The Towers at Wildwood Atlanta, Georgia 30339 Phone (678 ... · Reporting Limit Result Client:...
Transcript of The Towers at Wildwood Atlanta, Georgia 30339 Phone (678 ... · Reporting Limit Result Client:...
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June 21, 2013 Mr. David Brownlee Acting Program Manager Response & Remediation Program Georgia Environmental Protection Division 2 Martin Luther King Jr. Dr., SE, Suite 1462 Atlanta, Georgia 30334
Subject: Second Annual Ground Water Monitoring Report for Compliance with the Environmental Covenant Former Dickies Industrial Services, Inc. (DISI) 2411 Sullivan Road, College Park, Fulton County, Georgia
I have enclosed two electronic versions of Transmittal of Electronic version of the Second Annual Ground Water Monitoring Report for Compliance with the Environmental Covenant Former Dickies Industrial Services, Inc. (DISI) 2411 Sullivan Road, College Park, Fulton County, Georgia as .pdf files on Compact Disc to accompany the hard copy report. This certification states that the electronic copy is complete, identical to the paper copy and virus free.
I, Holly H. Mason, on June 21, 2013 made a complete electronic copy of the
following document:
Transmittal of Electronic Version of the Second Annual Ground Water Monitoring Report for Compliance with the Environmental Covenant Former
Dickies Industrial Services, Inc. (DISI) 2411 Sullivan Road, College Park, Fulton County, Georgia
I then confirmed that the electronic copies did not contain a virus utilizing
Symantec antivirus software. You can contact me at 678.486.2700 with any questions or comments. Best regards,
Holly H. Mason CC: Joan B. Sasine, Esq. (via email) Tobin Clark (via email) Teri Fields (via email)
Environmental Resources Management The Towers at Wildwood 3200 Windy Hill Road SE, Suite 1500W Atlanta, Georgia 30339 Phone (678) 486-2700 Fax (678) 745-0103
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Letter of Transmittal
If enclosures are not as noted, kindly notify us at once.
Environmental Resources Management The Towers at Wildwood 3200 Windy Hill Road SE, Suite 1500W Atlanta, Georgia 30339 Phone (678) 486-2700 Fax (678) 745-0103
DATE: June 21, 2013 WO NUMBER: 0121103
To: Mr. David Brownlee Acting Program Manager Response & Remediation Program Georgia Environmental Protection Division 2 Martin Luther King Jr. Dr., SE, Suite 1462 Atlanta, Georgia 30334
ATTENTION: MR. DAVID BROWNLEE
WE ARE SENDING YOU:
Attached Under separate cover via:
Shop drawings Prints Plans Samples Specifications Copy of letter Change order (other) MSA
COPIES DATE NO. DESCRIPTION 1 6/21/13 Report Hard Copy
2 6/21/13 Report Electronic Copy
THESE ARE TRANSMITTED AS CHECKED BELOW
For approval Approved as submitted Resubmit ___ copies for approval For your use Approved as noted Submit ___ copies for distribution As requested Returned for corrections Returned ___ corrected prints For review and comment Prints returned after loan to us For bids due ___________________________ (other) ________________________
REMARKS: PLEASE SIGN ORIGNINAL AND SEND BACK ATTENTION TO DAVID DUNN.
Amy Griswold, E.I.T COPY TO:
SIGNED
cc:
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Environmental Resources Management (ERM)
3200 Windy Hill Rd., SE Suite 1500W Atlanta, GA 30339 (678) 486-2700 (404) 745-0103 (fax)
June 21, 2013 Mr. David Brownlee Acting Program Manager Response & Remediation Program Georgia Environmental Protection Division 2 Martin Luther King Jr. Dr., SE, Suite 1462 Atlanta, Georgia 30334
Subject: Second Annual Ground Water Monitoring Report for Compliance with the Environmental Covenant
Former Dickies Industrial Services, Inc. (DISI) 2411 Sullivan Road, College Park, Fulton County, Georgia Dear Mr. Brownlee: Environmental Resources Management, Inc. (ERM) is submitting this report on behalf of Dickies Industrial Services, Inc. (DISI) in accordance with the Environmental Covenant. Per the Environmental Covenant, DISI will sample the following 14 wells annually for five years: MW-1, MW-9, MW-10, MW-10A, MW-18D, MW-19, MW-20, MW-25, MW-28R, MW-29R, MW-37, MW-37A, MW-38, and MW-38A. Year 2013 is the second year of the five year monitoring period, and this letter is the second annual report to EPD under the Environmental Covenant. GROUND WATER SAMPLING The annual ground water sampling event was conducted on May 20-23, 2013. Ground water samples were collected from 13 of the 14 monitoring wells during the second annual sampling event. A ground water sample could not be collected from MW-28R due to residual injectant in the well. Ground water samples were collected utilizing low flow/low volume techniques in accordance with the SESDPROC-301-R2 sampling protocol. Temperature, specific conductance, pH, and turbidity were measured in the field as the ground water samples were collected. The ground water samples and associated trip blank were analyzed for VOCs by EPA Method 8260B. Results from the ground water sampling event are summarized in the attached Table 1. Sampling results were consistent with those reported in 2012 with the exception of tetrachloroethylene (PCE) concentrations at MW-10 and MW-10A. However, we believe the increase in PCE concentrations at MW-10 and MW-10A can be attributed to fluctuating ground water levels. Ground water sampling log forms and the laboratory report are also attached.
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June 21, 2013 Mr. Brownlee Page 2
Environmental Resources Management (ERM) If you have any questions or comments about this report, please contact us at
678-486-2700. Sincerely,
Amy Griswold, E.I.T. Jeffrey N. Bilkert Project Manager Principal Attachments: Table 1 – 2013 Ground Water Data Ground Water Sampling Logs Laboratory Reports cc: Joan B. Sasine, Esq. (via email) Tobin Clark (via email) Teri Fields (via email)
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Table 1Ground Water Analytical DataFormer Dickies Industrial Services, Inc.ug/L
PCE TCE 1,1-DCE trans-1,2-DCE cis-1,2-DCE VC 1,4-Dioxane
MW-1 5/22/2013 27,000 < 2,500 < 2,500 < 2,500 < 2,500 < 1,000 < 75,000MW-9 5/23/2013 < 5 < 5 < 5 < 5 < 5 < 2 < 150MW-10 5/23/2013 1,700 < 5 < 5 < 5 < 5 < 2 < 150
MW-10A 5/23/2013 1,300 99 < 5 < 5 260 < 2 < 150MW-18D 5/23/2013 < 5 < 5 < 5 < 5 < 5 < 2 < 150MW-19 5/21/2013 < 5 < 5 < 5 < 5 < 5 < 2 < 150MW-20 5/22/2013 < 5 50 < 5 < 5 180 29 < 150MW-25 5/21/2013 100 14 < 5 < 5 63 < 2 < 150MW-29/29R 5/22/2013 < 5 < 5 < 5 < 5 < 5 < 2 < 150MW-37 5/22/2013 < 5 < 5 < 5 < 5 < 5 < 2 < 150MW-37A 5/22/2013 < 5 < 5 < 5 < 5 310 7.6 < 150MW-38 5/21/2013 17 11 < 5 < 5 7.3 < 2 < 150MW-38A 5/21/2013 < 5 < 5 27 8.7 6500 32 < 150
Analysis Results (ug/L)Well ID Date Sampled
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May 31, 2013
Dear Order No:
RE:
Analytical Environmental Services, Inc. received samples on for the analyses presented in following report.
FAX:TEL:
15
No problems were encountered during the analyses. Additionally, all results for the associated
Quality Control samples were within EPA and/or AES established limits. Any discrepancies
associated with the analyses contained herein will be noted and submitted in the form of a
project Case Narrative.
AES’ certifications are as follows:
-NELAC/Florida Certification number E87582 for analysis of Environmental Water,
soil/hazardous waste, and Drinking Water Microbiology, effective 07/01/12-06/30/13.
-AIHA-LAP, LLC Laboratory ID: 100671 for Industrial Hygiene samples (Organics,
Inorganics), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental
Microbiology (Fungal) effective until 09/01/13.
These results relate only to the items tested. This report may only be reproduced in full.
If you have any questions regarding these test results, please feel free to call.
(770) 590-8383(770) 590-9164
Project Manager
1305L37
Amy GriswoldERM-Southeast3200 Windy Hill Rd., Suite 1500 WAtlanta GA 30339
Williamson Dickie
Mirzeta Kararic
5/24/2013 11:35:00 AM
Amy Griswold:
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31-May-13Date:Analytical Environmental Services, Inc
Client:
Case NarrativeWilliamson Dickie
ERM-Southeast
Lab ID:
Project:
1305L37
Volatile Organic Compounds Analysis by Method 8260B:
Due to sample matrix, samples 1305L37-009A and -014A required dilution during preparation and/or analysis resulting in
elevated reporting limits.
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1305L37-001
31-May-13Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDilution
FactorBatchIDUnitsQual
Reporting
LimitResult
Client:
Groundwater
5/21/2013 10:00:00 AM
MW-38A
Matrix:
Collection Date:
Client Sample ID:
Williamson Dickie
ERM-Southeast
Lab ID:
Project Name:
Analyst
(SW5030B)Volatile Organic Compounds by GC/MS SW8260B
1,4-Dioxane BRL 150 ug/L 176691 1 05/29/2013 15:46 NP
Vinyl chloride 32 2.0 ug/L 176691 1 05/29/2013 15:46 NP
1,1-Dichloroethene 27 5.0 ug/L 176691 1 05/29/2013 15:46 NP
trans-1,2-Dichloroethene 8.7 5.0 ug/L 176691 1 05/29/2013 15:46 NP
cis-1,2-Dichloroethene 6500 500 ug/L 176691 100 05/28/2013 18:50 NP
Trichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 15:46 NP
Tetrachloroethene BRL 5.0 ug/L 176691 1 05/29/2013 15:46 NP
Surr: 4-Bromofluorobenzene 85.3 64.6-123 %REC 176691 1 05/29/2013 15:46 NP
Surr: 4-Bromofluorobenzene 85.7 64.6-123 %REC 176691 100 05/28/2013 18:50 NP
Surr: Dibromofluoromethane 101 76.6-133 %REC 176691 100 05/28/2013 18:50 NP
Surr: Dibromofluoromethane 105 76.6-133 %REC 176691 1 05/29/2013 15:46 NP
Surr: Toluene-d8 97.6 77.8-120 %REC 176691 1 05/29/2013 15:46 NP
Surr: Toluene-d8 96.4 77.8-120 %REC 176691 100 05/28/2013 18:50 NP
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
NC Not confirmed
< Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit
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1305L37-002
31-May-13Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDilution
FactorBatchIDUnitsQual
Reporting
LimitResult
Client:
Groundwater
5/21/2013 10:45:00 AM
MW-38
Matrix:
Collection Date:
Client Sample ID:
Williamson Dickie
ERM-Southeast
Lab ID:
Project Name:
Analyst
(SW5030B)Volatile Organic Compounds by GC/MS SW8260B
1,4-Dioxane BRL 150 ug/L 176691 1 05/29/2013 11:39 NP
Vinyl chloride BRL 2.0 ug/L 176691 1 05/29/2013 11:39 NP
1,1-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 11:39 NP
trans-1,2-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 11:39 NP
cis-1,2-Dichloroethene 7.3 5.0 ug/L 176691 1 05/29/2013 11:39 NP
Trichloroethene 11 5.0 ug/L 176691 1 05/29/2013 11:39 NP
Tetrachloroethene 17 5.0 ug/L 176691 1 05/29/2013 11:39 NP
Surr: 4-Bromofluorobenzene 89.1 64.6-123 %REC 176691 1 05/29/2013 11:39 NP
Surr: Dibromofluoromethane 104 76.6-133 %REC 176691 1 05/29/2013 11:39 NP
Surr: Toluene-d8 98.4 77.8-120 %REC 176691 1 05/29/2013 11:39 NP
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
NC Not confirmed
< Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit
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1305L37-003
31-May-13Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDilution
FactorBatchIDUnitsQual
Reporting
LimitResult
Client:
Groundwater
5/21/2013 12:20:00 PM
MW-25
Matrix:
Collection Date:
Client Sample ID:
Williamson Dickie
ERM-Southeast
Lab ID:
Project Name:
Analyst
(SW5030B)Volatile Organic Compounds by GC/MS SW8260B
1,4-Dioxane BRL 150 ug/L 176691 1 05/29/2013 10:38 NP
Vinyl chloride BRL 2.0 ug/L 176691 1 05/29/2013 10:38 NP
1,1-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 10:38 NP
trans-1,2-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 10:38 NP
cis-1,2-Dichloroethene 63 5.0 ug/L 176691 1 05/29/2013 10:38 NP
Trichloroethene 14 5.0 ug/L 176691 1 05/29/2013 10:38 NP
Tetrachloroethene 100 5.0 ug/L 176691 1 05/29/2013 10:38 NP
Surr: 4-Bromofluorobenzene 88.7 64.6-123 %REC 176691 1 05/29/2013 10:38 NP
Surr: Dibromofluoromethane 101 76.6-133 %REC 176691 1 05/29/2013 10:38 NP
Surr: Toluene-d8 96.8 77.8-120 %REC 176691 1 05/29/2013 10:38 NP
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
NC Not confirmed
< Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit
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1305L37-004
31-May-13Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDilution
FactorBatchIDUnitsQual
Reporting
LimitResult
Client:
Groundwater
5/21/2013 1:50:00 PM
MW-19
Matrix:
Collection Date:
Client Sample ID:
Williamson Dickie
ERM-Southeast
Lab ID:
Project Name:
Analyst
(SW5030B)Volatile Organic Compounds by GC/MS SW8260B
1,4-Dioxane BRL 150 ug/L 176691 1 05/29/2013 11:09 NP
Vinyl chloride BRL 2.0 ug/L 176691 1 05/29/2013 11:09 NP
1,1-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 11:09 NP
trans-1,2-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 11:09 NP
cis-1,2-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 11:09 NP
Trichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 11:09 NP
Tetrachloroethene BRL 5.0 ug/L 176691 1 05/29/2013 11:09 NP
Surr: 4-Bromofluorobenzene 89.6 64.6-123 %REC 176691 1 05/29/2013 11:09 NP
Surr: Dibromofluoromethane 102 76.6-133 %REC 176691 1 05/29/2013 11:09 NP
Surr: Toluene-d8 96.1 77.8-120 %REC 176691 1 05/29/2013 11:09 NP
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
NC Not confirmed
< Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit
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1305L37-005
31-May-13Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDilution
FactorBatchIDUnitsQual
Reporting
LimitResult
Client:
Groundwater
5/22/2013 10:10:00 AM
MW-20
Matrix:
Collection Date:
Client Sample ID:
Williamson Dickie
ERM-Southeast
Lab ID:
Project Name:
Analyst
(SW5030B)Volatile Organic Compounds by GC/MS SW8260B
1,4-Dioxane BRL 150 ug/L 176691 1 05/29/2013 14:44 NP
Vinyl chloride 29 2.0 ug/L 176691 1 05/29/2013 14:44 NP
1,1-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 14:44 NP
trans-1,2-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 14:44 NP
cis-1,2-Dichloroethene 180 5.0 ug/L 176691 1 05/29/2013 14:44 NP
Trichloroethene 50 5.0 ug/L 176691 1 05/29/2013 14:44 NP
Tetrachloroethene BRL 5.0 ug/L 176691 1 05/29/2013 14:44 NP
Surr: 4-Bromofluorobenzene 85.4 64.6-123 %REC 176691 1 05/29/2013 14:44 NP
Surr: Dibromofluoromethane 104 76.6-133 %REC 176691 1 05/29/2013 14:44 NP
Surr: Toluene-d8 97.7 77.8-120 %REC 176691 1 05/29/2013 14:44 NP
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
NC Not confirmed
< Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit
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1305L37-006
31-May-13Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDilution
FactorBatchIDUnitsQual
Reporting
LimitResult
Client:
Groundwater
5/22/2013 12:15:00 PM
MW-29R
Matrix:
Collection Date:
Client Sample ID:
Williamson Dickie
ERM-Southeast
Lab ID:
Project Name:
Analyst
(SW5030B)Volatile Organic Compounds by GC/MS SW8260B
1,4-Dioxane BRL 150 ug/L 176691 1 05/29/2013 12:41 NP
Vinyl chloride BRL 2.0 ug/L 176691 1 05/29/2013 12:41 NP
1,1-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 12:41 NP
trans-1,2-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 12:41 NP
cis-1,2-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 12:41 NP
Trichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 12:41 NP
Tetrachloroethene BRL 5.0 ug/L 176691 1 05/29/2013 12:41 NP
Surr: 4-Bromofluorobenzene 87.8 64.6-123 %REC 176691 1 05/29/2013 12:41 NP
Surr: Dibromofluoromethane 104 76.6-133 %REC 176691 1 05/29/2013 12:41 NP
Surr: Toluene-d8 98.6 77.8-120 %REC 176691 1 05/29/2013 12:41 NP
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
NC Not confirmed
< Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit
Page 10 of 24
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1305L37-007
31-May-13Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDilution
FactorBatchIDUnitsQual
Reporting
LimitResult
Client:
Groundwater
5/22/2013 1:20:00 PM
MW-37A
Matrix:
Collection Date:
Client Sample ID:
Williamson Dickie
ERM-Southeast
Lab ID:
Project Name:
Analyst
(SW5030B)Volatile Organic Compounds by GC/MS SW8260B
1,4-Dioxane BRL 150 ug/L 176691 1 05/29/2013 13:12 NP
Vinyl chloride 7.6 2.0 ug/L 176691 1 05/29/2013 13:12 NP
1,1-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 13:12 NP
trans-1,2-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 13:12 NP
cis-1,2-Dichloroethene 310 50 ug/L 176691 10 05/29/2013 17:19 NP
Trichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 13:12 NP
Tetrachloroethene BRL 5.0 ug/L 176691 1 05/29/2013 13:12 NP
Surr: 4-Bromofluorobenzene 84.8 64.6-123 %REC 176691 1 05/29/2013 13:12 NP
Surr: 4-Bromofluorobenzene 81.3 64.6-123 %REC 176691 10 05/29/2013 17:19 NP
Surr: Dibromofluoromethane 104 76.6-133 %REC 176691 1 05/29/2013 13:12 NP
Surr: Dibromofluoromethane 105 76.6-133 %REC 176691 10 05/29/2013 17:19 NP
Surr: Toluene-d8 96.1 77.8-120 %REC 176691 1 05/29/2013 13:12 NP
Surr: Toluene-d8 96.2 77.8-120 %REC 176691 10 05/29/2013 17:19 NP
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
NC Not confirmed
< Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit
Page 11 of 24
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1305L37-008
31-May-13Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDilution
FactorBatchIDUnitsQual
Reporting
LimitResult
Client:
Groundwater
5/22/2013 2:55:00 PM
MW-37
Matrix:
Collection Date:
Client Sample ID:
Williamson Dickie
ERM-Southeast
Lab ID:
Project Name:
Analyst
(SW5030B)Volatile Organic Compounds by GC/MS SW8260B
1,4-Dioxane BRL 150 ug/L 176691 1 05/29/2013 13:43 NP
Vinyl chloride BRL 2.0 ug/L 176691 1 05/29/2013 13:43 NP
1,1-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 13:43 NP
trans-1,2-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 13:43 NP
cis-1,2-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 13:43 NP
Trichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 13:43 NP
Tetrachloroethene BRL 5.0 ug/L 176691 1 05/29/2013 13:43 NP
Surr: 4-Bromofluorobenzene 83 64.6-123 %REC 176691 1 05/29/2013 13:43 NP
Surr: Dibromofluoromethane 102 76.6-133 %REC 176691 1 05/29/2013 13:43 NP
Surr: Toluene-d8 96.8 77.8-120 %REC 176691 1 05/29/2013 13:43 NP
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
NC Not confirmed
< Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit
Page 12 of 24
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1305L37-009
31-May-13Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDilution
FactorBatchIDUnitsQual
Reporting
LimitResult
Client:
Groundwater
5/22/2013 5:00:00 PM
MW-1
Matrix:
Collection Date:
Client Sample ID:
Williamson Dickie
ERM-Southeast
Lab ID:
Project Name:
Analyst
(SW5030B)Volatile Organic Compounds by GC/MS SW8260B
1,4-Dioxane BRL 75000 ug/L 176691 500 05/28/2013 17:30 NP
Vinyl chloride BRL 1000 ug/L 176691 500 05/28/2013 17:30 NP
1,1-Dichloroethene BRL 2500 ug/L 176691 500 05/28/2013 17:30 NP
trans-1,2-Dichloroethene BRL 2500 ug/L 176691 500 05/28/2013 17:30 NP
cis-1,2-Dichloroethene BRL 2500 ug/L 176691 500 05/28/2013 17:30 NP
Trichloroethene BRL 2500 ug/L 176691 500 05/28/2013 17:30 NP
Tetrachloroethene 27000 2500 ug/L 176691 500 05/28/2013 17:30 NP
Surr: 4-Bromofluorobenzene 87.7 64.6-123 %REC 176691 500 05/28/2013 17:30 NP
Surr: Dibromofluoromethane 103 76.6-133 %REC 176691 500 05/28/2013 17:30 NP
Surr: Toluene-d8 98.3 77.8-120 %REC 176691 500 05/28/2013 17:30 NP
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
NC Not confirmed
< Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit
Page 13 of 24
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1305L37-010
31-May-13Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDilution
FactorBatchIDUnitsQual
Reporting
LimitResult
Client:
Groundwater
5/23/2013 10:05:00 AM
MW-18
Matrix:
Collection Date:
Client Sample ID:
Williamson Dickie
ERM-Southeast
Lab ID:
Project Name:
Analyst
(SW5030B)Volatile Organic Compounds by GC/MS SW8260B
1,4-Dioxane BRL 150 ug/L 176691 1 05/29/2013 15:15 NP
Vinyl chloride BRL 2.0 ug/L 176691 1 05/29/2013 15:15 NP
1,1-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 15:15 NP
trans-1,2-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 15:15 NP
cis-1,2-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 15:15 NP
Trichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 15:15 NP
Tetrachloroethene BRL 5.0 ug/L 176691 1 05/29/2013 15:15 NP
Surr: 4-Bromofluorobenzene 87.8 64.6-123 %REC 176691 1 05/29/2013 15:15 NP
Surr: Dibromofluoromethane 105 76.6-133 %REC 176691 1 05/29/2013 15:15 NP
Surr: Toluene-d8 98.1 77.8-120 %REC 176691 1 05/29/2013 15:15 NP
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
NC Not confirmed
< Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit
Page 14 of 24
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1305L37-011
31-May-13Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDilution
FactorBatchIDUnitsQual
Reporting
LimitResult
Client:
Groundwater
5/23/2013 10:50:00 AM
MW-10
Matrix:
Collection Date:
Client Sample ID:
Williamson Dickie
ERM-Southeast
Lab ID:
Project Name:
Analyst
(SW5030B)Volatile Organic Compounds by GC/MS SW8260B
1,4-Dioxane BRL 150 ug/L 176691 1 05/29/2013 16:48 NP
Vinyl chloride BRL 2.0 ug/L 176691 1 05/29/2013 16:48 NP
1,1-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 16:48 NP
trans-1,2-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 16:48 NP
cis-1,2-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 16:48 NP
Trichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 16:48 NP
Tetrachloroethene 1700 50 ug/L 176691 10 05/28/2013 20:24 NP
Surr: 4-Bromofluorobenzene 87 64.6-123 %REC 176691 10 05/28/2013 20:24 NP
Surr: 4-Bromofluorobenzene 88.4 64.6-123 %REC 176691 1 05/29/2013 16:48 NP
Surr: Dibromofluoromethane 102 76.6-133 %REC 176691 10 05/28/2013 20:24 NP
Surr: Dibromofluoromethane 104 76.6-133 %REC 176691 1 05/29/2013 16:48 NP
Surr: Toluene-d8 97.9 77.8-120 %REC 176691 10 05/28/2013 20:24 NP
Surr: Toluene-d8 102 77.8-120 %REC 176691 1 05/29/2013 16:48 NP
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
NC Not confirmed
< Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit
Page 15 of 24
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1305L37-012
31-May-13Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDilution
FactorBatchIDUnitsQual
Reporting
LimitResult
Client:
Groundwater
5/23/2013 12:05:00 PM
MW-10A
Matrix:
Collection Date:
Client Sample ID:
Williamson Dickie
ERM-Southeast
Lab ID:
Project Name:
Analyst
(SW5030B)Volatile Organic Compounds by GC/MS SW8260B
1,4-Dioxane BRL 150 ug/L 176691 1 05/29/2013 16:17 NP
Vinyl chloride BRL 2.0 ug/L 176691 1 05/29/2013 16:17 NP
1,1-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 16:17 NP
trans-1,2-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 16:17 NP
cis-1,2-Dichloroethene 260 50 ug/L 176691 10 05/28/2013 20:54 NP
Trichloroethene 99 5.0 ug/L 176691 1 05/29/2013 16:17 NP
Tetrachloroethene 1300 50 ug/L 176691 10 05/28/2013 20:54 NP
Surr: 4-Bromofluorobenzene 85.4 64.6-123 %REC 176691 1 05/29/2013 16:17 NP
Surr: 4-Bromofluorobenzene 88.4 64.6-123 %REC 176691 10 05/28/2013 20:54 NP
Surr: Dibromofluoromethane 102 76.6-133 %REC 176691 10 05/28/2013 20:54 NP
Surr: Dibromofluoromethane 105 76.6-133 %REC 176691 1 05/29/2013 16:17 NP
Surr: Toluene-d8 97.4 77.8-120 %REC 176691 1 05/29/2013 16:17 NP
Surr: Toluene-d8 99.8 77.8-120 %REC 176691 10 05/28/2013 20:54 NP
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
NC Not confirmed
< Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit
Page 16 of 24
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1305L37-013
31-May-13Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDilution
FactorBatchIDUnitsQual
Reporting
LimitResult
Client:
Groundwater
5/23/2013 1:15:00 PM
MW-9
Matrix:
Collection Date:
Client Sample ID:
Williamson Dickie
ERM-Southeast
Lab ID:
Project Name:
Analyst
(SW5030B)Volatile Organic Compounds by GC/MS SW8260B
1,4-Dioxane BRL 150 ug/L 176691 1 05/29/2013 14:14 NP
Vinyl chloride BRL 2.0 ug/L 176691 1 05/29/2013 14:14 NP
1,1-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 14:14 NP
trans-1,2-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 14:14 NP
cis-1,2-Dichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 14:14 NP
Trichloroethene BRL 5.0 ug/L 176691 1 05/29/2013 14:14 NP
Tetrachloroethene BRL 5.0 ug/L 176691 1 05/29/2013 14:14 NP
Surr: 4-Bromofluorobenzene 85.9 64.6-123 %REC 176691 1 05/29/2013 14:14 NP
Surr: Dibromofluoromethane 101 76.6-133 %REC 176691 1 05/29/2013 14:14 NP
Surr: Toluene-d8 99.9 77.8-120 %REC 176691 1 05/29/2013 14:14 NP
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
NC Not confirmed
< Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit
Page 17 of 24
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1305L37-014
31-May-13Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDilution
FactorBatchIDUnitsQual
Reporting
LimitResult
Client:
Groundwater
5/22/2013 11:59:00 PM
DUP-01
Matrix:
Collection Date:
Client Sample ID:
Williamson Dickie
ERM-Southeast
Lab ID:
Project Name:
Analyst
(SW5030B)Volatile Organic Compounds by GC/MS SW8260B
1,4-Dioxane BRL 75000 ug/L 176694 500 05/28/2013 14:40 NP
Vinyl chloride BRL 1000 ug/L 176694 500 05/28/2013 14:40 NP
1,1-Dichloroethene BRL 2500 ug/L 176694 500 05/28/2013 14:40 NP
trans-1,2-Dichloroethene BRL 2500 ug/L 176694 500 05/28/2013 14:40 NP
cis-1,2-Dichloroethene BRL 2500 ug/L 176694 500 05/28/2013 14:40 NP
Trichloroethene BRL 2500 ug/L 176694 500 05/28/2013 14:40 NP
Tetrachloroethene 25000 2500 ug/L 176694 500 05/28/2013 14:40 NP
Surr: 4-Bromofluorobenzene 83.7 64.6-123 %REC 176694 500 05/28/2013 14:40 NP
Surr: Dibromofluoromethane 113 76.6-133 %REC 176694 500 05/28/2013 14:40 NP
Surr: Toluene-d8 99 77.8-120 %REC 176694 500 05/28/2013 14:40 NP
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
NC Not confirmed
< Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit
Page 18 of 24
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1305L37-015
31-May-13Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDilution
FactorBatchIDUnitsQual
Reporting
LimitResult
Client:
Aqueous
5/21/2013 8:00:00 AM
TRIP BLANK
Matrix:
Collection Date:
Client Sample ID:
Williamson Dickie
ERM-Southeast
Lab ID:
Project Name:
Analyst
(SW5030B)Volatile Organic Compounds by GC/MS SW8260B
1,4-Dioxane BRL 150 ug/L 176694 1 05/28/2013 15:08 NP
Vinyl chloride BRL 2.0 ug/L 176694 1 05/28/2013 15:08 NP
1,1-Dichloroethene BRL 5.0 ug/L 176694 1 05/28/2013 15:08 NP
trans-1,2-Dichloroethene BRL 5.0 ug/L 176694 1 05/28/2013 15:08 NP
cis-1,2-Dichloroethene BRL 5.0 ug/L 176694 1 05/28/2013 15:08 NP
Trichloroethene BRL 5.0 ug/L 176694 1 05/28/2013 15:08 NP
Tetrachloroethene BRL 5.0 ug/L 176694 1 05/28/2013 15:08 NP
Surr: 4-Bromofluorobenzene 87.3 64.6-123 %REC 176694 1 05/28/2013 15:08 NP
Surr: Dibromofluoromethane 113 76.6-133 %REC 176694 1 05/28/2013 15:08 NP
Surr: Toluene-d8 101 77.8-120 %REC 176694 1 05/28/2013 15:08 NP
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
NC Not confirmed
< Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limit
Page 19 of 24
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Page 20 of 24
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31-May-13Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORT
Williamson Dickie
1305L37
ERM-Southeast
176691
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType: BatchID: Analysis Date: Seq No:TestCode: 176691MBLK 05/28/2013Volatile Organic Compounds by GC/MS SW8260B
Units: Prep Date:Sample ID: Client ID: Run No:ug/L 05/28/2013 244785MB-176691
5127747
1,1-Dichloroethene 5.0BRL 00 0 0 0 0 0 0
1,4-Dioxane 150BRL 00 0 0 0 0 0 0
cis-1,2-Dichloroethene 5.0BRL 00 0 0 0 0 0 0
Tetrachloroethene 5.0BRL 00 0 0 0 0 0 0
trans-1,2-Dichloroethene 5.0BRL 00 0 0 0 0 0 0
Trichloroethene 5.0BRL 00 0 0 0 0 0 0
Vinyl chloride 2.0BRL 00 0 0 0 0 0 0
Surr: 4-Bromofluorobenzene 046.90 050.00 0 93.8 64.6 123 0 0
Surr: Dibromofluoromethane 050.61 050.00 0 101 76.6 133 0 0
Surr: Toluene-d8 048.64 050.00 0 97.3 77.8 120 0 0
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType: BatchID: Analysis Date: Seq No:TestCode: 176691LCS 05/28/2013Volatile Organic Compounds by GC/MS SW8260B
Units: Prep Date:Sample ID: Client ID: Run No:ug/L 05/28/2013 244785LCS-176691
5127746
1,1-Dichloroethene 5.055.77 050.00 0 112 61.1 142 0 0
Trichloroethene 5.051.03 050.00 0 102 70 135 0 0
Surr: 4-Bromofluorobenzene 047.49 050.00 0 95.0 64.6 123 0 0
Surr: Dibromofluoromethane 049.78 050.00 0 99.6 76.6 133 0 0
Surr: Toluene-d8 048.47 050.00 0 96.9 77.8 120 0 0
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType: BatchID: Analysis Date: Seq No:TestCode: 176691MS 05/28/2013Volatile Organic Compounds by GC/MS SW8260B
Units: Prep Date:Sample ID: Client ID: Run No:ug/L 05/28/2013 2447851305L71-003AMS
5127749
1,1-Dichloroethene 5.069.20 050.00 0 138 60 168 0 0
Trichloroethene 5.060.17 050.00 0 120 71.1 154 0 0
Surr: 4-Bromofluorobenzene 048.59 050.00 0 97.2 64.6 123 0 0
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit
Page 21 of 24
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31-May-13Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORT
Williamson Dickie
1305L37
ERM-Southeast
176691
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType: BatchID: Analysis Date: Seq No:TestCode: 176691MS 05/28/2013Volatile Organic Compounds by GC/MS SW8260B
Units: Prep Date:Sample ID: Client ID: Run No:ug/L 05/28/2013 2447851305L71-003AMS
5127749
Surr: Dibromofluoromethane 051.52 050.00 0 103 76.6 133 0 0
Surr: Toluene-d8 049.80 050.00 0 99.6 77.8 120 0 0
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType: BatchID: Analysis Date: Seq No:TestCode: 176691MSD 05/28/2013Volatile Organic Compounds by GC/MS SW8260B
Units: Prep Date:Sample ID: Client ID: Run No:ug/L 05/28/2013 2447851305L71-003AMSD
5127750
1,1-Dichloroethene 5.066.16 18.650.00 0 132 60 168 69.20 4.49
Trichloroethene 5.058.46 2050.00 0 117 71.1 154 60.17 2.88
Surr: 4-Bromofluorobenzene 047.26 050.00 0 94.5 64.6 123 48.59 0
Surr: Dibromofluoromethane 050.92 050.00 0 102 76.6 133 51.52 0
Surr: Toluene-d8 049.21 050.00 0 98.4 77.8 120 49.80 0
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit
Page 22 of 24
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31-May-13Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORT
Williamson Dickie
1305L37
ERM-Southeast
176694
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType: BatchID: Analysis Date: Seq No:TestCode: 176694MBLK 05/28/2013Volatile Organic Compounds by GC/MS SW8260B
Units: Prep Date:Sample ID: Client ID: Run No:ug/L 05/28/2013 244791MB-176694
5126827
1,1-Dichloroethene 5.0BRL 00 0 0 0 0 0 0
1,4-Dioxane 150BRL 00 0 0 0 0 0 0
cis-1,2-Dichloroethene 5.0BRL 00 0 0 0 0 0 0
Tetrachloroethene 5.0BRL 00 0 0 0 0 0 0
trans-1,2-Dichloroethene 5.0BRL 00 0 0 0 0 0 0
Trichloroethene 5.0BRL 00 0 0 0 0 0 0
Vinyl chloride 2.0BRL 00 0 0 0 0 0 0
Surr: 4-Bromofluorobenzene 044.15 050.00 0 88.3 64.6 123 0 0
Surr: Dibromofluoromethane 055.62 050.00 0 111 76.6 133 0 0
Surr: Toluene-d8 049.22 050.00 0 98.4 77.8 120 0 0
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType: BatchID: Analysis Date: Seq No:TestCode: 176694LCS 05/28/2013Volatile Organic Compounds by GC/MS SW8260B
Units: Prep Date:Sample ID: Client ID: Run No:ug/L 05/28/2013 244791LCS-176694
5126825
1,1-Dichloroethene 5.058.25 050.00 0 116 61.1 142 0 0
Trichloroethene 5.049.12 050.00 0 98.2 70 135 0 0
Surr: 4-Bromofluorobenzene 051.22 050.00 0 102 64.6 123 0 0
Surr: Dibromofluoromethane 055.35 050.00 0 111 76.6 133 0 0
Surr: Toluene-d8 051.18 050.00 0 102 77.8 120 0 0
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType: BatchID: Analysis Date: Seq No:TestCode: 176694MS 05/28/2013Volatile Organic Compounds by GC/MS SW8260B
INFLUENT Units: Prep Date:Sample ID: Client ID: Run No:ug/L 05/28/2013 2447911305K84-001AMS
5126830
1,1-Dichloroethene 50000683400 0500000 0 137 60 168 0 0
Trichloroethene 50000554700 0500000 0 111 71.1 154 0 0
Surr: 4-Bromofluorobenzene 0523000 0500000 0 105 64.6 123 0 0
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit
Page 23 of 24
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31-May-13Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORT
Williamson Dickie
1305L37
ERM-Southeast
176694
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType: BatchID: Analysis Date: Seq No:TestCode: 176694MS 05/28/2013Volatile Organic Compounds by GC/MS SW8260B
INFLUENT Units: Prep Date:Sample ID: Client ID: Run No:ug/L 05/28/2013 2447911305K84-001AMS
5126830
Surr: Dibromofluoromethane 0564000 0500000 0 113 76.6 133 0 0
Surr: Toluene-d8 0525600 0500000 0 105 77.8 120 0 0
RPT Limit QualAnalyte Result SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType: BatchID: Analysis Date: Seq No:TestCode: 176694MSD 05/28/2013Volatile Organic Compounds by GC/MS SW8260B
INFLUENT Units: Prep Date:Sample ID: Client ID: Run No:ug/L 05/28/2013 2447911305K84-001AMSD
5126831
1,1-Dichloroethene 50000637300 18.6500000 0 127 60 168 683400 6.98
Trichloroethene 50000534700 20500000 0 107 71.1 154 554700 3.67
Surr: 4-Bromofluorobenzene 0516600 0500000 0 103 64.6 123 523000 0
Surr: Dibromofluoromethane 0564100 0500000 0 113 76.6 133 564000 0
Surr: Toluene-d8 0530100 0500000 0 106 77.8 120 525600 0
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit
Page 24 of 24