Thin ply composites: Experimental characterization and modeling

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Thin ply composites: Experimental characterization and modeling ICCM19 Montréal 2013 In partnership with North-TPT, FHNW, RUAG Technology, RUAG space, and Connova Robin Amacher, Joël Cugnoni , John Botsis Ecole polytechnique fédérale de Lausanne , Switzerland

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Thin ply composites: Experimental characterization and modeling. In partnership with North-TPT, FHNW, RUAG Technology, RUAG space, and Connova. ICCM19 Montréal 2013. Robin Amacher , Joël Cugnoni , John Botsis Ecole polytechnique fédérale de Lausanne , Switzerland. - PowerPoint PPT Presentation

Transcript of Thin ply composites: Experimental characterization and modeling

Page 1: Thin ply composites: Experimental  characterization and  modeling

Thin ply composites: Experimental characterization and modeling

ICCM19 Montréal 2013

In partnership with North-TPT, FHNW, RUAG Technology, RUAG space, and Connova

Robin Amacher, Joël Cugnoni, John Botsis

Ecole polytechnique fédérale de Lausanne , Switzerland

Page 2: Thin ply composites: Experimental  characterization and  modeling

o Advantages: Improved delamination resistance, higher onset of damage & ultimate failure Improved fatigue properties and in some case damage tolerance More design degrees of freedom = more optimal laminate Easier to design ply drops / small angle laminates / local reinforcements Can produce “homogeneous” laminates, no more dependency on stacking Can produce mixed “thin & thick” laminates for structures with large shell thickness variations. Thin ply materials are now commercially available

o Challenges:o Characterization and understanding of ply-thickness effect for a wide range of constituentso Efficient and accurate models for prediction of thin ply composite performanceo Flexible manufacturing (assembly of complex preform) & automation to reduce layup timeo Develop & validate efficient design method to account for the performance benefit without

blowing up the degree of complexity of the problem

Relevant literature (small subset): [1] S. Sihn, R.Y. Kim, K. Kawabe, S. Tsai, Experimental studies of thin-ply laminated composites, Composites Science and Technology, 67, 2007[2] M.R. Wisnom, B. Kahn, S.R. Hallet, Size effects in unnotched tensile strength of unidirectional and quasi-isotropic carbon/epoxy composites,

Composite Structures, 84, 2008[3] A. Arteiro, G. Catalanotti, J. Xavier, P.P. Camanho, Notched response of non-crimp fabric thin-ply laminates, Composites Science and

Technology, 79, 2013

Why Thin Ply composites?

Intro

Lamina level

Laminate level

Element level

Simulation

Design

Conclusion

Thin ply : below 125 g/m2, down to 15g/m2 today

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Objectives: Understand, characterize and model thin ply composites from the ply level to part level.

Experimental study of thin ply size effects • Constant specimen thickness • UD prepregs of varying ply thickness & number of

sub-laminate repetitions Material• North TPT Thin ply composites UD prepreg with

ATL production of complex laminates• Thick = 300 (2x150) g/m2 ~300 microns / ply• Intermediate = 100 g/m2 ~100 microns / ply• Thin = 30 g/m2 ~30 microns / ply• M40JB fiber / NTPT TP80ep (80°C epoxy resin)

from the same batches and production on the same machine the same week. Autoclave production, 55% fiber volume fraction

Objectives & Method

Intro

Lamina level

Laminate level

Element level

Simulation

Design

Conclusion

Page 4: Thin ply composites: Experimental  characterization and  modeling

Experimental characterization of Thin-ply size effects

Page 5: Thin ply composites: Experimental  characterization and  modeling

UD ply level properties

o Thin Ply : more uniform microstructure and improved 0° compressive strength

Compressive strength (ASTM D5467*)

Thick 300 g/m2

Intermediate 100g/m2

Thin 30g/m2

Intro

Lamina level

Laminate level

Element level

Simulation

Design

Conclusion

o Overall no change in intrinsic lamina properties when reducing ply thickness

o One exception: 0° compression

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Quasi isotropic laminate, tensileASTM D3039, constant thickness, sub-laminate scaling: [+45°/90°/-45°/0°]ns with n=1 for thick, n=3 for interm. and n=10 for thin ply.

Intro

Lamina level

Laminate level

Element level

Simulation

Design

Conclusion

Damage (Acoustic emission)

Appl

ied

stre

ss

Page 7: Thin ply composites: Experimental  characterization and  modeling

QISO tensile properties

Intro

Lamina level

Laminate level

Element level

Simulation

Design

Conclusion

Ultimate strength: +42%

[+45°/90°/-45°/0°]ns

n=1

n=3n=10& n=3

Onset of damage: +227%

Change of failure mode:• Thick: extensive

matrix cracking & delamination

• Thin: brittle rupture by fiber failure (max strain of fiber)

• Little effect of n

Page 8: Thin ply composites: Experimental  characterization and  modeling

Open Hole Compression

Intro

Lamina level

Checklist

Simulation

Design

Laminate level

Element level

+18%

Open Hole Compression [+45°/90°/-45°/0°]ns (ISO 14126 / ASTM D6484)

OHC

Str

engt

h [M

pa]

Page 9: Thin ply composites: Experimental  characterization and  modeling

Open Hole Tensile fatigue

o Lower static ultimate strength. No damage around hole means no stress concentration relief but better predictability (Wisnom & al)

-34%

+31%Thick plies 300g/m2, n=1 @12k cycles, 316MPa

Thin plies 30g/m2, n=10 @1M, 316MPa

[+45°/90°/-45°/0°]ns

Ruin = -10% stiffness

o Strong improvement in fatigue life (<20k vs >1M cycles)

Open Hole Tensile: static and fatigue (ASTM D5766 & D7615, R=0.1)

Intro

Lamina level

Simulation

Design

Conclusion

Laminate level

Element level

Page 10: Thin ply composites: Experimental  characterization and  modeling

Bolted joint bearing strength

o Strength improvement for as produced @ 20°C +18%o Strength improvement for Hot Wet @ 90°C +58%

Single lap bearing test, standard and Hot Wet condition (ASTM 5961), fastener type EN-6115Hot Wet cond. 95%RH/70°C, test 90°C

sbr_ult = 156 MPa

sbr_ult = 476 MPasbr_ult = 573 MPa

sbr_ult = 294 MPa

sbr_ult = 584 MPa

sbr_ult = 372 MPa

Thick Ply 300g/m2, n=2 Intermediate 100g/m2, n=5 Thin Ply 30g/m2, n=18

Hot Wet 90°C

Hot Wet 90°C

As Produced, 20°C

As produced, 20°C

Intro

Lamina level

Simulation

Design

Conclusion

Laminate level

Element level

[+45°/90°/-45°/0°]ns

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Low energy impact

o Transition of failure mode from delamination to fiber failure

o An optimal ply thickness can be found to achieve the smallest damage area

o Thin-Ply technology allows tailoring the material properties wrt impact induced damage

Intro

Lamina level

Summary

Simulation

Design

o Rectangular specimen clamped on the short sides; bending is dominant QI [0°/+45°/90°/-45°]ns, 300 x 140 x 2.4 mm Thick (300 g/m2) n=1, Intermediate (100g/m2) n=3, Thin (30g/m2) n=10

o Energy: 11.5 J & 18J

Back

side

THICK, n=1 INTERMEDIATE, n=3 THIN, n=10

delamination delamination &fiber failure

mostlyfiber failure

Laminate level

Element level

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Modeling of Thin-ply size effects

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Ply thickness effects:1. reduction of interlaminar shear

stresses at the free edges & delayed free edge delamination

2. Constrained intra laminar transverse cracks => apparent 90° and in-plane shear strength increase => in-situ ply strength model (*)

3. Matrix cracking induced delamination also delayed by constraining plies

4. Other mechanisms (bridging?, plasticity of matrix?)

Modeling thin-ply size effects

Intro

Lamina level

Laminate level

Element level

Simulation

Design

Conclusion

2D generalized plane strain or 3D continuum model

In-situ shear / normal strength (*) + coarse 3D modelOr high fidelity 3D continuum model + cohesive zone

High fidelity 3D continuum model + cohesive zone

(*) Camanho et al., Composites Part A, 37, 2006 Fracture mechanics : onset ~ 1/sqrt(t)

Page 14: Thin ply composites: Experimental  characterization and  modeling

Simulation of ‘thin ply’ effectso Goal: capture the transition in dominant failure mode in order to

understand and predict ply size effects with interacting damage modeso Hypotheses:

no change in intrinsic properties of ply and interface wrt ply thickness

First ply: 0° (symetry)

User material withfiber failure (subroutine)

UD mx. without fiber failure

Cohesive elements> lateral cracking

2nd ply: -45°3rd ply: 90°

Between the layers: cohesive surfaces => delamination

Simulation: force controlled(sigmoid ramp, quasi-static)

o High fidelity 3D modeling of quasi isotropic unnotched tensile test in Abaqus Explicit, [45°/90°/-45°/0°]ns laminate.

o All material properties coming from tests, no fitting parameters.

Intro

Lamina level

Conclusion

Design

Simulation

Laminate level

Element level

Cohesive elements=> Intralaminar matrix cracking

45°90°

-45°0°

User material withfiber failure (subroutine)

Symmetry BC

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Simulation of ‘thin ply’ effectso Damage models: cohesive interfaces between plies,

cohesive elements for transverse cracking, continuum damage model for fiber failure

o Mesh convergence study: 6 linear hex. element C3D8R per ply thickness, 0.5mm in plane elem. size, up to 650k elements, 2.1M dofs

o Mass scaling & time step convergence study: dt = ~5e-6 s, ~500’000 time steps

Intro

Lamina level

Conclusion

Design

Simulation

Laminate level

Element level

0

100

200

300

400

500

600

700

800

0 2 4 6 8

Stre

ngth

[MPa

]

# elements ply thickness

#element/ply & mass scaling target dt

1e-4_ultimate strength

1e-4_onset of damage

5e-5_ultimate strength

5e-5_onset of damage

1e-5_ultimate strength

1e-5_onset of damage

5e-6_ultimate strength

5e-6_onset of damage

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Thick ply (300 g/m2) QISO tensile

Intro

Lamina level

Conclusion

Design

Simulation

Laminate level

Element level

Delamination damage Intra laminar cracking(matrix failure) Fiber failure

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Thick ply (300 g/m2) QISO tensile

Damage sequence: o cracking of 90° ply, then cracking of 45° plies & delamination from edgeso Final failure after extensive delamination / damage of all off-axis plieso Ultimate strength: fiber failure in 0° plies with all other plies broken

Intro

Lamina level

Conclusion

Design

Simulation

Laminate level

Element level

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Intermediate ply (100 g/m2), n=3

Damage sequence: o cracking of 90° plies then outer 45° ply then final failure (localization of damage

starting from the free edges and fiber failure in 0° plies o Transverse normal and shear cracking delayed, Delamination nearly suppressed

Intro

Lamina level

Conclusion

Design

Simulation

Laminate level

Element level

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Simulation of ‘thin ply’ effects

o Good predictions for thick & intermediate ply thickness for both onset of damage and ultimate strength.

o High fidelity FE model can capture the change of damage mode sequence wrt ply thickness (with constant intrinsic properties)

o Coarse 3D FE Models (1 elem/ply) with in-situ strength (scaled by 1/sqrt(t)) provide comparable results, could be extended towards shell modeling (work in progress)

FE Analysis

Intermediate100 g/m2

Thick300 g/m2

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Towards part level modeling and design

Intro

Lamina level

Design

Model First ply failure 0° ply failure Experiment Damage Ult strengthCLT with damage 287 MPa 609 MPa Thick ply 300g/m2 248 MPa 595 MPa

Simulation

Conclusion

Laminate level

Element level

High fidelity 3D FE modeling

Shell models or CLT with in-situ

strength

Com

puta

tion

time

All damage modes with interactions

o Thin Ply composites : closer to classical laminate theory as no delamination!!Model First ply failure 0° ply failure Experiment Damage Ult strength

CLT with damage 287 MPa 609 MPa Thick ply 300g/m2 248 MPa 595 MPa CLT no damage 287 MPa 819 MPa Thin ply 30g/m2 821 Mpa 847 MPa

Separate damage models for transverse cracking and

delamination

Coarse 3D FE modeling with in-

situ strength

Damage models for transverse cracking

Delamination

Delamination follows intra laminar cracking(no complex interaction)

Ply thickness small enough to avoid delamination

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o Advantages: Improved delamination resistance, higher onset of damage & ultimate failure Improved fatigue properties and in some case damage tolerance More design degrees of freedom = more optimal laminate Easier to design ply drops / small angle laminates / local reinforcements Can produce “homogeneous” laminates, no more dependency on stacking Can produce mixed “thin & thick” laminates for structures with large shell thickness variations. Thin ply materials are now commercially available

o Challenges:o Characterization and understanding of ply-thickness effect for a wide range of constituentso Efficient and accurate models for prediction of thin ply composite performanceo Flexible manufacturing (assembly of complex preform) & automation to reduce layup timeo Develop & validate efficient design method to account for the performance benefit without

blowing up the degree of complexity of the problem

Why Thin Ply composites?

Intro

Lamina level

Laminate level

Element level

Simulation

Design

Conclusion

Thin ply : below 125 g/m2, down to 15g/m2 today

Page 22: Thin ply composites: Experimental  characterization and  modeling
Page 23: Thin ply composites: Experimental  characterization and  modeling