TPV Seal Geometry Effects on Compression Set (CSet) and Compression Load Defglection -...
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7/30/2019 TPV Seal Geometry Effects on Compression Set (CSet) and Compression Load Defglection - Above-The-belt 2006
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TPV Seal Geometry Effects On
Compression Set (CSet) andCompression Load Deflection (CLD)
Jere Anderson, Trexel, Inc
Felix Zacarias, Santoprene Specialty Products
ExxonMobil Chemical
Above-The-Belt 2006 Novi, MI
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Outline Background
Study objectives
Approach
Sample production
Materials
Process Results
Conclusions
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Background Primary and secondary automotive weatherseals are
complex, multifunctional profiles that:
Control or affect:
Water ingression
Wind noise
Door closing effort
Aesthetics at vehicle entry
Typically consist of:
Sponge sealing section
Mounting section
Dense polymer
Metal reinforcement
Trim
Secondary lip
Skin coat
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Background Performance requirements for weatherseal sponge
Surface contact area for sealing
Conform to sealing surface imperfections and build tolerances Low compression force
Withstand high deformations
Provide rapid, elastic deformation recovery
Operate over a wide temperature range Maintain properties with cyclical deformations
Provide consistent properties over long product life
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Background
Meeting weatherseal performance needs requires:
Materials
Process Part Design Trexel MuCell process
Closed cellular structure
Designed for performance Foamability
Surface aspect
Low CLD
Low CSet
Elongation
Geometry
Dimensions Sponge specific gravity
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Background EPDM material properties TPV material properties
Current weatherseal designs based on EPDM properties
Historical material of choice Seal designer and manufacturer experiences
Different design rules anticipated for optimal seal performance with TPV
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Objective The objective of this investigation was to quantify the
effects of varying TPV profile design on key weatherseal
performance criteria to define TPV sponge designs for
optimal weatherseal performance.
Study variables
Profile shape
Profile wall thickness Sponge density
Measured results
CSet
Short term
Long term
CLD
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Approach Produce D shaped profiles of equal height varying:
Shape
Wall thickness 1.5 and 2.0 mm
Sponge density 0.55 to 0.65 gm/cc
Assess performance differences
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Sample Preparation Process
MuCell foam extrusion process
Physical foaming technology Direct injection of supercritical N2 or CO2
Equipment
Trexel extrusion system 63 mm diameter, 32:1 L/D
Throughput 45 kg/hr (100 lb/hr)
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Sample Preparation Materials
Santoprene X121-60F150 polymer
typ. properties test method Specific gravity 0.97 g/cc TPE-0105/1
Hardness 60 Shore A TPE-0104
Ultimate tensile str. 4.5 MPa (650 psi) TPE-0153
Elongation @ break 390% TPE-0153
SCF
Type N2
Delivery pressure 172 bar (2,500 psi)
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Results Samples Produced
Actual optical comparator tracings
-2O Profile 22O Profile 57O Profile
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Results11
Short Term Cset - 22hr @ 70OCSantoprene
TMX121-60F150, Spong e S.g. 0.54 - 0.60 g/cc , Test Me tho d TPE 0016
20.0
25.0
30.0
35.0
40.0
45.0
50.0
1.2 1.3 1.4 1.5 1.6 1.7 1.8 1.9 2 2.1 2.2 2.3 2.4 2.5
Wall Thicknes s (m m )
CSet
(%)
-2O
Profile
22O Profile
57O
Profile
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Results12
CLD - 50% and 25% Com pressionSantoprene
TMX121-60F150, Spon ge S.g. 0.54 - 0.60 g/cc, Tes t Met ho d A STM D 1667
0
2
4
6
8
10
12
14
16
18
20
22
24
26
28
30
32
34
36
1.2 1.3 1.4 1.5 1.6 1.7 1.8 1.9 2 2.1 2.2 2.3 2.4 2.5
Wall Thickness (mm )
CLD
(N/1
00mm)
-2O
Pro file - 50%
22O
Pro file - 50%
57O
Pro file - 50%
-2O
Pro file - 25%
22O
Prof ile - 25%
57O
Pro file - 25%
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Results13
50% Com pressio n CLD vs. Short Term CSetSantoprene
TMX121-60F150, Sponge S.g. 0.54 - 0.60 g/cc, Tes t Me tho ds ASTM D 1667 & TPE 0016
0
5
10
15
20
25
30
35
40
1.2 1.3 1.4 1.5 1.6 1.7 1.8 1.9 2 2.1 2.2 2.3 2.4 2.5
Wall Thickness (m m )
CLD
(N/10
0mm)
10
15
20
25
30
35
40
45
50
CSet(%)
-2O
Profile
22O
Profile
57O Profile
-2O Profile
22O
Profile
57O
Profile CSet
CL D
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Results14
Lo ng Term Cset - 1,000 ho urs @ 70OCSantoprene
TMX121-60F150, Spong e S.g. 0.54 - 0.60 g/cc , Test Metho d TPE 0016
0
10
20
30
40
50
60
70
0 100 200 300 400 500 600 700 800 900 1000
Time (hours)
CSet(%
)
Typical EPDM
Typical 60F150
-2O
Profile
57O
Profile
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Results SummarySantoprene X121-60F150 Sponge 0.54 0.60 g/cc
Anticipated CLD and CSet range:
Min. Max. Units
CLD (25% compression) 2.6 10.8 N/100 mmCLD (50% compression) 7.0 34.5 N/100 mm
CSet 32 48 %
Shape and wall thickness changes from 1.4 to 2.2 mm.
Sponge density changes did not affect CSet or CLD.
Short term CSet is reduced with:
Shape change parallel to load 5% points at fixed wall thickness.
Wall thickness increase 1.4% points/0.1 mm increase.
A total of 16% points with both shape and wall thickness changes.
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Results SummarySantoprene X121-60F150 Sponge 0.54 0.60 g/cc
CLD is reduced with :
Shape change to more round profiles at fixed wall thickness
11 to 12 N/100 mm (50% compression)
1.7 to 3.8 N/100 mm (25% compression)
Decreased wall thickness
2 N/100 mm for a 0.1 mm wall thickness reduction
(50% compression)
1.7 N/100 mm for 0.1 mm wall thickness reduction
(25% compression)
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Conclusions Profile shape has a large effect on TPV sponge CSet
and CLD.
Profile shape for TPV can be optimised for CSet and
CLD independently of sponge specific gravity.
TPV CSet is consistent over time
TPV sponge CSet EPDM sponge CSet after 700
hours (29 days).
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THANK YOU
FOR YOUR ATTENTION!
The authors would like to thank Curt Waddle from
ExxonMobil Chemical for profile testing support.
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2006 Exxon Mobil Corporation. To the extent the user is entitled to disclose anddistribute this document, the user may forward, distribute, and/or photocopy thiscopyrighted document only if unaltered and complete, including all of itsheaders, footers, disclaimers, and other information. You may not copy thisdocument to a Web site. The information in this document relates only to thenamed product or materials when not in combination with any other product ormaterials. We based the information on data believed to be reliable on the datecompiled, but we do not represent, warrant, or otherwise guarantee, expresslyor impliedly, the merchantability, fitness for a particular purpose, suitability,accuracy, reliability, or completeness of this information or the products,materials, or processes described. The user is solely responsible for alldeterminations regarding any use of material or product and any process in itsterritories of interest. We expressly disclaim liability for any loss, damage, orinjury directly or indirectly suffered or incurred as a result of or related to anyoneusing or relying on any of the information in this document. There is noendorsement of any product or process, and we expressly disclaim any contraryimplication. The terms, we, our, "ExxonMobil Chemical", or "ExxonMobil" areused for convenience, and may include any one or more of ExxonMobilChemical Company, Exxon Mobil Corporation, or any affiliates they directly orindirectly steward. The ExxonMobil Emblem, the Interlocking X Device,Santoprene and Vistalon are trademarks of ExxonMobil Corporation.
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