TRACE 1300 Series New Presentation

7/22/2019 TRACE 1300 Series New Presentation

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Moving from TRACE GC Ultra

to………..



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Mov ing from TRACE GC Ultra to ......

• How Thermo TRACE GC Ultra was structurallyconcepted:

• Mainframe - Oven Overview

• Injectors - Detectors Overview

• Detector base body concept Gas

ModulesOverview

Detectors Overview



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DPFC module

Injectors

detectorscassette

Keypad

Electronics

DGFC module

Detectors

Detectorsbasebodies

Mainframe & Oven Overview



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In ject ions Overview

True coldOn-Column

Split/Splitless PTV Packed and

wide-bore

columns



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It allows simple detector

interchangeability

It ensures flexibility without

adding complexity

Base body

Detector

Oven

GC top deck

Detector base body concept



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Detector base body concept

A common base whichprovides the detector

with main heating and

gas feeding

All detectors are

available with both

Digital Gas Flow Control

(DGFC) and conventional

pressure regulators (non-DGFC)



Mov ing from TRACE GC Ult ra to ............

.....................................



.........TRACE 1300 Series Modular Concept



.....TRACE 1300 - 1310 Series Modu lar Concep t

• A main electronic module that includes: main CPU, oven control,

power supply.

- 2 versions: 220V and 120V

• Injector modules include injector body, electronics for injector

temperature and carrier gas control.

• Detector modules include detector cell and electronics for signal

amplifier –digitalization, for temperature and detector gas control.

• TRACE 1300 – TRACE 1310 can accommodate 2 inlet and 2 detector

modules (2 channels) self-recognized

• Additional external devices can be located into dedicated housing.



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TRACE 1300 - 1310 Series Modular i ty Advantages

• Modules can be tested (also

analytically) separately prior testing

the assembled unit

• Modules can be shipped separately

and assembled during the

installation in field

• Modules can be kept in stock for fast

replacement, upgrading, or change

of configuration

• Possibly modules would be replaced

without requiring a field service

engineer



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TRACE 1300 - 1310 Modu lar Concep t

Trace GC 1300: Local built-in ultra-

simplified user interface - two

buttons and four LEDs.

Trace GC 1310: Touch screen

interface provides instant access for

ease of use and local control



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TRACE 1300 - 1310 Series Modu lar Con cep t

Where the parts were on TRACE GC Ul t ra

and

Where they are now on TRACE 1300 Series



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TRACE GC Ultra TRACE 1300 - 1310

• Injector

• DPFC/DCC module

• EPC Board

• Thermoregulator

(I/O Feedback board)

• Power control

• Injector Module



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TRACE GC Ultra TRACE 1300 – 1310

• Detector Module• Detector

• Base body

• DGFC module

• Detector board

• Thermoregulator

(I/O Feedback board)

• EPC board• Power control



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• CPU Board

• I/O Feedback board

• Mother board

• Power supply

• Electronic Compartment



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• User Interfaces 1300

• User Interfaces 1310

• GC Keypad



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TRACE 1310

Instrument Control



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TRACE 1310

Configuration



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TRACE 1310

Diagnostics



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TRACE 1310

Status



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TRACE 1310

Maintenance

*When Graph Pack adapters will be used,

the column insertion into the Injector and

Detector inlets must be added of 12mm.



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TRACE 1300 - 1310 HW connect iv i ty

• Two RS-232 ports for Autosamplercontrol

• Thermo Fisher bus I2C with 5V

power for additional auxiliarydevices

• GC Control through Ethernet IP address

• Direct connection to PC (reversed RED cable)

• Connection to LAN (standard GREY cable)



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TRACE 1300 - 1310 Ethernet con figurat ion

• MAC address fixed and assigned in the factory

• IP Address -> need to be assigned

• TCP Port -> 2551 (different from the one used on Trace

GC)

• Chrom-Card and Xcalibur accepts TCP Port=2551

• ChromQuest has a different TCP Port -> need to be changed in

TRACE 1300-1310

• Ethernet Configuration details listed within “Diagnostic”

menu



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TRACE 1300 – 1310 Set up

• From the PC, launch the Setup.exe file named TR1300ST (Service

Tool) entering ThermoFisher as password, then, press OK.• This SW load the whole package zip file as it is. Do not change any file

inside.



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• Automatically the SCAN will start to check how many systems are present.



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• Selecting the instrument on which IP set-up and Firmware updating must

be performed, automatically the two dedicated options will be activated



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TRACE 1300 – 1310 IP Set up

• Selecting IP Set-up a new page will be shown where GC name and IP

address can be modified.



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TRACE 1300 – 1310 F/W update

Selecting F/W update a new page will be shown, click on “Browse

package name” and select where the package with the new firmware

version is present (C: or USB, or..... ) Do not change any file inside.



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• On the new page will be shown the TRACE 1300-1310 configuration with

the current F/W version of the modules installed and the package of the

new firmware version. Select Update to start the F/W updating.



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• F/W updating in progress..............



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• At the end of the F/W updating, all the status cell must be OK.

• Click Done to close the program.

TRACE 1300 - 1310



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TRACE 1300 1310

HMI SW update from USB st ick

• HMI SW can be updated through the USB port positioned below the

touch screen

TRACE 1300 - 1310



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TRACE 1300 1310

HMI SW update from USB s t ick

Configuration



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TRACE 1300 – 1310 Series

..............more in depth



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TRACE 1300 – 1310 SSL In jecto r Modu le

• Manifold (Plumbing)

• Removable SSL Injector Body

• 2 Electronic Boards

• 3 Solenoid Valves

(Carrier, Split & Purge)

• 2 Removable Filters (Carrier & Split)

C SS



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TRACE 1300 – 1310 SSL Injecto r Modu le

• Designed to have a cool head and

septum.• Septa is kept below 150°C even

with inlet set to 350°C

• Lower septum bleeding

(siloxanes)

• No septum sticking• Lower air (oxygen) diffusion

• Longer septa lifetime

• The cool head SSL is optimized

for cold needle injection

0

10

20

30

40

50

60

70

80

90

100

100 150 200 250 300 350 400

T (°C)

D e p t h ( m m )

TRACE 1300 1310



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TRACE 1300 –1310 SSL Technical Speci f icat ion

• Temperature range:

• Maximum temperature 400º C with temperature settings resolution of 1º C units

• Temperature stability 1º C

• Heater cartridge 80W 48Va.c.

• Pneumatics:

• Electronic control only

• Constant pressure

• Constant flow

• Flow regulation through calculated pressure

• Pressure or flow programming in three ramps and four plateaus

• Pressure range:

• 0 to 1000 KPa, with a resolution of .015 KPa, and stability of 0.1 KPa along the entire scale

• Flow ranges:

• Column flow from 0.1 to 100 ml/min, with resolution of 0.01 ml/min

• Split flow from 10 to 1250 ml/min He with resolution of 1mL/min

• Septum purge flow from 0 to 50 ml/min with resolution of 1mL/min

• Ambient temperature and pressure compensation

• Gas saver function

• Operating modes:

• Split /Split less

• Surged Split/Surged Split less

• Large Volume Split less

• Back-flush capability (*) NOTE: Standard SSL CANNOT BE con verted to SSL BKF a new mo dule MUST BE requested.

TRACE 1300 1310 PTV I j t M d l



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TRACE 1300 – 1310 PTV In jecto r Modu le


• Removable PTV top head

• Removal of bottom column

connection for easier cleaning of

internal body


• 3 Solenoid Valves

(Carrier, Split & Purge)

• 2 Removable Filters (Carrier & Split)

• Cooling Fan

TRACE 1300 1310 PTV I j t M d l



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TRACE 1300 – 1310 PTV In jecto r Modu le

• Removal top body plus tubing

for easier cleaning

• Removal of bottom column

connection for easier cleaningof internal body

TRACE 1300 1310 PTV T h i l S if i t i



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TRACE 1300 – 1310 PTV Technical Specif icat ion

• Temperature operating range:

• Maximum temperature 450º C with temperature settings resolution in 1º C units

• Temperature stability 1º C maximum at 250º C for 30 minutes

• Temperature program rate up to 14.5ºC/sec

• Heater assy 120W 48Va.c.

• Capable of sub ambient operation to -50º C with LN2, 0º C with CO2

• Sub-ambient control will be optional and should not add cost to base unit.

• Three different temperature programmable ramps, four plateaus

• Pneumatics:

• Electronic control only

• Constant pressure

• Constant flow (Flow regulation through calculated pressure)

• Pressure or flow programming in three ramps and four plateaus

• Pressure programming: 0 to 1000 KPa, with a resolution of .015 KPa, and stability of 0.1 KPa along the entire scale

• Flow programming: 0.1 to 100 ml/min, with resolution of 0.01 ml/min

• Independent pressure/flow set points during injection

• Ambient pressure compensation.

• Control of split flow in 1mL/min from 10 to 1250 mL/min He• Gas consumption saver

• Purge flow from 0 to 50 ml/min

• Operating modes:

• Split, Splitless, Solvent Split (Large Volume)

• Back-flush capability (*) NOTE: Standard PTV CANNOT BE co nverted to PTV BKF a new m odu le MUST BE requested.

TRACE 1300 1310 I j t M d l



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TRACE 1300 – 1310 In jecto r Modu les

SSL Body PTV Head

TRACE 1300 1310 FID D t t M d l

http://localhost/var/www/apps/conversion/tmp/scratch_2/PTV%20head%20replacment.MP4

http://localhost/var/www/apps/conversion/tmp/scratch_2/SSL%20Body%20replacment.MP4



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TRACE 1300 – 1310 FID Detecto r Modu le


• Detector body


• 3 Solenoide Valves

(Air, Hydrogen & Make up)

TRACE 1300 1310 D t t S if i t i



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TRACE 1300 – 1310 Detecto r Specif ic at ions

• FID Techn ical Specif ic ations

• Maximum operating temperature, 450º C

• Flameout detection and warning

• Automatic flame re-ignition with shutdown of gases upon failure (3

times)• MDA: <2 pg carbon/sec as propane

• Linear dynamic range 10^7

• Acquisition rate up to 300 Hz

TRACE 1300 1310 Detecto r Specif ic at ions



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• TCD Techn ical Specif icat ions

• Maximum operating temperature, 400º C, filament ambient to 450º C

• Operating modes: constant mean temperature

• Filament protection in case of carrier gas failure

• Compatible with Fe/Ni or W/Re filaments• MDA: 600 pg ethane/ml He carrier

• Linear dynamic range >= 10^6




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• NPD Technical Specif icat ions

• Compatibility with DET’s TID-2, Agilent’s BLOSand other DET TID types.

• MDL: Nitrogen: 0.05 pg N/s or better;

Phosphorus: 0.02 pg P/s or better.

• Dynamic and Linear Range: Dynamic range of response: 10E6; Linear

range: 10E4 or better.

• Selectivity: N/C = 50,000 to 1 gN/gC or better; P/C = 200,000 to 1 gP/gC

or better.

• Data acquisition rate: Up to 300Hz to be compatible with fast and

ultrafast GC.

• Maximum Operating Temperature: Up to 450°C.

• Heating Current setting: 1.00 to 3.50 A (or different range according to

the source requirements) in 0.01 steps.

• Source protection in case of gas failure




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• ECD Techn ical Specif icat ions

• Maximum operating temperature: 400º C

• Cell volume <= 150 µl

• Acquisition rate up to 100 Hz

• Operating mode: constant current, pulse modulated• MDA <= 5 fg Lindane

• Linear dynamic range: >10^4 Ar/CH4 make-up

• Equipped with removable collector electrode for local maintenance

TRACE 1300 1310 Pneumatic Net



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TRACE 1300 – 1310 Pneumatic Net

TRACE 1300 1310 Gas Net Assembly



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TRACE 1300 – 1310 Gas Net Assembly

TRACE 1300 1310 Gas Net Location



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TRACE 1300 – 1310 Gas Net Location

TRACE 1300 – 1310 Components lo cat ion



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TRACE 1300 1310 Components locat ion

Hermes back view

toroidal

transform

electronic box

gases inlet

fan motor

H2

sensor

(optional)

Hot air

outlet duct

main switch

detector

moduleinjector

module

oven

door

insulation

material

TRACE 1300 – 1310 Oven heating



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TRACE 1300 – 1310 Oven heating

• The tension rate changes from 230V to 120V but not the baffle.

• The serial or parallel heaters wiring is driven by the electronic box,

according to the tension rate. heating element

RTD

back viewfront view

TRACE 1300 – 1310 Module “Electronics”



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Backplane

TRACE 1300 – 1310 Module Electronics

CONTROL AREA

Connections for:

2 x injector

2 x detectors

1 x PT100

1 x door switch

1 x stepper (flaps)

1 x H2 sensor

3 x 24V auxiliary

POWER AREA

Connections for:

1 x main line

1 x 500VA pri.

1 x 500VA sec.

1 x heater

1 x fan (oven)

TRACE 1300 – 1310 Module “Electronics”



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Electronic compartment

Oven & Power

Main CPU

External Interface

Power switching

Breaker

Fan Handles

TRACE 1300 – 1310 Module Electronics

TRACE 1300 – 1310 Series Auto samplers



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In ject ion posi t ion Inlet maintenance posit ion




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In let Maintenance pos it ionInject ion posi t ion

TRACE 1300 1310 Series Auto samplers




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TRACE 1300 - 1310 Series & ISQ



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TRACE 1300 1310 Series & ISQ

TRACE 1310 & ISQ must look like a single instrument

when coupled

TRACE 1300 – 1310 Series



TRACE 1300 1310 Series

Questions?

TRACE 1300 Series New Presentation

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