TFA Gold Etchant (diluted 9:1)
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Transcript of TFA Gold Etchant (diluted 9:1)
TFA Gold Etchant (diluted 9:1)
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Low limitHigh limit
y = +24.3100x1 -11.9000
a=0.801686,
b=14.9982
y = +25.8800x1 -0.700000
a=0.172626,
b=3.22954
Etch time (sec.)
Etc
h de
pth
(Å
)
Au etch rate of 10x diluted TFA etchant
24-26 Å / sec.Conditions: 2 mL concentrated TFA in 18 mL of DI H2O. Room temp. Clean room. Sample was agitated continuously by hand. Rinsed in DI H2O afterwards. Profilometry done at CHANL.
Performed 12.05.09 – Dmitry
RIE etching (@ SMiF)Fe = 0 Å / sec. Nb = 9.25 - 15 Å / sec. Ge = 726 – 900 Å / sec. Conditions: 100 W, CF4 = 40 sccm, O2 = 4 sccm.
Performed 06.02.09 – Alex and/or Liang
AuNb
Fe
Ge (15mm*15mm)6
3
5
2
4
1
Each section is about3mm*7mm
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0 40 80 120
20W, 80 m device25 W, 80 m device30 W, 80 m device
Ashing time (sec)
Am
oun
t re
mov
ed
(m
)
S1813 removal via ashing (CHANL plasma asher)
Plasma Asher (CHANL)S 1813 polymer. Non-linear.
Conditions: 1 sccm O2 flow, varied power. Etching profile of square device
Performed 12.03.09 – Dmitry
10 mM HCl
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y = +11.8533x1 -22.1665, max dev:15.8999, r2=0.986500
a=0.980487,
b=26.8518
Time (sec)
Etc
h d
epth
(Å
)
Etch Rate of Pure Sputtered Fe (on Si) via 10 mM HCl
11-13 Å / sec.Conditions: 1mL of 3N (=3M) HCl diluted in ~ 300 mL of DI H2O. Continuously stirred with a magnetic stir bar. Washed with running DI H2O for 5+ min. Room temp., CHANL clean room. Profilometry done at CHANL. Mask – S1813.
Performed 02.03.10 – Dmitry
ICP – RIE Fe etch (SMiF)6-7 Å / sec.Conditions: SMiF Trion Minilock II. 300 W ICP, 125 W RIE. BCl3 = 5±1 sccm, Cl2 = 45±1 sccm. Manual runs to make sure flow is stabilized. Sample: Si substrate, Ti/Fe 60/1000 Å. Profilometry done at SMiF. Mask – S1813.
Performed 11.02.11 – Dmitry
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y = +6.60000x1 -88.0000
a=0.264575,
b=14.8492
300 W ICP125 W RIEBCl
3 - 5 sccm
Cl2 - 45 sccm
Etch time (sec)
Etc
h de
pth
(Å
)
Fe etching [ICP-RIE, Trion Minilock II]
Note: although the rate was not measured, the etch does go through the Ti wetting layer and Si substrate, albeit at 500 W ICP.