Thin layer chromatography in drug analysis - · PDF fileMariuszStolarczyk,...
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Thin Layer Chromatography in Drug Analysis Edited by tukasz Komsta Monika Waksmundzka-Hajnos Joseph Sherma CRC Press Taylor & Francis Group Boca Raton London NewYork CRC Press is an imprint of the Taylor & Francis Croup, an informa business
Transcript of Thin layer chromatography in drug analysis - · PDF fileMariuszStolarczyk,...
Thin Layer
Chromatographyin Drug Analysis
Edited by
tukasz Komsta
Monika Waksmundzka-HajnosJoseph Sherma
CRC PressTaylor&Francis GroupBoca Raton London NewYork
CRC Press is an imprint of the
Taylor & Francis Croup, an informa business
Contents
Preface xvii
Editors xi*
Contributors xxiii
PART I Theory of Thin Layer Chromatography in Context
of Pharmaceutical Analysis
Chapter 1 Overview of Drug Analysis and Structure of the Book 3
Lukasz Komsta, Monika Waksmundzka-Hajnos, and Joseph Sherma
Chapter 2 Chemistry of Drugs and Its Influence on Retention 7
Oliwia Szerkus and Michat J. Markuszewski
Chapter 3 Sorbents and Layers Used in Drug Analysis 23
Fred Rabel and Joseph Sherma
Chapter 4 Optimization of the Mobile Phase Composition 41
Miroslaw Hawryl and Anna Hawryt
Chapter 5 Chromatographic Analysis of Ionic Drugs 63
Monika Waksmundzka-Hajnos
Chapter 6 Ionic Liquid Additives to Mobile Phases 83
Roman Kaliszan and Michat Piotr Marszall
Chapter 7 Chromatographic Analysis of Chiral Drugs 97
Shuchi Dixit and Ravi Bhushan
Chapter 8 Chambers, Sample Application, and New Devices in the Chromatographyof Drugs
"
131
Beata Polak, Radostaw Gwarda, Ewelina Kopcial, and Tadeusz H. Dzido
Chapter 9 2D Planar Chromatography 147
Huba Kaldsz
xi
xii Contents
Chapter 10 Quantitative Detection of Drugs by Densitometry and Video Scanning 169
Bernd Spangenberg
Chapter 11 Statistical Evaluation and Validation of Quantitative Methods of Drug Analysis 187
Lukasz Komsta
Chapter 12 Detection and Identification in TLC Drug Analysis 193
Lukasz Ciesla and Iwona Kowalska
Chapter 13 TLC Determination of Drug Lipophilicity 225
Zivoslav Lj. Tesic and Dusanka M. Milojkovic-Opsenica
Chapter 14 Screening of Substandard and Fake Drugs in Underdeveloped Countries by TLC 247
Eliangiringa Kaale, Peter Risha, Thomas Layloff, and Joseph Sherma
PART II Planar Chromatography of Particular Drug Groups
Chapter 15 TLC of Antidepressants and Neuroleptics 267
Robert Skibinski
Chapter 16 TLC of Anxiolytics and Sedatives 279
Claudia Cimpoiu and Anamaria Hosu
Chapter 17 TLC of Morphine Analogs 323
Grzegorz Jozwiak
Chapter 18 TLC of Nonopioid Analgesics, Anti-Infiammatics, and Antimigraine Drugs 333
Arkadiusz Pomykalski
Chapter 19 TLC of Ergot Alkaloid Derivatives 351
Anna Petruczynik
Chapter 20 Thin-Layer Chromatography of Anesthetics 355
Maja M. Natic
Chapter 21 TLC of Psychostimulants 399
Joanna Drozd
Contents xiii
Chapter 22 TLC of Antiepileptics 437
Beata Paw
Chapter 23 TLC of Alzheimer's Disease Medicines 449
Lukasz Ciesla
Chapter 24 TLC of Antiparkinsonians 459
Sigrid Mennickent, Marta de Diego, Mario Vega, and Carmen Gloria Godoy
Chapter 25 Thin-Layer Chromatography of Cardiac Drugs 469
Rafat Pietras
Chapter 26 TLC of Antihypertensive and Antihypotensive Drugs 481
Danica Agbaba and Katarina Nikolic
Chapter 27 TLC of Beta-Blockers and Beta-Agonists 527
Anna Gumieniczek and Anna Berecka
Chapter 28 TLC of Antithrombotics 549
Marica Medic-Saric, Mirza Bojic, and Zeljko Debeljak
Chapter 29 TLC of Antihyperlipidemics 563
Lukasz Komsta
Chapter 30 TLC of Spasmolytics 569
Przemyslaw Talik and Jan Krzek
Chapter 31 TLC of Mucolytic, Antitussive, and Antiasthmatic Drugs 591
Radoslaw J. Ekiert and Jan Krzek
Chapter 32 TLC of Neuromuscular Blockers 605
Dusanka M. Milojkovic-Opsenica andMaja M. Natic
Chapter 33 TLC of Antiulcers 631
Tadeusz Inglot
Chapter 34 TLC of Antiemetic Drugs 637
Lukasz Komsta
xiv Contents
Chapter 35 TLC of Steroids and Analogs 641
Rada M. Baosic
Chapter 36 TLC of Drugs Used in Obesity and Sexual Dysfunction Treatment 691
Lukasz Komsta
Chapter 37 TLC ofProstaglandins 695
Mariusz Stolarczyk, Anna Apola, and Jan Krzek
Chapter 38 TLC of Diuretics 707
Urszula Hubicka, Anna Maslanka, and Jan Krzek
Chapter 39 TLC of Antidiabetics 739
Anna Gumieniczek andAnna Berecka
Chapter 40 TLC of Antihistamines 751
Danica Agbaba and Gordana Popovic
Chapter 41 TLC of Vitamins Including Nicotinic Acid Derivatives 773
Alina Pyka
Chapter 42 TLC of Antiseptics 811
Anna Apola, Mariusz Stolarczyk, and Jan Krzek
Chapter 43 TLC of Sulfonamides 819
Irena Choma and Wioleta Jesionek
Chapter 44 TLC of Quinolones 845
Dorota Kowalczuk
Chapter 45 Thin-Layer Chromatography of Tuberculostatic Drugs 865
Anamaria Hosu and Claudia Cimpoiu
Chapter 46 TLC ofAntifungal and Antiprotozoal Drugs 875
Zivoslav Lj. Tesic and Jelena D. Trifkovic
Chapter 47 TLC of P-Lactam Antibiotics 921
Monika Dabrowska and Malgorzata Starek
Contents xv
Chapter 48 TLC of Other Antibiotics 947
Malgorzata Starek and Monika Dabrowska
Chapter 49 Thin-Layer Chromatography of Antiviral Drugs 985
Anna Gumieniczek and Anna Berecka
Chapter 50 Thin-Layer Chromatography of Anticancer Drugs 995
Duygu Yeniceli
Chapter 51 Uncertainty Factors in the Enantioseparation of Chiral Drugs on Silica Gel
Layers 1009
Mieczystaw Sajewicz and Teresa Kowalska
Index 1017
