UNCLASSIFIED AD NUMBER - apps.dtic.milFig. 2 HBX-3 -Density-exposure time, 250 Kvcp, M film Fig. 3...
Transcript of UNCLASSIFIED AD NUMBER - apps.dtic.milFig. 2 HBX-3 -Density-exposure time, 250 Kvcp, M film Fig. 3...
UNCLASSIFIED
AD NUMBER
AD236687
NEW LIMITATION CHANGE
TOApproved for public release, distributionunlimited
FROMDistribution authorized to U.S. Gov't.agencies and their contractors;Administrative/Operational Use; MAR 1960.Other requests shall be referred to NavalOrdnance Labs., Silver Spring, MD.
AUTHORITY
USNOL ltr, 29 Aug 1974
THIS PAGE IS UNCLASSIFIED
128172
NAVORD REPORT 6806
"FILE COPYa*" *A*t I wth€l•m eat
/ RADIOGRAPHY OF CAST HIGH EXPLOSIVES (U)
15 MARCH 1960
OF
/U. S. NAVAL ORDNANCE LAaORATORY
WHITE OAK/MARYLAND
'-
Naval Ordnance Lab., Wr~te Oak N~AVOiRLRADIO~rAHY OF CAST HIGH EXPLOSIVES. 6806
NAVORD Report 6806_i
RADIOGRAPHY OF CAST HIGH EXPLOSIVES (U)
Prepared by:
R. A. Youshaw, W. R. Maddy and E. L. Criscuolo
ABSTRACT: Data on the radiographic techniques forthe inspection of cast high explosives at 150, 250and 2000 Kvp are presented in tabular and graphicalform to assist the radiographer in the selection ofa suitable technique. Sensitivity limits for variousconditions of explosive encasement have also beende-ermined. Inert materials for use as penetrametershave been investigated and nylon was found to besatisfactory.
Published May 1960
U. S. NAVAL ORDNANCE LABORATORYWhite Oak, Silver Spring, Maryland
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NAVORD Report 6806 15 March 1960
The purpose of this report is to present information onradiographic techniques for the inspection of cast highexplosives. It is intended as a practical guide for usewith radiographic specifications.
This work was performed by the Nondestructive Analysis Groupof the Physics Research Department of the Naval OrdnanceLaboratory and by the Research and Development Division ofthe Naval Weapons Station, Yorktown, Virginia, for ReU3aand QC of the Bureau of Ordnance (Bureau of Naval Weapons).That portion of the work accomplished by the Naval OrdnanceLaboratory was funded under Task NO 301-664/43004/01040.
Two other documents are also in preparation, (1) OD 15533,Reference Radiographs for the Inspection of Cast HighExplosives, and (2) A Method for Controlling the Quality ofRadiographic Inspection of High Explosives.
The work on this task is Unclassified.
JOHN A. QUENSE'Captain, USNActing Commander
By direction [
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NAVORD Report 6806
ACKNOWLEDGIIENT
The authors wish to thank Mr. Baxter C. Carr, Jr.,Mr. Robert B. Smoot, and the members of the Researchand Development Division of the Naval Weapons Station,Yorktown, Virginia, for their cooperative efforts onthis task. Their skill and ability to produce therequired explosive samples made possible the successfulcompletion of this task assignment.
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CONTENTS
Page
INTRODUCTION 1
PREPARATION OF MATERIALS 1
EXPERIMENTAL PROCEDURE 2
TECHNIQUE AND SENSITIVITY CURVES 2
EQUILIBRIUM HALF VALUE LAYERS AND ABSORPTIONCOEFFICIENTS 3
RADIOGRAPHIC EFFECT OF STEEL CONTAINEPS 4
INERT PENETRAMETERS 5
SUMMARY 5
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ILLUSTRATIONS
Fig. 1 Sketch - The cast explosive penetrameter
Fig. 2 HBX-3 - Density-exposure time, 250 Kvcp, M film
Fig. 3 HBX-3 - Technique curve for 250 Kvcp, M film
Fig. 4 HBX-3 - Sensitivity loop at 250 Kvcp, M film
Technique and Sensitivity Curves
Fig. 5 HBX-3 - 250 Kvcp, M film
Fig. 6 Comp B - 150 Kvp, M film
Fig. 7 Comp B - 250 Kvcp, M film
Fig. 8 Comp B - 2000 Kvp, M film
Fig. 9 Comp B - 150 Kvp, AA film
Fig. 10 Comp B - 250 Kvcp, AA film
Fig. 11 Comp B - 2000 Kvp, AA film, .120" Pb filter
Fig. 12 H-6 - 150 Kvp, M film
Fig. 13 H-6 - 250 Kvcp, M film
Fig. 14 H-6 - 2000 Kvp, M fVlm, .120" Pb filter
Fig. 15 H-6 - 150 Kvp, AA film
Fig. 16 H-6 - 250 Kvcp, AA film
Fig. 17 H-6 - 2000 Kvp, AA film .120" Pb filter
Technique Curves
Fig. 18 Comp B - 2 Mev, 200,m a, M film
Fig. 19 H-6 - 2 Mev, 200 /4a, M film
Fig. 20 Comp B - 2 Mev, 200 A"a. AA film
Fig. 21 H-6 - 2 Mev, 200 la a, AA film
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NAVORD Report 6806 'j
ILLUSTRATIONS continued
Techntque and Sensitivity Curves
Fig. 22 H-6 - 250 Kvcp, AA film, 1/8" steel front & back
Fig. 23 H-6 - 250 Kvcp, AA film, 1/4" steel front & back
Fig. 24 H-6 - 250 Kvcp, AA film, 1/2" steel front & back
Fig. 25 H-6 - 2000 Kvp, M film, 1/4" steel front & back
Fig. 26 H-6 - 2000 Kvp, M f-1m, 3/4" steel front & back
Fig. 27 Exposure factors to compensate for attenuation byvarious thickness steel walls - 250 Kvcp and 2000 Kvp
aI
TABLES
Table I Explosive Materials
Table II Sensitivities for Different Thicknesses ofComp B and H-6
Table III Half Value Layers for Explosive Materials atDifferent Energies
Table IV Linear Absorption Coefficients for ExplosiveMaterials
Table V Radiographic Sensitivities for H-6 with Steel Wallsof Various Thicknesses
Table VI Sensitivity Comparison of Magnesium and ExplosivePenetrameters - 250 Kvcp, H-6
Table VII Sensitivity Comparison of Nylon and ExplosivePenetrameters
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F . NAVORD Report 6806
RADIOGRAPHY OF CAST HIGH EXPLOSIVES
INTRODUCTION
1. The performance requirements of explosive ordnance arebecoming more stringent. The evolution of missile warheadswith shaped charge characteristics has placed added emphasisupon the inspection of the explosive load. Although radiog-rapiiv has been used extensively for the nondestructive inspec-tion of explosive ordnance, very little technical data has beenpublished ?, the X-ray absorption characteristics of explosive"•.Aterip.ls.f/ The object of this investigation was to determine
-. absorption characteristics of the common cast explosives-c different X-ray energies and to determine the capabilitiesand limitations of X-ray inspection as applied to explosiveordnance.
PREPARATION OF MATERIALS
2. The explosives used in this investigation are listedin Table I along with the .ensity and aluminum content of tnematerial. It can be seen that the material density increaseswith the increase in aluminum c~ontent. Since the absorption ofX-rays by material is a function of density (also atomic number)it is to be expected that these explosives will differ inabsorption characteristics. In order to obtain experimentaldata special castings were made from these explosives. Eachmaterial was vacuum cast in 1-1/2-inch thick slabs which wereindividually X-ray inspected to assure sound castings. Enoughslabs were made from each material so that approximately 17inches could be attained by stacking.
3. One slab of each type explosive was used as a penetra-meter. A number of flat-bottomed holes with the diameter twice
l_/ OP 1681 Handbook of Ordnance Radiograpny, Bureau of Ordnance,7 June 1946.
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NAVORD Report 6806
the depth were drilled into these slabs. Figure 1 illustratesthe arrangement and dimensions of the holes. Sensitivity wascalculated in the usual manner, where the depth of the hole isexpressed as a percentage of the total thickness X-rayed.V/3i
EXPERIMENTAL PROCEDURE
4. Experience has shown that technique and sensitivitycurves present the maximum information concerning radiographictechnique for a particular material and X-ray energy. Suchcurves were obtained by exposing various thicknesses of theexplosive material (3/4" to 17") to X-ray energies of 150, 250and 2000 Kvp for varying periods of time so that film densitiesfrom 0.5 to 6.0 were obtained. The exposure time was thencorrelated with the film density for each thickness as shownin Figure 2. From this graph the technique curve was obtained,see Figure 3.
5. The penetrameter was included in each exposure andradiographic sensitivity was determined from the smallest holeperceptible. This information was plotted on a graph ofthickness versus exposure time and points of equal sensitivitywere connected to form the sensitivity loop shown in Figure 4.Since the technique curve and sensitivity loop have an identicalabscissa and ordinate, they are combined to form the techniqueand sensitivity curve, Figure 5.
T&CHNIQUE. AND SENSITIVITY CURVES
6. Technique curves were made for the materials listedin Table I at 150, 250 and 2000 Kvp and 2 million volts constantpotential. A comparison of the data revealed a similarity inthe X-ray absorption characteristics of Comp B and TNT, the twomaterials which do not contain aluminum. A similarity was alsonoted between H-6, HBX-1 and HBX-3, materials containing aluminum.Because of the similarities in absorption characteristics,Comp B and H-6 were selected as representative of each group.
7. The technique and sensitivity curves for Comp B andH-6 with fine and medium grained film at 150 Kvp, 250 Kvcpand 2000 Kvp are shown in Figures 6 through 17. Technique
_ MIL-STD-271A - Military Standards for Nondestructive TestingRequirements for Metals.
3_/ ASTM E7-141-59T.
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curves are snown in Figures 18 through 21 for two million voltsconstant potential. Although the technique curves for the twomaterials differ at each of the above energies the sensitivityvalues are almost identical. Radiographically, these materialsare characterized by a very wide 2% sensitivity loop whichencompasses a film density range of 05 to 6.0. Because 2%was obtained over such a wide range, the 1% loop was consideredmore informative. This loop extends through a density range ofapproximately 0.75 through 5.0, however, the finest sensitivi-ties were obtained with film densities between 3.0 and 4.0.
8. Table II presents the sensitivities which were obtainedfor different thicknesses of Comp B and H-6 at the various X-rayvoltages. Equivalent sensitivities were obtained for Com~p Band H-6 with both slow and medium speed film. The values forless than five inches of explosive indicates that sensitivitiesat least this fine can be obtained, however, the difficulty ofdrilling small flat-bottomed holes prevented the determinationof the lower limit of radiographic sensitivity for these smallthicknesses. That greater differences in sensitivity were notobtained between the fine and medium grained film is thoughtto be due to the comparatively large penetrameter increments.
EQUILIBRIUM HALF VALUE LAYERSAND ABSORPTION COEFFICIENTS
9. The equilibrium half value layer is defined as thethickness of absorber that will reduce the intensity of an X-raybeam to cne-half. It is often used to determine the exposuretime for some thicknesses of material. The number of halfvalue layers of material to be radiographed and the intensityof the X-ray source determines the X-ray intensity transmittedthrough the absorber and received by the film. The exposuretime can then be estimated from the dose response of the film.
10. From the technique cur':es the equilibrium half valuelayers for each of the X-ray voltages were determined and arepresented in Table III. A comparison of the half value layersreveals very little difference between the explosive materialsat 2000 Kvp (2 million volts half wave rectified) and 2 Mev(2 million volts constant potential). As expected, at 250 Kvcpand 150 Kvp there is an appreciable difference between thematerials containing aluminum and those containing no aluminum.
11. Because the differences are small between the halfvalue layers of the various types of explosives at high energies,a common radiographic technique should be suitable. However,
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at lower energies the larger differences between the half valuelayers of the various explosives necessitates a separate tech-nique for each material.
12. The linear aborption coefficient for each materialcan be determined at the different X-ray voltages by utilizingthe half value layer data in the following equation
.693 (1)HVL
where A- = linear absorption coefficientHVL = half value layer
Table IV lists the linear absorption coefficients for each ofthe explosive materials at the different energies.
RADIOGRAPHIC EFFECT OF STEEL CONTAINERS
13. In ordnance application explosives are usually encasedin steel containers. The walls of these containers lengthenthe exposure time and affect the quality of the image. Todetermine the extent of these effects, technique and sensitivitycurves were made for H-6 at 250 Kvcp and 2000 Kvp with variousthicknesses of steel added to each side of the explosive.Figures 22, 23 and 24 show such curves at 250 Kvcp with 1/8",1/4" and 1/2" of steel added to each side of the explosive.Similar curves at 2000 Kvp with the addition of 1/4" and 3/4"of steel are shown in Figures 25 and 26. These curves werecompared to those made at the same energies but witbnut theaddition of steel, Figures 14 and 16. It was found that thegreatest effect was increased exposure time; there was littlechange in radiographic sensitivity. In determining radiog-raphic sensitivity only the thickness of explosive was con-sidered.
14. As shown in Figures 22 through 26, a 1% sensitivityloop was obtained for all of the conditions described. Table Vlists the sensitivities obtained with each thickness of explosivefor each set of conditions.
15. The increase in exposure time cannot readily bepredicted by utilizing the half value layer of the steel sinceit is the first rather than the equilibrium half value layerwhich applies to composites. It was possible however from areview of the experimental data to derive exposure factors tocompensate for the steel walls. For example, at 250 Kvcp the
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addition of 1/4" of steel increases the exposure time by afactor of four. The exposure factors for the addition of thevaricus thicknesses of steel to both sides of the explosivewere obtained by Comparing the technique curves for H-6 withand without steel absorbers, Figure 27.
INbRT PENETBAMETERS
16. Military specifications require that penietrametersbe made of a material radiographically similar to that beingexamined; this is usually done by fabricating the penetrameterfrom a material of approximately the same composition as theobject being examined. In the case of explosives this createsa safety hazard since small pieces of explosive materials areeasily broken or mislaid. Also, it is not desirable to handlesuch material in its "raw" state. For these reasons, penetra-meters for use with explosives should be made from a radiog-raphically similar but inert material. From a considerationof the atomic numbers and densities, magnesium and nylon werechosen for study; these materials are durable, easily machinedand are commercially available.
17. The sensitivities obtained with magnesium andexplosive penetrameters under identical conditions at 250 Kvcpare presented in Table VI. The sensitivities obtained withmagnesium are consistently lower than those obtained withexplosive penetrameters. This misleading differenc. in sensi-tivity makes magnesium undesirable as a substitute materialfor explosives.
18. The sensitivities obtained with nylon and explosivepenetrameters under identical conditions with Comp B and H-6at 250 Kvcp and 2000 Kvp are presented in Table VII. Althoughthe sensitivities differed under some conditions, the differenceis not large and does not lead to false indications of satis-factory sensitivity. For these reasons nylon is a satisfactorysubstitute penetrameter material. It is recommended that nylonpenetrameters be used for production inspection of explosives.
SUMMARY
19. This study of the X-ray absorption characteristicsof cast explosives revealed a similarity between the explosiveswhich contain aluminum and also a similarity between thosewhich do not contain aluminum. Comp B and H-6 were found tobe representative of these two groups. It was determined thatthe explosives which contain aluminum have a greater absorptionfor X-rays than those which do not contain aluminum.
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20. Sensitivities better than 2% were obtained with allthicknesses of explosive materials at each of the X-ray energiesconsidered. Sensitivities of 1/2% were obtained in the thick-ness range of 8 to 17 inches at 2000 Kvp with the finestsensitivities being obtained at film densities between 3.0 and4.0.
21. The addition of steel walls to the explosive materialsdegrades the radiographic sensitivity. However, sensitivitiesfiner than 1% were still obtained at 2000 Kvp for all thicknessesof explosive between 3-1/2" and 17" with 3/4' of steel added toeach side of the explosive. Exposure factors were derivedfrom the experimental data which enabled a correction in theexposure time to compensate for the attenuation by steel wallsof varied thickness.
22. Nylon was found to be suitable as a penetrametermaterial for cast explosives. Although the sensitivitiesobtained with nylon penetrameters are not in complete agreementwith those obtained with explosive penetrameters, the differenceis small and not misleading.
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TABLE I
Explosive MaterialsExplosives Material Aluminum Content
Density (percent)
TNT 1.65 0
Comp B 1.72 0
HBX-i 1.76 17
H-6 1.80 21
HBX-3 1.89 35
TABLE II
Sensitivities for Different Thicknesses of Comp Band H-6
Thickness of Sensitivity Obtained atExplosive 350 Kvp 250 Kvc- 2000 Kvp
(inches) (percent) (percent) (percent)
2.3 0.85 o.85 1.7
3.8 1.05 1.05 1.05
5.3 0.75 0.75 0.75
8.3 0.72 0.48
11.3 0.53 0.35
74-03 o.42
17.3 0.35
NOTE: Equivalent sensitivities were obtained for Comp B and H-6with both slow and medium speed film.
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TABLE III
Half Value Layers for Explosive Materialsat Different Energies (inches)
Material X-ray Voltage150 Kvp 250 Kvcp 2000 Kvp 2 Mev
TNT 1.45 I.60 3.0 3.2
Comp B 1.40 1.55 2.9 3.0
HBX-I 1.2 1.45 2.95 3.0H-6 1.15 1.5 2.95 2.95
HBX-3 1.1 1.4 2.9 2.95
TABLE IV I LLinear Absorption Coefficients for Explosive Materials
cm-1
X-ray Vo.lageMaterial 515 Kvp 25U Avcp 2eU00KVp 2e
TNT .188 .171 .091 .085
Comp B .195 .176 .094 .091
HBX-1 .228 .188 .0925 .091
H-6 .237 .182 .0925 .0925
HBX-3 .248 .195 .094 .0925
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NAVORD Report 6806
TABLE V
Radiographic Sensitivities for H-6 withSteel Walls of Various Thicknesses
Thickness of Thickness of Steel Added to Each SideExplosive off(inohes) 1/8" 1/4" 1/2" 3/4"
% Sensitivity obtained at 250 Kvcp
2.3 0.85 1.7 1.7 1.7
3.8 1.05 1.05 1.05 1.05
5.3 0.75 0.75 0.75 0.75
8.3 0.48 0.72 0.72 0.72
11.3 0.35 -- 0.88 ....
% Sensitivity obtained at 2000 Kvp
2.3 1.7 1.7 1.7 -- 1.7
3.8 1.05 1.05 1.05 -- 1.05
5.3 0.75 0.75 0.75 -- 0.75
8.3 0.72 0.72 0.72 -- 0.72
11.3 0.53 -- 0.88 ..--
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NAVORD Report 6806
TABLE VI
Sensitivity Comparison of Magnesium andExplosive Penetrameters--250 Kvcp - H-6
Thickness of Explosive Penetrameter Magnesium Penetra-Explosive Sensitivity meter Sensitivity
(inches) (percent) (percent)
2.3 1.28* 1.19
3.8 1.23 1.05
5.3 1.22 1.05
8.3 1.12 0.97
*All of the sensitivities listed above are the averageobtained from several films
TABLE VII
Sensitivity Comparison of Nylon andExplosive Penetrameters
Thickness of Comp B H-6Explosive Explosive Nylon Explosive Nylon
(inches) (percent) (percent) (percent) (percent)
250 Kvcp
2.3 1.7 1.7 1.7 1.73.8 1.1 1.1 1.1 1.15.3 0.8 0.8 0.8 0.88.3 0.7 1.0 0.7 0.7
2000 Kvp
2.3 1.7 1.7 0.9 0.93.8 1.1 1.1 1.1 1.15.3 0.8 0.8 0.8 0.88.3 0.5 0.5 0.5 0.711.3 0.5 0.5 o.4 0.414.3 0.4 0.6 0.4 0.417.3 0.4 o.4 0.4 0.5
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NAVORD REPORT 6806
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NAVORO REPORT 6806
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NAVORD REPORT 680610,000
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NAVORO REPORT 6806
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NAVORD REPORT 6806
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NAVORD REPORT 680610,000 _- -- - r_____
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NAVORD REPORT 6806
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NAVORD REPORT 68061,000.~.'-*.-
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NAVORD REPORT 6806
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FIG. 24 TECHNIQUE AND SENSITIVITY CURVE FOR H-6
NAVORD REPORT 6806
:Z: -7-
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0t 2/ 4 6l 8 tI 12 14 16 0 22 2 6 2THCKES OF 1-(ICHS
FIG. 25HE TEHNQEFN STENSITIVIDTY CURVTE FRORT AND-6
NAVORD REPORT 680610,000 - -.
I0 H~7 i III I I
LLLL ~ ~ ~ - ----LL - ------ --- L
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1.1 I.'LW5T IMII I I I I I I
FIG. 26~ TECHIQU AND SESITVIYEUREEORH-
_ __ _ ___ _ _O .2 O " b F LT E R S T N D A D D E E LO M E N
NAVORD REPORT 6806
-250 KVCP
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