Tray Dryer Experiment

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ABSTRACT In this experiment, we use tray dryers to dry the wet sample. We choose the tea herbs as our sample because we believe that tea herbs requires short drying time, and the moisture content will decrease faster with time. The measurement of the moisture content is based on the weight of the sample which inversely proportional with the temperature & time. Thus, we can determine the drying rate of the sample. Based on the data from the experiment, the mass and moisture content is decreasing with time, whereas the drying rate is varying rapidly with time. INTRODUCTION Drying is the process of thermally removing volatile substances (e.g., moisture) to yield a solid product. Mechanical methods for separating a liquid from a solid are not considered in thermal drying. When a wet solid is subjected to thermal drying, two processes occur simultaneously; first is the transfer of energy, mostly as heat from the surrounding

Transcript of Tray Dryer Experiment

Page 1: Tray Dryer Experiment

ABSTRACT

I n th is exper iment , we use t ray d ryers to d ry the wet sample .

We choose the tea herbs as our sample because we be l ieve tha t tea

herbs requ i res shor t d ry ing t ime, and the mo is tu re con ten t w i l l

dec rease fas te r w i th t ime. The measurement o f the mo is tu re con ten t

i s based on the we igh t o f the sample wh ich inverse ly p ropor t iona l

w i th the tempera tu re & t ime. Thus , we can de te rmine the d ry ing ra te

o f the sample . Based on the da ta f rom the exper iment , the mass and

mo is tu re con ten t i s decreas ing w i th t ime, whereas the d ry ing ra te i s

va ry ing rap id ly w i th t ime.

INTRODUCTION

Dry ing i s the p rocess o f the rma l l y remov ing vo la t i l e subs tances

(e .g . , mo is tu re ) to y ie ld a so l id p roduc t . Mechan ica l methods fo r

separa t ing a l i qu id f rom a so l id a re no t cons idered in therma l d ry ing .

When a wet so l id i s sub jec ted to therma l d ry ing , two p rocesses occur

s imu l taneous ly ; f i r s t i s the t rans fe r o f energy , mos t l y as hea t f rom

the sur round ing env i ronment to evapora te the sur face mo is tu re , and

second i s the t rans fe r o f in te rna l mo is tu re to the sur face o f the so l id

and i t s subsequent evapora t ion due to the f i r s t p rocess .

Severa l t ypes o f d ryers a re used in d i f fe ren t f i e lds and

spec ia l t i es . The common type o f d ryer in many indus t r ia l

app l i ca t ions tha t invo lve d ry ing opera t ion i s t ray d ryers (o r cab ine t

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dryers ) . The d ryers a re made o f t rays he ld in a cab ine t , wh ich i s

connec ted to a source o f hea ted a i r by gas , d iese l o r b iomass . The

food , wh ich i s to be d r ied , i s sp read ou t , genera l l y qu i te th in ly , on

t rays wh ich the d ry ing takes p lace . Hea t ing may be by an a i r cu r ren t

sweep ing ac ross the t rays , by conduc t ion f rom hea ted t rays o r

hea ted she lves on wh ich the t rays l i e , o r by rad ia t ion f rom hea ted

sur faces . Mos t t ray d ryers a re hea ted by a i r , wh ich a lso removes the

mo is t vapours . The tempera tu re o f amb ien t a i r i s con t ro l led by

thermos ta t wh ich i s usua l l y se t in the range o f 50 to 700 °C. The a i r

en te rs the bo t tom o f the chamber be low the t rays and then r i ses ,

th rough the t rays o f food be ing d r ied , and ex i t s f rom an open ing in

the top o f the chamber . F resh a i r i s a l lowed to en te r the cab ine t and

mo is t a i r i s exhaus ted by us ing a dehumid is ta t to con t ro l an exhaus t

fan and a i r i n take shu t te rs . The d ryer t rays a re t igh t - f i t t i ng in the

cab ine t to p reven t a i r f rom bypass ing the mate r ia l to be d r ied .

Depend ing upon the food and the des i red f ina l mo is tu re , d ry ing t ime

may be o f the o rder o f 10 o r even 20 hours . T ray d ryers requ i re low

cap i ta l and ma in tenance cos ts bu t have re la t i ve ly poor con t ro l and

p roduces more var iab le p roduc t qua l i t y .

However , i n rec i rcu la t ion des igns , the mo is tu re laden a i r , a f te r

evapora t ing wate r f rom food , wou ld have to be d r ied be fo re be ing

undergo rec i rcu la t ion , o r e lse i t wou ld soon become sa tu ra ted and

fu r ther d ry ing o f the food wou ld s top . In such a case pass ing i t

th rough a des iccan t such as a bed o f s i l i ca ge l , o r condens ing

mo is tu re ou t by pass ing the mo is t a i r over co ld p la tes o r co i l s cou ld

d ry the a i r . No te a lso tha t i f we a re no t go ing to d ry the exhaus t a i r

fo r rec i rcu la t ion , then the exhaus t ven t shou ld no t be c lose to the

f resh a i r i n take a rea , o therw ise the mo is t exhaus t a i r w i l l be d rawn

back th rough the d r ie r and d ry ing e f f i c iency w i l l be los t .

Thermometers a re ins ta l led w i th the sens i t i ve e lements d i rec t l y in

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t he ma in a i r cu r ren t approach ing the d ry ing t rays , and o f ten a lso in

the a i r cu r ren t leav ing t rays .

One o f the mos t impor tan t p rob lems encounte red i s no t to supp ly the

same dry ing ra te a t the a l l pos i t i on w i th in the t ray d ryers . The o ther

i s the fas t d ry ing o f food in the pos i t ion where the a i r f i r s t en te rs to

the sys tem and the s low d ry ing o f food in the o ther pos i t ion .

There fo re , add i t iona l hea te rs and fans may be p laced above o r

a longs ide the t rays to inc rease the ra te o f d ry ing . T ray d ryers a re

used fo r sma l l - sca le p roduc t ion o r fo r p i lo t -sca le work .

OBJECTIVES

The purpose o f th i s exper iment i s to de te rmine the d ry ing ra te

o f the sample by d ry ing method us ing t ray d ryer bes ides lea rn to use

and opera te the t ray d ryer .

THEORY

Dry ing occurs w i th the he lp o f evapora t ion by supp ly ing hea t to

the wet feeds tock . There a re two op t ions fo r med ium o f hea t t rans fe r

tha t i s th rough convec t ion by d i rec t d r ie rs o r conduc t ion by con tac t

o r ind i rec t d r ie rs . The remova l o f wa te r f rom dry ing i s to inh ib i t the

g rowth o f m ic roorgan isms and there fo re the food i s we l l p reserved

bes ides reduc ing the we igh t and bu lk o f food fo r cheaper t ranspor t

and s to rage . When car r ied ou t co r rec t l y , any a l te ra t ion o f nu t r i t i ona l

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qua l i t y , co lour , f l avour and tex tu re o f rehydra ted foods w i l l no t be

a f fec ted too much .

Dry ing methods and p rocesses can be c lass i f i ed as ba tch ,

where the mate r ia l i s inser ted in to the d ry ing equ ipment and d ry ing

p roceeds fo r a g iven per iod o f t ime, o r as con t inuous , where the

mate r ia l i s con t inuous ly added to the d ryer and d r ied mate r ia l

con t inuous ly removed. Dry ing p rocesses can a lso be ca tegor ized

accord ing to the phys ica l cond i t ions used to add hea t and remove

wate r vapour . In the f i r s t ca tegory , hea t i s added by d i rec t con tac t

w i th hea ted a i r a t a tmospher ic p ressure , and the wate r vapour

fo rmed i s removed by the a i r . In vacuum dry ing , the evapora t ion o f

wa te r p roceeds more rap id ly a t low p ressures , and the hea t i s added

ind i rec t l y by con tac t w i th a meta l wa l l o r by rad ia t ion ( low

tempera tu res can a lso be used under vacuum fo r ce r ta in mate r ia ls

tha t may deco lour i ze o r decompose a t h igher tempera tu res ) . In

f reeze d ry ing , wa te r i s sub l imed f rom the f rozen mater ia l .

The f i r s t cons idera t ion in se lec t ing a d ryer i s i t s operab i l i t y ;

above a l l e l se , the equ ipment mus t p roduce the des i red p roduc t in

the fo rm a t the des i red ra te . The qua l i t y requ i red in a f in i shed

p roduc t , and i t s necessary phys ica l charac te r i s t i cs , a re de te rmined

by i t s end use . The f ina l cho ice i s then made on the bas is o f cap i ta l

and opera t ing cos ts . A t ten t ion mus t be pa id , however , to the cos ts o f

the en t i re i so la t ion sys tem, no t jus t the d ry ing un i t a lone .

Therma l l y sens i t i ve mate r ia ls mus t be d r ied a t low tempera tu re

under vacuum, w i th a low- tempera tu re hea t ing med ium, o r ve ry

rap id ly . The d ryer mus t a lso opera te re l iab ly , sa fe ly , and

economica l l y . Opera t ion and ma in tenance cos ts mus t be excess ive ;

po l lu t ion mus t be con t ro l led ; energy consumpt ion mus t be min im ised .

As fa r as the d ry ing opera t ion i t se l f i s concerned , ad iaba t i c d ryers

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are genera l l y less expens ive than non-ad iaba t i c d ryers , in sp i te o f

the lower therma l e f f i c iency o f ad iaba t i c un i t s .

Un fo r tuna te ly there i s usua l l y a lo t o f dus t ca r ry over f rom ad iaba t i c

d ryers , and these en t ra ined par t i c les mus t be removed a lmos t

quan t i ta t i ve ly f rom the d ry ing gas .

In herbs and med ic ina l i ndus t ry , mos t med ic ina l and cu l ina ry

herbs a re so ld d r ied . When d ry ing la rge quan t i t i es o f herbs fo r

commerc ia l sa le , g rowers shou ld use a fo rced-a i r d ryer to p reserve

the i r co lo r , f l avour , o i l con ten t , and med ic ina l p roper t ies . To ach ieve

th is , good a i r c i r cu la t ion w i th in the d ryer i s impor tan t , as i t reduces

d ry ing t ime and a l lows the use o f lower tempera tu res , bo th o f wh ich

can p reven t the degrada t ion o f chemica l cons t i tuen ts dur ing the

d ry ing p rocess . There- fo re , dependab le tempera tu re con t ro l and the

ab i l i t y to p rov ide h igh a i r f l ow th roughout the p lan t mate r ia l a re

impor tan t . Dry ing tempera tu res and t imes d i f fe r by p lan ts , and p lan t

par ts , thus mos t herbs shou ld be d r ied a t low tempera tu res , idea l l y

a round 90-100°F . When ou ts ide cond i t ions a re ho t and humid ,

however , i t may be necessary to ra ise tempera tu res to as h igh as

130°F . The s ize o f the d ryer shou ld be based on the herb p roduc t ion

a rea and how much w i l l be harves ted a t one t ime.

The d ryer shou ld have we l l - spaced racks to ensure tha t a l l

s ides o f the p lan t rece ive su f f i c ien t a i r f l ow and the p lan t mate r ia l

d r ies even ly . The she lves shou ld be cons t ruc ted o f food g rade

sc reens o r covered w i th an accep tab le food g rade mater ia l . The

d ryer shou ld be f ree o f dus t , d i r t , i nsec ts , and roden ts . Ev idence o f

any o f these in the f ina l p roduc t can lower i t s va lue o r render i t

unmarke tab le .

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The d ryer shou ld be ab le to ho ld an en t i re harves t and d ry i t

fas t enough tha t the c rop does no t spo i l . E f f i c iency and economic

concerns mus t be taken in to cons idera t ion to ensure the cos t -

e f fec t i veness o f i t s opera t ion . L ikew ise , a d ryer can be cons t ruc ted

f rom a new or ex is t ing shed ou t f i t ted w i th a hea te r , fan , and

dehumid i f ie r . Add i t iona l l y , a g rower may choose to cons t ruc t one

f rom sc ra tch .

In th is exper iment , tea leaves a re chosen as herbs tha t undergo

d ry ing p rocess by opera t ing t ray d ryer . The bes t method to d ry herb

w i l l depend la rge ly on the phys ica l charac te r i s t i cs o f the mate r ia l ,

the vo lume o f herb in the d ryer , and the re la t i ve humid i t y o f the

ou ts ide a i r .

D i f fe ren t herbs w i l l requ i re d i f fe ren t tempera tu res . Typ ica l l y ,

the h igher the amb ien t humid i t y , the h igher the tempera tu re tha t i s

requ i red to d ry the mate r ia l tho rough ly . In t roduc ing d r ie r a i r w i l l

reduce the amount o f t ime the mate r ia l i s in the d ryer , thus reduc ing

the cos t o f d ry ing the mate r ia l .

The mo is tu re con ten t o f d r ied p roduc ts i s ve ry impor tan t , and i f

i t i s too h igh , mou lds and yeas ts tend to g row. The mo is tu re con ten t

may be checked us ing sca les and an oven . The fo l low ing i s the

express ion tha t we may use in o rder to ca lcu la te the mo is tu re

con ten t o f our d ry ing tea leaves ;

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Other impor tan t parameter fo r d ry ing p rocess i s the d ry ing ra tes , v

(m in - 1 ) ;

v = X t 1 – X t 2

T 2 – T 1

EXPERIMENTAL PROCEDURE

1. A l l o f the equ ipment wh ich used in th is exper iment were

sw i tched on .

2 . R inse the empty t ray us ing wate r be fo re s ta r t

3 . The mass o f the empty t ray were measured and ta red . The da ta

was recorded .

4 . The d ry tea herbs were spr ink led w i th enough o f wa te r to make i t

we t .

5 . The tea herbs were p laced on to the empty t ray and pu t in to the

t ray d ryers to be p repared to be d r ied .

6 . The in i t i a l mass o f the wet tea herbs were measured and

recorded be fo re be ing d r ied .

7 . The in i t i a l tempera tu re and humid i t y wh ich shown on the t ray

d ryers taken and recorded . The in i t i a l a i r f l ow ins ide the t ray

d ryers were measured us ing the anemometer and the read ings

was recorded .

8 . The d ry ing p rocess i s s ta r ted by p ress ing the ‘HEAT’ bu t ton on

the t ray d ryers .

9 . A l l o f the da ta readed and recorded every 3 m inu tes in one hour

t ime o f the d ry ing p rocess o f the tea herbs .

10 . The mo is tu re con ten t and the d ry ing ra te were ca lcu la ted .

11 . The g raph o f d ry ing ra te aga ins t mo is tu re con ten t was p lo t ted .

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APPARATUS

Tray dryers

Analytical balance

Water

Anemometer

Stopwatch

Dry tea herbs

RESULT

Mass o f t ray = 1391 .3 g

Mass o f d ry tea leaves = 99 .4 g

T i m e

( m i n )

H u m i d i t y

( % r F )

T e m p e r a t u r e s

( ° C )

M a s s o f

s a m p l e ( g )

A n e n o -

m e t e r

( m / s )

M o i s t u r e

C o n t e n t

D r y i n g

r a t e

( m i n - 1 )I I I I I I

0 10 .6 0 .5 41 .9 39 .5 109 .4 1 .47 0 .1198 0 .0084

5 8 .4 0 .5 45 .3 43 .0 105 .3 1 .21 0 .0778 0 .01004

10 8 .0 0 .5 45 .8 44 .3 100 .4 1 .51 0 .0276 0 .00326

15 8 .0 0 .5 45 .7 44 .6 98 .8 1 .49 0 .0113 0 .00104

20 8 .0 0 .5 45 .6 44 .7 98 .3 1 .49 0 .0061 0 .001

23 8 .0 0 .5 45 .6 44 .8 98 .0 1 .52 0 .0031 0 .00037

26 8 .0 0 .5 45 .7 44 .7 97 .9 1 .52 0 .002 0 .00067

29 8 .0 0 .5 45 .6 44 .7 97 .7 1 .51 0 0

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0 5 10 15 20 25 30 35

90

95

100

105

110

115Mass versus Time

0 5 10 15 20 25 30 350

0.020.040.060.080.1

0.120.14

Moisture Content versus Time

0 5 10 15 20 25 30 350

0.0020.0040.0060.0080.01

0.012Drying Rate (1/min) versus Time (min)

SAMPLE CALCULATIONS

1. Mo is tu re con ten t ,x ca lcu la ted us ing the fo l low ing fo rmu la :

Mo is tu re con ten t ,x = mass1−massfinal

mass final

Example :

Mo is tu re Conten t 1 , x 1 = 109.4−97.7

97.7

= 0.11975

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Mo is tu re Conten t 2 , x 2 = 105.3−97.7

97.7

= 0.07779

2. A f te r ca lcu la ted the mo is tu re con ten t , the d ry ing ra te ca lcu la ted

us ing the fo l low ing fo rmu la :

Dry ing Rate , v = Δ xΔ t

Example : For tea herbs sample :

Dry ing Rate , v = x1− x2

∆ t

= 0.11975−0.07779

5

= 0 .008392

DISCUSSION

Based on g raph mass versus t ime , i t shows tha t the mass o f the

tea herbs a re decreas ing w i th t ime. Th is i s the same w i th g raph o f

mois tu re con ten t ve rsus t ime , where the mo is tu re con ten t i s

decreas ing w i th t ime.

Dry ing occurs in th ree d i f fe ren t per iods , o r phases , wh ich can

be c lear l y de f ined . The f i r s t phase , o r in i t i a l pe r iod , i s where

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sens ib le hea t i s t rans fe r red to the p roduc t and the con ta ined

mo is tu re . F rom bo th g raph , the f i r s t phase can be seen c lear l y a t

t ime be tween the f i r s t m inu te un t i l m inu te 9 . The second phase , o r

cons tan t ra te per iod , i s when the f ree mo is tu re pers is ts on the

sur faces and the ra te o f evapora t ion a l te rs ve ry l i t t l e as the mo is tu re

con ten t reduces . Th is i s seen f rom the g raph a t m inu te 9 un t i l m inu te

12 . The th i rd phase , o r fa l l i ng ra te per iod , i s the phase dur ing wh ich

mig ra t ion o f mo is tu re f rom the inner in te rs t i ces o f each par t i c le to

the ou te r su r face becomes the l im i t ing fac to r tha t reduces the d ry ing

ra te .

P r inc ip les o f t ray d ryer s ta tes tha t dur ing the ear l y s tages o f

d ry ing , the cond i t ions in the d ryer , wh ich i s a t h igh humid i t y and

modera te tempera tu re , a re idea l fo r the g rowth o f m ic roorgan isms.

The qu icker the d ry ing t ime the be t te r the f ina l m ic rob ia l qua l i t y o f

the p roduc t . F rom the g raph o f dry ing ra te versus t ime , we can see

tha t the chang ing pa t te rn i s no t cons is ten t o r in mannered pa t te rn .

Hence , i t i s we l l sa id tha t the d ry ing ra tes i s no t depend ing much

upon t ime.

CONCLUSION

Based on the da ta p lo t ted on each g raph , we can conc lude tha t

the mo is tu re con ten t and mass o f the tea herbs a re bo th decreas ing

w i th t ime. Never the less , the d ry ing ra tes o f the herbs a re vary ing

w i th t ime.

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RECOMMENDATION

I n o rder to ob ta in be t te r resu l t s , the re a re a few methods o r

recommendat ions tha t may be cons idered . F i rs t l y , the d ry ing ra tes

can be inc reased w i th two d i f fe ren t op t ions ; by inc reas ing the a i r

f l ow o r inc reas ing the a i r tempera tu re . However , the tempera tu re

mus t no t be se t to too h igh fo r i t may cause damage o r change to the

p roduc ts . Th is i s t rue fo r herbs and sp ices , as h igh tempera tu re w i l l

have the r i sk o f los ing de l i ca te f lavours o r co lours .

As a mat te r o f fac t , fan d r i ven d ryers may suck in f i ne dus t

par t i c les in dus ty a reas , caus ing con tamina t ion o f the p roduc t . In

ve ry dus ty a reas , powered d ryers may need a mus l in f i l t e r over the

a i r i n le t . Herbs and sp ices mus t be d r ied to a mo is tu re con ten t tha t

i s low enough to p reven t the g rowth o f m ic ro -o rgan isms such as

mou lds and bac te r ia .

Mos t commerc ia l d ryers a re insu la ted to reduce hea t losses ,

and they rec i rcu la te ho t a i r to save energy . Many des igns have

energy-sav ing dev ices , wh ich recover hea t f rom the exhaus t a i r o r

au tomat ica l l y con t ro l the a i r humid i t y . Computer con t ro l o f d ryers i s

inc reas ing ly soph is t i ca ted and a lso resu l t s in impor tan t sav ings in

energy .

I f the exhaus t a i r i s no t d r ied fo r rec i rcu la t ion , then the exhaus t

ven t shou ld no t be c lose to the f resh a i r i n take a rea , o therw ise the

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mois t exhaus t a i r w i l l be d rawn back th rough the d r ie r and d ry ing

e f f i c iency w i l l be los t .

Good a i r c i r cu la t ion w i th in the d ryer i s impor tan t , as i t reduces

d ry ing t ime and a l lows the use o f lower tempera tu res , bo th o f wh ich

can p reven t the degrada t ion o f chemica l cons t i tuen ts dur ing the

d ry ing p rocess . The d ryer shou ld have we l l - spaced racks to ensure

tha t a l l s ides o f the p lan t rece ive su f f i c ien t a i r f l ow and the p lan t

mate r ia l d r ies even ly . The d ryer shou ld be f ree o f dus t , d i r t , i nsec ts ,

and roden ts . Ev idence o f any o f these in the f ina l p roduc t can lower

i t s va lue o r render i t unmarke tab le .

REFERENCES

1 . ht tp : / /www. fao .o rg /docrep /V5380E/V5380E09.h tm

2 . ht tp : / /www.eno tes .com/how-produc ts -encyc loped ia /g reen- tea

3 . B i rd ,R .B ,S teward .WE,and L igh t foo t ,EN, T ranspor t Phenomena,

John Wi ley and Sons , Inc ,1960

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APPENDICES