THRU: Mike Zickler, TATL, Region lU-ff— TD D #9010-11FROM: Luis Loarca, TAT Region III SUBJECT:...
Transcript of THRU: Mike Zickler, TATL, Region lU-ff— TD D #9010-11FROM: Luis Loarca, TAT Region III SUBJECT:...
* 5 Underwood CourtDetroit, NJ 08075 1.609-461-4003
TECHNICAL ASSISTANCE TEAM FOR EMERGENCY RESPONSE REMOVAL AND PREVENTIONERV CONTRACT 68-WO-OQ36
MEMORANDUM
TO: Glen Lapsley, EPA Region IIIEnforcement and Title III Section
THRU: Mike Zickler, TATL, Region l U - f f — TDD #9010-11v PCS #1198
FROM: Luis Loarca, TAT Region IIISUBJECT: Snow Hill lane Sample Reoults
DATE: January 3, 1991Enclosed you will find the analytical results for Snow Hill LaneSite, as you requested yesterday, (January 2).
Sample Label Sample Location
W-l FIELD BLANKW-2 325 Cedar Hill Lane residency, non-
filtered i/ir.,-H-3 325 Cedar Hill Lane residency, .filteredw-4 upstream, non-filtered AW-5 Downstream, non-filteredH-6 GE drumW-8 Uptream, filteredW-9 Downstream, filteredS-l Soil backgroundS-2 Neville drumS-3 Monsanto drums-4 Soil around Neville drumS-5 Soil around Monsato drumS-6 Soil around the Rohm & Haas drumS-7 Offsite soil backgroundS-8 Soil around the GE drumS-9 Rohm & Haas DrumS-10 Soil Background on Snow Hill Lane
W0005MAJOR PROGRAMS DIVISIONIn Auociadon with Foster Wheeler Envireiponse, Inc., Retourct Applications, Inc., C.C, Johnson Mulhotra, RC,ind RE. Swrlcra Auodatet
the. pa,g<L Wmd in thi* faamr. i* not O.A ne.ndable. o*. Itaibte. mit U *.* due to AubAtanda/id aoto/i o/i conditional tht original
Bridgeport Environmental Inc. ucti»«umiyii«iuiw.iariM fM(____________________________________________________H 08S55 IJlP.O.Box 247 609/467.0380510 Heron Drive Suite 107Bridgeport, NJ 08014-0247
HESTON
PROJECT: SNOW HILL LANE
DATE RECEIVED: NOVEMBER 11, 1990
REPORT NO: E627S - E6288
BRIDGEPORT ENVIRONMENTAL, INC.
RICHARD W. LINCH ,nnnnftLABORATORY MANAGER lUUUUO
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SAMPLE JdCATION AND IDENTIFICATION
ANALYSIS NO CLIENT ID
E6275 W-l
E6276 • W-2
E6277 W-3
E6278 N-4
E6279 W-5
E6280 W-6
E6281 s-2
E6282 S-3
E6283 S-4
E6284 S-5
E6285 S-6
E6286 S-7
E6287 S-8
E6288 s-9
woo?O
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COMP.
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METHODOLOGY' SUMMARY
PURGEABLES U.S.E.P.A. Method 624 - This is « purge andcrap Gas Chromatagraph/Masa Spectrometer (GC/MS)method applicable to the determination of thecompounds listed in the U.S.E.P.A. Manualentitled " Test Procedures for tha Analysis ofOrganic Pollutants".
Ac RF5996 GC/MS was used with a capillary column.
Method detection Units are as stated,
Soil samples are prepared for analysis aa prescribedin Method 8240 frsw 3H846.
ACID EXTRACTABLESBASE NEUTRALS D.S.E.F.A. Method 625 - This method covers
the determination of a number of organic compoundsthat an partitioned in an organic solvent and••enable to gas chroaatography. Thii it a gaichromatography/mass ipectrometer (GC/MS) methodapplicable to the determination of the compound!listed in the D.S.E.P.A. Manual entitled "leitProcedures for the Analysis of Organic Pollutants".
/
A HP5970 was used with a DB-S FSCC.
Method detection limits are as stated.
Soil samples were prepared for analysis asprescribed in Method 3550 from SH846.
PESTICIDES/PCB's U.S.E.P.A. Method 608 - This method covers thedetermination of pesticides and PCS' a in samplesby uittr*. ztlbn/concentractlon with organic solventsand subsequent qualification/quantification byGas Chromatography. The gas chromatograph utilizesan electron capture .detector (ECD) which isapplicable for the determination of the compounds listedfor this method in the U.S.E.P.A. Manual entitle"Test Procedures for the Analysis of Organic Pollutants".
Soil samples were prepared as prescribed in Method3SSO from SW846.
100009
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nMETIIODOLOCY SUMMARY
METALS Soil samples Cor metal analysis were run inaccordance with the methods prescribed inSU846, This Includes a nitric acid digestionfollowed by either furnace flame atomicabsorption, Flaneless Atomic Absorption, orInductively Coupled Plasma analysis.
Aqueous samples for metals analysis were runin accordance) with the methods prescribed inMethods for Chemical Analysis of Watur andWastes, EPA-600/4-79-020 March 1979.
PHEHOLS Analysis performed according to U.S.E.P.A.420 (coloxlneccic, Automated 4AAP withDistillation). Samples that are high insolids are predlstllled according to 420,1(8.1). Sample is reacted with four (A)Amlnoantlpyrine and Alkaline ferrlcyanl.de tofora a red color, which is read at SOSnm.Equipment used; Technlcon Autoanalyzer 1IC.
Analysis performed according to U.S.E.P.A.335.3 (colormetric, automated), Samples highin solids are predlstllled according Cofigure 1, 335-2. All samples pass throughautomated distillation. Sample is reactedwith Chloroaroine T Co produce cyanogenchloride, which developes a red color whencombined with pyrldina/barblturlc acidreagent; which is read at 570nm, Equipment:used: Technicon Autoanalyzer I1C,
PETROLEUMHYDROCARBONS Aqueous 'samples were analyzed following Method
418.1 as prescribed in Methods for ChemicalAnalysis of Water and Wastes, EPA-600/4-79-020March 1979,
Soil samples were extracted in accordance with *•'»'"*"the methods prescribed in SW-846 andsubsequently analyzed as scored above,
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LABORATORY CHRONICLE
RECEIPT/REFRIGERATION _____________ 11/11/90
ORCANICSEXTRACTION
1. Acids
2. Base/Neutrals
3. Pestlcidea/PCB'B/Berbicldea 11/13/90 - 11/19/90
4. Petroleum Hydrocarbons_______*____________
ANALYSIS
1. Volatlles_______________!{_•_____________
2. Acids ________ HA
3. Base/Neutrals
4. Pestlcldes/PCB'a/Herbicides UW9Q - 12/4/90
5. Petroleua Hydrocarbons______NA___________
6. Total Organic Carbon________^ _______
Sectlon SupervisorT.uvlew & Approval
INORGANICS
1. Metals_________________ii/Ti/on - ii/9n/qn
2. Cyanides__________________11/13/90________
3. Phenols_________._______HA
OTHER ANALYTES
Section SupervisorReview & Approval__
Quality Control Supervisor 100011Review & Approval____________g UA________*
—^ If fractions are re-extracted and re-analyzed because initial endeavorsdid not _eet quality control acceptance criteria, Include dates for both.
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RESDT.T SUMMARY
0
100012
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CERTIFICATE OF ANALYSIS
SAMPLE ID: K6275
CMENT ID: w-1
SAMPLE DATE: 11/9/90
"PALS MDL(_g/L) RESDLT(-g/L)
b.Ol N.D.
1,00013
J
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CERTIFICATE OF ANALYSIS
SAMPLE ID: £6276
CLIENT ID: W-2
SAMPLE DATE: 11/9/90
METALS MDL(_g/L) RESULT (ag/I.)LEAD 0.01 N.D.
u
100014
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CERTIFICATE OF ANALYSIS
SAMPLE ID: E6277
CLIENT ID: tf-3
SAMPLE DATE: 11/9/90
METALS HDL(Dg/L) -ESOLT(Bg/L)
LEAD 0.01 0.015
. 100015
O
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CERTIFICATE OF ANALYSIS———————
SAMPLE ID: E6278
CLIENT ID: H-4
SAMPLE DATE: 11/9/90
METALS , HDL(-g/L) RESOLT(nE/L)
LEAD 0.01 N.D.
100016 ^•' U
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CERTIFICATE OP ANALYSIS
SAMPLE ID: E6279
CLIENT ID: W-5
SIMPLE DATE: 11/9/90
METALS MOL(mg/L) RESULT(ag/L)LEAD 0.01 N.D.
O 100017
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CERTIFICATE OF ANALYSIS
HAZARDOUS SUBSTANCE LIST(aqueoua)
SAMPLE ID: E62BO
CLIENT ID: H-6
SAMPLE DATE: 11/9/90
METALS MDL (mil) RESDLT (_g/L)ALUMUm 0.10 0.11ANTIMONY 0.005 N.D.ARSENIC 0.005 N.D.BARIUM 0.50 N.D.BERYLLIUM 0.01 N.D. ,CADMIUM 0.01 N.D.CALCIUM 0.05 34.9CHROMIUM 0.01 N.D.COBALT 0.05 N.D.COPPER , 0.01 3.39 (~~\IRON 0.05 0.50LEAD 0.05 1>UMAGNESIUM 0.05 2.71MANGANESE 0.01 0.39MERCURY 0.0005 0.028NICKEL 0.05 N.D.POTASSIUM 0.10 9.69SELENIUM 0.005 N.D.SILVER 0.01 . N.D.SODIUM 0.05 12.3THALLIUM 0.10 N.D.VANADIUM 0.05 . N.D.ZINC 0.01 1.45
CYANIDE 0.10 N.D.
100018
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LabNam: Bridgeport Environiantal, Inc. I Saiplo Hurter Ibig No i N/A I E6260 I
ORGANICS ANALYSIS DATA SHEET »..,-........—.«(Pago 3)
Pesticides/PCBs ><
Conctntration: (toT) Itediui ( Circla Dng ) GPC Clianup _ Vis J Ho xDal« Extricttd/PrejISfcd; 11/13/90 Sepiratory Funnel Extraction _/ YogCite Analyzadi 12/03/90 Continuous Liquid-Liquid Extraction _ YetCore/Oil Factor! IdOiL/frlPircent toitture; N/A
C.A.S.Huibir
12674-11-211104-26-211141-16-;55469-21-912672-29-611097-69-111096-62-;
Arochlor-1016, ,flrochlor-1221. ,Arochlor-1232. ,Arochlor-1242, ,Arochlor-1248, ,
Arochlor-1260, ,
13 U13 UHU13 U13 U13 U13 U•J
Fori 1 7/85
100019
xj
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CERTIFICATE OF ANALYSIS
HAZARDOUS SUBSTANCE LIST
SAMPLE ID: E6281
CLIENT ID: S-2
SAMPLE DATE: 11/9/90
METALS MDL (ag/kg) RESULT (an/kg)
ALUMINUM 5.00 2640ANTIMONY 0.13 2.57ARSENIC 0.13 9.53BARIUM 12.5 N.D.BERYLLIUM 0.50 N.D.CADMIUM 0.50 N.D.CALCIUM 2.50 13900CHROMIUM 0,50 1860COBALT 2.50 „_„_COPPER ' 0.50 186000 0IRON 2.50 1MOOOLEAD 2.50 6530MAGNESIUM 2.50 M600MANGANESE 0.50 404MERCURY 0.05 legNICKEL 2.50 66<4POTASSIUM 5.00 1030SELENIUM 0.13 30<0SILVER 0.50 H<1)_SODIUM 2.50 2550THALLIUM 2.50 „_„_VANADIUM 2.50 . U3ZINC 0.50 19700
100020CYANIDE 0.10 39.0
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r Lab HIM ! Bridgeport Environmental, Inc. I Saiple Nuwor ICaiaNo I N/A I E6261 I
ORGANICS ANALYSIS DATA SHEET «•••-• •-•——«(Page 3)
PeJticides/PCBs ••
Concantrationi (to* nediim ( Circle Ono ) GPC Cleanup _ Yas __ NoData Extracted/Prepared! 11/13/90 Sepiratory Funnel Extraction _YesData Analytadi 12/04/90 Continuous Liquid-Liquid Extraction _ YeaConc/Dil Factor) 10,08/lOnLPercent toiiture: 3.9
C.A.S,Nurier
12674-11-2 Arochlor-1016. ..... 2700011104-26-2 Arochlor-1221. ..... 13000 U11141-16-; Arochlor-1232. ..... 17000 U53469-21-9 Arochlor-1242, . . , , , 13000 U12672-29-6 Arochlor-1248. ..... 13000 U11097-69-1 Arochlor-1254, ..... $000011096-B2-5 Arochlor-1260. ..... 17000 U
Fori 1 7/B5
100021O
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CERTIFICATE OF ANALYSIS
HAZARDOUS SUBSTANCE LIST(solid)
SAMPLE ID: E6282
CLIENT ID: S-3
SAMPLE DATE: 11/9/90
METALS MDL (_g/kg) RESULT (ag/kg)
ALUMIKDH 5.00 460
ANTIMONY 0.13 N.D.ARSENIC 0.13 8.36BARIUM 12.5 N.D.BERYLLIUM 0.50 N.D.CADMIUM 0.50 1.19CALCIUM 2.50 467CHROMIUM 0.50 12.6COBALT 2.50 N.D.COPPER ' 0.50 86.4 BON 2.50 26500 ^LEAD 2.50 526MAGNESIUM 2.50 163MANGANESE 0.50 189MERCURY 0.05 0.088NICKEL 2.50 77.!POTASSIUM 5.00 148SELENIUM 0.13 0.13SILVER . 0.50 N.D.SODIUM 2.50 507THALLIUM 2.50 N.D.VANADIUM 2.50 27.2ZINC 0.50 2300
CYANIDE 0.10 4.01
100022O
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Lab New i Bridgeport Environnental, Inc. I Staple Nuiber IGate No ! M I E6262 I
ORGANICS ANALYSIS DATA SHEET ,———...—.,(Page 7)
Pejticidea/PCBs '•/••••s.
Concentration! (fcm) Ifediui ( Circle One ) GPC Cleanup _ Yat j VaData Extracted/Prepared! 11/13/90 Separator)) Funnel Extraction _YeiData Analyzed! 12/04/90 Continuona Liquid-Liquid Extraction _ YetCone/Oil Factor: 10,07/lOiLPercent Koiilurei 2.!
C.A.S.Nuaber
12674-11-2 Arochlor-1016. , , . . , 13000 U11104-28-2 Arochlor-1221, ..... 13000 U11141-16-; Arochlor-1232. , , , , , 17000 U53469-21-9 Arochlor-1242. ..... 13000 U12672-29-6 Arochlor-1248. , . , . , 17000 U11097-69-1 Arochlor-1254. ..... 3500011096-82-; Arochlor-1260. , . . , , 13000 U
Fori 1 7/fl5
100023
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CERTIFICATE OF ANALYSIS
HAZARDOUS SUBSTANCE LIST(aolld)
SAMPLE ID: g6283
CLIENT ID: S-4
SAMPLE DATE: 11/9/90
METALS HDL (ng/kg) RESULT (mg/kg)
ALUMINUM 5.00 7B10ANTIMONY 0.13 0.26ARSENIC 0.13 18.1BARIUM 12.5 679BERYLLIUM 0.50 0.86CADMIUM 0.50 11.0CALCIUM 2.50 10400CHROMIUM 0.50 1710COBALT 2.50 42.0COPPER ' 0.50 , 224000HON 2.50 199000LEAD 2.50 6220MAGNESIUM 2.50 15000MANGANESE 0.50 1270MERCURY 0.05 76.0NICKEL 2.50 112POTASSIUM 5.00 456SELENIUM 0.13 18.9SILVER • 0.50 , N.D.SODIUM 2.50 714THALLIUM 2.50 N.D.VANADIUM 2.50 , 46.6ZINC 0.50 13100
CYANIDE 0.10 62.0100024
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Lab Na*e t Bridgeport Environmental, Inc. i Saiplo Nuiber ICaaeNo : N/A I E6283 I
ORGANICS ANALYSIS DATA SHEET t................*(Paga 3)
Peiticides/PCBs ••
Concentration! (\M) Ifediui ( Circle Una ) 6PC Cleanup _ Yea i/mData Extracted/Prepared! 11/13/90 Separator^ Funnel Extraction _ YeaData Analyzed! 12/04/90 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor! 10.09/lOiLPercent ttoiature! 19.9
C,A,S,Nuiber
12674-11-2 Arochlor-1016, , , , , , 13000 U11104-28-2 Arochlor-1221. ..... 17000 U11141-16-; Arochlor-1272. ..... 13000 UH469-21-9 Arochlor-1242, ..... 13000 U12672-29-6 Arochlor-1248, ..... 17000 U11097-69-1 flrochlor-125'4. . , . . , 3300011096-82-; Aroctilor-1260. ..... 17000 U
'•-J
Fori 1 7/85
0 ' 100025
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CERTIFICATE OF ANALYSIS
HAZARDOUS SUBSTANCE LIST ^(solid) ' '
SAMPLE ID: E6284
CLIENT ID: S-5
SAMPLE DATE: 11/9/90
METALS MDL (ag/kg) RESULT (ag/kg)
ALUMINUM 5.00 8300ANTIMONY 0.13 N.D.ARSENIC 0.13 11.6BARIUM 12.5 103BERYLLIUM 0.50 0.68CADMIUM 0.50 N.D.CALCIUM 2.50 545CHROMIUM 0.50 111COBALT 2.50 16.0COPPER ' . 0.50 209 0'IRON 2.50 50400LEAD 2.50 941MAGNESIUM 2.50 783MANGANESE 0.50 649MERCURY 0.05 1.30NICKEL 2.50 15.4POTASSIUM 5.00 447SELENIUM 0.13 1.53SILVER . 0.50 H-DSODIUM 2.50 630THALLIUM 2.50 N-D-VANADIUM 2.50 < 55>2ZINC 0.50 142
CYANIDE 0.10 100026 *-60
o
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Lab Kant I Bridgeport Enviroimntel, Inc. I Saiple Nurier ICase No i N/A I E6284 I
ORGANICS ANALYSIS DATA SHEET ..................(Paga 7)
Pe«ticido8/PC8s ••
Concinlrationi (!OM> hediui .( Circle One ) GPC Cleanup „ Yea _/DifData Extrected/PrepTfed! 11/13/90 Separator^ Funnel Extraction _YesData Analyzed! 12/04/90 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor: 10.01/lOiLPercent Itoisture: 24,8
C.A.S.Nuiber
12674-11-2 Arochlor-1016, , , . . . 13000 U11104-28-2 Arochlor-1221, ..... 13000 U11141-16-; Arochlor-1232, ..... 13000 U53469-21-9 flrochlor-1242, ..... 13000 U12672-29-6 Ai'Ochlor-1246. ..... 17000 U11097-69-1 Arochlor-1254, ..... 14000011096-62-; Arochlor-1260. ..... 17000 U
Fori 1 7/6;
100027
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CERTIFICATE OF ANALYSIS
HAZARDOUS SUBSTANCE LIST(solid)
SAMPLE ID: E6285
CLIENT ID: g-o
SAMPLE DATE: 11/9/90
METALS MDL (ag/kg) RESULT (ng/kg)
ALUMINUM 5.00 13800ANTIMONY 0.13 „_„ARSENIC 0.13 16.4BARIUM 12.5 230
CADMIUM 0.50BERYLLIUM 0.50 u „n.u.
N.D.CALCIUM 2.50 996CHROMIUM 0.50 54<9COBALT 2.50 1?]9COPPER ' 0.50HON 2.50USAD 2.50MAGNESIUM 2.50MANGANESE 0.50MERCURY 0.05NICKEL 2.50POTASSIUM 5.00SELENIUM 0.13
HON 2.50 299003280
MAGNESIUM 2.50
MERCURY 0.05 0>261M
POTASSIUM 5.00 6710>51
SILVER , 0.50 „ -SODIUM 2.50 620THALLIUM 2.50 N QVANADIUM 2.50 -j jZINC 0.50 ' 19j
100028CYANIDE 0.10 1.07
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Lab Nam i Bridgeport Environnntal, Inc. I Saiplo Nurtor ICase No i N/A I E62B5 I
ORSANICS ANALYSIS DATA SHEET «•-•••——-••••»(Page 7)
Pesticidia/PCBs '•x-C\
Concentration! (UMJ Nedlu*. ( Circle One ) CPC Cleanup _ Yea ,/NoDate Extracted/ProjnTedi 11/13/90 Soparatory Funnel Extraction „ YesDale Analyzed! 12/04/90 Continuous Liquid-Liquid Extraction _ YeaCone/Oil Factor! 10,15/10-.Percent toisturei 27,;
C.A.S, ug/L orNuiber
12674-11-2 Arochlor-1016. . . , . , 17000 U11104-28-2 Arochlor-1221. , , , . . 17000 U11141-16-; Arochlor-1232. , , , . . 13000 U;7469-21-9 Arochlor-1242. ..... 13000 U12672-29-6 Arochlor-1248, , . . . , 13000 U11097-69-1 flrochlor-1254, ..... 29000011096-82-; Arochlor-1260. ..... 17000 U
For* 1 7/B;
100029
J
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CERTIFICATE OF ANALYSIS
HAZARDOUS SUBSTANCE LIST(solid)
SAMPLE ID: E6286
CLIENT ID: S-7
SAMPLE DATE: 11/9/90
METALS HDL (ag/kg) RESULT (ag/kg)
ALUMINUM 5.00 1900ANTIMONY 0.13 N.D.ARSENIC 0.13 0.84BARIUM 12.5 N.D.BERYLLIUM 0,30 N.D.CADMIUM 0.50 N.D.CALCIUM 2.50 177CHROMIUM 0.50 630COBALT 2.50 N.D.COPPER ' 0.50 2.21IRON 2.50 1900LEAD 2.50 5.99MAGNESIUM 2.50 122MANGANESE 0.50 4.09MERCURY 0.05 N.D.NICKEL 2.50 N.D.POTASSIUM 5.00 132SELENIUM 0.13 0.15SILVER . 0.50 < N.D.SODIUM 2.50 281THALLIUM 2.50 N.D.VANADIUM 2.50 , 9.16ZINC 0.50 3.88
CYANIDE 0.10 N.D.
100030
H the. page, med in thiA frame. iA not aA ne.adablt.on Itgiblt aA.thiAlabe.1, it iA due to AubAtandand colon on condition orf the oniginal page.
Lab KtM i Bridgeport Environmental, Inc. I Saiple Nuiber ICase No i N/A I E62B6 I
GRGANICS ANALYSIS DATA SHEET »-.....—.—..,(Page 3)
Pasticidea/PCBs >•
Concentration! I'toT) Itediui ( Circle One ) CPC Cleanup _ Yes j NoDate Extractid/PreTnrod! 11/19/90 Separatory Funnel Extraction _ YesDate Analyzed! 12/04/90 Continuous Liquid-Liquid Extraction YesCone/Oil Factor! 10.15/10-.Percent Itoisturoi 1.7
C.A.S,Nuiber
12674-11-2 Arochlor-1016. ..... 250 U11104-28-2 Arochlor-1221. ..... 250 U11141-16-; Arochlor-1232. ..... 250 U53469-21-9 Arochlor-1242. ..... 250 U12672-29-6 Arochlor-1246. ..... 250 U11097-69-1 Arochlor-1254, ..... 250 U11096-62-; Arochlor-1260. ..... 250 U
Fr,rn 1 7/85
100031
U the page filmed in thiA frame. iA not AA ntadablt.on ttgible, aA thiAlabtl, U 4.A due to 4u6^tanda/td colon on condition oi the oniginal page.
CERTIFICATE OF ANALYSIS
HAZARDOUS SUBSTANCE LIST(solid)
SAMPLE ID: E6287
CLIENT ID: S-8
SAMPLE DATE: 11/9/90
METALS MDL (ag/kg) RESULT (ng/kg)
ALUMINUM 5.00 11500ANTIMONY 0.13 N.D.ARSENIC 0.13 9.90BARIUM 12.5 146BERYLLIUM 0.50 N.D.CADMIUM 0.50 N.D.CALCIUM 2.50 1394CHROMIUM 0.50 28.2COBALT 2.50 9.12COPPER ' 0.50 60.3IMH 2.50 16700LEAD 2.50 237MAGNESIUM 2.50 1310MANGANESE 0.50 732MERCURY 0.05 1.00NICKEL 2.50 12.3POTASSIUM 5.00 1210SELENIUM 0.13 1.14SILVER 0.50 H.D.SODIUM 2.50 342THALLIUM 2.50 N.D.VANADIUM 2.50 44.8zrac o.so 101
CYANIDE 0.10 , 4.70
100032
11 the.-pa'gir'i'ilme.d in thiA frame iA not aA ntadabtt on ttgible. aA thiAlabzl, it iA due to .substandard co*o« on condition o< the o*,ig,oia,_ page.
I.—..........—ILab NIM i Bridgeport Environitntal, Inc. I Ssiple Nuiber IUse No i N/A I E6287 I
ORGANICS ANALYSIS DATA SHEET '-———•—•-•(Page 3)
Pesticides/PCBa '•
Concentration! (toi,/ Itediun ( Circle One ) GPC Cleanup _ Yea _fNoData Extracted/Prepared! 11/13/90 Saparatory Funnel Extraction _ YesDate Analyzed! 12/04/90 Continuous Liquid-Liquid Extraction _YeaConc/Dil Factor: 10,08/10-.Percent Itoiaturei 20,3
C.A.S. ug/L orNuiber
12674-11-2 Arochlor-1016, ..... 250 011104-28-2 Arochlor-1221. ..... 250 U11141-16-; Arochlor-1272. ..... 250 U53469-21-9 Arochlor-1242, ..... 250 U12672-29-6 Arochlor-1248, ..... 250 U11097-69-1 flrochlor-1254, ..... 76011096-62-; Arochlor-1260. ..... 250 U
Fon 1 7/8;
100033
li the page, itmtd in thiA frame iA not aA ntadabl.t..on ttgiblt, a.labtl, it iA due to substandard colon on condition o< the oniginal page.
CERTIFICATE OF ANALYSIS
HAZARDOUS SUBSTANCE LIST(solid)
SAMPLE ID: £6288
CLIENT ID: s-9
SAMPLE DATE: 11/9/90
METALS MDL (ag/kg) RESULT (ag/kg)
ALUMINUM 5.00 13000ANTIMONY 0.13 3.55ARSENIC 0.13 1.95BARIUM 12.5 70.8BERYLLIUM 0.50 N.D.CADMIUM 0.50 11.0CALCIUM 2.50 108000CHROMIUM 0.50 8950COBALT 2.50 53.5COPPKK ' 0.50 236IRON 2.50 51700 ^LEAD 2.50 4460MAGNESIUM 2.50 13700MANGANESE 0.50 322MERCURY 0.05 0.86NICKEL 2.50 21.7POTASSIUM 5.00 3350SELENIUM 0.13 1.20SILVER • 0.50 N.D.SODIUM 2.30 893THALLIUM 2.50 N.D.VANADIUM 2.50 43.1ZINC 0.50 1730
CYANIDE 0.10 15.0
00034 o
U the. page filmed in thiA frame. iA not aA ntadabtc. on :itgib.lt aA\thiA-.tabtl, it iA due to substandard colon on condition o& t/ie original 'page.
Lab HIM I Bridgeport Environmental, Inc. I Saiple Nurier ICase No I N/A I E62B6 I
ORGANICS ANALYSIS DATA SHEET ..................(Page 7)
Paaticidis/PCBs ••
Concentration! (ioTyttadiu* ( Circle One ) GPC Cleanup _ Yea j/hData Extracted/Prepared! 11/13/90 Separatory Funnel Extraction _ YeaData Anilyzedi 12/04/90 Continuous Liquid-Liquid Extraction YesCone/Oil Factor! 10.31/10iLPercent Mature: 44,2
C.A.S.Nutter
12674-11-2 Arochlor-1016, ..... 13000 U11104-28-2 Arocblor-1221. ..... 13000 U11141-16-; Arochlor-1232, ..... 13000 U53469-21-9 Arochlor-1242. ..... 13000 U12672-29-6 Arochlor-1248, ..... 17000 U11097-69-1 flrochlor-1254, . , . , , 22000011996-62-; Arochlor-1260. ..... 17000 U
Fon 1 7/85
•J
100035
U the. page Yarned in thiA framt iA not aA ne.adable...on ltgibtt.uA,thiAlabe.1, -it iA due to substandard co^or or co«d^t*on o< the oniginal page., ''
DATA PACKAGE
100036
I<_the page *-ed ^n th/s <rane iA not aA readab/_e_.or ttgiblt., aA thiA,labtl, it 4.A due to substawrfard co^or or eond.it.iort o{ the or^gina^ page.
CERTIFICATE OF ANALYSIS
P"'.I
SAMPLE ID: E6275
CLIENT ID: w-1
SAMPLE DATE: .11/9/90
METALS MDL(_g/L) RESDLT(ag/L)
LEAD 0.01 N.D.
100037•N y
H the. page filmed in thiA frant iA not aA ntaddbt.t.jn ligibtt aA Alabtl, 4.t iA due to substandard colon on condition o< the. oniginat page.
CERTIFICATE OF ANALYSIS
SAMPLE ID: £6276
CLIENT ID: H-2
SAMPLE DATE: 11/9/90
HDL(Bg/L) RESULT(ag/L)
0.01 N.D.
100038
U the. page, ilmtd in thiA frame. iA not aA ntadabl.t J>n Itgiblt aA thiAlabel, 4.t IA due to AubAtandand colon on condition o< the oniginal page.
CERTIFICATE OF ANALYSIS
SAMPLE ID: E6277
CLIENT ID: H-3
SAMPLE DATE: 11/9/90
METALS MDL(ng/L) RESULT(Bg/L)
LEAD 0.01 0.015
0 100039
H the. pagt^itmtd in thiA frame. iA not aA ntadable.. on Itgibte,, aA *labtl, it iA due to substandard color or co«dit*on otf the oniginat page.
CERTIFICATE OF ANALYSIS
0SAMPLE ID: £6278
CLIENT ID: w-4
SAMPLE DATE: 11/9/90
METALS , NDL(ag/L) Rj_SDLT(ag/L)
LEAD 0.01 N.D.
0
100040
o
H the. page, filmed in thiA frame. iA not aA ntadable,.,or Itgiblt a ^ . A - 'labtl, it iA due to substandard color or condition ot the oniginal page.
CERTIFICATE OF ANALYSIS——————————
SAMPLE ID: E6279
CLIENT ID: W-5
SAMPLE DATE: 11/9/90
METALS HDL(»g/L) RESULT(ag/L)LEAD 0.01 N.D.
100041s-_-X
U the. pagt \|il-ed in thiA frame. iA not aA readable or ttgible, aA thiAlabe.1, *t 4.A due to substandard color or condition o< the original page.
CERTIFICATE OF ANALYSIS
HAZARDOUS SUBSTANCE LIST(aqueous)
SAMPLE ID: E6280
CLIENT ID: W-6
SAMPLE DATE: 11/9/90
METALS MDL (ng/L) RESULT (dg/L)ALUMINUM 0.10 0.11ANTIMONY 0.005 N.D.ARSENIC 0.005 N.D.BARIUM "' 0.50 N.D.BERYLLIUM 0.01 N.D. ,CADMIUM 0.01 N.D.CALCIUM 0.05 34.9CHROMIUM 0.01 N.D.COBALT 0.05 N.D.COPPER .- 0.01 3.39IRON 0.05 0.50LEAD 0.05 1-1*MAGNESIUM 0.05 2.71MANGANESE 0.01 0.39MERCURY 0.0005 0.028NICKEL 0.05 N.D.POTASSIUM 0.10 9.69SELENIUM 0.005 N.D.SILVER 0.01 N.D.SODIUM 0.05 12.3THALLIUM 0.10 N.D.VANADIUM 0.05 N.D.ZINC 0.01 1.45
CYANIDE 0.10 N.D.
100042
lo" the page \jilmed in thiA frame. iA not aA readable ..or legible aA thiAlabel, it is due to substandard color or condition o< the original page.
Lab Haie i Bridgeport Environmental, Inc. I Sseple Nsnbtr ICaieHo i N/A I E6280 I
ORGANICS ANALYSIS DATA SHEET .........——...(Page 3)
Peslicides/PCBs ..
Concentration! (urn) Itediim ( Circle One ) GPC Cleanup _ Yes _/No *Data Extrected/Prejnffad! 11/13/90 Saparatory Funnel Extrection _/YesData Analyzed! 12/03/90 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor; lOOt/hlPercent Itoialurai N/A
C.A.5,Nuiber
12674-11-2 Arochlor-1016. .11104-28-2 Arochlor-122111141-16-; Arochlor-1232, .53469-21-9 Arochlor-124212672-29-6 Arochlor-1248,11097-69-1 Arochlor-125411196-82-5 Arochlor-1260,
Fori 1 7/8;
100043
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I *>DU I 13 AniTilt'
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100044• \J
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ub vc»- .";>i.''. UK, ;-., .
.on en IviM-
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: 100045: V~^_____ ;I ! ii M iH/a
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CERTIFICATE OP ANALYSIS
HAZARDOUS SUBSTANCE LIST(oolW)
SAMPLE ID: E6281
CLIENT ID: S-2
SAMPLE DATE: 11/9/90
METALS MDL (pg/kg) RESULT (ng/kg)
ALUMINUM 5.00 2640ANTIMONY 0.13 2.57ARSENIC 0.13 9.53BARIUM 12.5 N.D.BERYLLIUM 0.50 N.D.CADMIUM 0.50 H.D.CALCIUM 2.50 13900CHROMIUM 0.50 1860COBALT 2.50 N>D>COPPER " 0.50 186000IRON 2.50 moonLEAD 2.50 6J30MAGNESIUM 2.50 14600MANGANESE 0.50 404MERCURY 0.05 __QNICKEL 2.50 66-4POTASSIUM 5.00 1030SELENIUM 0.13 30,0SILVER , 0.50 H-J)tSODIUM 2.50 2550THALLIUM 2.50 N>D<VANADIUM 2.50 113ZINC 0.50 19700
CYANIDE 0.10 39.0100048
O
U the. page Yarned in this frame, is not as readab!e~or <«gi6le, as,t/iis ~ .label, 4.t *s due to substandard color or condition 04* the original page.
Lab Nan ! Bridgeport Envirnniental, Inc. I Seqilt Nuiber ICaaaNo i N/A I E6281 I
OR6ANICS ANALYSIS DATA SHEET <——-—•—«<P«ge 7)
Pesticides/PEs ..
Concentration! (utiyKediui t Circle One I EPC Cleanup _ Yes __ NoData Extracted/Prepared! 11/17/90 Separatory Funnel Extrection _ YesData Analyzed! 12/04/90 Continuous Liquid-Liquid Extraction _YasConc/Dll Factor! 11.08/lOiLPercent Matures 3.9
C.A.S.Huifaer
12674-11-2 Arochlor-1016, ..... 2700011104-28-2 Arochlor-1221. ..... 13000 U11141-16-; Arochlor-1272. ..... 17000 U53469-21-9 Arochlor-1242. ..... 17000 U12672-29-6 Arochlor-1248. ..... 17000 U11097-69-1 flrochlor-1254. ..... $000011196-02-; Arochlor-1260. ..... 17000 U
Fon 1 7/85
100047
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4,111 «inic«'H« irwpi•Mil
1000.8
Mil ii«iw»iwnw n
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100049
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CERTIFICATE OF ANALYSIS
HAZARDOUS SUBSTANCE LIST(solid)
SAMPLE ID: B6282
CLIENT ID: S-3
SAMPLE DATE: 11/9/90
METALS KPL (pg/ke) RESOLT
100050
ALUMINUM 5.00 «0AHTDIOHT 0.13 H-D.ARSENIC 0-13 8.36BARIUM 12.5' S-D>BERILH0M 0.50 H D.CADMIUM 0.50 1.19CALCIUM 2.50 467CHROMIUM 0.50 12.6COBALT 2.50 N.D.COPPER v< 0.50 86.4 fjHON 2.50 26500LE_D 2.50 526MAQJESIUM 2.50 163MANGANESE 0.50 189MERCURY 0.05 0.088NICKEL . 2.50 77.1POTASSIUM " '" 5.00 148SELENIUM 0.13 0.13SILVER 0.50 N.D.SODUM 2.50 507THALLIUM 2.50 N.D.VANADIUM 2.50 • 27.2ZINC . 0.50 2300
CTANtOE 0.10 *-°l
o
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n I................I
Lab Hi* i Bridgeport Environmental, Inc. I Saaple Nu*er I""' Cue (to i N/A I E6282 I
ORGANICS ANALYSIS DATA SHEET «--————-'(Page 7)
Pesticides/FCBs ,.
Concentration! (S) Hud in ( Circle One ) EPC Cleanup „ Yes VoDate Extracted/Prepared! 11/17/90 Seperatory Funnel Extraction _, YesDate Analyzed! 12/04/90 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor! 10.07/lOiLPercent Moisture! 2.;
C.A.S.Nuaber
12674-11-2 Arochlor-1116. ..... 17000 U11104-28-2 Arochlor-1221. ..... 17000 U11141-16-; Arochloi-1272. ..... 17000 U5J469-2H Arochlor-1242. ..... 17000 U12672-29-6 Arnchlor-1240. ..... 17000 U11097-69-1 Arochlor-1254. ..... 7500011096-B2-; Arochlor-1260. ..... 17000 U
Fori 1 7/8;
J 100051
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100052,.11.11! D11IIK lUDIWt
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100053
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CERTIFICATE OF ANALYSIS
HAZARDOUS SUBSTANCE LIST(solid)
SAMPLE ID: B6283
CLIENT ID: S-4
SAMPLE DATE: 11/9/90
METALS MBL fag/kg) RESDT.T (_g/kg)
ALUMINUM 5.00 7810ANT-MONT < 0.13 0.26ARSENIC 0.13 18.1BARIDH 12.5 679BERYLLIUM 0.50 0.86CADMIUM 0.50 11.0CALCIUM 2.50 10400CHROMIUM 0.50 1710COBALT 2.50 42.0COPPER " 0.50 224000IROH 2.50 199000 v—/LEAD 2.50 6220MACHESIUM 2.50 15000MANGANESE 0.50 1270MERCDKT 0.05 76.0NICKEL 2.50 112POTASSIUM 5.00 456SELENIUM 0.13 18.9SILVER . 0.50 N.D.SODIUM 2.50 714THALLIUM 2.50 N.D.VANADIUM 2.50 46.6ZINC . 0.50 13100
CTANIDE 0.10 100054 M'°
o
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Lab Neie i Bridgeport Environmental, Inc. I Simile NutberCaaeNo ! N/A I E6287
ORGANICS ANALYSIS DATA StEET <•——————(Page 7)
Pesttaides/PCBs1 ..
Concentration: (urn/ ttediui ( Circle One ) GPC Cleanup _ YesDate Extracted/Prepared! 11/17/90 Stparatory Funnel Extraction _ YesDate Analyzed! 12/04/90 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor: 10.19/1W.Parcanl tloialurei 19.9
C.A.S.Nuibar
12674-11-2 Arochlor-1016. ..... 17000 U11104-28-2 Arochlor-1221. ..... 17000 U11141-16-; Arochlor-1272. ..... 17000 U57469-21-9 Arochlor-1242, ..... 1)000 U12672-29-6 Arochlor-1243. ..... 17000 U11097-69-1 firochlor-1254. ..... 7700011196-82-5 Arochlor-1260. ..... 17000 U
For* 1 7/ft
100055
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100056
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O. ______ 100057
ITiii
' U_the page \jil-ed in this <rame is not as rea-able or legible as thislabel, it AS due to substandard color or condition 04* the original panriginal page.
CERTIFICATE OF ANALYSIS
HAZARDOUS SUBSTANCE LIST(solid)
SAMPLE 10: E6284
CLIENT ID: S-5
SAMPLE DATE: 11/9/90
METALS HDL (ro/kg) RESULT (»s/kg)
AUnONDM 5.00 8300ANTIMONY 0.13 H.D.ARSENIC 0.13 11.6BARIDH 12.5 103BERYLLIUM 0.50 0.68CADMIUM 0.50 H.D.CALCIUM 2.50 545CHROMIUM 0.50 111COBALT 2.50 16.0COFFER * 0.50 209DON 2.50 50400LEAD 2.50 941MAGNESIUM 2.50 783MANGANESE 0.50 649MERCDRT 0.05 1.30NICKEL 2.50 15.4POTASSIUM 5.00 447SELENIUM 0.13 1.53SILVER , 0.50 H.D.SODIUM 2.50 630THALLIUM 2.50 H.D.VANADIUM 2.50 55. 2ZINC . 0.50 ' 142
CIAHIDE 0.10 4.60
100058
Id the page filmed in this frame, is not as ntadablt.j>n l,t,£iblt, aA A-:-label, At AS due to substandard color or condition o< thf/ original page.
\' i Lib HJK ! Bridgeport Environenntal, Inc. I Saiplft Hu-er I-' C«>aNo i N/A I E42B4 I
OflGflNICS ANALYSIS DATA SHEET »••••»-————»(Page 3)
Pesticidos/PCBs
Concentration! /LoV)/t1ediu« ( Circle One I EPC Cleanup _V« _/DoData Extrected/Pre^aiedi 11/13/?0 Separatory Funnel Extraction _ VetDue Analyzed: 12/04/90 Continuous Liquid-Liquid Extraction _ Ve«Cone/Oil Factor: 10,01/10-.Percent toisturei 24.8
C.A.S.Huaber
12674-11-2 Arochlor-lOU. ..... UOOO U11104-28-2 Arochlor-1221. ..... 1)000 U11U1-16-5 Arochler-1232. ..... 13000 U53W-21-9 Arochlor-1242. ..... 13000 U12672-29-6 Arochlor-124B. ..... 13900 U1U97-69-1 Arochlor-1254, ..... 14000011094-82-5 Arochlor-1260. ..... 13000 U
Fon 1 7/8$
100059
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100061
I^ the page filmed in this <rawe is not as readabl.e,,or legible.as..thislabel, it is due to substandard color or condition of, the original page.
CERTIFICATE OF ANALYSIS
HAZARDOUS SUBSTANCE LIST(solid)
SAMPLE ID: E628S
CLIENT ID: s-6
SAMPLE DATE: 11/9/90
METALS MDL (eg/kg) RESULT (ng/fcg)
ALUMINUM 5.00 13800ANTIMONY 0.13 N.D<AKSENIC 0.13 ifi.4BARIUM 12.5 230BERYLLIUM 0.50 H.D.CADMIUM 0.50 H.D,CALCIUM 2.5C 996CHROMIUM 0.50 54.9COBALT 2.50 19.9COWER " 0.50 248 /"">,DON 2.50 29900LEAD 2.50 328QMAGNESIUM 2.50 1310MANGANESE 0.50 744MERCURY 0.05 0,26NICKEL 2.50 16.1POTASSIUM 5.00 £71SELENIUM 0.13 0.51SILVER , 0.50 NiD.SODIUM 2.50 6ZOTHALLIUM 2.50 N.D.VANADIUM 2.50 • 72.7ZINC 0.50 193
CYANIDE 0.10 1.07
o1C0062
U the, page, filmed in this frame, is not aA readable or legible as this -,label, At AS due to substandard color or condition o< the original page.'
Lab Ham i Bridgeport Environiental, Inc. I Staple Nueber ICase* i N/A I E«B5 I
ORGANICS fWLVSIS DATA SHEET «—-———--•(Page Jl
Pe«ticidea/PC8j-*.
Concentration! (uijtlodiui (Circle One) ETC Cleanup „ Yes i/HoDate ExtracttdifrcjUfedi 11/11/90 Separatory Funnel Extraction _YesData Analyzed! 12/04/70 Continuous Liquid-Liquid Entraction „ YetCone/Oil Factor: 10.15/10-.Pircent Itoislure: 27.$
C.fl.S, ug/l orNuater "
12674-11-2 flrochlor-1016. ..... 1)000 U11104-28-2 Arochlor-1221. ..... 13000 U11141-16-5 drochlor-12)2. ..... 13000 U5J465-21-9 Arochlor-1242. ..... 13000 U12672-29-6 flrochlor-1248. ..... 13000 U11097-69-1 flrochlor-1254. ..... 27000011096-82-5 ftrochlor-1260. ..... 13000 U
Fon 1 7/8;
100063
H the. page filmed in this frant iA not aA readable ..or legible as thislabel, it AS due to substandard color or condition bij the original page.
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100064
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1 Tvti* i j.tnibit
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100065
I< the page filmed in this frame. iA not aA readable ,or. legible, a>./th.<>label, At AS due to substandard color or condition o(, the original page.
CERTIFICATE OF ANALYSIS
HAZARDOUS SUBSTANCE LIST(uolld) _
SAMPLE ID: E6286
CLIENT ID: S-7
SAMPLE DATE: 11/9/90
KETALS HDL (-g/kg) RESULT (ng/kg)
AUnOMUH 5.00 1900AMTDtONI 0.13 H.D.ARSENIC 0.13 0.84B-UDH 12.5 H.D.MimilM 0.50 N.D.CiDHIDM 0.50 H.D.CALCICM Z.50 177CHROMIUM 0.50 630COBALT 2.50 R.D.COWER *' 0.50 2.21IBOH 2.50 1900 V_>LEAD 2.50 5.99MACHESniH 2.50 122MAHGANESE 0.50 4.09HEBCDRT 0.05 H.D.NICKEL 2.50 N.D.POTASSIUM 5.00 132SELENIUM 0.13 0.15SILVER , . 0.50 N.D.SODIUM 2.50 281THALLIUM 2.50 N.D.VAHADIUM 2.50 9.16ZINC . 0.50 3.88
CTAHIDE 0.10 N.D.
. 1COOB6
n the page filmed in this frame. iA not aA readable or legible a.* thislabel, At is due to substandard color or condition o< the original page.
Lab NaM i Bridgeport Environuntal, Inc. I Stiplo rtaber ICase No i N/A I K286 I
OREftNICS ANALYSIS MTA SHEET «•-—•——••—-»(Page 3)
Pesticides/PCBs
Concentration! (Cm} ttediui ( Circle Ono ) GPC Cleanup _ Yea JflbDate Entracted/PreHfMi 11/19/90 Separatory Funnel Extraction _ YesData Analytedi 12/04 0 Continuout Liquid-Liquid Extraction _ YesConc/Dil Factor! 10,15/lOiLPercent Itoiature! 1.1
C.A.S.Nualier
12674-11-2 Arochlor-lOU, ..... 250 U11104-28-2 ftrochlor-1221, ..... 250 U11141-16-5 rVochlor-1232. ..... 250 U53469-21-9 ftroctilor-1242. ..... 250 U12672-29-6 Arochlor-1248, ..... 250 U11097-69-1 (Vochlor-1254, ..... 250 U11196-82-5 Arochlor-1260, ..... 250 U
Fon 1 7/85
100087
If, the page \jil-ed in this framt iA not aA readable or ,',e'gib|e as thislabel, At is due to substandard color or condition of, the original page.
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100069
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CERTIFICATE OF ANALYSIS
HAZARDOUS SUBSTANCE LIST(solid)
SAMPLE ID: £6287
CLIENT ID: s-8
SAMPLE DATE; 11/9/90
METALS HDL (as/kg) RESULT (_g/kg)
ALUWWm 5.00 11500ANTIMONY 0.13 N.D.ARSENIC 0.13 9.90BARIUM 12.5 146BERYLLIUM 0.50 N.D.CADMIUM 0.50 N.D.CALCIUM 2.50 1394CHROHIUH 0.50 28.2COBALT 2.50 9.12r'PER '« 0.50 60.3_.-/N 2.50 16700LEAD 2.50 237HACHESIUH 2.50 1310MAHGAHESE 0.50 732MERCDKY 0.05 1.00NICKEL 2.50 12.3POTASSIUM 5.00 1210SELENIUM 0.13 1.14SILVER , 0.50 N.D.SODIUM 2.50 342THALLIUM 2.50 N.D.VANADIUM 2.50 44.8ZINC 0.50 101
CYANIDE 0.10 4.70
o100070
If, tht page, filmed in thiC frame is not as rea-able^cr legible,as .this-label, it is due to substandard color or condition of] the. original page.
I.-......——..* _Lab Neie i Bridgeport Environiental, Inc. I Saaple Hunter I . iCeaaNo i H/A I E62B7 I
ORGflNICS ANALYSIS DATA SHEET ,......— .......f(Page 3)
Pealicid«-/PC8s
Concentration: (jS) fedim ( Circle One ) ETC Cleanup „ Yee _C"NoData Extracted/Prepared! 11/13/90 Separator^ Funnul Extraction _ YesDate Analyzed! 12/04/90 Continuous Liquid-Liquid Extraction _ YeaCone/Oil Factor: 10.t8/10iiPercent Itoiiturai 28.3
C.A.S. ua/L orNuaber
12674-11-2 flrochlor-1016. . . , . , 250 U11104-28-2 Arochkr-1221. ..... 250 U11141-16-5 Arochior-1232. ..... 250 U5J469-21-9 Arochlor-1242. , .... 250 U12(72-29-6 Arochlor-1248. ..... 290 U11097-69-1 Arochlor-1254. ..... 76011196-82-5 Arochlor-1260, . . , . , 250 U
Fori 1 7/65
100071
U the page, filmed in thiA framt iA not aA readable tor legible as this.-label, At AS due to AubAtandand color or condition o< the. original page.
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CERTIFICATE Of ANALYSIS
HAZARDOUS SUBSTANCE LIST(solid)
SAMPLE ID: E6288
CLIENT ID: S-9
SAMPLE DATE: 11/9/90
METALS MDL to/kg) RESULT (_g/kg)
ALOMINDM 5.00 13000ANTIMONY . 0.13 3.55ARSENIC 0.13 1.95BARIUM 12.5 70.8BERYLLIUM 0.50 N.D.CADMIUM 0.50 11.0CALCIUM 2.50 108000CHROMIUM 0.50 8950COBALT 2.50 53.5r™PER '' 0.50 236. ..-,N 2.50 51700LEAD 2.50 4460MAGNESIUM 2.50 13700MANGANESE 0.50 322MERCURY 0.05 0.86NICKEL 2.50 21.7POTASSIUM 5.00 3350SELENIUM 0.13 1.20SILVUR , 0.50 , N.D.SODIUM 2.50 893THALLIUM 2.50 N.D.VANADIUM 2.50 43.1ZINC 0.50 1730
CYANIDE 0.10 15.0
100074
If, the page filmed in this frame, is not as readable .or legible as this' ''label, At AS due to substandard color or condition of, the original page.
Lab Hate i Bridgeport Environmental, Inc. I Saaple NuaberCase No i N/A I £4268
ORSANICS ANALYSIS DATA SHEET • —— — ---- —(Page 3)
Pesticides/PCBs
Concentration! (Wjlfcdiui ( Circle One I GPC Cleanup „ Yea j_DoData E«tracted/Pre)nredi 11/13/90 Septratory Funnel Extraction „ YesDate Analyzed: 12/04/90 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor: 10.31/10aLPercent Itoiature: 44.2
C.A.S.Huefcor
12674-11-2 Arochlor-1016, ..... 13000 U11104-28-2 Arochlor-1221. ..... 13000 U11141-16-$ Arochlor-1232, ..... 13000 U53469-21-9 ftrothlor-1242. ..... 13000 U12672-29-6 Arochlor-1248. ..... 13000 U11097-69-1 Arocblor-1254. ..... 22000011096-82-$ Arochlor-1260. ..... 13000 U
Fori 1 7/8$
100075s~~*-(J
U the. page, filmed in this rframe is not as readable jtn legible as thislabel, At AS due to substandard color or condition o< the original page.
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100075
I< the page filmed in this <rame is not as readable or legible aslabel, At AS due to substandard color or condition of, the original page.
i.i.-rnnn i Cl'l-i;.' t iivitm H1* hue <,'•» 1770 .'"JMoiJ I LM-'Utii '. Hfcl'l'. tli. hire O'l l'i"fo j
( 5V!J7, ai:.i' uni nown{-^Sll ,Ou.uO Unnnonn2 WO. d US unl 'nowri
Unt.-nouriioQt«cnlar
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i-ir:/'1. ... i 'wfl-4 "" nor'.,),'.»: n («»)> j iHSBIiiiOii'.ni unt;nonn
T(1,0 «—
3.. i
"^
/I E T . 100076/ 11,11?
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Q C RESULTS
100077
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QUALITY ASSURANCE DATA
ANALYSIS NO: E6275 BATCH NO: H331
MATRIX: Aqueoua
HETAL AHOIIHT OF SPIKE I RECOVERY X DUPLICATE SPIKE RECOVERY
LEAD 50 ppb 101 100
100078
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QUALITY ASSURANCE PATA
ANALYSIS NO: E6276 BATCH NO: M331
MATRIX: Aqueous
HETAL AMOUNT OF SPIKE Z RECOVERY Z DUPLICATE.SPIKE RECOVERY
LEAD SO ppb 103 108
100079
If, the page filmed in this frame iA not aA readable .or legible as this nlabel, it is due to substandard color or condition of, the original page.'
QUALITY ASSURANCE PATA
ANALYSIS NO: E6277 BATCH NO: M331
MATRIX: Aqueous
METAL AMOUNT OF SPIKE I RECOVERY I DUPLICATE .SPUE RECOVERY
LEAD 50 ppb 116 92
1000SO
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QUALITY ASSPRANCE DATA
ANALYSIS NO: E6278 BATCH BO: H331
MATRIX: Aqueous
METAL AMOUNT OF SPIKE X RECOVERY Z DUPLICATE .SPUE RECOVERY
LEAD 50 ppb 111 111
o100081
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QUALITY ASSURANCE DATA
HAZARDOUS SUBSTANCE LIST
ANALYSIS NO. E6286 { I
BATCH NO. M330
MATRIX: Solid
METAL AMOUNT OF SPIKE (ug) Z 'SPIKE RECOVERY Z DUPLICATE RECOVERY
ALUMINUM 10000 100 98
ANTIMONY 50 96 83
ARSENIC 50 101 101
BARIUM 1000 108 113
BERYLLIUM 1000 104 109
CADMIUM 1000 95 99
CHROMIUM 1000 102 109
COBALT 1000 102 106
COPPER 1000 113 116 _
IRON 10000 98 96
LEAD 10000 101 101
MANGANESE 1000 97 104
MERCURY 1.00 97 97
NICKEL 1000 100 104
SELENIUM 50.0. 115 111
THALLIUM 50 99 _Q4
VANADIUM 1000 104 116
10000 96 100
100082
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QUALITY ASSURANCE DATA
HAZARDOUS SUBSTANCE LIST
nBATCH NO: M 33°
MATRIX: Solid
METAL METHOD BLANK (BE/,.) AMOUNT OF SPIKE (ug/L) X SPIKE RECOVERY
ALUMINUM «'D- 1000° 10S
ANTIMONY »•">• 50 103
ARSENIC »•»• 50 10Z
BARIUM »•»• 100° 103
BERYLLIUM "-D- 100° "
(aaoDM »-D- 100° 90
CHROMIUM "•"• 100° "
COBALT '. "•"• 100° 9B».D. 1000 98
I.D. 10000 102
H.D. 10000 106
IJARGANESE "•"• 100° 103
MERCURY "•"• * *"'
»•»• 100° 98
SELENIUM "• ' "
THALLIUM "•»• 50 8Z
VANADIUM ••»• 100° 99
"•D< 500° 98
O " • • 100083
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1
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S5£
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2EWATER PESTICIDE SURROGATE RECOVERY
>b NameiBridgeport Environmental, Contract : N/A
sb Code; NJ 08555 Case Ho.: N/A SAS No.: N/A SDG No.: N/A
1 ERA1 SAMPLE NO.
01IPBLK 266-202I_E628Q ____031 MSQ4I MSD051061071OBI091101111121131141151161171181191201211221231241251261271291291301
SI 1 OTHER(HBB)*I
135__U2_11990
BB) • Hexabromobenzene
. ———— ,
ADVISORYQC LIMITS(24-154)
# Column used to flag recovery values
* Values outside of QC li m i t s
D Surrogates diluted out
.go 1 of 1_____ FDRh II PEST-1____________ 1/87 Rev.
If, the page filmed in this frame iA not aA readable .or legible as thislabel, it iA due to substandard color or condition oi the original page.
2FSOIL PESTICIDE SURROGATE RECOVERY
»b NameiBridgeport Environmental, Contract : N/A
tb Code: NJ 08555 Case No.: N/A SAS No.: N/A SDG No.: N/fl
jvel: (low/mod) LOW
I EPAI SAMPLE NO.
Oil PBLK 288-502lmPBLK 292-1.,03|_E62B1 ____041 E6282 ____05I_E6283 ____061 E8284 ____07I_,E6285 ____081 E6286 _____09I_E6287 ____101 E6288 ____
121 MSD131141151161171181191201211221 ___231241251261271 ___281291301
SI I OTHER(HBB)#I
109JL14_D_D_D_D_D
ADVISORYPC LIMITS
51 (HBB) - Hexabromcbenzene (20-150)
4 Column used to flag recovery values
* Values outside of OC limits
D Surrogates diluted out (J
»» Surrogate recovery cannot be calculated due tocoelution of PCB 1260 and HBB peaks.
age 1 of 1FORM 11 PEST-2 1/87 Rov.
I(i the page filmed in this tframe is not aA readable..or,.legible.as,tfcis.label, it is due to substandard color or condition of, the original page.
3F
! JUEOUS PCS MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
NameiBridgeport Environmental, Contract:N/A
Codes M 08555 Case No.: N/A SAS No.: N/A SDG No.: N/A
rix Spike - EPA Sample No.: E34S5 ''Level! (low/med) LOU
COMPOUND
rochlor 1016,., _„...,.rochlor 1221 . . .. „roohlor 1232:rochlor 1242rochlor 1242.rochlor 124B _rochlor 1254in lor 1260, ,..,,
COMPOUND
.rochlor 1016 , ,„„., ,
.rochlor 1221 ,
.rochlor 1232,,,, ,,,, , ,. l,rochlor 1242irochlor 1248.. . ., „ ,. ,,.rochlor 1254irochlor 1260 ,
SPIKEADDED(ug/L)
N/A50
N/AN/AN/AN/AN/AN/A
1 SAMPLE1 CONCENTRATION
<ug/L)
O.Q0.00.00.00.00.00.00.0
SPIKEADDED'(ug/Kg)
N/A50N/AN/AN/AN/AN/A •
MSDCONCENTRATION
(ug/Kg)
N/A74N/AN/AN/AN/A
MSCONCENTRATION
(ug/1)
N/A52
N/AN/AN/AN/AN/AN/A
MSDX
REC ft
N/A147N/AN/AN/AN/AN/A
SRPD ft
N/A34
N/AN/AN/AN/A_N/A_
MS1 H
REC ft
N/A104N/AN/AN/AN/AN/A_N/A_
QC LRPD
QCLIMITS
REC.
MITSREC.
lolumn to ba used to flag recovery and RPD values with an asterisk
'•lues outaida of qc limits
): 0 out of 6 outside limits 1000 7.ke Recovery: 0 out of 12 outside l i m i t s 4.UUU-M
1MENTS: BA 266.
FORM 111 9/90 Rev.
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*- <<; »« jugs : SK! i HISS W S
.••MMini flTONimni) i ARM i
*„. K B-PRI «• ""•"« •""u l lAOMttO 9MIW.WOO UnVnoxnv ', ooo,,g MM9.0COO UnhnoHO
' «S«.S6!3 UnknQHnI.7W.9S7S UnHnsm
SSS:SSIl(aol7""s"
Ml! i 111T ' "iWWi«0 S5BS9I.MOO
,w; S T !"1r*
i ». SWW.BW
MWS.WW Unkno-n . •.
X-x'
. h.' ft S
|«_
N ti M H NC U t f »s ': f t f
« Ft it ! nc it
100088
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.'l'i'JWU rtvml !t i:«»9«nant N|,«o«r i I Tvp» I Unwilt
uctum'tV/ilM.* mm '•'•' ' "":' 111'""!! ' ""l." c ISiSSiW nufl 0= I99D )HI 4Hunt Minimi.-. '««l v.1 iv"" niiitiinl i niK.il I UiJSlJV nun gi' i'i'/i, Jn i iMidiv* nuii u.i iwv finthoo i null I I OHiOuu*. mm us uw Jl>l \i I .uiMXnnXiO PMIutimi I.OOiMU»««iO
i I rcKNAl. STflNUflhU I (WEfl I
.1 nr.. K EllBFiT RF PICMRAna N...
153750 1UfaUSJ? 1
IS'.B "
.449 III33I T
.7*0 . 40117 T145. /ISS705 T
'.1S6 ««' T 4.I4W4S9 94G7B T 4.497;K 40412 1 9.011:M :»llMl :7U4i'l 1.415Iv-i si.'!!.'. '>.•>!>.'
IO.QI111,371
UnknpnnUnknpnnUnknnnnUul'minli
M>u6.>li'/ti UnHnpwn131:31.4688 Unknpnn40147.3031 Unknpnn
.OOOOO.tO 133703,6330 Unknpnn
.OOOOOntO 301303.9373 Unknpnn,930561-4 A-BHC.iMmiXicitrj 'l',i4llS.I,'.'50 Unknpnn
3.5641.BIG
,90640*-4 19,0903 HEPTACHUQR. IBOIB.-4 17,3078 D-BHC.1Q742I-4 9, 8479 (1LDRIN.ODOOOQtO 3f.lll.'J/M) UnhnQnn.»IJ07i-4 J.A'17 HBPTW!Ml.l)» Win I ISi :. I.NIIU-I
PP-DD6»Ut-4 DIEUOnlN
tut IttlOlt 13. 85! 2, 384781-4 6.3751 CNDRIN16,976 3.3143M-1 OOU/tHCU-l I19.843 i,7t337.-« PP-CPI31,313 ;,36490>-4 ENDRIN HLOEHrDE
U8D 100707 23.830 S,91330t-4 39.7611 ENDOSUkFdN UUUFftTE473 71Q733 T 31.969 S, 649791-4 19U.IS93 HEX«6llOnDUtHJENli.'ai;117 2B9902 1.00000«»0 VOW!, 0009 Unknonn . ,
».1J; 4,6ll}4«-4 nCTHOXVCHUOR
3 ,« «»»-'"•«•» «"j ' l 4'f'i>
N T ) N M
t«,i +
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II )>,« i
100069 !
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3F
SOIL PCS MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
3 NameiBridgeport Environmental, Contract:N/A
3 Code: NJ 08555 Case No.: N/A SAS No.: N/A SDG No.: N/A
trix Spike - EPA Sample No.: E6241 'Level:(low/mod) LOW
COMPOUND
Irochlor 1016Irorihlor 1221Irochlor 1232irochlor 1242irochlor 1242Irochlor 1248irochlor 1254irochlor 1260
COMPOUND
irochlor 1016irochlor 1221frochlor 1232irochlor 1242irochlor 1248trochlor 1254Irochlor 1260
SPIKEADDED(ug/Kg)
N/AN/AN/AN/AN/AN/AN/A
1000
SPIKEADDED(ug/Kg)
N/AN/AN/AN/AN/AN/A
1000
1 SAMPLE1 CONCENTRATION
(ug/Kg)
Q.O0.00.00.00.00.00.00.0
MSDCONCENTRATION
(ug/Kg)
N/AN/AN/AN/AN/AN/A
1300
1 MS[CONCENTRATION
(ug/Kg)
N/AN/AN/AN/AN/AN/AN/A890
MSDN
REC «
N/AN/AN/AN/AN/AN/A130_
SRPD ft
N/AN/AN/AN/AN/AN/A35
1 MS1 XREC *
N/AN/AN/AN/AN/AN/AN/AB9
QC(LIMITS1 REC.
QC LRPD
HITSREC.
Column to be used to flag recovery and RPD values with, an asterisk
Values outside of qc limits
): 0 out of 6 outside limits•.ke Recovery: 0 out of 12 outside lim i t s
1MENTS; BA 288.
luuoyo
FORM III 9/90 Rev.
If, the page filmed in this frame is not as readable or legible as thislabel, At AS due to substandard color or condition of, the original page,
I •-: '• ..'"'.. . ..'il'lli I0u thl HlU»»m«(W. i ':: fvot i &«mp|»> u.' i .1 -•.•::;.:,u'..». i .ii-:i:i we '.c iviij .lotnon i ".ui.ii i IDHSI.I& L'.I- i.; 119(1 jInuprmoni u'ti/ino rue ,c, 1*10 notnoo i nui.1I : ,<,i.>5i46 u«; 05 IWi )>«wt , i:tii>ti,t in. v: ivx- -.nan i HULTI i lotusiM \at os 1990 I
f \ iiiffipl
..lOOi!) Jnl.nph'...0000 jnknpn
( ,. L'HL' Unl.nflnn
T.496 ;.MS77«-«. ,Voi ..^HliViB-l -l.llioo ll-HHC-.lOCi •,:.I79M«-A i.i'HBi-
...i gCW*.'.. •. . ijui.ii.i
6.?- 72757S 1 O.OOOCJOt^O v.OOOO unnnnnnJ.l'lt 735.167 T V.90C .•,331191-4, 35.9S5B ENOD-IB.IS ' 4S«sVi' v I.I.OIWCIMV v.VUMi Unlinp»r
>, . , ..u..l»- likin. 341 A 763 II 1 O.OOOOfmtO v.OOOO Unknpnn11.107 145310 v O.OOOdOtn'i .'..;MUU unhnn.r<
\ I1.US3 :;.B«H7l«-4 ENBR1NU.a;- )S8"3'." " %'.(i4<iMwt(i 0.00'.*.. unKnonr.(::v.v;i v 17.14.055 Vs;?'.''a T O.OOOOOotO 0.0000 unlinonn
14.450 S,160:SO"H fP-l)DT17.231 (I6a4':i« .;i,uC,W"iinii :.,«nv, .jniinpnn
^ :..,':.'.' •LMamv-ii BNURINJl.S7i HHIVI: '
T :t,164 -.1449711-4 !7o,8409I'j.OOOOC'p O C>,M'>;iC> Unhnpnn
.U.060 7.0B667«--
, -<! « U t * «t : i : c s
i ••»•
100091
Ifj the page filmed in this iSrame is not as readable or legible as this-label, At AS due to substandard color or condition of, the original page.
.;ilUc'.>:r. I .LlMlVi !« ,V! \11v :ictncd I nuuT! t IOI4SI46 5«r 03 H90 I\r •.nan-.iHtt .JiS'.H!! !>- o1.' il'':1 fQtnos i rji.ri ; iui4MH6 If: 03 I9»ft :I'.awr.f -. i :'!•• -.1 .iiu' ...' si-*, "ss.ua i .-L.i.n .. KM'i5i4f. .«« u'J 1940 )
rj.i.oOM <*ni nownO.oywo ,unl:nphnO.i.'yC'O 'unknuwn0.0000 Unknpn".js.snvs n-wn
J',,I4J1 D-DHC
n,T/t ;i,-w.'- 0.i.<p."X'...»+o i''.0'.'''Xi unknownft, 645 <*l*?6-» • 0 . .';OCii.H'.'»+0 0.0000 Unknown
i,l')S EJ.!3'7:0>-3 HfpTflt'llLOfis.11;!: -*.ua70 T 0 . 'X'MOaTO 0.0000 Unlinonn7. M,I .:,'..ivi i i.. i,,r. .',:.T«»,O..(I IS9.P/W l"NI)0-iU.^VI .'lif'll I ',. A.'.'WWH> II.I.U.JI.. Ulll M(>nl.9,341 IS'.HV T B, 9V l./4!77e-4 '.'6.425V PI—UkE
7, MB !.«r9:!u-J DIGWRINO.oOOMoK' 0.0000 UnhnonnO.'ivO'WB'O O.ooOO gnlmpm
11.6:3 3,S947le-4 tNDRINo.i|.X"X'V<u 0, 0000 UnKnown
O: V 1C.90:. 3.1f)374p-4 la.uTIt DDP/ENDq-llI6,n'i9 -Aim"! '' u.iWidfmiMn D.oi'ifif. unKncmn
I*,, •»»!.• U.^W^OIt-4 H'"l)IH17.245 U'sCMD «J.OC.OOO«rO U.OOOO Unknpnn
18.437 3,;6i99>-4 tNUFlIN AUOEh^DE:ii60B I'!I347 1 O.uOWOt-f. 0,0000 Unknpnn
V'2,64* 3.:i'7;a«-<. CNDOSULFAN SULFATE:3,10? l:oc043 V ;;,I64 4.l«670it-4 SSS. 6199 HEXflURDNODENIiNE-sE30.014 mi)4994 0.00000»»(i O.OOilO Unknown
51.060 7.0B667P-4 M6THIHYCHI.OR
» s> !PF3 _ M,mu> hi),o«K'1
100092
H the page filmed in thiA frame is not as readable .or legible as thislabel, At AS due to substandard color or condition of, the original page.
BE^ PESTICIDE EMALUATION STANDARDS SUMMARY, sluation of Retention Time Shift for Haxabromobonzeno
ib NameiBridgeport Environmental, Contraot:N/A
ib Code: NO 08555 Case No.: N/A SAS No.: N/A SDB No.: N/A
istrument ID: PE-1 GC Column ID: PRIMARY
ites of Analyses: 12/03/90 10:10 to 12/04/90 20:04
•J
1 EPA 1 LAB SAMPLE1 SAMPLE NO. ID
Oil IPCB 1221/1254021031
PCS 1016/126Q_PBLK 266-2
041 IE628D051 IPBLK 2U8-3061 IPBLK 292-1 _071081091
PCB 1016/1260_PCB 1221/1254_E62B5
101 IE6286111 IE62B1121 IE6282131 IE62B3141 IE6284151 IE62B7161 IE628B1711811912012112212312412512612712BI301311321331341351361371381
DATEANALYZED
_12/Q3/90__12/03/9Q12/07/90
_12/03/90,__12/03/90_,_12/03/9Q_12/04/90
_12/04/90__12/04/90__12/04/90_._12/04/9Q__12/Q4/90__12/04/9Q,,_12/04/90__12/04/90__12/04/90_
TIMEANALYZED
10:1013:0413:47U:2515:0615:4507:3508;2515:3516:1616:5917:3618:131B:5019:2720:04
———— 11
SD„
_o.i_0.2_
_o.i_o.i_0.1
_0.6_0.4_D
_0.1^DD0.6~ D0.2-D
fWJS
i* Values outside of QC limits (2. OS for packed columns.0.3H for capillary columns)
»m
q_*
ge 1 of 1FORM UIII PEST-2
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. «u_r i :.i.*ir' £« ol mo flotnon i nuuTI . v7ior)i3S DKC gs WO Jnt.:*: '.-t','-' if?i 0" 1'*'"' !«i?r.rK»fi i MUL "J t I'.''|4!J|46 Dur O'i l-'/V't :
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hltt ! 1 .',"•• I'-'l-'V-*1.1-'!.. UllUtlOl't i .OCiOin.ipi-001.'
,i6S l'Bi6; v l,i*.ui.0>*
S67 ilvJ1; '1 I.V'XKmt107 i-l'Mt; t J.065 A.HSiK'l)-
.ava a»:it • l.ilwut*,1*1 B'.P|J'!I ' iiiaS 4,s i.i ',p->>i3Z «3'4-', " 1 , OOOUUtf .•a>. .'„••£; • .•.,;ii'. •;.ir'i...iu»i'.l; 'a>'lb ' ' ' lixv'iiU'..'s' ^..|i '. ,«."«lnr
llA" I.1.'*.... ..'.".... J1.1 *
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r/Mvioli:920«v.VltJU99S6.6U5I
adSle.iiiiOOMS6.0V034nsi]4. i«30i62'..;6'j?07011!. ?tdutMl'I.VKU
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:t;:i.;:0«;;..K*n
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100094
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t, , .. ,,, : ... !-. ,:,,-; ;'.',o '.no dillum*, tt. " _ t_ i vi»« i ruiinim-
•>*4ifc<:-_;'i i i:t';-iiH five 0.; l?i» ivtnao i ruuft ; .tfctSHt, u*c 05 1*90 JIr.t.-rniont I'l'.-fl-: JVc H-* f.-V, i-flthoa I MUuTI C 1 a 1 86 1 33 &«c i* 1»90 1'_•;-.•• I ..II-.HI was O-i 1 ; '. Hrtt-.hfi.l t MULT I . ..OHUlOl !)t!- '>H I1? 'JO i
i'l' • -.'UA 1 \ MWHUflLLV
n , 1.11,11/1 ' 'jr.i'noHn
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1 1 H'II..I:OO+ "".,%>«••-«
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;. Iki.Nh.. ii.'iiniMi.i. . ..i.;.' 1 - .'IMI.UHU... ....-i''
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ENDU-I
DICUDrilNCNt/hlll
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-i.in !•
'ii.in »«,'[*»• 11l I'
. , |II.M) PIIIIH (tlfflltl
jo.a - '. '
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100096
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8E-N PESTICIDE EVALUATION STANDARDS SUMMARY
I aluation of Retention Time Shift for Hoxabromobonzone
| ab NameiBridgeport Environmental, Contract:N/A
ab Coda: NJ 08555 Case No.! N/A SAS No.: N/A SDG No.: N/A
Natr-m-nt ID: PE-2 GC Column ID: CONFIRMATORY
ates of Analyses: 12/03/90 13:47 to 12/04/90 22:15
1 EPA1 SAMPLE NO.
O i l021031041051061071081091101111121131141151161171181191201211221231241251261271281301311321331341351361371381
1 LAB SAMPLE1 ID
IPCB 1016/1260IPCB 1221/1254PBLK 266-2IE6280PBLK 292-1IPBLK 288-3E6281IPCB 1016/1260.,E62B2PCB 1221/1254E6283E62B4E6285E6286E6287E62BB
DATEANALYZED
12/03/9012/03/9012/03/90
_12/03/90_,_12/Q3/9Q_,_12/03/90__.12/03/9Q__12/04/90__12/04/90_12/04/90_12/04/9012/04/90
_12/04/90__12/04/90__12/04/90_12/04/90_
TIMEANALYZED
13:4714:2314:56,15:2916:0317:1017:5608:3B09:2711:3315:4416:1916:5121:0021:3722:15_
SD
_0. 10.40. 10.0
_0.2_D0.3D0.3DDD0, 10,2D
___
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PEST/HERB/PCB ^^ BLANK SUMMARY
ab NameiBridgeport
ab Code: NJ 08555 Case ^O.i N^ QflS No.s N/A SDG No.: N/A
)b Sample ID: BA266 Uab File ID' BLflNK #2
at rix: (soil/water) WATER Uovel s ( iow/med) LOW
ate Extracted: 11/13/9Q Extraction: ^SepF/Cont/Sonc )SepF
ste Analyzed (1): 12 03 5,0 Pate Analyzed (2): 12/03/90
ime Analyzed (1): Uftj? Time final yz"d (2): 14:56
istrument ID (1): PS>i 'natPunient 1° ^2): PE-2
: Column ID (1): PRIORY SC Column ID (2): CONFIRMATORY
THIS METHOD BkANK AfPUlES TO THE FOLLOWING SAMPLES, MS AND MSDi
DATE I DATE ISAMPLE No- SIMPLE IP I ANALYZED 11 ANALYZED 21
1MMENTS:
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100105
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4CPEST/HERB/PCB METHOD BLANK SUMMARY
ab NameiBridgeport Environmental, Con tract: N/A
ab Code: NJ OB555 Case No.: N/A SAS No.: N/A SDG No.: N/A
sb Sample ID: BA2BB Lab File ID: BLANK #3
atrix: (soil/water) SOIL Level :( low/mod) LOW
ate Extracted: 11/13/90 Extraction: (SopF/Cont/Sonc )Sonc
ite Analyzed (1): 12/03/90 Date Analyzed (2)1 12/03/90
ime Analyzed (1): 15:06 Time Analyzed (2): 17:10
istrument ID (1): PE-1 Instrument ID (2): PE-2
: Column ID (1): PRIMARY GC Column ID (2): CONFIRMATORY
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:
1 EPA1 SAMPLE NO.
Oil021031041051061071081091101111121131141151161171iei191201211221231241251261
LAB 1 DATE 1 DATESAMPLE ID (ANALYZED 11 ANALYZED 2
E5281E52B2E52B3E52B4E52B5E52B7E52BB
_12/04/90__12/04/90_12/04/90
_12/04/90_12/04/90_
_12/04/90__12/Q4/90_,
12/03/90_12/04/90__12/04/90__12/04/90__12/04/90_12/04/90..
_12/04/90_,
JMMENTS:
100106
O-.go 1 of 1
FORM IY PEST 1/87 Rev.
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100107
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4CPEST/HERB/PCB METHOD BLANK SUMMARY
ah NameiBridgeport Environmental, ContractiN/A
ab Code: NJ 08555 Case No.: N/A SAS No.: N/A SDG No.: N/A
ab Sample ID: BA292 Labfilo ID: BLANK #1
atrix:(soil/water) SOIL Levo1;(low/mod) LOW
ato Extracted; 11/19/90 Extraction: (SepF/Cont/Sonc)Sonc
ate Analyzed (1): 12/03/90 Date Analyzed (2): 12/03/90
ime Analyzed (1): 15:46 Time Analyzed (2): 16:03
istrumont ID (1): PE-1 Instrument ID (2): PE-2
: Column ID (1): PRIMARY GC Column ID (2): CONFIRMATORY
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:
1 EPA1 SAMPLE NO.
Oil021031041051061071OBI0911011111211311411511611711BI191201211221231241 ,'251 ''261
LAB 1 DATE 1 DATESAMPLE ID 1 ANALYZED 11 ANALYZED 2
E5286
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_12/04/90_ _12/03/90_
100108
3MMENTS:
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UbKaiai Bridgeport Environmental, Inc. I Saiolt Nuabar ICm No i N/A I PBLK 266-2 I
OR9ANIC5 ANALYSIS DATA SHEET (................t(Page }>
PetticidBS/PCBs ••
Continuation: t \s&j Ifediui ( Circle Una ) GPC Cleanup _Vnj _.NoDale Extracted/Prepared: 11/13/VO Saparatory Funnal Extraction _,YaaData Analyiad: 12/03/50 Cantinuaua Liquid-Liquid Entraclion _ VaaCone/Oil Factor: 100iL/5_.Perctnt tloisturo: N/A
C.A.S.Nuibar iig/Kg
12674-11-2 Arochlor-1016, ..... 1} U11104-28-2 Arochlor-1221. ..... 13 U11141-16-5 flrochlor-1232, , . , , . 13 U5J«?-21-9 Arochlor-1242. ..... 1J U12672-27-6 Arochlor-1248. . , , , . 13 U110??-69-l Arochlor-1254, ..... 1} U110W-62-5 Arochlor-1260, 15 U
Fori 1 7/85
.100110
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Lib HIM : Bridgiport Environmental, Inc. I Saipla Nuafcer ICate No : N/A I PBLK 280-J I
ORCANICS ANALYSIS DATA SHEET t................*(Page 3)
Pesticidea/PCBs ••
Concentration; ^ Low , flediui ( Circle One ) GPC Cleanup _, Yes j. NoData Extracted/Prepared! 11/13/90 Separator^ Funnel Extraction _ YeaData Analyied: 12/03/90 Continuous Liquid-Liquid Extraction _ YeaCone/Oil Factor: 10.00g/10ilPircant Itoisturei N/A
C.A.S. ug/L orNuabir
12674-11-2 Arochlor-1016, , , . , . 250 U11104-28-2 Arochlor-1221, ..... 250 U11141-16-5 Arochlor-1232, ..... 250 U53W9-21-9 Arochlor-1242. ..... 250 U12672-29-6 Arochlor-1248, . , . . , 250 U11097-69-1 Arochlor-1254, ..... 250 U11096-82-5 Arochlor-1260. ..... 250 U
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Lab Nan i Bridgeport Environmental, Inc. I Saiola Nuriter ICaaaNo i N/A I PBLK 292-1 I
ORGANICS ANALYSIS DATA SHEET ..................(Page 3)
Pesticides/PCBs ••
Concentration; > _oj> IfediiM ( Circle One ) GPC Cleanup _ Yet _. NoData Extracted/Prepared: 11/19/90 Sepiratory Funnel Extraction _ YeaDate Analyzed; 12/03/90 Continuous Liquid-Liquid Extraction _ YoaCone/Oil Factor: lO.OOg/KM.Percent Matures N/A
C.A.S. ug/L orNuiber /ub7Kr,
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100114
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Bridgeport Environmental Inc. u.,««iA..ylic,iui»r.wri«, W[,___________________________________________________j_08665__§lP.O.Box 247 609/467-0380510 Heron Orlva Suite 107Bridgeport, NJ 08014-0247
WESTON
PROJECT: SNOW HILL LANE
DATE RECEIVED: NOVEMBER 16, 1990
RETORT NO: E6327-E6330
BRIDGEPORT ENVIRONMENTAL, INC.
RICHARD W. MUCH ALABORATORY MANAGER . i
IV0116
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r-AMPLE LOCATION AND IDENTIFICATION
ANALYSIS HO. CLIENT ID
B 6327 W8
E 6328 N9
B 6329 SI
E 6330 S10
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METHODOLOGY SUMMARY
METALS Soil Samples for- metal analysis ware run inaccording with the methods prescribed in SW846.This includes a nitric acid digestion followedby either Furnace, Flame Atomic absorption,Flameless Atomic Absorption, or InductivelyCoupled Plasma analysis,
Aqueous samples for metals analysis were runin accordance with the methods prescribed inMethods for Chemical Analysis of Hater and Hastes,EPA-600/4-79-020 March 1983.
PHENOLS Analysis performed according to U.S.E.P.A. 420.1(Spectrophotometric, Manual 4AAP with distillation).Phenolic materials react with four (4) Aminoantlpyrineand Potassium Ferrlcyanlde at pH 10, Red coloris read at 510 nm.
-CYANIDE Analysis performed according to U.S.E.P.A. 335.2(Spectrophotometric with distillation). Sampleis reacted with Chloranlne-T to produce Cyanogen,Chloride, CNC1, Red color develops when combinedwith Pyrldlne/Barblturic Acid Reagent; which is redat 578 nm.
Soil samples are prepared for anlysis as prescribedin Method 9010 from SH846.
PETROLEUMHYDROCARBONS Aqueous samples were analyzed following Method 4,18,1
as prescribed in Methods for Ch-mical Analysis ofHater and Hastes, EPA-600/4-79-020 March 1983.
Soil Samples were extracted in accordance with themethods prescribed in SW-846 and subsequentlyanalyzed as stated above.
[00119
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LABORATORY CHRONICLE
nRECEIPT/REFRIGERATION______________11/16/90_________________
ORGAHICSEXTRACTION
1. Acids________________'• NA_________________
2. Bane/Neutrals___________HA________________________
3. Pesticides/PCD'a/Berblcides____NA
4. Petiole™ Hydrocarbons________NA
ANALYSIS
1. VolatUes________ NA
2. Acids__________ NA
3. Base/Neutrals______________HA
4. Pesticides/FCB'a/Herbicides_____HA
5. Petroleum Hydrocarbons_______HA
6. Total Organic Carbon_________HA
Section SupervisorReview & Approval_
INORGANICS
t. Metals__________________11/16/90 - 11/19/90
2. Cyanides________________HA___________
3. Phenols_________________HA
OTHER AHALTTES
Section Supervisor I ft n 1 O QReview t Approval ______ ______________________ *VU * *
Quality Control SupervisorReview t Approval
If fractions are re-extracted and re-analyzed because Initial endeavors v-/did not Met quallty'control acceptance criteria, Include dates for both.
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nCERTIFICATE OF ANALYSIS
SAMPLE ID: E 6327
CLIENT ID: "8
SAMPLE DATE: 11/9/90
METALS MDL (-g/L) RESULT (_g/L)
LEAD 0.01 N.D.
100121O
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CERTIFICATE OF ANALYSIS
SAMPLE ID: E 6328
CLIENT ID: W9
SAMPLE BATE: 11/9/90
METALS HDL (ag/L) RESULT (-g/L)
LEAD 0.01 N.D.
100122
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oCERTIFICATE OF ANALYSIS
SAMPLE ID: B 6329
CLIENT ID: SI
SAMPLE DATE: 11/9/90
MKIALS MDL (_g/kg) RESULT (-g/kg)
LEAD 2.50 40.0
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CERTIFICATE OF ANALYSIS
SAMPLE ID: B 6330
CLIENT ID: S10
SAMPLE DATE: 11/9/90
MBTALS MDL (_g/kg) RBSHL't (mg/kg)
LEAD 2.50 25.3
J00124
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QUALITY ASSURANCE DATAHAZARDOUS SDB5TANCE LIST
JJMLYSIS NO. E6190BATCH NO. M331MATRIX: AQUEOUS
METAL AHOUHT OF SPIKE (ug) X SPIKE RECOVERY Z DUPLICATE RECOVERY
ALUMINUM 10000 91 91AHTIHONY 50 113 114
ARSENIC 50 105 101
BARIDM 1000 99 100
BERILLIUH 1000 101 101
CADMIOM 1000 93 93.
CUROMIOM 1000 102 102
COBALT 1000 99 99
'"WEB, 1000 96 97/
IttON 10000 91 91
LEAD 10000 89 90
MANGANESE 1000 98 98
MERCDRX 1.00 101 105
NICKEL 1000 97 97
SELENIUM 50 105! 105
THALLIUM 50 87 87
VAHADIUM 1000 100 100
ZINC 5000 88 88
100125
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QUALITY ASSURANCE DATA
HAZARDOUS SUBSTANCE LIST
BATCH NO: 331
MATRIX: AQUEOUS
METAL METHOD BLAH- (-8/L) AHODHT OF SPIKE (ug/L) X SPIKE RECOVER!
ALUHKUH ND 10000 96
ABTQIONY HD 50 119
AHSEHIC HD 50 105
BARIUM HD 1000 96
BERYLLIUM ND 1000 96
CADMIUM HD 1000 89
CHROMIUM HD 1000 98
COBALT HD 1000 96
COFPE. ND 1000 93
DON ND 10000 98
LEAD HD 10000 98
MANGANESE HD 1000 99
MERCURY HD 1.00 117
NICKEL HD 1000 95
SELENIUM HD 50 104
THALLIUM HD 50 99 •
VANADIUM HD 1000 97
ZHC HD 5000 96
100126
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