane111 Trichloroethane2 Butanon e1 1 Dichl oropropeneCarbon te trachloride1 2 DibromoethaneBenzeneTrichloroethene1 2 Dichl oropropaneBromodich loromethaneDibromome thane4 Methyl 2 pentanoneToluene1 1 2 -Trichloroethane1 2 Dichl oroethaneTetrachlo roethene2-HexanoneDibromoch loromethaneChlorobenzene1 1 1 2 Tetrachloroethane
Work Order #Date Rece:n.T0ffidAnalysis E&teAnalysis TTmtne
Instrument IDMethod
RESULTNDNDNDNDNDND
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
FX07M1AA09/10/0309/10/0321 08
MSHSW846 826
REPORTINGLIMIT1 02 02 02 02 01 0
1 01 01 01 0101 01 01 01 01 01 01 05 01 00 501 01 01 01 01 01 05 01 01 00 501 05 01 01 01 0
KattOLT10 00 MS SBuran
OB
UNITSug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
WATERf 3254202
MDL0 400 300 301 00 300 40
0 300 300 500 303 00 300 200 300 300 300 300 203 00 300 300 300 300 300 300 300 403 00 300 300 400 303 00 400 300 30
(Continued on next page)
IIIIIIIIIIIIIIIIIII
HALEY & ALDRICH INC
Client San^le ID MW31B_WG090903_0001
GC/MS Volatiles
Lot-Sample # E3I100190 005 Work Order # FX07M1AA Hatrxx WATER
PARAMETEREthylbenzeneVinyl chlorideXylenes (total)StyreneBromoformI sopropyl benzene1 1 2 2 T etrachloroe thane123 Tri chloropropanen PropylbenzeneBromobenz ene135 Tnmethylbenzene2 Chlorotoluene4 -Chlorot oluenetert Butylbenzene124 Tnmethylbenzenesec Butylbenzenep I sopropyl toluene1 3 Dichlorobenzene1 4 Dichlorobenzenen Butylbenzene1 2 Dichlorobenzene1 2 Dibromo 3 chloro
propane124 Tri chloro
benzeneHexachlor obutadieneNaphthalene123 Tri chlorobenzeneAcroleinAcrylonit rilelodomethane2 Chloroethyl vinyl etherTetrahydrofuranVinyl acetate
SURROGATEBr omo f luo robenz ene1 2 Dichloroethane d4Toluene d8
RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
ND
NDNDNDNDNDNDNDNDND
PERCENTRECOVERY9786103
REPORTINGLIMIT1 00 501 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 02 0
1 0
1 01 01 020202 05 0105 0
RECOVERYLIMITS(75 130)(65 135)(80 - 130)
UNITSug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
ug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
MDL0000000000000000000000
0
00012101222
20308030303040404030203030203030303030303070
30
305040
0000
IIIIIIIIIIIIIIIIIII
HALEY & ALDRICH INC
Client Sample ID MC002_STS090903_0001
GC/MS Volatiles
Lot-Sample # E3I100190 -006Date Sampled 09/09/03 11 20Prep Date 09/11/03Prep Batch # 3255091Dilution Factor 1% Moisture
PARAMETERAcetoneAcroleinAcrylonit rileBenzeneBromobenz eneBromochlo romethaneBromodi ch loromethaneBromoformBromomethane2 But anon en Butylbenzenesec Butylbenzenetert ButylbenzeneCarbon disulfideCarbon tetrachlorideChloroben zeneDlbromoch loromethaneChloroethane2 Chloroethyl vinyl etherChloroformChloromet hane2 Chlorotoluene4 Chlorotoluene1 2 Dibromo 3 chloro
propane1 2 Dibromoe thaneDibromome thane1 2 Dichlorobenzene1 3 Dichlorobenzene1 4 DichlorobenzeneDichlorodif luoromethane1 1 Dichloroethane1 2 -Dichloroethanecis 1 2 Dichloroethenetrans-1 2 Dichloroethene1 1 Dichloroethene1 2 Dichl oropropane
Work Order tDate Rece:n.T»edAnalysis EtotteAnalysis Tnjme
Analyst IPMethod
RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
NDNDNDNDNDNDNDNDNDNDNDND
FX07W1AA09/10/0309/11/0317 12
015590SW846 826
REPORTINGLIMIT25100505 05 05 05 05 010255 05 05 05 05 05 05 010105 0105 05 010
5 05 05 05 05 0105 05 05 05 05 05 0
Matrix10 00 HE5 Kmnn
SOLID# 3255002
XmsltKiuiineimtJt HD MSDOB
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
MDL1530402 02 01 01 03 08 0152 02 02 03 01 02 01 02 05 01 03 02 02 03 0
3 01 02 02 02 01 01 01 02 02 02 01 0
(Continued on next page)
1111111111111111111
Client
Lot-Sample # E3I100190 006
PARAMETER2 2 Dichloropropanecis 1 3 Dichloropropenetrans-1 3 Dichloropropene1 1 DichloropropeneEthylbenz eneHexachlor obutadiene2 HexanonelodomethaneIsopropyl benzenep Isopropyl tolueneMethylene chloride4 Methyl -2 pentanoneMethyl tert butyl etherNaphthalenen PropylbenzeneStyrene1 1 1 2 Tetrachloroethane1 1 2 2 TetrachloroethaneTetrachlo roetheneTetrahydrofuranToluene123 Trichlorobenzene124 Trichloro
benzene111 Trichloroethane112 TrichloroethaneTrichloro etheneTrichloro f luoromethane123 Tri chloropropane124 Tnmethylbenzene135 TnmethylbenzeneVinyl acetateVinyl chlorideXylenes (total)
SURROGATEBromofluorobenzene1 2 Dichloroethane d4Toluene d8
HALEY &
Sample ID
GC/MS
ALDRICH INC
MC002_ST S090903_0001
Volatiles
Work Order # FX07W1AA
RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
NDNDNDNDNDNDNDNDNDND
PERCENTRECOVERY787775
REPORTINGLIMIT5 05 05 05 05 05 025105 05 05 0255 05 05 0105 05 05 0205 05 05 0
5 05 05 0105 05 05 010105 0
RECOVERYLIMITS(60 - 130)(60 140)(60 130)
Matrzx
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
SOLID
MDL2 01 03 01 02 02 010102 02 03 0101 02 02 02 03 03 02 02 02 02 02 0
1 03 02 02 03 02 02 05 02 03 0
IIIIIIIIIIIIIIIIIII
HALEY & ALDRICH INC
Client Sample ID MC004_STS090903_0001
GC/MS Volatiles
Lot-Sample # E3I100190 007Date Sampled 09/09/03 14 30Prep Date 09/11/03Prep Batch # 3255091Dilution Factor 1% Moisture
PARAMETERAcetoneAcroleinAcrylonit rileBenzeneBromobenz eneBromochl o rome thaneBromodich loromethaneBromoformBromomethane2 Butanonen Butylbenzenesec Butylbenzenetert ButylbenzeneCarbon disulfideCarbon tetrachlorideChloroben zeneDlbromoch loromethaneChloroethane2 Chloroethyl vinyl etherChloroformChloromethane2 Chlorotoluene4 Chlorotoluene1 2 Dibromo 3 chloro
propane1 2 DibromoethaneDibromome thane1 2 Dichlorobenzene1 3 Dichl orobenzene1 4 DichlorobenzeneDichlorodif luoromethane1 1 Dichl oroethane1 2 Dichl oroethanecis 1 2-Dichloroethenetrans 1 2 Dichloroethene1 1 Dichloroethene1 2 Dichl oropropane
Work Order #Date ReceivedAnalysis TTOattreAnalysis TPnrne
Analyst IPMethod
RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
NDNDNDNDNDNDNDNDNDNDNDND
FX0791AA09/10/0309/11/0317 44
015590SW846 826
REPORTINGLIMIT25100505 05 05 05 05 010255 05 05 05 05 05 05 010105 0105 05 010
5 05 05 05 05 0105 05 05 05 05 05 0
Wattimc10 00 MB Hum
SOLIDt 3255002
irmmlt- mmmmnin- HD MSD
OB
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
MDL1530402 02 01 01 03 08 0152 02 02 03 01 02 01 02 05 01 03 02 02 03 0
3 01 02 02 02 01 01 01 02 02 02 01 0
(Continued on next page)
IIIIIIIIIIIIIIIIIII
HALEY & ALDRICH INC
Client Bangle ID MC004_STS090903_0001
GC/MS Volatiles
Lot-Sample # E3I100190 007 Work Order FX0791AA Matrix SOLID
PARAMETER2 2 Dichl oropropanecis 1 3 Dichloropropenetrans 1 3 Dichloropropene1 1 DichloropropeneEthylbenzeneHexachlorobutadlene2 HexanonelodomethaneI sopropyl benzenep I sopropyl tolueneMethylene chloride4 Methyl 2 pentanoneMethyl tert butyl etherNaphthalenen PropylbenzeneStyrene1 1 1 2 Tetrachloroethane1 1 2 2 TetrachloroethaneTetrachlo roetheneTetrahydrofuranToluene123 Tri chlorobenzene124 Trichloro
benzene111 Trichloroethane112 TrichloroethaneTrichloroetheneTrichloro f luoromethane123 Tri chloropropane124 Tnmethylbenzene135 TnmethylbenzeneVinyl acetateVinyl chlorideXylenes (total)
SURROGATEBromofluorobenzene1 2 Dichloroethane-d4Toluene d8
RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
NDNDNDNDNDNDNDNDNDND
PERCENTRECOVERY807975
REPORTINGLIMIT5 05 05 05 05 05 025105 05 05 0255 05 05 0105 05 05 0205 05 05 0
5 05 05 0105 05 05 010105 0
RECOVERYLIMITS(60 - 130)(60 140)(60 130)
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
MDL2 0\ 03 01 02 02 010102 02 03 0101 02 02 02 03 03 02 02 02 02 02 0
1 03 02 02 03 02 02 05 02 03 0
Boeing/CCI Olathe KS
Lot # E31150165
IIIII_ ANALYTICAL REPORT
IIIIIIIIIIIII
Haley & Aldrich Inc
SEVERN TRENT LABORATORIES INC
Diane SuzukiProject Manager
September 29 2003
IIIIIIm
I
I
I
I
I
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EXECUTIVE SUMMARY - Detection HighlightsE3I150165
PARAMETER RESULTREPORTINGLIMIT UNITS
MC001_WS100903_0001 09/10/03 11 30 001
Acetone 3 3 J
MW32B_WS091203_0001 09/12/03 15 30 003
Chloroform 0 56 J
MW32B_WS091203_0002 09/12/03 15 30 004
Chloroform 0 57 J
10
1 0
1 0
ug/L
ug/L
ug/L
ANAL YTICALMETHOD
SW846 8260B
SW846 8260B
SW846 8260B
IIIIIIIIIIIIIIIIIII
METHODS SUMMARYE3I150165
PARAMETERANALYTICALMETHOD
Volatile Or games by GC/MSVolatile Organics by GC/MS
Reference s
SW846 8260BSW846 8260B
PREPARATI ONMETHOD______
SW846 5030SW846 5030B/826
SW846 Test Methods for Evaluating Solid Waste Physical/ChemicalMethods Third Edition November 1986 and its updates
IIIIIIIIIIIIIIIIIII
SAMPLE SUMMARYB3I150165
SAMPLED SAMPWO # SAMPLEtf CLIENT SAMPLE ID____________ _______________________________ DATE TIME
FOC4VPOC44FOC46FOC47FOC5HFOC5L
NOTE(S)
001002003004005006
MC001MW33BMW32BMW32BMC001TRIP
_WS1009_WS0912_WS0912_WS0912_STS100BLANK
03_03_03_03_903
0001000100010002_0001
09/10/0309/12/0309/12/0309/12/0309/10/0309/02/03
1112151511
3045303025
The analytical results of the samples listed above are presented on the following pagesAll calculations an performed before rounding to avoid round off errors In calculated resultsResult! noted as NO were not detected at or above the staled limitThis repon must not be reproduced except in full without the written approval of the laboratoryResults for the following parameters are never reported on a dry weight basis color corroslvlty density flashpoint Igmtabihty layers odorpaint filter test pH porosity pressure reactivity redo* potential specific gravity spot tests solids solubility temperature viscosity and weight
IIIIIIIIIIIIIIIIIII
HALEY & ALDRICH INC
Client Sample ID MC001_WS 100903_0001
GC/MS Volatiles
Lot-Sample # E3I150165 -001Date Sampled 09/10/03 11 30Prep Date 09/16/03Prep Batch # 3259599Dilution Factor 1Analyst ID 015590
PARAMETERDichlorodif luoromethaneChloromet haneChloroethaneBromome thaneTnchlorof luoromethane112 Tnchlorotrifluoro
ethane1 1 DichloroetheneMethylene chlorideMethyl tert butyl etherCarbon disulfideAcetonetrans 1 2 Dichloroethene1 1 Dichl oroethane2 2 Dichl oropropanecis 1 2 DichloroetheneChloroformBromochlo romethane111 Tri chloroethane2 Butanone1 1 Dichl oropropeneCarbon te trachloride1 2 DibromoethaneBenzeneTr ichloro ethene1 2 Dichl oropropaneBromodich loromethaneDibromome thane4 Methyl 2 pentanoneToluene112 Tri chloroethane1 2 Dichl oroethaneTetrachlo roethene2 HexanoneDibromoch loromethaneChloroben zene1 1 1 2 Tetrachloroethane
Work Order #Date Recen̂ ffidAnalysis TUffitreAnalysis Tame
Instrument IDMethod
RESULTNDNDNDNDNDND
NDNDNDND3 3 JNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
FOC4V1AA09/15/0309/16/0315 17
MSKSW846 826
REPORTINGLIMIT1 02 02 02 02 01 0
1 01 01 01 0IdD1 01 01 01 01 01 01 05 01 00 SO1 01 01 01 01 01 05 01 01 00 501 05 01 01 01 0
Mbitt-im-ir
10 00 MB Sunn
OB
UNITSug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
WATERf 32603!
MDL0 400 300 301 00 300 40
0 300 300 500 303 00 300 200 300 300 300 300 203 00 300 300 300 300 300 300 300 403 00 300 300 400 303 00 400 300 30
(Continued on next page)
IIIIIIIIIIIIIIIIIII
HALEY & ALDRICH INC
Client San^le ID MC001_WS 100903_0001
GC/MS Volatiles
Lot-Sample # E3I150165 001 Work Order FOC4V1AA Matrix
) Estimated result Result is less than RU
WATER
PARAMETEREthylbenzeneVinyl chlorideXylenes (total)StyreneBromoformIsopropyl benzene1 1 2 2 Tetrachloroethane123 Tri chloropropanen PropylbenzeneBromobenz ene135 Trimethylbenzene2 Chlorot oluene4 Chlorot oluenetert Butylbenzene124 Trimethylbenzenesec Butylbenzenep Isopropyltoluene1 3 Dichlorobenzene1 4 Dichlorobenzenen Butylbenzene1 2 Dichlorobenzene1 2 Dibromo 3 chloro
propane124 Tri chloro-
benzeneHexachlorobutadleneNaphthalene123 Tri chlorobenzeneAcroleinAcrylonit rilelodomethane2 Chloroethyl vinyl etherTe t r ahydr o fur anVinyl acetate
SURROGATEBromof luo robenzene1 2 Dichl oroethane d4Toluene d8
NOTB(S)
RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
ND
NDNDNDNDNDNDNDNDND
PERCENTRECOVERY107121110
REPORTINGLIMIT1 00 50I 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 02 0
1 0
1 01 01 020202 05 0105 0
RECOVERYLIMITS(75 130)(65 135)(80 - 130)
UNITSug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
ug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
MDL0 200 300 800 300 300 300 400 400 400 300 200 300 300 200 300 300 300 300 300 300 300 70
0 30
0 300 500 4012101 02 02 02 0
IIIIIIIIIIIIIIIIIII
HALEY & ALDRICH INC
Client Sample ID MB33B_WS 091203_0001
GC/MS Volatiles
Lot-Sample # E3I150165 002Date Sampled 09/12/03 12 45Prep Date 09/16/03Prep Batch # 3259599Dilution Factor 1Analyst ID 015590
PARAMETERDichlorodif luoromethaneChloromet haneChloroethaneBromomethaneTrichloro f luoromethane112 Trichlorotrif luoro
ethane1 1 DichloroetheneMethylene chlorideMethyl tert butyl etherCarbon disulfideAcetonetrans 1 2 Dichloroethene1 1 Dichloroethane2 2 Dichl oropropanecis 1 2 DichloroetheneChloroformBromochlo romethane111 Tri chloroethane2 But anon e1 1 Dichl oropropeneCarbon tetrachlonde1 2 DibromoethaneBenzeneTrichloro ethene1 2 Dichl oropropaneBromodich loromethaneDibromome thane4 Methyl 2 pentanoneToluene112 Tri chloroethane1 2 DichloroethaneTetrachlo roethene2 HexanoneDibromoch loromethaneChloroben zene1 1 1 2 Tetrachloroethane
Work Order $Date ReceivedAnalysis matteAnalysis Tame
Instrument IDMethod
RESULTNDNDNDNDNDND
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
FOC441AA09/15/0309/16/0315 40
MSKSW846 826
REPORTINGLIMIT1 02 02 02 02 01 0
1 01 01 01 0101 01 01 01 01 01 01 05 01 00 501 01 01 01 01 01 05 01 01 00 501 05 01 01 01 0
Matnx10 00 USES Kmm
OB
UNITSug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
WATERi 3260331
MDL0 400 300 301 00 300 40
0 300 300 500 303 00 300 200 300 300 300 300 203 00 300 300 300 300 300 300 300 403 00 300 300 400 303 00 400 300 30
(Continued on next page)
IIIIIIIIIIIIIIIIIII
HALEY & ALDRICH INC
Client Sample ID MW33B_WS 091203_0001
GC/MS Volatiles
Lot-Sample # E3I150165 002 Work Ordeir # FOC441AA Katrxz WATER
PARAMETEREthylbenz eneVinyl chlorideXylenes (total)StyreneBromoformIsopropyl benzene1 1 2 2 T etrachloroethane123 Tri chloropropanen-PropylbenzeneBromobenz ene135 Trimethylbenzene2 Chlorotoluene4 Chlorot oluenetert Butylbenzene124 Trimethylbenzenesec Butylbenzenep Isopropyltoluene1 3 Dichlorobenzene1 4 Dichlorobenzenen Butylbenzene1 2 Dichlorobenzene1 2 Dibromo 3 chloro
propane124 Tri chloro
benzeneHexachlorobutadleneNaphthalene123 Tri chlorobenzeneAcroleinAcrylonit rilelodomethane2 Chloroethyl vinyl etherTetrahydr of uranVinyl acetate
SURROGATEBromof luo robenzene1 2 Dichloroethane d4Toluene-d8
RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
ND
NDNDNDNDNDNDNDNDND
PERCENTRECOVERY106119109
REPORTINGLIMIT1 00 501 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 02 0
1 0
1 01 01 020202 05 0105 0
RECOVERYLIMITS(75 130)(65 135)(80 130)
UNITSug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
ug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
MDL0 200 300 800 300 300 300 400 400 400 300 200 300 300 200 300 300 300 300 300 300 300 70
0 30
0 300 500 4012101 02 02 02 0
IIIIIIIIIIIIIIIIIII
HALEY & ALDRICH INC
Client Sample ID MW32B_WS 091203_0001
GC/MS Volatiles
Lot-Sample tt E3I150165 -003Date Sampled 09/12/03 15 30Prep Date 09/16/03Prep Batch # 3259599Dilution Factor 1Analyst ID 015590
PARAMETERDichlorod i f luoromethaneChloromet haneChloroethaneBromomethaneTrichloro f luoromethane112 Tnchlorotnfluoro
ethane1 1 DichloroetheneMethylene chlorideMethyl tert-butyl etherCarbon diaulfideAcetonetrans 1 2 DichloroetheneI 1 Dichl oroethane2 2-Dichloropropanecis 1 2 DichloroetheneChloroformBromochlo romethane111 Tri chloroethane2 But anon e1 1 Dichl oropropeneCarbon te trachloride1 2 DibromoethaneBenzeneTrichloro ethene1 2 Dichl oropropaneBromodi ch lorome thaneDibromome thane4 Methyl 2 pentanoneToluene112 Tri chloroethane1 2 Dichl oroethaneTetrachloroethene2 HexanoneDibromoch loromethaneChloroben zene1 1 1 2 Tetrachloroethane
Work Order $Date Recei^redAnalysis KtotteAnalysis TTume
Instrument IDMethod
RESULTNDNDNDNDNDND
NDNDNDNDNDNDNDNDND0 56 JNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
FOC461AA09/15/0309/16/0316 03
MSKSW846 826
REPORTINGLIMIT1 02 02 02 02 01 0
1 01 01 01 0101 01 01 01 01 CD1 01 05 01 00 501 01 01 01 01 01 05 01 01 00 501 05 01 01 01 0
Jtotz10 00 MS I
OB
UNITSug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
xx WATERturn $ 32603:
MDL0 400 300 301 00 300 40
0 300 300 500 303 00 300 200 300 300 300 300 203 00 300 300 300 300 300 300 300 403 00 300 300 400 303 00 400 300 30
(Continued on next page)
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HALEY & ALDRICH INC
Client Sample ID MW32BJHS 091203_0001
GC/MS Volatiles
Lot-Sample # E3I150165-003 Work Order POC461AA Matrix
i Estimated result Result Is less than RL
WATER
PARAMETEREthylbenz eneVinyl chlorideXylenes (total)StyreneBromoformIsopropyl benzene1 1 2 2 Tetrachloroethane123 Tri chloropropanen PropylbenzeneBromobenz ene135 Trimethylbenzene2 Chlorot oluene4 Chlorot oluenetert Butylbenzene124 Trimethylbenzenesec Butylbenzenep Isopropyl toluenel 3 Dichlorobenzene1 4 Dichlorobenzenen Butylbenzene1 2 Dichlorobenzene1 2 Dibromo 3 chloro-
propane124 Trichloro
benzeneHexachlorobutadleneNaphthalene123 Tri chlorobenzeneAcroleinAcrylonitrilelodomethane2 Chloroethyl vinyl etherTetrahydrofuranVinyl acetate
SURROGATEBromofluorobenzene1 2-Dichloroethane d4Toluene d8
NOTE(S)
RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
ND
NDNDNDNDNDNDNDNDND
PERCENTRECOVERY109122107
REPORTINGLIMIT1 00 501 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 02 0
1 0
1 01 01 020202 05 0105 0
RECOVERYLIMITS(75 130)(65 135)(80 130)
UNITSug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
ug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
MDL0 200 300 800 300 300 300 400 400 400 300 200 300 300 200 300 300 300 300 300 300 300 70
0 30
0 300 500 4012101 02 02 02 0
IIIIIIIIIIIIIIIIIII
HALEY & ALDRICH INC
Client Sample ID MW32BJWS 091203_0002
GC/MS Volatiles
Lot-Sample #Date Sampled
E3I150165 004 Work Order t09/12/03 15 30 Date Received
Prep Date 09/16/03Prep Batch # 3259599Dilution Factor 1
Analysis BateAnalysis TTnmie
FOC471AA09/15/03 10 00 MS Hum09/16/0316 26
(Continued on next page)
WATER3260331
Analyst ID 015590
PARAMETERDichlorod if luoromethaneChloromet haneChloroethaneBromome thaneTrichloro f luoromethane112 Tnchlorotnf luoro
ethane1 1 DichloroetheneMethylene chlorideMethyl tert butyl etherCarbon disulfideAcetonetrans 1 2 Dichloroethene1 1 Dichl oroethane2 2 Dichl oropropanecis 1 2 DichloroetheneChloroformBromochlo romethane111 Tri chloroethane2 But anon e1 1 Dichl oropropeneCarbon te trachlonde1 2 DibromoethaneBenzeneTrichloro ethene1 2 Dichl oropropaneBromodich loromethaneDibromome thane4 -Methyl 2 pentanoneToluene112 Tri chloroethane1 2 Dichl oroethaneTetrachloroethene2 HexanoneDibromoch loromethaneChloroben zene1 1 1 2 Tetrachloroethane
Instrument IDMethod
RESULTNDNDNDNDNDND
NDNDNDNDNDNDNDNDND0 57 JNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
MSKSW846 826
REPORTINGLIMIT1 02 02 02 02 01 0
1 01 01 01 0101 01 01 01 0i Q>1 01 05 01 00 501 01 01 01 01 01 05 01 01 00 501 05 01 01 01 0
OB
UNITSug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
MDL0 400 300 301 00 300 40
0 300 300 500 303 00 300 200 300 300 300 300 203 00 300 300 300 300 300 300 300 403 00 300 300 400 303 00 400 300 30
IIIIIIIIIIIIIIIIIII
HALEY & ALDRICH INC
Client Sample ID HW32B_WS 091203_0002
GC/MS Volatiles
Lot-Sample # E3I150165-004 Work Order f FOC471AA Matrix
J Estimated result Result is less than RL
WATER
PARAMETEREthylbenzeneVinyl chlorideXylenes (total)StyreneBromoformIsopropyl benzene1 1 2 2 Tetrachloroethane123 Tri chloropropanen PropylbenzeneBromobenz ene1 3 5-Trimethylbenzene2 Chlorotoluene4 Chlorotoluenetert-Butylbenzene124 Trimethylbenzenesec Butyl benzenep Isopropyl toluene1 3 Dichlorobenzene1 4 Dichlorobenzenen Butylbenzene1 2 Dichlorobenzene1 2 Dibromo-3 chloro
propane124 Tri chloro
benzeneHexachlorobutadieneNaphthalene123 Tri chlorobenzeneAcroleinAcrylonitrilelodomethane2 Chloroethyl vinyl etherTetrahydr of uranVinyl acetate
SURROGATEBromof luo robenzene1 2 Dichloroethane d4Toluene d8
NOTE(S)
RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
ND
NDNDNDNDNDNDNDNDND
PERCENTRECOVERY103115108
REPORTINGLIMIT1 00 501 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 02 0
1 0
1 01 01 020202 05 0105 0
RECOVERYLIMITS(75 130)(65 135)(80 130)
UNITSug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
ug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
MDL0 200 300 800 300 300 300 400 400 400 300 200 300 300 200 300 300 300 300 300 300 300 70
0 30
0 300 500 4012101 02 02 02 0
IIIIIIIIIIIIIIIIIII
HALEY & ALDRICH INC
Client Sample ID MC001_ST S100903_0001
GC/MS Volatiles
Lot-Sample # E3I150165 005Date Sampled 09/10/03 11 25Prep Date 09/19/03Prep Batch # 3265544Dilution Factor 1% Moisture
PARAMETERAcetoneAcroleinAcrylonit rileBenzeneBromobenz eneBromochlo romethaneBromodich loromethaneBromoformBromomethane2 But anon en Butylbenzenesec Butylbenzenetert ButylbenzeneCarbon disulfideCarbon tetrachlondeChloroben zeneDlbromoch loromethaneChloroethane2 Chloroethyl vinyl etherChloroformChloromet hane2 Chlorotoluene4 Chlorotoluene1 2 Dibromo 3-chloro
propane1 2 DibromoethaneDibromome thane1 2 Dichlorobenzene1 3 Dichlorobenzene1 4 -DichlorobenzeneDichlorodif luoromethane1 1 Dichloroethane1 2 Dichloroethanecis 1 2 Dichloroethenetrans 1 2 Dichloroethene1 1 Dichloroethene1 2 Dichloropropane
Work Order #Date ReceivedAnalysis matteAnalysis Tame
Analyst IE)Method
RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
NDNDNDNDNDNDNDNDNDNDNDND
FOC5H1AA09/15/0309/19/0317 17
999998SW846 626
REPORTINGLIMIT25100505 05 05 05 05 010255 05 05 05 05 05 05 010105 0105 05 010
5 05 05 05 05 0105 05 05 05 05 05 0
Matrix10 00 MB Stonm
SOLID# 3265309
Innstmnineinitt HD MSDOB
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
MDL1530402 02 01 01 03 08 0152 02 02 03 01 02 01 02 05 01 03 02 02 03 0
3 01 02 02 02 01 01 01 02 02 02 01 0
(Continued on next page)
IIIIIIIIIIIIIIIIIII
HALEY & ALDRICH INC
Client Sanqple ID MC001_ST S100903_0001
GC/MS Volatiles
Lot-Sample # E3I150165 005 Work Order FOC5H1AA Matrix
Surrogate recovery is outside slated control limits
SOLID
PARAMETER2 2 Dichloropropanecis 1 3 Dichloropropenetrang 1 3 Dichloropropene1 1 DichloropropeneEthylbenzeneHexachlorobutadiene2-HexanonelodomethaneI sopropyl benzenep IsopropyltolueneMethylene chloride4 Methyl 2 pentanoneMethyl tert butyl etherNaphthalenen PropylbenzeneStyrene1 1 1 2 Tetrachloroethane1 1 2 2 TetrachloroethaneTetrachloroetheneTetrahydrofuranToluene123 Tri chlorobenzene124 Trichloro
benzene111 Tri chloroethane112 Tri chloroethaneTrichloro etheneTrichloro fluoromethane1 2 3-Trichloropropane124 Trimethylbenzene135 TrimethylbenzeneVinyl acetateVinyl chlorideXylenes (total)
SURROGATEBromof luorobenzene1 2 Dichloroethane d4Toluene d8
NOTE(S)
RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
NDNDNDNDNDNDNDNDNDND
PERCENTRECOVERY37 *32 *37 *
REPORTINGLIMIT5 05 05 05 05 05 025105 05 05 0255 05 05 0105 05 05 0205 05 05 0
5 05 05 0105 05 05 010105 0
RECOVERYLIMITS(60 130)(60 140)(60 130)
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
MDL2 01 03 01 02 02 010102 02 03 0101 02 02 02 03 03 02 02 02 02 02 0
1 03 02 02 03 02 02 05 02 03 0
IIIIIIIIIIIIIIIIIII
HALBY &. ALDRICH INC
Client Sample ID TRIP BLANK
GC/MS Volatiles
Lot-Sample # E3I150165 -006Date Sampled 09/02/03Prep Date 09/16/03Prep Batch # 3259599Dilution Factor 1Analyst ID 015590
PARAMETERDichlorod if luoromethaneChloromet haneChloroethaneBromomethaneTrichloro f luoromethane112 Trichlorotrifluoro
ethane1 1 DichloroetheneMethylene chlorideMethyl tert -butyl etherCarbon disulfideAcetonetrans 1 2 Dichloroethene1 1 Dichloroethane2 2-Dichloropropanecis 1 2 DichloroetheneChloroformBromochlo rome thane111 Tri chloroethane2 Butanone1 1 DichloropropeneCarbon te trachloride1 2 DibromoethaneBenzeneTrichloro ethene1 2 DichloropropaneBromodich loromethaneDibromome thane4 -Methyl 2 pentanoneToluene112 Tri chloroethane1 2 DichloroethaneTetrachlo roethene2 HexanoneDibromoch loromethaneChloroben zene1 1 1 2 Tetrachloroethane
Work Order #Date ReceiiuedAnalysis UtoteAnalysis TTume
Instrument IDMethod
RESULTNDNDNDNDNDND
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
FOC5L1AA09/15/0309/16/0314 30
MSKSW846 826
REPORTINGLIMIT1 02 02 02 02 01 0
1 01 01 01 0101 01 01 01 01 01 01 05 01 00 501 01 01 01 01 01 05 01 01 00 501 05 01 01 01 0
IMIatt-ir-inr
10 00 90S ffifflmt
OB
UNITSug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
WATERf 32603:
MDL0 400 300 301 00 300 40
0 300 300 500 303 00 300 200 300 300 300 300 203 00 300 300 300 300 300 300 300 403 00 300 300 400 303 00 400 300 30
(Continued on next page)
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HALEY & ALDRICH INC
Client Sample ID TRIP BLANK
GC/MS Volatiles
Lot-Sample # E3I150165 -006 Work Ordes: FOC5L1AA Matrix WATER
PARAMETEREthylbenzeneVinyl chlorideXylenes (total)StyreneBromoformIsopropyl benzene1 1 2 2 T etrachloroethane1 2 3-Trichloropropanen PropylbenzeneBromobenzene135 Trimethylbenzene2 Chlorotoluene4 Chlorotoluenetert -Buty Ibenzene124 Trimethylbenzenesec Butyl benzenep - 1 soprop yl toluene1 3 Dichlorobenzene1 4 -Dichlorobenzenen Butylbenzene1 2 -Dichlorobenzene1 2 Dibromo 3 chloro-
propane124 Trichloro
benzeneHexachlor obutadieneNaphthalene123 TnchlorobenzeneAcroleinAcrylonit rilelodomethane2 Chloroethyl vinyl etherTetrahydrofuranVinyl acetate
SURROGATEBromofluorobenzene1 2 Dichloroe thane d4Toluene d8
RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
ND
NDNDNDNDNDNDNDNDND
PERCENTRECOVERY105123109
REPORTINGLIMIT1 00 501 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 02 0
1 0
1 01 01 020202 05 0105 0
RECOVERYLIMITS(75 130)(65 135)(80 130)
UNITSug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
ug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
MDL0 200 300 800 300 300 300 400 400 400 300 200 300 300 200 300 300 300 300 300 300 300 70
0 30
0 300 500 4012101 02 02 02 0
ANALYTICAL REPORT
Boeing/CCI Olathe KS
Lot # E31180205
Haley & Aldrich Inc
SEVERN TRENT LABORATORIES INC
Diane SuzukiProject Manager
September 24 2003
IEXECUTIVE SUMMARY - Detection Highlights
• B3I180205
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REPORTING ANAL YTICALPARAMETER RESULT LIMIT UNITS METHOD
MW_22B_WG091703_0001 09/17/03 14 00 001
Carbon disulfide 0 68 J 10 ug/L SW846 8260B
IMETHODS SUMMARY
I E3I180205
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ANALYTICAL PREPARATI ONPARAMETER ____ ___ ____ METHOD________ METHOD
Volatile Organics by GC/MS SW846 8260B SW846 5030B/826
References
SW846 Test Methods for Evaluating Solid Waste Physical/ ChemicalMethods Third Edition November 1986 and its updates
1SAMPLE SUMMARY
• E3I180205
I WO # SAMPLE* CLIENT SAMPLE ID
FOLQG 001 MW_22B_WG091 703_0001• FOLQR 002 MW_23B_WG091 703_0001• FOLQW 003 TRIP BLANK E3G280120
I NOTB(S)The analytical results of the samples listed above aro presented on the following pagesAll calculations are performed before rounding to avoid round off errors In calculated resultsResults noted as NO were not detected at or above the stated limit
H This report must not be reproduced except In full without the written approval of the laboratoryB Results for the following parameters are never reported on o dry weight basis color corrosivity density flashpoint ignitabihty layers odor
paint filler test pH porosity pressure reactivity redox potential specific gravity spot tests solids solubility temperature viscosity and weight
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SAMPLED SAMPDATE TIME
09/17/03 14 0009/17/03 14 4009/02/03
IIIIIIIIIIIIIIIIIII
HALEY & ALDRICH INC
Client Sample ID MW_22B_WG091703_0001
GC/MS Volatiles
Lot-Sample # E3I180205 001Date Sampled 09/17/03 14 00Prep Date 09/19/03Prep Batch # 3262567Dilution Factor 1Analyst ID 015590
PARAMETERAcetoneAcroleinAcrylonit rileBenzeneBromobenzeneBromochlo romethaneBromodich loromethaneBromoformBromomethane2 -But anon en Butylbenzenesec Butylbenzenetert ButylbenzeneCarbon disulfideCarbon te trachlorideChloroben zeneDlbromoch loromethaneChloroe thane2 Chloroe thyl vinyl etherChloroformChloromethane2 Chlorotoluene4 Chlorotoluene1 2 Dibromo-3 chloro
propane1 2 DibromoethaneDibromome thane1 2 Dichlorobenzene1 3 Dichlorobenzene1 4 DichlorobenzeneDlchlorodlfluoromethane1 1 Dichloroethane1 2 Dichloroethanecis 1 2 -Dichloroethenetrans-1 2 Dichloroethene1 1 Dichloroethene1 2 Dichloropropane
Work Order ftDate Recea.T»edAnalysis lateAnalysis Tmme
Instrument IDMethod
RESULTNDNDNDNDNDNDNDNDNDNDNDNDND0 68 JNDNDNDNDNDNDNDNDNDND
NDNDNDNDNDNDNDNDNDNDNDND
FOLQG1AA09/18/0309/19/0314 08
MSHSW846 826
REPORTINGLIMIT1020201 01 01 01 01 02 05 01 01 01 01 <D0 501 01 02 05 01 02 01 01 02 0
1 01 01 01 01 01 01 00 501 01 01 01 0
Mtali10 00 KB
OB
UNITSug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
:nx WATERBnnm i 3262279
MDL3 012100 300 300 300 300 301 03 00 300 300 200 300 300 300 400 302 00 300 300 300 300 70
0 300 400 300 300 300 400 200 400 300 300 300 30
(Continued on next page)
IIIIIIIIIIIIIIIIIII
HALEY & ALDRICH INC
Client Sample ID MW_22B_WG091703_0001
GC/MS Volatiles
Lot-Sample # E3I180205 001 Work Order FOLQG1AA Matruc
J Estimated result Result Is less than RL
WATER
PARAMETER2 2 Dichloropropane1 1 Dichl oropropeneEthylbenzeneHexachlorobutadlene2 HexanonelodomethaneIsopropyl benzenep Isopropyl tolueneMethylene chloride4 Methyl 2 pentanoneMethyl tert butyl etherNaphthalenen PropylbenzeneStyrene1 1 1 2 Tetrachloroethane1 1 2 2 TetrachloroethaneTetrachlo roetheneTetrahydrofuranToluene123 Tri chlorobenzene124 Trichloro
benzene111 Tri chloroethane112 Tri chloroethaneTrichloro etheneTrichloro f luoromethane123 Tri chloropropane112 Tri chlorotnf luoro
ethane1 2 4-Tnmethylbenzene135 TnmethylbenzeneVinyl acetateVinyl chl orideXylenes (total)
SURROGATEBromof luo robenzene1 2 Dichloroethane d4Toluene d8
NOTE(S)
RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
NDNDNDNDNDND
NDNDNDNDND
PERCENTRECOVERY110111108
REPORTINGLIMIT1 01 01 01 05 02 01 01 01 05 01 01 01 01 01 01 01 0101 01 01 0
1 01 01 02 01 01 0
1 01 05 00 501 0
RECOVERYLIMITS(75 130)(65 135)(80 - 130)
UNITSug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/L
MDL0 300 300 200 303 01 00 300 300 303 00 500 500 400 300 300 400 302 00 300 400 30
0 200 300 300 300 400 40
0 300 202 00 300 80
IIIIIIIIIIIIIIIIIII
HALEY & ALDRICH INC
Client Sample ID MW_23B_WG091703_0001
GC/MS Volatiles
Lot-Sample # E3I180205 002Date Sampled 09/17/03 14 40Prep Date 09/19/03Prep Batch # 3262567Dilution Factor 1Analyst ID 015590
PARAMETERAcetoneAcroleinAcrylonit rileBenzeneBromobenzeneBromochlo romethaneBromodlchloromethaneBromoformBromome thane2 Butanonen Butylbenzenesec Butylbenzenetert ButylbenzeneCarbon disulfideCarbon tetrachlorideChloroben zeneDibromoch loromethaneChloroethane2 Chloroethyl vinyl etherChloroformChloromet hane2-Chlorotoluene4 Chlorotoluene1 2 Dibromo-3 chloro
propane1 2 DibromoethaneDibromome thane1 2 Dichlorobenzene1 3 Dichlorobenzene1 4 DichlorobenzeneDichlorodif luoromethane1 1 Dichloroethane1 2 Dichloroethanecis 1 2 Dichloroethenetrans I 2 Dichloroethene1 1 Dichloroethene1 2 Dichloropropane
Work Order #Date ReceRwedAnalysis DateAnalysis Tmme
Instrument IDMethod
RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
NDNDNDNDNDNDNDNDNDNDNDND
FOLQR1AA09/18/0309/19/0314 39
MSHSW846 826
REPORTINGLIMIT1020201 01 01 01 01 02 05 01 01 01 01 00 501 01 02 05 01 02 01 01 02 0
1 01 01 01 01 01 01 00 501 01 01 01 0
BBatt-ir-ii -w10 00 MB Pmnrn
OB
UNITSug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
WATERf 32622'
MDL3 012100 300 300 300 300 301 03 00 300 300 200 300 300 300 400 302 00 300 300 300 300 70
0 300 400 300 300 300 400 200 400 300 300 300 30
(Continued on next page)
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HALEY & ALDRICH INC
Client Sanqale ID MW_23B_WG091703_0001
GC/MS Volatlles
Lot-Sample # E3I180205 002 Work Order FOLQR1AA Matrix WATER
PARAMETER2 2 Dichloropropane1 1 DichloropropeneEthylbenzeneHexachlorobutadlene2 Hexanonelodometha neI sopropyl benzenep IsopropyltolueneMethylene chloride4 Methyl 2 pentanoneMethyl tert butyl etherNaphthalenen PropylbenzeneStyrene1 1 1 2 Tetrachloroethane1 1 2 2 TetrachloroethaneTetrachlo roetheneTetrahydrofuranToluene123 Tri chlorobenzene124 Trichloro
benzene111 Tnchloroethane112 TnchloroethaneTrichloro etheneTrichloro f luoromethane123 Tri chloropropane112 Tri chlorotrif luoro
ethane124 Trimethylbenzene135 TrimethylbenzeneVinyl acetateVinyl chlorideXylenes (total)
SURROGATEBromof luorobenzene1 2 Dichloroethane d4Toluene d8
RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
NDNDNDNDNDND
NDNDNDNDND
PERCENTRECOVERY112114111
REPORTINGLIMIT1 01 01 01 05 02 01 01 01 05 01 01 01 01 01 01 01 0101 01 01 0
1 01 01 02 01 01 0
1 01 05 00 501 0
RECOVERYLIMITS(75 - 130)(65 - 135)(80 130)
UNITSug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/L
MDL0 300 300 200 303 01 00 300 300 303 00 500 500 400 300 300 400 302 00 300 400 30
0 200 300 300 300 400 40
0 300 202 00 300 80
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HALEY & ALDRICH INC
Client Sample ID TRIP BLANK E3G280120
GC/MS Volatiles
Lot-Sample # E3I180205 003Date Sampled 09/02/03Prep Date 09/19/03Prep Batch # 3262567Dilution Factor 1Analyst ID 015590
PARAMETERAcetoneAcroleinAcrylonitrileBenzeneBromobenz eneBromochlo rome thaneBromodich loromethaneBromoformBromomethane2-Butanonen Butylbenzenesec-Butyl benzenetert-ButylbenzeneCarbon disulfideCarbon tetrachlorideChloroben zeneDlbromoch loromethaneChloroethane2 Chloroethyl vinyl etherChloroformChloromet hane2-Chlorotoluene4 Chlorotoluene1 2 Dibromo 3 chloro
propane1 2 DibromoethaneDibromome thane1 2 Dichlorobenzene1 3 Dichlorobenzene1 4 DichlorobenzeneDichlorodifluoromethane1 1 Dichloroethane1 2 Dichloroethanecis 1 2 Dichloroethenetrans 1 2 Dichloroethene1 1 Dichloroethene1 2-Dichloropropane
Work Order #Date ReceivedAnalysis EtotteAnalysis TTmroe
Instrument IDMethod
RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
NDNDNDNDNDNDNDNDNDNDNDND
FOLQW1AA09/18/0309/19/0315 09
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REPORTINGLIMIT1020201 01 01 01 01 02 05 01 01 01 01 00 501 01 02 05 01 02 01 01 02 0
1 01 01 01 01 01 01 00 501 01 01 01 0
Mattmjc10 00 MS ffimnm
OB
UNITSug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
WATERf 32622'
MDL3 012100 300 300 300 300 301 03 00 300 300 200 300 300 300 400 302 00 300 300 300 300 70
0 300 400 300 300 300 400 200 400 300 300 300 30
(Continued on next page)
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HALEY & ALDRICH INC
Client Sample ID TRIP BLANK E3G280120
GC/MS Volatiles
Lot-Sample # E3I180205 003 Work Order FOLQW1AA Matrix WATER
PARAMETER2 2 Dichloropropane1 1 DichloropropeneEthylbenz eneHexachlorobutadlene2 HexanonelodomethaneI aopropyl benzenep I sopropyl tolueneMethylene chloride4 Methyl 2 pentanoneMethyl tert butyl etherNaphthalenen PropylbenzeneStyrene1 1 1 2 Tetrachloroethane1 1 2 2 TetrachloroethaneTetrachlo roetheneTetrahydrofuranToluene123 Tri chlorobenzene124 Tri chloro
benzene111 Trichloroethane112 TrichloroethaneTrichloro etheneTrichloro f luoromethane1 2 3-Trichloropropane112 Tri chlorotrif luoro
ethane124 Trimethylbenzene135 TrimethylbenzeneVinyl acetateVinyl chlorideXylenes (total)
SURROGATEBromof luo robenzene1 2-Dichloroethane d4Toluene d8
RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
NDNDNDNDNDND
NDNDNDNDND
PERCENTRECOVERY112110109
REPORTINGLIMIT1 01 01 01 05 02 01 01 01 05 01 01 01 01 01 01 01 0101 01 01 0
1 01 01 02 01 01 0
1 01 05 00 501 0
RECOVERYLIMITS(75 130)(65 135)(80 - 130)
UNITSug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/Lug/L
ug/Lug/Lug/Lug/Lug/L
MDL0 300 300 200 303 01 00 300 300 303 00 500 500 400 300 300 400 302 00 300 400 30
0 200 300 300 300 400 40
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Boeing/CCI Olathe KS
Lot # E31170215
IIIII_ ANALYTICAL REPORT
IIIIIIIIIIIII
Haley & Aldrxch Inc
SEVERN TRENT LABORATORIES INC
Diane SuzukxProject Manager
September 24 2003
I1 EXECUTIVE SUMMARY - Detection HighlightsI E3I170215
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REPORTING ANAL YTICALPARAMETER RESULT LIMIT UNITS METHOD
MW_26C_COTTINGS_COMPOSITE 09/16/03 14 30 003
Trichloroethene 0 026 0 025 mg/L SW846 8260B
I• METHODS SUMMARY• E3I170215
I ANALYTICAL PREPARATI ONPARAMETER ___ _______ _____________________ METHOD________ METHOD
I Volatile Organics by GC/MS SW846 8260B SW846 1311/5030
References
• SW846 Test Methods for Evaluating Solid Waste Physical/Chemical™ Methods Third Edition November 1986 and its updates
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SAMPLE SUMMARYE3I170215
SAMPLED SAMPWO ft SAMPLEft CLIENT SAMPLE ID ____________________________________ DATE TIME
FOH2TFOH27FOH29FOH3FFOH3HFOH3K
KOTE(S)
001002003004005006
MW_23B_CUTTI NGSMW_22B_CUTTI NGSMW_26C_CUTTI NGS_COMPOSITEMW_30B_CUTTINGSMW_31B_CUTTINGSMW_32B/MW33B _CUTTINGS
09/16/0309/16/0309/16/0309/16/0309/16/0309/16/03
131314131313
503530452505
The analytical results of the samples listed above are presented on the following pagesAll calculations are performed before founding to avoid round off errors In calculated resultsResults noted as NO were not detected at or above the stated limitThis report must not be reproduced except in full without the written approval of the laboratoryResults for the following parameters are never reported on a dry weight basis color corrosivlty density flashpoint Ignitablllty layers odorpaint filter test pH porosity pressure reactivity redox potential specific gravity spot tests solids solubility temperature viscosity and weight
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HALEY & ALDRICH INC
Client Sample ID MW_23B_C DTTINGS
TCLP GC/MS Volatiles
Lot-Sample # E3I170215 001Date Sampled 09/16/03 13 50Leach Date 09/18/03Leach Batch # P326112Dilution Factor 1% Moisture
PARAMETERVinyl chloride1 1 DichloroetheneChloroform1 2 Dichloroethane2 ButanoneCarbon tetrachlondeTnchloroetheneBenzeneTetrachlo roetheneChloroben zene
SURROGATE4 Bromof luorobenzeneToluene d81 2 -Dichloroethane d4
NOTE(S)
Work Order fDate ReceivedPrep DatePrep BatcBa #
Analyst IE)Method
RESULTNDNDNDNDNDNDNDNDNDND
PERCENTRECOVERY97100104
FOH2T1AA Hattrax09/17/03 10 20 HE S&unm #09/18/03 analysis mate3261563 Analysis THume
015590 TTimmtt-iniiiiiiMiMill HD
SW846 826 OB
REPORTINGLIMIT UNITS MDL0 025 mg/L 0 00750 025 mg/L 0 00750 025 mg/L 0 00750 025 mg/L 0 0100 12 mg/L 0 0750 025 mg/L 0 00750 025 mg/L 0 00750 025 mg/L 0 00750 025 mg/L 0 0120 025 mg/L 0 0075
RECOVERYLIMITS(80 120)(75 125)(70 135)
SOLID326128509/23/0311 52
MSK
Analysis performed in accordance with USEPA Toxiclty Characteristic Leaching Procedure Method 1311
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HALEY t ALDRICH INC
Client Sample ID MW_22B_CDTTINGS
TCLP GC/MS Volatiles
Lot-Sample # E3I170215 002Date Sampled 09/16/03 13 35Leach Date 09/18/03Leach Batch # P326112Dilution Factor 1% Moisture
PARAMETERVinyl chloride1 1 DichloroetheneChloroform1 2 Dichl oroethane2 ButanoneCarbon te trachlorideTnchloro etheneBenzeneTetrachlo roetheneChloroben zene
SURROGATE4 BromofluorobenzeneToluene d81 2 Dichl oroethane d4
NOTK(S)
Work Order #Date Recer^edPrep DatePrep BatcBn $
Analyst IPMethod
RESULTNDNDNDNDNDNDNDNDNDND
PERCENTRECOVERY103103109
FOH271AA09/17/0309/18/033261563
015590SW846 826
REPORTINGLIMIT0 0250 0250 0250 0250 120 0250 0250 0250 0250 025
RECOVERYLIMITS(80 120)(75 125)(70 135)
MattnLx10 20 MB Baxm f
Amalysasanalysis
mateTCbnrie
Trnijafr miiiin-iinrt- HD
OB
UNITSmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L
SOLID326128509/23/0312 15
MSK
MDL0000000000
0075007500750100750075007500750120075
Analysis performed in eccordance with USEPA Toxicity Characteristic Leaching Procedure Method 1311
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HALEY & ALDRICH INC
Client Sample ID MW_26C_CDTTINGS_C»MPOSITE
TCLP GC/MS Volatiles
Lot-Sample # E3I170215 003Date Sampled 09/16/03 14 30Leach Date 09/18/03Leach Batch # P3 26112Dilution Factor 1% Moisture
PARAMETERVinyl chloride1 1 DichloroetheneChloroform1 2 Dichloroethane2 ButanoneCarbon tetrachlorideTrichloro etheneBenzeneTetrachlo roetheneChlorobenzene
SURROGATE4 Bromof 1 uorobenzeneToluene d81 2 Dichloroethane d4
NOTE(S)
Work Order #Date ReceivedPrep DatePrep BatcHu ft
Analyst IPMethod
RESULTNDNDNDNDNDND0 026NDNDND
PERCENTRECOVERY104107107
FOH291AA Matmuc09/17/03 10 20 MS Kmnm #09/18/03 Analysis Usate3261563 Aimalysis TEhrme
015590 1Timn»tt- IT min»»iMitt- HD
SW846 826 OB
REPORTINGLIMIT UNITS MDL0 025 mg/L 0 00750 025 mg/L 0 00750 025 mg/L 0 00750 025 mg/L 0 0100 12 mg/L 0 0750 025 mg/L 0 0075(ID SD25 mg/L 0 00750 025 mg/L 0 00750 025 mg/L 0 0120 025 mg/L 0 0075
RECOVERYLIMITS(80 120)(75 125)(70 135)
SOLID326128509/23/0312 39
MSK
Analysis performed In accordance with USEPA Toxicity Characteristic Leaching Procedure Method 1311
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HALEY & ALDRICH INC
Client Sample ID MW_30B_COTTINGS
TCLP GC/MS Volatiles
Lot-Sample # E3I170215 004Date Sampled 09/16/03 13 45Leach Date 09/18/03Leach Batch # P326112Dilution Factor 1% Moisture
PARAMETERVinyl chloride1 1 DichloroetheneChloroform1 2 Dichloroethane2 But anon eCarbon tetrachlorideTnchloroetheneBenzeneTetrachlo roetheneChloroben zene
SURROGATE4 BromofluorobenzeneToluene d81 2 Dichloroethane d4
NOTE(S)
Work Order fDate ReceorswsdPrep DatePrep Batcto #
Analyst intMethod
RESULTNDNDNDNDNDNDNDNDNDND
PERCENTRECOVERY9999116
FOH3F1AA Mateuc09/17/03 10 20 MB Hmran09/18/03 Amalysi
*us IBstte
3261563 analysis TEbnrie
015590 lastttwnSW846 826 OB
REPORTINGLIMIT UNITS0 025 mg/L0 025 mg/L0 025 mg/L0 025 mg/L0 12 mg/L0 025 mg/L0 025 mg/L0 025 mg/L0 025 mg/L0 025 mg/L
RECOVERYLIMITS(80 120)(75 125)(70 135)
mmtr HD
MDL0 00750 00750 00750 0100 0750 00750 00750 00750 0120 0075
SOLID326128509/23/0313 02
MSK
Analysis performed in iccordance with USEPA Toxicity Characteristic Leaching Procedure Method 1311
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HALEY & ALDRICH INC
Client Sample ID MW_31B_CDTTINGS
TCLP GC/MS Volatiles
Lot-Sample # E3I170215 005Date Sampled 09/16/03 13 25Leach Date 09/18/03Leach Batch # P326112Dilution Factor 1* Moisture
PARAMETERVinyl chloride1 1 DichloroetheneChloroform1 2 Dichloroethane2 ButanoneCarbon tetrachlorideTrichloroetheneBenzeneTetrachloroetheneChloroben zene
SURROGATE4 Bromof luorobenzeneToluene d81 2 Dichloroethane d4
NOTE(S)
Work Order *Date ReceivedPrep DatePrep Batch #
Analyst IBMethod
RESULTNDNDNDNDNDNDNDNDNDND
PERCENTRECOVERY105109119
FOH3H1AA Matin09/17/03 10 20 MS Hn
LK
mm f09/18/03 Analysis mate3261563 Analysis TCbnme
015590 ImstmamEJUitt HDSW846 826 OB
REPORTINGLIMIT UNITS0 025 mg/L0 025 mg/L0 025 mg/L0 025 mg/L0 12 mg/L0 025 mg/L0 025 mg/L0 025 mg/L0 025 mg/L0 025 mg/L
RECOVERYLIMITS(80 120)(75 125)(70 135)
MDL0 00750 00750 00750 0100 0750 00750 00750 00750 0120 0075
SOLID326128509/23/0313 25
MSK
Analysis performed In accordance with USEPA Toxicity Characteristic Letching Procedure Method 1311
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HALEY & ALDRICH INC
Client Sample ID MW_32B/M W33B_CUTTINGS
TCLP GC/MS Volatiles
Lot-Sample # E3I170215 006Date Sampled 09/16/03 13 05Leach Date 09/18/03Leach Batch # P326112Dilution Factor 1% Moisture
PARAMETERVinyl chloride1 1 DichloroetheneChloroform1 2 Dichloroethane2 ButanoneCarbon tetrachlorideTrichloro etheneBenzeneTetrachlo roetheneChloroben zene
SURROGATE4 Bromof luorobenzeneToluene d81 2 Dichloroethane d4
NOTE(S)
Work Order #Date Recex^rodPrep DatePrep BatcBn $
Analyst IPMethod
RESULTNDNDNDNDNDNDNDNDNDND
PERCENTRECOVERY106107109
FOH3K1AA09/17/0309/18/033261563
015590SW846 826
REPORTINGLIMIT0 0250 0250 0250 0250 120 0250 0250 0250 0250 025
RECOVERYLIMITS(80 120)(75 125)(70 135)
Mattntx10 20 MS Hum t
AmaJLysisftmallyraim
XnnsttjnmOB
UNITSmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L
nen
natteTriune
att ED
SOLID326128509/23/0313 49
MSK
MDL0000000000
0075007500750100750075007500750120075
Analysis performed In accordance with USEPA Toxlclty Characteristic Leaching Procedure Method 1311